#------------------------------------------------------------------------------ #$Date: 2019-11-16 08:08:04 +0200 (Sat, 16 Nov 2019) $ #$Revision: 227940 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/31/2243199.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243199 loop_ _publ_author_name 'Daoui, Said' '\,C\?inar, Emine Berrin' 'El Kalai, Fouad' 'Saddik, Rafik' 'Dege, Necmi' 'Karrouchi, Khalid' 'Benchat, Noureddine' _publ_section_title ; Crystal structure, Hirshfeld surface analysis and DFT studies of 6-[(E)-2-(thiophen-2-yl)ethenyl]-4,5-dihydropyridazin-3(2H)-one ; _journal_coeditor_code MW2150 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 1880 _journal_page_last 1883 _journal_paper_doi 10.1107/S2056989019015147 _journal_volume 75 _journal_year 2019 _chemical_formula_iupac 'C10 H10 N2 O S' _chemical_formula_moiety 'C10 H10 N2 O S' _chemical_formula_sum 'C10 H10 N2 O S' _chemical_formula_weight 206.26 _chemical_name_systematic ; 6-[(E)-2-(Thiophen-2-yl)ethenyl]-4,5-dihydropyridazin-3(2H)-one ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2015 _cell_angle_alpha 90 _cell_angle_beta 110.168(6) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.9932(5) _cell_length_b 16.2916(9) _cell_length_c 9.3544(7) _cell_measurement_reflns_used 6992 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 29.98 _cell_measurement_theta_min 2.32 _cell_volume 1000.40(12) _computing_cell_refinement ; X-AREA (Stoe & Cie, 2002) ; _computing_data_collection ; X-AREA (Stoe & Cie, 2002) ; _computing_data_reduction ; X-RED32 (Stoe & Cie, 2002) ; _computing_molecular_graphics ; PLATON (Spek, 2009) and Mercury (Macrae et al., 2008) ; _computing_publication_material ; WinGX (Farrugia, 2012) and PLATON (Spek, 2009) ; _computing_structure_refinement ; SHELXL2015 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2015 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296(2) _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device '2-circle goniometer' _diffrn_measurement_device_type 'Stoe IPDS 2' _diffrn_measurement_method 'rotation method' _diffrn_radiation_monochromator 'plane graphite' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0432 _diffrn_reflns_av_unetI/netI 0.0382 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 6292 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.995 _diffrn_reflns_theta_min 2.500 _diffrn_source 'sealed X-ray tube, 12 x 0.4 mm long-fine focus' _diffrn_source_current 45 _diffrn_source_power 2.25 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.290 _exptl_absorpt_correction_T_max 0.9316 _exptl_absorpt_correction_T_min 0.7665 _exptl_absorpt_correction_type integration _exptl_absorpt_process_details ; (X-RED32; Stoe & Cie, 2002) ; _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.369 _exptl_crystal_description stick _exptl_crystal_F_000 432 _exptl_crystal_size_max 0.780 _exptl_crystal_size_mid 0.430 _exptl_crystal_size_min 0.250 _refine_diff_density_max 0.241 _refine_diff_density_min -0.343 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.022 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 131 _refine_ls_number_reflns 1971 _refine_ls_number_restraints 19 _refine_ls_restrained_S_all 1.035 _refine_ls_R_factor_all 0.0657 _refine_ls_R_factor_gt 0.0446 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0790P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1265 _refine_ls_wR_factor_ref 0.1346 _reflns_number_gt 1394 _reflns_number_total 1971 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file mw2150sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2243199 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 1 0 0 87.22 4.40 0 -1 0 0 91.84 4.00 0 2 0 0 92.99 3.30 0 -2 0 0 91.09 3.29 0 3 0 0 159.58 3.16 0 -3 0 0 184.47 3.60 0 -4 0 0 383.65 4.43 0 4 0 0 358.21 4.36 0 5 0 0 57.74 2.49 0 -5 0 0 61.38 2.57 0 -6 0 0 17.31 2.47 0 6 0 0 17.37 2.26 0 -7 0 0 1.20 2.29 0 7 0 0 1.51 2.32 0 8 0 0 20.62 2.89 0 -8 0 0 29.62 2.99 0 -9 0 0 0.93 3.35 0 9 0 0 3.01 3.18 0 -1 1 0 209.27 7.21 0 -1 -1 0 191.80 5.16 0 1 -1 0 177.50 6.97 0 1 1 0 190.81 5.16 0 -2 1 0 166.35 4.31 0 2 1 0 157.50 3.65 0 -2 -1 0 157.89 3.64 0 2 -1 0 158.30 4.22 0 -3 -1 0 305.28 4.24 0 3 1 0 293.85 4.17 0 3 -1 0 293.30 4.56 0 -3 1 0 307.52 4.71 0 -4 1 0 65.20 2.62 0 4 -1 0 65.01 2.55 0 -4 -1 0 73.82 2.47 0 4 1 0 66.44 2.43 0 -5 -1 0 7.24 2.06 0 5 1 0 8.02 2.11 0 5 -1 0 6.26 2.05 0 -5 1 0 7.26 1.55 0 -6 -1 0 9.48 1.61 0 6 -1 0 11.91 2.08 0 -6 1 0 13.62 2.25 0 6 1 0 12.03 2.36 0 -7 1 0 1.56 2.40 0 7 1 0 4.45 2.20 0 -7 -1 0 1.31 2.32 0 7 -1 0 3.06 2.35 0 8 1 0 0.18 2.60 0 -8 -1 0 0.44 2.68 0 8 -1 0 0.44 2.69 0 -8 1 0 1.01 2.79 0 9 1 0 1.33 3.22 0 9 -1 0 -0.17 3.25 0 -9 1 0 0.06 3.36 0 -9 -1 0 -0.79 3.21 0 0 -2 0 1185.62 15.28 0 0 2 0 1132.39 15.44 0 1 -2 0 41.54 4.87 0 -1 2 0 41.55 4.96 0 -1 -2 0 36.71 2.34 0 1 2 0 36.77 2.35 0 2 -2 0 1844.20 14.50 0 -2 2 0 1823.91 14.38 0 2 2 0 1881.61 10.25 0 -2 -2 0 1832.19 9.84 0 3 -2 0 324.81 5.05 0 -3 2 0 336.74 5.11 0 3 2 0 331.91 4.20 0 -3 -2 0 347.61 4.29 0 4 -2 0 4.35 1.89 0 4 2 0 4.54 1.88 0 -4 -2 0 5.34 1.36 0 -4 2 0 5.22 2.02 0 -5 2 0 1.32 2.13 0 5 2 0 1.82 1.86 0 -5 -2 0 0.63 1.92 0 5 -2 0 0.52 1.99 0 -6 2 0 3.97 2.42 0 6 2 0 3.03 2.24 0 -6 -2 0 2.47 2.24 0 6 -2 0 3.54 1.99 0 -7 -2 0 -1.10 2.32 0 7 2 0 2.38 2.31 0 -7 2 0 1.17 2.40 0 7 -2 0 1.05 2.44 0 8 2 0 1.71 2.78 0 -8 -2 0 -0.60 2.59 0 8 -2 0 -0.31 2.68 0 -8 2 0 1.15 2.94 0 -9 2 0 0.18 3.29 0 9 2 0 0.84 3.22 0 -9 -2 0 2.78 3.31 0 9 -2 0 -0.60 3.42 0 1 3 0 36.42 2.70 0 1 -3 0 41.64 5.09 0 -1 -3 0 38.31 2.66 0 -2 -3 0 30.28 2.38 0 -2 3 0 33.99 3.50 0 2 -3 0 31.44 2.88 0 2 3 0 31.23 2.31 0 -3 -3 0 207.85 3.09 0 -3 3 0 224.55 4.87 0 3 3 0 204.37 3.12 0 3 -3 0 200.92 4.35 0 -4 3 0 8.23 2.14 0 4 3 0 8.45 1.93 0 -4 -3 0 6.99 1.38 0 4 -3 0 6.66 2.02 0 -5 -3 0 43.18 1.74 0 5 3 0 40.30 2.33 0 -5 3 0 43.88 2.65 0 5 -3 0 40.47 2.46 0 -6 -3 0 9.42 2.15 0 -6 3 0 9.59 2.48 0 6 -3 0 8.64 2.13 0 6 3 0 8.19 1.67 0 7 -3 0 0.16 2.32 0 -7 -3 0 2.54 2.55 0 -7 3 0 0.53 2.42 0 7 3 0 -0.04 1.67 0 8 -3 0 1.31 2.84 0 8 3 0 -0.53 2.73 0 -8 3 0 0.62 3.48 0 -8 -3 0 1.37 2.78 0 9 3 0 0.98 3.25 0 0 -4 0 5705.76 23.30 0 0 4 0 5280.01 23.94 0 1 4 0 394.60 5.59 0 -1 -4 0 410.81 5.18 0 1 -4 0 433.43 9.85 0 1 -4 0 437.72 9.70 0 2 4 0 48.63 2.06 0 2 -4 0 49.48 3.91 0 -2 -4 0 49.92 2.05 0 -2 4 0 54.65 4.29 0 3 4 0 123.41 2.88 0 -3 -4 0 131.82 2.89 0 -3 4 0 128.92 4.42 0 3 -4 0 123.42 4.22 0 4 4 0 19.27 2.06 0 4 -4 0 21.61 2.62 0 -4 4 0 24.03 2.88 0 -4 -4 0 23.37 1.98 0 5 -4 0 6.69 2.07 0 -5 -4 0 9.26 2.17 0 5 4 0 8.15 2.16 0 -5 4 0 7.23 2.30 0 6 -4 0 22.57 2.54 0 6 4 0 24.63 2.25 0 -6 4 0 25.27 3.34 0 -6 -4 0 20.87 2.30 0 7 4 0 1.64 2.44 0 -7 -4 0 1.93 1.74 0 -7 4 0 2.59 2.58 0 7 -4 0 0.62 2.70 0 -8 4 0 3.73 3.11 0 8 4 0 5.42 2.75 0 -8 -4 0 2.65 2.10 0 8 -4 0 2.68 3.58 0 1 -5 0 648.30 9.84 0 -1 -5 0 626.68 5.82 0 1 5 0 570.10 5.86 0 -2 -5 0 144.04 3.15 0 2 -5 0 141.92 6.74 0 2 5 0 139.32 3.13 0 3 5 0 91.15 2.59 0 -3 -5 0 86.12 2.49 0 -3 5 0 94.70 4.65 0 3 -5 0 85.02 4.34 0 4 5 0 62.73 1.97 0 4 -5 0 68.77 3.07 0 -4 5 0 74.83 3.71 0 -4 -5 0 75.33 2.48 0 -5 -5 0 91.06 2.64 0 -5 5 0 96.09 3.39 0 5 -5 0 90.94 3.56 0 5 5 0 80.41 2.66 0 -6 5 0 4.55 2.50 0 6 -5 0 5.03 2.23 0 -6 -5 0 5.74 1.60 0 6 5 0 4.37 2.20 0 -7 5 0 13.65 3.49 0 7 -5 0 12.92 2.72 0 -7 -5 0 12.51 1.94 0 7 5 0 16.66 2.55 0 -8 -5 0 1.07 2.84 0 -8 5 0 0.62 3.61 0 8 -5 0 1.12 3.49 0 8 5 0 0.82 2.84 0 0 6 0 895.59 8.39 0 0 -6 0 1019.14 8.36 0 1 6 0 97.25 2.94 0 -1 -6 0 115.78 2.94 0 1 -6 0 110.85 3.85 0 2 -6 0 267.91 8.78 0 -2 -6 0 266.69 3.70 0 2 -6 0 256.42 8.11 0 2 6 0 236.05 3.68 0 3 6 0 210.72 2.97 0 3 -6 0 224.31 7.47 0 -3 -6 0 222.12 