#------------------------------------------------------------------------------ #$Date: 2019-01-16 05:24:24 +0200 (Wed, 16 Jan 2019) $ #$Revision: 213113 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/28/2242815.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242815 loop_ _publ_author_name 'Chkirate, Karim' 'Kansiz, Sevgi' 'Karrouchi, Khalid' 'Mague, Joel T.' 'Dege, Necmi' 'Essassi, El Mokhtar' _publ_section_title ; Crystal structure and Hirshfeld surface analysis of N-{2-[(E)-(4-methylbenzylidene)amino]phenyl}-2-(5-methyl-1-H-pyrazol-3-yl)acetamide hemihydrate ; _journal_coeditor_code XU5954 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 154 _journal_page_last 158 _journal_paper_doi 10.1107/S2056989018017747 _journal_volume 75 _journal_year 2019 _chemical_formula_iupac 'C20 H20 N4 O, 0.5H2 O' _chemical_formula_moiety 'C20 H20 N4 O, 0.5(H2 O)' _chemical_formula_sum 'C20 H21 N4 O1.5' _chemical_formula_weight 341.41 _chemical_name_systematic 'N-{2-[(E)-(4-Methylbenzylidene)amino]phenyl}-2-(5-methyl-1-H-pyrazol-3-yl)acetamide hemihydrate' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/1 _cell_angle_alpha 101.991(3) _cell_angle_beta 97.535(3) _cell_angle_gamma 99.847(3) _cell_formula_units_Z 4 _cell_length_a 11.546(3) _cell_length_b 12.564(3) _cell_length_c 13.172(3) _cell_measurement_reflns_used 5130 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.1808 _cell_measurement_theta_min 2.2069 _cell_volume 1813.8(8) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; DIAMOND (Brandenburg & Putz, 2012) and Mercury (Macrae et al., 2008) ; _computing_publication_material ; SHELXL2018/1 (Sheldrick, 2015b), PLATON (Spek, 2009) and publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2018/1 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.972 _diffrn_measured_fraction_theta_max 0.969 _diffrn_measurement_device_type 'Bruker SMART APEX CCD' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0328 _diffrn_reflns_av_unetI/netI 0.0643 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 17171 _diffrn_reflns_theta_full 28.150 _diffrn_reflns_theta_max 28.181 _diffrn_reflns_theta_min 1.605 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.082 _exptl_absorpt_correction_T_max 0.99 _exptl_absorpt_correction_T_min 0.88 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.250 _exptl_crystal_density_method 'not measured' _exptl_crystal_description rod _exptl_crystal_F_000 724 _exptl_crystal_size_max 0.210 _exptl_crystal_size_mid 0.134 _exptl_crystal_size_min 0.116 _refine_diff_density_max 0.278 _refine_diff_density_min -0.187 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 628 _refine_ls_number_reflns 8663 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.035 _refine_ls_R_factor_all 0.0749 _refine_ls_R_factor_gt 0.0463 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0564P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1105 _refine_ls_wR_factor_ref 0.1218 _reflns_number_gt 5888 _reflns_number_total 8663 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file xu5954sup1.cif _cod_data_source_block I _cod_original_cell_volume 1813.8(7) _cod_database_code 2242815 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.983 _shelx_estimated_absorpt_t_max 0.991 _shelx_hkl_file ; -1 0 0 332.67 19.00 -1 0 0 334.57 19.00 1 0 0 339.77 19.00 -2 0 0 24.80 1.60 -2 0 0 27.80 1.60 2 0 0 26.10 1.60 -3 0 0 50.49 3.00 -3 0 0 51.69 3.00 3 0 0 48.90 3.00 -4 0 0 349.27 19.80 -4 0 0 342.47 19.80 4 0 0 353.16 19.90 -5 0 0 61.19 3.60 -5 0 0 61.99 3.60 5 0 0 57.29 3.70 -6 0 0 19.60 1.50 -6 0 0 24.60 1.60 6 0 0 23.00 1.70 -7 0 0 56.89 3.40 -7 0 0 58.09 3.40 7 0 0 47.90 3.50 -8 0 0 98.89 6.10 -8 0 0 106.69 6.10 8 0 0 103.79 6.30 -9 0 0 17.60 1.60 -9 0 0 16.20 1.60 9 0 0 18.20 1.90 -10 0 0 44.50 3.20 -10 0 0 43.70 3.10 10 0 0 46.40 3.30 -11 0 0 -0.40 1.30 11 0 0 0.40 1.40 12 0 0 3.20 1.70 13 0 0 0.00 1.80 14 0 0 2.40 2.20 15 -1 0 1.40 2.50 14 -1 0 0.80 2.00 13 -1 0 -1.10 1.60 12 -1 0 16.70 2.30 -12 1 0 10.10 2.00 11 -1 0 23.20 2.40 -11 1 0 25.60 2.20 10 -1 0 11.40 1.70 -10 1 0 9.90 1.40 9 -1 0 7.70 1.40 -9 1 0 6.70 1.00 -9 1 0 6.10 1.10 8 -1 0 0.60 0.90 -8 1 0 0.00 0.70 -8 1 0 1.10 0.70 7 -1 0 99.79 6.00 -7 1 0 98.69 5.90 -7 1 0 99.09 5.90 6 -1 0 16.50 1.40 -6 1 0 16.60 1.30 -6 1 0 17.00 1.20 5 -1 0 0.50 0.50 -5 1 0 0.70 0.50 -5 1 0 0.30 0.40 4 -1 0 34.70 2.20 -4 1 0 37.10 2.20 -4 1 0 35.90 2.20 3 -1 0 0.80 0.50 -3 1 0 0.40 0.30 -3 1 0 1.00 0.30 2 -1 0 1953.80 106.59 -2 1 0 1789.02 106.59 -2 1 0 1901.11 106.59 1 -1 0 397.36 22.30 1 -1 0 391.36 22.30 -1 1 0 391.06 22.30 0 -1 0 166.08 9.60 0 1 0 168.38 9.60 0 1 0 172.98 9.60 -1 -1 0 117.29 6.80 -1 -1 0 121.69 6.80 1 1 0 117.49 6.80 -2 -1 0 21.70 1.40 -2 -1 0 24.30 1.40 2 1 0 23.40 1.50 -3 -1 0 465.85 26.50 -3 -1 0 482.25 26.50 3 1 0 450.35 26.50 -4 -1 0 45.40 2.70 -4 -1 0 44.90 2.70 4 1 0 44.10 2.80 -5 -1 0 279.47 15.90 -5 -1 0 282.67 15.90 5 1 0 271.37 16.00 -6 -1 0 9.10 0.90 -6 -1 0 9.50 1.00 6 1 0 8.70 1.10 -7 -1 0 18.70 1.50 -7 -1 0 18.80 1.50 7 1 0 22.40 1.80 -8 -1 0 5.90 1.00 -8 -1 0 4.90 0.90 8 1 0 5.10 1.10 -9 -1 0 -0.10 1.00 -9 -1 0 0.20 0.90 9 1 0 -0.50 1.10 -10 -1 0 -0.20 0.90 -10 -1 0 0.70 1.10 10 1 0 -1.80 1.20 11 1 0 2.30 1.50 12 1 0 1.20 1.70 13 1 0 -1.20 1.90 14 1 0 3.70 2.50 15 -2 0 -0.90 2.50 14 -2 0 0.60 1.90 13 -2 0 1.40 1.60 -13 2 0 2.90 1.80 12 -2 0 4.90 1.60 -12 2 0 4.70 1.50 11 -2 0 -0.10 1.20 -11 2 0 -0.20 1.30 10 -2 0 4.40 1.20 -10 2 0 2.60 1.20 9 -2 0 12.90 1.50 -9 2 0 12.60 1.30 -9 2 0 10.40 1.40 8 -2 0 0.40 0.90 -8 2 0 -0.10 0.70 -8 2 0 1.00 0.70 7 -2 0 1.80 0.80 -7 2 0 1.70 0.60 -7 2 0 2.50 0.70 6 -2 0 383.76 22.40 -6 2 0 396.76 22.40 -6 2 0 392.26 22.30 5 -2 0 83.99 5.00 -5 2 0 83.19 5.00 -5 2 0 83.99 4.90 4 -2 0 79.69 4.80 4 -2 0 83.19 4.80 -4 2 0 83.99 4.80 3 -2 0 22.90 1.50 3 -2 0 24.40 1.40 -3 2 0 20.60 1.50 2 -2 0 192.88 11.20 2 -2 0 206.78 11.30 -2 2 0 192.08 11.30 1 -2 0 836.02 46.50 1 -2 0 791.72 46.50 -1 2 0 832.92 46.50 0 -2 0 1238.68 71.59 0 2 0 1315.77 71.59 0 2 0 1235.78 71.59 -1 -2 0 427.76 24.60 1 2 0 438.96 24.60 1 2 0 432.66 24.60 -2 -2 0 15.80 1.20 -2 -2 0 18.30 1.00 2 2 0 15.70 1.20 -3 -2 0 185.38 10.60 -3 -2 0 182.18 10.70 3 2 0 189.18 10.70 -4 -2 0 116.89 6.90 -4 -2 0 122.29 6.80 4 2 0 113.89 6.90 -5 -2 0 256.57 14.80 -5 -2 0 258.77 14.70 5 2 0 258.27 14.90 -6 -2 0 20.90 1.40 -6 -2 0 19.60 1.60 6 2 0 18.60 1.70 -7 -2 0 0.10 0.70 -7 -2 0 -0.60 0.60 7 2 0 -0.20 0.90 -8 -2 0 0.10 0.80 -8 -2 0 0.80 0.80 8 2 0 0.40 1.10 -9 -2 0 3.70 1.00 -9 -2 0 3.70 1.10 9 2 0 4.50 1.40 -10 -2 0 77.49 5.00 10 2 0 79.19 5.30 11 2 0 8.40 2.00 12 2 0 21.50 2.70 13 2 0 3.10 2.20 14 2 0 1.70 2.50 14 -3 0 4.70 2.10 -14 3 0 3.50 2.00 13 -3 0 1.40 1.90 -13 3 0 0.90 1.70 12 -3 0 3.70 1.50 -12 3 0 3.00 1.50 11 -3 0 3.40 1.50 -11 3 0 2.70 1.30 10 -3 0 13.40 1.70 -10 3 0 13.20 1.70 9 -3 0 4.70 1.20 9 -3 0 3.10 0.80 -9 3 0 4.20 1.20 8 -3 0 277.77 15.70 8 -3 0 262.97 15.80 -8 3 0 279.67 15.80 7 -3 0 0.80 0.70 7 -3 0 0.60 0.50 -7 3 0 0.20 0.70 6 -3 0 131.59 7.30 6 -3 0 128.79 7.40 -6 3 0 117.99 7.40 5 -3 0 19.90 1.40 5 -3 0 18.30 1.40 -5 3 0 20.80 1.40 4 -3 0 19.10 1.30 4 -3 0 19.50 1.40 -4 3 0 18.30 1.40 3 -3 0 777.92 44.90 3 -3 0 814.72 44.90 -3 3 0 778.52 44.90 2 -3 0 73.39 4.20 2 -3 0 71.49 4.20 -2 3 0 70.49 4.20 1 -3 0 8882.61 510.25 1 -3 0 8632.04 510.35 -1 3 0 9507.85 510.35 0 -3 0 2749.82 155.78 0 3 0 2706.73 155.88 0 3 0 2793.52 155.88 -1 -3 0 5.90 0.60 1 3 0 5.20 0.40 1 3 0 5.00 0.60 -2 -3 0 2.60 0.50 2 3 0 1.70 0.50 2 3 0 1.90 0.30 -3 -3 0 53.19 3.20 -3 -3 0 52.79 3.00 3 3 0 50.69 3.20 -4 -3 0 153.08 8.70 -4 -3 0 148.59 8.90 4 3 0 156.98 8.90 -5 -3 0 83.09 5.10 -5 -3 0 86.19 5.00 5 3 0 86.19 5.20 -6 -3 0 10.70 0.90 -6 -3 0 9.70 1.10 6 3 0 8.80 1.20 -7 -3 0 23.50 1.90 -7 -3 0 23.20 1.60 7 3 0 22.90 2.00 -8 -3 0 180.08 10.60 8 3 0 182.28 10.80 -9 -3 0 8.40 1.40 9 3 0 10.40 1.70 -10 -3 0 33.20 3.00 10 3 0 41.20 3.20 11 3 0 0.80 1.70 12 3 0 1.50 1.90 13 3 0 7.90 2.60 14 3 0 -2.30 3.00 -15 4 0 -2.70 2.50 -14 4 0 5.30 2.40 13 -4 0 6.60 1.90 -13 4 0 5.90 2.10 12 -4 0 1.00 1.70 -12 4 0 2.90 1.50 11 -4 0 3.60 1.50 -11 4 0 1.90 1.30 10 -4 0 89.09 5.40 -10 4 0 80.59 5.30 9 -4 0 9.30 1.40 9 -4 0 9.60 1.10 -9 4 0 13.80 1.50 8 -4 0 0.30 0.80 8 -4 0 0.40 0.70 -8 4 0 -0.80 0.80 7 -4 0 0.60 0.80 7 -4 0 0.60 0.60 -7 4 0 -0.40 0.70 6 -4 0 68.09 4.00 6 -4 0 67.39 4.10 -6 4 0 65.09 4.10 5 -4 0 15.20 1.20 5 -4 0 16.70 1.20 -5 4 0 16.20 1.30 4 -4 0 10.50 0.90 4 -4 0 9.80 0.90 -4 4 0 10.40 1.00 3 -4 0 10.00 0.80 3 -4 0 10.10 0.80 -3 4 0 9.40 0.90 2 -4 0 1383.66 79.19 2 -4 0 1425.06 79.19 -2 4 0 1381.16 79.19 1 -4 0 5462.65 301.97 1 -4 0 5114.49 301.97 -1 4 0 5417.16 302.17 0 -4 0 6.60 0.70 0 4 0 6.70 0.70 0 4 0 6.40 0.60 -1 -4 0 109.09 6.20 1 4 0 105.09 6.10 1 4 0 103.69 6.20 -2 -4 0 136.29 8.10 2 4 0 141.09 7.90 2 4 0 137.69 8.10 -3 -4 0 20.00 1.40 -3 -4 0 18.20 1.20 3 4 0 18.90 1.50 -4 -4 0 169.88 9.50 -4 -4 0 153.08 9.70 4 4 0 176.98 9.80 -5 -4 0 35.40 2.40 -5 -4 0 34.50 2.10 5 4 0 33.80 2.40 -6 -4 0 60.99 3.70 -6 -4 0 57.99 3.50 6 4 0 58.49 3.80 -7 -4 0 10.40 1.30 7 4 0 12.50 1.40 -8 -4 0 233.18 13.90 8 4 0 241.58 14.00 -9 -4 0 2.30 1.20 9 4 0 3.00 1.50 -10 -4 0 5.50 1.40 10 4 0 5.20 1.70 11 4 0 0.30 1.60 12 4 0 2.30 2.10 13 4 0 13.20 3.00 -15 5 0 -0.80 2.30 -14 5 0 -1.20 1.90 -13 5 0 -1.30 1.70 12 -5 0 5.50 1.80 -12 5 0 3.90 1.60 11 -5 0 5.20 1.60 -11 5 0 6.90 1.60 10 -5 0 15.90 1.80 -10 5 0 19.20 2.00 9 -5 0 9.10 1.10 9 -5 0 8.60 1.40 -9 5 0 10.20 1.40 8 -5 0 370.56 21.20 8 -5 0 370.46 21.20 -8 5 0 366.86 21.30 7 -5 0 189.28 11.00 7 -5 0 192.08 10.90 -7 5 0 180.98 11.00 6 -5 0 7.20 0.90 6 -5 0 7.70 1.00 -6 5 0 8.00 1.00 5 -5 0 9.00 0.90 5 -5 0 10.10 1.00 -5 5 0 9.40 1.00 4 -5 0 22.60 1.50 4 -5 0 24.50 1.60 -4 5 0 19.80 1.60 3 -5 0 986.10 55.19 3 -5 0 942.21 55.09 -3 5 0 985.90 55.19 2 -5 0 197.88 11.20 2 -5 0 194.28 11.20 -2 5 0 191.58 11.20 1 -5 0 214.48 12.40 -1 5 0 216.58 12.30 -1 5 0 214.28 12.30 0 -5 0 224.68 13.00 0 5 0 228.18 12.90 0 5 0 223.68 13.00 -1 -5 0 19.00 1.40 1 5 0 19.00 1.50 1 5 0 19.90 1.30 -2 -5 0 597.54 34.40 2 5 0 604.04 34.20 2 5 0 607.44 34.40 -3 -5 0 79.49 5.00 3 5 0 88.89 5.10 -4 -5 0 188.88 11.20 -4 -5 0 196.18 10.90 4 5 0 188.08 11.20 -5 -5 0 12.90 1.40 -5 -5 0 14.50 1.10 5 5 0 14.60 1.50 -6 -5 0 4.80 1.00 6 5 0 4.40 1.10 -7 -5 0 11.60 1.40 7 5 0 10.00 1.60 -8 -5 0 174.78 10.40 8 5 0 176.08 10.60 -9 -5 0 3.50 1.30 9 5 0 2.20 1.50 -10 -5 0 56.09 4.00 10 5 0 49.00 4.10 -11 -5 0 -0.90 1.60 11 5 0 -0.30 2.00 12 5 0 -1.40 2.30 13 5 0 7.00 3.40 -14 6 0 0.70 2.10 -13 6 0 21.10 2.80 -12 6 0 23.10 2.60 11 -6 0 10.20 1.80 -11 6 0 9.80 1.80 10 -6 0 103.29 6.20 -10 6 0 93.09 6.20 9 -6 0 47.20 3.00 9 -6 0 42.00 3.10 -9 6 0 45.30 3.20 8 -6 0 52.79 3.30 8 -6 0 46.30 3.20 -8 6 0 53.89 3.40 7 -6 0 55.79 3.50 7 -6 0 52.19 3.40 -7 6 0 54.99 3.50 6 -6 0 1.80 0.70 6 -6 0 2.50 0.70 -6 6 0 0.60 0.80 5 -6 0 19.70 1.60 5 -6 0 21.70 1.50 -5 6 0 17.80 1.50 4 -6 0 23.80 1.70 4 -6 0 23.10 1.70 -4 6 0 25.20 1.80 3 -6 0 199.68 11.60 3 -6 0 204.98 11.70 -3 6 0 201.98 11.70 2 -6 0 197.78 10.80 2 -6 0 183.48 10.80 -2 6 0 180.98 10.80 1 -6 0 10.70 0.90 -1 6 0 2.50 0.60 -1 6 0 0.60 0.60 0 -6 0 91.89 5.60 0 6 0 96.69 5.50 0 6 0 91.69 5.60 -1 -6 0 67.59 4.10 1 6 0 63.89 3.90 1 6 0 70.89 4.10 -2 -6 0 80.69 5.20 2 6 0 90.69 5.20 2 6 0 86.99 5.00 -3 -6 0 73.69 4.70 3 6 0 77.69 4.50 3 6 0 78.59 4.70 -4 -6 0 0.20 0.80 4 6 0 -0.60 0.80 -5 -6 0 11.10 1.30 5 6 0 8.60 1.30 -6 -6 0 4.30 1.10 6 6 0 2.60 1.20 -7 -6 0 174.48 10.70 7 6 0 187.08 10.80 -8 -6 0 1.30 1.20 8 6 0 1.70 1.40 -9 -6 0 6.50 1.60 9 6 0 6.40 1.80 -10 -6 0 17.90 2.30 10 6 0 14.40 2.40 -11 -6 0 -0.40 1.60 11 6 0 -1.20 2.00 12 6 0 16.20 2.90 -14 7 0 18.90 2.70 -13 7 0 8.50 2.40 -12 7 0 9.70 2.00 -11 7 0 -0.80 1.40 10 -7 0 48.40 3.50 -10 7 0 44.70 3.50 9 -7 0 8.60 1.40 -9 7 0 8.90 1.50 8 -7 0 67.69 4.20 8 -7 0 64.29 4.20 -8 7 0 68.59 4.40 7 -7 0 0.80 0.80 7 -7 0 0.60 0.90 -7 7 0 0.10 0.90 6 -7 0 10.70 1.10 6 -7 0 10.40 1.30 -6 7 0 15.10 1.40 5 -7 0 46.20 3.10 5 -7 0 53.19 3.10 -5 7 0 45.20 3.10 4 -7 0 12.10 1.10 4 -7 0 11.50 1.10 -4 7 0 8.20 1.10 3 -7 0 232.28 13.30 3 -7 0 230.68 13.30 -3 7 0 227.88 13.30 2 -7 0 2873.91 166.08 -2 7 0 2972.80 166.08 -2 7 0 2942.11 166.08 1 -7 0 71.29 4.40 -1 7 0 72.99 4.40 -1 7 0 73.59 4.40 0 -7 0 107.39 6.60 0 7 0 112.09 6.60 0 7 0 112.99 6.50 -1 -7 0 5.20 0.90 1 7 0 4.90 0.70 1 7 0 5.70 0.90 -2 -7 0 1.20 0.80 2 7 0 1.80 0.50 2 7 0 1.50 0.80 -3 -7 0 0.10 0.80 3 7 0 0.30 0.80 -4 -7 0 25.10 2.10 4 7 0 29.10 2.20 -5 -7 0 8.20 1.30 5 7 0 10.50 1.50 -6 -7 0 1.50 1.10 6 7 0 1.60 1.20 -7 -7 0 10.70 1.60 7 7 0 6.90 1.70 -8 -7 0 25.00 2.50 8 7 0 26.30 2.70 -9 -7 0 5.40 1.60 9 7 0 4.60 1.80 -10 -7 0 4.70 1.80 10 7 0 4.20 2.10 -11 -7 0 0.20 2.00 11 7 0 -2.00 2.20 -14 8 0 3.20 2.20 -13 8 0 7.20 2.10 -12 8 0 6.80 2.00 -11 8 0 0.80 1.50 -10 8 0 7.10 1.60 -9 8 0 157.28 9.50 8 -8 0 37.50 2.70 8 -8 0 35.00 2.60 -8 8 0 31.10 2.70 7 -8 0 1.20 0.80 7 -8 0 1.60 1.00 -7 8 0 2.80 0.90 6 -8 0 4.50 0.90 6 -8 0 5.30 1.00 -6 8 0 6.70 1.20 5 -8 0 30.10 2.20 5 -8 0 32.20 2.20 -5 8 0 26.30 2.20 4 -8 0 161.38 9.80 4 -8 0 177.28 9.80 -4 8 0 163.98 9.80 3 -8 0 26.70 2.00 3 -8 0 24.90 1.80 -3 8 0 25.90 1.90 2 -8 0 7.70 1.00 -2 8 0 6.20 1.00 -2 8 0 6.30 0.90 1 -8 0 28.60 2.10 -1 8 0 26.50 2.00 -1 8 0 28.00 1.90 0 -8 0 5.00 0.90 0 8 0 3.30 0.90 0 8 0 4.90 0.70 -1 -8 0 25.60 2.10 1 8 0 27.60 1.90 1 8 0 29.70 2.20 -2 -8 0 41.20 3.00 2 8 0 47.80 3.10 -3 -8 0 168.28 10.10 3 8 0 175.28 10.20 -4 -8 0 1.00 1.00 4 8 0 0.30 1.10 -5 -8 0 3.30 1.20 5 8 0 7.10 1.40 -6 -8 0 -0.30 1.20 6 8 0 1.00 1.30 -7 -8 0 0.00 1.20 7 8 0 2.40 1.60 -8 -8 0 2.00 1.50 8 8 0 3.00 1.80 -9 -8 0 1.60 1.80 9 8 0 1.90 2.10 -10 -8 0 15.90 2.40 10 8 0 9.90 2.60 -11 -8 0 2.10 2.30 11 8 0 7.10 2.80 -13 9 0 -0.30 1.90 -12 9 0 9.30 2.20 -11 9 0 0.80 1.60 -10 9 0 1.80 1.40 -9 9 0 1.30 1.30 8 -9 0 72.39 4.60 7 -9 0 36.80 2.60 7 -9 0 31.70 2.70 -7 9 0 43.70 2.90 6 -9 0 1.30 0.90 6 -9 0 0.80 1.00 -6 9 0 1.00 0.90 5 -9 0 0.60 0.90 5 -9 0 1.20 1.00 -5 9 0 -0.30 0.90 4 -9 0 -0.20 0.80 4 -9 0 -0.70 0.70 -4 9 0 0.40 0.80 3 -9 0 12.00 1.40 -3 9 0 11.20 1.30 -3 9 0 9.50 1.20 2 -9 0 18.50 1.60 -2 9 0 16.30 1.50 -2 9 0 14.10 1.50 1 -9 0 117.19 6.80 -1 9 0 107.89 6.70 -1 9 0 113.59 6.70 0 -9 0 4.60 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24.90 1.60 -6 5 3 22.30 1.80 5 -5 -3 333.27 19.50 5 -5 -3 347.27 19.30 -5 5 3 334.27 19.40 4 -5 -3 42.40 2.50 4 -5 -3 40.40 2.70 -4 5 3 39.40 2.60 3 -5 -3 51.79 2.90 3 -5 -3 47.30 3.10 -3 5 3 43.90 2.90 2 -5 -3 104.89 5.90 2 -5 -3 97.59 6.00 -2 5 3 99.19 5.90 1 -5 -3 0.20 0.50 1 -5 -3 1.10 0.60 -1 5 3 0.80 0.50 0 -5 -3 35.30 2.20 0 5 3 33.10 2.30 0 5 3 32.00 2.00 -1 -5 -3 360.96 20.80 1 5 3 370.86 20.50 1 5 3 350.76 20.80 -2 -5 -3 17.70 1.50 2 5 3 15.70 1.50 -3 -5 -3 35.80 2.30 3 5 3 31.00 2.40 -4 -5 -3 8.20 1.20 4 5 3 9.80 1.30 -5 -5 -3 27.90 2.20 5 5 3 25.40 2.20 -6 -5 -3 4.30 1.20 6 5 3 4.30 1.40 -7 -5 -3 10.10 1.60 7 5 3 15.20 1.90 -8 -5 -3 10.30 1.70 8 5 3 9.10 1.80 -9 -5 -3 20.40 2.20 9 5 3 12.60 2.20 -10 -5 -3 19.80 2.50 10 5 3 15.20 2.60 -11 -5 -3 3.60 2.00 11 5 3 3.30 2.70 -12 -5 -3 0.10 2.30 12 5 3 1.70 3.10 14 -6 -3 38.60 3.80 -14 6 3 41.70 3.90 13 -6 -3 23.00 2.70 -13 6 3 26.20 2.90 12 -6 -3 0.20 1.60 -12 6 3 -0.20 1.60 11 -6 -3 9.30 1.90 -11 6 3 6.80 1.60 10 -6 -3 19.00 2.10 -10 6 3 20.20 2.10 9 -6 -3 252.27 14.90 -9 6 3 254.27 14.80 8 -6 -3 -0.40 1.00 -8 6 3 -0.50 1.00 7 -6 -3 7.80 1.20 -7 6 3 