#------------------------------------------------------------------------------
#$Date: 2019-01-16 05:21:35 +0200 (Wed, 16 Jan 2019) $
#$Revision: 213105 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/24/28/2242807.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2242807
loop_
_publ_author_name
'Murthy, T. N. Sanjeeva'
'Atio\(glu, Zeliha'
'Akkurt, Mehmet'
'Veeraiah, M. K.'
'Quah, Ching Kheng'
'Chidan Kumar, C. S.'
'Siddaraju, B. P.'
_publ_section_title
;
 Crystal structure and Hirshfeld surface analysis of
 (<i>E</i>)-3-(2-chlorophenyl)-1-(2,5-dichlorothiophen-3-yl)prop-2-en-1-one
;
_journal_coeditor_code           QM2131
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              124
_journal_page_last               128
_journal_paper_doi               10.1107/S2056989018018066
_journal_volume                  75
_journal_year                    2019
_chemical_formula_iupac          'C13 H7 Cl3 O S'
_chemical_formula_moiety         'C13 H7 Cl3 O S'
_chemical_formula_sum            'C13 H7 Cl3 O S'
_chemical_formula_weight         317.60
_chemical_name_systematic
(<i>E</i>)-3-(2-chlorophenyl)-1-(2,5-dichlorothiophen-3-yl)prop-2-en-1-one
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/1
_cell_angle_alpha                90
_cell_angle_beta                 96.998(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   3.9017(6)
_cell_length_b                   22.038(3)
_cell_length_c                   15.127(2)
_cell_measurement_reflns_used    2207
_cell_measurement_temperature    294(2)
_cell_measurement_theta_max      23.29
_cell_measurement_theta_min      2.71
_cell_volume                     1291.0(3)
_computing_cell_refinement
;
SAINT (Bruker, 2007)
;
_computing_data_collection
;
APEX2 (Bruker, 2007)
;
_computing_data_reduction
;
SAINT (Bruker, 2007)
;
_computing_molecular_graphics
;
ORTEP-3 for Windows (Farrugia, 2012)
;
_computing_publication_material
;
PLATON (Spek, 2009)
;
_computing_structure_refinement
;
SHELXL2014 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS97 (Sheldrick, 2008)
;
_diffrn_ambient_temperature      294(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker APEXII CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0393
_diffrn_reflns_av_unetI/netI     0.0369
_diffrn_reflns_limit_h_max       4
_diffrn_reflns_limit_h_min       -4
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            10683
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.598
_diffrn_reflns_theta_min         1.641
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.853
_exptl_absorpt_correction_T_max  0.953
_exptl_absorpt_correction_T_min  0.907
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(SADABS; Sheldrick, 2007)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.634
_exptl_crystal_description       needle
_exptl_crystal_F_000             640
_exptl_crystal_size_max          0.555
_exptl_crystal_size_mid          0.095
_exptl_crystal_size_min          0.056
_refine_diff_density_max         0.298
_refine_diff_density_min         -0.320
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.082
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     163
_refine_ls_number_reflns         2669
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.082
_refine_ls_R_factor_all          0.0570
_refine_ls_R_factor_gt           0.0382
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0397P)^2^+0.3125P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0896
_refine_ls_wR_factor_ref         0.0990
_reflns_number_gt                1977
_reflns_number_total             2669
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            qm2131sup1.cif
_cod_data_source_block           I
_cod_database_code               2242807
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.649
_shelx_estimated_absorpt_t_max   0.954
_shelx_hkl_file
;
  -1   0   0 331.743 11.2566   1
   1   0   0 334.463 11.3041   1
   1   0   0 338.910 11.3158   2
   1   0   0 322.828 10.8291   3
   2   0   0 340.481 13.3158   1
   2   0   0 342.769 13.3217   2
  -2   0   0 351.396 13.3041   1
  -3   0   0 163.293 8.93591   1
   3   0   0 153.750 8.83845   2
   3   0   0 142.072 8.40898   1