2.95 0 -3 6 0 227.02 7.38 0 4 -6 0 22.46 2.77 0 -4 6 0 24.90 3.01 0 -4 -6 0 21.04 1.58 0 4 6 0 20.48 2.10 0 5 -6 0 3.63 2.10 0 5 6 0 3.69 2.06 0 -5 -6 0 3.06 2.06 0 -5 6 0 4.34 2.85 0 6 6 0 38.63 1.96 0 -6 6 0 43.46 3.64 0 -6 -6 0 40.07 1.87 0 6 -6 0 41.05 3.33 0 7 6 0 1.08 2.52 0 7 -6 0 1.23 2.53 0 -7 6 0 1.33 3.25 0 -7 -6 0 1.08 1.72 0 8 -6 0 1.34 3.61 0 -8 -6 0 2.34 2.86 0 8 6 0 -0.38 1.97 0 -8 6 0 0.79 3.77 0 -1 -7 0 88.16 2.32 0 1 7 0 80.05 2.35 0 1 -7 0 89.55 3.46 0 2 -7 0 11.28 3.41 0 -2 -7 0 11.06 1.96 0 2 7 0 8.15 1.90 0 2 -7 0 10.05 2.94 0 3 7 0 1.88 1.26 0 -3 -7 0 1.09 1.32 0 -4 7 0 4.79 3.31 0 -4 -7 0 5.28 2.00 0 4 7 0 6.68 1.98 0 4 -7 0 4.55 3.61 0 -5 7 0 7.04 3.30 0 -5 -7 0 6.57 1.50 0 5 -7 0 7.03 3.17 0 5 7 0 8.11 2.14 0 -6 -7 0 1.35 2.26 0 6 7 0 0.42 1.48 0 6 -7 0 -0.05 3.26 0 -6 7 0 0.77 3.00 0 7 -7 0 6.73 3.40 0 -7 7 0 7.40 3.57 0 -7 -7 0 5.11 1.89 0 7 7 0 5.64 1.95 0 -8 -7 0 2.78 2.94 0 8 7 0 0.05 2.81 0 -8 7 0 0.16 3.86 0 0 8 0 855.85 7.53 0 0 -8 0 966.47 7.26 0 1 8 0 123.63 2.70 0 1 -8 0 146.43 3.80 0 -1 -8 0 141.44 2.68 0 2 -8 0 269.34 6.86 0 -2 -8 0 249.65 3.14 0 2 -8 0 265.29 6.66 0 2 8 0 237.04 3.48 0 -3 -8 0 18.93 1.55 0 3 8 0 17.41 2.07 0 -4 -8 0 56.84 2.30 0 4 8 0 53.64 2.35 0 -5 -8 0 10.47 2.31 0 5 8 0 8.29 1.55 0 -6 8 0 1.18 4.25 0 -6 -8 0 1.72 1.65 0 6 8 0 1.61 1.57 0 7 8 0 3.61 1.78 0 -7 8 0 1.99 5.11 0 -7 -8 0 1.40 2.55 0 8 8 0 0.68 2.07 0 -8 -8 0 2.36 2.09 0 1 9 0 42.57 2.35 0 1 -9 0 50.93 2.62 0 -1 -9 0 51.15 2.35 0 2 -9 0 60.40 3.60 0 2 -9 0 58.21 3.67 0 -2 -9 0 59.01 2.42 0 2 9 0 50.42 2.34 0 3 9 0 34.21 2.26 0 -3 -9 0 37.89 2.26 0 -4 -9 0 5.33 2.05 0 4 9 0 5.26 1.47 0 5 9 0 10.20 1.63 0 -5 -9 0 15.30 2.23 0 6 9 0 3.42 1.70 0 -6 -9 0 2.60 2.44 0 7 9 0 2.42 2.57 0 -7 -9 0 -0.76 1.89 0 8 9 0 0.45 2.16 0 -8 -9 0 0.74 2.97 0 0 -10 0 0.71 1.80 0 0 10 0 0.49 1.79 0 1 -10 0 25.20 2.25 0 -1 -10 0 23.95 2.11 0 1 10 0 19.90 2.12 0 2 10 0 288.48 3.75 0 2 -10 0 332.35 6.21 0 -2 -10 0 340.41 3.78 0 2 -10 0 336.06 6.37 0 3 10 0 3.02 1.99 0 -3 -10 0 1.56 1.37 0 4 10 0 1.59 2.09 0 -4 -10 0 -0.74 2.09 0 5 10 0 2.62 2.14 0 -5 -10 0 1.46 2.17 0 6 10 0 17.97 2.52 0 -6 -10 0 22.41 2.55 0 7 10 0 1.65 2.70 0 -7 -10 0 0.83 1.90 0 -8 -10 0 0.90 3.14 0 8 10 0 2.07 3.12 0 1 11 0 132.33 3.04 0 1 -11 0 159.05 3.50 0 -1 -11 0 151.27 2.99 0 2 11 0 3.97 2.02 0 2 -11 0 3.84 2.34 0 2 -11 0 3.47 2.44 0 -2 -11 0 2.43 2.04 0 3 11 0 174.35 2.75 0 -3 -11 0 211.70 3.21 0 4 11 0 15.71 1.69 0 -4 -11 0 19.89 1.67 0 -5 -11 0 -1.28 1.58 0 5 11 0 0.69 1.59 0 -6 -11 0 2.17 2.48 0 6 11 0 -0.02 2.47 0 -7 -11 0 0.54 2.02 0 7 11 0 1.07 2.70 0 0 12 0 87.85 2.92 0 0 -12 0 108.34 2.84 0 1 12 0 5.60 2.00 0 -1 -12 0 4.43 1.93 0 1 -12 0 7.43 2.08 0 2 -12 0 35.04 3.07 0 -2 -12 0 36.05 2.36 0 2 12 0 28.66 2.31 0 2 -12 0 39.32 3.11 0 -3 -12 0 53.07 2.41 0 3 12 0 38.48 1.81 0 4 12 0 18.53 2.27 0 -4 -12 0 16.10 2.23 0 5 12 0 1.38 2.40 0 -5 -12 0 -0.86 1.68 0 -6 -12 0 5.56 1.84 0 6 12 0 4.02 2.58 0 7 12 0 1.14 2.05 0 -7 -12 0 1.80 2.02 0 -1 -13 0 9.54 2.03 0 1 -13 0 8.23 2.07 0 1 13 0 6.28 1.98 0 -2 -13 0 19.89 2.18 0 2 -13 0 20.60 3.01 0 2 -13 0 23.28 3.02 0 2 13 0 17.93 2.19 0 3 13 0 2.93 2.15 0 -3 -13 0 1.89 2.09 0 4 13 0 1.97 2.24 0 -4 -13 0 0.78 2.20 0 5 13 0 7.77 1.74 0 -5 -13 0 12.48 2.42 0 6 13 0 1.99 1.91 0 -6 -13 0 3.63 2.72 0 -7 -13 0 -0.45 2.06 0 7 13 0 0.52 2.15 0 0 -14 0 18.02 2.15 0 0 14 0 16.19 2.14 0 1 14 0 23.69 2.24 0 -1 -14 0 29.53 2.31 0 1 -14 0 25.30 2.54 0 2 -14 0 87.52 3.79 0 -2 -14 0 74.48 2.10 0 2 14 0 72.66 2.63 0 2 -14 0 90.84 3.72 0 -3 -14 0 2.73 2.26 0 3 14 0 4.32 2.23 0 4 14 0 1.07 1.65 0 -4 -14 0 3.67 1.67 0 -5 -14 0 6.91 2.46 0 5 14 0 5.38 2.51 0 -6 -14 0 3.06 2.79 0 6 14 0 2.06 2.81 0 -7 -14 0 0.98 3.15 0 7 14 0 1.54 3.18 0 1 -15 0 70.28 3.03 0 1 15 0 56.16 2.61 0 -1 -15 0 69.13 2.13 0 -2 -15 0 1.12 2.16 0 2 -15 0 -0.09 2.75 0 2 -15 0 2.30 2.75 0 2 15 0 1.02 2.21 0 3 15 0 25.09 2.40 0 -3 -15 0 30.18 2.37 0 -4 -15 0 0.73 1.83 0 4 15 0 -0.70 2.51 0 5 15 0 -1.08 1.88 0 -5 -15 0 4.07 1.88 0 -6 -15 0 1.50 2.87 0 6 15 0 1.03 2.07 0 0 -16 0 49.84 2.65 0 1 -16 0 13.79 2.85 0 -1 -16 0 18.73 2.34 0 1 16 0 9.97 2.24 0 -2 -16 0 0.80 2.41 0 2 16 0 1.86 2.27 0 2 -16 0 3.33 2.96 0 2 -16 0 2.07 2.36 0 3 16 0 0.60 2.36 0 -3 -16 0 0.66 2.26 0 4 16 0 0.78 2.48 0 -4 -16 0 0.80 1.75 0 5 16 0 2.55 2.77 0 -5 -16 0 2.00 2.00 0 -6 -16 0 -0.80 2.12 0 6 16 0 -0.11 2.92 0 1 -17 0 22.06 2.58 0 -1 -17 0 26.17 2.52 0 1 17 0 18.58 1.91 0 2 -17 0 1.72 2.32 0 2 -17 0 0.64 2.93 0 2 17 0 0.28 2.41 0 -2 -17 0 2.41 2.33 0 3 17 0 13.93 2.66 0 -3 -17 0 11.09 1.83 0 4 17 0 3.15 2.67 0 -4 -17 0 3.42 1.91 0 -5 -17 0 -2.17 2.82 0 5 17 0 1.62 1.93 0 0 -18 0 6.48 2.48 0 1 -18 0 4.55 3.18 0 -1 -18 0 2.98 2.53 0 2 -18 0 7.44 2.88 0 2 18 0 6.40 2.59 0 -2 -18 0 10.18 1.84 0 2 -18 0 9.30 2.81 0 3 18 0 0.74 2.47 0 -3 -18 0 -0.29 2.56 0 -4 -18 0 1.47 2.78 0 4 18 0 0.50 1.94 0 5 18 0 0.62 2.12 0 -5 -18 0 -0.77 2.95 0 -1 -19 0 6.14 2.70 0 1 -19 0 4.80 2.74 0 2 19 0 2.68 2.58 0 -2 -19 0 1.48 2.62 0 2 -19 0 1.30 2.84 0 2 -19 0 2.04 3.36 0 3 19 0 1.66 2.86 0 -3 -19 0 3.60 2.91 0 -4 -19 0 1.57 3.02 0 4 19 0 1.15 1.97 0 0 -20 0 4.51 2.84 0 1 -20 0 1.73 2.90 0 -1 -20 0 1.36 2.80 0 2 -20 0 0.77 3.69 0 2 -20 0 0.77 3.69 0 -2 -20 0 2.19 2.79 0 3 20 0 -0.93 2.83 0 -3 -20 0 0.67 2.93 0 -4 -20 0 0.30 2.18 0 4 20 0 -0.95 3.05 0 1 -21 0 4.63 3.01 0 1 -21 0 2.92 3.02 0 -1 -21 0 3.66 2.91 0 2 -21 0 1.71 3.89 0 2 -21 0 0.52 3.88 0 -2 -21 0 0.59 2.25 0 -3 -21 0 -1.72 3.18 0 0 -22 0 -0.56 3.18 0 -1 -22 0 1.00 3.08 0 1 -22 0 -0.55 4.07 0 1 -22 0 0.92 3.30 0 9 1 -1 -0.21 3.07 0 -9 1 1 0.81 3.27 0 -9 -1 1 -0.21 3.22 0 9 -1 -1 0.53 3.15 0 8 -1 -1 5.34 2.63 0 -8 1 1 4.14 2.72 0 -8 -1 1 7.56 2.71 0 8 1 -1 5.53 2.60 0 7 -1 -1 4.45 2.30 0 -7 -1 1 4.30 1.84 0 -7 1 1 4.77 2.35 0 7 1 -1 3.95 1.76 0 -6 1 1 5.46 2.10 0 6 1 -1 5.26 2.13 0 6 -1 -1 5.44 2.07 0 -6 -1 1 6.05 2.24 0 -5 -1 1 7.37 1.93 0 5 1 -1 9.04 1.98 0 5 -1 -1 7.39 2.03 0 -5 1 1 8.18 2.15 0 4 1 -1 344.98 4.06 0 -4 1 1 375.58 4.78 0 4 -1 -1 363.97 4.74 0 -4 -1 1 357.17 3.96 0 3 -1 -1 19.07 2.07 0 3 1 -1 22.46 2.07 0 -3 1 1 18.22 2.06 0 -3 -1 1 22.91 2.07 0 2 -1 -1 284.03 6.07 0 -2 -1 1 287.98 4.77 0 -2 1 1 269.84 5.71 0 2 1 -1 282.28 4.78 0 -1 1 1 467.36 10.03 0 -1 -1 1 445.59 7.16 0 0 -1 -1 221.78 6.24 0 0 1 1 210.82 5.72 0 0 -1 1 211.48 6.06 0 0 1 -1 203.08 5.88 0 -1 -1 -1 1777.59 11.51 0 1 1 1 1807.12 11.83 0 1 -1 1 1854.87 13.59 0 -1 1 -1 1733.22 12.98 0 -2 1 -1 2.54 1.50 0 -2 -1 -1 3.05 1.45 0 2 1 1 5.39 2.03 0 2 -1 1 3.39 2.01 0 3 1 1 133.98 3.02 0 -3 1 -1 138.74 3.28 0 -3 -1 -1 129.98 3.01 0 3 -1 1 126.23 2.83 0 4 -1 1 36.07 2.24 0 -4 1 -1 34.84 2.35 0 4 1 1 31.43 1.71 0 -4 -1 -1 34.21 1.74 0 -5 -1 -1 13.52 1.60 0 5 -1 1 13.43 1.56 0 5 1 1 13.21 2.10 0 -5 1 -1 14.66 1.68 0 6 -1 1 1.03 2.14 0 6 1 1 0.62 2.22 0 -6 1 -1 2.18 2.23 0 -6 -1 -1 2.09 2.24 0 -7 -1 -1 10.85 2.58 0 7 -1 1 8.50 2.47 0 7 1 1 8.91 2.53 0 -7 1 -1 6.74 2.61 0 -8 -1 -1 2.19 2.90 0 8 -1 1 -1.18 2.81 0 -8 1 -1 1.41 2.98 0 8 1 1 0.70 2.76 0 -9 2 1 -0.43 3.20 0 -9 -2 1 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-5 5 2 0.18 2.63 0 5 5 -2 2.70 2.03 0 -5 -5 2 0.25 1.42 0 -4 -5 2 8.34 1.95 0 -4 5 2 9.04 3.08 0 -4 5 2 9.36 3.10 0 4 5 -2 9.69 1.95 0 -3 5 2 142.36 6.75 0 3 5 -2 131.11 2.87 0 -3 5 2 146.45 7.03 0 -3 -5 2 139.49 2.87 0 -2 5 2 38.62 3.40 0 -2 -5 2 37.20 2.31 0 2 -5 -2 41.31 3.29 0 1 -5 -2 1592.57 11.42 0 -1 5 2 1513.37 11.23 0 -1 -5 2 1456.05 8.38 0 0 -5 2 324.01 4.39 0 0 5 2 332.10 4.81 0 0 -5 -2 360.35 4.82 0 -1 -5 -2 165.08 3.32 0 -1 5 -2 168.23 3.62 0 1 5 2 149.63 2.99 0 1 -5 2 170.33 3.75 0 2 -5 2 351.33 5.00 0 -2 5 -2 357.82 4.90 0 2 5 2 320.12 3.66 0 -2 -5 -2 345.20 3.69 0 3 5 2 34.19 2.23 0 -3 -5 -2 34.09 2.24 0 -3 5 -2 35.72 2.53 0 3 -5 2 36.26 2.55 0 -4 5 -2 0.38 2.27 0 4 -5 2 0.80 2.08 0 4 5 2 0.23 2.11 0 -4 -5 -2 0.44 2.01 0 5 5 2 30.12 1.83 0 5 -5 2 34.99 2.78 0 -5 -5 -2 37.80 2.47 0 -5 5 -2 39.49 3.00 0 6 -5 2 0.97 2.29 0 6 5 2 1.19 2.40 0 -6 5 -2 1.41 2.61 0 -6 -5 -2 0.19 2.36 0 -7 -5 -2 0.80 1.88 0 7 5 2 0.69 2.67 0 7 -5 2 1.75 2.71 0 -7 5 -2 1.03 2.77 0 -8 -5 -2 1.75 3.21 0 8 5 2 2.15 3.05 0 8 -5 2 1.99 3.21 0 -8 5 -2 3.93 3.30 0 -9 -6 2 1.27 3.08 0 -9 6 2 0.12 4.79 0 9 6 -2 3.39 2.17 0 -9 6 2 1.06 4.53 0 -8 6 2 0.82 3.53 0 8 6 -2 1.12 1.86 0 -8 -6 2 0.70 2.03 0 -8 6 2 0.66 3.35 0 -7 6 2 15.15 3.49 0 7 6 -2 12.99 1.86 0 -7 -6 2 14.25 1.88 0 6 6 -2 4.34 2.18 0 -6 6 2 4.38 3.27 0 -6 6 2 4.72 3.13 0 -6 -6 2 4.67 1.52 0 -5 6 2 0.78 3.91 0 -5 6 2 0.51 3.49 0 -5 -6 2 -0.33 2.01 0 5 6 -2 0.61 1.40 0 4 6 -2 109.29 2.71 0 -4 -6 2 109.26 2.25 0 -3 -6 2 2.30 1.25 0 3 6 -2 -0.24 1.76 0 2 -6 -2 665.92 10.34 0 -2 6 2 574.61 9.51 0 -2 -6 2 554.35 4.68 0 -1 -6 2 576.01 5.29 0 1 -6 -2 620.21 6.92 0 -1 6 2 565.80 6.97 0 0 -6 2 168.41 3.45 0 0 6 2 163.07 3.53 0 0 -6 -2 180.13 3.59 0 1 -6 2 -0.28 1.98 0 1 6 2 1.47 1.87 0 -1 -6 -2 0.10 1.93 0 2 6 2 2226.15 9.13 0 -2 -6 -2 2411.20 9.13 0 -2 6 -2 2312.90 11.93 0 2 -6 2 2438.48 12.36 0 3 6 2 2.39 2.03 0 3 -6 2 3.19 2.18 0 -3 6 -2 3.51 2.04 0 -3 -6 -2 2.74 1.46 0 4 6 2 14.64 2.12 0 -4 6 -2 19.00 2.34 0 4 -6 2 18.98 2.41 0 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28.84 2.82 0 -3 -8 -2 27.95 1.75 0 -4 -8 -2 46.92 1.98 0 4 8 2 51.17 2.45 0 4 -8 2 54.23 3.08 0 -4 8 -2 54.80 2.96 0 5 -8 2 31.63 3.20 0 -5 8 -2 28.15 2.70 0 -5 -8 -2 30.30 2.47 0 5 8 2 24.96 1.84 0 -6 8 -2 1.65 2.60 0 6 -8 2 1.11 2.49 0 -6 -8 -2 1.86 2.56 0 6 8 2 0.99 2.50 0 7 -8 2 0.02 3.50 0 7 8 2 -0.63 2.74 0 -7 -8 -2 2.24 2.88 0 -7 8 -2 2.66 3.65 0 8 9 -2 -0.53 2.04 0 -8 -9 2 0.03 2.85 0 7 9 -2 8.19 1.77 0 -7 -9 2 14.27 2.61 0 -6 -9 2 6.29 2.28 0 6 9 -2 5.88 2.29 0 -5 -9 2 12.83 2.21 0 5 9 -2 12.32 2.23 0 -4 -9 2 3.80 2.03 0 4 9 -2 2.43 1.95 0 -3 -9 2 82.51 2.48 0 3 9 -2 72.59 2.47 0 -2 -9 2 4.28 1.34 0 -2 9 2 3.69 2.45 0 2 -9 -2 4.22 2.77 0 -1 -9 2 871.53 5.98 0 -1 9 2 776.87 7.33 0 1 -9 -2 955.29 7.56 0 0 -9 -2 109.92 2.92 0 0 9 2 88.66 2.70 0 0 -9 2 98.99 2.35 0 1 -9 2 2.61 1.94 0 1 9 2 2.04 1.83 0 1 -9 2 0.37 1.94 0 -1 -9 -2 0.77 1.82 0 -2 -9 -2 31.17 2.30 0 2 9 2 25.32 1.71 0 2 -9 2 30.29 3.02 0 3 9 2 88.94 2.23 0 -3 -9 -2 105.50 2.69 0 3 -9 2 103.41 3.63 0 4 9 2 9.75 2.19 0 4 -9 2 8.16 2.27 0 -4 -9 -2 7.65 2.27 0 -4 9 -2 7.55 2.67 0 5 9 2 6.47 2.29 0 -5 -9 -2 5.76 1.69 0 5 -9 2 6.68 2.95 0 -5 9 -2 6.01 3.03 0 6 -9 2 -0.21 3.12 0 6 9 2 0.43 1.78 0 -6 9 -2 0.39 3.27 0 -6 -9 -2 2.45 2.53 0 7 -9 2 0.41 4.23 0 -7 9 -2 0.94 3.67 0 7 9 2 -1.13 2.81 0 -7 -9 -2 3.15 2.00 0 -8 -10 2 1.46 2.96 0 8 10 -2 -0.34 2.93 0 -7 -10 2 1.64 1.88 0 7 10 -2 2.02 2.54 0 -6 -10 2 4.15 2.34 0 6 10 -2 5.41 2.27 0 5 10 -2 41.32 1.94 0 -5 -10 2 48.55 2.48 0 -4 -10 2 4.40 1.40 0 4 10 -2 4.21 1.45 0 -3 -10 2 1.27 1.39 0 3 10 -2 -1.80 1.95 0 -2 10 2 0.68 2.35 0 -2 -10 2 -0.06 1.91 0 2 -10 -2 1.56 2.67 0 1 -10 -2 403.64 5.00 0 -1 -10 2 357.64 3.71 0 -1 10 2 326.14 4.97 0 0 10 2 3.03 1.85 0 0 -10 2 5.34 1.85 0 0 -10 -2 5.21 1.92 0 1 -10 2 34.01 2.35 0 1 -10 2 31.44 2.29 0 1 10 2 28.62 2.14 0 -1 -10 -2 31.75 2.09 0 2 10 2 154.85 2.69 0 2 -10 2 206.41 4.41 0 -2 -10 -2 190.12 2.74 0 2 -10 2 186.28 3.85 0 -3 -10 -2 256.02 2.97 0 3 -10 2 275.39 5.61 0 3 10 2 238.08 3.37 0 4 10 2 1.80 2.20 0 -4 -10 -2 0.91 1.55 0 4 -10 2 1.50 2.78 0 5 10 2 2.01 2.38 0 5 -10 2 0.52 2.90 0 -5 -10 -2 3.57 2.40 0 6 -10 2 -0.01 3.78 0 6 10 2 1.27 2.65 0 -6 -10 -2 1.46 2.64 0 7 10 2 0.69 2.09 0 7 -10 2 0.60 5.75 0 -7 -10 -2 1.49 3.01 0 8 11 -2 1.54 2.02 0 -8 -11 2 1.26 2.94 0 7 11 -2 4.66 2.63 0 -7 -11 2 4.38 2.68 0 6 11 -2 7.34 2.38 0 -6 -11 2 3.54 1.70 0 -5 -11 2 20.70 1.71 0 5 11 -2 18.74 1.70 0 -4 -11 2 45.84 1.85 0 4 11 -2 40.61 1.84 0 -3 -11 2 119.50 2.33 0 3 11 -2 109.68 2.78 0 -2 11 2 -0.09 2.24 0 2 -11 -2 1.03 2.51 0 -2 -11 2 0.71 1.90 0 -1 11 2 13.59 2.21 0 1 -11 -2 17.92 2.23 0 -1 -11 2 16.70 1.52 0 0 -11 2 92.03 2.65 0 0 -11 -2 92.88 2.75 0 0 11 2 82.63 2.69 0 1 11 2 33.49 2.11 0 1 -11 2 41.85 2.48 0 1 -11 2 39.65 2.45 0 -1 -11 -2 39.97 1.80 0 2 -11 2 53.03 2.69 0 2 11 2 49.65 2.44 0 -2 -11 -2 56.94 1.94 0 2 -11 2 61.88 2.90 0 3 11 2 1.83 2.16 0 3 -11 2 3.29 2.73 0 -3 -11 -2 1.19 1.58 0 3 -11 2 2.51 2.55 0 4 -11 2 10.04 3.54 0 4 11 2 10.57 2.34 0 -4 -11 -2 10.28 2.24 0 5 11 2 0.57 1.75 0 5 -11 2 0.47 3.41 0 -5 -11 -2 1.50 1.73 0 6 11 2 1.27 1.94 0 -6 -11 -2 1.47 1.86 0 7 11 2 -3.14 2.18 0 -7 -11 -2 -0.44 2.97 0 -8 -12 2 2.34 3.11 0 8 12 -2 1.57 3.14 0 -7 -12 2 2.00 2.78 0 7 12 -2 -1.14 1.99 0 -6 -12 2 2.74 1.79 0 6 12 -2 3.88 1.73 0 -5 -12 2 -0.92 1.60 0 5 12 -2 -1.19 1.57 0 4 12 -2 76.43 2.19 0 -4 -12 2 90.15 2.71 0 3 12 -2 7.13 2.01 0 -3 -12 2 8.88 2.03 0 -2 12 2 2.76 2.07 0 2 -12 -2 4.23 2.66 0 -2 -12 2 3.52 2.06 0 1 -12 -2 31.27 2.40 0 -1 -12 2 28.50 1.67 0 -1 12 2 24.75 2.28 0 0 12 2 43.97 2.45 0 0 -12 -2 53.03 2.49 0 0 -12 2 52.11 2.49 0 1 12 2 59.94 2.00 0 1 -12 2 70.73 2.70 0 -1 -12 -2 70.09 2.58 0 1 -12 2 71.82 2.71 0 2 -12 2 71.69 2.94 0 2 12 2 62.61 2.50 0 -2 -12 -2 70.81 2.04 0 2 -12 2 76.89 3.15 0 3 -12 2 -0.48 2.55 0 3 12 2 1.36 1.56 0 3 -12 2 -1.07 2.38 0 -3 -12 -2 0.61 1.51 0 4 -12 2 2.85 3.07 0 4 12 2 2.55 2.26 0 -4 -12 -2 4.68 2.31 0 4 -12 2 2.02 3.42 0 5 12 2 1.90 1.77 0 -5 -12 -2 -0.52 1.76 0 -6 -12 -2 2.03 1.97 0 6 12 2 2.27 2.73 0 7 12 2 4.23 3.12 0 -7 -12 -2 -0.55 2.27 0 -7 -13 2 2.62 2.89 0 7 13 -2 0.83 2.07 0 6 13 -2 1.09 1.84 0 -6 -13 2 2.02 2.56 0 5 13 -2 22.72 1.87 0 -5 -13 2 22.01 1.87 0 -4 -13 2 6.17 2.24 0 4 13 -2 5.54 1.57 0 3 13 -2 1.34 2.08 0 -3 -13 2 -0.89 2.14 0 2 -13 -2 31.89 3.26 0 -2 13 2 23.30 2.66 0 -2 -13 2 27.19 1.70 0 -1 -13 2 0.64 1.99 0 -1 13 2 1.20 2.01 0 1 -13 -2 1.05 2.05 0 0 13 2 12.55 2.08 0 0 -13 2 13.84 2.12 0 0 -13 -2 16.76 2.21 0 -1 -13 -2 39.21 2.40 0 1 -13 2 42.87 2.62 0 1 -13 2 40.03 2.45 0 1 13 2 33.25 1.83 0 2 13 2 24.10 1.71 0 2 -13 2 30.66 3.25 0 2 -13 2 29.85 3.04 0 -2 -13 -2 28.73 2.30 0 3 -13 2 0.73 2.74 0 3 -13 2 0.77 3.22 0 -3 -13 -2 3.00 2.25 0 3 13 2 1.43 2.29 0 4 13 2 6.08 2.42 0 4 -13 2 4.86 3.50 0 4 -13 2 4.59 3.60 0 -4 -13 -2 4.77 1.75 0 5 13 2 -2.66 2.68 0 -5 -13 -2 -0.39 1.87 0 6 13 2 -1.15 2.03 0 -6 -13 -2 0.20 1.98 0 -7 -14 2 1.39 2.02 0 7 14 -2 -1.57 2.09 0 6 14 -2 16.86 2.07 0 -6 -14 2 20.37 2.83 0 -5 -14 2 3.45 1.75 0 5 14 -2 2.53 1.74 0 -4 -14 2 0.95 1.60 0 4 14 -2 -0.06 2.24 0 -3 -14 2 0.35 1.55 0 -2 -14 2 89.53 2.22 0 2 -14 -2 108.46 3.62 0 -1 -14 2 0.53 2.10 0 1 -14 -2 1.66 2.21 0 -1 14 2 1.21 2.18 0 0 -14 -2 18.47 2.36 0 0 -14 2 18.80 2.28 0 0 14 2 14.96 2.24 0 1 -14 2 17.30 2.41 0 1 14 2 12.68 1.73 0 1 -14 2 16.15 2.40 0 -1 -14 -2 17.48 1.74 0 2 -14 2 -0.12 2.89 0 2 -14 2 0.15 2.21 0 2 14 2 1.81 2.12 0 -2 -14 -2 -0.71 1.58 0 3 14 2 16.02 2.40 0 3 -14 2 20.03 3.71 0 -3 -14 -2 21.95 2.47 0 3 -14 2 18.60 3.19 0 4 -14 2 10.99 5.61 0 4 -14 2 9.90 5.39 0 4 14 2 7.13 2.50 0 -4 -14 -2 9.76 2.51 0 -5 -14 -2 1.25 2.73 0 5 14 2 -0.39 2.74 0 6 14 2 2.78 3.01 0 -6 -14 -2 0.58 2.10 0 7 15 -2 0.77 2.23 0 -7 -15 2 0.98 3.13 0 6 15 -2 0.79 1.90 0 -6 -15 2 3.35 2.68 0 -5 -15 2 9.05 2.59 0 5 15 -2 4.03 2.62 0 -4 -15 2 8.43 2.42 0 4 15 -2 7.28 2.40 0 -3 -15 2 15.35 2.31 0 -2 -15 2 -0.07 2.19 0 2 -15 -2 0.60 2.13 0 -1 -15 2 10.88 2.25 0 -1 15 2 9.11 2.44 0 1 -15 -2 11.68 2.34 0 0 -15 2 113.43 2.91 0 0 15 2 89.95 2.93 0 0 -15 -2 112.11 3.10 0 1 -15 2 1.89 2.23 0 1 -15 2 3.18 2.25 0 -1 -15 -2 1.69 2.21 0 1 15 2 1.68 2.16 0 2 -15 2 18.45 2.78 0 2 -15 2 17.12 2.66 0 2 15 2 15.81 2.49 0 -2 -15 -2 22.23 2.40 0 3 -15 2 1.84 3.38 0 3 -15 2 0.47 2.88 0 -3 -15 -2 -0.03 1.69 0 3 15 2 -0.17 1.63 0 -4 -15 -2 3.70 2.63 0 4 15 2 1.49 1.85 0 -5 -15 -2 2.60 2.77 0 5 15 2 1.26 2.83 0 6 15 2 1.98 3.17 0 -6 -15 -2 0.92 3.13 0 6 16 -2 1.48 2.89 0 -6 -16 2 -0.34 2.93 0 5 16 -2 -0.95 2.70 0 -5 -16 2 2.29 2.68 0 -4 -16 2 2.29 1.60 0 -3 -16 2 3.90 2.37 0 2 -16 -2 1.32 3.00 0 -2 -16 2 2.12 2.28 0 -1 16 2 1.89 2.30 0 1 -16 -2 1.09 2.42 0 -1 -16 2 2.47 2.15 0 0 16 2 20.54 2.45 0 0 -16 2 22.34 2.44 0 0 -16 -2 24.81 2.45 0 1 -16 2 -0.07 2.33 0 1 16 2 1.50 2.15 0 1 -16 2 0.89 2.32 0 -1 -16 -2 -1.17 2.35 0 2 -16 2 -0.26 2.69 0 2 -16 2 1.34 2.43 0 -2 -16 -2 2.07 2.37 0 2 16 2 2.09 2.26 0 3 -16 2 0.74 3.68 0 3 -16 2 0.07 3.13 0 3 16 2 -0.58 2.30 0 -3 -16 -2 -0.67 1.64 0 4 16 2 1.13 1.90 0 -4 -16 -2 1.73 2.72 0 5 16 2 0.60 2.12 0 -5 -16 -2 0.18 2.92 0 -6 -17 2 1.72 3.03 0 -5 -17 2 3.38 1.96 0 -4 -17 2 5.24 2.67 0 -3 -17 2 11.25 2.61 0 2 -17 -2 0.46 3.13 0 -2 -17 2 3.09 2.33 0 1 -17 -2 14.48 2.75 0 -1 -17 2 14.16 2.50 0 -1 17 2 12.38 2.42 0 0 -17 2 30.81 2.66 0 0 -17 2 28.18 2.62 0 0 -17 -2 26.76 2.57 0 0 17 2 20.48 2.49 0 1 17 2 37.95 2.65 0 1 -17 2 50.79 3.13 0 1 -17 2 50.31 3.09 0 -1 -17 -2 49.10 2.71 0 2 17 2 0.94 2.56 0 2 -17 2 1.55 2.56 0 2 -17 2 -0.26 2.60 0 -2 -17 -2 -0.01 1.87 0 3 -17 2 3.60 3.99 0 3 -17 2 2.81 3.86 0 3 17 2 3.74 2.61 0 -3 -17 -2 2.73 2.67 0 -4 -17 -2 5.48 1.97 0 4 17 2 3.98 2.01 0 5 17 2 1.28 2.03 0 -5 -17 -2 -0.44 2.17 0 -5 -18 2 3.35 3.01 0 -4 -18 2 -0.89 1.95 0 -3 -18 2 4.49 2.60 0 2 -18 -2 11.83 3.41 0 -2 -18 2 10.16 2.52 0 1 -18 -2 7.35 3.23 0 -1 -18 2 4.16 1.75 0 -1 18 2 3.56 2.61 0 0 -18 2 3.70 2.54 0 0 18 2 4.53 2.48 0 0 -18 2 3.49 2.55 0 0 -18 -2 4.45 1.86 0 1 -18 2 6.58 3.32 0 -1 -18 -2 5.64 2.55 0 1 -18 2 3.52 2.62 0 1 18 2 1.71 2.52 0 2 -18 2 5.33 2.86 0 2 -18 2 3.30 3.43 0 2 18 2 3.28 1.87 0 -2 -18 -2 2.38 1.92 0 3 18 2 -1.50 1.90 0 3 -18 2 0.31 4.59 0 3 -18 2 -0.12 4.02 0 -3 -18 -2 -0.57 2.67 0 4 18 2 2.68 2.07 0 -4 -18 -2 4.96 2.96 0 -5 -19 2 4.32 3.20 0 -4 -19 2 0.85 2.97 0 -3 -19 2 2.70 1.99 0 2 -19 -2 0.20 3.52 0 -2 -19 2 -0.94 2.00 0 -1 -19 2 3.85 2.63 0 1 -19 -2 3.70 2.88 0 0 -19 2 1.13 2.69 0 0 -19 2 1.53 1.91 0 0 -19 -2 2.56 2.65 0 0 19 2 1.24 2.60 0 -1 -19 -2 10.18 2.08 0 1 -19 2 10.63 2.80 0 1 19 2 10.09 2.71 0 1 -19 2 10.10 2.74 0 2 -19 2 3.66 3.04 0 2 19 2 2.09 2.79 0 2 -19 2 4.16 2.92 0 -2 -19 -2 2.77 2.87 0 -3 -19 -2 3.32 2.98 0 3 19 2 0.96 2.79 0 3 -19 2 0.52 4.82 0 3 -19 2 0.63 5.35 0 4 19 2 0.66 2.28 0 -4 -19 -2 1.55 3.17 0 -4 -20 2 0.84 3.12 0 -3 -20 2 -0.87 2.01 0 2 -20 -2 0.09 3.78 0 -2 -20 2 2.26 2.80 0 1 -20 -2 -0.09 2.96 0 -1 -20 2 1.82 2.02 0 0 -20 2 18.42 3.05 0 0 -20 2 11.54 2.19 0 0 20 2 13.13 2.97 0 0 -20 -2 19.81 3.04 0 1 -20 2 6.32 3.04 0 -1 -20 -2 8.24 2.88 0 1 -20 2 6.05 3.02 0 1 20 2 7.23 2.88 0 2 -20 2 3.14 3.28 0 2 20 2 0.57 2.10 0 2 -20 2 1.62 3.88 0 -2 -20 -2 2.54 3.01 0 3 -20 2 0.33 7.22 0 3 20 2 2.63 3.05 0 -3 -20 -2 -3.53 3.08 0 3 -20 2 0.39 7.13 0 -3 -21 2 0.98 2.33 0 2 -21 -2 0.84 4.11 0 -2 -21 2 2.06 3.03 0 2 -21 -2 0.45 3.81 0 1 -21 -2 -1.00 3.87 0 -1 -21 2 1.22 2.94 0 0 -21 2 0.93 2.00 0 0 -21 2 0.85 3.01 0 0 -21 -2 0.68 3.01 0 1 -21 2 2.83 3.88 0 1 21 2 1.68 2.95 0 -1 -21 -2 -0.58 3.01 0 1 -21 2 1.62 3.79 0 2 -21 2 -0.35 4.26 0 2 21 2 0.73 3.19 0 2 -21 2 0.72 4.04 0 -2 -21 -2 -0.13 3.24 0 1 -22 -2 0.35 4.06 0 -1 -22 2 -0.03 3.21 0 0 -22 2 -0.42 2.28 0 0 -22 2 -0.94 2.28 0 0 -22 -2 0.46 3.32 0 -9 -1 3 0.82 2.92 0 -9 1 3 1.06 2.98 0 -8 -1 3 -0.85 2.41 0 -8 1 3 1.10 2.63 0 -7 -1 3 65.91 2.77 0 -7 1 3 67.74 2.93 0 -6 -1 3 83.51 2.71 0 -6 1 3 85.33 2.82 0 -5 1 3 2.43 2.00 0 -5 -1 3 2.57 1.89 0 -4 -1 3 14.33 1.96 0 -4 1 3 11.27 1.90 0 -3 -1 3 208.77 3.55 0 -3 1 3 228.78 4.00 0 -3 1 3 203.14 3.84 0 -2 1 3 560.54 5.88 0 -2 -1 3 550.67 5.29 0 1 1 -3 30.45 1.94 0 1 -1 -3 32.76 2.39 0 -1 -1 3 24.37 1.89 0 -1 1 3 33.52 2.49 0 0 1 3 2331.80 11.05 0 0 -1 -3 2405.75 11.32 0 0 -1 3 2475.68 11.40 0 0 1 -3 2248.19 10.81 0 -1 -1 -3 3.12 1.49 0 1 1 3 3.10 2.12 0 1 -1 3 3.34 2.15 0 -1 1 -3 4.28 2.11 0 -2 -1 -3 16.68 1.71 0 2 -1 3 15.14 1.77 0 -2 1 -3 18.48 1.75 0 2 1 3 16.86 1.66 0 -3 1 -3 2.80 2.06 0 -3 -1 -3 1.53 2.00 0 3 1 3 4.24 1.90 0 3 -1 3 2.91 1.99 0 -4 1 -3 3.68 1.50 0 4 -1 3 5.83 2.03 0 -4 -1 -3 2.75 2.15 0 4 1 3 3.58 1.42 0 5 -1 3 6.26 2.29 0 -5 1 -3 4.29 1.64 0 5 1 3 2.23 2.18 0 -5 -1 -3 5.40 2.15 0 -6 -1 -3 0.15 2.51 0 -6 1 -3 2.70 2.41 0 6 1 3 0.61 1.66 0 6 -1 3 -0.03 2.33 0 -7 -1 -3 1.39 2.01 0 -7 1 -3 1.64 2.85 0 7 -1 3 1.41 2.71 0 7 1 3 1.20 2.86 0 8 1 3 -2.11 2.26 0 8 -1 3 1.62 3.11 0 -8 -1 -3 0.76 2.44 0 -8 1 -3 -1.37 3.31 0 -9 2 3 0.19 3.76 0 -9 -2 3 1.94 2.96 0 -8 2 3 7.54 2.68 0 -8 -2 3 5.63 2.43 0 -7 -2 3 30.29 2.51 0 -7 2 3 33.36 2.67 0 -6 2 3 71.20 2.78 0 -6 -2 3 69.37 2.10 0 -5 2 3 181.91 3.94 0 -5 -2 3 179.74 3.15 0 -4 2 3 2.82 1.76 0 -4 -2 3 2.51 1.81 0 -3 -2 3 1492.31 7.97 0 -3 2 3 1587.26 10.23 0 2 -2 -3 32.68 2.34 0 -2 -2 3 30.52 2.20 0 -2 2 3 32.41 2.45 0 -1 -2 3 43.93 2.54 0 -1 2 3 44.51 2.69 0 1 -2 -3 41.83 2.19 0 1 2 -3 46.63 2.57 0 0 -2 3 514.72 5.28 0 0 -2 -3 516.31 5.31 0 0 2 3 493.93 5.25 0 0 2 -3 530.26 5.44 0 -1 2 -3 31.62 2.30 0 -1 -2 -3 32.21 1.97 0 1 -2 3 29.86 2.35 0 1 2 3 30.05 1.88 0 2 2 3 13.94 1.65 0 -2 -2 -3 12.46 1.65 0 -2 2 -3 12.43 1.68 0 2 -2 3 13.30 2.27 0 3 2 3 73.89 2.47 0 -3 2 -3 71.88 2.19 0 3 -2 3 73.66 2.62 0 -3 -2 -3 72.32 2.11 0 -4 -2 -3 13.31 2.27 0 4 2 3 12.90 1.65 0 -4 2 -3 13.62 2.19 0 4 -2 3 13.18 2.21 0 -5 2 -3 -0.40 1.67 0 5 2 3 0.68 2.17 0 -5 -2 -3 -0.29 1.48 0 5 -2 3 0.28 1.62 0 -6 -2 -3 1.24 2.51 0 -6 2 -3 -0.28 1.80 0 6 2 3 -0.95 1.77 0 6 -2 3 1.54 2.42 0 -7 -2 -3 -0.44 2.98 0 7 -2 3 -0.15 2.83 0 -7 2 -3 -0.38 2.05 0 7 2 3 2.03 2.74 0 8 2 3 2.05 3.17 0 -8 2 -3 0.93 2.44 0 8 -2 3 -0.40 3.28 0 -8 -2 -3 -1.63 3.34 0 -9 -3 3 -0.97 2.93 0 -9 3 3 -0.31 3.13 0 -8 3 3 1.68 2.67 0 -8 -3 3 1.35 1.79 0 -7 -3 3 12.14 2.37 0 -7 3 3 17.30 2.51 0 -6 -3 3 55.60 2.54 0 -6 3 3 54.99 3.32 0 -5 3 3 35.93 2.51 0 -5 -3 3 33.61 2.23 0 -4 3 3 35.05 2.31 0 -4 -3 3 36.26 1.66 0 -4 3 3 41.15 2.46 0 -3 3 3 52.14 2.66 0 -3 -3 3 45.66 1.80 0 2 -3 -3 24.51 2.22 0 -2 3 3 23.26 2.34 0 1 -3 -3 11.73 2.29 0 -1 3 3 12.18 2.27 0 -1 -3 3 12.84 2.14 0 0 3 3 164.64 3.51 0 0 -3 3 163.07 3.16 0 0 3 -3 155.24 3.09 0 0 -3 -3 167.23 3.52 0 -1 -3 -3 36.40 2.49 0 1 -3 3 40.48 2.51 0 -1 3 -3 37.57 2.40 0 1 3 3 37.49 2.50 0 -2 -3 -3 264.44 3.61 0 2 -3 3 259.96 4.02 0 2 3 3 248.54 3.20 0 -2 3 -3 274.65 4.11 0 -3 -3 -3 11.35 1.55 0 3 3 3 13.09 2.12 0 -3 3 -3 9.60 2.20 0 3 -3 3 9.42 1.58 0 4 3 3 36.52 1.85 0 4 -3 3 37.98 2.47 0 -4 3 -3 39.09 2.50 0 -4 -3 -3 38.20 2.37 0 -5 -3 -3 1.79 2.24 0 5 -3 3 1.70 2.12 0 5 3 3 -1.13 2.18 0 -5 3 -3 0.51 2.22 0 6 3 3 3.41 2.42 0 -6 -3 -3 5.11 2.59 0 6 -3 3 2.52 2.55 0 -6 3 -3 2.01 2.68 0 7 -3 3 1.15 2.80 0 -7 3 -3 0.13 2.84 0 -7 -3 -3 0.29 2.74 0 7 3 3 0.69 2.00 0 -9 4 3 0.88 3.90 0 -9 -4 3 1.88 2.11 0 -8 -4 3 2.34 1.89 0 -8 4 3 2.55 3.38 0 -7 -4 3 -0.30 2.34 0 7 4 -3 0.27 1.63 0 -7 4 3 0.22 2.43 0 6 4 -3 306.44 3.91 0 -6 4 3 306.95 5.63 0 -6 -4 3 299.47 3.40 0 -5 4 3 155.69 3.98 0 -5 4 3 159.14 4.14 0 -5 -4 3 159.68 2.98 0 -4 -4 3 91.73 2.54 0 -4 4 3 93.20 3.77 0 -4 4 3 86.47 3.60 0 -3 4 3 348.10 5.76 0 -3 -4 3 321.44 3.91 0 -2 4 3 32.76 2.82 0 -2 -4 3 30.43 2.25 0 2 -4 -3 31.05 2.36 0 -1 -4 3 159.62 3.23 0 1 -4 -3 165.14 3.77 0 -1 4 3 158.56 3.62 0 0 -4 -3 48.67 2.53 0 0 -4 3 45.78 2.03 0 0 4 3 48.11 2.55 0 0 4 -3 43.47 1.98 0 -1 -4 -3 448.12 4.39 0 1 4 3 469.81 4.79 0 -1 4 -3 472.78 5.10 0 1 -4 3 486.51 5.22 0 -2 -4 -3 620.19 4.86 0 2 4 3 589.41 4.88 0 -2 4 -3 633.30 5.68 0 2 -4 3 601.27 5.57 0 -3 -4 -3 113.47 2.76 0 -3 4 -3 116.75 3.07 0 3 4 3 107.82 2.74 0 3 -4 3 103.15 2.52 0 -4 -4 -3 5.86 1.55 0 4 4 3 6.96 2.08 0 4 -4 3 5.08 