6.50 1.20 6 -6 -3 0.80 0.60 6 -6 -3 1.00 1.00 -6 6 3 0.60 0.90 5 -6 -3 12.80 1.40 5 -6 -3 10.80 1.00 -5 6 3 8.60 1.20 4 -6 -3 48.70 3.00 4 -6 -3 49.60 3.10 -4 6 3 44.50 3.00 3 -6 -3 48.80 3.00 3 -6 -3 45.60 3.10 -3 6 3 47.70 3.00 2 -6 -3 203.98 12.10 2 -6 -3 210.38 12.00 -2 6 3 208.18 11.90 1 -6 -3 24.70 1.70 1 -6 -3 20.10 1.70 -1 6 3 20.70 1.50 0 -6 -3 100.99 6.10 0 6 3 98.69 6.20 0 6 3 106.59 6.00 -1 -6 -3 177.48 10.40 1 6 3 179.68 10.50 -2 -6 -3 173.18 10.20 2 6 3 174.38 10.20 -3 -6 -3 23.20 1.90 3 6 3 22.70 2.00 -4 -6 -3 2.90 0.80 4 6 3 1.10 1.00 -5 -6 -3 26.30 2.30 5 6 3 28.10 2.40 -6 -6 -3 6.40 1.40 6 6 3 2.30 1.40 -7 -6 -3 12.90 1.80 7 6 3 14.10 2.00 -8 -6 -3 76.19 5.10 8 6 3 77.29 5.30 -9 -6 -3 34.00 3.00 9 6 3 28.80 3.10 -10 -6 -3 -1.30 1.70 10 6 3 1.40 2.10 -11 -6 -3 4.80 2.20 11 6 3 6.90 2.70 -14 7 3 17.90 3.00 13 -7 -3 14.70 2.40 -13 7 3 15.10 2.40 12 -7 -3 20.90 2.50 -12 7 3 19.90 2.50 11 -7 -3 22.70 2.60 -11 7 3 21.70 2.50 10 -7 -3 34.60 2.90 -10 7 3 33.40 2.90 9 -7 -3 25.30 2.40 -9 7 3 27.50 2.40 8 -7 -3 19.10 2.00 -8 7 3 21.10 2.00 7 -7 -3 1.30 1.10 -7 7 3 0.70 1.00 6 -7 -3 0.50 0.70 6 -7 -3 0.20 0.90 -6 7 3 0.80 0.90 5 -7 -3 3.10 0.80 5 -7 -3 1.10 0.90 -5 7 3 0.90 0.80 4 -7 -3 8.30 1.00 4 -7 -3 6.10 1.10 -4 7 3 7.90 1.00 3 -7 -3 73.39 4.30 3 -7 -3 71.79 4.40 -3 7 3 66.49 4.30 2 -7 -3 1.00 0.70 2 -7 -3 0.40 0.80 -2 7 3 1.90 0.70 1 -7 -3 10.00 1.10 -1 7 3 11.00 1.30 -1 7 3 11.00 1.00 0 -7 -3 4.50 0.90 0 7 3 4.20 0.70 0 7 3 6.40 1.10 -1 -7 -3 66.99 4.10 1 7 3 62.79 4.10 -2 -7 -3 29.80 2.10 2 7 3 27.60 2.20 -3 -7 -3 17.60 1.80 3 7 3 20.70 1.90 -4 -7 -3 13.20 1.70 4 7 3 20.10 1.90 -5 -7 -3 2.30 1.20 5 7 3 2.90 1.30 -6 -7 -3 11.80 1.70 6 7 3 14.50 2.00 -7 -7 -3 17.40 2.10 7 7 3 16.80 2.30 -8 -7 -3 -0.20 1.50 8 7 3 0.20 1.70 -9 -7 -3 11.50 2.20 9 7 3 14.90 2.70 -10 -7 -3 -0.30 1.90 10 7 3 2.10 2.40 -11 -7 -3 6.00 2.90 -14 8 3 0.00 2.40 -13 8 3 0.60 2.20 12 -8 -3 1.50 2.00 -12 8 3 0.50 1.80 11 -8 -3 19.90 2.40 -11 8 3 20.40 2.40 10 -8 -3 7.60 1.90 -10 8 3 6.40 1.70 9 -8 -3 7.00 1.70 -9 8 3 3.80 1.50 8 -8 -3 0.20 1.30 -8 8 3 0.60 1.20 7 -8 -3 13.40 1.70 -7 8 3 14.00 1.70 6 -8 -3 24.50 2.00 6 -8 -3 26.40 2.20 -6 8 3 24.80 2.10 5 -8 -3 28.20 2.20 5 -8 -3 26.80 2.10 -5 8 3 27.70 2.10 4 -8 -3 1.50 0.90 4 -8 -3 3.00 0.90 -4 8 3 2.60 0.80 3 -8 -3 44.50 2.80 3 -8 -3 39.00 2.90 -3 8 3 41.60 2.80 2 -8 -3 3.40 1.00 -2 8 3 3.10 0.80 1 -8 -3 34.80 2.60 -1 8 3 38.10 2.40 -1 8 3 36.30 2.60 0 -8 -3 20.50 1.80 0 8 3 22.20 1.90 -1 -8 -3 10.10 1.40 1 8 3 11.90 1.50 -2 -8 -3 27.70 2.40 2 8 3 34.00 2.50 -3 -8 -3 42.60 3.10 3 8 3 42.50 3.10 -4 -8 -3 34.40 2.70 4 8 3 32.00 2.80 -5 -8 -3 45.40 3.40 5 8 3 45.50 3.50 -6 -8 -3 58.39 4.00 6 8 3 51.89 4.10 -7 -8 -3 25.80 2.60 7 8 3 25.90 2.80 -8 -8 -3 15.40 2.30 8 8 3 17.10 2.60 -9 -8 -3 8.40 2.20 9 8 3 12.10 2.60 -10 -8 -3 1.20 2.30 10 8 3 2.80 2.60 -13 9 3 15.30 2.80 -12 9 3 -1.20 1.90 11 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1.50 7 -10 -3 -0.10 1.50 -7 10 3 0.30 1.30 6 -10 -3 4.70 1.50 6 -10 -3 4.20 1.30 -6 10 3 5.30 1.40 5 -10 -3 47.00 3.60 5 -10 -3 49.30 3.40 -5 10 3 48.70 3.40 4 -10 -3 3.90 1.30 4 -10 -3 5.90 1.20 -4 10 3 6.80 1.30 3 -10 -3 2.90 1.10 -3 10 3 2.90 1.20 2 -10 -3 9.50 1.40 -2 10 3 7.20 1.40 1 -10 -3 0.80 1.10 -1 10 3 1.00 1.10 0 -10 -3 0.30 1.10 0 10 3 0.00 1.10 -1 -10 -3 40.80 3.10 1 10 3 39.50 3.10 -2 -10 -3 56.99 4.00 2 10 3 55.79 4.00 -3 -10 -3 0.40 1.30 3 10 3 -1.90 1.30 -4 -10 -3 5.80 1.50 4 10 3 7.50 1.80 -5 -10 -3 -0.60 1.50 5 10 3 -0.30 1.60 -6 -10 -3 2.40 1.70 6 10 3 3.60 2.00 -7 -10 -3 -1.40 1.80 7 10 3 -0.80 2.00 -8 -10 -3 5.00 2.60 8 10 3 0.30 2.40 -12 11 3 2.30 2.50 -11 11 3 11.50 2.60 -10 11 3 2.70 1.90 -9 11 3 -2.00 1.60 8 -11 -3 1.00 1.80 -8 11 3 0.80 1.60 7 -11 -3 17.10 2.20 -7 11 3 21.70 2.40 6 -11 -3 1.00 1.40 -6 11 3 1.80 1.40 5 -11 -3 1.70 1.30 5 -11 -3 1.00 1.30 -5 11 3 0.10 1.20 4 -11 -3 3.00 1.40 -4 11 3 3.20 1.40 3 -11 -3 8.50 1.50 -3 11 3 9.10 1.60 2 -11 -3 7.50 1.50 -2 11 3 10.30 1.70 1 -11 -3 71.79 4.80 -1 11 3 73.69 4.80 0 -11 -3 51.59 3.90 0 11 3 57.59 4.00 -1 -11 -3 0.80 1.30 1 11 3 2.00 1.40 -2 -11 -3 16.60 2.10 2 11 3 18.20 2.20 -3 -11 -3 0.60 1.40 3 11 3 1.40 1.60 -4 -11 -3 1.30 1.50 4 11 3 -1.00 1.70 -5 -11 -3 40.30 3.40 5 11 3 31.70 3.40 -6 -11 -3 22.50 2.80 6 11 3 25.10 3.10 -7 -11 -3 9.10 2.70 7 11 3 13.30 2.80 -11 12 3 2.60 2.30 -10 12 3 3.40 2.10 -9 12 3 3.60 2.10 -8 12 3 1.10 1.60 -7 12 3 0.30 1.70 6 -12 -3 -0.10 1.70 -6 12 3 0.60 1.40 5 -12 -3 30.10 2.90 -5 12 3 30.80 3.00 4 -12 -3 0.30 1.30 -4 12 3 1.40 1.70 3 -12 -3 24.70 2.50 -3 12 3 25.20 2.50 2 -12 -3 120.69 7.40 -2 12 3 118.59 7.50 1 -12 -3 63.49 4.60 -1 12 3 68.59 4.60 0 -12 -3 2.40 1.50 0 12 3 8.20 1.80 -1 -12 -3 0.30 1.40 1 12 3 0.50 1.50 -2 -12 -3 4.80 1.70 2 12 3 5.60 1.80 -3 -12 -3 21.40 2.50 3 12 3 18.60 2.70 -4 -12 -3 -0.10 1.80 4 12 3 1.30 2.10 -5 -12 -3 6.40 2.20 5 12 3 2.10 2.30 6 12 3 -1.40 2.30 -10 13 3 7.00 2.30 -9 13 3 4.10 2.40 -8 13 3 13.10 2.50 5 -13 -3 19.10 2.40 -5 13 3 19.00 2.40 4 -13 -3 8.60 2.00 -4 13 3 8.30 2.10 3 -13 -3 1.50 1.50 -3 13 3 1.10 1.60 2 -13 -3 2.80 1.60 -2 13 3 1.00 1.90 1 -13 -3 0.70 1.50 -1 13 3 -0.30 1.60 0 -13 -3 3.40 1.80 0 13 3 3.70 1.80 -1 -13 -3 11.80 2.10 1 13 3 11.70 2.40 -2 -13 -3 -0.50 1.70 2 13 3 3.10 2.20 -3 -13 -3 4.30 2.10 3 13 3 1.40 2.40 -4 -13 -3 5.70 2.20 4 13 3 6.20 2.50 -9 14 3 1.90 2.70 4 -14 -3 4.90 1.80 3 -14 -3 17.70 2.40 -3 14 3 13.40 2.40 2 -14 -3 1.20 1.80 -2 14 3 2.50 1.90 1 -14 -3 -0.70 1.80 -1 14 3 -0.70 2.10 0 -14 -3 6.40 2.10 0 14 3 6.80 2.40 -1 -14 -3 16.50 2.60 1 14 3 11.60 2.50 -2 -14 -3 0.70 2.00 2 14 3 1.40 2.40 4 -15 -3 0.90 2.00 3 -15 -3 -2.10 2.00 2 -15 -3 -0.70 2.10 1 -15 -3 -0.20 2.10 -1 15 3 2.60 2.50 0 -15 -3 3.30 2.20 0 15 3 5.00 2.70 0 -16 4 0.80 2.30 1 -16 4 2.10 2.40 2 -16 4 5.40 2.30 3 -16 4 24.10 3.10 4 -16 4 -0.30 2.20 5 -16 4 1.10 2.30 -6 16 -4 18.50 2.90 6 -16 4 20.20 3.10 -3 -15 4 42.90 4.30 -2 -15 4 6.10 2.30 -1 -15 4 12.20 2.50 0 -15 4 2.50 1.90 1 -15 4 3.60 2.00 2 -15 4 4.60 2.10 3 -15 4 1.40 1.90 -4 15 -4 2.30 1.80 4 -15 4 2.60 2.10 5 -15 4 27.30 3.10 -6 15 -4 -0.70 1.90 6 -15 4 -1.00 2.00 -7 15 -4 0.10 2.10 7 -15 4 -1.20 2.10 -8 15 -4 -0.60 2.30 8 -15 4 -1.00 2.20 -6 -14 4 1.20 2.60 -5 -14 4 7.10 2.50 -4 -14 4 10.90 2.30 -3 -14 4 5.00 2.10 -2 -14 4 1.20 1.90 -1 -14 4 7.90 2.00 0 -14 4 42.10 3.70 1 -14 4 10.70 2.10 2 -14 4 15.30 2.20 -3 14 -4 16.20 2.10 3 -14 4 16.90 2.40 -4 14 -4 1.60 1.60 4 -14 4 2.90 1.80 -5 14 -4 41.90 3.50 5 -14 4 32.70 3.40 -6 14 -4 0.60 1.80 6 -14 4 0.70 1.70 -7 14 -4 -0.40 1.80 7 -14 4 -0.80 1.80 -8 14 -4 6.90 2.30 8 -14 4 5.30 2.20 -9 14 -4 -0.80 2.30 9 -14 4 2.10 2.10 7 13 -4 42.20 4.20 -7 -13 4 38.20 3.90 6 13 -4 7.10 2.40 -6 -13 4 8.20 2.60 -5 -13 4 -0.60 1.80 -4 -13 4 8.00 2.10 -3 -13 4 12.20 2.10 -2 -13 4 15.50 2.10 -1 -13 4 12.50 2.00 0 -13 4 1.10 1.50 1 -13 4 6.10 1.60 -2 13 -4 22.60 2.20 2 -13 4 19.00 2.40 -3 13 -4 0.80 1.50 3 -13 4 0.60 1.50 -4 13 -4 2.20 1.60 4 -13 4 -0.60 1.40 -5 13 -4 20.20 2.20 5 -13 4 15.00 2.20 -6 13 -4 0.70 1.50 6 -13 4 0.70 1.60 -7 13 -4 0.30 1.70 7 -13 4 1.40 1.60 -8 13 -4 0.20 1.70 8 -13 4 2.70 2.00 -9 13 -4 1.00 2.00 9 -13 4 2.50 2.20 -10 13 -4 7.50 2.50 8 12 -4 7.80 2.70 -8 -12 4 5.50 2.30 7 12 -4 0.00 2.10 -7 -12 4 1.10 2.00 6 12 -4 13.30 2.40 -6 -12 4 21.10 2.50 5 12 -4 -0.60 1.90 -5 -12 4 -0.20 1.60 4 12 -4 40.30 3.50 -4 -12 4 38.60 3.30 -3 -12 4 46.40 3.60 -2 -12 4 2.80 1.40 -1 -12 4 1.90 1.40 0 12 -4 12.90 1.80 0 -12 4 11.90 1.70 -1 12 -4 85.49 5.40 1 -12 4 82.99 5.50 -2 12 -4 33.40 2.80 2 -12 4 29.40 2.80 -3 12 -4 4.50 1.30 3 -12 4 6.30 1.50 -4 12 -4 15.10 1.80 4 -12 4 13.90 2.00 -5 12 -4 -1.20 1.20 5 -12 4 -0.70 1.40 -6 12 -4 20.30 2.30 6 -12 4 19.20 2.20 -7 12 -4 51.29 3.90 7 -12 4 53.19 3.90 -8 12 -4 0.60 1.50 8 -12 4 0.70 1.80 -9 12 -4 -1.10 1.70 9 -12 4 -0.10 1.60 -10 12 -4 27.10 3.00 10 -12 4 30.20 2.90 -11 12 -4 0.00 2.10 9 11 -4 -2.00 2.40 -9 -11 4 1.90 2.50 8 11 -4 -0.80 2.20 -8 -11 4 0.20 1.80 7 11 -4 1.70 2.00 -7 -11 4 2.10 1.90 6 11 -4 4.00 1.80 -6 -11 4 2.10 1.60 5 11 -4 4.40 1.70 -5 -11 4 7.20 1.70 4 11 -4 20.50 2.20 -4 -11 4 14.40 2.00 3 11 -4 0.10 1.20 -3 -11 4 -0.30 1.20 2 11 -4 8.90 1.50 -2 -11 4 9.90 1.60 1 11 -4 26.00 2.10 -1 -11 4 17.40 2.10 0 11 -4 160.58 9.50 0 -11 4 159.08 9.60 -1 11 -4 18.50 1.80 1 -11 4 17.90 2.00 -2 11 -4 36.60 2.80 2 -11 4 36.30 2.90 -3 11 -4 15.60 1.80 3 -11 4 16.60 1.90 -4 11 -4 0.90 1.20 4 -11 4 -0.20 1.10 -5 11 -4 17.00 2.00 5 -11 4 16.90 2.00 -6 11 -4 8.70 1.60 6 -11 4 11.30 1.60 -7 11 -4 6.10 1.60 7 -11 4 8.30 1.60 -8 11 -4 24.00 2.50 8 -11 4 21.10 2.30 -9 11 -4 4.50 1.70 9 -11 4 1.30 1.50 10 -11 4 26.40 2.80 -11 11 -4 5.10 2.00 -12 11 -4 0.70 2.20 10 10 -4 0.50 2.70 9 10 -4 1.70 2.20 -9 -10 4 0.90 2.10 8 10 -4 6.50 2.20 -8 -10 4 9.80 2.10 7 10 -4 2.20 1.80 -7 -10 4 2.00 1.70 6 10 -4 71.39 5.00 -6 -10 4 72.29 4.90 5 10 -4 9.40 1.70 -5 -10 4 4.90 1.50 4 10 -4 0.10 1.40 -4 -10 4 2.80 1.30 3 10 -4 38.00 3.00 -3 -10 4 47.90 3.20 2 10 -4 88.19 5.40 2 10 -4 84.09 5.50 -2 -10 4 93.29 5.60 1 10 -4 3.70 1.00 1 10 -4 0.70 1.00 -1 -10 4 2.90 1.10 0 10 -4 5.90 1.10 0 -10 4 8.00 1.30 1 -10 4 153.18 9.20 -2 10 -4 26.30 2.20 2 -10 4 30.40 2.40 -3 10 -4 8.90 1.30 3 -10 4 5.90 1.20 -4 10 -4 10.80 1.50 4 -10 4 10.90 1.50 -5 10 -4 0.30 1.00 5 -10 4 0.50 1.10 -6 10 -4 -0.70 1.10 6 -10 4 0.70 1.10 -7 10 -4 -0.50 1.20 7 -10 4 0.40 1.20 -8 10 -4 4.50 1.40 8 -10 4 2.10 1.30 -9 10 -4 -0.60 1.40 9 -10 4 0.10 1.60 -10 10 -4 4.80 1.70 10 -10 4 5.00 1.60 -11 10 -4 61.19 4.60 -12 10 -4 6.50 2.20 11 9 -4 -1.60 2.80 10 9 -4 35.70 3.70 9 9 -4 1.40 2.00 -9 -9 4 0.70 1.80 8 9 -4 29.40 3.20 -8 -9 4 32.00 3.10 7 9 -4 84.99 5.70 -7 -9 4 83.99 5.50 6 9 -4 12.00 1.90 -6 -9 4 11.40 1.70 5 9 -4 14.00 1.80 -5 -9 4 12.80 1.70 4 9 -4 83.29 5.60 -4 -9 4 93.79 5.60 3 9 -4 34.90 2.50 3 9 -4 32.10 2.50 -3 -9 4 37.70 2.70 2 9 -4 79.59 4.80 2 9 -4 78.19 4.80 -2 -9 4 73.69 4.90 1 9 -4 1.30 0.80 1 9 -4 0.90 0.80 -1 -9 4 1.80 1.00 0 9 -4 47.40 3.00 0 9 -4 42.00 3.00 0 -9 4 50.19 3.20 -1 9 -4 23.60 1.90 -1 9 -4 21.60 1.80 1 -9 4 23.00 2.00 -2 9 -4 9.40 1.20 2 -9 4 8.50 1.30 -3 9 -4 14.00 1.60 3 -9 4 17.90 1.70 -4 9 -4 108.99 6.90 4 -9 4 116.89 6.90 -5 9 -4 42.10 3.00 5 -9 4 44.00 3.10 -6 9 -4 97.49 5.80 6 -9 4 88.29 5.80 -7 9 -4 11.20 1.60 7 -9 4 13.00 1.60 -8 9 -4 9.00 1.60 8 -9 4 9.60 1.50 -9 9 -4 5.50 1.60 9 -9 4 7.30 1.50 -10 9 -4 2.20 1.50 10 -9 4 2.90 1.60 -11 9 -4 3.10 1.70 11 -9 4 3.30 1.60 -12 9 -4 5.90 2.10 -13 9 -4 -0.50 2.40 11 8 -4 -1.10 2.20 10 8 -4 15.40 2.60 9 8 -4 -2.00 1.60 8 8 -4 7.70 1.80 -8 -8 4 6.30 1.70 7 8 -4 25.40 2.60 -7 -8 4 27.80 2.40 6 8 -4 77.29 5.00 -6 -8 4 76.69 4.90 5 8 -4 4.20 1.30 5 8 -4 8.90 1.50 -5 -8 4 7.50 1.30 4 8 -4 52.29 3.50 4 8 -4 47.80 3.30 -4 -8 4 55.49 3.50 3 8 -4 66.99 4.30 3 8 -4 67.59 4.20 -3 -8 4 71.69 4.40 2 8 -4 14.30 1.30 2 8 -4 13.90 1.40 -2 -8 4 14.20 1.50 1 8 -4 59.39 3.50 1 8 -4 54.59 3.40 -1 -8 4 52.59 3.50 0 8 -4 75.59 4.30 0 8 -4 66.99 4.40 0 -8 4 73.09 4.50 -1 8 -4 32.00 1.90 -1 8 -4 29.40 2.10 1 -8 4 22.10 2.10 -2 8 -4 0.20 0.70 -2 8 -4 1.30 0.60 2 -8 4 0.40 0.60 -3 8 -4 47.00 3.00 3 -8 4 41.20 3.00 -4 8 -4 8.40 1.10 4 -8 4 6.50 1.10 -5 8 -4 -0.30 0.90 5 -8 4 0.10 0.90 -6 8 -4 89.79 5.50 6 -8 4 88.59 5.50 -7 8 -4 50.49 3.60 7 -8 4 55.99 3.60 -8 8 -4 74.39 5.00 8 -8 4 80.19 5.00 -9 8 -4 79.89 5.30 9 -8 4 83.59 5.20 -10 8 -4 19.70 2.20 10 -8 4 18.20 2.10 -11 8 -4 6.00 1.80 11 -8 4 8.90 1.80 -12 8 -4 8.90 2.30 -13 8 -4 35.90 3.70 12 7 -4 2.40 2.40 11 7 -4 -0.30 2.10 10 7 -4 3.30 1.90 9 7 -4 32.50 3.10 8 7 -4 31.30 3.00 -8 -7 4 39.30 2.90 7 7 -4 9.40 1.60 -7 -7 4 8.20 1.40 6 7 -4 12.40 1.70 -6 -7 4 13.60 1.40 -6 -7 4 15.70 1.50 5 7 -4 0.60 1.10 5 7 -4 1.80 0.90 -5 -7 4 1.20 0.90 4 7 -4 7.70 1.20 4 7 -4 7.10 1.00 -4 -7 4 8.70 1.10 3 7 -4 2.60 0.90 3 7 -4 1.50 0.80 -3 -7 4 1.00 0.80 2 7 -4 104.29 6.20 2 7 -4 108.99 6.20 -2 -7 4 100.89 6.30 1 7 -4 3.50 0.70 1 7 -4 3.00 0.70 -1 -7 4 2.50 0.80 0 7 -4 24.60 1.60 0 7 -4 18.20 1.70 0 -7 4 22.60 1.70 -1 7 -4 17.10 1.60 -1 7 -4 20.80 1.30 1 -7 4 21.50 1.60 -2 7 -4 21.10 1.70 -2 7 -4 23.90 1.40 2 -7 4 22.30 1.80 -3 7 -4 54.19 3.50 3 -7 4 54.79 3.50 -4 7 -4 6.60 1.10 4 -7 4 8.60 1.00 -5 7 -4 28.10 2.20 5 -7 4 32.40 2.30 -6 7 -4 88.39 5.30 6 -7 4 83.69 5.30 -7 7 -4 2.20 1.00 7 -7 4 1.30 1.00 -8 7 -4 38.90 2.90 8 -7 4 38.20 2.90 -9 7 -4 162.78 9.80 9 -7 4 164.68 9.80 -10 7 -4 13.60 1.90 10 -7 4 11.80 1.80 -11 7 -4 1.80 1.50 11 -7 4 1.50 1.40 -12 7 -4 0.10 1.70 -13 7 -4 3.90 2.10 -14 7 -4 8.00 2.50 12 6 -4 2.80 2.40 11 6 -4 11.10 2.30 10 6 -4 -0.70 1.60 9 6 -4 -0.80 1.40 8 6 -4 30.20 2.70 -8 -6 4 32.10 2.60 7 6 -4 56.59 3.80 -7 -6 4 52.29 3.50 -7 -6 4 53.69 3.50 6 6 -4 21.70 2.10 -6 -6 4 24.40 1.90 -6 -6 4 23.50 1.70 5 6 -4 1.50 0.70 5 6 -4 1.90 0.90 -5 -6 4 2.90 0.80 4 6 -4 57.09 3.60 4 6 -4 56.09 3.60 -4 -6 4 57.69 3.60 3 6 -4 501.45 28.30 3 6 -4 481.75 28.30 -3 -6 4 506.05 28.40 2 6 -4 192.98 11.40 2 6 -4 200.78 11.40 -2 -6 4 197.98 11.40 1 6 -4 102.39 6.10 1 6 -4 105.19 6.00 -1 -6 4 98.49 6.10 0 6 -4 -0.10 0.50 0 6 -4 0.90 0.60 0 -6 4 0.80 0.60 -1 6 -4 3.40 0.40 -1 6 -4 3.60 0.60 1 -6 4 2.80 0.70 -2 6 -4 101.09 6.00 -2 6 -4 104.09 6.20 2 -6 4 114.79 6.30 -3 6 -4 158.78 9.60 3 -6 4 168.88 9.60 -4 6 -4 31.90 2.50 4 -6 4 38.40 2.20 4 -6 4 37.50 2.50 -5 6 -4 14.30 1.50 5 -6 4 17.80 1.50 -6 6 -4 14.70 1.40 6 -6 4 12.50 1.30 -7 6 -4 31.60 2.40 7 -6 4 30.20 2.40 -8 6 -4 27.30 2.20 8 -6 4 24.60 2.30 -9 6 -4 1.60 1.20 9 -6 4 1.30 1.20 -10 6 -4 68.89 4.60 10 -6 4 69.39 4.70 -11 6 -4 7.50 1.70 11 -6 4 12.50 1.90 -12 6 -4 -1.80 1.80 -13 6 -4 15.40 2.40 -14 6 -4 4.20 2.20 13 5 -4 1.30 2.40 12 5 -4 8.80 2.30 11 5 -4 34.60 3.30 10 5 -4 -1.20 1.50 9 5 -4 -0.20 1.30 8 5 -4 134.69 8.30 -8 -5 4 136.29 8.10 -8 -5 4 138.59 8.10 7 5 -4 21.90 2.00 -7 -5 4 19.80 1.70 -7 -5 4 16.60 1.70 6 5 -4 123.89 7.20 -6 -5 4 115.39 7.00 -6 -5 4 116.19 7.00 5 5 -4 6.20 1.10 -5 -5 4 6.50 0.90 -5 -5 4 7.40 1.00 4 5 -4 39.20 2.70 4 5 -4 50.39 2.80 -4 -5 4 39.90 2.80 3 5 -4 66.39 4.00 3 5 -4 65.99 4.00 -3 -5 4 66.59 4.00 2 5 -4 49.00 3.10 2 5 -4 54.99 3.10 -2 -5 4 45.50 3.10 1 5 -4 178.88 10.40 1 5 -4 178.38 10.30 -1 -5 4 179.48 10.40 0 5 -4 3.70 0.50 0 5 -4 3.90 0.70 0 -5 4 2.80 0.70 -1 5 -4 7.00 0.80 -1 5 -4 7.10 0.60 1 -5 4 9.10 0.90 -2 5 -4 55.19 3.60 2 -5 4 61.69 3.60 -3 5 -4 178.18 10.20 3 -5 4 174.38 10.20 -4 5 -4 540.15 31.30 4 -5 4 559.54 31.10 4 -5 4 541.05 31.30 -5 5 -4 32.40 2.50 5 -5 4 38.70 2.50 5 -5 4 38.10 2.30 -6 5 -4 1.50 0.80 6 -5 4 1.30 0.80 6 -5 4 3.20 0.70 -7 5 -4 171.28 10.20 7 -5 4 175.28 10.20 -8 5 -4 237.38 13.90 8 -5 4 239.38 13.90 -9 5 -4 54.69 3.90 9 -5 4 62.49 4.00 -10 5 -4 0.80 1.20 10 -5 4 0.40 1.30 -11 5 -4 0.60 1.50 11 -5 4 0.10 1.20 -12 5 -4 43.50 3.50 -13 5 -4 7.10 2.30 13 4 -4 -1.90 2.20 12 4 -4 3.20 2.00 11 4 -4 24.00 2.70 10 4 -4 2.30 1.50 9 4 -4 32.40 2.90 -9 -4 4 36.00 2.60 8 4 -4 -1.50 1.10 -8 -4 4 0.20 0.90 -8 -4 4 0.20 0.80 7 4 -4 25.10 2.10 -7 -4 4 24.50 1.80 -7 -4 4 20.20 1.80 6 4 -4 5.10 1.10 -6 -4 4 5.00 0.90 -6 -4 4 6.20 0.90 5 4 -4 25.60 2.00 -5 -4 4 27.50 1.90 -5 -4 4 28.80 1.90 4 4 -4 16.40 1.40 4 4 -4 17.30 1.30 -4 -4 4 14.50 1.20 3 4 -4 11.40 1.10 3 4 -4 10.30 1.00 -3 -4 4 10.90 1.00 2 4 -4 432.06 24.40 2 4 -4 436.36 24.40 -2 -4 4 414.86 24.40 1 4 -4 3.40 0.50 1 4 -4 0.90 0.50 -1 -4 4 1.70 0.50 0 4 -4 5.60 0.60 0 4 -4 8.10 0.80 0 -4 4 5.60 0.70 -1 4 -4 302.87 17.10 -1 4 -4 298.07 17.30 1 -4 4 303.97 17.30 -2 4 -4 110.89 6.60 2 -4 4 113.49 6.60 -3 4 -4 219.38 12.80 3 -4 4 