#------------------------------------------------------------------------------ #$Date: 2019-11-20 07:56:16 +0200 (Wed, 20 Nov 2019) $ #$Revision: 231079 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/32/2243205.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243205 loop_ _publ_author_name 'Yang, Hequn' 'Zhao, Jiangyu' 'Talipov, Samat' 'Izotova, Lidiya' 'Aisa, Hadji Akbar' 'Ibragimov, Bakhtiyar' _publ_section_title ; Crystal and molecular structure of jatrophane diterpenoid (2R,3R,4S,5R,7S,8S,9S,13S,14S,15R)-2,3,8,9-tetraacetoxy-5,14-bis(benzoyloxy)-15-hydroxy-7-(isobutanoyloxy)jatropha-6(17),11(E)-diene ; _journal_coeditor_code FY2141 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 1884 _journal_page_last 1887 _journal_paper_doi 10.1107/S205698901901541X _journal_volume 75 _journal_year 2019 _chemical_absolute_configuration rm _chemical_formula_iupac 'C46 H56 O15' _chemical_formula_moiety 'C46 H56 O15' _chemical_formula_sum 'C46 H56 O15' _chemical_formula_weight 848.90 _chemical_melting_point 166 _chemical_name_common jatrophan _chemical_name_systematic (2R,3R,4S,5R,7S,8S,9S,13S,14S,15R)-2,3,8,9-Tetraacetoxy-5,14-bis(benzoyloxy)-15-hydroxy-7-(isobutanoyloxy)jatropha-6(17),11(E)-diene _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.9730(5) _cell_length_b 20.9171(9) _cell_length_c 23.9201(11) _cell_measurement_reflns_used 5355 _cell_measurement_temperature 104(2) _cell_measurement_theta_max 69.5640 _cell_measurement_theta_min 4.2370 _cell_volume 4489.5(4) _computing_cell_refinement ; CrysAlis PRO (Agilent, 2014) ; _computing_data_collection ; CrysAlis PRO (Agilent, 2014) ; _computing_data_reduction ; CrysAlis PRO (Agilent, 2014) ; _computing_molecular_graphics ; XP (Siemens, 1994) ; _computing_publication_material ; XP (Siemens, 1994) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 104(7) _diffrn_detector_area_resol_mean 10.2576 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Agilent Xcalibur Ruby' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0584 _diffrn_reflns_av_unetI/netI 0.0422 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 37870 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.461 _diffrn_reflns_theta_min 3.696 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.778 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.74820 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis PRO; Agilent, 2014) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.256 _exptl_crystal_density_meas 1.256 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 1808 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.258 _refine_diff_density_min -0.186 _refine_ls_abs_structure_details ; Flack x determined using 2403 quotients [(I^+^)-(I^-^)]/[(I^+^)+(I^-^)] (Parsons et al., 2013) ; _refine_ls_abs_structure_Flack -0.06(11) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.016 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 587 _refine_ls_number_reflns 9301 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.016 _refine_ls_R_factor_all 0.0793 _refine_ls_R_factor_gt 0.0563 _refine_ls_shift/su_max 0.010 _refine_ls_shift/su_mean 0.002 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0710P)^2^+1.4583P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1360 _refine_ls_wR_factor_ref 0.1534 _reflns_number_gt 7007 _reflns_number_total 9301 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file fy2141sup1.cif _cod_data_source_block I _cod_database_code 2243205 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.830 _shelx_estimated_absorpt_t_max 0.925 _shelx_hkl_file ; 0 0 -2 884811. 2802.87 6 0 0 -2 848432. 2694.50 4 0 0 -3 942.365 166.306 29 0 0 -3 734.187 167.167 4 0 0 -4 3690.98 284.648 29 0 0 -4 3719.64 313.481 4 0 0 -4 3646.11 328.785 6 0 0 -5 15.7927 225.135 4 0 0 -5 60.9310 255.050 6 0 0 -5 164.493 202.574 29 0 0 -6 527367. 3832.00 6 0 0 -6 522708. 