2.20 0 -4 4 -3 5.71 1.58 0 -5 -4 -3 11.71 2.43 0 5 -4 3 13.35 2.35 0 -5 4 -3 14.47 2.41 0 5 4 3 11.40 1.72 0 6 4 3 21.34 2.75 0 6 -4 3 24.69 2.82 0 -6 -4 -3 24.96 2.71 0 -6 4 -3 22.37 2.88 0 -7 -4 -3 -0.73 2.89 0 7 -4 3 2.31 2.94 0 7 4 3 1.21 2.10 0 -7 4 -3 2.73 3.02 0 -9 5 3 -0.06 3.93 0 -9 5 3 1.00 3.82 0 -9 -5 3 2.09 2.13 0 -8 5 3 -0.04 3.49 0 -8 5 3 1.32 3.33 0 -8 -5 3 0.94 2.66 0 -7 5 3 5.14 3.02 0 7 5 -3 4.67 2.38 0 -7 5 3 5.44 3.06 0 -7 -5 3 10.53 2.32 0 -6 -5 3 64.78 1.96 0 -6 5 3 64.97 3.69 0 6 5 -3 62.35 2.04 0 -6 5 3 65.67 3.68 0 -5 5 3 15.69 2.78 0 -5 5 3 17.12 2.74 0 -5 -5 3 13.82 1.60 0 5 5 -3 15.30 2.11 0 -4 -5 3 20.34 2.05 0 -4 5 3 18.69 2.73 0 -4 5 3 21.89 3.37 0 -3 -5 3 -0.26 1.81 0 -3 5 3 0.98 2.45 0 -2 5 3 24.85 2.70 0 2 -5 -3 25.85 2.37 0 -2 -5 3 20.90 1.61 0 1 -5 -3 184.18 3.86 0 -1 -5 3 162.83 2.86 0 -1 5 3 172.90 3.71 0 0 -5 -3 1147.51 7.32 0 0 5 3 1004.67 6.94 0 0 -5 3 1102.12 7.15 0 -1 -5 -3 41.55 1.85 0 -1 5 -3 41.10 2.39 0 1 5 3 36.27 1.83 0 1 -5 3 41.54 2.51 0 2 -5 3 15.22 2.22 0 2 5 3 14.27 2.08 0 -2 5 -3 15.11 1.64 0 -2 -5 -3 14.89 1.54 0 -3 -5 -3 212.02 3.32 0 3 5 3 186.16 2.84 0 -3 5 -3 217.58 3.78 0 3 -5 3 211.23 3.78 0 -4 -5 -3 0.58 1.51 0 -4 5 -3 0.76 1.58 0 4 5 3 0.06 2.07 0 4 -5 3 0.24 1.58 0 -5 -5 -3 3.20 2.37 0 5 -5 3 3.71 2.36 0 5 5 3 0.36 2.35 0 -5 5 -3 2.20 2.34 0 -6 -5 -3 1.48 1.67 0 6 -5 3 2.51 2.61 0 -6 5 -3 4.53 2.74 0 6 5 3 1.91 2.47 0 -7 5 -3 1.49 2.96 0 7 -5 3 0.15 2.93 0 -7 -5 -3 2.62 2.00 0 7 5 3 1.75 2.02 0 -9 -6 3 6.31 3.03 0 -9 6 3 0.62 5.36 0 -9 6 3 1.28 5.21 0 -8 -6 3 14.67 2.13 0 -8 6 3 18.67 4.31 0 -8 6 3 19.25 4.25 0 -7 6 3 6.42 3.63 0 -7 6 3 6.41 3.65 0 -7 -6 3 4.34 2.36 0 7 6 -3 10.16 2.41 0 -6 -6 3 0.23 2.10 0 -6 6 3 1.35 3.12 0 6 6 -3 0.42 1.49 0 -6 6 3 1.06 3.14 0 5 6 -3 16.10 2.18 0 -5 6 3 18.76 3.90 0 -5 -6 3 16.38 2.14 0 -5 6 3 15.85 3.33 0 -4 6 3 268.42 7.14 0 -4 6 3 248.02 6.83 0 -4 -6 3 248.37 3.38 0 -3 -6 3 23.48 1.94 0 -3 6 3 23.78 3.00 0 2 -6 -3 11.03 2.23 0 -2 -6 3 11.67 1.97 0 -2 6 3 10.42 2.15 0 -1 6 3 38.19 2.03 0 -1 -6 3 43.43 2.23 0 1 -6 -3 43.75 2.57 0 0 -6 -3 1104.32 6.90 0 0 -6 3 1065.78 6.80 0 0 6 3 1039.09 6.94 0 -1 -6 -3 4.15 2.09 0 1 -6 3 4.70 2.07 0 -1 6 -3 4.51 1.94 0 1 6 3 3.82 1.97 0 2 6 3 2.31 2.00 0 2 -6 3 0.94 2.13 0 -2 -6 -3 0.67 1.43 0 -2 6 -3 1.08 2.01 0 3 6 3 12.61 2.16 0 3 -6 3 12.86 2.40 0 -3 6 -3 16.08 2.32 0 -3 -6 -3 14.91 2.27 0 -4 -6 -3 130.30 2.96 0 4 6 3 122.23 2.83 0 -4 6 -3 131.08 3.53 0 4 -6 3 130.66 3.52 0 -5 -6 -3 1.85 2.29 0 -5 6 -3 1.54 2.44 0 5 6 3 0.12 2.32 0 5 -6 3 2.17 2.45 0 -6 6 -3 2.50 2.68 0 6 -6 3 2.88 2.59 0 -6 -6 -3 2.32 2.49 0 6 6 3 3.31 1.74 0 7 -6 3 -0.59 3.04 0 -7 -6 -3 1.12 2.90 0 -7 6 -3 -2.16 3.15 0 7 6 3 1.55 2.07 0 -9 -7 3 -0.72 2.25 0 -8 -7 3 2.99 2.65 0 7 7 -3 0.80 2.31 0 -7 -7 3 1.54 1.66 0 -6 -7 3 2.62 2.15 0 6 7 -3 1.29 2.20 0 5 7 -3 0.18 2.02 0 -5 -7 3 1.84 1.99 0 -4 -7 3 10.31 1.49 0 -3 -7 3 52.20 2.21 0 -3 7 3 47.72 3.55 0 -2 -7 3 918.78 5.70 0 -2 7 3 919.79 8.76 0 2 -7 -3 1055.77 9.29 0 1 -7 -3 40.43 2.49 0 -1 -7 3 36.54 2.24 0 -1 7 3 32.82 1.81 0 0 -7 -3 682.87 5.48 0 0 -7 3 703.89 5.80 0 0 7 3 632.74 5.74 0 1 7 3 51.04 2.02 0 1 -7 3 57.32 2.51 0 -1 -7 -3 59.44 2.45 0 -2 7 -3 91.41 3.00 0 2 7 3 80.10 2.13 0 2 -7 3 99.40 3.13 0 -2 -7 -3 95.81 2.66 0 3 7 3 104.02 2.76 0 -3 7 -3 112.28 3.19 0 3 -7 3 115.29 3.29 0 -3 -7 -3 117.15 2.89 0 4 -7 3 84.59 3.28 0 -4 -7 -3 88.93 2.80 0 -4 7 -3 91.98 3.33 0 4 7 3 83.00 2.76 0 -5 -7 -3 4.21 1.73 0 5 7 3 6.77 1.61 0 -5 7 -3 5.14 2.55 0 5 -7 3 4.38 2.59 0 6 7 3 -0.98 2.60 0 -6 -7 -3 0.34 2.52 0 6 -7 3 0.46 2.60 0 -6 7 -3 1.66 2.75 0 -7 -7 -3 -1.11 2.96 0 7 7 3 1.10 2.06 0 -7 7 -3 0.88 3.06 0 7 -7 3 -1.24 3.07 0 -8 -8 3 1.56 2.74 0 -7 -8 3 2.21 2.44 0 7 8 -3 4.76 2.36 0 -6 -8 3 16.17 1.75 0 6 8 -3 13.88 1.76 0 -5 -8 3 3.87 2.09 0 5 8 -3 5.16 2.08 0 -4 -8 3 4.21 1.97 0 -3 -8 3 40.47 1.77 0 -3 8 3 34.85 3.60 0 -2 -8 3 0.73 1.87 0 -2 8 3 1.27 2.35 0 2 -8 -3 1.55 2.69 0 1 -8 -3 77.37 2.38 0 -1 -8 3 74.44 2.42 0 -1 8 3 69.92 2.72 0 0 8 3 85.30 2.76 0 0 -8 3 90.54 2.23 0 0 -8 -3 98.44 2.36 0 -1 -8 -3 280.70 3.68 0 1 -8 3 278.38 4.06 0 1 8 3 246.69 3.27 0 -2 -8 -3 8.80 1.55 0 -2 8 -3 8.88 2.13 0 2 8 3 11.09 2.10 0 2 -8 3 12.11 2.39 0 3 8 3 320.23 3.43 0 -3 8 -3 374.23 4.88 0 -3 -8 -3 364.54 3.84 0 3 -8 3 381.03 5.09 0 4 8 3 3.95 1.56 0 -4 -8 -3 2.97 2.29 0 4 -8 3 4.18 2.59 0 -4 8 -3 2.67 2.45 0 5 -8 3 2.92 2.53 0 5 8 3 3.44 1.65 0 -5 8 -3 3.60 2.73 0 -5 -8 -3 2.94 1.76 0 -6 8 -3 1.91 2.91 0 -6 -8 -3 1.51 2.66 0 6 -8 3 2.08 2.80 0 6 8 3 3.45 1.84 0 -7 -8 -3 0.10 3.00 0 7 8 3 5.00 3.09 0 7 -8 3 0.55 3.80 0 -7 8 -3 0.22 3.17 0 -8 -9 3 3.72 2.83 0 -7 -9 3 0.75 2.38 0 7 9 -3 2.65 2.39 0 -6 -9 3 0.25 2.25 0 6 9 -3 -0.60 1.58 0 -5 -9 3 7.06 2.17 0 5 9 -3 5.88 2.15 0 -4 -9 3 22.39 1.59 0 3 -9 -3 5.02 3.18 0 -3 9 3 4.00 2.77 0 -3 -9 3 5.44 1.45 0 -2 -9 3 75.02 2.46 0 -2 9 3 76.40 3.06 0 2 -9 -3 92.30 3.39 0 1 -9 -3 146.22 3.34 0 -1 9 3 123.47 3.17 0 -1 -9 3 130.04 2.82 0 0 -9 -3 1.63 1.92 0 0 9 3 0.90 1.25 0 0 -9 3 1.84 1.35 0 0 -9 3 1.32 1.87 0 1 9 3 17.53 1.64 0 -1 -9 -3 26.22 2.16 0 1 -9 3 23.13 2.26 0 2 -9 3 63.23 2.81 0 -2 -9 -3 66.83 2.48 0 2 9 3 58.49 2.53 0 3 -9 3 61.86 3.63 0 3 9 3 54.42 2.47 0 -3 9 -3 54.75 2.93 0 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47.78 2.57 0 1 -14 3 7.27 2.47 0 1 -14 3 7.97 2.21 0 -1 -14 -3 6.72 1.62 0 1 14 3 6.48 1.46 0 2 -14 3 24.35 2.51 0 2 14 3 20.04 1.80 0 -2 -14 -3 22.10 1.89 0 2 -14 3 24.68 2.80 0 3 -14 3 3.22 3.14 0 3 14 3 0.88 1.84 0 3 -14 3 3.46 3.47 0 -3 -14 -3 1.54 2.37 0 4 -14 3 3.80 3.39 0 -4 -14 -3 3.76 2.63 0 4 14 3 1.03 2.62 0 4 -14 3 3.74 3.68 0 5 14 3 -0.39 2.08 0 5 -14 3 1.15 5.97 0 5 -14 3 1.45 5.97 0 -5 -14 -3 2.16 2.86 0 6 14 3 4.82 3.19 0 -7 -15 3 7.35 3.06 0 -6 -15 3 1.40 1.92 0 -5 -15 3 -0.28 2.58 0 -4 -15 3 24.07 2.61 0 -3 -15 3 36.44 2.51 0 3 -15 -3 45.21 5.73 0 -2 15 3 4.02 2.35 0 -2 -15 3 4.89 2.17 0 2 -15 -3 4.80 2.41 0 1 -15 -3 10.49 2.49 0 -1 15 3 7.97 2.46 0 -1 -15 3 9.28 2.22 0 0 -15 3 9.25 2.32 0 0 15 3 5.33 2.31 0 0 -15 3 6.41 2.21 0 0 -15 -3 8.52 2.35 0 1 15 3 13.34 2.26 0 -1 -15 -3 13.38 2.33 0 1 -15 3 18.09 2.50 0 1 -15 3 19.54 2.61 0 2 -15 3 26.99 3.37 0 2 -15 3 25.92 2.62 0 2 15 3 22.14 2.55 0 -2 -15 -3 28.50 2.63 0 3 -15 3 0.47 3.04 0 3 -15 3 0.62 2.93 0 3 15 3 -0.12 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3.00 0 -9 3 4 1.21 3.10 0 -9 -3 4 2.14 2.89 0 -9 3 4 3.16 3.83 0 -8 -3 4 1.06 1.77 0 -8 3 4 3.30 2.58 0 -8 3 4 3.06 3.20 0 -7 -3 4 0.76 2.24 0 -7 3 4 -0.42 2.31 0 -7 3 4 0.30 2.85 0 -6 3 4 35.05 2.98 0 -6 3 4 34.22 2.58 0 -6 -3 4 35.46 2.39 0 -5 -3 4 226.82 2.95 0 -5 3 4 224.70 3.99 0 -5 3 4 250.12 4.30 0 -4 3 4 3.08 1.97 0 -4 -3 4 2.15 1.31 0 -4 3 4 3.36 1.88 0 -3 3 4 127.86 3.18 0 -3 -3 4 122.51 2.78 0 2 -3 -4 37.51 2.53 0 -2 3 4 36.92 2.52 0 -2 -3 4 34.31 1.77 0 1 -3 -4 806.39 6.35 0 -1 3 4 752.82 6.24 0 1 3 -4 701.10 5.52 0 -1 -3 4 713.41 5.41 0 0 -3 -4 49.83 2.48 0 0 3 4 45.15 2.45 0 0 3 -4 48.28 1.92 0 0 -3 4 48.63 1.97 0 -1 -3 -4 1677.89 7.85 0 -1 3 -4 1653.54 8.34 0 1 -3 4 1524.80 7.78 0 1 3 4 1635.73 7.78 0 -2 3 -4 46.47 1.90 0 2 -3 4 45.92 1.89 0 -2 -3 -4 45.98 2.41 0 2 3 4 43.76 1.88 0 -3 -3 -4 -0.44 2.14 0 3 -3 4 2.65 2.03 0 3 3 4 -0.29 2.09 0 -3 3 -4 0.90 1.46 0 4 3 4 23.02 2.32 0 4 -3 4 28.78 2.57 0 -4 -3 -4 26.61 2.40 0 -4 3 -4 25.91 2.61 0 -5 -3 -4 24.53 2.08 0 5 3 4 23.00 1.86 0 5 -3 4 23.16 2.08 0 -5 3 -4 26.99 2.84 0 -6 -3 -4 1.44 2.70 0 6 3 4 -0.71 1.91 0 -6 3 -4 0.80 1.90 0 6 -3 4 -0.73 1.89 0 7 -3 4 -0.99 3.03 0 7 3 4 -1.36 2.24 0 -7 -3 -4 -0.42 2.21 0 -7 3 -4 1.10 3.10 0 -9 4 4 1.68 3.20 0 -9 -4 4 1.33 2.95 0 -9 4 4 0.25 3.12 0 -8 -4 4 -0.52 2.53 0 -8 4 4 -0.91 3.29 0 -8 4 4 -0.93 2.70 0 -7 -4 