   4   0   0 -0.7436 2.15624   2
  -4   0   0 -1.0062 2.11277   1
   0   1   0 -0.5580 0.03823   2
   1  -1   0 302.316 10.4078   1
   1  -1   0 315.411 10.0810   3
   1  -1   0 304.395 10.6637   2
  -1  -1   0 314.545 10.8389   1
   1   1   0 290.654 10.2697   3
  -1   1   0 309.482 10.4096   1
   1   1   0 308.426 10.5303   2
   1   1   0 324.489 10.8740   1
   2  -1   0 143.208 6.52910   3
   2  -1   0 154.295 7.52467   2
  -2  -1   0 143.519 7.40831   1
   2  -1   0 143.715 7.14704   1
   2   1   0 159.331 7.52243   2
   2   1   0 148.982 7.56444   1
  -2   1   0 156.774 7.28224   1
   3  -1   0 0.68923 1.39316   2
   3  -1   0 1.44784 1.37185   1
  -3  -1   0 0.75212 1.78050   1
   3  -1   0 -0.2814 1.15044   3
   3   1   0 -0.6463 1.29371   1
   3   1   0 1.92959 1.63979   2
  -3   1   0 0.89499 1.42348   1
   4  -1   0 5.11681 2.56946   2
  -4  -1   0 6.56860 3.23188   1
  -4   1   0 8.91483 3.00768   1
   4   1   0 1.84699 2.47921   2
   0   2   0 409.689 12.1202   2
   1  -2   0 1901.55 54.9612   3
   1  -2   0 1888.16 55.7700   2
  -1  -2   0 1891.79 56.0243   1
   1  -2   0 1904.56 55.1654   1
  -1   2   0 1857.96 55.0914   1
   1   2   0 1938.40 56.0901   1
   1   2   0 1890.91 55.4360   2
   2  -2   0 139.051 6.44844   3
  -2  -2   0 145.703 7.55958   1
   2  -2   0 143.081 7.38613   2
   2  -2   0 161.609 7.20296   1
   2   2   0 147.368 7.24318   2
  -2   2   0 159.478 7.14561   1
   2   2   0 141.093 7.57466   1
   3  -2   0 79.3861 5.27725   3
   3  -2   0 72.8985 5.52302   1
  -3  -2   0 73.8072 6.06787   1
   3  -2   0 75.6342 7.37183   2
   3   2   0 75.6140 5.97583   2
  -3   2   0 79.0276 5.66565   1
   3   2   0 73.5070 7.26469   1
   4  -2   0 0.31157 1.90795   2
  -4  -2   0 -1.3277 2.25002   1
   4   2   0 1.85591 2.49394   2
   4   2   0 -1.9097 1.43279   1
  -4   2   0 -0.2540 1.74485   1
   0   3   0 -0.5671 0.35407   2
   0   3   0 -0.9015 0.20856   1
  -1  -3   0 9482.18 279.582   1
   1  -3   0 9999.99 281.685   3
   1  -3   0 9955.08 278.284   1
  -1   3   0 9748.30 278.988   1
   1   3   0 9819.38 278.739   2
   2  -3   0 1.20645 0.89773   3
   2  -3   0 -0.3286 0.86274   2
  -2  -3   0 1.74094 1.24773   1
   2  -3   0 -0.3774 0.59347   1
  -2   3   0 -0.2011 0.70285   1
   2   3   0 -0.7441 0.84535   2
   2   3   0 0.26671 1.13948   1
   3  -3   0 22.2065 3.69267   1
  -3  -3   0 33.3572 4.90112   1
   3  -3   0 25.8370 4.42133   2
   3  -3   0 31.3632 3.79996   3
   3   3   0 33.3644 4.66211   2
  -3   3   0 23.3713 3.63283   1
   3   3   0 31.7734 4.95924   1
  -4  -3   0 67.5020 8.02747   1
   4  -3   0 77.0428 8.73478   2
   4   3   0 58.2625 7.42907   1
   4   3   0 72.9847 8.09485   2
  -4   3   0 84.1931 7.92517   1
   0   4   0 1404.50 41.7483   2
   0   4   0 1483.05 41.6950   1
   1  -4   0 2941.92 81.6494   1
   1  -4   0 2993.84 82.0745   3
  -1   4   0 2944.52 81.6489   1
   1   4   0 2406.81 83.0892   1
   1   4   0 2960.76 82.4595   2
   2  -4   0 36.4551 4.09169   2
   2  -4   0 37.3582 2.83945   3
  -2  -4   0 40.9954 4.51270   1
   2   4   0 37.9245 3.91481   2
   2   4   0 31.7816 4.05095   1
  -2   4   0 42.6396 3.06806   1
   3  -4   0 5.42434 1.73538   3
  -3  -4   0 6.96291 2.52181   1
   3  -4   0 7.79061 2.61448   2
  -3   4   0 9.43519 2.37756   1
   3   4   0 2.85283 2.23505   1
   3   4   0 10.3583 2.73670   2
  -4  -4   0 1.27114 2.20276   1
   4  -4   0 1.39790 2.35726   2
   4   4   0 -1.5334 1.82245   1
  -4   4   0 3.96317 2.25684   1
   4   4   0 2.29792 2.41667   2
   0  -5   0 -1.0563 0.49475   1
   0   5   0 -2.7959 0.63681   2
   0   5   0 -1.6364 0.41782   1
   1  -5   0 98.7150 3.92305   3
   1   5   0 90.3794 4.92659   1
   1   5   0 93.7489 4.16050   2
  -1   5   0 86.7210 3.26033   1
  -2  -5   0 90.3092 6.01927   1
   2  -5   0 90.6177 4.68853   3
   2  -5   0 87.0844 5.64211   2
   2   5   0 97.0706 5.42002   2
   2   5   0 86.2113 5.95503   1
  -2   5   0 82.9697 4.49792   1
   3  -5   0 7.43686 2.04631   3
  -3  -5   0 10.9631 3.01678   1
   3  -5   0 6.23312 2.48559   2
   3   5   0 7.64967 2.79548   1
   3   5   0 2.69755 2.07177   2
  -3   5   0 6.22654 1.98484   1
   4  -5   0 3.16606 2.78616   2
  -4  -5   0 4.56626 3.01109   1