3705.78 4 0 0 -7 245.391 292.387 4 0 0 -7-99.5051 333.148 6 0 0 -8 3419.19 496.733 6 0 0 -9 119.157 374.016 6 0 0 -10-73.7405 412.047 6 0 0 -11 110.841 423.156 6 0 0 -12 1961.97 530.124 6 0 0 -13-708.302 495.829 6 0 0 -14 2539.31 659.769 6 0 0 -15-2.13590 522.590 6 0 0 -16 1377.20 622.065 6 0 0 -17 73.6844 563.182 6 0 0 -18 569.883 591.969 28 0 0 -18 362.147 628.549 6 0 0 -18 1712.27 715.144 26 0 0 -19 421.274 608.548 6 0 0 -19 525.200 628.068 28 0 0 -19 439.896 558.491 26 0 0 -19-711.208 575.090 13 0 0 -20 8760.45 1190.97 26 0 0 -20 11797.9 1449.44 28 0 0 -20 10337.0 1288.38 6 0 0 -21 528.545 611.886 28 0 0 -21-81.0754 570.599 26 0 0 -22 8322.74 1146.43 26 0 0 -22 4793.12 1008.77 28 0 0 -23-286.365 594.839 28 0 0 -23-661.648 617.281 26 0 0 -24 5380.72 920.619 26 0 0 -24 5439.36 980.729 28 0 0 -25-62.8536 491.411 28 0 0 -25-351.176 602.334 26 0 0 -26 2110.12 720.663 28 0 0 -26 2214.92 757.787 26 0 0 -27-191.999 537.340 26 0 0 -28 370.617 456.774 26 0 0 -29-153.278 430.203 26 0 0 -30 895.045 337.299 26 0 1 -2 233178. 1600.31 29 0 -1 -2 232362. 1440.10 3 0 -1 -2 235594. 1507.85 6 0 -1 -3 184461. 1600.60 6 0 1 -3 175615. 1612.36 29 0 -1 -3 176968. 1532.37 3 0 -1 -3 182869. 1495.26 4 0 1 -4 57941.7 1047.68 29 0 -1 -4 61607.4 1065.53 6 0 1 -4 60716.4 1150.58 6 0 -1 -4 57346.3 1005.27 3 0 -1 -4 55298.5 969.013 4 0 -1 -5 89925.2 1432.36 6 0 1 -5 85338.8 1364.99 29 0 1 -5 91276.0 1542.76 6 0 -1 -5 84555.7 1360.11 4 0 -1 -6 14625.8 657.060 4 0 -1 -6 14093.8 685.563 6 0 1 -6 12089.7 680.500 6 0 1 -6 12468.6 631.304 29 0 -1 -7 753.025 377.440 6 0 1 -7 480.735 132.246 5 0 1 -7 768.312 368.800 6 0 -1 -7 557.053 313.483 4 0 1 -7 582.809 305.258 29 0 1 -8 7542.40 281.118 5 0 -1 -8 8143.35 645.867 6 0 -1 -8 7888.87 619.628 4 0 1 -8 8611.89 688.309 6 0 -1 -9 5990.26 626.776 6 0 1 -9 4397.77 178.744 5 0 -1 -9 6355.37 579.950 4 0 1 -9 5922.79 635.636 6 0 -1 -10 106377. 2280.60 6 0 1 -10 100810. 2298.76 6 0 -1 -11 283.684 442.150 6 0 1 -11 760.443 493.422 6 0 1 -12 17247.3 1139.21 6 0 -1 -12 16781.1 1092.41 6 0 -1 -13 51551.6 1891.09 6 0 1 -13 53992.6 1994.93 6 0 1 -14 28087.7 1563.61 6 0 -1 -14 27374.9 1496.64 6 0 1 -15-757.488 546.271 6 0 -1 -15-692.172 575.575 6 0 1 -16 2104.59 673.554 6 0 -1 -16 2643.41 760.729 6 0 -1 -17 7633.69 992.007 6 0 1 -17 5929.56 959.621 6 0 1 -18 8375.77 1194.69 17 0 -1 -18 9114.44 1158.17 26 0 -1 -18 9177.86 1202.42 28 0 1 -18 8292.15 1235.79 28 0 1 -18 8258.08 1125.89 26 0 -1 -18 9236.14 1148.39 6 0 1 -18 8727.57 1166.44 6 0 1 -19 5245.26 950.591 13 0 -1 -19 4378.52 924.229 28 0 1 -19 6275.88 1063.83 26 0 1 -19 5156.37 1045.20 28 0 -1 -19 3791.76 839.149 26 0 1 -19 4490.92 938.363 6 0 -1 -19 2224.60 736.696 6 0 -1 -20 38383.2 2390.45 28 0 -1 -20 39052.7 2189.24 26 0 1 -20 38711.7 2186.64 26 0 1 -20 36343.3 2205.93 6 0 -1 -20 37349.8 2209.31 6 0 1 -20 35753.9 2263.02 28 0 1 -20 40563.2 2125.39 13 0 1 -21 13903.6 1536.79 28 0 1 -21 12668.1 1334.20 13 0 1 -21 10930.3 1256.21 26 0 -1 -21 10210.9 1352.99 28 0 -1 -21 10622.2 1241.11 26 0 -1 -22 1285.77 737.329 26 0 1 -22 257.627 607.519 28 0 -1 -22 1856.65 802.226 28 0 1 -22 714.838 619.897 26 0 -1 -23 3366.43 830.548 28 0 -1 -23 2974.41 794.424 26 0 1 -23 3069.52 835.026 26 0 1 -23 3738.74 870.515 28 0 1 -24 223.280 614.101 28 0 -1 -24 565.272 487.057 28 0 1 -24-54.2028 602.038 26 0 -1 -24 8.48955 530.383 26 0 1 -25 6843.00 1099.94 28 0 1 -25 6633.13 1007.73 26 0 -1 -25 6068.81 980.873 26 0 -1 -25 5444.32 1015.30 28 0 1 -26 788.547 649.336 26 0 -1 -26 76.7520 498.095 26 0 1 -26 887.262 615.099 28 0 1 -27 11725.1 1086.47 26 0 -1 -27 11522.3 1125.55 26 0 -1 -28-64.8838 473.414 26 0 1 -28 213.978 455.207 26 0 1 -29 1322.64 471.365 26 0 -1 -29 1142.67 431.380 26 0 -1 -30 1139.91 347.502 26 0 1 -30 1311.17 354.120 26 0 -2 0 103911. 1055.99 2 0 2 0 105686. 960.846 29 0 -2 -1 903479. 3135.20 6 0 2 -1 891998. 3274.54 29 0 -2 -2 545197. 2680.13 6 0 2 -2 544321. 2881.93 29 0 2 -3 185770. 1909.41 29 0 -2 -3 191008. 1770.63 6 0 -2 -3 188167. 1653.38 3 0 -2 -4 345626. 2369.52 4 0 2 -4 350135. 2816.37 29 0 2 4 349352. 