4 0.64 2.44 0 -7 4 4 0.68 2.47 0 -7 4 4 1.19 2.98 0 -6 -4 4 36.60 1.89 0 -6 4 4 37.93 3.22 0 -6 4 4 38.76 3.23 0 -5 4 4 2.04 2.08 0 -5 4 4 3.66 2.02 0 -5 -4 4 4.37 1.53 0 -4 -4 4 28.23 2.09 0 -4 4 4 29.03 2.42 0 -4 4 4 28.03 2.30 0 -3 -4 4 144.26 2.86 0 -3 4 4 162.73 3.92 0 -2 4 4 1.48 2.07 0 -2 -4 4 -0.07 1.35 0 2 -4 -4 0.73 2.01 0 -1 -4 4 84.22 2.62 0 1 -4 -4 92.00 2.91 0 -1 4 4 93.05 2.88 0 0 -4 -4 32.97 2.31 0 0 4 -4 28.89 1.67 0 0 -4 4 27.71 1.71 0 0 4 4 32.34 2.31 0 1 -4 4 88.71 2.83 0 1 4 4 79.28 2.12 0 -1 4 -4 86.41 2.76 0 -1 -4 -4 92.44 2.60 0 -2 -4 -4 48.52 2.40 0 -2 4 -4 42.92 2.35 0 2 -4 4 43.73 2.46 0 2 4 4 45.27 2.40 0 -3 4 -4 13.38 2.22 0 -3 -4 -4 10.56 1.66 0 3 4 4 11.92 1.63 0 3 -4 4 14.79 2.18 0 -4 4 -4 45.49 2.65 0 -4 -4 -4 41.44 1.88 0 4 4 4 41.29 2.42 0 4 -4 4 38.12 2.63 0 -5 -4 -4 19.91 1.85 0 5 4 4 20.37 2.45 0 5 -4 4 22.38 2.80 0 -5 4 -4 19.49 2.04 0 6 4 4 -1.01 2.62 0 6 -4 4 -0.21 2.63 0 -6 -4 -4 0.98 1.98 0 -6 4 -4 0.28 2.80 0 -7 -4 -4 1.90 3.03 0 7 4 4 -0.18 2.08 0 7 -4 4 2.59 3.10 0 -7 4 -4 1.89 3.15 0 -9 5 4 1.41 3.81 0 -9 5 4 1.98 3.85 0 -9 -5 4 2.82 2.14 0 -8 -5 4 8.98 1.90 0 -8 5 4 7.63 3.49 0 -8 5 4 9.02 3.42 0 -7 -5 4 2.06 2.26 0 -7 5 4 0.59 2.46 0 -7 5 4 1.53 2.94 0 -6 -5 4 10.33 2.21 0 -6 5 4 10.35 2.77 0 -6 5 4 11.16 3.15 0 -5 5 4 0.10 2.43 0 -5 -5 4 1.11 1.40 0 -5 5 4 -0.22 2.10 0 -4 5 4 2.04 1.99 0 -4 -5 4 4.10 2.01 0 -4 5 4 2.24 2.10 0 -3 5 4 44.61 2.70 0 3 -5 -4 45.38 2.57 0 -3 -5 4 40.67 1.74 0 -2 5 4 91.99 2.93 0 -2 -5 4 93.97 2.53 0 2 -5 -4 97.46 3.06 0 -1 5 4 253.76 3.92 0 -1 -5 4 249.04 3.57 0 1 -5 -4 257.16 4.02 0 0 -5 4 34.91 2.31 0 0 -5 -4 37.71 2.46 0 0 5 4 33.75 2.35 0 0 5 -4 36.70 2.32 0 -1 5 -4 254.11 3.77 0 -1 -5 -4 274.61 3.56 0 1 -5 4 277.95 3.92 0 1 5 4 233.65 3.15 0 2 -5 4 173.38 3.37 0 -2 -5 -4 168.91 3.03 0 2 5 4 161.70 3.02 0 -2 5 -4 164.30 3.30 0 3 -5 4 64.25 2.80 0 -3 -5 -4 61.85 1.95 0 -3 5 -4 68.49 2.71 0 3 5 4 62.54 1.98 0 4 5 4 40.52 2.52 0 -4 -5 -4 41.64 1.93 0 4 -5 4 44.53 2.61 0 -4 5 -4 45.65 2.65 0 -5 -5 -4 3.18 2.45 0 5 5 4 5.38 1.74 0 5 -5 4 6.71 2.56 0 -5 5 -4 7.05 2.40 0 -6 5 -4 3.04 2.89 0 6 -5 4 2.43 2.04 0 6 5 4 8.97 2.69 0 -6 -5 -4 4.51 2.69 0 -7 5 -4 0.67 3.20 0 -7 -5 -4 0.34 3.03 0 7 -5 4 1.93 3.16 0 7 5 4 -1.73 2.08 0 -9 -6 4 0.32 3.11 0 -9 6 4 1.67 5.71 0 -9 6 4 0.72 5.76 0 -8 6 4 0.76 3.91 0 -8 -6 4 0.78 2.62 0 -8 6 4 -0.03 3.97 0 -7 6 4 15.80 3.36 0 -7 -6 4 13.63 2.60 0 -7 6 4 15.44 3.34 0 -6 6 4 46.42 3.94 0 -6 6 4 40.04 3.41 0 -6 -6 4 41.40 1.90 0 -5 -6 4 240.13 2.91 0 -5 6 4 239.75 5.49 0 -5 6 4 271.23 5.97 0 -4 -6 4 105.60 2.62 0 -4 6 4 108.07 3.61 0 -4 6 4 102.74 3.72 0 -3 6 4 47.18 2.79 0 3 -6 -4 45.71 2.60 0 -3 -6 4 41.33 2.18 0 2 -6 -4 702.75 6.55 0 -2 -6 4 670.03 4.81 0 -2 6 4 666.26 6.21 0 -1 -6 4 17.97 2.06 0 1 -6 -4 17.06 2.27 0 -1 6 4 17.16 2.14 0 0 -6 -4 15.77 2.15 0 0 -6 4 9.49 1.55 0 0 6 4 11.34 1.53 0 -1 6 -4 -0.01 1.94 0 -1 -6 -4 0.86 1.45 0 1 6 4 0.14 2.08 0 1 -6 4 0.99 2.05 0 -2 6 -4 73.40 2.74 0 -2 -6 -4 75.58 2.66 0 2 -6 4 75.82 2.81 0 2 6 4 65.63 2.10 0 3 -6 4 27.21 2.57 0 -3 -6 -4 28.50 2.28 0 3 6 4 28.19 2.27 0 -3 6 -4 30.18 2.46 0 -4 -6 -4 10.08 2.40 0 -4 6 -4 10.86 2.40 0 4 6 4 11.40 2.34 0 4 -6 4 10.98 2.48 0 5 -6 4 5.77 2.49 0 -5 -6 -4 5.31 1.74 0 5 6 4 4.17 1.81 0 -5 6 -4 4.26 2.54 0 -6 -6 -4 3.11 2.72 0 6 -6 4 0.47 2.79 0 -6 6 -4 1.32 2.89 0 6 6 4 2.58 1.84 0 7 6 4 2.96 3.12 0 -7 -6 -4 3.48 3.13 0 7 -6 4 2.35 3.20 0 -7 6 -4 1.40 3.12 0 -9 -7 4 5.16 3.13 0 -8 -7 4 -1.09 2.66 0 -7 -7 4 0.48 2.23 0 -6 7 4 3.47 4.78 0 -6 -7 4 2.04 2.28 0 -6 7 4 3.22 4.15 0 -5 -7 4 233.39 2.91 0 -5 7 4 266.73 7.33 0 -5 7 4 245.16 6.84 0 -4 -7 4 34.67 1.70 0 -4 7 4 37.35 3.24 0 -4 7 4 35.81 2.98 0 -3 -7 4 1.69 1.98 0 -3 7 4 4.07 2.14 0 3 -7 -4 4.34 2.07 0 2 -7 -4 2.12 2.06 0 -2 -7 4 1.50 1.33 0 -2 -7 4 1.88 1.34 0 -2 7 4 1.49 2.00 0 1 -7 -4 7.11 2.19 0 -1 -7 4 6.62 1.92 0 -1 7 4 9.77 1.48 0 0 -7 4 16.63 2.13 0 0 7 4 13.65 2.12 0 0 -7 -4 15.45 1.64 0 -1 7 -4 75.74 2.52 0 1 -7 4 82.17 2.73 0 1 7 4 75.58 2.58 0 -1 -7 -4 78.70 2.14 0 -2 -7 -4 11.58 2.16 0 2 -7 4 10.22 1.70 0 2 7 4 10.78 2.16 0 -2 7 -4 10.55 2.21 0 -3 -7 -4 165.55 2.61 0 3 7 4 153.56 2.62 0 -3 7 -4 172.90 3.47 0 3 -7 4 170.24 3.09 0 -4 -7 -4 22.80 2.40 0 4 7 4 19.74 1.76 0 4 -7 4 23.11 2.65 0 -4 7 -4 22.87 2.54 0 5 7 4 3.65 2.49 0 5 -7 4 1.96 2.76 0 -5 7 -4 2.37 2.62 0 -5 -7 -4 1.25 2.54 0 -6 -7 -4 4.07 2.84 0 6 7 4 -1.11 2.77 0 6 -7 4 0.87 3.05 0 -6 7 -4 0.97 2.99 0 -7 -7 -4 1.33 2.33 0 7 -7 4 2.79 3.38 0 -7 7 -4 4.28 4.16 0 7 7 4 0.86 3.21 0 -9 -8 4 1.59 3.26 0 -8 -8 4 3.78 2.73 0 -7 -8 4 2.70 2.49 0 -6 -8 4 24.16 2.39 0 -5 -8 4 35.53 2.38 0 -4 8 4 209.91 6.13 0 -4 -8 4 199.89 2.68 0 -4 8 4 213.96 6.41 0 -3 -8 4 50.71 1.86 0 3 -8 -4 60.92 2.99 0 -3 8 4 57.95 3.26 0 -2 -8 4 102.50 2.59 0 -2 8 4 103.15 3.12 0 2 -8 -4 120.56 3.38 0 -1 -8 4 121.57 2.66 0 1 -8 -4 131.00 3.08 0 -1 8 4 115.01 2.93 0 0 -8 -4 87.58 2.19 0 0 8 4 80.76 2.58 0 0 -8 4 87.85 2.57 0 1 -8 4 13.77 1.66 0 1 8 4 13.88 2.16 0 -1 -8 -4 14.87 2.22 0 -2 8 -4 1.19 2.06 0 2 8 4 1.04 2.08 0 2 -8 4 0.97 2.33 0 -2 -8 -4 1.42 1.60 0 3 8 4 4.27 2.25 0 3 -8 4 2.09 1.76 0 -3 8 -4 -0.09 2.11 0 -3 -8 -4 2.87 2.29 0 -4 -8 -4 1.18 1.63 0 -4 8 -4 1.09 2.38 0 4 8 4 1.98 1.61 0 4 -8 4 1.45 2.67 0 -5 8 -4 13.67 2.86 0 5 8 4 14.12 2.65 0 -5 -8 -4 14.44 2.65 0 5 -8 4 15.74 2.87 0 -6 -8 -4 3.60 2.74 0 -6 8 -4 0.90 2.97 0 6 8 4 0.53 1.93 0 6 -8 4 -2.76 3.07 0 -8 -9 4 6.30 2.06 0 -7 -9 4 34.11 2.71 0 -6 -9 4 -1.69 2.27 0 -5 -9 4 82.23 2.67 0 -4 -9 4 16.46 2.03 0 -4 9 4 13.77 3.78 0 -4 9 4 13.76 4.02 0 -3 -9 4 128.36 2.77 0 -3 9 4 126.11 3.69 0 3 -9 -4 149.16 4.37 0 -2 -9 4 4.49 2.01 0 -2 9 4 6.40 2.16 0 2 -9 -4 8.18 2.86 0 -1 -9 4 252.20 3.42 0 -1 -9 4 252.00 3.50 0 1 -9 -4 258.08 3.53 0 -1 9 4 230.93 3.84 0 0 9 4 36.93 1.76 0 0 -9 4 44.35 2.26 0 0 -9 -4 43.89 2.40 0 -1 -9 -4 17.16 1.70 0 1 -9 4 17.03 2.15 0 1 9 4 15.02 1.57 0 2 9 4 77.23 2.57 0 2 -9 4 85.80 2.96 0 -2 -9 -4 82.73 2.10 0 3 -9 4 1.69 2.35 0 -3 9 -4 1.89 2.26 0 3 9 4 -1.25 2.24 0 -3 -9 -4 2.98 2.33 0 -4 -9 -4 59.52 2.81 0 -4 9 -4 61.93 3.08 0 4 9 4 57.15 2.74 0 4 -9 4 63.61 3.29 0 5 9 4 1.59 2.58 0 -5 -9 -4 0.95 2.53 0 5 -9 4 2.42 2.80 0 -5 9 -4 2.11 2.72 0 -6 -9 -4 0.74 2.88 0 6 9 4 -1.84 2.92 0 6 -9 4 1.14 3.05 0 -6 9 -4 1.29 3.10 0 -8 -10 4 0.98 2.79 0 -7 -10 4 0.42 2.50 0 -6 -10 4 9.36 2.41 0 -5 -10 4 44.96 1.89 0 -4 -10 4 12.71 2.17 0 -3 10 4 8.78 2.62 0 3 -10 -4 10.91 2.97 0 -3 -10 4 12.72 2.02 0 -2 -10 4 3.22 2.03 0 -2 10 4 5.23 2.06 0 2 -10 -4 5.10 2.33 0 1 -10 -4 1.31 2.14 0 -1 -10 4 1.18 2.03 0 -1 10 4 0.15 1.43 0 -1 -10 4 2.01 1.95 0 0 -10 4 -0.05 1.31 0 0 -10 -4 -0.05 1.36 0 0 10 4 -0.69 1.87 0 1 -10 4 24.26 2.36 0 -1 -10 -4 26.46 1.78 0 1 10 4 22.92 2.28 0 2 10 4 41.43 2.38 0 2 -10 4 47.36 2.66 0 -2 -10 -4 40.68 2.49 0 -3 -10 -4 1.13 1.59 0 3 -10 4 1.75 2.78 0 3 10 4 1.47 1.59 0 -4 -10 -4 4.94 2.48 0 4 10 4 3.98 2.41 0 -4 10 -4 3.27 2.47 0 4 -10 4 3.80 2.95 0 -5 -10 -4 1.58 1.95 0 5 10 4 1.38 1.90 0 -5 10 -4 0.67 2.71 0 5 -10 4 -0.89 2.77 0 -6 -10 -4 1.16 2.07 0 6 10 4 0.24 2.07 0 6 -10 4 0.68 3.08 0 -6 10 -4 -0.25 3.12 0 -8 -11 4 1.74 2.14 0 -7 -11 4 12.43 1.98 0 -6 -11 4 1.28 2.43 0 -5 -11 4 6.44 2.20 0 -4 -11 4 28.85 2.34 0 -3 -11 4 25.45 1.67 0 -3 11 4 24.71 3.09 0 3 -11 -4 33.68 3.35 0 -2 11 4 9.62 2.52 0 2 -11 -4 9.79 2.31 0 -2 -11 4 8.73 2.13 0 -1 -11 4 137.91 2.89 0 1 -11 -4 148.82 3.32 0 -1 11 4 122.14 3.14 0 -1 -11 4 137.51 2.94 0 0 -11 4 1.64 1.43 0 0 -11 -4 1.40 1.48 0 0 11 4 1.87 1.99 0 0 -11 4 1.54 1.36 0 -1 -11 -4 20.10 2.23 0 1 11 4 16.19 2.19 0 1 -11 4 21.59 2.28 0 2 11 4 15.49 2.32 0 2 -11 4 17.55 2.38 0 -2 -11 -4 18.72 2.47 0 3 -11 4 22.43 2.96 0 -3 -11 -4 19.94 2.40 0 3 11 4 18.41 2.47 0 