217.88 12.60 3 -4 4 228.88 12.80 -4 4 -4 -0.30 0.60 4 -4 4 -0.40 0.50 4 -4 4 0.10 0.40 -5 4 -4 26.50 1.90 5 -4 4 26.00 1.90 5 -4 4 26.60 1.70 -6 4 -4 37.00 2.50 6 -4 4 37.30 2.50 6 -4 4 38.40 2.40 -7 4 -4 6.40 1.10 7 -4 4 8.10 1.00 7 -4 4 6.40 1.00 -8 4 -4 91.19 5.80 8 -4 4 97.99 5.70 8 -4 4 93.59 5.80 -9 4 -4 96.09 6.10 9 -4 4 99.99 6.10 -10 4 -4 0.60 1.30 10 -4 4 -0.30 1.10 -11 4 -4 9.30 1.70 11 -4 4 12.50 1.80 -12 4 -4 4.30 1.80 12 -4 4 0.40 1.60 14 3 -4 9.80 2.80 13 3 -4 1.90 2.30 12 3 -4 0.20 1.80 11 3 -4 3.00 1.60 -11 -3 4 1.70 1.40 10 3 -4 10.00 1.70 -10 -3 4 8.70 1.50 9 3 -4 2.20 1.20 -9 -3 4 2.70 1.10 8 3 -4 2.30 1.20 -8 -3 4 3.10 1.00 7 3 -4 61.39 3.90 -7 -3 4 59.09 3.70 -7 -3 4 61.69 3.80 6 3 -4 4.60 1.00 -6 -3 4 9.10 1.00 -6 -3 4 7.30 0.90 5 3 -4 43.90 2.80 -5 -3 4 45.40 2.70 -5 -3 4 39.70 2.60 4 3 -4 433.76 25.10 -4 -3 4 434.46 25.00 -4 -3 4 448.16 25.00 3 3 -4 7.30 0.80 3 3 -4 6.90 0.80 -3 -3 4 6.20 0.70 2 3 -4 134.49 7.70 2 3 -4 126.69 7.70 -2 -3 4 134.89 7.60 1 3 -4 52.69 3.10 1 3 -4 51.29 3.20 -1 -3 4 51.99 3.10 0 3 -4 617.24 34.10 0 3 -4 585.74 34.20 0 -3 4 598.34 34.20 -1 3 -4 26.50 1.50 1 -3 4 22.40 1.70 -2 3 -4 623.44 34.70 2 -3 4 617.94 34.60 2 -3 4 588.44 34.70 -3 3 -4 6.40 0.80 3 -3 4 6.10 0.50 3 -3 4 5.10 0.70 -4 3 -4 123.69 7.10 4 -3 4 123.19 7.00 4 -3 4 117.99 7.10 -5 3 -4 142.49 8.20 -5 3 -4 138.79 8.20 5 -3 4 137.39 8.10 -6 3 -4 80.89 5.00 -6 3 -4 81.09 5.00 6 -3 4 84.69 4.90 -7 3 -4 2.90 0.90 -7 3 -4 2.30 0.90 7 -3 4 1.80 0.80 -8 3 -4 434.06 25.30 -8 3 -4 435.26 25.30 8 -3 4 452.25 25.30 -9 3 -4 74.39 4.80 -9 3 -4 74.99 4.90 9 -3 4 75.69 4.80 -10 3 -4 2.70 1.30 -10 3 -4 3.30 1.30 10 -3 4 1.50 1.40 -11 3 -4 0.10 1.50 -11 3 -4 -0.30 1.20 12 -3 4 2.60 1.50 14 2 -4 1.90 2.20 13 2 -4 32.60 3.50 12 2 -4 -0.20 1.60 -12 -2 4 1.00 1.40 11 2 -4 34.00 2.90 -11 -2 4 29.00 2.80 10 2 -4 5.70 1.50 -10 -2 4 4.80 1.30 9 2 -4 209.28 12.10 -9 -2 4 201.18 12.00 8 2 -4 20.70 1.90 -8 -2 4 20.10 1.70 7 2 -4 63.89 4.20 -7 -2 4 66.79 4.00 -7 -2 4 69.49 4.10 6 2 -4 0.30 0.70 -6 -2 4 0.70 0.50 -6 -2 4 -0.40 0.60 5 2 -4 5.30 0.90 -5 -2 4 6.40 0.70 -5 -2 4 6.70 0.80 4 2 -4 170.68 9.80 -4 -2 4 171.58 9.60 -4 -2 4 161.58 9.70 3 2 -4 0.80 0.50 3 2 -4 0.50 0.50 -3 -2 4 0.50 0.40 2 2 -4 133.19 7.90 2 2 -4 137.39 7.80 -2 -2 4 135.89 7.80 1 2 -4 0.80 0.50 1 2 -4 1.00 0.40 -1 -2 4 0.90 0.30 0 2 -4 0.60 0.30 0 2 -4 1.10 0.40 0 -2 4 0.30 0.40 -1 2 -4 233.48 13.50 -1 2 -4 242.48 13.40 1 -2 4 228.98 13.50 -2 2 -4 446.16 25.40 -2 2 -4 433.76 25.30 2 -2 4 453.95 25.30 -3 2 -4 103.79 5.90 -3 2 -4 99.79 5.90 3 -2 4 99.69 5.80 -4 2 -4 98.39 5.50 -4 2 -4 90.89 5.50 4 -2 4 90.09 5.40 -5 2 -4 3.70 0.80 -5 2 -4 5.90 0.80 5 -2 4 5.50 0.80 -6 2 -4 68.49 4.00 -6 2 -4 66.99 4.10 6 -2 4 62.79 4.00 -7 2 -4 0.40 0.80 -7 2 -4 -0.30 0.70 7 -2 4 0.00 0.90 -8 2 -4 21.70 1.80 -8 2 -4 18.60 1.70 8 -2 4 18.40 1.90 -9 2 -4 18.40 1.90 -9 2 -4 21.50 2.00 9 -2 4 19.40 2.00 -10 2 -4 0.30 1.20 -10 2 -4 -0.90 1.20 10 -2 4 0.90 1.30 -11 2 -4 -0.70 1.50 11 -2 4 -0.20 1.50 -12 2 -4 10.40 1.80 14 1 -4 -1.40 2.20 13 1 -4 11.40 2.20 -13 -1 4 6.40 2.00 12 1 -4 0.40 1.40 -12 -1 4 0.00 1.40 11 1 -4 0.70 1.30 -11 -1 4 0.60 1.20 10 1 -4 123.09 7.60 -10 -1 4 124.39 7.50 9 1 -4 0.10 1.00 -9 -1 4 -0.50 0.90 8 1 -4 42.10 3.10 -8 -1 4 50.09 3.10 7 1 -4 164.88 10.00 -7 -1 4 173.18 9.90 -7 -1 4 170.28 9.70 6 1 -4 26.50 1.90 -6 -1 4 24.60 1.60 -6 -1 4 24.40 1.80 5 1 -4 117.99 7.30 -5 -1 4 118.99 7.20 -5 -1 4 129.49 7.10 4 1 -4 9.30 1.00 -4 -1 4 9.00 0.70 -4 -1 4 8.20 0.90 3 1 -4 265.77 14.80 -3 -1 4 257.07 14.70 -3 -1 4 250.67 14.80 2 1 -4 72.19 4.10 2 1 -4 66.99 4.10 -2 -1 4 68.99 4.00 1 1 -4 2480.65 145.49 1 1 -4 2562.54 145.49 -1 -1 4 2660.93 145.49 0 1 -4 206.98 11.90 0 1 -4 210.98 12.00 -1 1 -4 10.30 0.80 -1 1 -4 8.70 0.80 -1 1 -4 10.60 0.90 -2 1 -4 32.60 2.10 -2 1 -4 33.60 2.10 2 -1 4 34.50 2.10 -3 1 -4 5.30 0.70 -3 1 -4 4.90 0.60 3 -1 4 4.40 0.60 -4 1 -4 70.79 4.40 -4 1 -4 74.39 4.30 4 -1 4 71.59 4.30 -5 1 -4 36.60 2.60 -5 1 -4 40.80 2.50 5 -1 4 39.00 2.50 -6 1 -4 6.10 1.00 -6 1 -4 7.40 0.90 6 -1 4 7.80 1.00 -7 1 -4 121.59 7.10 -7 1 -4 120.19 7.00 7 -1 4 111.29 7.00 -8 1 -4 172.28 10.40 -8 1 -4 182.98 10.60 8 -1 4 183.78 10.60 -9 1 -4 27.40 2.10 -9 1 -4 25.20 2.20 9 -1 4 22.50 2.30 -10 1 -4 -0.70 1.20 10 -1 4 -0.90 1.30 -11 1 -4 35.50 3.00 11 -1 4 37.60 3.40 -12 1 -4 0.50 1.60 12 -1 4 -0.20 1.90 14 0 -4 0.10 2.10 -14 0 4 -1.30 2.10 13 0 -4 10.00 2.10 -13 0 4 8.60 2.10 12 0 -4 -0.60 1.70 -12 0 4 -0.60 1.50 11 0 -4 68.59 4.80 -11 0 4 71.89 4.70 10 0 -4 1.40 1.20 -10 0 4 -0.60 1.00 9 0 -4 41.50 3.20 -9 0 4 48.70 3.20 8 0 -4 1.60 0.90 -8 0 4 1.10 0.80 7 0 -4 2.90 0.90 -7 0 4 4.00 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14.70 1.60 -8 8 -5 3.20 1.30 8 -8 5 2.60 1.40 -9 8 -5 17.90 2.00 9 -8 5 15.60 1.90 -10 8 -5 144.79 9.00 10 -8 5 147.99 9.00 -11 8 -5 17.30 2.20 11 -8 5 16.40 2.10 -12 8 -5 7.30 2.10 -13 8 -5 0.90 2.40 12 7 -5 0.10 2.40 11 7 -5 38.30 3.80 10 7 -5 3.10 1.90 9 7 -5 9.00 1.90 8 7 -5 102.79 6.80 -8 -7 5 110.29 6.60 7 7 -5 31.40 2.80 -7 -7 5 37.30 2.50 -7 -7 5 35.60 2.70 6 7 -5 252.67 15.20 -6 -7 5 266.17 15.10 -6 -7 5 261.97 15.10 5 7 -5 9.80 1.20 5 7 -5 9.70 1.40 -5 -7 5 7.70 1.20 4 7 -5 3.80 1.00 4 7 -5 3.90 1.00 -4 -7 5 4.00 1.00 3 7 -5 11.70 1.20 3 7 -5 12.00 1.20 -3 -7 5 10.50 1.30 2 7 -5 10.60 1.10 2 7 -5 6.70 1.00 -2 -7 5 7.00 1.00 1 7 -5 378.86 21.60 1 7 -5 383.06 21.50 -1 -7 5 364.86 21.60 0 7 -5 69.39 4.10 0 7 -5 67.79 4.00 0 -7 5 62.89 4.20 -1 7 -5 24.70 1.90 -1 7 -5 27.90 1.70 1 -7 5 25.00 2.00 -2 7 -5 156.38 9.10 2 -7 5 152.48 9.10 -3 7 -5 18.30 1.60 3 -7 5 17.30 1.60 -4 7 -5 0.60 0.90 4 -7 5 1.50 0.90 -5 7 -5 -0.70 0.80 5 -7 5 0.60 0.90 -6 7 -5 33.80 2.60 6 -7 5 35.00 2.50 -7 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5 -5 165.98 10.10 4 -5 5 176.88 10.10 4 -5 5 175.18 9.90 -5 5 -5 4.70 0.80 5 -5 5 4.20 0.90 -6 5 -5 28.60 2.10 6 -5 5 26.10 2.10 -7 5 -5 66.69 4.20 7 -5 5 65.89 4.20 -8 5 -5 8.20 1.30 8 -5 5 8.80 1.40 -9 5 -5 286.97 17.20 9 -5 5 306.47 17.30 -10 5 -5 29.20 2.80 10 -5 5 31.60 2.60 -11 5 -5 6.40 1.60 11 -5 5 7.00 1.70 -12 5 -5 9.20 2.10 12 -5 5 11.90 1.90 13 4 -5 0.30 2.20 12 4 -5 74.89 5.40 11 4 -5 66.19 4.80 10 4 -5 1.20 1.40 -10 -4 5 -0.50 1.30 9 4 -5 138.59 8.30 -9 -4 5 131.29 8.00 8 4 -5 59.19 3.90 -8 -4 5 55.99 3.70 7 4 -5 62.89 4.00 -7 -4 5 58.79 3.80 -7 -4 5 58.09 3.70 6 4 -5 31.50 2.20 -6 -4 5 23.70 2.00 -6 -4 5 28.70 2.00 5 4 -5 67.59 4.20 -5 -4 5 68.69 4.10 -5 -4 5 66.39 4.10 4 4 -5 21.40 1.50 4 4 -5 17.10 1.40 -4 -4 5 16.80 1.40 3 4 -5 315.97 18.00 3 4 -5 313.47 18.00 -3 -4 5 310.67 17.90 2 4 -5 1057.69 59.19 2 4 -5 1018.30 59.19 -2 -4 5 1050.89 59.19 1 4 -5 182.48 10.30 1 4 -5 183.38 10.40 -1 -4 5 174.08 10.40 0 4 -5 68.89 4.10 0 4 -5 71.69 4.00 0 -4 5 63.39 4.10 -1 4 -5 297.87 16.80 -1 4 -5 299.97 16.90 1 -4 5 287.37 16.90 -2 4 -5 7.40 0.90 2 -4 5 6.80 0.90 -3 4 -5 1.40 0.70 3 -4 5 1.10 0.30 3 -4 5 0.30 0.60 -4 4 -5 461.75 26.70 4 -4 5 481.05 26.60 4 -4 5 457.65 26.80 -5 4 -5 143.49 8.60 5 -4 5 145.39 8.40 5 -4 5 149.79 8.60 -6 4 -5 36.30 2.40 6 -4 5 33.60 2.30 6 -4 5 34.30 2.40 -7 4 -5 19.20 1.80 7 -4 5 25.80 1.90 -8 4 -5 0.40 1.00 8 -4 5 1.80 1.00 -9 4 -5 117.29 7.40 9 -4 5 129.29 7.50 -10 4 -5 -1.20 1.20 10 -4 5 0.60 1.40 -11 4 -5 1.10 1.40 11 -4 5 0.30 1.40 -12 4 -5 5.40 2.60 12 -4 5 3.10 1.60 14 3 -5 3.40 2.50 13 3 -5 0.00 1.90 12 3 -5 0.20 1.70 11 3 -5 1.00 1.40 -11 -3 5 1.80 1.30 10 3 -5 56.99 4.00 -10 -3 5 52.99 3.80 9 3 -5 43.10 3.10 -9 -3 5 38.50 2.90 8 3 -5 180.18 10.80 -8 -3 5 183.28 10.60 7 3 -5 94.19 5.80 -7 -3 5 92.79 5.60 -7 -3 5 97.39 5.70 6 3 -5 1.20 0.90 -6 -3 5 0.20 0.60 -6 -3 5 0.60 0.80 5 3 -5 49.00 3.20 -5 -3 5 47.10 3.00 -5 -3 5 51.69 3.10 4 3 -5 28.50 1.90 4 3 -5 30.20 1.90 -4 -3 5 25.30 1.80 3 3 -5 32.90 2.20 3 3 -5 34.10 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14.00 1.80 -3 11 -6 4.20 1.40 3 -11 6 3.50 1.30 -4 11 -6 0.60 1.20 4 -11 6 1.80 1.30 -5 11 -6 1.80 1.20 5 -11 6 1.50 1.30 -6 11 -6 4.10 1.50 6 -11 6 2.40 1.50 -7 11 -6 0.40 1.40 7 -11 6 -1.40 1.40 -8 11 -6 8.70 1.90 8 -11 6 7.40 1.80 -9 11 -6 10.30 2.00 9 -11 6 9.00 2.00 -10 11 -6 14.40 2.50 10 -11 6 15.70 2.40 -11 11 -6 1.90 2.10 11 -11 6 0.50 2.20 10 10 -6 1.70 2.50 9 10 -6 1.90 2.20 8 10 -6 28.00 3.00 7 10 -6 4.30 2.00 -7 -10 6 9.20 1.80 6 10 -6 11.50 1.90 -6 -10 6 9.20 1.80 5 10 -6 72.39 4.70 -5 -10 6 69.19 4.80 4 10 -6 1.80 1.40 4 10 -6 4.00 1.40 -4 -10 6 4.70 1.40 3 10 -6 0.20 1.20 -3 -10 6 0.50 1.20 2 10 -6 26.00 2.30 -2 -10 6 29.30 2.50 1 10 -6 19.50 1.90 -1 -10 6 17.60 2.00 0 10 -6 18.30 1.80 0 -10 6 20.00 2.00 -1 10 -6 28.50 2.30 1 -10 6 23.70 2.30 -2 10 -6 42.50 3.20 2 -10 6 49.60 3.30 -3 10 -6 63.09 4.20 3 -10 6 64.89 4.30 -4 10 -6 88.19 5.80 4 -10 6 97.29 5.90 -5 10 -6 11.50 1.60 5 -10 6 7.20 1.50 -6 10 -6 6.00 1.40 6 -10 6 1.20 1.30 -7 10 -6 2.40 1.30 7 -10 6 -0.80 1.30 -8 10 -6 3.00 1.40 8 -10 6 0.30 1.40 -9 10 -6 1.00 1.60 9 -10 6 4.70 1.60 -10 10 -6 5.00 2.00 10 -10 6 5.50 1.80 -11 10 -6 1.70 2.00 11 -10 6 2.30 1.90 -12 10 -6 14.10 2.60 11 9 -6 3.60 2.50 10 9 -6 19.70 2.90 9 9 -6 12.30 2.40 8 9 -6 16.60 2.30 7 9 -6 21.30 2.50 -7 -9 6 22.90 2.40 6 9 -6 69.59 4.60 -6 -9 6 63.59 4.60 5 9 -6 37.00 3.10 5 9 -6 39.10 2.90 -5 -9 6 38.40 3.10 4 9 -6 1.60 1.00 4 9 -6 2.60 1.10 -4 -9 6 2.30 1.10 3 9 -6 1.10 1.10 3 9 -6 1.90 1.20 -3 -9 6 0.40 1.00 2 9 -6 2.90 1.00 2 9 -6 4.70 1.10 -2 -9 6 4.20 1.20 1 9 -6 175.48 10.40 -1 -9 6 174.98 10.40 0 9 -6 13.60 1.60 0 -9 6 10.80 1.40 -1 9 -6 117.59 7.10 1 -9 6 116.99 7.10 -2 9 -6 0.30 0.90 2 -9 6 -0.50 0.90 -3 9 -6 14.30 1.70 3 -9 6 16.70 1.70 -4 9 -6 4.50 1.20 4 -9 6 4.10 1.20 -5 9 -6 4.50 1.30 5 -9 6 5.50 1.10 -6 9 -6 64.39 4.20 6 -9 6 59.19 4.10 -7 9 -6 0.00 1.00 7 -9 6 0.30 1.20 -8 9 -6 1.60 1.30 8 -9 6 -0.10 1.30 -9 9 -6 22.20 2.40 9 -9 6 22.10 2.30 -10 9 -6 129.39 8.10 10 -9 6 128.39 8.00 -11 9 -6 6.60 2.00 11 -9 6 5.50 1.80 -12 9 -6 0.70 2.10 12 -9 6 0.40 1.80 11 8 -6 7.10 2.80 10 8 -6 1.30 2.00 9 8 -6 -0.60 1.70 8 8 -6 2.10 1.60 7 8 -6 4.80 1.50 -7 -8 6 4.80 1.30 6 8 -6 -0.80 1.30 -6 -8 6 0.20 1.10 -6 -8 6 1.80 1.20 5 8 -6 1.90 1.10 5 8 -6 2.70 1.30 -5 -8 6 2.40 1.10 4 8 -6 0.90 0.90 4 8 -6 0.60 0.90 -4 -8 6 2.80 1.00 3 8 -6 1.60 1.00 3 8 -6 1.30 0.90 -3 -8 6 4.70 1.10 2 8 -6 3.00 1.00 2 8 -6 2.40 0.90 -2 -8 6 2.10 1.00 1 8 -6 58.89 3.60 1 8 -6 57.89 3.80 -1 -8 6 57.19 3.80 0 8 -6 25.60 2.10 0 -8 6 29.20 2.10 -1 8 -6 7.50 1.10 1 -8 6 5.50 1.10 -2 8 -6 102.09 6.00 2 -8 6 93.79 6.00 -3 8 -6 14.50 1.60 3 -8 6 16.10 1.60 -4 8 -6 24.90 2.00 4 -8 6 23.00 2.00 -5 8 -6 0.00 1.00 5 -8 6 0.80 1.00 -6 8 -6 -0.20 1.00 6 -8 6 -1.10 1.00 -7 8 -6 238.08 14.20 7 -8 6 246.68 14.20 -8 8 -6 -1.30 1.30 8 -8 6 1.10 1.20 -9 8 -6 11.50 1.80 9 -8 6 11.50 1.70 -10 8 -6 58.49 4.30 10 -8 6 60.89 4.30 -11 8 -6 2.40 1.80 11 -8 6 5.10 1.90 -12 8 -6 6.40 2.10 12 -8 6 0.30 2.00 -13 8 -6 4.90 2.60 12 7 -6 0.60 2.30 11 7 -6 22.80 3.00 10 7 -6 5.70 2.00 9 7 -6 57.39 4.30 8 7 -6 3.00 1.50 -8 -7 6 2.60 1.30 7 7 -6 6.60 1.50 -7 -7 6 9.40 1.40 -7 -7 6 10.90 1.50 6 7 -6 92.59 6.20 -6 -7 6 105.79 6.10 -6 -7 6 99.79 6.10 5 7 -6 4.10 1.00 5 7 -6 3.80 1.10 -5 -7 6 1.90 1.00 4 7 -6 0.30 0.90 4 7 -6 1.00 1.00 -4 -7 6 -0.40 0.80 3 7 -6 40.90 2.80 3 7 -6 41.00 2.80 -3 -7 6 45.10 2.90 2 7 -6 35.10 2.30 2 7 -6 35.80 2.40 -2 -7 6 29.30 2.40 1 7 -6 3.20 0.90 1 7 -6 3.00 0.70 -1 -7 6 3.40 0.90 0 7 -6 9.40 0.80 0 7 -6 6.80 1.00 0 -7 6 7.40 1.10 -1 7 -6 13.60 1.30 1 -7 6 12.50 1.30 -2 7 -6 39.90 2.80 2 -7 6 44.10 2.90 -3 7 -6 94.39 5.80 3 -7 6 98.09 5.90 -4 7 -6 25.60 2.10 4 -7 6 26.20 2.10 -5 7 -6 2.70 1.00 5 -7 6 2.70 1.00 -6 7 -6 32.10 2.50 6 -7 6 32.20 2.50 -7 7 -6 58.39 4.10 7 -7 6 65.99 4.10 -8 7 -6 38.10 2.80 8 -7 6 30.50 2.70 -9 7 -6 29.90 3.00 9 -7 6 37.40 2.80 -10 7 -6 13.20 1.90 10 -7 6 11.40 1.80 -11 7 -6 4.60 1.80 11 -7 6 2.10 1.60 -12 7 -6 28.80 3.10 12 -7 6 28.80 2.90 -13 7 -6 2.20 2.20 12 6 -6 2.20 2.30 11 6 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7 8.80 2.30 -8 14 -7 -1.60 2.20 8 -14 7 0.20 2.50 -7 -13 7 7.10 2.90 -6 -13 7 0.10 2.20 -5 -13 7 3.70 2.10 -4 -13 7 4.20 2.00 -3 -13 7 4.10 1.90 -2 -13 7 31.40 3.10 1 13 -7 66.79 4.70 -1 -13 7 62.69 4.70 0 13 -7 5.90 1.80 0 -13 7 3.20 1.70 -1 13 -7 77.39 5.10 1 -13 7 69.19 5.10 -2 13 -7 28.20 2.80 2 -13 7 29.20 2.90 -3 13 -7 9.00 2.00 3 -13 7 7.80 1.80 -4 13 -7 5.60 1.70 4 -13 7 6.60 1.80 -5 13 -7 9.40 2.00 5 -13 7 15.50 2.40 -6 13 -7 0.70 1.70 6 -13 7 -1.80 1.70 -7 13 -7 6.90 2.00 7 -13 7 6.80 2.10 -8 13 -7 -1.00 2.00 8 -13 7 0.90 2.00 -9 13 -7 1.60 2.10 9 -13 7 4.70 2.60 10 -13 7 32.70 3.80 -7 -12 7 1.10 2.00 -6 -12 7 45.20 3.90 -5 -12 7 10.30 2.10 -4 -12 7 -0.20 1.50 -3 -12 7 5.50 1.70 2 12 -7 12.30 1.80 -2 -12 7 11.60 2.00 1 12 -7 25.70 2.50 -1 -12 7 23.50 2.50 0 12 -7 7.60 1.60 0 -12 7 7.00 1.70 -1 12 -7 27.60 2.60 1 -12 7 28.90 2.80 -2 12 -7 14.10 1.90 2 -12 7 10.70 1.90 -3 12 -7 12.00 1.80 3 -12 7 7.10 1.70 -4 12 -7 -0.60 1.40 4 -12 7 0.60 1.50 -5 12 -7 1.00 1.50 5 -12 7 3.70 1.60 -6 12 -7 4.70 1.70 6 -12 7 2.80 1.60 -7 12 -7 4.40 1.70 7 -12 7 5.40 1.90 -8 12 -7 16.20 2.40 8 -12 7 17.10 2.50 -9 12 -7 -0.90 1.90 9 -12 7 0.10 1.90 -10 12 -7 0.50 2.10 10 -12 7 2.80 2.10 9 11 -7 4.70 2.80 8 11 -7 0.90 2.30 7 11 -7 2.80 2.10 -7 -11 7 1.40 2.00 -6 -11 7 41.60 3.50 -5 -11 7 53.09 4.00 -4 -11 7 0.80 1.40 3 11 -7 -0.30 1.20 -3 -11 7 0.20 1.30 2 11 -7 13.30 1.80 -2 -11 7 11.20 1.80 1 11 -7 27.20 2.40 -1 -11 7 26.40 2.50 0 11 -7 1.60 1.20 0 -11 7 0.30 1.20 -1 11 -7 2.70 1.30 1 -11 7 2.70 1.30 -2 11 -7 16.10 2.00 2 -11 7 21.30 2.10 -3 11 -7 10.90 1.70 3 -11 7 14.60 1.90 -4 11 -7 6.50 1.30 4 -11 7 4.10 1.50 -5 11 -7 3.10 1.40 5 -11 7 4.70 1.50 -6 11 -7 45.30 3.50 6 -11 7 47.80 3.60 -7 11 -7 -0.30 1.30 7 -11 7 0.40 1.50 -8 11 -7 3.50 1.80 8 -11 7 2.00 1.70 -9 11 -7 2.90 1.80 9 -11 7 1.30 2.00 -10 11 -7 57.89 4.70 10 -11 7 60.39 4.70 -11 11 -7 0.60 2.20 11 -11 7 1.70 2.40 10 10 -7 2.30 2.50 9 10 -7 0.70 2.10 8 10 -7 1.20 2.10 7 10 -7 12.10 2.10 -7 -10 7 16.60 2.30 6 10 -7 7.00 1.90 -6 -10 7 8.40 1.70 5 10 -7 7.50 1.90 5 10 -7 9.50 1.60 -5 -10 7 7.80 1.70 4 10 -7 46.30 3.40 -4 -10 7 48.80 3.50 3 10 -7 1.00 1.30 -3 -10 7 -0.10 1.20 2 10 -7 12.30 1.80 -2 -10 7 15.10 1.80 1 10 -7 14.30 1.70 -1 -10 7 14.30 1.80 0 10 -7 119.29 7.50 0 -10 7 128.59 7.60 -1 10 -7 23.90 2.30 1 -10 7 27.80 2.20 -2 10 -7 5.00 1.30 2 -10 7 5.60 1.40 -3 10 -7 -0.30 1.10 3 -10 7 1.70 1.30 -4 10 -7 63.19 4.30 4 -10 7 64.69 4.30 -5 10 -7 16.50 1.80 5 -10 7 17.00 2.00 -6 10 -7 16.00 1.90 6 -10 7 11.90 1.80 -7 10 -7 44.40 3.30 7 -10 7 41.60 3.40 -8 10 -7 2.30 1.50 8 -10 7 4.80 1.60 -9 10 -7 12.40 2.10 9 -10 7 12.90 2.10 -10 10 -7 5.60 2.00 10 -10 7 5.30 1.90 -11 10 -7 4.90 2.20 11 -10 7 3.30 2.40 11 9 -7 0.50 2.50 10 9 -7 28.00 3.30 9 9 -7 0.30 2.20 8 9 -7 0.40 1.70 7 9 -7 17.60 2.40 -7 -9 7 18.50 2.30 6 9 -7 24.30 2.30 6 9 -7 22.80 2.40 -6 -9 7 23.60 2.30 5 9 -7 35.70 2.70 5 9 -7 34.80 2.90 -5 -9 7 33.50 2.90 4 9 -7 35.30 2.80 4 9 -7 38.60 2.80 -4 -9 7 37.20 2.80 3 9 -7 60.79 4.00 -3 -9 7 61.59 4.10 2 9 -7 0.10 1.20 -2 -9 7 1.20 1.10 1 9 -7 28.20 2.20 -1 -9 7 24.50 2.30 0 9 -7 139.09 8.10 0 -9 7 128.29 8.10 -1 9 -7 1.90 1.00 1 -9 7 1.50 1.10 -2 9 -7 34.80 2.80 2 -9 7 40.00 2.80 -3 9 -7 21.80 1.90 3 -9 7 17.30 1.90 -4 9 -7 97.59 6.10 4 -9 7 98.09 6.10 -5 9 -7 1.80 1.20 5 -9 7 0.20 0.90 -6 9 -7 34.50 2.90 6 -9 7 38.50 2.90 -7 9 -7 29.00 2.70 7 -9 7 32.80 2.70 -8 9 -7 62.59 4.60 8 -9 7 71.09 4.60 -9 9 -7 -1.00 1.50 9 -9 7 0.30 1.50 -10 9 -7 3.50 1.90 10 -9 7 1.10 1.70 -11 