#------------------------------------------------------------------------------ #$Date: 2017-07-25 12:40:22 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199162 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/21/2242192.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242192 _cell_angle_alpha 90.000 _cell_angle_beta 100.405 _cell_angle_gamma 90.000 _cell_length_a 8.7203 _cell_length_b 20.1237 _cell_length_c 19.5261 _exptl_crystal_F_000 1440.00 _reflns_d_resolution_high 0.7312 _cod_data_source_file nk2238Isup2.hkl _cod_data_source_block I _shelx_title ' JTM444_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 396.64 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12957.29 14467.24 331.08 o 2 0 0 13543.05 14029.83 273.03 o 3 0 0 1633.44 2073.07 59.45 o 4 0 0 4087.36 3748.34 129.90 o 5 0 0 29348.75 28762.41 635.46 o 6 0 0 22532.31 22952.72 610.98 o 7 0 0 3422.09 3389.68 123.21 o 8 0 0 16.69 48.88 36.67 o 9 0 0 260.73 265.05 78.73 o 10 0 0 897.08 1139.11 124.46 o 11 0 0 2367.79 2433.94 172.55 o 1 1 0 5024.58 4969.05 81.23 o 2 1 0 19793.40 19742.81 291.76 o 3 1 0 8750.35 8523.13 128.98 o 4 1 0 32.74 41.76 9.13 o 5 1 0 624.40 599.72 24.25 o 6 1 0 0.04 -5.46 9.71 o 7 1 0 96.17 87.92 15.63 o 8 1 0 516.58 453.54 39.31 o 9 1 0 2079.85 2122.23 101.65 o 10 1 0 1379.57 1483.93 96.93 o 11 1 0 287.46 240.66 50.55 o 0 2 0 435.29 296.71 25.50 o 1 2 0 625.90 802.16 20.58 o 2 2 0 6085.80 6077.21 105.63 o 3 2 0 9282.09 10271.62 148.93 o 4 2 0 35.38 15.67 7.40 o 5 2 0 3759.34 3898.95 76.00 o 6 2 0 7446.11 7587.58 137.02 o 7 2 0 2115.29 2057.50 58.15 o 8 2 0 3191.95 3152.30 98.24 o 9 2 0 500.11 460.23 59.20 o 10 2 0 427.50 346.93 53.83 o 11 2 0 1670.78 1737.03 107.56 o 1 3 0 4171.11 4262.11 71.35 o 2 3 0 2898.87 2544.27 53.44 o 3 3 0 24495.95 25458.97 361.82 o 4 3 0 10286.83 10297.77 147.35 o 5 3 0 337.28 293.99 22.06 o 6 3 0 9.35 3.26 11.07 o 7 3 0 1284.20 1278.66 41.58 o 8 3 0 3011.51 3245.74 101.67 o 9 3 0 5254.78 5099.65 168.15 o 10 3 0 2087.39 1903.33 102.05 o 11 3 0 95.57 69.64 54.18 o 0 4 0 5741.07 6225.81 119.12 o 1 4 0 3487.36 3583.25 58.41 o 2 4 0 2740.50 2543.76 52.21 o 3 4 0 308.85 308.75 18.49 o 4 4 0 1898.93 2140.75 63.47 o 5 4 0 1725.78 1651.14 47.32 o 6 4 0 4201.17 4200.61 84.97 o 7 4 0 394.65 418.25 31.89 o 8 4 0 300.11 212.85 30.90 o 9 4 0 259.33 245.89 29.00 o 10 4 0 450.42 575.42 65.44 o 11 4 0 396.09 343.59 67.37 o 1 5 