4 11 4 4.35 2.47 0 4 -11 4 3.17 2.93 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2.40 0 -7 6 6 2.81 2.98 0 -7 6 6 4.45 2.62 0 -6 6 6 46.45 2.87 0 -6 -6 6 50.70 2.53 0 -6 6 6 47.96 2.99 0 -5 -6 6 2.86 1.60 0 -5 -6 6 4.59 1.65 0 -5 6 6 3.66 2.39 0 -4 -6 6 3.17 1.94 0 -4 6 6 2.53 2.19 0 -4 -6 6 3.49 1.98 0 -3 6 6 15.03 2.33 0 3 -6 -6 16.09 2.28 0 -3 -6 6 15.37 2.19 0 -2 6 6 524.17 4.91 0 2 -6 -6 553.78 5.03 0 -2 -6 6 487.59 3.98 0 -1 6 6 23.97 2.26 0 -1 -6 6 27.87 2.26 0 1 -6 -6 26.80 2.29 0 0 6 -6 41.29 2.52 0 0 -6 -6 45.41 1.93 0 0 6 6 40.76 1.85 0 0 -6 6 46.47 2.52 0 -1 -6 -6 1.20 2.13 0 1 -6 6 -0.33 2.31 0 -1 6 -6 -0.06 2.18 0 1 6 6 1.00 1.54 0 2 -6 6 1.91 1.74 0 -2 6 -6 0.75 2.15 0 -2 -6 -6 2.68 2.32 0 2 6 6 -0.79 1.69 0 3 -6 6 0.61 2.50 0 -3 6 -6 1.55 2.41 0 -3 -6 -6 2.07 1.63 0 3 6 6 0.21 2.31 0 -4 -6 -6 3.36 2.62 0 4 6 6 1.92 1.81 0 -4 6 -6 4.27 2.56 0 4 -6 6 1.21 2.63 0 5 6 6 2.37 2.85 0 -5 -6 -6 6.06 2.81 0 5 -6 6 5.83 3.12 0 -5 6 -6 3.46 2.87 0 6 6 6 1.50 2.28 0 -6 -6 -6 -0.05 3.18 0 6 -6 6 1.60 3.44 0 -6 6 -6 -3.26 3.29 0 -9 -7 6 1.51 2.27 0 -8 -7 6 2.33 2.74 0 -8 7 6 0.45 4.34 0 -8 7 6 -0.09 4.10 0 -7 7 6 0.80 3.17 0 -7 7 6 0.63 3.82 0 -7 -7 6 1.36 2.40 0 -6 7 6 0.63 2.84 0 -6 -7 6 3.12 2.19 0 -6 7 6 1.15 2.55 0 -5 -7 6 10.84 1.63 0 -5 -7 6 7.47 2.22 0 -5 7 6 8.76 2.52 0 -4 -7 6 168.41 2.53 0 -4 7 6 179.57 4.22 0 -4 -7 6 172.93 3.00 0 3 -7 -6 233.19 3.92 0 -3 7 6 222.94 3.81 0 -3 -7 6 212.31 2.77 0 -3 -7 6 204.52 3.10 0 -2 7 6 22.19 1.75 0 -2 -7 6 26.33 2.15 0 2 -7 -6 25.89 1.79 0 -1 -7 6 10.81 2.18 0 1 -7 -6 10.34 1.67 0 -1 7 6 9.44 2.09 0 0 7 -6 1.70 1.56 0 0 -7 6 4.89 2.25 0 0 -7 -6 2.80 1.60 0 0 7 6 2.39 1.61 0 -1 7 -6 28.61 2.31 0 -1 -7 -6 31.30 2.40 0 1 -7 6 30.69 2.40 0 1 7 6 26.39 2.27 0 2 -7 6 -0.27 1.72 0 -2 -7 -6 4.59 2.33 0 2 7 6 -0.24 2.33 0 -2 7 -6 0.45 2.26 0 3 -7 6 2.26 2.37 0 -3 7 -6 2.66 1.72 0 -3 -7 -6 -1.29 2.39 0 3 7 6 2.83 1.76 0 -4 7 -6 7.76 2.66 0 -4 -7 -6 6.02 2.64 0 4 7 6 9.73 1.90 0 4 -7 6 11.94 2.81 0 -5 7 -6 0.49 2.96 0 -5 -7 -6 2.55 2.00 0 5 7 6 1.80 2.91 0 5 -7 6 3.64 3.11 0 -8 -8 6 1.93 2.78 0 -7 8 6 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0.68 2.05 0 0 -9 10 1.21 2.09 0 0 9 10 1.76 2.90 0 -1 -9 -10 1.62 2.17 0 1 -9 10 2.76 3.19 0 1 9 10 2.57 3.00 0 -6 -10 10 3.98 3.13 0 -6 10 10 5.37 3.32 0 -6 -10 10 6.99 3.03 0 -5 -10 10 1.87 2.10 0 -5 -10 10 4.16 2.85 0 -5 10 10 2.44 3.17 0 4 -10 -10 -1.56 3.10 0 -4 -10 10 0.42 1.96 0 -4 10 10 0.96 2.04 0 -4 -10 10 3.01 1.97 0 3 -10 -10 3.81 2.24 0 -3 -10 10 3.50 2.72 0 -3 10 10 2.91 2.89 0 2 -10 -10 13.69 3.11 0 -2 10 10 17.82 2.95 0 -2 -10 10 18.17 2.80 0 1 -10 -10 0.26 3.08 0 -1 -10 10 -0.72 1.96 0 -1 10 10 -0.77 2.85 0 0 -10 -10 1.06 2.12 0 0 -10 10 1.00 2.02 0 0 10 10 3.03 2.10 0 -1 -10 -10 0.73 3.12 0 1 -10 10 0.49 3.18 0 1 10 10 -1.55 2.15 0 -6 -11 10 3.44 3.14 0 -6 11 10 -0.21 4.16 0 -6 -11 10 2.72 2.22 0 -5 -11 10 4.93 2.26 0 -5 -11 10 7.97 2.22 0 -5 11 10 9.04 3.18 0 4 -11 -10 2.58 3.20 0 -4 -11 10 -0.77 2.07 0 -4 11 10 1.17 3.01 0 -4 -11 10 2.08 2.97 0 3 -11 -10 7.46 2.97 0 -3 -11 10 5.05 2.00 0 -3 11 10 0.34 2.92 0 -3 -11 10 2.06 2.94 0 -2 -11 10 2.39 2.91 0 2 -11 -10 0.41 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3 11 5.33 3.14 0 -7 -4 11 -0.83 3.15 0 -7 -4 11 1.31 3.09 0 -7 4 11 2.51 3.26 0 -7 4 11 1.85 3.19 0 -6 -4 11 0.75 2.08 0 -6 4 11 -0.00 3.03 0 -6 -4 11 1.58 2.18 0 -5 -4 11 21.67 2.96 0 -5 4 11 18.28 2.90 0 4 -4 -11 1.37 2.14 0 -4 4 11 1.17 2.09 0 -4 -4 11 -0.46 2.79 0 3 -4 -11 11.76 2.15 0 -3 4 11 10.80 2.09 0 -3 -4 11 13.85 2.91 0 -2 4 11 7.69 2.75 0 2 -4 -11 7.43 1.97 0 -2 -4 11 4.99 2.81 0 -1 4 11 6.09 2.94 0 1 4 -11 2.47 2.97 0 -1 -4 11 7.68 2.86 0 1 -4 -11 5.27 1.98 0 0 -4 11 0.74 2.19 0 0 4 -11 0.64 2.13 0 0 -4 -11 0.08 2.00 0 0 4 11 1.98 2.86 0 1 -4 11 1.79 3.06 0 -1 -4 -11 2.74 3.08 0 -1 4 -11 1.30 2.13 0 1 4 11 1.63 3.06 0 -7 -5 11 -0.68 3.28 0 -7 -5 11 -0.51 3.22 0 -7 5 11 0.58 3.35 0 -7 5 11 1.12 3.31 0 -6 -5 11 13.26 2.99 0 -6 5 11 10.65 2.29 0 -6 -5 11 14.36 3.15 0 -5 -5 11 0.37 2.82 0 -5 5 11 2.53 2.90 0 -4 5 11 -0.31 2.78 0 4 -5 -11 0.61 2.87 0 -4 -5 11 -0.72 1.90 0 -3 5 11 7.30 2.03 0 -3 -5 11 4.83 2.78 0 3 -5 -11 3.10 2.88 0 -2 5 11 3.38 2.75 0 2 -5 -11 3.92 2.82 0 -2 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2.15 2.10 0 -3 -7 11 0.51 1.96 0 -2 -7 11 5.09 2.98 0 -2 7 11 6.62 2.91 0 2 -7 -11 5.71 2.93 0 -1 -7 11 2.56 2.96 0 1 -7 -11 3.54 2.12 0 -1 7 11 7.27 3.00 0 0 -7 11 1.71 2.25 0 0 -7 -11 4.91 2.27 0 0 7 11 9.12 3.08 0 1 7 11 0.31 3.34 0 -6 -8 11 1.15 3.06 0 -6 8 11 2.38 3.32 0 -6 -8 11 -1.49 3.14 0 -5 8 11 1.67 3.10 0 -5 -8 11 1.96 2.10 0 -5 -8 11 0.87 3.07 0 -4 8 11 -0.04 2.98 0 -4 -8 11 1.19 2.07 0 4 -8 -11 -1.43 2.99 0 3 -8 -11 4.68 2.33 0 -3 -8 11 7.90 2.90 0 -3 8 11 3.15 2.04 0 -2 -8 11 16.02 3.00 0 -2 8 11 10.83 3.09 0 2 -8 -11 13.55 3.05 0 -1 -8 11 3.36 2.97 0 1 -8 -11 2.77 3.07 0 -1 8 11 7.82 2.96 0 0 -8 -11 1.85 2.13 0 0 -8 11 4.39 2.27 0 0 8 11 2.99 3.10 0 -5 9 11 1.06 3.22 0 -5 -9 11 0.62 2.12 0 -5 -9 11 -0.68 3.06 0 -4 -9 11 6.24 2.12 0 4 -9 -11 4.77 3.36 0 -4 9 11 5.34 3.01 0 3 -9 -11 9.36 2.34 0 -3 9 11 7.69 3.12 0 -3 -9 11 8.94 3.07 0 -2 -9 11 0.67 2.08 0 2 -9 -11 1.19 3.11 0 -2 9 11 -1.34 2.91 0 1 -9 -11 -0.18 3.13 0 -1 -9 11 1.72 3.08 0 -1 9 11 2.01 2.21 0 0 -9 -11 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3.46 2.94 0 -3 -1 12 0.73 2.02 0 3 -1 -12 -1.12 2.00 0 2 1 -12 0.36 2.05 0 -2 1 12 -1.00 2.13 0 2 -1 -12 1.01 3.07 0 -2 -1 12 -1.96 2.15 0 1 1 -12 1.42 2.13 0 -1 1 12 1.34 2.24 0 -1 -1 12 3.68 3.04 0 1 -1 -12 0.64 3.16 0 0 1 12 -3.95 3.33 0 0 -1 12 1.74 2.26 0 0 -1 -12 0.96 2.34 0 0 1 -12 -3.71 3.18 0 -6 2 12 4.17 2.35 0 -6 -2 12 2.48 3.28 0 -5 2 12 1.97 2.18 0 -5 -2 12 2.10 2.17 0 -4 2 12 2.85 2.77 0 -4 -2 12 3.13 2.92 0 -3 2 12 -0.41 2.85 0 3 -2 -12 1.86 3.03 0 -3 -2 12 -0.59 2.10 0 -2 2 12 8.22 3.08 0 -2 -2 12 3.80 2.20 0 2 2 -12 2.98 2.19 0 2 -2 -12 3.41 2.23 0 -1 2 12 -0.69 2.14 0 -1 -2 12 2.18 3.04 0 1 -2 -12 0.47 3.06 0 1 2 -12 0.93 2.16 0 0 -2 12 2.98 2.38 0 0 -2 -12 3.36 3.27 0 0 2 -12 1.32 3.21 0 0 2 12 2.54 3.28 0 -6 3 12 1.01 2.27 0 -6 -3 12 0.97 3.35 0 -6 -3 12 6.94 3.18 0 -5 3 12 8.68 2.42 0 -5 -3 12 11.36 2.30 0 -4 3 12 3.49 3.03 0 -4 -3 12 0.67 2.16 0 -3 3 12 1.83 2.97 0 -3 -3 12 -0.04 3.03 0 3 -3 -12 1.35 2.15 0 -2 3 12 0.09 3.00 0 -2 -3 12 0.83 3.11 0 2 3 -12 -0.66 2.03 0 2 -3 -12 -0.47 3.05 0 -1 3 12 2.15 3.06 0 1 3 -12 0.23 2.11 0 1 -3 -12 -2.06 2.22 0 -1 -3 12 0.85 2.19 0 0 -3 12 4.37 3.32 0 0 3 -12 0.00 3.34 0 0 3 12 2.05 3.26 0 -6 4 12 0.77 2.36 0 -6 -4 12 -0.95 2.40 0 -6 -4 12 -0.14 2.29 0 -5 4 12 0.83 3.16 0 -5 -4 12 1.62 2.15 0 -4 4 12 1.43 2.06 0 4 -4 -12 -0.91 2.12 0 -4 -4 12 0.39 2.14 0 -3 4 12 -0.69 2.19 0 3 -4 -12 0.74 3.04 0 -3 -4 12 -0.57 3.05 0 -2 4 12 3.76 2.21 0 -2 -4 12 2.06 2.16 0 2 -4 -12 1.66 2.26 0 1 -4 -12 2.04 3.06 0 -1 -4 12 4.26 3.10 0 1 4 -12 1.95 2.14 0 -1 4 12 -0.93 3.15 0 -5 5 12 2.70 2.38 0 -5 -5 12 2.38 3.14 0 -4 5 12 -0.68 2.24 0 4 -5 -12 1.00 3.17 0 -4 -5 12 2.83 3.04 0 3 -5 -12 4.71 2.21 0 -3 5 12 2.56 3.15 0 -3 -5 12 3.99 2.26 0 -2 5 12 5.03 3.09 0 2 -5 -12 2.17 3.19 0 -2 -5 12 2.97 3.00 0 1 -5 -12 4.20 3.21 0 -1 -5 12 1.32 2.25 0 1 5 -12 0.42 2.24 0 -1 5 12 -0.11 2.19 0 -5 6 12 0.39 3.25 0 -5 -6 12 1.83 3.09 0 -4 6 12 5.79 2.38 0 4 -6 -12 3.29 3.42 0 -4 -6 12 3.92 2.30 0 -3 6 12 0.80 3.09 0 -3 -6 12 -0.21 2.13 0 3 -6 -12 -0.90 2.08 0 2 -6 -12 6.82 3.29 0 -2 -6 12 2.74 2.22 0 -2 6 12 5.67 3.25 0 -1 -6 12 9.52 3.27 0 -1 6 12 9.88 3.19 0 1 -6 -12 3.51 2.24 0 -5 7 12 -0.21 3.24 0 -4 7 12 1.91 3.17 0 4 -7 -12 1.59 3.42 0 -4 -7 12 2.16 2.27 0 -3 7 12 0.48 3.20 0 3 -7 -12 -0.21 2.29 0 -3 -7 12 0.77 3.12 0 2 -7 -12 2.73 3.29 0 -2 -7 12 6.48 