   4   5   0 4.95165 3.07298   2
   4   5   0 1.04949 2.15898   1
   0  -6   0 411.722 12.9142   1
   0   6   0 419.800 12.9479   1
   0   6   0 404.460 13.0698   2
   1  -6   0 108.643 4.51315   3
   1  -6   0 109.550 5.27794   2
   1   6   0 110.632 5.71835   1
  -1   6   0 111.010 3.62499   1
   1   6   0 112.427 4.76711   2
  -2  -6   0 1282.05 42.0860   1
   2  -6   0 1347.52 39.6692   3
   2  -6   0 1281.88 41.4388   2
  -2   6   0 1285.94 41.5985   2
  -2   6   0 1281.77 39.1446   1
   2   6   0 1329.23 40.8158   2
   2   6   0 1343.30 42.4878   1
  -3  -6   0 7.65506 3.00585   1
   3  -6   0 4.69253 1.70410   3
   3  -6   0 10.2215 2.81728   2
   3   6   0 3.68882 2.37356   1
   3   6   0 9.05421 2.75729   2
  -3   6   0 5.90708 1.93762   1
   4  -6   0 6.23905 3.27044   2
  -4  -6   0 10.2458 3.87887   1
   4   6   0 5.23634 3.07896   1
   4   6   0 8.62911 3.34092   2
  -4   6   0 12.7888 4.19060   2
   0  -7   0 -0.9772 0.39716   1
   0   7   0 -0.3663 0.53076   1
   0   7   0 0.22800 0.92882   2
   1  -7   0 629.023 20.8487   2
   1  -7   0 641.709 19.8368   3
   1   7   0 642.430 21.4139   1
   1   7   0 642.325 20.0483   2
   2  -7   0 23.9666 2.71179   3
   2  -7   0 22.9791 3.43937   2
   2   7   0 22.8119 3.02408   2
  -2   7   0 15.8236 1.94588   1
  -2   7   0 29.4683 4.04112   2
   3  -7   0 26.7822 4.43547   2
  -3  -7   0 28.8923 5.10365   1
  -3   7   0 33.7419 5.18508   2
   3   7   0 25.9831 4.70581   1
   3   7   0 30.8392 4.50277   2
  -3   7   0 29.6760 3.56222   1
   4  -7   0 0.68299 2.19722   2
  -4  -7   0 -0.8633 2.77206   1
  -4   7   0 0.23002 1.91615   2
   4   7   0 2.51390 2.63397   2
   4   7   0 -0.1668 2.02047   1
   0  -8   0 81.7664 3.74784   1
   0   8   0 80.9144 3.70912   1
   0   8   0 79.9690 3.98943   2
  -1  -8   0 786.319 25.9764   1
   1  -8   0 773.921 25.4178   2
   1   8   0 801.763 26.0721   1
   1   8   0 825.968 24.6550   2
  -1   8   0 780.702 25.5378   2
  -2  -8   0 2.08514 1.79328   1
   2  -8   0 -0.3893 0.69396   3
   2  -8   0 2.26823 1.27087   2
   2   8   0 3.55682 1.35762   2
  -2   8   0 -0.2175 0.65636   1
   2   8   0 -2.0544 1.35667   1
  -2   8   0 -0.5251 0.81100   2
  -3  -8   0 76.0728 8.04692   1
   3  -8   0 71.7589 7.45512   2
   3   8   0 69.7517 5.64021   2
   3   8   0 68.8853 7.72934   1
  -3   8   0 84.5793 8.12227   2
   4  -8   0 3.96089 2.70558   2
  -4  -8   0 9.32839 3.80307   1
   4   8   0 8.64340 3.40665   2
  -4   8   0 7.30501 3.25925   2
   4   8   0 9.36283 3.59090   1
   0  -9   0 0.01317 0.64393   1
   0   9   0 -0.0849 0.56182   1
   0   9   0 -0.8592 0.51999   2
  -1  -9   0 583.996 19.8542   1
   1  -9   0 556.865 19.1571   2
   1   9   0 570.763 19.8593   1
  -1   9   0 569.090 19.3381   2
  -2  -9   0 10.3257 2.81481   1
   2  -9   0 9.99886 1.82530   3
   2   9   0 12.0640 2.26948   2
   2   9   0 11.6769 2.78239   1
  -2   9   0 12.4609 1.41190   1
   3  -9   0 -0.4831 1.25479   2
  -3  -9   0 -0.9846 1.71134   1
   3   9   0 -0.4673 1.21942   2
  -3   9   0 0.23844 1.62219   2
   3   9   0 -1.0229 1.42524   1
   4  -9   0 -0.2979 1.80456   2
  -4  -9   0 -1.1009 2.12408   1
   4   9   0 0.96042 2.31769   1
   4   9   0 1.00486 2.28908   2
  -4   9   0 0.12361 2.30110   2
   0 -10   0 1450.68 43.2817   1
   0  10   0 1465.16 43.3583   1
   1 -10   0 16.1119 2.35841   2
  -1 -10   0 24.3563 3.23139   1
   1  10   0 13.1614 1.94198   2
  -1  10   0 20.0029 2.70090   2
   1  10   0 21.1843 3.08895   1
   2 -10   0 -0.5535 0.70073   2
  -2 -10   0 1.99911 1.71378   1
   2 -10   0 -0.2039 0.63864   3
  -2  10   0 1.58225 0.56121   1
  -2  10   0 -0.4513 0.79084   2
   2  10   0 2.21228 1.73013   1
   2  10   0 1.89755 1.18072   2
  -3 -10   0 0.96928 1.90736   1
   3 -10   0 1.06212 1.64676   2
   3  10   0 1.41472 1.49108   2
  -3  10   0 -0.6468 1.25800   2
   3  10   0 -2.3905 1.48765   1
  -4 -10   0 16.1372 4.78718   1
   4 -10   0 18.4595 4.63673   2
   4  10   0 10.4842 3.40826   2
  -4  10   0 5.50023 3.00827   2
   4  10   0 13.5799 4.19336   1
   0 -11   0 -0.1398 0.67066   1
   0  11   0 -0.2251 0.65409   1
   0  11   0 2.05436 1.26148   2
  -1 -11   0 525.715 18.4977   1
   1 -11   0 507.988 17.7911   2