0 5182.71 5048.74 79.31 o 2 5 0 13213.65 13771.75 204.58 o 3 5 0 614.32 595.65 25.72 o 4 5 0 384.97 430.27 23.10 o 5 5 0 476.26 521.83 26.55 o 6 5 0 123.21 100.55 16.26 o 7 5 0 1327.52 1386.31 42.55 o 8 5 0 35.39 61.13 23.27 o 9 5 0 98.18 73.16 23.58 o 10 5 0 694.95 852.51 82.70 o 11 5 0 500.68 497.67 70.77 o 0 6 0 13752.90 15728.00 285.48 o 1 6 0 4583.68 4663.66 79.95 o 2 6 0 401.91 398.49 19.06 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9315.90 139.81 o 3 9 0 14322.46 13849.66 199.15 o 4 9 0 9292.65 9055.94 164.38 o 5 9 0 4184.17 4051.39 89.74 o 6 9 0 61.27 83.73 18.85 o 7 9 0 2436.33 2412.40 68.88 o 8 9 0 3976.56 3970.22 136.17 o 9 9 0 3652.81 3677.76 118.97 o 10 9 0 1414.57 1315.27 96.26 o 11 9 0 624.87 857.95 263.05 o 0 10 0 12.07 82.06 18.27 o 1 10 0 15236.47 15219.42 206.14 o 2 10 0 9116.19 10182.19 153.15 o 3 10 0 16.26 25.98 12.71 o 4 10 0 1939.21 1819.51 56.40 o 5 10 0 7401.78 7203.77 137.48 o 6 10 0 6413.74 6829.67 136.32 o 7 10 0 8712.12 8263.87 165.32 o 8 10 0 2691.95 2644.47 93.24 o 9 10 0 7.86 18.28 28.00 o 10 10 0 1389.65 1473.13 78.15 o 1 11 0 334.04 356.92 22.45 o 2 11 0 3892.51 4215.74 79.39 o 3 11 0 7.65 9.84 12.41 o 4 11 0 976.34 1076.97 44.73 o 5 11 0 80.31 108.59 20.41 o 6 11 0 277.11 266.02 28.29 o 7 11 0 1317.68 1327.55 65.78 o 8 11 0 298.02 348.36 41.30 o 9 11 0 2.34 44.89 27.50 o 10 11 0 391.76 388.65 78.95 o 0 12 0 10150.14 9555.11 201.77 o 1 12 0 4646.74 5052.16 90.26 o 2 12 0 4574.75 4539.94 89.03 o 3 12 0 1804.27 1659.43 50.77 o 4 12 0 5118.63 5428.76 123.44 o 5 12 0 2230.80 2395.94 69.23 o 6 12 0 610.62 556.93 40.26 o 7 12 0 646.40 618.84 40.73 o 8 12 0 34.63 19.97 25.77 o 9 12 0 594.26 664.57 62.12 o 10 12 0 183.10 135.91 37.99 o 1 13 0 105.92 124.05 18.50 o 2 13 0 1360.40 1199.85 53.81 o 3 13 0 2326.96 2321.22 63.55 o 4 13 0 1645.23 1631.77 60.41 o 5 13 0 2065.79 2354.12 72.94 o 6 13 0 7.65 -7.97 18.01 o 7 13 0 277.74 211.85 29.47 o 8 13 0 1824.95 1931.53 78.74 o 9 13 0 1778.04 1780.81 88.78 o 10 13 0 1419.36 1397.05 177.26 o 0 14 0 2566.45 2469.99 108.61 o 1 14 0 2411.52 2470.04 62.97 o 2 14 0 5147.81 4729.94 100.91 o 3 14 0 497.02 493.37 40.00 o 4 14 0 259.18 363.31 35.25 o 5 14 0 5920.70 5982.05 133.65 o 6 14 0 2366.10 2250.13 75.39 o 7 14 0 741.28 760.38 49.74 o 8 14 0 167.42 189.62 36.30 o 9 14 0 13.63 -31.34 31.34 o 10 14 0 198.50 196.67 113.08 o 1 15 0 1085.39 1077.79 46.89 o 2 15 0 35.38 40.99 