1503.37 5 0 -2 -5 11930.7 533.065 4 0 2 -5 11587.9 607.607 29 0 -2 -5 12419.5 595.810 6 0 -2 -5 11107.1 555.270 3 0 2 -6 51376.9 1354.03 6 0 -2 -6 53279.3 1187.40 4 0 -2 -6 54930.1 1250.68 6 0 -2 -6 54188.5 1227.75 3 0 2 -6 53521.4 1285.59 29 0 2 -7 235794. 2786.60 29 0 -2 -7 243416. 2678.65 4 0 -2 -7 235861. 2758.46 6 0 2 -7 234734. 3040.97 6 0 2 -8 139082. 2267.44 29 0 2 -8 139785. 1555.79 5 0 2 -8 142706. 2498.12 6 0 -2 -8 140442. 2294.13 6 0 -2 -8 142227. 2228.02 4 0 -2 -9 82963.4 1888.72 6 0 2 -9 80685.7 1159.81 5 0 2 -9 79914.1 1993.42 6 0 -2 -9 79533.6 1842.61 4 0 -2 -10 3465.88 591.107 6 0 2 -10 3658.46 258.177 5 0 -2 -10 4016.70 534.333 4 0 2 -10 3673.30 647.303 6 0 -2 -11 33247.6 1405.06 6 0 2 -11 34261.3 1493.05 6 0 -2 -12 63233.5 1993.32 6 0 2 -12 62943.6 2097.89 6 0 2 -13 84887.3 2542.56 6 0 -2 -13 80704.6 2352.67 6 0 2 -14 8558.77 979.184 6 0 -2 -14 8432.39 929.192 6 0 2 -15 5431.33 840.272 6 0 -2 -15 5384.66 819.248 6 0 -2 -16 3832.49 750.757 6 0 2 -16 2746.40 723.057 6 0 -2 -17 5.00540 580.477 6 0 2 -17 315.075 617.547 6 0 2 -18 5235.83 988.969 26 0 2 -18 7021.94 1062.65 14 0 -2 -18 6685.17 1164.43 28 0 2 -18 7339.07 1078.46 6 0 -2 -18 7569.76 1087.56 26 0 2 -18 6754.71 1038.93 17 0 -2 -18 7382.12 1014.82 6 0 2 -18 6785.49 1139.49 28 0 2 -19-418.962 470.883 17 0 -2 -19-879.252 724.487 28 0 2 -19 490.357 587.341 28 0 2 -19 766.108 635.125 6 0 2 -19-121.576 513.736 26 0 -2 -19 452.325 658.612 26 0 2 -19 516.714 523.330 13 0 -2 -19-372.006 578.935 6 0 2 -20 5016.49 997.522 6 0 -2 -20 4185.26 1020.76 6 0 2 -20 4778.71 982.764 26 0 -2 -20 4958.77 1037.19 28 0 -2 -20 5291.23 963.684 26 0 2 -20 4806.49 1028.42 13 0 2 -20 4220.08 1035.39 28 0 -2 -21 3249.49 816.748 26 0 2 -21 2071.38 767.251 26 0 -2 -21 2169.07 832.158 28 0 2 -21 2183.78 760.642 13 0 2 -21 3420.17 935.621 28 0 2 -22 1038.74 624.927 13 0 -2 -22 442.245 677.728 28 0 -2 -22 807.300 624.733 26 0 2 -22 300.074 573.712 28 0 2 -22 678.056 526.600 26 0 -2 -23 2938.99 813.884 26 0 2 -23 2443.94 883.724 28 0 2 -23 2339.26 824.239 26 0 -2 -23 1900.78 707.400 28 0 2 -24-84.9344 534.604 28 0 -2 -24 442.687 672.093 26 0 2 -24 588.202 680.930 26 0 -2 -24-283.263 611.745 28 0 2 -25 458.708 529.959 28 0 -2 -25-86.2997 624.462 26 0 2 -25 158.488 594.279 26 0 -2 -25 31.7477 579.136 28 0 2 -26 1803.02 708.137 28 0 -2 -26 2478.41 770.157 26 0 2 -26 2763.66 742.539 26 0 2 -27-126.439 559.712 26 0 -2 -27-196.514 539.600 26 0 2 -28 216.888 433.466 26 0 -2 -28-113.828 437.919 26 0 2 -29-295.415 390.720 26 0 -2 -29 596.873 407.896 26 0 2 -30-208.975 276.000 26 0 -2 -30-36.6885 276.004 26 0 3 0 68.2880 162.012 29 0 -3 0 346.001 180.987 2 0 3 1 132927. 1154.45 29 0 -3 -1 134574. 1386.28 2 0 -3 -1 132791. 1222.01 1 0 3 -1 129825. 1476.14 29 0 -3 -1 127542. 1453.99 6 0 3 -2 20785.4 675.156 29 0 -3 -2 20240.2 571.416 3 0 3 2 21577.0 394.350 29 0 -3 -2 20292.4 619.046 6 0 -3 -2 20318.4 505.124 1 0 -3 -3 223941. 2100.95 6 0 -3 -3 219668. 1963.36 3 0 -3 -4 164495. 1817.39 3 0 -3 -4 165937. 1933.51 6 0 -3 -5 882490. 4575.84 3 0 3 5 881963. 3070.76 5 0 -3 -5 887202. 4754.13 6 0 -3 -6 109905. 1676.90 4 0 -3 -6 106511. 1775.92 3 0 3 -6 109800. 1967.49 29 0 3 6 104404. 914.480 5 0 -3 -6 109570. 1813.88 6 0 -3 -7 65348.8 1506.87 6 0 3 -7 65777.3 1615.59 29 0 -3 -7 67914.4 1433.53 4 0 -3 -7 65079.5 1484.27 3 0 3 -8 151444. 2514.97 29 0 -3 -8 144361. 2368.12 6 0 -3 -8 153163. 2297.47 4 0 3 -8 143895. 2654.06 6 0 -3 -9 344.216 299.255 4 0 3 -9 312.250 466.028 6 0 3 -9 104.144 361.154 29 0 3 -9 561.023 221.443 5 0 -3 -9 727.626 408.791 6 0 -3 -10 5839.22 608.908 4 0 3 -10 5642.05 398.747 5 0 -3 -10 5630.65 657.594 6 0 3 -10 5921.24 736.697 6 0 -3 -11 1637.49 422.120 4 0 -3 -11 2386.47 557.208 6 0 3 -11 2119.31 553.176 6 0 -3 -12 78152.2 2205.86 6 0 3 -12 80062.6 2393.71 6 0 -3 -13 1638.74 557.414 6 0 3 -13 1951.95 622.395 6 0 -3 -14 4310.85 726.045 6 0 3 -14 4482.92 776.919 6 0 -3 -15 441.156 452.994 6 0 3 -15 159.661 568.873 6 0 3 -16 803.703 592.125 6 0 -3 -16 1040.62 580.072 6 0 -3 -17 3727.76 818.848 6 0 3 -17 3960.55 823.015 6 0 3 -18 1470.08 682.477 13 0 3 -18 1831.05 609.547 17 0 3 -18 1408.01 727.584 6 0 -3 -18 1421.90 703.057 28 0 -3 -18 619.664 591.935 6 0 3 -18 1212.88 746.668 28 0 3 -18 2957.12 792.762 14 0 -3 -18 2827.83 716.811 26 0 -3 -19 26045.7 2004.85 28 0 3 -19 29981.0 1850.28 13 0 3 -19 28790.0 1993.79 28 0 3 -19 28616.8 1940.37 14 0 -3 -19 26280.6 1791.46 26 0 3 -19 27819.8 1866.32 26 0 3 -19 26186.5 1851.89 6 0 -3 -19 28802.5 1890.24 6 0 3 -19 26338.0 1919.65 17 0 3 -20 1593.84 718.467 28 0 3 -20 358.289 681.826 26 0 3 -20 2565.33 836.419 6 0 -3 -20 786.278 667.740 28 0 -3 -20 1920.10 804.009 26 0 -3 -20 2096.38 852.710 6 0 3 -20 552.607 632.151 13 0 3 -21 35270.1 2284.51 28 0 3 -21 38637.0 2116.22 13 0 -3 21 33627.2 2275.62 18 0 -3 -21 37513.9 2222.48 26 0 -3 -21 37696.8 2389.14 28 0 3 -21 33946.3 2089.84 26 0 3 -22 2435.32 820.449 28 0 3 -22 790.305 701.401 26 0 -3 -22 3323.64 851.671 28 0 3 -22 2501.83 747.554 13 0 -3 -22 3346.64 869.811 26 0 -3 -23 1660.65 727.761 26 0 3 -23 1627.58 829.920 28 0 3 -23 2003.53 830.653 26 0 -3 -23 1258.99 711.542 28 0 3 -23 1122.45 611.984 13 0 -3 -24-612.433 651.727 26 0 3 -24-254.302 582.083 28 0 -3 -24 400.989 655.437 28 0 3 -24 30.9856 667.753 26 0 -3 -25 722.514 630.102 26 0 3 -25 1055.84 681.313 26 0 3 -25 361.738 595.535 28 0 -3 -25 145.067 536.759 28 0 -3 -26 3142.05 798.907 26 0 3 -26 3675.80 838.131 26 0 3 -27 473.411 519.442 26 0 -3 -27 127.305 517.447 26 0 -3 -28 2754.81 620.065 26 0 3 -28 2484.42 630.247 26 0 -3 -29 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2264.42 11 0 -14 15 14468.3 1471.32 16 0 14 -15 12578.9 1301.01 12 0 14 -15 12132.0 1311.61 14 0 -14 15 16370.9 1443.32 11 0 -14 15 13163.0 1511.35 18 0 -14 -15 11956.8 1213.31 26 0 -14 -15 11720.5 1488.58 25 0 -14 16 12883.3 1567.74 18 0 14 -16 13843.7 1353.56 12 0 14 -16 11286.7 1306.90 14 0 -14 -16 13705.0 1532.18 25 0 -14 -16 14148.4 1316.38 26 0 -14 16 14062.4 1519.65 16 0 -14 -17 5567.20 927.590 26 0 14 -17 4672.61 913.056 14 0 -14 -17 5692.86 1109.97 25 0 14 -17 5266.85 920.236 12 0 -14 17 4722.90 936.235 16 0 -14 17 6196.00 1110.78 18 0 -14 -18 2680.91 678.242 26 0 14 -18 2378.10 728.420 12 0 -14 18 3795.47 898.951 18 0 -14 -18 2242.74 788.693 25 0 14 -18 2610.02 691.886 13 0 -14 18 3942.44 855.544 16 0 14 -18 2821.26 798.388 14 0 -14 -19 624.713 618.041 25 0 -14 19 1900.41 784.656 18 0 14 -19 1473.35 663.456 13 0 14 -19 682.422 610.983 14 0 14 -19 1951.69 616.162 12 0 -14 -19 1576.03 620.268 26 0 -14 20 4779.80 924.353 18 0 14 -20 3872.52 782.548 14 0 -14 -20 5698.44 823.108 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629.050 25 0 15 -17-331.419 574.493 14 0 -15 18 3075.81 824.145 16 0 15 -18 2068.47 661.391 12 0 15 -18 2276.65 663.823 14 0 -15 -18 2711.91 682.255 26 0 15 -18 2927.38 743.264 13 0 -15 18 1557.21 780.761 18 0 -15 -18 1991.27 793.754 25 0 -15 -19 3182.31 864.027 25 0 15 -19 1774.88 678.698 14 0 -15 -19 3073.30 710.834 26 0 15 -19 2560.75 738.464 13 0 15 -19 3015.33 728.583 12 0 -15 19 2450.34 706.374 18 0 -15 -20-324.943 490.922 26 0 -15 20 307.432 602.383 18 0 15 -20 81.7451 481.203 13 0 15 -20-455.686 498.066 14 0 -15 -20 601.891 572.500 25 0 15 -21 444.715 478.470 14 0 15 -21-1.81431 450.300 13 0 -15 21 133.321 531.250 18 0 15 -22 1281.88 497.118 26 0 -15 22 2436.26 659.222 18 0 15 -22 1834.08 486.476 13 0 -15 23 346.631 443.845 18 0 15 -23-697.330 371.111 13 0 15 -23-459.619 374.267 26 0 -15 24 591.787 341.442 18 0 -16 0-309.463 432.231 3 0 16 0-448.249 471.304 5 0 -16 0 427.582 687.738 16 0 -16 0 571.240 639.897 9 0 -16 0 1526.80 641.277 11 0 -16 -1 207.175 667.700 11 0 -16 -1 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613.165 16 1 20 -5 10.7318 587.501 20 -1 -20 -5 477.617 604.208 10 1 20 -4 1372.18 636.938 12 1 -20 4 1529.32 650.830 11 1 20 -4 898.252 719.700 20 1 20 -4 817.777 691.611 21 1 -20 4-48.7801 544.726 16 -1 -20 -4 561.902 632.027 10 1 -20 3 2493.19 771.518 16 -1 20 3 2588.31 862.198 22 1 20 -3 2443.63 846.923 21 1 20 -3 2532.31 721.230 12 1 -20 3 1788.59 736.659 11 -1 -20 -3 2019.08 772.865 