9 -7 16.60 2.70 11 -9 7 25.30 2.80 -12 9 -7 1.90 2.30 12 -9 7 -0.30 2.00 11 8 -7 3.10 2.40 10 8 -7 23.90 2.90 9 8 -7 9.30 2.00 8 8 -7 50.99 3.90 7 8 -7 114.79 7.10 -7 -8 7 108.99 6.90 6 8 -7 0.70 1.10 6 8 -7 -0.20 1.20 -6 -8 7 -0.10 1.20 5 8 -7 24.80 2.40 5 8 -7 25.30 2.20 -5 -8 7 27.90 2.30 4 8 -7 38.40 2.90 4 8 -7 42.70 2.90 -4 -8 7 40.70 2.90 3 8 -7 43.10 3.00 3 8 -7 45.90 3.00 -3 -8 7 42.00 3.10 2 8 -7 3.30 0.90 2 8 -7 3.30 1.20 -2 -8 7 2.60 1.00 1 8 -7 0.60 0.90 -1 -8 7 0.90 1.10 0 8 -7 82.19 5.20 0 -8 7 85.69 5.20 -1 8 -7 1.20 1.00 1 -8 7 1.50 1.00 -2 8 -7 4.70 1.10 2 -8 7 8.40 1.30 -3 8 -7 7.20 1.30 3 -8 7 8.60 1.30 -4 8 -7 24.30 2.10 4 -8 7 22.20 2.10 -5 8 -7 79.99 5.20 5 -8 7 84.49 5.20 -6 8 -7 5.00 1.30 6 -8 7 4.80 1.30 -7 8 -7 21.70 2.20 7 -8 7 21.90 2.20 -8 8 -7 1.60 1.40 8 -8 7 1.80 1.30 -9 8 -7 83.09 5.90 9 -8 7 98.89 6.00 -10 8 -7 73.39 5.00 10 -8 7 69.59 4.90 -11 8 -7 14.50 2.40 11 -8 7 11.80 2.10 -12 8 -7 3.20 2.20 12 -8 7 3.70 2.10 12 7 -7 20.40 3.00 11 7 -7 2.60 2.20 10 7 -7 2.60 1.90 9 7 -7 15.10 2.20 8 7 -7 10.00 1.80 -8 -7 7 9.60 1.50 7 7 -7 224.98 13.50 -7 -7 7 230.88 13.30 6 7 -7 28.10 2.50 -6 -7 7 37.20 2.60 -6 -7 7 32.60 2.40 5 7 -7 17.80 1.70 5 7 -7 20.00 2.00 -5 -7 7 15.90 1.60 4 7 -7 6.50 1.10 4 7 -7 7.70 1.10 -4 -7 7 4.10 1.10 3 7 -7 44.10 3.10 3 7 -7 48.60 3.20 -3 -7 7 49.90 3.20 2 7 -7 5.80 1.20 2 7 -7 6.70 0.90 -2 -7 7 5.20 1.00 1 7 -7 0.10 0.60 1 7 -7 -0.30 0.90 -1 -7 7 -0.60 0.80 0 7 -7 41.10 2.80 0 -7 7 37.90 2.70 -1 7 -7 -0.20 0.80 1 -7 7 0.30 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1.80 -8 -7 8 6.20 1.60 7 7 -8 5.80 1.40 -7 -7 8 3.80 1.40 6 7 -8 4.00 1.30 6 7 -8 1.50 1.20 -6 -7 8 4.40 1.30 5 7 -8 0.20 1.00 5 7 -8 1.20 1.10 -5 -7 8 -0.50 1.10 4 7 -8 9.20 1.20 4 7 -8 8.10 1.30 -4 -7 8 6.20 1.30 3 7 -8 5.20 1.00 3 7 -8 2.10 1.00 -3 -7 8 3.80 1.00 2 7 -8 118.19 7.10 2 7 -8 116.49 6.90 -2 -7 8 114.49 7.00 1 7 -8 14.60 1.60 -1 -7 8 15.90 1.60 0 7 -8 20.30 1.90 0 -7 8 22.80 1.90 -1 7 -8 54.59 3.60 1 -7 8 54.69 3.60 -2 7 -8 0.00 0.90 2 -7 8 0.20 0.90 -3 7 -8 0.40 1.00 3 -7 8 0.10 0.90 -4 7 -8 14.20 1.70 4 -7 8 16.60 1.70 -5 7 -8 17.70 1.80 5 -7 8 16.00 1.80 -6 7 -8 6.90 1.40 6 -7 8 6.90 1.40 -7 7 -8 6.60 1.50 7 -7 8 7.60 1.50 -8 7 -8 44.70 3.50 8 -7 8 51.39 3.60 -9 7 -8 1.70 1.50 9 -7 8 4.00 1.60 -10 7 -8 5.40 2.00 10 -7 8 4.30 2.00 -11 7 -8 1.40 1.90 11 -7 8 4.50 1.90 -12 7 -8 -0.50 2.30 12 -7 8 -1.40 2.40 12 6 -8 19.90 2.90 11 6 -8 3.40 2.00 10 6 -8 10.30 2.00 -10 -6 8 12.30 2.00 9 6 -8 40.30 3.60 -9 -6 8 50.09 3.40 8 6 -8 16.80 2.00 -8 -6 8 21.90 2.10 7 6 -8 213.98 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2.30 1.00 -6 -5 8 2.50 1.00 5 5 -8 45.80 3.10 5 5 -8 44.50 3.00 -5 -5 8 43.20 2.90 4 5 -8 64.69 4.30 4 5 -8 71.29 4.40 -4 -5 8 70.79 4.20 3 5 -8 1.40 0.90 3 5 -8 1.40 0.80 -3 -5 8 0.10 0.70 2 5 -8 209.28 12.60 2 5 -8 219.08 12.50 -2 -5 8 219.68 12.60 1 5 -8 149.99 8.80 1 5 -8 156.58 8.70 -1 -5 8 139.39 8.70 0 5 -8 2.50 0.60 0 5 -8 1.70 0.70 0 -5 8 1.70 0.80 -1 5 -8 0.80 0.80 1 -5 8 0.70 0.70 -2 5 -8 0.80 0.90 2 -5 8 0.70 0.80 -3 5 -8 2.40 1.00 3 -5 8 3.30 0.90 -4 5 -8 37.50 2.70 4 -5 8 39.90 2.80 -5 5 -8 40.20 2.80 5 -5 8 39.30 2.90 -6 5 -8 22.20 2.10 6 -5 8 26.30 2.20 -7 5 -8 192.78 11.40 7 -5 8 192.28 11.40 -8 5 -8 -0.30 1.20 8 -5 8 3.40 1.30 -9 5 -8 19.90 2.10 9 -5 8 16.20 2.10 -10 5 -8 26.50 2.60 10 -5 8 26.20 2.70 11 -5 8 45.20 3.80 12 -5 8 14.80 2.80 13 4 -8 18.90 2.90 12 4 -8 3.00 2.00 -12 -4 8 1.70 1.80 11 4 -8 23.40 2.80 -11 -4 8 27.70 2.60 10 4 -8 2.80 1.50 -10 -4 8 0.50 1.30 9 4 -8 24.70 2.50 -9 -4 8 28.40 2.60 8 4 -8 95.59 6.10 -8 -4 8 99.19 6.10 7 4 -8 83.19 5.20 -7 -4 8 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26.60 2.90 2 12 -9 15.00 2.20 -2 -12 9 17.30 2.20 1 12 -9 58.49 4.20 -1 -12 9 54.89 4.30 0 12 -9 35.00 3.10 0 -12 9 34.30 3.30 -1 12 -9 11.60 2.10 1 -12 9 9.80 1.90 -2 12 -9 0.10 1.70 2 -12 9 1.60 1.60 -3 12 -9 9.00 1.80 3 -12 9 5.90 1.80 -4 12 -9 12.40 2.00 4 -12 9 9.70 2.10 -5 12 -9 2.00 1.70 5 -12 9 1.00 1.80 -6 12 -9 5.50 1.90 6 -12 9 4.30 1.90 -7 12 -9 3.40 2.00 7 -12 9 3.70 2.00 -8 12 -9 -0.60 1.90 8 -12 9 1.90 2.10 -9 12 -9 21.30 3.00 9 -12 9 24.30 3.10 5 11 -9 1.20 1.60 -5 -11 9 0.80 1.80 4 11 -9 80.99 5.50 -4 -11 9 79.09 5.40 3 11 -9 7.40 1.70 -3 -11 9 4.80 1.90 2 11 -9 0.30 1.40 -2 -11 9 -0.20 1.50 1 11 -9 1.60 1.40 -1 -11 9 1.80 1.50 0 11 -9 1.30 1.40 0 -11 9 0.20 1.40 -1 11 -9 26.50 2.60 1 -11 9 28.40 2.70 -2 11 -9 17.40 2.10 2 -11 9 18.20 2.10 -3 11 -9 66.09 4.90 3 -11 9 81.69 5.10 -4 11 -9 0.70 1.40 4 -11 9 0.00 1.40 -5 11 -9 14.00 2.00 5 -11 9 12.50 2.00 -6 11 -9 2.60 1.60 6 -11 9 3.60 1.70 -7 11 -9 20.30 2.40 7 -11 9 19.80 2.60 -8 11 -9 -0.30 1.80 8 -11 9 2.80 1.90 -9 11 -9 2.90 2.00 9 -11 9 -0.10 2.00 -10 11 -9 1.60 2.20 10 -11 9 -0.30 2.10 9 10 -9 22.90 2.90 6 10 -9 16.60 2.10 5 10 -9 6.20 1.80 -5 -10 9 5.10 1.60 4 10 -9 7.40 1.70 -4 -10 9 10.70 1.90 3 10 -9 74.29 5.00 -3 -10 9 77.69 5.10 2 10 -9 28.50 2.40 -2 -10 9 20.60 2.30 1 10 -9 37.50 3.00 -1 -10 9 35.70 3.00 0 10 -9 2.10 1.30 0 -10 9 -2.00 1.20 -1 10 -9 83.99 5.60 1 -10 9 89.09 5.60 -2 10 -9 31.40 2.90 2 -10 9 42.50 2.90 -3 10 -9 1.60 1.30 3 -10 9 2.20 1.30 -4 10 -9 -0.80 1.30 4 -10 9 -0.20 1.30 -5 10 -9 0.10 1.30 5 -10 9 1.40 1.40 -6 10 -9 13.00 2.00 6 -10 9 11.80 1.90 -7 10 -9 33.30 3.00 7 -10 9 30.30 3.00 -8 10 -9 9.70 2.00 8 -10 9 15.80 2.20 -9 10 -9 2.60 1.90 9 -10 9 2.00 1.90 -10 10 -9 1.60 2.10 10 -10 9 0.50 2.00 10 9 -9 2.10 2.20 9 9 -9 23.20 2.80 8 9 -9 3.70 1.80 7 9 -9 17.80 2.10 -7 -9 9 13.50 2.10 6 9 -9 12.50 1.90 5 9 -9 7.90 1.70 -5 -9 9 8.40 1.70 4 9 -9 11.50 1.90 -4 -9 9 15.10 1.90 3 9 -9 33.40 2.70 -3 -9 9 28.60 2.80 2 9 -9 4.90 1.40 -2 -9 9 5.60 1.40 1 9 -9 12.50 1.80 -1 -9 9 20.00 1.90 0 9 -9 11.40 1.60 0 -9 9 7.00 1.50 -1 9 -9 88.89 5.60 1 -9 9 84.39 5.50 -2 9 -9 80.39 5.30 2 -9 9 83.59 5.30 -3 9 -9 42.60 3.30 3 -9 9 49.99 3.50 -4 9 -9 5.30 1.40 4 -9 9 4.30 1.40 -5 9 -9 -0.40 1.30 5 -9 9 1.30 1.30 -6 9 -9 -0.80 1.30 6 -9 9 -1.60 1.20 -7 9 -9 35.20 3.00 7 -9 9 33.70 3.00 -8 9 -9 4.60 1.70 8 -9 9 5.10 1.70 -9 9 -9 4.60 1.80 9 -9 9 4.70 1.90 -10 9 -9 7.70 2.10 10 -9 9 0.40 1.90 -11 9 -9 2.90 2.20 11 -9 9 -0.50 2.10 11 8 -9 9.20 2.50 10 8 -9 -0.10 1.90 9 8 -9 67.99 4.90 8 8 -9 -0.50 1.60 -8 -8 9 -0.60 1.40 7 8 -9 17.70 2.10 -7 -8 9 22.60 2.30 6 8 -9 5.40 1.50 6 8 -9 3.60 1.30 5 8 -9 62.79 4.30 5 8 -9 68.29 4.40 -5 -8 9 62.19 4.40 4 8 -9 8.10 1.50 -4 -8 9 8.40 1.60 3 8 -9 -0.30 1.10 -3 -8 9 -0.60 1.10 2 8 -9 31.70 2.70 -2 -8 9 37.80 2.80 1 8 -9 64.19 4.10 -1 -8 9 58.89 4.10 0 8 -9 79.19 5.10 0 -8 9 79.19 5.00 -1 8 -9 13.50 1.70 1 -8 9 16.20 1.70 -2 8 -9 -0.10 1.10 2 -8 9 -0.50 1.00 -3 8 -9 3.50 1.20 3 -8 9 2.30 1.10 -4 8 -9 -0.20 1.10 4 -8 9 -0.40 1.10 -5 8 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-9 -0.80 1.50 9 -7 9 -1.00 1.60 -10 7 -9 2.20 2.10 10 -7 9 2.10 2.10 -11 7 -9 4.30 2.30 11 -7 9 5.20 2.20 12 6 -9 21.40 3.10 11 6 -9 -1.90 1.90 -11 -6 9 0.50 1.70 10 6 -9 20.30 2.60 -10 -6 9 20.50 2.40 9 6 -9 1.00 1.50 -9 -6 9 0.60 1.60 8 6 -9 4.10 1.50 -8 -6 9 1.90 1.30 7 6 -9 8.80 1.70 -7 -6 9 12.10 1.60 6 6 -9 4.00 1.20 -6 -6 9 5.00 1.30 5 6 -9 54.29 3.80 5 6 -9 58.39 3.80 -5 -6 9 57.29 3.80 4 6 -9 0.70 1.00 4 6 -9 1.80 1.00 -4 -6 9 2.40 0.90 3 6 -9 0.20 0.80 3 6 -9 0.60 1.00 -3 -6 9 -0.10 0.90 2 6 -9 73.69 4.70 2 6 -9 74.89 4.50 -2 -6 9 72.49 4.60 1 6 -9 1.80 1.00 -1 -6 9 3.20 0.90 0 6 -9 5.20 1.10 0 -6 9 3.20 1.00 -1 6 -9 14.50 1.70 1 -6 9 18.60 1.70 -2 6 -9 49.70 3.40 2 -6 9 49.70 3.40 -3 6 -9 19.70 1.80 3 -6 9 15.70 1.70 -4 6 -9 0.10 1.00 4 -6 9 1.60 1.10 -5 6 -9 5.40 1.30 5 -6 9 6.80 1.20 -6 6 -9 13.10 1.80 6 -6 9 17.70 1.80 -7 6 -9 0.90 1.30 7 -6 9 1.10 1.30 -8 6 -9 -0.40 1.40 8 -6 9 4.90 1.50 -9 6 -9 2.30 1.70 9 -6 9 0.50 1.50 -10 6 -9 39.40 3.30 10 -6 9 34.50 3.40 11 -6 9 0.30 1.90 12 5 -9 4.70 2.30 -12 -5 9 6.90 2.00 11 5 -9 18.10 2.60 -11 -5 9 15.00 2.30 10 5 -9 5.90 1.80 -10 -5 9 4.90 1.60 9 5 -9 17.70 2.20 -9 -5 9 16.00 2.00 8 5 -9 1.20 1.40 -8 -5 9 3.80 1.30 7 5 -9 4.60 1.30 -7 -5 9 4.20 1.20 6 5 -9 3.30 1.30 -6 -5 9 2.40 1.10 5 5 -9 1.40 1.10 5 5 -9 -0.30 1.00 4 5 -9 41.00 2.70 4 5 -9 44.30 2.90 -4 -5 9 35.70 2.70 3 5 -9 21.70 1.90 3 5 -9 15.80 1.60 -3 -5 9 21.20 1.70 2 5 -9 38.10 2.50 2 5 -9 39.30 2.70 -2 -5 9 37.10 2.60 1 5 -9 236.28 13.50 1 5 -9 234.98 13.30 -1 -5 9 224.48 13.40 0 5 -9 6.30 1.10 0 -5 9 5.40 1.00 -1 5 -9 24.00 1.80 1 -5 9 15.70 1.70 -2 5 -9 29.40 2.40 2 -5 9 32.90 2.40 -3 5 -9 0.70 1.00 3 -5 9 1.20 1.00 -4 5 -9 46.60 3.10 4 -5 9 42.80 3.10 -5 5 -9 157.78 9.20 5 -5 9 149.59 9.20 -6 5 -9 25.80 2.50 6 -5 9 27.70 2.40 -7 5 -9 78.39 5.10 7 -5 9 80.79 5.20 -8 5 -9 -0.50 1.30 8 -5 9 1.00 1.30 -9 5 -9 14.40 2.10 9 -5 9 13.90 2.00 10 -5 9 2.30 1.80 11 -5 9 11.20 2.30 12 -5 9 6.00 2.30 -13 -4 9 1.80 2.00 12 4 -9 1.40 2.40 -12 -4 9 0.00 1.80 11 4 -9 10.70 2.30 -11 -4 9 17.80 2.20 10 4 -9 20.40 2.50 -10 -4 9 23.50 2.30 9 4 -9 21.90 2.40 -9 -4 9 24.20 2.30 8 4 -9 11.30 1.70 -8 -4 9 10.30 1.60 7 4 -9 82.79 5.60 -7 -4 9 95.49 5.60 6 4 -9 30.80 2.50 -6 -4 9 33.20 2.50 5 4 -9 2.10 1.10 5 4 -9 3.60 1.10 4 4 -9 2.50 1.00 4 4 -9 0.50 0.80 -4 -4 9 2.20 0.80 3 4 -9 6.40 1.10 3 4 -9 3.00 0.90 -3 -4 9 3.70 0.80 2 4 -9 19.50 1.60 2 4 -9 17.50 1.70 -2 -4 9 20.00 1.60 1 4 -9 18.60 1.60 1 4 -9 17.50 1.50 -1 -4 9 17.80 1.60 0 4 -9 2.20 0.70 0 4 -9 4.30 1.00 0 -4 9 2.80 0.80 -1 4 -9 27.40 2.10 1 -4 9 25.00 2.00 -2 4 -9 14.60 1.50 2 -4 9 14.90 1.50 -3 4 -9 18.80 1.80 3 -4 9 23.50 1.90 -4 4 -9 3.30 1.00 4 -4 9 1.30 1.00 -5 4 -9 92.29 5.80 5 -4 9 93.69 5.80 -6 4 -9 3.50 1.20 6 -4 9 2.80 1.20 -7 4 -9 4.70 1.50 7 -4 9 7.40 1.40 -8 4 -9 2.00 1.30 8 -4 9 2.30 1.40 9 -4 9 -0.40 1.50 10 -4 9 -0.40 1.70 11 -4 9 6.60 2.20 13 3 -9 1.20 2.30 -13 -3 9 -1.40 2.00 12 3 -9 23.20 3.20 -12 -3 9 26.70 2.80 11 3 -9 3.70 1.80 -11 -3 9 5.50 1.70 10 3 -9 75.79 5.30 -10 -3 9 78.19 5.10 9 3 -9 11.50 1.90 -9 -3 9 13.40 1.80 8 3 -9 117.79 7.40 -8 -3 9 119.59 7.30 7 3 -9 2.20 1.20 -7 -3 9 2.10 1.10 6 3 -9 -0.10 1.00 -6 -3 9 -0.60 0.90 5 3 -9 41.00 2.80 -5 -3 9 37.90 2.80 4 3 -9 0.10 0.90 4 3 -9 0.40 0.80 -4 -3 9 0.60 0.70 3 3 -9 178.88 10.70 3 3 -9 185.68 10.70 -3 -3 9 182.98 10.60 2 3 -9 104.49 6.60 2 3 -9 112.19 6.50 -2 -3 9 108.99 6.50 1 3 -9 47.20 2.90 1 3 -9 51.19 3.00 -1 -3 9 36.70 2.80 0 3 -9 1.10 0.70 0 3 -9 -0.20 0.80 0 -3 9 0.20 0.70 -1 3 -9 0.00 0.70 -1 3 -9 -0.10 0.80 1 -3 9 0.30 0.70 -2 3 -9 17.60 1.70 2 -3 9 17.70 1.50 2 -3 9 21.30 1.70 -3 3 -9 1.50 1.00 3 -3 9 3.00 1.00 -4 3 -9 1.40 1.10 4 -3 9 2.10 1.00 -5 3 -9 26.40 2.20 -5 3 -9 23.40 2.20 -6 3 -9 87.99 5.60 -6 3 -9 92.39 5.80 -7 3 -9 6.60 1.50 -7 3 -9 5.90 1.30 -8 3 -9 2.20 1.40 -9 3 -9 2.60 1.70 -10 3 -9 1.70 1.70 13 2 -9 0.30 2.20 -13 -2 9 -1.20 2.00 12 2 -9 67.59 5.00 -12 -2 9 64.49 4.80 11 2 -9 0.20 1.70 -11 -2 9 4.00 1.60 10 2 -9 73.99 5.00 -10 -2 9 70.59 4.90 9 2 -9 6.90 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-10 10 15.30 2.00 -3 10 -10 0.70 1.40 3 -10 10 1.70 1.40 -4 10 -10 1.00 1.40 4 -10 10 -1.20 1.40 -5 10 -10 40.60 3.40 5 -10 10 45.50 3.50 -6 10 -10 3.50 1.60 6 -10 10 0.40 1.50 -7 10 -10 12.60 2.20 7 -10 10 20.50 2.60 -8 10 -10 17.50 2.50 8 -10 10 18.60 2.50 -9 10 -10 15.40 2.50 9 -10 10 15.40 2.70 -10 10 -10 0.80 2.10 10 -10 10 -2.40 2.40 10 9 -10 27.90 3.60 9 9 -10 0.00 2.00 -8 -9 10 1.90 1.60 -7 -9 10 8.40 1.80 6 9 -10 4.90 1.80 5 9 -10 11.70 1.90 4 9 -10 0.90 1.40 -4 -9 10 -0.30 1.30 3 9 -10 41.20 3.20 -3 -9 10 39.40 3.20 2 9 -10 77.49 5.20 -2 -9 10 80.09 5.20 1 9 -10 3.40 1.40 -1 -9 10 6.50 1.60 0 9 -10 20.90 2.20 0 -9 10 21.70 2.20 -1 9 -10 29.90 2.60 1 -9 10 25.40 2.50 -2 9 -10 6.40 1.50 2 -9 10 10.00 1.60 -3 9 -10 43.30 3.70 3 -9 10 61.39 3.90 -4 9 -10 16.40 2.00 4 -9 10 17.00 2.00 -5 9 -10 3.80 1.50 5 -9 10 3.10 1.50 -6 9 -10 84.89 5.70 6 -9 10 87.29 5.70 -7 9 -10 2.50 1.60 7 -9 10 1.40 1.60 -8 9 -10 0.00 1.70 8 -9 10 0.00 1.70 -9 9 -10 11.50 2.20 9 -9 10 14.60 2.40 -10 9 -10 6.70 2.30 10 -9 10 6.10 2.30 10 8 -10 0.00 2.10 9 8 -10 3.70 2.20 -9 -8 10 7.20 1.90 8 8 -10 0.50 1.60 -8 -8 10 2.00 1.50 7 8 -10 17.90 2.20 -7 -8 10 21.70 2.40 6 8 -10 -0.60 1.40 5 8 -10 44.20 3.40 4 8 -10 17.50 2.10 -4 -8 10 18.40 2.10 3 8 -10 10.10 1.70 -3 -8 10 12.50 1.80 2 8 -10 45.50 3.30 -2 -8 10 43.60 3.40 1 8 -10 64.09 4.40 -1 -8 10 67.39 4.40 0 8 -10 3.10 1.30 0 -8 10 6.80 1.50 -1 8 -10 6.10 1.40 1 -8 10 3.40 1.30 -2 8 -10 69.59 4.70 2 -8 10 71.69 4.70 -3 8 -10 39.70 3.20 3 -8 10 44.50 3.20 -4 8 -10 29.40 2.70 4 -8 10 35.00 2.60 -5 8 -10 -1.00 1.30 5 -8 10 1.20 1.30 -6 8 -10 37.60 3.20 6 -8 10 40.50 3.20 -7 8 -10 42.50 3.60 7 -8 10 50.99 3.70 -8 8 -10 0.80 1.60 8 -8 10 -0.70 1.60 -9 8 -10 3.20 1.90 9 -8 10 2.50 1.90 -10 8 -10 -0.10 2.00 10 -8 10 -0.50 1.90 11 7 -10 13.70 2.70 10 7 -10 5.50 2.30 -10 -7 10 3.90 2.10 9 7 -10 1.20 2.00 -9 -7 10 -0.70 1.50 8 7 -10 61.79 4.20 -8 -7 10 49.90 4.00 7 7 -10 9.30 1.70 -7 -7 10 11.60 1.90 6 7 -10 -1.00 1.20 6 7 -10 1.50 1.40 5 7 -10 2.20 1.30 5 7 -10 1.50 1.20 4 7 -10 4.60 1.40 -4 -7 10 3.40 1.30 3 7 -10 -0.80 1.10 -3 -7 10 -0.30 1.00 2 7 -10 3.80 1.20 -2 -7 10 2.50 1.10 1 7 -10 10.80 1.50 -1 -7 10 7.30 1.30 0 7 -10 68.59 4.70 0 -7 10 74.59 4.70 -1 7 -10 67.09 4.50 1 -7 10 68.29 4.40 -2 7 -10 26.10 2.40 2 -7 10 28.30 2.40 -3 7 -10 16.40 1.90 3 -7 10 17.10 1.90 -4 7 -10 66.59 4.60 4 -7 10 74.19 4.70 -5 7 -10 54.19 3.90 5 -7 10 54.49 3.90 -6 7 -10 1.90 1.30 6 -7 10 1.20 1.30 -7 7 -10 12.30 1.90 7 -7 10 16.80 2.00 -8 7 -10 4.60 1.70 8 -7 10 3.10 1.70 -9 7 -10 -0.40 1.70 9 -7 10 0.00 1.70 -10 7 -10 -0.30 2.20 10 -7 10 1.00 2.00 11 -7 10 -0.20 2.40 12 6 -10 4.00 2.80 11 6 -10 19.70 2.80 -11 -6 10 19.90 2.60 10 6 -10 9.40 2.40 -10 -6 10 16.10 2.20 9 6 -10 25.80 2.70 -9 -6 10 25.20 2.50 8 6 -10 2.30 1.70 -8 -6 10 -0.40 1.30 7 6 -10 1.30 1.40 -7 -6 10 1.30 1.30 6 6 -10 6.60 1.60 -6 -6 10 8.30 1.50 5 6 -10 12.20 1.70 5 6 -10 12.60 1.60 4 6 -10 0.70 1.20 4 6 -10 0.80 1.00 -4 -6 10 1.50 1.10 3 6 -10 18.40 1.90 -3 -6 10 18.30 1.80 2 6 -10 68.49 4.80 -2 -6 10 82.09 4.80 1 6 -10 4.10 1.20 -1 -6 10 4.40 1.10 0 6 -10 17.90 1.70 0 -6 10 19.90 1.80 -1 6 -10 178.88 10.50 1 -6 10 175.08 10.50 -2 6 -10 2.90 1.10 2 -6 10 3.90 1.10 -3 6 -10 1.50 1.10 3 -6 10 1.50 1.10 -4 6 -10 2.40 1.20 4 -6 10 2.90 1.20 -5 6 -10 1.40 1.30 5 -6 10 1.00 1.30 -6 6 -10 92.09 5.90 6 -6 10 94.39 6.00 -7 6 -10 0.30 1.30 7 -6 10 0.40 1.30 -8 6 -10 5.00 1.60 8 -6 10 2.70 1.60 -9 6 -10 2.30 1.70 9 -6 10 0.60 1.70 -10 6 -10 0.80 1.80 10 -6 10 -2.00 1.80 11 -6 10 -0.50 2.10 12 5 -10 11.80 3.00 -12 -5 10 13.50 2.70 11 5 -10 9.90 2.40 -11 -5 10 13.50 2.40 10 5 -10 12.30 2.20 -10 -5 10 10.00 1.90 9 5 -10 0.80 1.60 -9 -5 10 -0.20 1.40 8 5 -10 3.30 1.50 -8 -5 10 1.60 1.30 7 5 -10 1.40 1.30 -7 -5 10 2.70 1.20 6 5 -10 14.10 1.80 -6 -5 10 13.20 1.70 5 5 -10 35.70 2.50 5 5 -10 22.90 2.40 4 5 -10 143.89 8.30 4 5 -10 132.89 8.40 -4 -5 10 138.59 8.20 3 5 -10 15.00 1.70 3 5 -10 16.20 1.60 -3 -5 10 12.80 1.40 2 5 -10 1.90 0.90 2 5 -10 3.40 1.10 -2 -5 10 1.20 0.90 1 5 -10 138.89 8.30 -1 -5 10 138.79 8.30 0 5 -10 7.90 1.40 0 -5 10 10.20 1.30 -1 5 -10 177.18 10.40 1 -5 10 174.68 10.40 -2 5 -10 33.70 2.60 2 -5 10 35.40 2.60 -3 5 -10 0.20 1.00 3 -5 10 0.20 1.00 -4 5 -10 61.19 4.00 4 -5 10 59.59 4.10 -5 5 -10 14.10 1.70 5 -5 10 13.10 1.70 -6 5 -10 6.20 1.50 6 -5 10 7.70 1.50 -7 5 -10 23.00 2.20 7 -5 10 17.30 2.10 -8 5 -10 0.40 1.40 8 -5 10 -1.10 1.50 -9 5 -10 5.60 2.00 9 -5 10 7.00 2.00 10 -5 10 0.80 1.90 11 -5 10 1.10 2.10 12 4 -10 -0.30 2.20 -12 -4 10 -1.40 2.20 11 4 -10 5.80 2.10 -11 -4 10 