18.92 o 3 15 0 16.12 22.92 20.91 o 4 15 0 760.26 851.28 54.94 o 5 15 0 167.31 113.15 27.36 o 6 15 0 31.36 9.40 22.29 o 7 15 0 179.63 123.10 39.68 o 8 15 0 5.85 23.64 27.13 o 9 15 0 0.94 57.42 35.76 o 0 16 0 30795.11 31021.75 696.15 o 1 16 0 10978.28 10052.63 215.52 o 2 16 0 302.95 262.89 35.39 o 3 16 0 442.65 425.48 46.20 o 4 16 0 3494.36 3247.56 102.55 o 5 16 0 5317.09 5304.91 134.31 o 6 16 0 4678.71 4824.40 158.54 o 7 16 0 1900.09 1859.44 87.41 o 8 16 0 163.50 203.08 42.18 o 9 16 0 267.11 246.70 48.27 o 1 17 0 6122.95 5916.69 149.37 o 2 17 0 5117.09 4980.43 133.72 o 3 17 0 2084.79 2328.92 100.63 o 4 17 0 3758.81 3546.12 129.56 o 5 17 0 2525.63 2726.21 123.85 o 6 17 0 60.98 30.80 29.92 o 7 17 0 404.84 358.26 47.66 o 8 17 0 3134.90 3196.31 162.16 o 0 18 0 1424.61 1497.07 115.23 o 1 18 0 187.56 128.11 29.77 o 2 18 0 656.34 706.19 55.72 o 3 18 0 847.76 818.22 71.34 o 4 18 0 0.52 6.02 29.78 o 5 18 0 46.52 52.02 41.72 o 6 18 0 79.18 78.42 35.67 o 7 18 0 591.02 363.52 64.32 o 8 18 0 430.74 449.17 72.73 o 1 19 0 3699.28 3629.62 123.35 o 2 19 0 4372.46 4408.90 152.49 o 3 19 0 6215.78 5826.45 183.07 o 4 19 0 8492.10 8691.45 243.11 o 5 19 0 48.90 -0.12 46.98 o 6 19 0 234.77 176.58 43.10 o 7 19 0 1838.51 1902.45 111.41 o 8 19 0 1486.41 1538.45 146.05 o 0 20 0 531.59 621.25 93.75 o 1 20 0 2586.34 2716.42 115.93 o 2 20 0 964.51 901.25 77.02 o 3 20 0 1.45 -13.22 31.71 o 4 20 0 948.28 968.59 79.14 o 5 20 0 1227.37 1176.96 86.89 o 6 20 0 1144.00 1014.68 82.50 o 7 20 0 740.20 596.11 64.38 o 1 21 0 158.94 237.19 48.00 o 2 21 0 31.45 48.29 44.67 o 3 21 0 74.08 17.15 36.51 o 4 21 0 4.72 13.01 33.47 o 5 21 0 0.42 2.52 33.14 o 6 21 0 0.00 8.31 37.11 o 7 21 0 10.21 -0.94 41.01 o 0 22 0 323.58 278.91 74.81 o 1 22 0 19.17 17.00 40.26 o 2 22 0 286.75 223.96 57.87 o 3 22 0 89.85 31.56 54.10 o 4 22 0 7.41 39.51 37.40 o 5 22 0 399.31 380.66 60.78 o 6 22 0 429.65 431.31 60.67 o 7 22 0 710.07 824.26 197.28 o 1 23 0 1129.76 1328.68 131.44 o 2 23 0 4856.82 4755.87 217.26 o 3 23 0 3111.49 3346.10 178.37 o 4 23 0 1868.32 1856.16 122.65 o 5 23 0 165.87 157.24 51.75 o 6 23 0 63.85 28.16 54.57 o 0 24 0 490.56 583.03 103.71 o 1 24 0 535.23 564.03 77.94 o 2 24 0 573.78 490.61 84.51 o 3 24 0 187.77 114.02 59.33 o 4 24 0 400.85 422.93 71.86 o 5 24 0 400.27 321.03 95.30 o 1 25 0 0.50 20.09 44.00 o 2 25 0 73.82 -0.26 67.91 o 3 25 0 52.99 112.31 56.50 o 4 25 0 623.16 652.03 112.08 o 0 