10 1 20 -3 1125.70 733.285 20 1 -20 2 2518.59 820.655 16 -1 20 2 882.243 666.583 22 1 -20 2 1454.28 687.799 11 -1 -20 -2 2296.83 737.018 10 1 20 -2 1838.79 662.454 12 1 20 -2 2458.13 812.184 20 1 -20 1 2874.70 805.527 16 1 20 -1 2582.31 705.166 20 -1 -20 -1 3629.76 961.563 10 -1 20 1 3120.08 747.193 12 1 -20 1 3238.32 840.646 11 -1 20 1 5023.71 969.619 22 -1 20 0 295.001 650.974 22 1 20 0 510.931 599.561 20 -1 20 0 3549.72 750.215 12 -1 -20 0 2242.17 791.667 11 1 -20 0 2060.57 767.923 11 -1 -20 0 1824.87 764.709 10 -1 -20 1 2874.00 799.016 18 -1 20 -1 3605.51 919.952 22 -1 -20 1 1678.08 794.956 10 1 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832.094 11 1 -20 -6 2013.01 745.053 25 -1 -20 6 2881.28 786.275 18 -1 20 -6 2890.46 807.404 20 -1 -20 7-209.042 519.240 10 -1 20 -7-660.088 623.239 21 -1 20 -7-319.961 647.163 20 -1 20 -7-335.862 591.218 12 1 -20 -7 335.512 566.798 25 -1 20 -7 476.237 620.075 22 -1 -20 7 216.398 590.386 18 -1 -20 8 5508.49 984.031 18 -1 20 -8 4786.10 1029.15 21 1 -20 -8 5467.31 986.327 25 -1 20 -8 4719.71 908.212 12 -1 20 -8 5362.39 1020.87 22 -1 20 -8 4110.08 948.107 20 -1 -20 8 5067.24 1064.27 10 1 -20 -9 3224.32 869.946 25 -1 20 -9 3769.77 937.969 20 -1 -20 9 4294.84 881.380 18 -1 20 -9 4460.56 915.436 12 -1 -20 9 2030.14 731.339 10 -1 20 -9 4082.31 978.050 21 -1 -20 10 395.271 571.507 18 -1 20 -10-383.290 572.457 20 1 -20 -10-622.551 621.642 25 -1 -20 10 862.018 652.217 10 -1 20 -10 52.6638 565.352 21 -1 20 -10 162.273 522.375 12 1 -20 -11 1414.41 665.097 25 -1 -20 11 667.395 665.373 10 -1 20 -11 1106.63 609.346 12 -1 -20 11 1467.24 598.699 18 -1 20 -11 579.909 667.452 21 -1 20 -11 204.358 534.395 20 1 -20 -12 3716.02 846.782 25 -1 -20 12 4720.12 849.632 18 -1 20 -12 4445.85 914.819 21 -1 20 -12 5087.44 880.749 12 -1 20 -12 4248.56 846.650 20 -1 -20 12 4098.99 929.334 10 -1 20 -13 1517.35 643.700 12 1 -20 -13 862.549 603.465 25 -1 -20 13 680.500 519.661 18 -1 20 -13-353.265 516.418 14 -1 -20 13 588.916 497.891 10 1 -20 -14 1138.96 608.913 25 -1 20 -14 210.574 450.033 14 -1 20 -14 1571.20 592.291 12 -1 -20 14 999.406 530.630 18 -1 20 -15 59.6718 420.794 14 -1 20 -15 183.513 410.497 12 1 -20 -15 194.304 452.454 25 -1 -20 15 246.205 445.845 18 -1 -20 16 890.896 507.689 18 -1 20 -16 384.156 317.845 23 -1 20 -16 736.165 454.687 14 -1 20 -16 698.619 438.170 13 -1 20 -16 861.965 442.633 12 1 -20 -16 295.731 482.319 25 -1 20 -17-39.0934 334.551 14 -1 20 -17-347.445 150.600 23 1 -20 -17-35.7946 468.003 25 -1 20 -17-283.662 386.093 12 -1 -20 17 736.300 490.686 18 -1 20 -17-108.802 334.891 13 -1 20 -18 1076.62 373.772 13 -1 20 -18 56.7802 280.062 14 -1 -20 18 924.476 394.961 18 -1 -20 19 697.974 325.813 18 1 -21 17 1253.61 367.224 18 1 21 -17 764.707 366.102 13 1 -21 16 240.008 347.447 18 1 21 -16 762.448 330.697 23 1 21 -16-171.722 378.377 13 1 21 -15 5467.37 632.036 23 1 -21 15 4561.78 629.161 18 1 21 -15 4153.21 656.284 13 1 21 -14 2382.41 544.766 23 1 -21 14 2494.84 563.610 18 1 -21 14 2561.79 546.313 10 1 -21 13 1773.88 595.806 10 1 21 -13 1917.31 618.310 12 1 -21 13 1559.61 546.490 18 1 21 -13 2223.27 532.945 23 1 -21 12 1369.73 523.246 18 1 -21 12-362.457 467.367 10 1 21 -12 780.735 504.598 12 1 -21 12 519.030 511.736 11 1 -21 11 200.176 504.363 10 1 -21 11 661.156 543.331 18 1 21 -11 1188.95 588.020 12 1 -21 11 1055.26 629.101 11 1 -21 10 2093.66 641.665 18 1 21 -10 2438.89 848.232 21 1 -21 10 3405.60 744.934 16 1 21 -10 2362.80 660.586 12 1 -21 10 2429.54 707.038 11 1 21 -9 1187.91 596.537 12 1 21 -9 213.853 523.367 21 1 -21 9 2114.65 635.469 18 1 -21 9 108.261 522.654 11 1 -21 9 422.009 595.474 16 1 21 -8 250.038 605.196 21 1 -21 8 1467.37 623.397 18 1 21 -8 317.863 483.855 12 1 -21 8 268.188 539.198 16 1 -21 8 237.100 573.475 11 1 21 -7 139.789 640.714 21 1 21 -7 443.936 610.936 20 -1 -21 -7-580.316 473.996 10 1 21 -7 1197.03 614.762 12 1 -21 7 414.698 568.702 11 1 -21 7 968.330 558.096 16 1 21 -6 618.046 636.635 21 1 21 -6 418.173 565.755 20 -1 -21 -6 544.110 536.230 10 1 21 -6 49.3332 