  -1  11   0 483.432 17.8208   2
   1  11   0 511.923 16.9780   2
   1  11   0 516.059 18.5389   1
  -2 -11   0 105.808 7.39856   1
   2 -11   0 113.192 5.66792   3
   2  11   0 123.097 7.93437   1
   2  11   0 105.430 6.11442   2
   3 -11   0 50.9679 6.45511   2
  -3 -11   0 49.4919 6.75834   1
  -3  11   0 54.7637 6.54580   2
   3  11   0 45.5040 6.40891   1
   3  11   0 42.2518 5.47366   2
   4 -11   0 54.3593 7.50033   2
  -4 -11   0 72.4401 9.68875   1
  -4  11   0 60.4066 7.92658   2
   4  11   0 52.6769 8.05630   1
   0 -12   0 267.457 9.80052   1
   0  12   0 260.924 9.80700   1
   0  12   0 270.244 10.3079   2
  -1 -12   0 113.245 6.53949   1
   1  12   0 108.263 6.48161   1
   1  12   0 124.716 5.76588   2
  -1  12   0 111.265 6.23298   2
  -2 -12   0 27.4549 4.46031   1
   2 -12   0 31.3520 4.28695   2
   2 -12   0 26.0380 3.06214   3
  -2  12   0 26.1930 3.96175   2
   2  12   0 30.7988 3.79519   2
   2  12   0 27.5878 4.50042   1
  -3 -12   0 8.85442 3.30616   1
   3 -12   0 2.07946 1.92189   2
   3  12   0 3.26962 2.31157   1
   3  12   0 4.22751 2.08195   2
  -3  12   0 2.63778 2.01889   2
   4 -12   0 2.25247 2.46252   2
  -4 -12   0 -2.2183 2.03469   1
  -4  12   0 -0.3830 2.25322   2
   4  12   0 0.86654 2.39196   1
   0 -13   0 0.14647 0.76303   1
   0  13   0 0.89074 1.24959   2
   0  13   0 0.46433 0.76563   1
  -1 -13   0 15.4953 2.86418   1
   1  13   0 25.2990 3.03901   2
  -1  13   0 20.4136 3.16799   2
   1  13   0 15.9477 2.93876   1
  -2 -13   0 1.88667 1.87938   1
   2 -13   0 2.39287 1.61082   2
   2 -13   0 5.55428 1.63917   3
   2  13   0 4.31505 2.22375   1
  -2  13   0 3.17564 1.97555   2
   2  13   0 6.06779 1.88322   2
  -3 -13   0 3.43040 2.64743   1
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   2  10 -16 1.35329 2.61213   1
  -2  10  16 -0.4608 2.76728   2
   1 -10 -16 1.38667 2.52108   3
   1 -10 -16 -1.0095 1.86280   1
   1  10 -16 -0.0887 2.58171   3
  -1  10  16 -4.0210 1.97442   2
   1  10 -16 -0.7661 2.08298   1
   0 -10 -16 15.3594 3.67213   1
   0 -10 -16 23.3391 5.23719   3
   0  10 -16 16.6574 4.12729   1
   0  10  16 19.9465 4.45407   2
  -1 -10 -16 30.3017 5.30221   1
  -1 -10 -16 34.8147 5.90112   3
  -1  10 -16 31.4773 5.28298   1
   1  10  16 29.8388 5.75794   2
   2 -11 -16 -0.4160 2.50828   3
  -2  11  16 -6.0876 2.51023   2
   2  11 -16 -0.2917 2.77155   3
   2  11 -16 -1.5243 1.83689   1
   1 -11 -16 26.7896 5.71973   3
   1 -11 -16 33.7574 5.43923   1
   1  11 -16 29.0951 5.52633   3
  -1  11  16 25.9323 4.99813   2
   1  11 -16 34.2612 6.19742   1
   0 -11 -16 58.6771 7.72199   3
   0 -11 -16 53.2531 6.40218   1
   0  11  16 67.5135 7.71642   2
   0  11 -16 51.7004 7.15765   1
  -1 -11 -16 23.5413 5.33649   3
  -1 -11 -16 26.8725 5.21336   1
  -1  11 -16 23.3981 4.92419   1
   1  11  16 25.9177 5.47905   2
   2 -12 -16 20.9152 5.72001   3
   2  12 -16 13.7286 4.69001   1
   2  12 -16 3.39189 3.35622   3
  -2  12  16 13.0787 4.44561   2
   1 -12 -16 41.0458 5.66505   1
   1 -12 -16 46.6518 7.37369   3
  -1  12  16 39.8056 6.11684   2
   1  12 -16 47.9508 6.93294   3
   1  12 -16 29.3782 5.81936   1
   0 -12 -16 9.99702 3.25697   1
   0 -12 -16 5.75509 3.49208   3
   0  12 -16 6.55979 3.20851   1
   0  12  16 10.7405 3.61045   2
  -1 -12 -16 -1.0201 2.72638   3
  -1 -12 -16 -0.5600 2.08393   1
  -1  12 -16 1.63213 2.78875   1
   1  12  16 2.11193 2.61600   2
   1 -13 -16 1.75415 2.89026   3
   1 -13 -16 2.29955 2.16286   1
   1  13 -16 0.17944 2.66257   1
  -1  13  16 0.81162 2.82542   2
   0 -13 -16 0.52382 2.31550   3
   0 -13 -16 1.20117 2.24431   1
   0  13  16 4.13336 2.99125   2
   0  13 -16 1.18579 2.57423   1
   1 -14 -16 12.8110 4.57444   3
   1  14 -16 3.03717 3.22850   1
  -1  14  16 3.95540 3.38080   2
   0 -14 -16 10.0137 3.79483   3
   0 -14 -16 6.92988 3.00511   1
   0  14  16 7.84121 3.28664   2
   0  14 -16 4.58315 3.10888   1
   2   0 -17 0.29911 2.25465   1
   2   0 -17 -0.0274 2.68510   3
   1   0 -17 -0.2664 2.36530   3
   1   0 -17 -0.6436 1.72591   1
   0   0 -17 2.12805 2.80302   3
   0   0 -17 -0.7879 1.45181   1
  -1   0 -17 -1.0094 1.45577   1
   1   0  17 -0.0324 2.43762   2
   2  -1 -17 33.1909 6.55333   3