26 0 3197.90 3170.56 583.03 o 1 26 0 3804.46 4035.40 231.93 o 2 26 0 983.51 951.97 113.34 o 3 26 0 7.04 -63.94 63.94 o 1 27 0 153.87 109.07 55.67 o -11 1 1 25.04 32.95 38.03 o -10 1 1 1444.19 1416.15 101.49 o -9 1 1 2095.91 2186.25 101.26 o -8 1 1 1352.80 1401.65 74.47 o -7 1 1 2149.86 2133.08 85.83 o -6 1 1 60.92 14.49 12.29 o -5 1 1 5504.43 5616.48 95.43 o -4 1 1 6457.06 6432.86 89.31 o -3 1 1 7628.97 8727.68 121.09 o -2 1 1 2114.27 1794.39 44.13 o -1 1 1 17559.54 18520.18 302.03 o 1 1 1 34046.59 35527.00 537.54 o 2 1 1 436.49 313.03 17.26 o 3 1 1 879.59 626.31 22.66 o 4 1 1 7276.46 7498.16 116.56 o 5 1 1 11626.98 12026.50 188.39 o 6 1 1 301.05 359.17 29.45 o 7 1 1 1127.15 1080.19 46.33 o 8 1 1 174.16 150.12 23.60 o 9 1 1 1297.81 1409.83 75.29 o 10 1 1 2383.25 2322.93 120.52 o 11 1 1 278.97 237.12 52.39 o -11 2 1 1515.82 1150.53 93.47 o -10 2 1 1378.95 1413.44 88.17 o -9 2 1 68.33 62.22 31.96 o -8 2 1 4.27 1.87 24.79 o -7 2 1 4016.56 4168.83 98.12 o -6 2 1 9975.91 9474.79 174.02 o -5 2 1 15754.01 15964.83 210.83 o -4 2 1 12002.21 12618.83 166.91 o -3 2 1 6371.54 6797.42 106.02 o -2 2 1 33487.75 36554.09 479.68 o -1 2 1 24667.61 25473.95 367.99 o 0 2 1 42200.54 43803.60 815.26 o 1 2 1 1026.94 1086.50 24.93 o 2 2 1 52947.47 53288.98 769.35 o 3 2 1 20.92 10.07 9.35 o 4 2 1 26099.17 27038.63 387.43 o 5 2 1 9992.08 9592.80 195.66 o 6 2 1 10750.70 10368.76 192.14 o 7 2 1 1054.05 1187.98 50.03 o 8 2 1 714.62 627.97 38.63 o 9 2 1 314.17 231.46 32.46 o 10 2 1 2451.85 2466.70 117.24 o 11 2 1 1673.77 1773.57 110.22 o -11 3 1 1320.71 1459.32 131.27 o -10 3 1 1730.45 1728.73 106.76 o -9 3 1 1401.03 1610.27 123.03 o -8 3 1 1020.17 1009.39 67.73 o -7 3 1 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1003.15 993.33 36.67 o 5 4 1 2052.86 1885.13 50.36 o 6 4 1 2922.78 2976.58 86.26 o 7 4 1 5232.63 5093.33 122.72 o 8 4 1 2162.97 2189.21 71.12 o 9 4 1 2.04 39.63 23.41 o 10 4 1 1175.85 1189.38 89.17 o 11 4 1 715.41 680.86 80.43 o -11 5 1 367.42 251.22 56.73 o -10 5 1 2696.83 2906.51 126.54 o -9 5 1 5694.40 5746.35 181.61 o -8 5 1 4924.65 4868.90 136.57 o -7 5 1 5089.63 5155.28 120.78 o -6 5 1 380.24 382.29 31.88 o -5 5 1 7402.45 7764.77 148.90 o -4 5 1 15407.23 15380.76 204.75 o -3 5 1 38126.00 39110.75 547.08 o -2 5 1 34494.60 35063.18 470.26 o -1 5 1 25881.40 26319.33 353.76 o 0 5 1 7850.24 8412.07 112.79 o 1 5 1 13257.02 14256.41 199.62 o 2 5 1 21570.11 