4.00 1.90 10 4 -10 0.50 1.90 -10 -4 10 5.20 1.70 9 4 -10 0.60 1.50 -9 -4 10 -0.50 1.30 8 4 -10 13.00 1.90 -8 -4 10 12.00 1.70 7 4 -10 19.50 2.20 -7 -4 10 26.40 2.20 6 4 -10 0.30 1.00 -6 -4 10 -0.80 1.00 5 4 -10 8.30 1.40 5 4 -10 8.20 1.30 4 4 -10 0.80 1.00 4 4 -10 -0.10 0.90 3 4 -10 6.80 1.30 3 4 -10 5.20 1.10 -3 -4 10 5.90 1.00 2 4 -10 53.99 3.60 2 4 -10 52.89 3.40 -2 -4 10 52.89 3.50 1 4 -10 39.80 2.70 1 4 -10 41.00 2.90 -1 -4 10 42.40 2.90 0 4 -10 0.90 0.90 0 -4 10 0.60 0.80 -1 4 -10 60.79 4.00 1 -4 10 59.89 3.90 -2 4 -10 43.90 3.10 2 -4 10 46.40 3.10 -3 4 -10 136.69 8.20 3 -4 10 133.29 8.10 -4 4 -10 54.49 3.90 4 -4 10 61.69 3.90 -5 4 -10 7.60 1.40 5 -4 10 6.30 1.40 -6 4 -10 4.10 1.30 6 -4 10 3.10 1.30 -7 4 -10 4.90 1.50 7 -4 10 7.80 1.60 -8 4 -10 8.20 2.30 8 -4 10 10.80 1.90 9 -4 10 3.00 1.80 10 -4 10 1.50 2.00 11 -4 10 21.20 2.80 -13 -3 10 -1.60 2.10 12 3 -10 4.80 2.30 -12 -3 10 4.40 2.00 11 3 -10 18.90 2.70 -11 -3 10 26.00 2.60 10 3 -10 5.70 1.70 -10 -3 10 5.30 1.60 9 3 -10 20.90 2.40 -9 -3 10 24.60 2.30 8 3 -10 1.70 1.30 -8 -3 10 1.60 1.30 7 3 -10 12.60 1.70 -7 -3 10 9.30 1.50 6 3 -10 27.80 2.40 -6 -3 10 32.00 2.50 5 3 -10 57.99 3.80 -5 -3 10 54.19 3.70 4 3 -10 10.70 1.30 4 3 -10 9.10 1.40 3 3 -10 1.40 0.90 3 3 -10 0.40 1.00 -3 -3 10 0.40 0.80 2 3 -10 6.90 1.30 2 3 -10 11.50 1.30 -2 -3 10 7.60 1.10 1 3 -10 32.00 2.30 1 3 -10 28.20 2.20 -1 -3 10 31.40 2.30 0 3 -10 161.08 9.10 0 3 -10 159.78 9.20 0 -3 10 143.69 9.10 -1 3 -10 3.50 1.00 -1 3 -10 4.80 1.00 1 -3 10 4.20 1.00 -2 3 -10 29.40 2.30 2 -3 10 30.30 2.30 -3 3 -10 1.30 1.00 3 -3 10 2.60 1.10 -4 3 -10 0.10 1.00 4 -3 10 1.00 1.10 -5 3 -10 -0.50 1.00 5 -3 10 0.60 1.10 -6 3 -10 1.90 1.40 -6 3 -10 2.00 1.30 -7 3 -10 27.00 2.70 -8 3 -10 -1.80 1.60 9 -3 10 47.00 3.90 10 -3 10 4.30 2.10 11 -3 10 7.70 2.40 13 2 -10 0.30 2.30 -13 -2 10 -0.90 2.00 12 2 -10 38.20 3.80 -12 -2 10 44.90 3.80 11 2 -10 0.90 1.80 -11 -2 10 1.30 1.70 10 2 -10 1.90 1.50 -10 -2 10 2.60 1.60 9 2 -10 12.30 1.90 -9 -2 10 14.90 1.90 8 2 -10 18.90 2.20 -8 -2 10 20.10 2.00 7 2 -10 0.70 1.20 -7 -2 10 -0.40 1.00 6 2 -10 28.20 2.30 -6 -2 10 23.10 2.20 5 2 -10 22.30 2.00 -5 -2 10 23.40 1.90 4 2 -10 278.97 15.40 4 2 -10 252.27 15.40 3 2 -10 81.79 5.50 3 2 -10 94.49 5.50 -3 -2 10 87.99 5.30 2 2 -10 2.00 1.00 2 2 -10 5.80 1.10 -2 -2 10 4.20 0.90 1 2 -10 74.29 4.40 1 2 -10 74.89 4.50 -1 -2 10 65.79 4.40 0 2 -10 0.00 0.90 0 2 -10 1.30 0.90 0 -2 10 0.50 0.80 -1 2 -10 0.00 0.80 -1 2 -10 0.30 1.00 1 -2 10 -0.70 0.80 -2 2 -10 22.30 1.90 -2 2 -10 24.60 2.00 2 -2 10 20.20 1.80 -3 2 -10 3.70 1.10 -3 2 -10 6.20 1.30 -4 2 -10 57.19 3.70 -4 2 -10 52.19 3.80 -5 2 -10 3.10 1.30 -5 2 -10 7.20 1.40 -6 2 -10 21.20 2.20 -7 2 -10 13.40 2.00 -8 2 -10 38.20 3.40 -9 2 -10 32.00 3.20 -10 2 -10 13.10 2.60 13 1 -10 3.40 2.60 -13 -1 10 0.30 2.40 12 1 -10 1.50 2.00 -12 -1 10 -0.90 1.80 11 1 -10 2.40 1.80 -11 -1 10 0.20 1.60 10 1 -10 0.10 1.50 -10 -1 10 1.00 1.40 9 1 -10 24.70 2.60 -9 -1 10 25.70 2.40 8 1 -10 51.89 4.00 -8 -1 10 62.69 3.90 7 1 -10 13.80 1.80 -7 -1 10 16.10 1.70 6 1 -10 24.00 2.10 -6 -1 10 20.70 2.00 5 1 -10 6.70 1.30 -5 -1 10 5.50 1.10 4 1 -10 6.00 1.20 -4 -1 10 3.40 1.10 3 1 -10 5.60 1.10 3 1 -10 8.80 1.30 -3 -1 10 6.00 0.90 2 1 -10 13.20 1.50 2 1 -10 10.10 1.30 -2 -1 10 8.80 1.10 1 1 -10 19.40 1.70 1 1 -10 17.20 1.70 -1 -1 10 17.90 1.60 0 1 -10 145.39 8.60 0 1 -10 147.19 8.60 0 1 -10 143.89 8.60 -1 1 -10 19.80 1.80 -1 1 -10 19.00 1.80 -1 1 -10 20.90 1.70 -2 1 -10 53.29 3.40 -2 1 -10 53.79 3.50 2 -1 10 49.90 3.40 -3 1 -10 30.60 2.40 -3 1 -10 30.30 2.50 3 -1 10 31.20 2.40 -4 1 -10 17.20 1.70 -4 1 -10 22.60 2.00 4 -1 10 14.70 1.80 -5 1 -10 12.60 1.60 -6 1 -10 6.20 1.60 -7 1 -10 14.60 1.80 -8 1 -10 89.39 6.10 -9 1 -10 -0.30 1.90 -10 1 -10 3.60 2.40 13 0 -10 1.40 2.30 -13 0 10 1.70 2.10 12 0 -10 0.10 1.90 -12 0 10 1.10 1.90 11 0 -10 6.20 2.00 -11 0 10 9.00 1.90 10 0 -10 2.50 1.60 -10 0 10 4.90 1.60 9 0 -10 0.50 1.40 -9 0 10 2.40 1.30 8 0 -10 0.70 1.30 -8 0 10 0.50 1.10 7 0 -10 -0.30 1.20 -7 0 10 0.40 1.10 6 0 -10 5.40 1.30 -6 0 10 5.10 1.30 5 0 -10 5.20 1.30 -5 0 10 4.60 1.10 4 0 -10 21.20 2.00 -4 0 10 21.90 1.80 3 0 -10 29.00 2.10 -3 0 10 22.90 1.80 -3 0 10 18.70 1.90 2 0 -10 4.90 1.10 2 0 -10 6.60 1.00 2 0 -10 9.20 1.20 1 0 -10 78.89 4.80 1 0 -10 83.09 4.90 1 0 -10 74.19 4.90 0 0 -10 27.70 2.30 0 0 -10 30.70 2.20 0 0 -10 31.10 2.30 -1 0 -10 31.40 2.20 -1 0 -10 25.60 2.10 1 0 10 24.60 2.20 -2 0 -10 29.50 2.20 -2 0 -10 30.60 2.30 2 0 10 27.10 2.30 -3 0 -10 9.70 1.50 -3 0 -10 11.90 1.40 3 0 10 9.80 1.40 -4 0 -10 0.80 1.20 4 0 10 -0.80 1.20 -5 0 -10 4.30 1.40 5 0 10 2.50 1.20 -6 0 -10 23.60 2.40 -7 0 -10 1.90 1.50 -8 0 -10 0.80 1.70 -9 0 -10 0.10 1.90 -10 0 -10 7.00 2.50 13 -1 -10 11.10 2.60 -13 1 10 19.50 2.90 12 -1 -10 9.60 2.20 -12 1 10 7.70 2.20 11 -1 -10 -0.60 1.70 -11 1 10 -0.20 1.60 10 -1 -10 42.60 3.50 -10 1 10 43.60 3.40 9 -1 -10 1.10 1.50 -9 1 10 1.10 1.30 8 -1 -10 43.00 3.40 -8 1 10 37.10 3.00 7 -1 -10 -0.80 1.20 -7 1 10 -0.70 1.10 6 -1 -10 38.70 2.90 -6 1 10 33.00 2.70 5 -1 -10 67.29 4.70 -5 1 10 75.39 4.60 4 -1 -10 567.04 32.00 -4 1 10 546.35 31.90 3 -1 -10 44.60 3.20 -3 1 10 40.90 2.90 2 -1 -10 59.79 3.70 2 -1 -10 55.59 3.80 -2 1 10 57.79 3.70 1 -1 -10 202.88 11.50 1 -1 -10 192.28 11.60 -1 1 10 195.38 11.50 0 -1 -10 12.70 1.50 0 -1 -10 14.80 1.50 0 -1 -10 13.40 1.60 -1 -1 -10 0.50 0.90 -1 -1 -10 -0.70 0.90 1 1 10 0.00 0.90 -2 -1 -10 2.00 1.00 -2 -1 -10 2.30 1.10 2 1 10 1.30 1.10 -3 -1 -10 1.90 1.20 3 1 10 3.20 1.20 -4 -1 -10 0.60 1.20 4 1 10 1.70 1.30 -5 -1 -10 0.50 1.40 5 1 10 0.20 1.30 -6 -1 -10 33.30 3.10 6 1 10 36.40 3.20 -7 -1 -10 0.90 1.60 -8 -1 -10 48.80 4.10 -9 -1 -10 2.60 2.20 13 -2 -10 14.80 2.80 -13 2 10 19.90 2.80 12 -2 -10 3.40 2.20 -12 2 10 2.20 1.90 11 -2 -10 1.20 1.70 -11 2 10 1.50 1.70 10 -2 -10 2.10 1.80 -10 2 10 3.20 1.60 9 -2 -10 0.30 1.40 -9 2 10 1.60 1.40 8 -2 -10 13.20 1.90 -8 2 10 8.20 1.60 7 -2 -10 0.90 1.30 -7 2 10 0.70 1.20 6 -2 -10 72.19 4.90 -6 2 10 74.99 4.70 5 -2 -10 9.90 1.60 -5 2 10 7.50 1.30 4 -2 -10 53.09 3.60 -4 2 10 48.70 3.40 3 -2 -10 -0.80 1.00 -3 2 10 1.10 1.00 2 -2 -10 42.30 3.20 2 -2 -10 49.30 3.10 -2 2 10 45.30 3.10 1 -2 -10 239.28 13.50 1 -2 -10 224.98 13.60 -1 2 10 232.88 13.50 0 -2 -10 -0.80 1.00 0 -2 -10 2.30 1.10 0 2 10 0.00 0.90 -1 -2 -10 58.19 4.00 1 2 10 59.49 4.00 -2 -2 -10 67.39 4.30 2 2 10 61.29 4.20 -3 -2 -10 17.40 2.00 3 2 10 24.10 2.20 -4 -2 -10 58.49 3.80 4 2 10 45.50 3.60 -5 -2 -10 -0.10 1.40 5 2 10 0.20 1.40 -6 -2 -10 2.90 1.60 6 2 10 -0.40 1.80 -7 -2 -10 3.40 1.80 7 2 10 4.90 2.10 -8 -2 -10 8.30 2.20 -9 -2 -10 3.70 2.60 13 -3 -10 1.70 2.40 -13 3 10 0.30 2.30 12 -3 -10 5.90 2.20 -12 3 10 5.30 2.20 11 -3 -10 10.00 2.20 -11 3 10 8.50 2.10 10 -3 -10 -0.20 1.60 -10 3 10 -0.10 1.60 9 -3 -10 6.50 1.70 -9 3 10 6.90 1.70 8 -3 -10 32.10 2.90 -8 3 10 30.10 2.70 7 -3 -10 7.00 1.70 -7 3 10 9.50 1.50 6 -3 -10 20.50 2.20 -6 3 10 23.00 2.20 5 -3 -10 0.30 1.20 -5 3 10 0.60 1.00 4 -3 -10 13.00 1.90 -4 3 10 15.80 1.70 3 -3 -10 40.90 3.10 -3 3 10 39.30 2.80 2 -3 -10 85.89 5.50 2 -3 -10 86.29 5.20 -2 3 10 82.29 5.20 1 -3 -10 157.38 9.40 1 -3 -10 159.88 9.30 -1 3 10 153.08 9.20 0 -3 -10 7.80 1.40 0 -3 -10 6.60 1.40 -1 -3 -10 12.00 1.70 1 3 10 13.20 1.70 -2 -3 -10 21.80 2.10 2 3 10 19.20 2.10 -3 -3 -10 -0.90 1.30 3 3 10 1.30 1.50 -4 -3 -10 0.30 1.40 4 3 10 0.40 1.40 -5 -3 -10 12.00 1.90 5 3 10 11.00 2.10 -6 -3 -10 11.60 2.10 6 3 10 12.70 2.20 -7 -3 -10 4.10 1.90 7 3 10 2.70 1.90 -8 -3 -10 2.30 2.10 8 3 10 -1.10 2.40 12 -4 -10 1.80 2.20 -12 4 10 0.00 2.10 11 -4 -10 22.00 2.70 -11 4 10 17.10 2.50 10 -4 -10 10.20 2.10 -10 4 10 8.30 1.90 9 -4 -10 28.30 3.00 -9 4 10 35.20 3.00 8 -4 -10 3.40 1.60 -8 4 10 2.60 1.40 7 -4 -10 0.60 1.40 -7 4 10 2.40 1.30 6 -4 -10 18.90 2.20 -6 4 10 18.20 2.00 5 -4 -10 67.79 4.70 -5 4 10 68.09 4.40 4 -4 -10 49.60 3.60 -4 4 10 49.10 3.50 3 -4 -10 1.50 1.30 -3 4 10 0.90 1.00 2 -4 -10 74.89 4.90 2 -4 -10 72.79 4.60 -2 4 10 71.59 4.50 1 -4 -10 20.40 2.10 1 -4 -10 18.00 1.80 0 -4 -10 1.50 1.10 0 4 10 1.50 1.20 -1 -4 -10 -0.30 1.10 1 4 10 1.30 1.30 -2 -4 -10 5.80 1.40 2 4 10 3.60 1.40 -3 -4 -10 3.00 1.40 3 4 10 3.90 1.70 -4 -4 -10 41.60 3.50 4 4 10 47.10 3.50 -5 -4 -10 1.70 1.70 5 4 10 2.00 1.70 -6 -4 -10 -0.20 1.70 6 4 10 -0.70 2.10 -7 -4 -10 12.80 2.40 7 4 10 16.50 2.80 -8 -4 -10 4.80 2.40 8 4 10 2.80 2.40 12 -5 -10 1.20 2.70 -12 5 10 0.60 2.20 11 -5 -10 0.30 2.00 -11 5 10 2.40 2.10 10 -5 -10 2.80 2.20 -10 5 10 4.30 1.90 9 -5 -10 0.90 1.60 -9 5 10 3.00 1.60 8 -5 -10 1.50 1.70 -8 5 10 1.10 1.50 7 -5 -10 50.09 3.90 -7 5 10 51.19 3.70 6 -5 -10 60.69 4.40 -6 5 10 58.99 4.10 5 -5 -10 57.29 4.20 -5 5 10 58.79 4.00 4 -5 -10 10.10 1.80 -4 5 10 9.00 1.40 3 -5 -10 5.10 1.50 -3 5 10 6.00 1.30 2 -5 -10 35.30 2.70 2 -5 -10 41.20 3.10 1 -5 -10 1.00 1.40 1 -5 -10 4.60 1.30 0 -5 -10 3.50 1.50 0 5 10 7.50 1.60 -1 -5 -10 7.20 1.50 1 5 10 9.30 1.70 -2 -5 -10 -0.10 1.30 2 5 10 0.90 1.40 -3 -5 -10 45.40 3.60 3 5 10 50.09 3.70 -4 -5 -10 25.10 2.80 4 5 10 36.80 3.00 -5 -5 -10 0.40 1.80 5 5 10 -0.70 1.70 -6 -5 -10 30.50 3.30 6 5 10 36.40 3.60 -7 -5 -10 14.20 2.70 7 5 10 16.50 3.10 12 -6 -10 16.30 3.10 -12 6 10 21.40 3.10 11 -6 -10 18.40 2.90 -11 6 10 19.80 2.90 10 -6 -10 6.10 2.20 -10 6 10 7.70 2.10 9 -6 -10 9.70 2.30 -9 6 10 9.80 2.00 8 -6 -10 1.90 1.80 -8 6 10 0.30 1.50 7 -6 -10 2.20 1.70 -7 6 10 4.90 1.60 6 -6 -10 0.20 1.50 -6 6 10 1.60 1.40 5 -6 -10 3.00 1.60 -5 6 10 6.60 1.60 4 -6 -10 18.40 2.20 3 -6 -10 0.90 1.50 2 -6 -10 -0.40 1.40 1 -6 -10 14.10 1.70 -1 6 10 10.40 1.80 0 -6 -10 37.40 3.20 0 6 10 41.10 3.30 -1 -6 -10 6.50 1.50 1 6 10 2.40 1.50 -2 -6 -10 1.40 1.70 2 6 10 4.80 1.70 -3 -6 -10 5.90 1.70 3 6 10 6.60 1.90 -4 -6 -10 18.50 2.40 4 6 10 14.00 2.30 -5 -6 -10 1.00 2.00 5 6 10 2.20 2.00 -6 -6 -10 3.20 2.20 6 6 10 6.90 2.50 7 6 10 0.20 2.60 11 -7 -10 3.80 2.60 -11 7 10 5.60 2.40 10 -7 -10 1.10 2.20 -10 7 10 2.00 2.10 9 -7 -10 0.40 2.10 -9 7 10 0.20 1.90 8 -7 -10 10.80 2.60 -8 7 10 19.60 2.50 7 -7 -10 -0.70 1.70 -7 7 10 -0.70 1.60 6 -7 -10 7.50 2.00 -6 7 10 8.90 1.80 5 -7 -10 1.50 1.60 4 -7 -10 2.80 1.70 3 -7 -10 1.10 1.60 2 -7 -10 145.79 9.10 1 -7 -10 1.00 1.30 -1 7 10 -0.20 1.40 0 -7 -10 1.90 1.40 0 7 10 3.20 1.70 -1 -7 -10 2.00 1.60 1 7 10 3.10 1.70 -2 -7 -10 0.50 1.60 2 7 10 -0.30 1.70 -3 -7 -10 34.40 3.30 3 7 10 33.20 3.40 -4 -7 -10 0.70 1.90 4 7 10 0.50 2.30 -5 -7 -10 8.80 2.30 5 7 10 6.40 2.50 6 7 10 26.40 3.60 -11 8 10 4.60 2.60 10 -8 -10 37.50 4.10 -10 8 10 41.90 4.00 9 -8 -10 8.90 2.60 -9 8 10 6.20 2.20 8 -8 -10 4.80 2.20 -8 8 10 3.90 1.90 7 -8 -10 3.90 2.30 -7 8 10 2.60 2.00 6 -8 -10 83.19 5.80 5 -8 -10 8.50 2.10 4 -8 -10 6.80 2.10 3 -8 -10 33.00 3.20 -2 8 10 9.50 2.10 1 -8 -10 9.70 1.90 -1 8 10 11.10 2.10 0 -8 -10 6.20 1.70 0 8 10 8.90 2.10 -1 -8 -10 1.20 1.60 1 8 10 1.80 1.80 -2 -8 -10 2.20 1.80 2 8 10 0.40 1.90 -3 -8 -10 -0.50 1.90 3 8 10 0.10 2.10 -4 -8 -10 4.50 2.20 4 8 10 12.70 2.70 -10 9 10 0.10 2.60 9 -9 -10 -0.60 2.40 -9 9 10 0.60 2.30 8 -9 -10 16.80 3.00 7 -9 -10 13.50 2.60 6 -9 -10 4.60 2.20 5 -9 -10 0.90 2.00 4 -9 -10 3.40 2.20 -3 9 10 0.20 1.90 -2 9 10 18.90 2.80 -1 9 10 9.70 2.30 0 -9 -10 3.70 1.70 0 9 10 8.40 2.30 -1 -9 -10 3.90 1.90 1 9 10 6.20 2.30 -2 -9 -10 52.29 4.40 2 9 10 57.29 4.70 -3 -9 -10 -0.40 2.00 3 9 10 0.50 2.40 8 -10 -10 0.00 2.50 7 -10 -10 6.50 2.50 6 -10 -10 -0.10 2.30 5 -10 -10 -1.20 2.30 -3 10 10 32.80 3.50 -2 10 10 4.70 2.30 -1 10 10 1.80 2.10 0 -10 -10 3.20 2.00 0 10 10 0.20 2.60 -1 -10 -10 -2.10 2.20 1 10 10 0.60 2.40 -2 -10 -10 -0.10 2.10 5 -11 -10 0.70 2.60 -4 11 10 15.20 2.90 -3 11 10 13.50 2.80 -3 -14 11 1.50 2.60 2 14 -11 19.60 3.00 -2 -14 11 22.80 3.30 1 14 -11 16.00 2.70 -1 -14 11 12.60 2.80 0 14 -11 2.10 2.30 0 -14 11 2.00 2.40 -1 14 -11 -0.50 2.40 1 -14 11 -0.10 2.70 -2 14 -11 -0.60 2.50 2 -14 11 2.40 2.70 -3 14 -11 75.99 5.90 3 -14 11 83.99 6.00 -4 14 -11 0.90 2.10 4 -14 11 -0.90 2.40 4 13 -11 0.90 3.30 -4 -13 11 -0.50 2.30 3 13 -11 -0.40 2.10 -3 -13 11 -1.10 2.20 2 13 -11 7.30 2.50 -2 -13 11 8.50 2.60 1 13 -11 -0.30 1.90 -1 -13 11 0.90 2.40 0 13 -11 15.10 2.70 0 -13 11 16.50 2.70 -1 13 -11 26.00 3.00 1 -13 11 26.30 3.10 -2 13 -11 15.90 2.50 2 -13 11 11.60 2.50 -3 13 -11 48.00 4.10 3 -13 11 48.90 4.30 -4 13 -11 5.00 2.20 4 -13 11 6.50 2.30 -5 13 -11 4.10 2.20 5 -13 11 3.10 2.40 -6 13 -11 0.60 2.20 6 -13 11 1.50 2.30 5 12 -11 -3.20 2.00 4 12 -11 -0.70 1.90 -4 -12 11 -1.30 2.20 3 12 -11 -0.40 1.90 -3 -12 11 0.20 1.90 2 12 -11 14.40 2.30 -2 -12 11 12.00 2.30 1 12 -11 3.10 1.90 -1 -12 11 5.90 2.20 0 12 -11 11.80 2.20 0 -12 11 15.70 2.30 -1 12 -11 -0.30 1.70 1 -12 11 1.10 1.80 -2 12 -11 14.10 2.40 2 -12 11 16.90 2.50 -3 12 -11 29.50 3.10 3 -12 11 38.00 3.40 -4 12 -11 15.20 2.30 4 -12 11 9.10 2.30 -5 12 -11 5.90 2.10 5 -12 11 6.10 2.20 -6 12 -11 10.50 2.40 6 -12 11 12.40 2.60 -7 12 -11 -0.80 2.10 7 -12 11 4.40 2.30 6 11 -11 3.20 2.10 5 11 -11 5.60 2.30 4 11 -11 1.30 2.00 -4 -11 11 2.20 1.80 3 11 -11 6.10 1.90 -3 -11 11 5.50 2.00 2 11 -11 37.80 3.40 -2 -11 11 32.40 3.20 1 11 -11 -0.40 1.60 -1 -11 11 -1.00 1.60 0 11 -11 -0.60 1.50 0 -11 11 3.60 1.70 -1 11 -11 2.40 1.60 1 -11 11 1.70 1.70 -2 11 -11 -0.40 1.50 2 -11 11 1.80 1.60 -3 11 -11 0.10 1.50 3 -11 11 0.40 1.60 -4 11 -11 3.70 1.70 4 -11 11 2.70 1.70 -5 11 -11 1.40 1.80 5 -11 11 3.20 1.90 -6 11 -11 -1.80 1.80 6 -11 11 0.30 1.70 -7 11 -11 3.20 2.00 7 -11 11 6.10 2.40 -8 11 -11 1.30 2.00 8 -11 11 3.30 2.10 -7 -10 11 0.20 1.80 6 10 -11 3.20 1.80 5 10 -11 6.70 1.90 4 10 -11 44.60 3.60 -4 -10 11 41.40 3.60 3 10 -11 55.99 4.20 2 10 -11 39.90 3.30 -2 -10 11 40.50 3.50 1 10 -11 30.20 3.00 -1 -10 11 36.40 3.00 0 10 -11 0.80 1.40 0 -10 11 0.40 1.60 -1 10 -11 147.39 9.30 1 -10 11 155.08 9.30 -2 10 -11 128.09 8.40 2 -10 11 142.49 8.40 -3 10 -11 14.50 2.00 3 -10 11 15.20 2.10 -4 10 -11 12.60 2.00 4 -10 11 5.30 1.70 -5 10 -11 26.00 2.60 5 -10 11 19.60 2.40 -6 10 -11 8.10 2.00 6 -10 11 11.80 2.10 -7 10 -11 22.70 2.80 7 -10 11 24.70 2.90 -8 10 -11 0.60 1.90 8 -10 11 -0.60 1.90 -9 10 -11 14.00 2.60 9 -10 11 11.40 2.50 -9 -9 11 9.50 2.40 -8 -9 11 7.00 2.00 -7 -9 11 14.60 2.20 6 9 -11 -1.00 1.60 5 9 -11 7.20 1.80 4 9 -11 4.60 1.60 -4 -9 11 7.40 1.90 3 9 -11 26.50 2.60 -3 -9 11 26.80 2.70 2 9 -11 38.30 3.20 -2 -9 11 42.70 3.40 1 9 -11 10.70 1.80 -1 -9 11 8.40 1.60 0 9 -11 75.99 5.10 0 -9 11 74.59 5.00 -1 9 -11 10.40 1.70 1 -9 11 9.40 1.70 -2 9 -11 70.79 4.80 2 -9 11 67.79 4.70 -3 9 -11 10.70 1.60 3 -9 11 10.60 1.70 -4 9 -11 47.50 3.60 4 -9 11 43.90 3.50 -5 9 -11 8.80 1.80 5 -9 11 7.90 1.80 -6 9 -11 -0.60 1.60 6 -9 11 -0.20 1.50 -7 9 -11 15.00 2.20 7 -9 11 12.30 2.20 -8 9 -11 4.10 2.20 8 -9 11 2.20 2.00 -9 9 -11 5.20 2.10 9 -9 11 6.10 2.20 10 8 -11 1.20 2.50 -10 -8 11 1.70 2.10 9 8 -11 34.20 3.40 -9 -8 11 30.30 3.10 -8 -8 11 2.90 1.70 -7 -8 11 0.60 1.60 6 8 -11 44.90 3.50 5 8 -11 -1.20 1.30 4 8 -11 52.49 4.10 -4 -8 11 57.69 4.10 3 8 -11 16.00 2.00 -3 -8 11 14.00 1.80 2 8 -11 -1.70 1.20 -2 -8 11 -0.80 1.20 1 8 -11 7.60 1.60 -1 -8 11 9.00 1.70 0 8 -11 -1.50 1.30 0 -8 11 -0.90 1.20 -1 8 -11 18.80 2.20 1 -8 11 23.40 2.20 -2 8 -11 125.29 7.30 2 -8 11 110.19 7.30 -3 8 -11 14.00 2.00 3 -8 11 15.60 1.90 -4 8 -11 -0.30 1.30 4 -8 11 0.10 1.30 -5 8 -11 7.70 1.80 5 -8 11 6.50 1.70 -6 8 -11 2.50 1.60 6 -8 11 5.60 1.60 -7 8 -11 2.00 1.70 7 -8 11 2.30 1.60 -8 8 -11 -0.90 1.70 8 -8 11 -0.30 1.70 -9 8 -11 5.10 2.10 9 -8 11 9.30 2.20 -10 8 -11 6.80 2.60 11 7 -11 2.10 2.40 -11 -7 11 2.10 2.10 10 7 -11 6.70 2.30 -10 -7 11 6.00 2.00 9 7 -11 3.20 1.90 -9 -7 11 0.80 1.80 8 7 -11 32.50 3.30 -8 -7 11 