   2  -1 -17 42.6270 6.78951   1
   2   1 -17 30.8700 6.55754   3
   2   1 -17 38.6074 6.41632   1
   1  -1 -17 2.01950 2.38364   3
   1  -1 -17 -1.6653 1.71694   1
   1   1 -17 2.45947 2.24713   1
   1   1 -17 -2.4670 2.29546   3
   0  -1 -17 39.7595 6.16206   3
   0  -1 -17 44.7687 6.30918   1
   0   1 -17 33.0526 5.41608   1
   0   1 -17 45.8447 7.20313   3
   1  -1  17 29.3867 5.57321   2
  -1  -1 -17 32.1610 5.17546   1
   1   1  17 32.0625 5.98856   2
  -1   1 -17 27.8281 5.01265   1
   2  -2 -17 -2.8930 2.64377   3
   2  -2 -17 9.61188 3.60678   1
   2   2 -17 10.2193 3.90596   3
   2   2 -17 7.16115 3.22474   1
   1  -2 -17 41.4617 7.02836   3
   1  -2 -17 41.4351 6.37085   1
   1   2 -17 36.4846 6.71812   3
   1   2 -17 42.0041 6.19854   1
   0  -2 -17 11.5308 3.22654   1
   0  -2 -17 9.67530 3.81129   3
   0   2 -17 9.61231 3.17696   1
  -1  -2 -17 9.05522 3.24648   1
  -1   2 -17 13.6236 3.68743   1
   1   2  17 18.6063 4.88145   2
   2  -3 -17 6.57719 3.46746   3
   2  -3 -17 9.39765 3.60952   1
   2   3 -17 8.92947 4.28415   3
   2   3 -17 4.18264 2.59608   1
   1  -3 -17 14.2152 3.91502   1
   1  -3 -17 12.8200 4.10643   3
   1   3 -17 10.3642 3.86678   3
   1   3 -17 23.6123 5.06631   1
   0  -3 -17 20.7421 4.29026   1
   0  -3 -17 15.2511 4.25570   3
   0   3 -17 17.7513 4.09883   1
   0   3  17 13.6432 3.56133   2
  -1  -3 -17 27.5199 5.19177   1
  -1   3 -17 21.6898 4.70788   1
   1   3  17 35.4954 6.18788   2
   2  -4 -17 9.61158 3.92311   3
   2  -4 -17 1.32626 2.42789   1
   2   4 -17 11.0288 3.90141   1
   2   4 -17 1.66545 3.25527   3
   1  -4 -17 -3.1674 2.23847   3
   1  -4 -17 3.80440 2.31663   1
   1   4 -17 0.88476 2.74685   3
   1   4 -17 2.25640 2.40373   1
   0  -4 -17 0.83710 1.66198   1
   0  -4 -17 0.79479 2.20933   3
   0   4  17 0.51920 2.28870   2
   0   4 -17 0.08044 1.68517   1
  -1  -4 -17 4.96593 2.65385   1
   1   4  17 7.35016 3.72990   2
  -1   4 -17 11.8256 3.37154   1
   2  -5 -17 17.4064 4.41235   1
   2  -5 -17 21.2395 5.63004   3
   2   5 -17 12.7713 4.01474   1
   2   5 -17 11.9675 4.41364   3
   1  -5 -17 43.1319 7.04626   3
   1  -5 -17 42.1530 6.34907   1
   1   5 -17 41.4356 7.01682   3
   1   5 -17 55.2929 7.56080   1
   0  -5 -17 17.6095 4.15118   1
   0  -5 -17 18.7359 4.77033   3
   0   5 -17 18.7189 4.42347   1
   0   5  17 19.4560 4.28942   2
  -1  -5 -17 25.4444 4.92365   1
  -1   5 -17 35.3357 5.74517   1
   1   5  17 32.1598 6.08794   2
   2  -6 -17 3.63451 2.65169   1
   2  -6 -17 3.20095 3.42685   3
   2   6 -17 4.57403 3.27677   3
   2   6 -17 3.67753 3.19399   1
   1  -6 -17 -0.3277 1.72037   1
   1  -6 -17 0.14213 2.33720   3
   1   6 -17 1.61481 2.78945   3
   1   6 -17 0.03241 2.16407   1
   0  -6 -17 36.4101 6.17896   3
   0  -6 -17 27.6745 5.03973   1
   0   6  17 40.7364 6.06309   2
   0   6 -17 34.8062 5.93098   1
  -1  -6 -17 10.6627 3.46331   1
   1   6  17 2.73021 2.59864   2
  -1   6 -17 5.33151 2.95513   1
   2  -7 -17 19.0268 5.23940   3
   2  -7 -17 19.2550 4.62775   1
   2   7 -17 11.9481 4.45423   3
   2   7 -17 17.1502 4.75452   1
   1  -7 -17 2.41643 2.76502   3
   1  -7 -17 2.60050 2.49170   1
   1   7 -17 3.51314 2.63488   1
  -1   7  17 2.27275 2.67314   2
   1   7 -17 5.80032 3.29818   3
   0  -7 -17 8.75048 3.36078   1
   0  -7 -17 11.9707 3.76150   3
   0   7  17 11.4527 3.78594   2
   0   7 -17 14.8517 4.03079   1
  -1  -7 -17 0.47823 1.97329   1
  -1   7 -17 0.31898 1.87889   1
   1   7  17 3.02251 3.32105   2
   2  -8 -17 25.4899 5.22295   1
   2  -8 -17 15.1822 5.40745   3
   2   8 -17 22.1790 5.62565   3
   2   8 -17 28.5208 5.97147   1
   1  -8 -17 102.977 8.27677   1
   1  -8 -17 105.630 11.2104   3
   1   8 -17 97.4297 9.99737   1
  -1   8  17 102.982 7.95066   2
   1   8 -17 103.653 10.3106   3
   0  -8 -17 9.00924 3.14416   1
   0  -8 -17 8.88090 3.75692   3
   0   8  17 15.1975 4.19751   2
   0   8 -17 12.5514 3.62608   1
  -1  -8 -17 2.21556 2.46526   1
   1   8  17 0.22682 2.64564   2
  -1   8 -17 2.81555 2.52181   1
   2  -9 -17 0.24224 2.30969   1
   2  -9 -17 0.30328 3.23466   3
   2   9 -17 2.48305 2.82482   1
   2   9 -17 1.73795 3.12651   3
   1  -9 -17 0.36748 2.90321   3
   1  -9 -17 4.18613 2.63311   1