448.212 12 1 -21 6-298.980 562.860 11 1 -21 6 373.583 532.428 16 1 -21 5 1549.57 687.342 16 1 21 -5 1660.10 775.128 21 1 21 -5 1990.67 604.161 12 -1 -21 -5 694.908 634.691 10 1 -21 5 1719.26 679.791 11 1 21 -5 2023.12 866.671 20 1 21 -4 1386.09 637.927 12 1 -21 4 852.805 662.459 11 1 21 -4 1210.74 702.308 21 1 -21 4 891.622 632.088 16 1 21 -4 1008.28 646.149 20 -1 -21 -4 1833.46 715.278 10 1 21 -3 723.545 546.340 20 1 21 -3 1800.51 638.171 12 1 -21 3 2248.13 779.968 11 -1 -21 -3 1311.92 674.716 10 1 21 -3 1046.28 728.869 21 1 21 -2 3085.69 737.132 12 1 21 -2 3507.60 854.291 20 -1 21 2 3079.41 807.119 22 1 -21 2 1628.77 709.329 11 1 21 -2 2760.88 947.741 21 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12 -1 -21 5 2114.29 750.327 10 -1 21 -5 2233.91 871.988 21 -1 -21 5 1326.88 665.422 18 -1 21 -5 2875.77 812.292 22 1 -21 -5 447.335 616.014 10 -1 21 -5 1887.46 825.739 20 -1 21 -6-177.653 512.271 22 -1 -21 6 43.5422 595.762 10 -1 21 -6-71.1388 516.488 21 -1 21 -6-825.233 655.224 20 -1 -21 6-454.135 572.466 18 -1 21 -6-464.601 596.081 12 1 -21 -6-148.037 524.593 10 -1 -21 7 1352.11 611.631 18 1 -21 -7 1440.16 600.002 25 -1 21 -7 973.867 656.564 21 -1 21 -7 1233.88 742.747 22 -1 21 -7 978.627 672.162 20 -1 -21 7 956.776 643.558 10 -1 21 -7 1254.95 625.553 12 1 -21 -8-77.2150 514.375 25 -1 -21 8 683.293 603.287 18 -1 21 -8 215.453 610.128 20 -1 21 -8 75.2741 545.363 12 -1 -21 8-229.426 625.865 10 -1 21 -8 811.236 592.044 21 -1 -21 9 156.475 609.925 10 -1 21 -9 778.080 628.130 20 -1 21 -9 1200.08 620.846 12 -1 -21 9 1170.16 649.925 18 1 -21 -9-570.637 572.476 25 -1 21 -9 202.553 589.109 21 1 -21 -10 2417.12 666.747 25 -1 -21 10 2745.29 747.603 10 -1 21 -10 2724.28 766.675 20 -1 21 -10 1946.30 801.192 21 -1 -21 10 2308.39 655.528 18 -1 21 -10 1827.65 631.757 12 -1 21 -11 1087.17 593.978 21 -1 21 -11 600.330 561.868 12 -1 -21 11 1661.83 612.362 18 -1 21 -11 981.793 582.286 20 -1 -21 11 143.255 474.863 10 1 -21 -11 422.930 616.218 25 -1 21 -12-755.137 509.211 14 1 -21 -12-355.052 502.106 25 -1 21 -12 272.370 466.927 12 -1 -21 12 773.999 544.956 18 -1 -21 12 1124.04 582.586 10 -1 21 -13 2906.18 645.027 12 -1 -21 13 1821.24 523.371 10 -1 -21 13 2434.14 649.231 18 1 -21 -13 2836.96 683.137 25 1 -21 -14 1889.92 643.042 25 -1 -21 14 1839.42 552.430 18 -1 21 -14 2417.30 593.758 12 -1 21 -14 378.831 472.666 14 -1 21 -15 5785.95 703.466 12 -1 -21 15 4675.81 684.545 18 1 -21 -15 4639.59 764.063 25 -1 21 -16 470.026 379.013 13 -1 21 -16 165.845 371.528 12 -1 21 -16 395.730 301.815 23 -1 -21 16 126.462 371.754 18 -1 21 -16-557.742 361.048 14 -1 -21 17 980.689 369.688 18 -1 -21 18 43.1034 253.416 18 1 22 -16-204.918 300.340 13 1 22 -15-74.7827 277.660 23 1 22 -15 382.583 356.947 13 1 22 -14 1183.39 409.719 23 1 -22 14 1342.86 395.851 18 1 22 -14 1180.49 482.316 13 1 -22 13 568.523 443.220 18 1 22 -13 1454.28 445.716 23 1 -22 13 916.229 453.029 10 1 -22 12 3083.84 532.380 18 1 -22 12 1707.65 619.393 10 1 22 -12 3227.93 651.007 12 1 22 -12 3289.33 608.824 23 1 -22 11 3059.15 675.354 10 1 -22 11 1896.43 417.484 18 1 22 -11 3715.75 679.222 12 1 -22 10 794.750 344.846 18 1 22 -10 1474.46 523.963 12 1 -22 10 2178.78 613.974 10 1 -22 10 1894.15 587.171 11 1 -22 9 680.343 596.660 10 1 22 -9 613.954 543.129 21 1 22 -9-146.424 449.325 12 1 -22 9 443.853 583.604 11 1 22 -8 1360.49 641.764 21 1 -22 8 1414.47 591.975 11 1 22 -8 813.958 489.138 12 1 -22 8 1019.69 595.443 10 1 22 -7 2592.53 796.653 21 1 22 -7 3101.39 693.062 12 1 -22 7 2219.71 668.896 11 1 -22 6 2124.09 709.755 11 1 22 -6 2381.66 787.318 21 1 22 -6 3089.79 708.593 20 -1 -22 -6 3195.40 727.461 10 1 22 -6 3259.66 716.487 12 1 22 -5 551.127 650.619 21 1 22 -5 1083.47 687.329 20 -1 -22 -5 491.023 564.960 10 1 22 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25 2 13 -8 26901.2 1780.56 29 2 13 -8 26136.2 1781.10 12 2 13 -8 25799.3 2062.97 21 2 -13 8 24259.6 1790.92 9 2 -13 8 26708.9 1897.28 2 -2 13 7 2592.71 584.415 5 2 13 -7 2960.87 748.135 29 2 -13 7 3563.45 828.458 2 -2 13 6 4003.61 