29.20 2.90 7 7 -11 4.70 1.60 -7 -7 11 3.30 1.60 6 7 -11 -0.50 1.60 5 7 -11 13.40 1.90 4 7 -11 31.30 2.80 3 7 -11 13.00 1.80 -3 -7 11 8.70 1.60 2 7 -11 63.79 4.60 -2 -7 11 74.39 4.60 1 7 -11 23.60 2.40 -1 -7 11 28.00 2.30 0 7 -11 -0.90 1.20 0 -7 11 -0.20 1.10 -1 7 -11 289.27 17.20 1 -7 11 298.07 17.10 -2 7 -11 6.90 1.50 2 -7 11 8.40 1.50 -3 7 -11 3.90 1.40 3 -7 11 6.30 1.40 -4 7 -11 23.40 2.30 4 -7 11 22.60 2.30 -5 7 -11 26.10 2.70 5 -7 11 33.40 2.80 -6 7 -11 2.80 1.50 6 -7 11 1.10 1.40 -7 7 -11 20.30 2.50 7 -7 11 24.10 2.50 -8 7 -11 10.90 2.10 8 -7 11 13.00 2.20 -9 7 -11 9.50 2.20 9 -7 11 10.10 2.30 -10 7 -11 0.40 2.00 10 -7 11 -1.90 2.00 11 6 -11 8.30 2.50 -11 -6 11 2.10 2.10 10 6 -11 26.40 3.10 -10 -6 11 31.20 3.00 9 6 -11 1.90 2.00 -9 -6 11 2.70 1.70 8 6 -11 5.40 2.00 -8 -6 11 8.30 1.70 7 6 -11 -0.80 1.50 -7 -6 11 1.50 1.40 6 6 -11 9.50 1.70 -6 -6 11 8.60 1.70 5 6 -11 16.00 1.90 5 6 -11 20.20 2.20 4 6 -11 75.19 5.00 3 6 -11 0.40 1.10 -3 -6 11 1.30 1.20 2 6 -11 0.50 1.20 -2 -6 11 1.00 1.20 1 6 -11 44.30 3.20 -1 -6 11 44.90 3.20 0 6 -11 9.10 1.60 0 -6 11 10.90 1.50 -1 6 -11 19.20 2.10 1 -6 11 23.00 2.10 -2 6 -11 1.90 1.20 2 -6 11 4.50 1.30 -3 6 -11 0.90 1.20 3 -6 11 0.50 1.10 -4 6 -11 -1.90 1.20 4 -6 11 -0.60 1.20 -5 6 -11 1.90 1.40 5 -6 11 3.00 1.40 -6 6 -11 178.48 11.00 6 -6 11 188.18 11.10 -7 6 -11 1.90 1.50 7 -6 11 1.60 1.50 -8 6 -11 11.80 2.00 8 -6 11 16.80 2.30 -9 6 -11 5.00 1.90 9 -6 11 2.40 1.90 10 -6 11 7.10 2.20 -12 -5 11 1.60 2.20 11 5 -11 -0.20 2.10 -11 -5 11 0.70 1.90 10 5 -11 0.20 1.90 -10 -5 11 1.80 1.70 9 5 -11 9.70 2.30 -9 -5 11 10.20 1.90 8 5 -11 22.50 2.50 -8 -5 11 29.90 2.60 7 5 -11 3.50 1.40 -7 -5 11 2.90 1.40 6 5 -11 22.10 2.20 -6 -5 11 25.10 2.30 5 5 -11 13.90 1.70 5 5 -11 12.40 1.80 4 5 -11 3.10 1.20 4 5 -11 2.40 1.20 3 5 -11 1.60 1.20 -3 -5 11 0.40 1.00 2 5 -11 113.09 7.30 -2 -5 11 124.99 7.20 1 5 -11 168.68 10.10 -1 -5 11 170.78 10.00 0 5 -11 148.89 9.00 0 -5 11 151.38 9.00 -1 5 -11 44.40 3.10 1 -5 11 40.30 3.00 -2 5 -11 -0.60 1.10 2 -5 11 0.30 1.10 -3 5 -11 1.90 1.20 3 -5 11 4.40 1.30 -4 5 -11 26.80 2.50 4 -5 11 29.20 2.50 -5 5 -11 3.40 1.40 5 -5 11 2.10 1.40 -6 5 -11 26.50 2.70 6 -5 11 28.40 2.70 -7 5 -11 3.40 1.70 7 -5 11 2.50 1.50 -8 5 -11 4.20 1.90 8 -5 11 2.90 1.80 9 -5 11 1.10 1.90 10 -5 11 10.00 2.40 12 4 -11 4.90 2.70 -12 -4 11 3.80 2.20 11 4 -11 4.30 2.10 -11 -4 11 4.30 2.20 10 4 -11 41.30 3.70 -10 -4 11 44.00 3.60 9 4 -11 -0.20 1.50 -9 -4 11 -0.10 1.40 8 4 -11 25.40 2.50 -8 -4 11 24.60 2.50 7 4 -11 0.90 1.30 -7 -4 11 -0.90 1.20 6 4 -11 41.20 3.30 -6 -4 11 48.90 3.30 5 4 -11 49.10 3.30 5 4 -11 41.70 3.30 4 4 -11 1.90 1.10 4 4 -11 0.60 1.10 3 4 -11 5.50 1.20 3 4 -11 7.80 1.50 -3 -4 11 8.80 1.20 2 4 -11 105.29 7.00 2 4 -11 121.79 6.90 -2 -4 11 114.69 6.90 1 4 -11 68.29 4.60 -1 -4 11 74.49 4.60 0 4 -11 3.10 1.10 0 -4 11 0.50 1.00 -1 4 -11 16.80 1.90 1 -4 11 18.40 1.80 -2 4 -11 41.00 3.00 2 -4 11 41.50 3.00 -3 4 -11 3.60 1.30 3 -4 11 3.60 1.20 -4 4 -11 0.50 1.20 4 -4 11 -0.40 1.10 -5 4 -11 -1.90 1.30 5 -4 11 -1.00 1.20 -6 4 -11 93.89 5.90 6 -4 11 92.69 6.00 -7 4 -11 21.20 2.20 7 -4 11 13.90 2.10 8 -4 11 10.10 2.10 9 -4 11 0.20 1.90 10 -4 11 2.90 2.20 12 3 -11 2.50 2.00 -12 -3 11 3.30 2.40 11 3 -11 17.40 2.50 -11 -3 11 16.40 2.40 10 3 -11 18.90 2.50 -10 -3 11 21.30 2.50 9 3 -11 7.30 1.80 -9 -3 11 7.80 1.70 8 3 -11 16.80 2.20 -8 -3 11 15.00 2.00 7 3 -11 9.20 1.60 -7 -3 11 11.70 1.60 6 3 -11 63.89 4.10 -6 -3 11 53.39 4.00 5 3 -11 15.40 1.70 -5 -3 11 8.50 1.50 4 3 -11 2.20 1.20 4 3 -11 3.00 1.00 3 3 -11 104.19 6.20 3 3 -11 104.59 6.20 -3 -3 11 94.19 6.10 2 3 -11 2.40 1.10 2 3 -11 3.00 1.00 -2 -3 11 3.20 1.00 1 3 -11 1.00 1.00 1 3 -11 1.20 1.00 -1 -3 11 1.00 1.00 0 3 -11 386.96 23.10 0 -3 11 414.16 23.10 -1 3 -11 0.70 1.20 1 -3 11 0.40 1.00 -2 3 -11 40.20 2.90 2 -3 11 38.90 2.90 -3 3 -11 10.70 1.70 3 -3 11 16.80 1.70 -4 3 -11 3.20 1.20 4 -3 11 0.90 1.20 -5 3 -11 2.20 1.40 5 -3 11 1.20 1.30 -6 3 -11 1.60 1.50 6 -3 11 5.00 1.50 7 -3 11 58.69 4.30 8 -3 11 -0.20 1.70 9 -3 11 13.20 2.40 10 -3 11 10.60 2.50 12 2 -11 1.00 2.40 -12 -2 11 -0.60 1.90 11 2 -11 27.20 3.30 -11 -2 11 43.60 3.40 10 2 -11 10.10 2.00 -10 -2 11 9.50 2.00 9 2 -11 -0.50 1.40 -9 -2 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6 -12 -0.60 1.20 -1 -6 12 0.10 1.10 0 6 -12 5.50 1.40 0 -6 12 7.50 1.50 -1 6 -12 9.90 1.70 1 -6 12 11.20 1.60 -2 6 -12 7.70 1.60 2 -6 12 7.40 1.50 -3 6 -12 0.50 1.50 3 -6 12 -0.10 1.20 -4 6 -12 0.80 1.40 4 -6 12 -0.10 1.30 -5 6 -12 23.90 2.50 5 -6 12 24.20 2.60 -6 6 -12 0.20 1.70 6 -6 12 3.10 1.60 -7 6 -12 -0.70 1.60 7 -6 12 -0.80 1.70 -8 6 -12 0.60 1.80 8 -6 12 0.20 1.80 9 -6 12 5.80 2.30 11 5 -12 -2.50 2.00 -11 -5 12 1.00 2.10 10 5 -12 1.50 2.10 -10 -5 12 1.90 1.90 9 5 -12 0.90 1.70 -9 -5 12 1.00 1.70 8 5 -12 5.70 1.80 -8 -5 12 7.00 1.80 7 5 -12 10.90 1.80 -7 -5 12 10.70 1.90 6 5 -12 1.30 1.30 -6 -5 12 2.70 1.50 5 5 -12 14.20 1.90 5 5 -12 17.80 2.00 4 5 -12 14.10 1.80 3 5 -12 1.40 1.30 2 5 -12 -0.30 1.20 -2 -5 12 -0.40 1.00 1 5 -12 9.30 1.60 -1 -5 12 13.30 1.60 0 5 -12 47.80 3.40 0 -5 12 43.90 3.20 -1 5 -12 84.39 5.30 1 -5 12 78.49 5.20 -2 5 -12 78.09 4.90 2 -5 12 69.39 4.80 -3 5 -12 51.19 3.70 3 -5 12 52.79 3.70 -4 5 -12 69.19 4.40 4 -5 12 58.49 4.30 -5 5 -12 -0.30 1.60 5 -5 12 -1.20 1.40 -6 5 -12 0.30 1.40 6 -5 12 -0.70 1.50 -7 5 -12 7.90 2.00 7 -5 12 8.50 2.00 8 -5 12 1.30 1.70 9 -5 12 9.40 2.30 11 4 -12 15.10 2.60 -11 -4 12 11.50 2.40 10 4 -12 16.10 2.70 -10 -4 12 19.60 2.50 9 4 -12 5.50 1.90 -9 -4 12 8.10 1.90 8 4 -12 91.69 6.10 -8 -4 12 89.19 5.90 7 4 -12 21.40 2.40 -7 -4 12 16.50 2.10 6 4 -12 4.60 1.60 -6 -4 12 5.80 1.50 5 4 -12 -0.60 1.30 -5 -4 12 0.10 1.00 4 4 -12 0.60 1.30 4 4 -12 1.80 1.20 3 4 -12 160.38 10.00 3 4 -12 176.68 10.70 2 4 -12 196.38 11.30 -2 -4 12 184.18 11.20 1 4 -12 1.00 1.20 -1 -4 12 1.50 1.20 0 4 -12 37.40 3.00 0 -4 12 41.80 3.00 -1 4 -12 1.60 1.20 1 -4 12 1.20 1.30 -2 4 -12 1.70 1.30 2 -4 12 1.50 1.20 -3 4 -12 35.80 3.00 3 -4 12 39.20 3.00 -4 4 -12 42.70 3.30 4 -4 12 37.40 3.10 -5 4 -12 116.59 7.30 5 -4 12 116.99 7.40 -6 4 -12 7.00 1.70 6 -4 12 16.70 2.00 7 -4 12 14.00 2.30 8 -4 12 9.60 2.10 9 -4 12 1.70 2.10 12 3 -12 11.10 3.00 -12 -3 12 14.70 3.10 11 3 -12 6.60 2.30 -11 -3 12 4.00 2.10 10 3 -12 1.10 1.90 -10 -3 12 0.90 1.80 9 3 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3 2 -12 2.80 1.20 3 2 -12 0.20 1.20 2 2 -12 1.10 1.30 2 2 -12 1.10 1.30 -2 -2 12 0.30 1.10 1 2 -12 113.79 7.40 1 2 -12 123.99 7.30 -1 -2 12 122.69 7.30 0 2 -12 27.80 2.50 0 2 -12 31.10 3.40 0 -2 12 30.30 2.50 -1 2 -12 6.60 1.40 1 -2 12 11.20 1.50 -2 2 -12 11.30 1.60 2 -2 12 11.80 1.60 -3 2 -12 28.30 2.60 -3 2 -12 30.50 2.60 -4 2 -12 0.10 1.40 -4 2 -12 -1.10 1.40 -5 2 -12 5.90 1.70 -6 2 -12 -0.60 1.60 -7 2 -12 2.30 1.90 -8 2 -12 7.70 2.30 -9 2 -12 1.30 2.80 12 1 -12 7.20 2.50 -12 -1 12 13.80 2.60 11 1 -12 4.20 2.20 -11 -1 12 5.80 2.10 10 1 -12 0.80 1.80 -10 -1 12 0.10 1.80 9 1 -12 0.00 1.70 -9 -1 12 1.20 1.60 8 1 -12 59.99 4.50 -8 -1 12 66.19 4.40 7 1 -12 1.90 1.60 -7 -1 12 1.10 1.30 6 1 -12 23.30 2.40 -6 -1 12 20.10 2.10 5 1 -12 0.20 1.30 -5 -1 12 2.30 1.20 4 1 -12 15.80 1.90 -4 -1 12 17.90 1.90 3 1 -12 1.70 1.40 -3 -1 12 0.40 1.10 2 1 -12 19.10 2.10 2 1 -12 24.70 2.30 1 1 -12 1.20 1.20 1 1 -12 1.10 1.20 -1 -1 12 0.90 1.00 0 1 -12 -0.10 1.10 0 1 -12 0.10 1.10 0 -1 12 -0.60 1.00 -1 1 -12 46.80 3.30 -1 1 -12 45.30 3.30 -2 1 -12 31.50 2.70 -2 1 -12 32.50 2.70 -3 1 -12 16.40 2.00 -4 1 -12 6.80 1.60 -5 1 -12 0.40 1.70 -6 1 -12 35.50 3.40 -7 1 -12 6.80 2.10 -8 1 -12 40.20 3.90 12 0 -12 12.50 2.70 -12 0 12 9.10 2.40 11 0 -12 0.80 2.10 -11 0 12 3.20 2.00 10 0 -12 3.10 2.00 -10 0 12 5.50 1.80 9 0 -12 1.40 1.70 -9 0 12 4.30 1.70 8 0 -12 18.00 2.30 -8 0 12 15.60 2.10 7 0 -12 10.90 2.00 -7 0 12 11.20 1.80 6 0 -12 -0.50 1.40 -6 0 12 -0.50 1.20 5 0 -12 0.20 1.30 -5 0 12 -0.50 1.10 4 0 -12 69.19 4.60 -4 0 12 68.39 4.50 3 0 -12 69.39 4.60 -3 0 12 69.09 4.50 2 0 -12 0.30 1.20 -2 0 12 -0.90 1.10 1 0 -12 198.68 11.20 1 0 -12 180.88 11.10 0 0 -12 8.30 1.40 0 0 -12 9.20 1.40 0 0 -12 10.50 1.60 -1 0 -12 2.30 1.20 -1 0 -12 0.70 1.10 1 0 12 1.10 1.30 -2 0 -12 7.50 1.50 2 0 12 11.30 1.80 -3 0 -12 0.20 1.30 -4 0 -12 -0.10 1.40 -5 0 -12 7.00 1.80 -7 0 -12 5.70 2.10 -8 0 -12 5.80 2.30 12 -1 -12 37.80 3.80 -12 1 12 34.10 3.90 11 -1 -12 9.30 2.50 -11 1 12 14.60 2.40 10 -1 -12 73.69 5.50 -10 1 12 79.69 5.40 9 -1 -12 1.90 2.00 -9 1 12 1.80 1.60 8 -1 -12 3.50 1.90 -8 1 12 1.90 1.50 7 -1 -12 -0.60 1.50 -7 1 12 3.40 1.50 6 -1 -12 23.70 2.50 -6 1 12 22.60 2.30 5 -1 -12 12.00 1.80 -5 1 12 8.80 1.60 4 -1 -12 -0.20 1.30 -4 1 12 -0.90 1.10 3 -1 -12 2.70 1.30 -3 1 12 0.60 1.10 2 -1 -12 3.30 1.40 -2 1 12 3.90 1.30 1 -1 -12 8.90 1.80 1 -1 -12 9.80 1.60 -1 1 12 14.30 1.50 0 -1 -12 15.40 2.10 0 -1 -12 23.30 2.20 -1 -1 -12 16.80 1.80 1 1 12 16.40 1.90 -2 -1 -12 4.80 1.40 2 1 12 5.10 1.50 -3 -1 -12 17.80 2.20 3 1 12 24.20 2.40 -4 -1 -12 0.90 1.50 -5 -1 -12 24.50 2.60 -6 -1 -12 4.00 1.80 -7 -1 -12 1.00 2.00 -8 -1 -12 7.80 2.60 11 -2 -12 19.20 3.00 -11 2 12 28.30 3.00 10 -2 -12 3.60 2.10 -10 2 12 0.90 1.80 9 -2 -12 1.00 1.80 -9 2 12 2.80 1.70 8 -2 -12 2.20 1.70 -8 2 12 -0.20 1.40 7 -2 -12 88.49 6.00 -7 2 12 89.99 5.80 6 -2 -12 1.30 1.60 -6 2 12 1.40 1.30 5 -2 -12 12.80 2.10 -5 2 12 23.20 2.10 4 -2 -12 3.40 1.50 -4 2 12 4.50 1.30 3 -2 -12 171.48 10.40 -3 2 12 172.98 10.30 -2 2 12 67.79 4.40 1 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2.40 1.60 5 2 -14 38.30 3.40 -5 -2 14 33.20 3.00 4 2 -14 1.00 1.50 -4 -2 14 0.20 1.40 -3 -2 14 -0.40 1.40 2 2 -14 3.60 1.50 1 2 -14 12.50 1.80 0 2 -14 1.20 1.40 0 -2 14 0.20 1.40 -1 2 -14 48.80 3.80 1 -2 14 45.00 3.70 -2 2 -14 8.10 1.70 2 -2 14 4.70 1.60 3 -2 14 1.80 1.50 4 -2 14 3.30 1.80 5 -2 14 20.30 2.60 6 -2 14 5.60 2.20 10 1 -14 -0.70 2.20 -10 -1 14 -1.60 2.00 9 1 -14 1.40 2.10 -9 -1 14 0.40 2.00 8 1 -14 4.10 2.00 -8 -1 14 2.30 1.80 7 1 -14 0.40 1.80 -7 -1 14 1.20 1.70 6 1 -14 34.10 3.10 -6 -1 14 29.60 2.90 5 1 -14 0.60 1.70 -5 -1 14 2.40 1.50 4 1 -14 4.30 1.90 -4 -1 14 5.00 1.60 3 1 -14 5.70 1.70 -3 -1 14 6.10 1.60 2 1 -14 25.60 2.60 -2 -1 14 28.70 2.60 1 1 -14 -1.20 1.60 0 1 -14 12.70 1.90 0 -1 14 15.70 1.90 -1 1 -14 0.70 1.70 1 -1 14 0.90 1.60 2 -1 14 31.90 2.90 -3 1 -14 4.00 1.70 -4 1 -14 3.10 1.90 -5 1 -14 19.50 2.70 -6 1 -14 13.30 2.60 10 0 -14 0.10 2.60 -10 0 14 1.40 2.10 9 0 -14 0.60 2.00 -9 0 14 -2.30 1.90 8 0 -14 2.20 2.00 -8 0 14 -1.80 1.80 7 0 -14 17.10 2.60 -7 0 14 25.60 2.60 6 0 -14 5.10 2.00 -6 0 14 6.60 1.80 5 0 -14 14.20 2.20 -5 0 14 10.50 1.90 4 0 -14 17.20 2.30 -4 0 14 14.00 2.00 3 0 -14 2.30 1.60 -3 0 14 -1.10 1.30 2 0 -14 -0.60 1.70 -2 0 14 -0.30 1.30 1 0 -14 0.10 1.50 -1 0 14 -1.70 1.50 0 0 -14 0.00 1.60 -1 0 -14 -1.40 1.60 -2 0 -14 4.70 1.70 -3 0 -14 11.90 2.10 -4 0 -14 1.40 1.90 -5 0 -14 0.50 2.40 -6 0 -14 6.00 2.40 10 -1 -14 1.80 2.30 -10 1 14 1.90 2.20 9 -1 -14 4.90 2.60 -9 1 14 4.20 2.10 8 -1 -14 7.10 2.20 -8 1 14 4.70 1.90 7 -1 -14 5.20 2.10 -7 1 14 8.90 2.00 6 -1 -14 32.80 3.40 -6 1 14 37.50 3.20 5 -1 -14 57.99 4.60 -5 1 14 63.79 4.40 4 -1 -14 16.30 2.50 -4 1 14 17.80 2.30 3 -1 -14 -0.40 1.70 -3 1 14 0.20 1.40 2 -1 -14 -0.20 1.60 -2 1 14 0.60 1.40 1 -1 -14 -0.20 1.60 0 1 14 2.60 1.60 -1 -1 -14 3.80 1.80 -2 -1 -14 0.40 1.60 -3 -1 -14 0.50 1.80 -4 -1 -14 4.70 2.00 -5 -1 -14 1.00 2.50 10 -2 -14 1.70 2.40 -10 2 14 -0.20 2.90 9 -2 -14 3.40 2.30 -9 2 14 0.90 2.10 8 -2 -14 2.00 2.20 -8 2 14 2.70 2.00 7 -2 -14 2.60 2.10 -7 2 14 4.50 1.90 6 -2 -14 4.30 2.10 -6 2 14 3.60 1.70 5 -2 -14 -0.80 2.00 -5 2 14 0.50 1.50 4 -2 -14 7.50 2.00 -4 2 14 12.40 1.90 3 -2 -14 11.20 2.30 -3 2 14 12.70 1.90 2 -2 -14 0.70 2.00 1 -2 -14 55.49 4.30 0 2 14 15.00 2.30 -1 -2 -14 -1.00 1.50 1 2 14 -0.50 1.90 -2 -2 -14 44.80 4.00 -3 -2 -14 2.00 1.90 -4 -2 -14 2.90 2.30 -5 -2 -14 12.20 2.60 9 -3 -14 1.30 2.40 -9 3 14 1.20 2.20 8 -3 -14 -1.00 2.20 -8 3 14 -0.70 2.10 7 -3 -14 3.40 2.20 -7 3 14 2.60 1.80 6 -3 -14 -0.10 2.00 -6 3 14 0.70 1.90 5 -3 -14 5.00 2.40 -5 3 14 10.40 1.90 4 -3 -14 2.50 1.90 3 -3 -14 114.99 7.50 2 -3 -14 1.00 1.80 -1 3 14 0.00 1.80 0 3 14 1.30 2.00 -1 -3 -14 25.10 2.80 1 3 14 18.50 2.70 -2 -3 -14 10.40 2.50 2 3 14 13.70 2.40 -3 -3 -14 3.30 2.20 -4 -3 -14 1.60 2.20 -9 4 14 16.10 2.80 8 -4 -14 3.30 2.40 -8 4 14 1.70 2.10 7 -4 -14 17.80 3.00 -7 4 14 25.70 3.00 6 -4 -14 0.30 2.20 -6 4 14 0.90 2.00 5 -4 -14 2.10 2.00 4 -4 -14 0.00 2.00 3 -4 -14 10.50 2.30 2 -4 -14 0.30 2.00 -1 4 14 -0.60 2.00 0 4 14 1.40 2.00 -1 -4 -14 7.60 2.50 1 4 14 5.50 2.30 -2 -4 -14 -0.50 2.00 2 4 14 -0.30 2.20 -3 -4 -14 5.10 2.30 3 4 14 5.90 2.60 -8 5 14 -0.70 2.20 7 -5 -14 4.50 2.40 -7 5 14 5.50 2.40 6 -5 -14 -0.80 2.20 5 -5 -14 2.50 2.30 4 -5 -14 0.60 2.20 3 -5 -14 1.30 2.20 -2 5 14 15.70 2.70 -1 5 14 17.80 2.80 0 5 14 3.10 2.30 1 5 14 1.20 2.30 -2 -5 -14 1.90 2.20 2 5 14 4.70 2.60 6 -6 -14 4.00 2.50 5 -6 -14 4.20 2.50 4 -6 -14 46.70 4.40 3 -6 -14 36.40 3.90 -2 6 14 8.30 2.70 -1 6 14 7.80 2.60 0 6 14 -3.10 2.70 -1 -11 15 0.60 2.80 0 -11 15 6.30 2.60 1 -11 15 2.10 2.50 2 -11 15 0.50 2.40 3 10 -15 4.20 2.40 2 10 -15 0.60 2.30 1 10 -15 0.00 2.20 -1 -10 15 0.00 2.10 0 10 -15 20.30 2.80 0 -10 15 19.10 3.10 -1 10 -15 0.20 2.10 1 -10 15 1.00 2.20 -2 10 -15 -0.30 2.30 2 -10 15 -1.00 2.20 -3 10 -15 4.40 2.70 3 -10 15 2.70 2.40 5 9 -15 4.60 2.80 4 9 -15 5.40 2.50 3 9 -15 7.30 2.30 2 9 -15 26.40 3.10 1 9 -15 5.60 2.20 -1 -9 15 4.10 3.20 0 9 -15 15.50 2.60 0 -9 15 15.40 2.70 -1 9 -15 2.10 2.20 1 -9 15 3.10 2.10 -2 9 -15 1.70 2.40 2 -9 15 0.20 2.00 3 -9 15 31.50 3.40 -4 9 -15 13.60 2.70 4 -9 15 13.30 2.70 -6 -8 15 5.50 2.60 5 8 -15 8.60 2.40 3 8 -15 17.10 2.80 2 8 -15 2.50 1.90 1 8 -15 20.00 2.70 0 8 -15 -1.20 1.90 0 -8 15 -1.00 1.80 -1 8 -15 9.20 2.30 1 -8 15 15.60 2.50 -2 8 -15 22.50 2.90 2 -8 15 21.10 2.70 -3 8 -15 2.40 2.20 3 -8 15 2.80 2.10 -4 8 -15 12.40 2.50 4 -8 15 8.40 2.40 -5 8 -15 -1.30 2.20 5 -8 15 1.60 2.30 -7 -7 15 12.40 2.50 -6 -7 15 6.20 2.20 5 7 -15 3.10 2.20 4 7 -15 7.20 2.10 3 7 -15 0.40 1.90 2 7 -15 9.60 2.20 1 7 -15 1.30 1.90 0 7 -15 17.20 2.60 0 -7 15 19.20 2.50 -1 7 -15 -1.80 1.80 1 -7 15 0.40 1.70 -2 7 -15 1.30 1.90 2 -7 15 3.50 2.10 -3 7 -15 1.70 2.30 3 -7 15 0.70 1.90 -4 7 -15 19.00 2.80 4 -7 15 20.40 2.70 -5 7 -15 2.80 2.20 5 -7 15 4.20 2.30 -7 -6 15 11.80 2.40 -6 -6 15 2.40 1.90 5 6 -15 2.70 1.90 4 6 -15 6.30 2.00 3 6 -15 59.79 4.60 2 6 -15 6.20 2.00 1 6 -15 1.60 1.80 0 6 -15 1.20 1.90 0 -6 15 2.10 1.60 -1 6 -15 13.50 2.30 1 -6 15 9.80 2.10 -2 6 -15 2.60 1.90 2 -6 15 5.80 1.90 -3 6 -15 0.10 1.90 3 -6 15 1.90 1.80 -4 6 -15 -0.20 2.30 4 -6 15 2.40 2.00 -5 6 -15 0.30 2.10 5 -6 15 1.40 2.10 -8 -5 15 4.00 2.20 -7 -5 15 23.40 2.90 -6 -5 15 8.20 2.10 -5 -5 15 0.30 1.70 4 5 -15 0.20 1.80 3 5 -15 56.49 4.40 2 5 -15 129.39 8.20 1 5 -15 -0.90 1.70 0 5 -15 -0.80 1.70 0 -5 15 0.40 1.50 -1 5 -15 14.80 2.20 1 -5 15 11.40 2.20 -2 5 -15 1.00 1.80 2 -5 15 -1.20 1.90 -3 5 -15 5.80 2.00 3 -5 15 9.20 2.30 -4 5 -15 15.70 2.50 4 -5 15 16.80 2.50 5 -5 15 19.60 2.90 -8 -4 15 0.20 2.30 -7 -4 15 6.70 2.10 -6 -4 15 1.50 1.80 -5 -4 15 3.50 1.70 4 4 -15 0.10 1.80 3 4 -15 6.30 2.10 2 4 -15 4.30 1.80 1 4 -15 9.20 2.10 0 4 -15 11.20 2.20 0 -4 15 22.10 2.20 -1 4 -15 10.00 2.00 1 -4 15 8.00 1.80 -2 4 -15 6.70 2.00 2 -4 15 11.00 2.00 -3 4 -15 30.50 3.10 3 -4 15 27.40 2.90 4 -4 15 -1.90 1.80 5 -4 15 24.50 3.00 9 3 -15 31.90 3.50 8 3 -15 2.10 2.10 -8 -3 15 1.00 2.00 7 3 -15 17.40 3.00 -7 -3 15 11.40 2.30 -6 -3 15 4.80 1.90 -5 -3 15 0.70 1.70 -4 -3 15 16.80 2.20 3 3 -15 77.39 5.40 2 3 -15 -1.10 1.50 1 3 -15 5.70 1.80 0 3 -15 