   1   9 -17 4.56242 3.56383   3
   1   9 -17 4.88898 3.05936   1
  -1   9  17 9.95615 3.45489   2
   0  -9 -17 2.83466 2.98796   3
   0  -9 -17 3.94644 2.42039   1
   0   9 -17 0.71260 2.34126   1
   0   9  17 2.48498 2.43965   2
   1 -10 -17 42.4011 6.11704   1
   1 -10 -17 34.7053 6.67596   3
   1  10 -17 42.9816 6.78222   3
   1  10 -17 52.1783 7.58879   1
  -1  10  17 36.3139 5.75439   2
   0 -10 -17 8.33735 2.99054   1
   0 -10 -17 7.90904 3.70720   3
   0  10  17 11.9250 4.00507   2
   0  10 -17 11.0853 3.78780   1
   1 -11 -17 4.21432 2.58881   1
   1 -11 -17 14.5330 4.57643   3
   1  11 -17 17.7355 4.74333   1
  -1  11  17 12.6902 4.20236   2
   0 -11 -17 15.7495 4.79688   3
   0 -11 -17 17.3475 4.09836   1
   0  11  17 15.6308 4.18360   2
   0  11 -17 15.5556 4.23174   1
   1 -12 -17 5.92159 3.92162   3
   1 -12 -17 7.39386 3.07776   1
  -1  12  17 11.5291 4.00189   2
   1  12 -17 5.86067 3.50851   1
   0 -12 -17 15.1316 3.86133   1
   0 -12 -17 16.0675 5.09257   3
   0  12 -17 9.22848 3.73699   1
   0  12  17 8.88835 3.70818   2
   2   0 -18 13.8502 4.59068   1
   2   0 -18 10.1307 4.31960   3
   1   0 -18 -0.3242 1.72838   1
   1   0 -18 -0.4084 2.62649   3
   0   0 -18 1.07492 2.28784   1
  -1   0 -18 16.3011 4.21720   1
   2  -1 -18 6.35944 3.23362   1
   2  -1 -18 0.48564 2.54409   3
   2   1 -18 0.26734 2.75320   1
   2   1 -18 -0.5642 2.92718   3
   1  -1 -18 -0.7319 1.64729   1
   1  -1 -18 0.03171 2.51589   3
   1   1 -18 0.64176 2.91333   3
   1   1 -18 1.59619 2.23445   1
   0  -1 -18 7.53294 2.90329   1
   0   1 -18 13.5004 3.70149   1
  -1  -1 -18 2.87750 2.32548   1
  -1   1 -18 3.61544 2.70360   1
   2  -2 -18 33.9902 7.10413   3
   2  -2 -18 26.7351 5.78144   1
   2   2 -18 31.6954 6.29488   1
   2   2 -18 43.4738 7.90530   3
   1  -2 -18 16.4639 4.39557   3
   1  -2 -18 6.03928 3.34309   1
   1   2 -18 10.0265 3.66752   1
   1   2 -18 12.2983 4.49492   3
   0  -2 -18 1.33710 2.89405   3
   0  -2 -18 5.90785 2.90408   1
   0   2 -18 0.75912 2.03579   1
   2  -3 -18 8.86796 3.65304   1
   2  -3 -18 20.7207 5.40295   3
   2   3 -18 22.4795 5.18110   1
   2   3 -18 19.8804 5.42325   3
   1  -3 -18 36.5828 6.80739   3
   1  -3 -18 29.9345 5.64087   1
   1   3 -18 20.6979 4.93878   1
   1   3 -18 16.5093 4.68453   3
   0  -3 -18 2.73839 2.46177   1
   0  -3 -18 1.40946 3.15895   3
   0   3 -18 0.25899 1.65602   1
   1  -4 -18 2.28454 2.18482   1
   1  -4 -18 -1.3862 2.77501   3
   1   4 -18 2.79600 2.36204   1
   1   4 -18 4.82898 3.80297   3
   0  -4 -18 -2.7254 2.31966   3
   0  -4 -18 1.65114 2.34167   1
   0   4 -18 0.02432 2.25044   1
   1  -5 -18 1.23349 2.57827   1
   1  -5 -18 4.28887 3.85450   3
   1   5 -18 -0.1889 2.80103   3
   1   5 -18 1.19546 2.63931   1
   0  -5 -18 7.42099 3.06277   1
   0  -5 -18 12.2961 3.98796   3
   0   5 -18 10.5055 3.82022   1
   0   5  18 15.3019 4.13531   2
   1  -6 -18 3.71041 2.69038   1
   1  -6 -18 5.42365 3.64522   3
   1   6 -18 8.94563 3.70384   1
   1   6 -18 6.93864 3.83757   3
   0  -6 -18 1.32532 2.69639   3
   0  -6 -18 -0.8175 1.75048   1
   0   6  18 3.98366 3.13091   2
   0   6 -18 0.33707 2.29640   1
   1  -7 -18 0.98892 2.03450   1
   1  -7 -18 5.17473 3.65682   3
   1   7 -18 8.26144 3.98460   3
   1   7 -18 6.58683 3.27985   1
   0  -7 -18 3.09398 3.60665   3
   0  -7 -18 7.16699 3.12345   1
   0   7 -18 9.06986 3.65165   1
   0   7  18 3.03589 2.70203   2
   1  -8 -18 17.7439 4.28633   1
   1  -8 -18 17.0881 4.68980   3
   1   8 -18 18.4254 4.87739   1
   0  -8 -18 14.4483 4.54269   3
   0  -8 -18 9.74203 3.32274   1
   0   8  18 6.31641 3.18099   2
   0   8 -18 9.74726 3.74069   1
   0   0   0    0.00    0.00   0
;
_shelx_hkl_checksum              99547
_shelx_res_file
;
TITL CH-54 in P2(1)/c
    shelx.res
    created by SHELXL-2018/1 at 17:40:16 on 30-Jun-2018
CELL 0.71073   3.90170  22.03790  15.12650  90.0000  96.9977  90.0000
ZERR    4.00   0.00060   0.00310   0.00220   0.0000   0.0027   0.0000
LATT  1
SYMM -X, 0.5+Y, 0.5-Z
SFAC C H O CL S
UNIT 52 28 4 12 4
TEMP 21.000
SIZE 0.056 0.095 0.555
L.S. 13
BOND $H
HTAB
FMAP 2
PLAN 3
ACTA
CONF
WGHT    0.039700    0.312500
FVAR       0.46722
S1    5    1.191358    0.578142    0.760521    11.00000    0.06093    0.03640 =