677.909 5 2 -13 6 3447.99 865.938 2 2 13 -6 3743.57 761.894 29 2 -13 5 29386.1 1864.45 2 -2 13 5 27471.0 1663.08 5 2 13 -5 27378.0 1695.53 29 2 -13 4 9792.70 1137.06 2 -2 13 4 10040.0 1065.32 5 2 13 -4 11620.4 1133.73 29 2 -13 4 9101.52 1060.59 1 -2 13 3 12705.3 1134.18 5 2 -13 3 12226.1 1218.85 2 2 13 -3 13693.2 1158.39 29 2 -13 3 14124.0 1259.67 1 -2 13 2 6571.27 899.394 5 2 -13 2 8047.73 1049.02 2 2 -13 2 8410.56 1000.05 1 2 13 -2 8778.77 985.836 29 2 -13 1 8199.07 966.715 1 -2 13 1 8632.68 1036.92 5 2 13 -1 10864.6 1030.18 29 -2 13 0-517.652 439.099 5 2 -13 0 631.420 480.988 1 2 -13 0 19.0753 559.759 3 2 13 0-82.0883 383.665 29 2 13 1 10728.0 1026.33 29 2 -13 -1 9159.59 1035.51 3 2 -13 -1 8446.28 951.939 1 -2 13 -1 8769.06 990.467 5 -2 13 -2 7260.91 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3362.52 768.941 13 2 -14 20 2631.03 747.049 18 2 -14 20 4066.61 748.420 16 2 14 -19 2097.14 689.692 13 2 -14 19 507.659 632.137 18 2 14 -19 250.525 369.844 23 2 -14 19 1514.24 646.881 16 2 14 -18 709.189 542.366 14 2 -14 18 2117.98 698.310 16 2 14 -18 1352.87 525.936 23 2 14 -18 1598.79 703.714 13 2 -14 18 1513.96 662.734 18 2 -14 17-43.2992 672.720 16 2 14 -17-250.872 563.001 14 2 14 -17 1332.12 475.210 23 2 14 -17 615.215 622.273 13 2 -14 17 605.939 682.301 18 2 -14 16 573.861 612.282 16 2 14 -16 885.482 474.172 23 2 14 -16 850.381 588.293 14 2 14 -16 418.645 544.713 12 2 -14 16 707.614 643.283 18 -2 -14 -16-42.7048 513.653 25 2 14 -15 1061.34 626.146 14 2 -14 15 1333.02 746.836 16 2 14 -15 1629.06 607.753 23 2 -14 15 1813.95 835.770 18 2 -14 15 1722.15 802.999 11 -2 -14 -15 907.664 778.168 25 2 14 -15 2161.44 768.947 12 2 -14 14 7286.98 1209.32 16 -2 -14 -14 9070.54 1358.79 25 2 14 -14 11781.8 1234.33 14 2 14 -14 8651.27 1211.24 12 2 -14 14 7288.37 1170.86 18 2 -14 14 7297.24 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4418.48 956.111 20 2 14 -9 4360.94 825.620 12 2 -14 9 3312.73 877.957 2 2 -14 9 3723.97 938.668 18 -2 -14 -9 3272.72 979.691 25 2 -14 9 2916.30 849.265 9 -2 -14 -8 4142.68 999.156 25 2 14 -8 2004.53 711.267 29 2 -14 8 2909.36 815.121 18 2 14 -8 3201.43 886.695 20 2 14 -8 2967.57 901.951 21 2 -14 8 2825.24 919.017 9 2 -14 8 2592.92 783.974 2 2 14 -8 2396.17 780.855 12 2 -14 8 3282.57 883.394 16 -2 -14 -7 25623.6 2084.18 25 2 -14 7 25219.4 1843.01 2 -2 14 7 26343.0 1684.34 5 2 14 -7 27228.4 1796.98 29 2 -14 7 27466.8 1890.93 9 2 14 -7 30605.6 2080.02 20 2 14 -7 27241.7 1824.62 12 2 -14 7 22761.2 1747.28 16 2 14 -7 25744.1 2022.83 21 2 14 -6 19306.0 1555.49 29 -2 -14 -6 23746.3 1921.68 25 2 -14 6 18470.2 1558.12 2 2 -14 6 17594.1 1579.25 16 2 14 -6 18732.0 1729.44 21 2 14 -6 17901.1 1492.89 12 -2 14 6 19168.8 1465.17 5 2 -14 6 19084.3 1600.09 9 -2 14 5 27996.2 1734.20 5 2 -14 5 26878.4 1885.62 2 2 -14 5 25861.0 1796.69 9 2 14 -5 30717.7 1831.16 29 2 -14 5 27866.5 1789.65 1 2 14 -4 1939.72 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2357.02 703.640 17 -2 14 -20 3114.45 713.254 14 2 -14 -20 2807.85 742.074 26 -2 -14 21 1498.26 656.232 18 2 -14 -21 343.262 503.450 25 2 -14 -21 459.200 527.887 26 -2 14 -21 904.357 497.309 14 2 -14 -22 1098.82 508.825 25 -2 14 -22 775.243 502.267 14 -2 -14 22 457.906 478.307 18 2 -14 -22 1033.29 526.222 26 -2 -14 23 273.694 368.887 18 -2 14 -23 509.678 477.196 26 -2 14 -24 1076.07 415.521 26 2 -15 24 500.537 326.915 18 2 15 -23-178.194 371.063 13 2 -15 23 564.559 388.281 18 2 15 -22 120.326 418.172 13 2 -15 22 974.146 534.883 18 2 15 -21 65.8827 445.560 13 2 -15 21-598.466 512.606 18 2 -15 20 6387.20 966.539 18 2 15 -20 6833.98 894.421 13 2 -15 20 6321.69 894.979 16 2 15 -19 586.728 327.584 23 2 15 -19 855.388 569.806 13 2 -15 19 707.314 550.709 18 2 -15 19 1027.96 649.938 16 2 15 -18 518.284 464.840 23 2 -15 18 142.755 575.563 16 2 15 -18 15.0876 466.098 13 2 -15 18 956.557 651.628 18 2 15 -17 254.025 359.934 23 2 15 -17-386.926 496.760 14 2 15 -17 160.674 568.040 13 2 -15 17-268.949 549.249 18 2 -15 17 686.647 641.017 16 2 15 -16 564.361 541.969 14 2 -15 