3.22 0 -2 7 12 2.93 2.28 0 -4 8 12 11.21 3.27 0 -4 -8 12 8.71 2.32 0 3 -8 -12 0.80 2.38 0 -3 -8 12 0.68 3.23 0 -3 8 12 0.64 3.30 0 -2 -8 12 1.30 3.36 0 ; _shelx_hkl_checksum 43198 _shelx_res_file ; TITL shelxt_a.res in P2(1)/c shelx.res created by SHELXL-2018/3 at 17:35:36 on 15-Aug-2019 CELL 0.71073 6.9932 16.2916 9.3544 90.000 110.168 90.000 ZERR 4.00 0.0005 0.0009 0.0007 0.000 0.006 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O S UNIT 40 40 8 4 4 MERG 2 OMIT -2.00 52.00 EQIV $1 -x+2, -y+1, -z+1 HTAB N1 O1_$1 EQIV $2 x-1, y, z+1 HTAB C10 O1_$2 DELU 0.0010 0.010 C8 C9 SIMU 0.0040 0.080 1.700 C8 C9 ISOR 0.0100 C8 C9 FMAP 2 PLAN 5 ACTA BOND $H CONF LIST 6 L.S. 25 WGHT 0.079000 FVAR 0.72643 S1 5 0.230307 0.425257 0.989253 11.00000 0.09786 0.07365 = 0.07292 -0.01387 0.04755 -0.01472 O1 4 0.884418 0.417240 0.362569 11.00000 0.08949 0.08159 = 0.07463 -0.01031 0.05401 -0.01438 N2 3 0.691022 0.456650 0.660003 11.00000 0.05936 0.06194 = 0.05265 -0.00293 0.02720 -0.00396 N1 3 0.809689 0.454513 0.568175 11.00000 0.06038 0.06438 = 0.05804 -0.00651 0.03117 -0.01077 C4 1 0.561781 0.398387 0.643974 11.00000 0.05335 0.05348 = 0.05223 -0.00070 0.02155 0.00116 C7 1 0.194873 0.348948 0.856302 11.00000 0.05214 0.05611 = 0.04649 0.00541 0.01649 0.00323 C6 1 0.306494 0.346664 0.751675 11.00000 0.05728 0.05298 = 0.05416 -0.00155 0.02416 0.00020 AFIX 43 H6 2 0.277544 0.303662 0.682065 11.00000 -1.20000 AFIX 0 C5 1 0.446794 0.400537 0.746091 11.00000 0.06099 0.05648 = 0.05249 -0.00425 0.02609 -0.00335 AFIX 43 H5 2 0.473561 0.443933 0.814790 11.00000 -1.20000 AFIX 0 C8 1 0.048420 0.293841 0.866043 11.00000 0.06514 0.06595 = 0.05427 0.00488 0.02492 -0.00875 AFIX 43 H8 2 0.005051 0.248100 0.803758 11.00000 -1.20000 AFIX 0 C1 1 0.773400 0.411331 0.438948 11.00000 0.06546 0.05541 = 0.05499 0.00144 0.02785 0.00231 C2 1 0.588045 0.359250 0.395967 11.00000 0.06961 0.06679 = 0.05995 -0.01177 0.02807 -0.00523 AFIX 23 H2A 2 0.607918 0.311934 0.339710 11.00000 -1.20000 H2B 2 0.473610 0.390273 0.329261 11.00000 -1.20000 AFIX 0 C3 1 0.537640 0.330007 0.532543 11.00000 0.07566 0.06387 = 0.07982 -0.01498 0.04593 -0.01334 AFIX 23 H3A 2 0.398564 0.309944 0.499271 11.00000 -1.20000 H3B 2 0.627316 0.285060 0.581438 11.00000 -1.20000 AFIX 0 C10 1 0.056969 0.383834 1.057223 11.00000 0.08686 0.08853 = 0.05828 0.00624 0.04030 0.00845 AFIX 43 H10 2 0.023862 0.405884 1.137400 11.00000 -1.20000 AFIX 0 C9 1 -0.025984 0.316344 0.982849 11.00000 0.06855 0.09095 = 0.06242 0.00972 0.03286 -0.00967 AFIX 43 H9 2 -0.124891 0.286306 1.005625 11.00000 -1.20000 AFIX 0 H1 2 0.901879 0.489682 0.592544 11.00000 0.05790 HKLF 4 REM shelxt_a.res in P2(1)/c REM wR2 = 0.1346, GooF = S = 1.022, Restrained GooF = 1.035 for all data REM R1 = 0.0446 for 1394 Fo > 4sig(Fo) and 0.0657 for all 1971 data REM 131 parameters refined using 19 restraints END WGHT 0.0790 0.0000 REM Highest difference peak 0.241, deepest hole -0.343, 1-sigma level 0.041 Q1 1 0.0242 0.3240 0.8286 11.00000 0.05 0.24 Q2 1 0.1397 0.2966 0.8791 11.00000 0.05 0.22 Q3 1 0.2395 0.3656 0.9256 11.00000 0.05 0.16 Q4 1 0.4517 0.3556 0.4647 11.00000 0.05 0.15 Q5 1 0.0422 0.2995 0.9222 11.00000 0.05 0.14 ; _shelx_res_checksum 65775 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy S S1 0.23031(12) 0.42526(4) 0.98925(7) 0.0768(3) Uani d 1 O O1 0.8844(3) 0.41724(11) 0.36257(19) 0.0752(5) Uani d 1 N N2 0.6910(3) 0.45665(12) 0.66000(19) 0.0559(5) Uani d 1 N N1 0.8097(3) 0.45451(13) 0.5682(2) 0.0581(5) Uani d 1 C C4 0.5618(3) 0.39839(14) 0.6440(2) 0.0521(5) Uani d 1 C C7 0.1949(3) 0.34895(13) 0.8563(2) 0.0517(5) Uani d 1 C C6 0.3065(3) 0.34666(13) 0.7517(2) 0.0535(5) Uani d 1 H H6 0.277544 0.303662 0.682065 0.064 Uiso calc 1 C C5 0.4468(3) 0.40054(14) 0.7461(2) 0.0549(5) Uani d 1 H H5 0.473561 0.443933 0.814790 0.066 Uiso calc 1 C C8 0.0484(4) 0.29384(15) 0.8660(2) 0.0607(6) Uani d 1 H H8 0.005051 0.248100 0.803758 0.073 Uiso calc 1 C C1 0.7734(3) 0.41133(14) 0.4389(2) 0.0568(6) Uani d 1 C C2 0.5880(4) 0.35925(15) 0.3960(2) 0.0640(6) Uani d 1 H H2A 0.607918 0.311934 0.339710 0.077 Uiso calc 1 H H2B 0.473610 0.390273 0.329261 0.077 Uiso calc 1 C C3 0.5376(4) 0.33001(16) 0.5325(3) 0.0681(6) Uani d 1 H H3A 0.398564 0.309944 0.499271 0.082 Uiso calc 1 H H3B 0.627316 0.285060 0.581438 0.082 Uiso calc 1 C C10 0.0570(4) 0.38383(19) 1.0572(3) 0.0739(7) Uani d 1 H H10 0.023862 0.405884 1.137400 0.089 Uiso calc 1 C C9 -0.0260(4) 0.31634(18) 0.9828(3) 0.0713(6) Uani d 1 H H9 -0.124891 0.286306 1.005625 0.086 Uiso calc 1 H H1 0.902(4) 0.4897(15) 0.593(2) 0.058(7) Uiso d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.0979(5) 0.0736(5) 0.0729(4) -0.0147(4) 0.0476(4) -0.0139(3) O1 0.0895(12) 0.0816(12) 0.0746(10) -0.0144(10) 0.0540(9) -0.0103(8) N2 0.0594(11) 0.0619(11) 0.0527(9) -0.0040(9) 0.0272(8) -0.0029(8) N1 0.0604(11) 0.0644(12) 0.0580(10) -0.0108(10) 0.0312(9) -0.0065(9) C4 0.0534(11) 0.0535(12) 0.0522(11) 0.0012(10) 0.0216(9) -0.0007(9) C7 0.0521(11) 0.0561(13) 0.0465(10) 0.0032(10) 0.0165(9) 0.0054(9) C6 0.0573(12) 0.0530(13) 0.0542(11) 0.0002(10) 0.0242(10) -0.0016(9) C5 0.0610(12) 0.0565(13) 0.0525(11) -0.0034(11) 0.0261(9) -0.0043(9) C8 0.0651(13) 0.0659(14) 0.0543(11) -0.0087(11) 0.0249(9) 0.0049(9) C1 0.0655(13) 0.0554(13) 0.0550(11) 0.0023(11) 0.0279(10) 0.0014(9) C2 0.0696(14) 0.0668(15) 0.0599(12) -0.0052(12) 0.0281(11) -0.0118(10) C3 0.0757(15) 0.0639(15) 0.0798(15) -0.0133(12) 0.0459(13) -0.0150(12) C10 0.0869(17) 0.0885(19) 0.0583(13) 0.0085(16) 0.0403(12) 0.0062(13) C9 0.0686(14) 0.0910(18) 0.0624(12) -0.0097(13) 0.0329(10) 0.0097(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_publ_flag C10 S1 C7 92.31(13) y C4 N2 N1 117.21(18) ? C1 N1 N2 127.1(2) ? C1 N1 H1 119.6(16) ? N2 N1 H1 112.7(16) ? N2 C4 C5 115.76(19) ? N2 C4 C3 122.57(19) ? C5 C4 C3 121.6(2) ? C8 C7 C6 127.6(2) ? C8 C7 S1 110.28(16) ? C6 C7 S1 122.15(16) ? C5 C6 C7 125.9(2) ? C5 C6 H6 117.1 ? C7 C6 H6 117.1 ? C6 C5 C4 126.5(2) ? C6 C5 H5 116.7 ? C4 C5 H5 116.7 ? C7 C8 C9 111.1(2) ? C7 C8 H8 124.4 ? C9 C8 H8 124.4 ? O1 C1 N1 121.4(2) y O1 C1 C2 123.8(2) ? N1 C1 C2 114.77(19) ? C1 C2 C3 112.76(18) ? C1 C2 H2A 109.0 ? C3 C2 H2A 109.0 ? C1 C2 H2B 109.0 ? C3 C2 H2B 109.0 ? H2A C2 H2B 107.8 ? C4 C3 C2 110.5(2) ? C4 C3 H3A 109.5 ? C2 C3 H3A 109.5 ? C4 C3 H3B 109.5 ? C2 C3 H3B 109.5 ? H3A C3 H3B 108.1 ? C9 C10 S1 112.02(19) ? C9 C10 H10 124.0 ? S1 C10 H10 124.0 ? C10 C9 C8 114.3(2) ? C10 C9 H9 122.9 ? C8 C9 H9 122.9 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_publ_flag S1 C10 1.691(3) y S1 C7 1.715(2) ? O1 C1 1.227(3) y N2 C4 1.283(3) y N2 N1 1.385(2) y N1 C1 1.345(3) y N1 H1 0.83(2) ? C4 C5 1.446(3) ? C4 C3 1.495(3) ? C7 C8 1.388(3) ? C7 C6 1.448(3) ? C6 C5 1.331(3) ? C6 H6 0.9300 ? C5 H5 0.9300 ? C8 C9 1.411(3) ? C8 H8 0.9300 ? C1 C2 1.484(3) ? C2 C3 1.515(3) ? C2 H2A 0.9700 ? C2 H2B 0.9700 ? C3 H3A 0.9700 ? C3 H3B 0.9700 ? C10 C9 1.323(4) ? C10 H10 0.9300 ? C9 H9 0.9300 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 O1 3_766 0.83(3) 2.07(3) 2.899(3) 175(2) yes C10 H10 O1 1_456 0.93 2.61 3.505(3) 160.5 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_publ_flag C4 N2 N1 C1 18.1(3) ? N1 N2 C4 C5 177.40(18) ? N1 N2 C4 C3 0.3(3) ? C10 S1 C7 C8 0.74(18) ? C10 S1 C7 C6 -179.65(18) ? C8 C7 C6 C5 -179.7(2) ? S1 C7 C6 C5 0.8(3) ? C7 C6 C5 C4 179.0(2) y N2 C4 C5 C6 -179.4(2) y C3 C4 C5 C6 -2.3(4) ? C6 C7 C8 C9 179.8(2) ? S1 C7 C8 C9 -0.6(2) ? N2 N1 C1 O1 176.4(2) ? N2 N1 C1 C2 -1.9(3) ? O1 C1 C2 C3 152.4(2) ? N1 C1 C2 C3 -29.5(3) ? N2 C4 C3 C2 -30.2(3) ? C5 C4 C3 C2 152.9(2) ? C1 C2 C3 C4 43.3(3) ? C7 S1 C10 C9 -0.7(2) ? S1 C10 C9 C8 0.5(3) ? C7 C8 C9 C10 0.1(3) ? _cod_database_fobs_code 2243199