21701.43 286.25 o 3 5 1 36616.18 36488.70 516.12 o 4 5 1 14129.50 13814.46 204.93 o 5 5 1 1599.33 1690.68 47.30 o 6 5 1 334.41 309.66 28.73 o 7 5 1 7982.01 7812.69 160.73 o 8 5 1 7558.42 7245.72 163.01 o 9 5 1 3886.54 4017.23 127.28 o 10 5 1 1784.96 1927.54 108.23 o 11 5 1 477.59 329.89 72.76 o -11 6 1 220.44 111.78 46.63 o -10 6 1 306.07 199.75 48.27 o -9 6 1 74.73 76.69 34.41 o -8 6 1 42.33 4.23 18.81 o -7 6 1 1276.04 1355.62 55.25 o -6 6 1 1352.30 1368.55 53.91 o -5 6 1 1310.63 1258.80 37.12 o -4 6 1 295.65 319.94 17.65 o -3 6 1 748.63 928.09 41.78 o -2 6 1 25.60 90.28 11.83 o -1 6 1 3624.66 3963.28 67.20 o 0 6 1 2089.94 2112.15 39.10 o 1 6 1 6085.33 6261.73 90.08 o 2 6 1 841.77 668.12 22.62 o 3 6 1 2.45 -8.98 8.98 o 4 6 1 498.00 535.99 29.27 o 5 6 1 2567.73 2613.01 67.30 o 6 6 1 1908.81 1923.31 59.17 o 7 6 1 11.56 24.41 16.30 o 8 6 1 50.34 4.13 15.76 o 9 6 1 145.54 134.28 36.98 o 10 6 1 123.59 58.55 28.02 o 11 6 1 188.10 91.84 60.19 o -11 7 1 196.29 188.47 56.43 o -10 7 1 338.33 343.62 55.46 o -9 7 1 1638.74 1537.24 67.84 o -8 7 1 439.21 360.57 53.40 o -7 7 1 128.03 150.00 25.61 o -6 7 1 9.12 1.43 8.86 o -5 7 1 278.99 320.71 22.13 o -4 7 1 4194.85 4360.48 76.40 o -3 7 1 24648.88 25343.35 337.68 o -2 7 1 6295.87 6721.11 106.72 o -1 7 1 2583.57 2565.61 50.45 o 0 7 1 63.83 116.24 11.87 o 1 7 1 1697.63 1599.35 34.66 o 2 7 1 10914.00 10935.60 150.94 o 3 7 1 6230.27 5961.29 93.26 o 4 7 1 3867.95 3747.47 100.34 o 5 7 1 31.06 47.09 15.70 o 6 7 1 84.30 79.65 19.19 o 7 7 1 789.29 816.46 44.94 o 8 7 1 2042.30 2162.01 72.23 o 9 7 1 2154.47 2113.99 90.61 o 10 7 1 598.42 535.97 51.15 o 11 7 1 40.14 55.84 68.83 o -11 8 1 1780.08 1971.88 193.64 o -10 8 1 1168.64 1104.24 90.94 o -9 8 1 0.04 10.48 22.62 o -8 8 1 3173.72 3359.81 108.54 o -7 8 1 4445.12 4732.51 119.21 o -6 8 1 1855.29 1839.54 48.01 o -5 8 1 1473.03 1479.27 55.25 o -4 8 1 1764.53 1953.89 60.65 o -3 8 1 118.06 83.63 13.20 o -2 8 1 85.35 72.58 13.00 o -1 8 1 12117.39 11433.13 169.02 o 0 8 1 2517.07 2493.51 47.49 o 1 8 1 5519.37 5453.96 84.58 o 2 8 1 1517.91 1534.85 37.89 o 3 8 1 3.72 2.46 9.26 o 4 8 1 4.61 -2.53 11.41 o 5 8 1 1657.23 1653.39 77.23 o 6 8 1 3156.58 3217.72 83.91 o 7 8 1 7633.97 7366.27 158.74 o 8 8 1 2873.55 2865.10 87.66 o 9 8 1 77.33 76.59 30.22 o 10 8 1 881.15 868.04 66.62 o 11 8 1 1820.93 1547.68 315.17 o -11 9 1 0.21 51.33 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