         0.04647   -0.00098    0.01173   -0.00549
O1    3    0.742150    0.378984    0.819445    11.00000    0.11853    0.04767 =
         0.05020    0.00619    0.00127   -0.02789
CL1   4    0.891824    0.519010    0.597963    11.00000    0.13427    0.05809 =
         0.03630    0.00204    0.00427   -0.01254
CL2   4    1.378753    0.581749    0.956152    11.00000    0.06112    0.04949 =
         0.05139   -0.01038   -0.00853   -0.00527
CL3   4    0.181919    0.210015    0.652866    11.00000    0.07218    0.04512 =
         0.04722    0.00622    0.00863   -0.01414
C1    1    1.002093    0.514654    0.710704    11.00000    0.05267    0.03773 =
         0.03569   -0.00300    0.00689    0.00157
C2    1    1.207449    0.543790    0.862988    11.00000    0.03950    0.04168 =
         0.03946   -0.00451    0.00133    0.00047
C3    1    1.074244    0.487851    0.857911    11.00000    0.04562    0.03752 =
         0.03823    0.00194    0.00008   -0.00008
AFIX  43
H3A   2    1.062770    0.463252    0.907420    11.00000   -1.20000
AFIX   0
C4    1    0.951076    0.469453    0.769070    11.00000    0.03659    0.03486 =
         0.03865   -0.00094    0.00287    0.00334
C5    1    0.790464    0.408365    0.754523    11.00000    0.04761    0.03556 =
         0.04517   -0.00005    0.00104    0.00024
C6    1    0.695234    0.384792    0.664190    11.00000    0.06356    0.04160 =
         0.04341   -0.00126    0.00277   -0.01112
AFIX  43
H6A   2    0.750113    0.407394    0.615933    11.00000   -1.20000
AFIX   0
C7    1    0.535394    0.332917    0.649482    11.00000    0.04958    0.03758 =
         0.04484    0.00134    0.00312   -0.00283
AFIX  43
H7A   2    0.484449    0.311865    0.699544    11.00000   -1.20000
AFIX   0
C8    1    0.427777    0.304265    0.563582    11.00000    0.03726    0.03322 =
         0.04400    0.00059    0.00367   -0.00113
C9    1    0.265761    0.247939    0.557296    11.00000    0.04136    0.03403 =
         0.04124    0.00235    0.00420    0.00044
C10   1    0.164845    0.220270    0.476284    11.00000    0.05178    0.03993 =
         0.05076   -0.00303    0.00235   -0.00812
AFIX  43
H10A  2    0.058424    0.182449    0.474158    11.00000   -1.20000
AFIX   0
C11   1    0.222751    0.248968    0.399186    11.00000    0.06853    0.05247 =
         0.04189   -0.00408    0.00111   -0.00378
AFIX  43
H11A  2    0.153881    0.230816    0.344393    11.00000   -1.20000
AFIX   0
C12   1    0.382771    0.304629    0.402876    11.00000    0.07104    0.05526 =
         0.04345    0.00898    0.00432   -0.01004
AFIX  43
H12A  2    0.423175    0.324019    0.350527    11.00000   -1.20000
AFIX   0
C13   1    0.482674    0.331555    0.483301    11.00000    0.05860    0.03832 =
         0.05318    0.00682    0.00406   -0.00819
AFIX  43
H13A  2    0.590560    0.369228    0.484531    11.00000   -1.20000
AFIX   0
HKLF 4
REM  CH-54 in P2(1)/c
REM R1 =  0.0382 for    1977 Fo > 4sig(Fo)  and  0.0570 for all    2669 data
REM    163 parameters refined using      0 restraints
END
WGHT      0.0397      0.3125
REM Instructions for potential hydrogen bonds
HTAB C6 Cl1
REM Highest difference peak  0.298,  deepest hole -0.320,  1-sigma level  0.053
Q1    1   1.0987  0.5044  0.6200  11.00000  0.05    0.30
Q2    1   1.2222  0.5560  0.8176  11.00000  0.05    0.25
Q3    1   0.3469  0.2271  0.7015  11.00000  0.05    0.24
;
_shelx_res_checksum              87929
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
S S1 1.19136(18) 0.57814(3) 0.76052(4) 0.0475(2) Uani d 1
O O1 0.7421(6) 0.37898(9) 0.81944(13) 0.0729(7) Uani d 1
Cl Cl1 0.8918(3) 0.51901(4) 0.59796(4) 0.0767(3) Uani d 1
Cl Cl2 1.37875(18) 0.58175(3) 0.95615(4) 0.0553(2) Uani d 1
Cl Cl3 0.18192(19) 0.21002(3) 0.65287(4) 0.0547(2) Uani d 1
C C1 1.0021(6) 0.51465(11) 0.71070(15) 0.0419(6) Uani d 1
C C2 1.2074(6) 0.54379(11) 0.86299(15) 0.0405(6) Uani d 1
C C3 1.0742(6) 0.48785(11) 0.85791(16) 0.0409(6) Uani d 1
H H3A 1.062770 0.463252 0.907420 0.049 Uiso calc 1
C C4 0.9511(6) 0.46945(11) 0.76907(15) 0.0368(5) Uani d 1
C C5 0.7905(7) 0.40836(12) 0.75452(17) 0.0432(6) Uani d 1
C C6 0.6952(7) 0.38479(12) 0.66419(17) 0.0498(7) Uani d 1