2.30 2.00 -1 3 -15 -0.60 1.60 1 -3 15 -1.20 1.40 -2 3 -15 1.70 1.70 2 -3 15 1.40 1.60 3 -3 15 19.90 2.70 4 -3 15 2.00 2.00 5 -3 15 32.60 3.60 9 2 -15 -0.90 2.20 -9 -2 15 -0.40 2.50 8 2 -15 57.19 4.70 -8 -2 15 58.69 4.60 7 2 -15 1.90 2.00 -7 -2 15 4.70 2.00 6 2 -15 8.10 2.10 -6 -2 15 6.20 2.00 -5 -2 15 5.00 1.80 -4 -2 15 1.20 1.60 -3 -2 15 33.90 3.10 2 2 -15 2.00 1.60 1 2 -15 -0.20 1.60 0 2 -15 2.20 1.70 -1 2 -15 0.20 1.70 1 -2 15 1.10 1.70 2 -2 15 9.30 1.90 3 -2 15 0.90 1.80 4 -2 15 3.20 2.00 5 -2 15 3.00 2.30 9 1 -15 16.20 3.10 -9 -1 15 13.00 2.90 8 1 -15 6.50 2.70 -8 -1 15 7.90 2.20 7 1 -15 -1.50 2.20 -7 -1 15 -0.10 1.90 6 1 -15 34.40 3.50 -6 -1 15 33.70 3.30 5 1 -15 -2.90 1.90 -5 -1 15 1.40 1.70 4 1 -15 13.00 2.20 -4 -1 15 13.70 2.10 -3 -1 15 36.50 3.40 -2 -1 15 0.10 1.40 1 1 -15 1.00 1.60 0 1 -15 12.90 2.20 1 -1 15 4.20 1.80 2 -1 15 27.10 2.80 3 -1 15 1.40 2.10 4 -1 15 6.80 2.30 -5 1 -15 16.50 2.90 9 0 -15 3.40 2.50 -9 0 15 1.50 2.20 8 0 -15 6.80 2.40 -8 0 15 6.40 2.20 7 0 -15 0.00 2.10 -7 0 15 0.10 1.90 6 0 -15 8.60 2.30 -6 0 15 5.70 2.00 5 0 -15 4.90 2.10 -5 0 15 4.30 2.00 4 0 -15 47.10 3.90 -4 0 15 44.20 3.60 3 0 -15 8.70 2.20 -3 0 15 4.90 1.80 2 0 -15 0.60 2.70 -2 0 15 0.10 1.70 -1 0 -15 2.30 1.60 -2 0 -15 6.90 2.30 -3 0 -15 8.20 2.50 -4 0 -15 21.90 2.90 9 -1 -15 1.70 2.70 8 -1 -15 5.50 2.50 -8 1 15 7.80 2.30 7 -1 -15 3.10 2.30 -7 1 15 2.80 2.00 6 -1 -15 3.80 2.50 -6 1 15 1.80 1.80 5 -1 -15 -1.00 1.90 -5 1 15 1.50 2.00 4 -1 -15 27.40 3.20 -4 1 15 35.40 3.20 3 -1 -15 4.30 1.90 -3 1 15 7.10 1.90 2 -1 -15 -1.10 1.70 1 -1 -15 0.30 1.80 -1 -1 -15 20.30 2.60 -2 -1 -15 10.10 2.50 -3 -1 -15 1.20 2.10 -4 -1 -15 2.20 2.20 8 -2 -15 1.80 2.30 -8 2 15 1.30 2.10 7 -2 -15 2.10 2.20 -7 2 15 0.30 2.30 6 -2 -15 1.40 2.20 -6 2 15 2.40 1.90 5 -2 -15 0.60 2.40 -5 2 15 1.60 1.80 4 -2 -15 112.39 7.40 -4 2 15 108.59 7.20 3 -2 -15 30.80 3.30 2 -2 -15 1.70 2.30 -1 2 15 24.80 3.10 -2 -2 -15 30.30 3.20 -3 -2 -15 3.10 2.20 8 -3 -15 4.00 2.60 -8 3 15 8.10 2.50 7 -3 -15 1.50 2.40 -7 3 15 -0.90 2.30 6 -3 -15 4.40 2.40 -6 3 15 4.90 2.30 5 -3 -15 29.80 3.40 4 -3 -15 29.10 3.30 3 -3 -15 0.70 2.40 2 -3 -15 1.70 2.10 -1 3 15 5.60 2.20 0 3 15 -0.70 2.10 1 3 15 1.30 2.70 -2 -3 -15 -0.90 1.90 7 -4 -15 0.20 2.70 -7 4 15 -1.90 2.20 6 -4 -15 2.20 2.40 5 -4 -15 2.20 2.40 4 -4 -15 1.80 2.30 3 -4 -15 10.10 2.60 -2 4 15 5.20 2.40 -1 4 15 -1.80 2.20 0 4 15 0.80 2.70 1 4 15 -1.20 2.40 5 -5 -15 0.50 2.70 4 -5 -15 25.70 3.40 3 -5 -15 4.50 2.60 -2 5 15 -0.50 2.50 -1 5 15 4.30 2.60 0 9 -16 6.00 2.80 0 -9 16 4.70 2.40 1 -9 16 -1.90 2.20 2 -9 16 2.40 2.40 3 8 -16 13.80 2.60 2 8 -16 3.00 2.40 1 8 -16 6.30 2.40 0 8 -16 3.00 2.30 -1 8 -16 1.20 2.50 1 -8 16 0.30 2.10 -2 8 -16 51.09 4.80 2 -8 16 54.19 4.90 -3 8 -16 -1.20 2.20 3 -8 16 -2.10 2.20 5 7 -16 -0.50 2.70 4 7 -16 3.00 2.20 3 7 -16 35.40 3.60 2 7 -16 9.40 2.70 1 7 -16 -1.30 2.00 0 7 -16 5.80 2.20 -1 7 -16 2.20 2.10 1 -7 16 0.20 1.90 -2 7 -16 -0.10 2.10 2 -7 16 4.00 2.40 -3 7 -16 1.20 2.30 3 -7 16 1.00 2.20 -5 -6 16 -0.20 2.20 4 6 -16 24.10 3.00 3 6 -16 1.10 2.10 2 6 -16 -0.40 2.00 1 6 -16 1.50 2.10 0 6 -16 10.10 2.40 -1 6 -16 9.30 2.40 1 -6 16 4.50 2.30 -2 6 -16 33.80 3.60 2 -6 16 39.60 3.70 -3 6 -16 12.40 2.90 3 -6 16 16.90 2.70 -4 6 -16 4.20 2.60 4 -6 16 2.70 2.30 -6 -5 16 2.60 2.20 -5 -5 16 -1.20 2.00 4 5 -16 4.10 2.20 3 5 -16 2.60 2.10 2 5 -16 1.50 2.00 1 5 -16 1.00 2.10 0 5 -16 0.10 1.90 -1 5 -16 50.49 4.30 1 -5 16 50.29 4.30 -2 5 -16 1.60 2.10 2 -5 16 2.20 2.20 -3 5 -16 0.80 2.10 3 -5 16 -0.60 2.30 4 -5 16 12.00 2.60 -7 -4 16 14.50 3.00 -6 -4 16 8.20 2.30 -5 -4 16 0.60 2.00 -4 -4 16 21.70 2.80 3 4 -16 10.70 2.30 2 4 -16 -1.90 1.80 1 4 -16 2.40 2.30 0 4 -16 0.40 2.00 -1 4 -16 18.50 2.70 1 -4 16 19.70 2.60 -2 4 -16 0.20 2.20 2 -4 16 0.80 2.20 3 -4 16 0.30 2.10 -7 -3 16 3.50 2.20 -6 -3 16 1.30 2.10 -5 -3 16 2.60 2.10 -4 -3 16 -1.70 1.80 -3 -3 16 1.70 1.90 2 3 -16 5.20 2.00 1 3 -16 -0.20 1.90 0 3 -16 5.40 2.10 -1 3 -16 39.40 3.70 2 -3 16 6.10 2.10 3 -3 16 -2.30 2.20 4 -3 16 40.40 4.10 -7 -2 16 7.00 2.40 -6 -2 16 0.50 2.00 -5 -2 16 9.00 2.20 -4 -2 16 10.20 2.30 -3 -2 16 7.60 2.00 -2 -2 16 6.60 2.00 1 2 -16 8.30 2.10 0 2 -16 1.00 1.80 2 -2 16 -0.40 1.90 3 -2 16 5.90 2.50 7 1 -16 13.00 2.70 -7 -1 16 15.90 2.70 6 1 -16 1.00 2.20 -6 -1 16 0.60 2.10 -5 -1 16 11.00 2.50 -4 -1 16 5.90 2.00 -3 -1 16 14.00 2.30 -2 -1 16 1.60 2.10 2 -1 16 0.40 2.00 3 -1 16 3.00 2.50 7 0 -16 -0.70 2.30 -7 0 16 1.30 2.20 6 0 -16 1.70 2.20 -6 0 16 -0.80 2.10 5 0 -16 4.60 2.30 -5 0 16 8.00 2.20 4 0 -16 2.90 3.90 -4 0 16 1.50 2.10 -3 0 16 1.80 1.80 2 0 16 13.80 2.60 7 -1 -16 -1.00 2.80 -7 1 16 0.00 2.20 6 -1 -16 6.00 2.50 -6 1 16 2.30 2.20 5 -1 -16 14.30 2.90 -5 1 16 12.00 2.60 4 -1 -16 20.00 2.90 -4 1 16 23.10 2.80 3 -1 -16 0.40 2.10 -2 -1 -16 -2.70 3.90 6 -2 -16 9.60 2.70 -6 2 16 7.40 2.40 5 -2 -16 2.20 2.70 -5 2 16 3.40 2.20 4 -2 -16 0.40 2.50 3 -2 -16 -0.40 2.20 2 -2 -16 1.70 2.60 5 -3 -16 2.50 2.80 4 -3 -16 1.00 2.30 3 -3 -16 2.50 2.80 -2 3 16 13.10 2.80 -1 3 16 -1.50 2.80 2 6 -17 3.70 2.40 1 6 -17 9.20 2.90 0 6 -17 8.80 2.50 -4 -5 17 2.30 2.70 3 5 -17 1.60 2.50 2 5 -17 14.10 2.70 1 5 -17 -1.00 2.60 0 5 -17 1.90 2.30 -1 5 -17 0.20 2.30 -4 -4 17 -0.80 2.20 2 4 -17 4.60 2.30 1 4 -17 9.20 2.50 0 4 -17 -1.60 2.20 -1 4 -17 6.10 2.70 -5 -3 17 1.80 2.20 -4 -3 17 1.90 2.30 -3 -3 17 -1.50 2.10 1 3 -17 6.60 2.60 0 3 -17 0.50 2.10 -5 -2 17 -0.10 2.50 -4 -2 17 3.70 2.20 -3 -2 17 8.60 2.40 -2 -2 17 -0.90 2.10 -1 -2 17 0.40 2.20 -5 -1 17 20.10 3.00 -4 -1 17 2.50 2.20 -3 -1 17 0.00 2.10 -4 0 17 9.00 2.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2015a)' ; _shelx_hkl_checksum 74937 _shelx_res_file ; TITL JTM931_0m_a.res in P-1 JTM931_0m_a.res created by SHELXL-2018/1 at 11:08:21 on 19-Apr-2018 REM Old TITL JTM931_0m in P-1 REM SHELXT solution in P-1 REM R1 0.128, Rweak 0.004, Alpha 0.022, Orientation as input REM Formula found by SHELXT: C40 N8 O3 CELL 0.71073 11.5462 12.5637 13.1721 101.991 97.535 99.847 ZERR 2.000 0.0026 0.0028 0.0030 0.003 0.003 0.003 LATT 1 SFAC C H N O UNIT 80 84 16 6 TEMP -173 SIZE 0.116 0.134 0.21 L.S. 5 BOND $H LIST 4 FMAP 2 PLAN 5 EQIV $1 -x+1, -y+1, -z+1 HTAB N1 O2_$1 HTAB N3 N4 EQIV $2 -x, -y, -z HTAB C1 O1_$2 HTAB C8 O1 EQIV $3 -x, -y+1, -z+1 HTAB N5 O3_$3 HTAB N7 N6 HTAB C28 O2 HTAB O3 N2 EQIV $4 x, y, z-1 HTAB O3 N6_$4 MPLA C2 C3 C4 N2 n1 MPLA C7 > C12 MPLA C14 > C19 MPLA C22 C23 C24 N6 N5 MPLA C27 > C32 MPLA C34 > C39 CONF ACTA 56.3 WGHT 0.056400 FVAR 0.42083 O1 4 -0.240382 0.136656 0.042348 11.00000 0.01942 0.04033 = 0.02907 0.00417 -0.00400 0.00350 N1 3 0.271041 0.267402 0.118624 11.00000 0.01827 0.02691 = 0.02783 0.00873 0.00494 0.00422 H1 2 0.342646 0.317278 0.136669 11.00000 0.04010 N2 3 0.168213 0.299668 0.087489 11.00000 0.02104 0.02617 = 0.02583 0.00832 0.00607 0.00543 N3 3 -0.097995 0.191070 0.190348 11.00000 0.01470 0.02513 = 0.02213 0.00508 0.00061 0.00137 H3A 2 -0.018970 0.216780 0.215522 11.00000 0.02321 N4 3 0.026224 0.224661 0.381128 11.00000 0.01984 0.02630 = 0.02182 0.00459 0.00174 0.00229 C1 1 0.354778 0.104608 0.147628 11.00000 0.02138 0.03245 = 0.03302 0.00885 0.00412 0.00878 H1A 2 0.332579 0.022934 0.118585 11.00000 0.05121 H1B 2 0.372213 0.114444 0.223770 11.00000 0.05102 H1C 2 0.424144 0.134898 0.125548 11.00000 0.05171 C2 1 0.254316 0.158065 0.115927 11.00000 0.02260 0.02386 = 0.02152 0.00590 0.00607 0.00603 C3 1 0.134323 0.116386 0.081397 11.00000 0.02294 0.02155 = 0.02610 0.00599 0.00277 0.00422 H3 2 0.094929 0.037544 0.068742 11.00000 0.03617 C4 1 0.084562 0.206756 0.064291 11.00000 0.02157 0.02288 = 0.01735 0.00469 0.00474 0.00412 C5 1 -0.042104 0.208245 0.021991 11.00000 0.02453 0.02333 = 0.02025 0.00448 0.00107 0.00608 H5A 2 -0.045756 0.285210 0.016834 11.00000 0.02570 H5B 2 -0.067816 0.159139 -0.050990 11.00000 0.02657 C6 1 -0.136840 0.174396 0.085077 11.00000 0.01953 0.02005 = 0.02385 0.00346 0.00102 0.00730 C7 1 -0.163400 0.166599 0.268032 11.00000 0.01910 0.01731 = 0.02489 0.00520 0.00467 0.00269 C8 1 -0.286142 0.125933 0.248424 11.00000 0.02015 0.02527 = 0.03041 0.00683 0.00165 0.00283 H8 2 -0.332178 0.115852 0.177729 11.00000 0.02563 C9 1 -0.342092 0.098083 0.328706 11.00000 0.01981 0.04709 = 0.04213 0.01424 0.00727 -0.00102 H9 2 -0.430372 0.070391 0.312628 11.00000 0.03841 C10 1 -0.277879 0.110761 0.427503 11.00000 0.03015 0.06776 = 0.03867 0.02010 0.01344 -0.00226 H10 2 -0.317218 0.092049 0.485211 11.00000 0.05537 C11 1 -0.156546 0.154209 0.449151 11.00000 0.03003 0.05298 = 0.02827 0.01268 0.00545 0.00086 H11 2 -0.112394 0.162967 0.519846 11.00000 0.04731 C12 1 -0.097686 0.183429 0.370427 11.00000 0.01854 0.02352 = 0.02515 0.00489 0.00462 0.00302 C13 1 0.096063 0.248426 0.469124 11.00000 0.02564 0.03144 = 0.02098 0.00618 0.00363 0.00192 H13 2 0.066810 0.241349 0.534757 11.00000 0.04710 C14 1 0.225092 0.283612 0.478153 11.00000 0.02358 0.02611 = 0.02136 0.00319 0.00125 0.00272 C15 1 0.277799 0.296774 0.390878 11.00000 0.02193 0.03160 = 0.02094 0.00264 0.00031 0.00150 H15 2 0.224333 0.282139 0.322516 11.00000 0.02690 C16 1 0.399899 0.327623 0.401787 11.00000 0.02649 0.03822 = 0.02609 0.00445 0.00615 0.00152 H16 2 0.432337 0.341066 0.341038 11.00000 0.03526 C17 1 0.474089 0.346492 0.499179 11.00000 0.02108 0.03048 = 0.03251 0.00093 -0.00001 0.00310 C18 1 0.420971 0.334465 0.585836 11.00000 0.02732 0.04876 = 0.02501 0.00687 -0.00439 0.00327 H18 2 0.472070 0.348308 0.655370 11.00000 0.03967 C19 1 0.298378 0.303736 0.575943 11.00000 0.02812 0.05086 = 0.02266 0.00861 0.00199 0.00046 H19 2 0.259494 0.295820 0.638986 11.00000 0.04764 C20 1 0.607286 0.379705 0.509719 11.00000 0.02157 0.05585 = 0.04439 0.00379 -0.00087 0.00132 H20A 2 0.642481 0.318760 0.469133 11.00000 0.10102 H20B 2 0.630037 0.448089 0.483251 11.00000 0.07193 H20C 2 0.646933 0.394236 0.583454 11.00000 0.08682 O2 4 0.528504 0.560257 0.824280 11.00000 0.01731 0.03306 = 0.04438 0.01040 0.00588 0.00045 N5 3 0.033818 0.523478 0.814148 11.00000 0.01671 0.02253 = 0.03031 0.00809 0.00506 0.00450 H5 2 -0.025345 0.505632 0.852767 11.00000 0.04485 N6 3 0.150113 0.558052 0.861436 11.00000 0.01787 0.02081 = 0.02434 0.00575 0.00355 0.00335 N7 3 0.366672 0.439534 0.843804 11.00000 0.01591 0.02320 = 0.02644 0.00672 0.00349 0.00314 H7 2 0.286476 0.428980 0.840077 11.00000 0.03734 N8 3 0.215611 0.250885 0.831585 11.00000 0.02318 0.02495 = 0.02226 0.00701 0.00486 0.00293 C21 1 -0.101656 0.481128 0.642523 11.00000 0.02730 0.03718 = 0.04105 0.01477 -0.00631 0.00146 H21A 2 -0.163225 0.488180 0.687853 11.00000 0.08563 H21B 2 -0.116798 0.401892 0.606277 11.00000 0.06464 H21C 2 -0.113536 0.531545 0.594324 11.00000 0.05167 C22 1 0.018552 0.516470 0.709775 11.00000 0.02322 0.02103 = 0.02738 0.00674 -0.00066 0.00224 C23 1 0.130643 0.547991 0.686769 11.00000 0.02647 0.02576 = 0.02377 0.00688 0.00405 0.00329 H23 2 0.152208 0.552320 0.618335 11.00000 0.02991 C24 1 0.208958 0.573277 0.782644 11.00000 0.02196 0.01715 = 0.02514 0.00670 0.00576 0.00472 C25 1 0.340886 0.615443 0.803397 11.00000 0.01986 0.02301 = 0.02712 0.00672 0.00547 0.00021 H25A 2 0.366677 0.681050 0.865949 11.00000 0.02696 H25B 2 0.365647 0.643221 0.743112 11.00000 0.03106 C26 1 0.420677 0.535750 0.825027 11.00000 0.01899 0.02500 = 0.02100 0.00178 0.00248 0.00063 C27 1 0.418563 0.352113 0.868889 11.00000 0.02176 0.02542 = 0.01690 0.00438 0.00318 0.00613 C28 1 0.540557 0.360372 0.897662 11.00000 0.02304 0.03407 = 0.02313 0.00485 0.00306 0.00660 H28 2 0.598218 0.431433 0.898841 11.00000 0.04414 C29 1 0.581760 0.270651 0.924520 11.00000 0.02555 0.04134 = 0.02312 0.00608 0.00347 0.01334 H29 2 0.670118 0.278318 0.948156 11.00000 0.03992 C30 1 0.502658 0.174274 0.924011 11.00000 0.03574 0.03522 = 0.02441 0.00807 0.00591 0.01897 H30 2 0.529097 0.114391 0.944609 11.00000 0.03236 C31 1 0.381728 0.164983 0.893643 11.00000 0.03348 0.02677 = 0.02249 0.00564 0.00661 0.00809 H31 2 0.323251 0.098194 0.894497 11.00000 0.02155 C32 1 0.337868 0.252607 0.863279 11.00000 0.02343 0.02646 = 0.01935 0.00354 0.00515 0.00777 C33 1 0.144671 0.158823 0.785368 11.00000 0.02712 0.02211 = 0.02622 0.00708 0.00813 0.00558 H33 2 0.175106 0.090904 0.769388 11.00000 0.03275 C34 1 0.016361 0.149707 0.755161 11.00000 0.02643 0.02166 = 0.02285 0.00709 0.00737 0.00230 C35 1 -0.056421 0.045796 0.708696 11.00000 0.02867 0.02195 = 0.03939 0.00489 0.01042 0.00230 H35 2 -0.021450 -0.020657 0.691995 11.00000 0.03726 C36 1 -0.178762 0.034140 0.683495 11.00000 0.03025 0.02444 = 0.03777 0.00334 0.00901 -0.00460 H36 2 -0.227675 -0.037907 0.653391 11.00000 0.03981 C37 1 -0.232708 0.125157 0.703952 11.00000 0.02459 0.03047 = 0.02575 0.01012 0.00840 -0.00136 C38 1 -0.159648 0.229136 0.749512 11.00000 0.02860 0.02454 = 0.02748 0.00938 0.00615 0.00542 H38 2 -0.194324 0.292688 0.764534 11.00000 0.02603 C39 1 -0.037361 0.241805 0.774405 11.00000 0.02735 0.02109 = 0.02424 0.00685 0.00330 0.00115 H39 2 0.013174 0.314798 0.808892 11.00000 0.01954 C40 1 -0.366080 0.111826 0.679823 11.00000 0.02556 0.04351 = 0.03548 0.00605 0.00956 0.00025 H40A 2 -0.401394 0.112411 0.744780 11.00000 0.04937 H40B 2 -0.395085 0.174281 0.650863 11.00000 0.05974 H40C 2 -0.404435 0.040951 0.628353 11.00000 0.04472 O3 4 0.153360 0.517071 0.074484 11.00000 0.02628 0.02665 = 0.03097 0.01155 0.00855 0.00782 H3B 2 0.168880 0.447482 0.071983 11.00000 0.06004 H3C 2 0.158006 0.529381 0.012476 11.00000 0.07474 HKLF 4 REM JTM931_0m_a.res in P-1 REM R1 = 0.0463 for 5888 Fo > 4sig(Fo) and 0.0749 for all 8663 data REM 628 parameters refined using 0 restraints END WGHT 0.0564 0.0000 REM Highest difference peak 0.278, deepest hole -0.187, 1-sigma level 0.046 Q1 1 0.2597 0.2602 0.4353 11.00000 0.05 0.28 Q2 1 0.3735 0.2022 0.8512 11.00000 0.05 0.27 Q3 1 0.3768 0.3056 0.8795 11.00000 0.05 0.26 Q4 1 0.2737 0.5754 0.7884 11.00000 0.05 0.25 Q5 1 0.1614 0.3396 0.0498 11.00000 0.05 0.24 ; _shelx_res_checksum 10963 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy O O1 -0.24038(9) 0.13666(9) 0.04235(8) 0.0313(3) Uani d 1 N N1 0.27104(11) 0.26740(10) 0.11862(10) 0.0240(3) Uani d 1 H H1 0.3426(15) 0.3173(14) 0.1367(13) 0.040(5) Uiso d 1 N N2 0.16821(10) 0.29967(10) 0.08749(9) 0.0238(3) Uani d 1 N N3 -0.09799(11) 0.19107(10) 0.19035(9) 0.0213(3) Uani d 1 H H3A -0.0190(13) 0.2168(12) 0.2155(12) 0.023(4) Uiso d 1 N N4 0.02622(10) 0.22466(10) 0.38113(9) 0.0233(3) Uani d 1 C C1 0.35478(14) 0.10461(14) 0.14763(14) 0.0284(3) Uani d 1 H H1A 0.3326(16) 0.0229(16) 0.1186(15) 0.051(5) Uiso d 1 H H1B 0.3722(16) 0.1144(15) 0.2238(16) 0.051(5) Uiso d 1 H H1C 0.4241(17) 0.1349(15) 0.1255(15) 0.052(6) Uiso d 1 C C2 0.25432(12) 0.15807(11) 0.11593(11) 0.0222(3) Uani d 1 C C3 0.13432(13) 0.11639(12) 0.08140(11) 0.0236(3) Uani d 1 H H3 0.0949(14) 0.0375(13) 0.0687(13) 0.036(5) Uiso d 1 C C4 0.08456(12) 0.20676(11) 0.06429(11) 0.0205(3) Uani d 1 C C5 -0.04210(13) 0.20825(13) 0.02199(11) 0.0229(3) Uani d 1 H H5A -0.0458(12) 0.2852(13) 0.0168(12) 0.026(4) Uiso d 1 H H5B -0.0678(13) 0.1591(12) -0.0510(13) 0.027(4) Uiso d 1 C C6 -0.13684(12) 0.17440(11) 0.08508(11) 0.0213(3) Uani d 1 C C7 -0.16340(12) 0.16660(11) 0.26803(11) 0.0204(3) Uani d 1 C C8 -0.28614(13) 0.12593(12) 0.24842(13) 0.0257(3) Uani d 1 H H8 -0.3322(13) 0.1159(12) 0.1777(12) 0.026(4) Uiso d 1 C C9 -0.34209(15) 0.09808(15) 0.32871(14) 0.0366(4) Uani d 1 H H9 -0.4304(15) 0.0704(13) 0.3126(13) 0.038(5) Uiso d 1 C C10 -0.27788(15) 0.11076(17) 0.42750(15) 0.0452(5) Uani d 1 H H10 -0.3172(17) 0.0920(15) 0.4852(16) 0.055(6) Uiso d 1 C