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Information card for entry 2242437
Preview
| Coordinates | 2242437.cif |
|---|---|
| Structure factors | 2242437.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis(tri-2-pyridylamine)iron(II) bis(perchlorate) |
|---|---|
| Formula | C30 H24 Cl2 Fe N8 O8 |
| Calculated formula | C30 H24 Cl1.998 Fe N8 O7.992 |
| Title of publication | Redetermination of the crystal structure of bis(tri-2-pyridylamine)iron(II) bis(perchlorate), and a new refinement of the isotypic nickel(II) analogue: treatment of the perchlorate anion disorder |
| Authors of publication | Setifi, Zouaoui; Setifi, Fatima; Dege, Necmi; El Ati, Rafika; Glidewell, Christopher |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2018 |
| Journal volume | 74 |
| Journal issue | 5 |
| Pages of publication | 668 - 672 |
| a | 8.3251 ± 0.0007 Å |
| b | 17.4731 ± 0.0011 Å |
| c | 11.0495 ± 0.0009 Å |
| α | 90° |
| β | 98.716 ± 0.007° |
| γ | 90° |
| Cell volume | 1588.8 ± 0.2 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0918 |
| Residual factor for significantly intense reflections | 0.0492 |
| Weighted residual factors for significantly intense reflections | 0.1 |
| Weighted residual factors for all reflections included in the refinement | 0.1142 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.947 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 207543 (current) | 2018-04-30 | cif/ hkl/ Adding structures of 2242437, 2242438 via cif-deposit CGI script. |
2242437.cif 2242437.hkl |
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Users of the data should acknowledge the original authors of the
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