H H6A 0.750113 0.407394 0.615933 0.060 Uiso calc 1
C C7 0.5354(7) 0.33292(12) 0.64948(16) 0.0442(6) Uani d 1
H H7A 0.484449 0.311865 0.699544 0.053 Uiso calc 1
C C8 0.4278(6) 0.30426(11) 0.56358(16) 0.0383(5) Uani d 1
C C9 0.2658(6) 0.24794(11) 0.55730(16) 0.0389(6) Uani d 1
C C10 0.1648(7) 0.22027(12) 0.47628(17) 0.0478(6) Uani d 1
H H10A 0.058424 0.182449 0.474158 0.057 Uiso calc 1
C C11 0.2228(8) 0.24897(13) 0.39919(17) 0.0548(7) Uani d 1
H H11A 0.153881 0.230816 0.344393 0.066 Uiso calc 1
C C12 0.3828(8) 0.30463(13) 0.40288(18) 0.0568(7) Uani d 1
H H12A 0.423175 0.324019 0.350527 0.068 Uiso calc 1
C C13 0.4827(7) 0.33156(12) 0.48330(17) 0.0503(7) Uani d 1
H H13A 0.590560 0.369228 0.484531 0.060 Uiso calc 1
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
S1 0.0609(4) 0.0364(4) 0.0465(4) -0.0055(3) 0.0117(3) -0.0010(3)
O1 0.1185(19) 0.0477(12) 0.0502(11) -0.0279(12) 0.0013(12) 0.0062(10)
Cl1 0.1343(8) 0.0581(5) 0.0363(4) -0.0125(5) 0.0043(4) 0.0020(3)
Cl2 0.0611(4) 0.0495(4) 0.0514(4) -0.0053(3) -0.0085(3) -0.0104(3)
Cl3 0.0722(5) 0.0451(4) 0.0472(4) -0.0141(3) 0.0086(3) 0.0062(3)
C1 0.0527(15) 0.0377(15) 0.0357(12) 0.0016(12) 0.0069(11) -0.0030(10)
C2 0.0395(13) 0.0417(15) 0.0395(13) 0.0005(11) 0.0013(10) -0.0045(11)
C3 0.0456(14) 0.0375(14) 0.0382(12) -0.0001(11) 0.0001(11) 0.0019(11)
C4 0.0366(12) 0.0349(14) 0.0387(12) 0.0033(10) 0.0029(10) -0.0009(10)
C5 0.0476(14) 0.0356(14) 0.0452(14) 0.0002(11) 0.0010(11) 0.0000(11)
C6 0.0636(17) 0.0416(16) 0.0434(14) -0.0111(13) 0.0028(12) -0.0013(12)
C7 0.0496(15) 0.0376(15) 0.0448(13) -0.0028(12) 0.0031(11) 0.0013(11)
C8 0.0373(13) 0.0332(14) 0.0440(13) -0.0011(10) 0.0037(10) 0.0006(10)
C9 0.0414(13) 0.0340(14) 0.0412(13) 0.0004(11) 0.0042(10) 0.0023(10)
C10 0.0518(15) 0.0399(15) 0.0508(15) -0.0081(12) 0.0023(12) -0.0030(12)
C11 0.0685(19) 0.0525(18) 0.0419(14) -0.0038(15) 0.0011(13) -0.0041(13)
C12 0.0710(19) 0.0553(19) 0.0434(15) -0.0100(15) 0.0043(13) 0.0090(13)
C13 0.0586(17) 0.0383(15) 0.0532(15) -0.0082(13) 0.0041(13) 0.0068(12)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C1 S1 C2 90.19(12)
C4 C1 Cl1 130.5(2)
C4 C1 S1 113.67(18)
Cl1 C1 S1 115.81(14)
C3 C2 Cl2 127.67(19)
C3 C2 S1 112.53(18)
Cl2 C2 S1 119.80(15)
C2 C3 C4 113.5(2)
C2 C3 H3A 123.2
C4 C3 H3A 123.2
C1 C4 C3 110.1(2)
C1 C4 C5 131.1(2)
C3 C4 C5 118.8(2)
O1 C5 C6 121.3(2)
O1 C5 C4 117.9(2)
C6 C5 C4 120.8(2)
C7 C6 C5 122.0(2)
C7 C6 H6A 119.0
C5 C6 H6A 119.0
C6 C7 C8 127.5(2)
C6 C7 H7A 116.2
C8 C7 H7A 116.2
C9 C8 C13 116.2(2)
C9 C8 C7 121.7(2)
C13 C8 C7 122.0(2)
C10 C9 C8 122.2(2)
C10 C9 Cl3 117.64(19)
C8 C9 Cl3 120.21(18)
C11 C10 C9 119.5(2)
C11 C10 H10A 120.2
C9 C10 H10A 120.2
C10 C11 C12 119.9(2)
C10 C11 H11A 120.0
C12 C11 H11A 120.0
C13 C12 C11 120.2(3)
C13 C12 H12A 119.9
C11 C12 H12A 119.9
C12 C13 C8 122.0(2)
C12 C13 H13A 119.0
C8 C13 H13A 119.0
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
S1 C1 1.713(3)
S1 C2 1.719(2)
O1 C5 1.210(3)
Cl1 C1 1.710(2)
Cl2 C2 1.704(2)
Cl3 C9 1.735(2)
C1 C4 1.362(3)
C2 C3 1.336(3)
C3 C4 1.430(3)
C3 H3A 0.9300
C4 C5 1.490(3)
C5 C6 1.467(3)
C6 C7 1.308(3)
C6 H6A 0.9300
C7 C8 1.460(3)
C7 H7A 0.9300
C8 C9 1.391(3)
C8 C13 1.395(3)
C9 C10 1.382(3)
C10 C11 1.369(4)
C10 H10A 0.9300
C11 C12 1.374(4)
C11 H11A 0.9300
C12 C13 1.367(4)
C12 H12A 0.9300
C13 H13A 0.9300
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C6 H6A Cl1 0.93 2.54 3.245(3) 133 yes
C7 H7A Cl3 0.93 2.59 3.043(3) 110 yes
C7 H7A O1 0.93 2.46 2.790(3) 101 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C2 S1 C1 C4 0.4(2)
C2 S1 C1 Cl1 177.73(16)
C1 S1 C2 C3 -0.3(2)
C1 S1 C2 Cl2 179.98(16)
Cl2 C2 C3 C4 179.88(19)
S1 C2 C3 C4 0.2(3)
Cl1 C1 C4 C3 -177.2(2)
S1 C1 C4 C3 -0.3(3)
Cl1 C1 C4 C5 1.6(4)
S1 C1 C4 C5 178.5(2)
C2 C3 C4 C1 0.0(3)
C2 C3 C4 C5 -178.9(2)
C1 C4 C5 O1 -172.0(3)
C3 C4 C5 O1 6.7(4)
C1 C4 C5 C6 8.1(4)
C3 C4 C5 C6 -173.2(2)
O1 C5 C6 C7 4.3(4)
C4 C5 C6 C7 -175.9(2)
C5 C6 C7 C8 -179.7(2)
C6 C7 C8 C9 178.5(3)
C6 C7 C8 C13 -1.2(4)
C13 C8 C9 C10 0.1(4)
C7 C8 C9 C10 -179.6(2)
C13 C8 C9 Cl3 -179.60(19)
C7 C8 C9 Cl3 0.7(3)
C8 C9 C10 C11 -0.4(4)
Cl3 C9 C10 C11 179.3(2)
C9 C10 C11 C12 0.5(4)
C10 C11 C12 C13 -0.3(5)
C11 C12 C13 C8 0.0(5)
C9 C8 C13 C12 0.1(4)
C7 C8 C13 C12 179.8(3)

_cod_database_fobs_code 2242807