C11 -0.15655(15) 0.15421(15) 0.44915(14) 0.0375(4) Uani d 1 H H11 -0.1124(15) 0.1630(14) 0.5198(15) 0.047(5) Uiso d 1 C C12 -0.09769(12) 0.18343(11) 0.37043(11) 0.0226(3) Uani d 1 C C13 0.09606(13) 0.24843(13) 0.46912(12) 0.0265(3) Uani d 1 H H13 0.0668(15) 0.2413(14) 0.5348(14) 0.047(5) Uiso d 1 C C14 0.22509(13) 0.28361(12) 0.47815(11) 0.0246(3) Uani d 1 C C15 0.27780(13) 0.29677(12) 0.39088(12) 0.0262(3) Uani d 1 H H15 0.2243(13) 0.2821(12) 0.3225(12) 0.027(4) Uiso d 1 C C16 0.39990(14) 0.32762(14) 0.40179(13) 0.0312(4) Uani d 1 H H16 0.4323(14) 0.3411(13) 0.3410(13) 0.035(5) Uiso d 1 C C17 0.47409(13) 0.34649(13) 0.49918(12) 0.0297(4) Uani d 1 C C18 0.42097(15) 0.33447(15) 0.58584(13) 0.0354(4) Uani d 1 H H18 0.4721(15) 0.3483(13) 0.6554(14) 0.040(5) Uiso d 1 C C19 0.29838(14) 0.30374(15) 0.57594(13) 0.0350(4) Uani d 1 H H19 0.2595(15) 0.2958(14) 0.6390(14) 0.048(5) Uiso d 1 C C20 0.60729(15) 0.37970(19) 0.50972(17) 0.0432(5) Uani d 1 H H20A 0.642(2) 0.319(2) 0.469(2) 0.101(9) Uiso d 1 H H20B 0.6300(18) 0.4481(18) 0.4833(17) 0.072(7) Uiso d 1 H H20C 0.647(2) 0.3942(19) 0.583(2) 0.087(8) Uiso d 1 O O2 0.52850(9) 0.56026(9) 0.82428(9) 0.0319(3) Uani d 1 N N5 0.03382(10) 0.52348(10) 0.81415(10) 0.0228(3) Uani d 1 H H5 -0.0253(16) 0.5056(14) 0.8528(14) 0.045(5) Uiso d 1 N N6 0.15011(10) 0.55805(9) 0.86144(9) 0.0210(3) Uani d 1 N N7 0.36667(11) 0.43953(10) 0.84380(9) 0.0218(3) Uani d 1 H H7 0.2865(15) 0.4290(13) 0.8401(13) 0.037(5) Uiso d 1 N N8 0.21561(10) 0.25089(10) 0.83158(9) 0.0234(3) Uani d 1 C C21 -0.10166(15) 0.48113(16) 0.64252(16) 0.0361(4) Uani d 1 H H21A -0.163(2) 0.4882(19) 0.6879(19) 0.086(8) Uiso d 1 H H21B -0.1168(17) 0.4019(18) 0.6063(16) 0.065(6) Uiso d 1 H H21C -0.1135(15) 0.5315(15) 0.5943(15) 0.052(5) Uiso d 1 C C22 0.01855(13) 0.51647(11) 0.70978(12) 0.0245(3) Uani d 1 C C23 0.13064(13) 0.54799(12) 0.68677(12) 0.0255(3) Uani d 1 H H23 0.1522(13) 0.5523(12) 0.6183(13) 0.030(4) Uiso d 1 C C24 0.20896(12) 0.57328(11) 0.78264(11) 0.0209(3) Uani d 1 C C25 0.34089(13) 0.61544(12) 0.80340(13) 0.0236(3) Uani d 1 H H25A 0.3667(13) 0.6811(12) 0.8659(12) 0.027(4) Uiso d 1 H H25B 0.3656(13) 0.6432(12) 0.7431(13) 0.031(4) Uiso d 1 C C26 0.42068(12) 0.53575(12) 0.82503(11) 0.0228(3) Uani d 1 C C27 0.41856(12) 0.35211(11) 0.86889(11) 0.0213(3) Uani d 1 C C28 0.54056(13) 0.36037(13) 0.89766(12) 0.0270(3) Uani d 1 H H28 0.5982(15) 0.4314(15) 0.8988(13) 0.044(5) Uiso d 1 C C29 0.58176(14) 0.27065(13) 0.92452(12) 0.0295(4) Uani d 1 H H29 0.6701(15) 0.2783(13) 0.9482(13) 0.040(5) Uiso d 1 C C30 0.50266(14) 0.17427(14) 0.92401(12) 0.0301(4) Uani d 1 H H30 0.5291(14) 0.1144(13) 0.9446(13) 0.032(4) Uiso d 1 C C31 0.38173(14) 0.16498(13) 0.89364(12) 0.0272(3) Uani d 1 H H31 0.3233(13) 0.0982(12) 0.8945(11) 0.022(4) Uiso d 1 C C32 0.33787(12) 0.25261(12) 0.86328(11) 0.0229(3) Uani d 1 C C33 0.14467(13) 0.15882(12) 0.78537(12) 0.0245(3) Uani d 1 H H33 0.1751(14) 0.0909(13) 0.7694(12) 0.033(4) Uiso d 1 C C34 0.01636(13) 0.14971(12) 0.75516(11) 0.0234(3) Uani d 1 C C35 -0.05642(14) 0.04580(13) 0.70870(13) 0.0303(4) Uani d 1 H H35 -0.0215(14) -0.0207(14) 0.6920(13) 0.037(5) Uiso d 1 C C36 -0.17876(14) 0.03414(13) 0.68350(13) 0.0324(4) Uani d 1 H H36 -0.2277(15) -0.0379(14) 0.6534(13) 0.040(5) Uiso d 1 C C37 -0.23271(13) 0.12516(12) 0.70395(12) 0.0269(3) Uani d 1 C C38 -0.15965(14) 0.22914(13) 0.74951(12) 0.0263(3) Uani d 1 H H38 -0.1943(13) 0.2927(12) 0.7645(12) 0.026(4) Uiso d 1 C C39 -0.03736(13) 0.24180(12) 0.77441(12) 0.0246(3) Uani d 1 H H39 0.0132(12) 0.3148(12) 0.8089(11) 0.020(4) Uiso d 1 C C40 -0.36608(15) 0.11183(16) 0.67982(15) 0.0358(4) Uani d 1 H H40A -0.4014(16) 0.1124(14) 0.7448(15) 0.049(5) Uiso d 1 H H40B -0.3951(17) 0.1743(17) 0.6509(15) 0.060(6) Uiso d 1 H H40C -0.4044(15) 0.0410(15) 0.6284(14) 0.045(5) Uiso d 1 O O3 0.15336(9) 0.51707(9) 0.07448(9) 0.0266(2) Uani d 1 H H3B 0.1689(17) 0.4475(17) 0.0720(16) 0.060(6) Uiso d 1 H H3C 0.1580(19) 0.5294(18) 0.0125(19) 0.075(7) Uiso d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0194(6) 0.0403(6) 0.0291(6) 0.0035(5) -0.0040(4) 0.0042(5) N1 0.0183(6) 0.0269(7) 0.0278(7) 0.0042(5) 0.0049(5) 0.0087(5) N2 0.0210(6) 0.0262(7) 0.0258(7) 0.0054(5) 0.0061(5) 0.0083(5) N3 0.0147(6) 0.0251(6) 0.0221(6) 0.0014(5) 0.0006(5) 0.0051(5) N4 0.0198(6) 0.0263(6) 0.0218(6) 0.0023(5) 0.0017(5) 0.0046(5) C1 0.0214(8) 0.0325(9) 0.0330(9) 0.0088(7) 0.0041(7) 0.0089(7) C2 0.0226(8) 0.0239(7) 0.0215(7) 0.0060(6) 0.0061(6) 0.0059(6) C3 0.0229(8) 0.0215(8) 0.0261(8) 0.0042(6) 0.0028(6) 0.0060(6) C4 0.0216(7) 0.0229(7) 0.0173(7) 0.0041(6) 0.0047(6) 0.0047(6) C5 0.0245(8) 0.0233(8) 0.0202(8) 0.0061(6) 0.0011(6) 0.0045(6) C6 0.0195(7) 0.0200(7) 0.0239(7) 0.0073(6) 0.0010(6) 0.0035(6) C7 0.0191(7) 0.0173(7) 0.0249(7) 0.0027(5) 0.0047(6) 0.0052(6) C8 0.0202(8) 0.0253(8) 0.0304(9) 0.0028(6) 0.0017(6) 0.0068(6) C9 0.0198(8) 0.0471(10) 0.0421(10) -0.0010(7) 0.0073(7) 0.0142(8) C10 0.0302(10) 0.0678(13) 0.0387(11) -0.0023(9) 0.0134(8) 0.0201(9) C11 0.0300(9) 0.0530(11) 0.0283(9) 0.0009(8) 0.0054(7) 0.0127(8) C12 0.0185(7) 0.0235(7) 0.0252(8) 0.0030(6) 0.0046(6) 0.0049(6) C13 0.0256(8) 0.0314(8) 0.0210(8) 0.0019(6) 0.0036(6) 0.0062(6) C14 0.0236(8) 0.0261(8) 0.0214(7) 0.0027(6) 0.0013(6) 0.0032(6) C15 0.0219(8) 0.0316(8) 0.0209(8) 0.0015(6) 0.0003(6) 0.0026(6) C16 0.0265(9) 0.0382(9) 0.0261(8) 0.0015(7) 0.0061(7) 0.0045(7) C17 0.0211(8) 0.0305(8) 0.0325(9) 0.0031(6) 0.0000(6) 0.0009(7) C18 0.0273(9) 0.0488(10) 0.0250(9) 0.0033(8) -0.0044(7) 0.0069(7) C19 0.0281(9) 0.0509(11) 0.0227(8) 0.0005(8) 0.0020(7) 0.0086(7) C20 0.0216(9) 0.0559(13) 0.0444(12) 0.0013(8) -0.0009(8) 0.0038(10) O2 0.0173(5) 0.0331(6) 0.0444(7) 0.0004(4) 0.0059(5) 0.0104(5) N5 0.0167(6) 0.0225(6) 0.0303(7) 0.0045(5) 0.0051(5) 0.0081(5) N6 0.0179(6) 0.0208(6) 0.0243(6) 0.0033(5) 0.0036(5) 0.0058(5) N7 0.0159(6) 0.0232(6) 0.0264(7) 0.0031(5) 0.0035(5) 0.0067(5) N8 0.0232(6) 0.0250(6) 0.0223(6) 0.0029(5) 0.0049(5) 0.0070(5) C21 0.0273(9) 0.0372(10) 0.0410(10) 0.0015(8) -0.0063(8) 0.0148(8) C22 0.0232(8) 0.0210(7) 0.0274(8) 0.0022(6) -0.0007(6) 0.0067(6) C23 0.0265(8) 0.0258(8) 0.0238(8) 0.0033(6) 0.0041(6) 0.0069(6) C24 0.0220(7) 0.0171(7) 0.0251(8) 0.0047(6) 0.0058(6) 0.0067(6) C25 0.0199(8) 0.0230(8) 0.0271(8) 0.0002(6) 0.0055(6) 0.0067(6) C26 0.0190(7) 0.0250(7) 0.0210(7) 0.0006(6) 0.0025(6) 0.0018(6) C27 0.0218(7) 0.0254(7) 0.0169(7) 0.0061(6) 0.0032(6) 0.0044(6) C28 0.0230(8) 0.0341(9) 0.0231(8) 0.0066(7) 0.0031(6) 0.0049(6) C29 0.0256(8) 0.0413(9) 0.0231(8) 0.0133(7) 0.0035(7) 0.0061(7) C30 0.0357(9) 0.0352(9) 0.0244(8) 0.0190(8) 0.0059(7) 0.0081(7) C31 0.0335(9) 0.0268(8) 0.0225(8) 0.0081(7) 0.0066(7) 0.0056(6) C32 0.0234(8) 0.0265(8) 0.0194(7) 0.0078(6) 0.0052(6) 0.0035(6) C33 0.0271(8) 0.0221(8) 0.0262(8) 0.0056(6) 0.0081(6) 0.0071(6) C34 0.0264(8) 0.0217(7) 0.0228(8) 0.0023(6) 0.0074(6) 0.0071(6) C35 0.0287(9) 0.0219(8) 0.0394(9) 0.0023(7) 0.0104(7) 0.0049(7) C36 0.0302(9) 0.0244(8) 0.0378(10) -0.0046(7) 0.0090(7) 0.0033(7) C37 0.0246(8) 0.0305(8) 0.0257(8) -0.0014(6) 0.0084(6) 0.0101(6) C38 0.0286(8) 0.0245(8) 0.0275(8) 0.0054(7) 0.0061(6) 0.0094(6) C39 0.0274(8) 0.0211(7) 0.0242(8) 0.0011(6) 0.0033(6) 0.0068(6) C40 0.0256(9) 0.0435(11) 0.0355(10) 0.0003(8) 0.0096(7) 0.0061(8) O3 0.0263(6) 0.0266(6) 0.0310(6) 0.0078(5) 0.0085(5) 0.0116(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C2 N1 N2 112.77(12) C2 N1 H1 126.3(10) N2 N1 H1 120.9(10) C4 N2 N1 104.56(11) C6 N3 C7 128.49(12) C6 N3 H3A 118.4(9) C7 N3 H3A 113.0(9) C13 N4 C12 122.39(13) C2 C1 H1A 110.3(10) C2 C1 H1B 111.5(11) H1A C1 H1B 105.2(15) C2 C1 H1C 110.8(11) H1A C1 H1C 110.7(15) H1B C1 H1C 108.1(15) N1 C2 C3 105.96(12) N1 C2 C1 121.99(13) C3 C2 C1 132.05(14) C2 C3 C4 105.94(13) C2 C3 H3 125.1(9) C4 C3 H3 128.9(9) N2 C4 C3 110.77(12) N2 C4 C5 120.30(12) C3 C4 C5 128.88(13) C4 C5 C6 117.61(12) C4 C5 H5A 107.9(8) C6 C5 H5A 106.3(8) C4 C5 H5B 110.6(8) C6 C5 H5B 106.5(8) H5A C5 H5B 107.4(12) O1 C6 N3 123.85(13) O1 C6 C5 120.84(13) N3 C6 C5 115.30(12) C8 C7 N3 123.57(13) C8 C7 C12 119.98(13) N3 C7 C12 116.44(12) C9 C8 C7 119.49(15) C9 C8 H8 120.4(9) C7 C8 H8 120.1(9) C10 C9 C8 120.69(15) C10 C9 H9 121.6(10) C8 C9 H9 117.7(10) C9 C10 C11 120.54(16) C9 C10 H10 121.1(11) C11 C10 H10 118.3(11) C10 C11 C12 120.21(16) C10 C11 H11 119.5(10) C12 C11 H11 120.3(11) C11 C12 C7 119.00(13) C11 C12 N4 125.82(14) C7 C12 N4 115.11(12) N4 C13 C14 121.94(14) N4 C13 H13 121.9(10) C14 C13 H13 116.1(10) C19 C14 C15 118.66(14) C19 C14 C13 119.64(14) C15 C14 C13 121.70(13) C16 C15 C14 120.17(14) C16 C15 H15 122.5(9) C14 C15 H15 117.3(9) C15 C16 C17 121.55(15) C15 C16 H16 117.6(10) C17 C16 H16 120.7(10) C18 C17 C16 117.97(14) C18 C17 C20 121.12(15) C16 C17 C20 120.91(15) C19 C18 C17 121.03(15) C19 C18 H18 120.0(10) C17 C18 H18 119.0(10) C18 C19 C14 120.62(15) C18 C19 H19 121.2(10) C14 C19 H19 118.2(10) C17 C20 H20A 112.0(14) C17 C20 H20B 111.1(12) H20A C20 H20B 108.0(19) C17 C20 H20C 111.5(14) H20A C20 H20C 105.7(19) H20B C20 H20C 108.4(18) C22 N5 N6 112.71(12) C22 N5 H5 126.5(11) N6 N5 H5 120.8(11) C24 N6 N5 104.31(11) C26 N7 C27 128.61(12) C26 N7 H7 116.3(10) C27 N7 H7 115.1(10) C33 N8 C32 119.62(13) C22 C21 H21A 109.1(13) C22 C21 H21B 110.9(11) H21A C21 H21B 105.8(18) C22 C21 H21C 111.2(10) H21A C21 H21C 105.3(16) H21B C21 H21C 114.0(16) N5 C22 C23 106.25(13) N5 C22 C21 121.78(14) C23 C22 C21 131.97(15) C22 C23 C24 105.66(13) C22 C23 H23 128.0(9) C24 C23 H23 126.3(9) N6 C24 C23 111.07(13) N6 C24 C25 120.87(13) C23 C24 C25 128.03(13) C24 C25 C26 118.03(12) C24 C25 H25A 111.9(8) C26 C25 H25A 104.5(8) C24 C25 H25B 109.9(9) C26 C25 H25B 106.3(9) H25A C25 H25B 105.3(12) O2 C26 N7 123.63(14) O2 C26 C25 120.04(13) N7 C26 C25 116.33(12) C28 C27 C32 120.48(13) C28 C27 N7 123.96(13) C32 C27 N7 115.56(12) C29 C28 C27 119.24(15) C29 C28 H28 120.9(10) C27 C28 H28 119.9(10) C30 C29 C28 120.68(15) C30 C29 H29 120.4(9) C28 C29 H29 118.8(9) C31 C30 C29 120.25(15) C31 C30 H30 118.3(10) C29 C30 H30 121.5(10) C30 C31 C32 120.37(15) C30 C31 H31 121.9(8) C32 C31 H31 117.7(8) C31 C32 C27 118.86(13) C31 C32 N8 124.36(13) C27 C32 N8 116.71(12) N8 C33 C34 122.69(14) N8 C33 H33 120.2(9) C34 C33 H33 117.1(9) C35 C34 C39 118.27(14) C35 C34 C33 119.59(13) C39 C34 C33 122.11(13) C36 C35 C34 120.77(15) C36 C35 H35 118.7(9) C34 C35 H35 120.5(9) C35 C36 C37 121.15(15) C35 C36 H36 119.8(10) C37 C36 H36 119.0(10) C36 C37 C38 117.97(14) C36 C37 C40 121.10(14) C38 C37 C40 120.91(15) C39 C38 C37 121.34(15) C39 C38 H38 119.0(9) C37 C38 H38 119.7(9) C38 C39 C34 120.47(14) C38 C39 H39 120.9(8) C34 C39 H39 118.6(8) C37 C40 H40A 110.8(10) C37 C40 H40B 114.9(11) H40A C40 H40B 104.2(15) C37 C40 H40C 112.1(10) H40A C40 H40C 107.4(14) H40B C40 H40C 106.9(15) H3B O3 H3C 106.3(19) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C6 1.2205(16) N1 C2 1.3464(18) N1 N2 1.3595(16) N1 H1 0.918(17) N2 C4 1.3333(17) N3 C6 1.3608(18) N3 C7 1.4021(18) N3 H3A 0.907(15) N4 C13 1.2695(19) N4 C12 1.4136(18) C1 C2 1.492(2) C1 H1A 0.993(19) C1 H1B 0.974(19) C1 H1C 0.935(19) C2 C3 1.374(2) C3 C4 1.4019(19) C3 H3 0.987(16) C4 C5 1.4999(19) C5 C6 1.515(2) C5 H5A 0.991(15) C5 H5B 1.004(16) C7 C8 1.3920(19) C7 C12 1.4134(19) C8 C9 1.383(2) C8 H8 0.982(15) C9 C10 1.374(2) C9 H9 0.998(16) C10 C11 1.382(2) C10 H10 0.98(2) C11 C12 1.389(2) C11 H11 0.976(18) C13 C14 1.461(2) C13 H13 0.984(18) C14 C19 1.395(2) C14 C15 1.395(2) C15 C16 1.377(2) C15 H15 0.986(15) C16 C17 1.397(2) C16 H16 0.960(17) C17 C18 1.388(2) C17 C20 1.503(2) C18 C19 1.383(2) C18 H18 0.987(17) C19 H19 1.009(18) C20 H20A 1.02(3) C20 H20B 1.00(2) C20 H20C 0.98(3) O2 C26 1.2322(17) N5 C22 1.3453(19) N5 N6 1.3596(16) N5 H5 0.928(18) N6 C24 1.3410(17) N7 C26 1.3484(18) N7 C27 1.4137(18) N7 H7 0.906(17) N8 C33 1.2775(18) N8 C32 1.4137(18) C21 C22 1.487(2) C21 H21A 0.99(3) C21 H21B 0.99(2) C21 H21C 1.00(2) C22 C23 1.379(2) C23 C24 1.396(2) C23 H23 0.976(16) C24 C25 1.493(2) C25 C26 1.516(2) C25 H25A 1.008(16) C25 H25B 0.987(16) C27 C28 1.390(2) C27 C32 1.408(2) C28 C29 1.388(2) C28 H28 1.014(18) C29 C30 1.385(2) C29 H29 1.009(17) C30 C31 1.379(2) C30 H30 0.935(16) C31 C32 1.396(2) C31 H31 0.986(14) C33 C34 1.461(2) C33 H33 0.971(16) C34 C35 1.394(2) C34 C39 1.397(2) C35 C36 1.383(2) C35 H35 0.985(16) C36 C37 1.388(2) C36 H36 0.955(17) C37 C38 1.394(2) C37 C40 1.504(2) C38 C39 1.381(2) C38 H38 0.949(15) C39 H39 0.981(14) C40 H40A 0.994(19) C40 H40B 1.03(2) C40 H40C 0.992(18) O3 H3B 0.92(2) O3 H3C 0.87(2) loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA N1 H1 O2 2_666 0.92(2) 1.88(2) 2.7863(18) 169(2) O3 H3B N2 . 0.92(2) 1.91(2) 2.8047(19) 165(2) O3 H3C N6 1_554 0.87(2) 2.09(2) 2.9530(18) 174(2) N5 H5 O3 2_566 0.93(2) 1.878(19) 2.8014(18) 173(2) N7 H7 N6 . 0.91(2) 2.447(17) 3.1314(19) 132.6(13) C1 H1A O1 2_555 0.99(2) 2.56(2) 3.436(2) 146.9(15) C8 H8 O1 . 0.98(2) 2.228(15) 2.858(2) 120.8(12) C28 H28 O2 . 1.01(2) 2.265(18) 2.890(2) 118.5(13) C35 H35 N4 2_556 0.99(2) 2.532(18) 3.451(2) 155.2(13) N3 H3A Cg1 . 0.91(2) 2.999(15) 3.6216(17) 127.4(12) C5 H5B Cg6 1_554 1.00(2) 2.820(16) 3.7171(18) 149.0(12) C11 H11 Cg6 . 0.98(2) 2.837(19) 3.713(2) 149.8(14) C15 H15 Cg1 . 0.99(2) 2.913(15) 3.7979(19) 149.8(12) C20 H20B Cg3 2_666 1.00(2) 2.88(2) 3.772(3) 148.9(16) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C2 N1 N2 C4 -0.19(15) N2 N1 C2 C3 -0.09(16) N2 N1 C2 C1 -179.53(13) N1 C2 C3 C4 0.31(16) C1 C2 C3 C4 179.67(15) N1 N2 C4 C3 0.39(15) N1 N2 C4 C5 -177.40(12) C2 C3 C4 N2 -0.45(17) C2 C3 C4 C5 177.10(13) N2 C4 C5 C6 -120.07(14) C3 C4 C5 C6 62.6(2) C7 N3 C6 O1 2.3(2) C7 N3 C6 C5 -178.85(12) C4 C5 C6 O1 -154.35(13) C4 C5 C6 N3 26.74(18) C6 N3 C7 C8 -4.5(2) C6 N3 C7 C12 174.38(13) N3 C7 C8 C9 176.28(14) C12 C7 C8 C9 -2.6(2) C7 C8 C9 C10 0.4(3) C8 C9 C10 C11 1.6(3) C9 C10 C11 C12 -1.3(3) C10 C11 C12 C7 -0.9(3) C10 C11 C12 N4 -177.53(16) C8 C7 C12 C11 2.8(2) N3 C7 C12 C11 -176.12(13) C8 C7 C12 N4 179.83(12) N3 C7 C12 N4 0.90(18) C13 N4 C12 C11 -6.3(2) C13 N4 C12 C7 176.92(13) C12 N4 C13 C14 175.65(13) N4 C13 C14 C19 -177.01(15) N4 C13 C14 C15 2.4(2) C19 C14 C15 C16 0.8(2) C13 C14 C15 C16 -178.54(14) C14 C15 C16 C17 0.0(2) C15 C16 C17 C18 -0.7(2) C15 C16 C17 C20 179.76(16) C16 C17 C18 C19 0.6(3) C20 C17 C18 C19 -179.91(17) C17 C18 C19 C14 0.3(3) C15 C14 C19 C18 -1.0(2) C13 C14 C19 C18 178.41(15) C22 N5 N6 C24 0.17(15) N6 N5 C22 C23 0.04(16) N6 N5 C22 C21 -179.52(13) N5 C22 C23 C24 -0.23(16) C21 C22 C23 C24 179.27(16) N5 N6 C24 C23 -0.32(15) N5 N6 C24 C25 177.99(12) C22 C23 C24 N6 0.35(16) C22 C23 C24 C25 -177.80(14) N6 C24 C25 C26 75.24(18) C23 C24 C25 C26 -106.77(17) C27 N7 C26 O2 2.3(2) C27 N7 C26 C25 -178.09(13) C24 C25 C26 O2 167.33(13) C24 C25 C26 N7 -12.3(2) C26 N7 C27 C28 12.5(2) C26 N7 C27 C32 -167.60(13) C32 C27 C28 C29 -2.3(2) N7 C27 C28 C29 177.62(13) C27 C28 C29 C30 -0.8(2) C28 C29 C30 C31 2.0(2) C29 C30 C31 C32 -0.1(2) C30 C31 C32 C27 -2.9(2) C30 C31 C32 N8 -179.62(13) C28 C27 C32 C31 4.1(2) N7 C27 C32 C31 -175.82(12) C28 C27 C32 N8 -178.92(12) N7 C27 C32 N8 1.15(18) C33 N8 C32 C31 -30.9(2) C33 N8 C32 C27 152.35(13) C32 N8 C33 C34 176.83(12) N8 C33 C34 C35 -177.46(14) N8 C33 C34 C39 0.4(2) C39 C34 C35 C36 -0.7(2) C33 C34 C35 C36 177.20(14) C34 C35 C36 C37 -0.2(2) C35 C36 C37 C38 0.8(2) C35 C36 C37 C40 -177.95(15) C36 C37 C38 C39 -0.4(2) C40 C37 C38 C39 178.34(14) C37 C38 C39 C34 -0.6(2) C35 C34 C39 C38 1.1(2) C33 C34 C39 C38 -176.75(13) _cod_database_fobs_code 2242815