16 2500.79 793.306 16 2 15 -16 1842.73 588.513 23 2 -15 16 2013.13 747.197 18 2 -15 15 346.112 581.439 11 -2 -15 -15 507.402 695.744 25 2 15 -15-1318.40 533.334 23 2 15 -15 228.424 460.809 12 2 -15 15 680.678 646.437 16 2 -15 15-834.106 626.359 18 -2 -15 -14 7650.16 1204.86 25 2 -15 14 7651.09 1187.95 16 2 -15 14 7563.91 1154.45 11 2 15 -14 7016.17 1070.04 12 2 -15 14 7415.51 1206.94 18 -2 -15 -13 6231.13 1215.82 25 2 15 -13 7057.74 1092.81 12 2 -15 13 8357.99 1162.18 11 2 -15 13 5972.58 1177.76 18 2 -15 13 5804.41 1052.38 16 -2 -15 -12 1026.10 722.535 25 2 -15 12 208.597 686.691 16 2 15 -12 1100.29 639.435 12 2 -15 12 1352.70 770.314 18 2 -15 11 6223.16 1068.17 16 2 -15 11 6304.54 1145.21 9 2 15 -11 5861.24 1219.69 21 2 15 -11 5911.04 990.130 12 2 -15 11 6502.78 1090.16 18 -2 -15 -11 6023.33 1206.95 25 2 -15 10 9130.68 1317.34 9 2 -15 10 9118.60 1250.66 16 2 15 -10 10364.7 1236.56 29 2 15 -10 8876.20 1387.24 21 2 15 -10 8104.65 1155.33 12 2 -15 10 9785.03 1271.38 2 2 -15 10 9222.91 1161.34 18 2 15 -10 9863.44 1264.66 5 -2 -15 -10 9543.83 1404.88 25 -2 -15 -9 9345.42 1484.47 25 2 -15 9 9087.60 1229.56 16 2 15 -9 9897.72 1331.02 20 2 15 -9 9352.14 1370.49 21 2 15 -9 9675.05 1176.71 12 2 -15 9 10932.5 1350.17 18 2 -15 9 8189.38 1191.38 2 2 15 -9 10091.5 1207.38 29 2 -15 9 8245.92 1240.42 9 -2 -15 -8 5192.64 1210.61 25 2 15 -8 4356.27 997.607 20 2 15 -8 4897.59 946.568 12 2 -15 8 2401.92 786.158 2 2 -15 8 1666.21 810.723 16 2 15 -8 5458.25 1189.01 21 2 15 -8 3618.88 896.688 29 2 -15 8 5564.81 1042.06 18 2 -15 8 3338.43 942.615 9 -2 -15 -7 14270.4 1500.72 10 -2 -15 -7 13638.9 1608.30 25 2 -15 7 10314.7 1332.81 16 2 15 -7 10287.4 1425.25 21 2 15 -7 12167.5 1447.23 20 2 -15 7 12979.4 1500.68 2 2 15 -7 10160.6 1210.34 12 2 -15 7 14523.5 1454.44 18 2 15 -7 11930.1 1258.49 29 2 -15 7 11248.3 1279.88 1 2 -15 7 10153.3 1282.06 9 -2 -15 -6 19142.7 1779.27 25 2 -15 6 16476.3 1538.40 16 -2 15 6 18387.3 1486.16 5 -2 -15 -6 21205.5 1829.66 10 2 15 -6 19751.3 1797.63 20 2 15 -6 17868.8 1512.46 12 2 15 -6 20016.4 1594.37 29 2 -15 6 17906.2 1585.76 2 2 15 -6 18224.0 1732.73 21 2 -15 6 18083.4 1595.99 9 2 -15 6 19486.9 1582.57 1 2 -15 5 3225.73 792.780 16 -2 -15 -5 3491.57 878.151 25 2 -15 5 2978.10 858.416 9 -2 15 5 3552.16 724.632 5 2 15 -5 2659.04 922.258 21 -2 -15 -5 3444.49 799.613 18 2 15 -5 3239.48 764.210 12 2 -15 5 3082.01 869.294 2 2 -15 5 4188.26 866.015 1 -2 -15 -5 2660.93 866.545 10 2 15 -5 3229.28 847.450 29 2 15 -5 4290.42 1032.57 20 2 -15 4 1232.24 608.474 1 2 -15 4 1911.03 655.480 16 2 15 -4 3919.55 891.424 20 -2 -15 -4 1322.70 646.364 18 2 15 -4 2207.73 781.863 12 -2 -15 -4 73.0244 720.583 25 -2 15 4 703.562 488.067 5 -2 -15 -4 1619.10 772.560 10 2 -15 4 1285.34 626.369 2 2 15 -4 1688.67 642.077 29 2 -15 4 2531.33 789.273 9 2 15 -4 373.417 711.827 21 2 -15 3 3539.26 820.369 9 2 -15 3 1875.25 724.160 16 2 -15 3 2223.45 674.641 1 2 15 -3 3177.57 760.650 29 -2 15 3 1828.46 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1735.84 760.651 19 2 -15 -3 3439.47 791.011 9 -2 15 -3 2742.53 661.380 5 2 -15 -3 1630.58 606.549 3 -2 15 -3 1783.12 767.549 19 -2 -15 3 2304.79 777.028 18 -2 -15 3 3651.66 889.776 11 2 -15 -4 3324.96 875.145 9 -2 15 -4-226.317 668.412 22 2 -15 -4 2189.67 830.948 3 -2 15 -4 2026.78 831.676 19 -2 -15 4 1202.77 699.369 18 -2 -15 4 2017.69 721.186 11 -2 15 -4 2164.70 674.747 5 -2 -15 4 766.914 669.539 10 2 -15 -4-1775.33 726.289 25 2 -15 -5 2898.78 839.518 25 -2 -15 5 3112.93 922.375 10 -2 15 -5 5384.37 1039.43 22 -2 15 -5 3477.96 918.991 19 2 -15 -5 2102.31 688.108 3 -2 -15 5 4063.56 905.973 18 -2 -15 5 2963.17 874.705 11 -2 15 -5 3601.67 823.485 5 2 -15 -6 19051.1 1505.70 3 2 -15 -6 17096.1 1626.95 25 -2 15 -6 19504.1 1549.21 5 -2 15 -6 17654.7 1737.92 19 -2 15 -6 17671.8 1723.62 22 -2 -15 6 20421.0 1720.94 18 -2 -15 6 20689.2 1765.39 11 -2 -15 6 18837.3 1770.79 10 2 -15 -7 12624.1 1307.31 3 2 -15 -7 12666.4 1492.46 25 -2 -15 7 10671.1 1479.86 10 -2 15 -7 9837.93 1409.88 22 -2 15 -7 11419.5 1515.51 19 -2 -15 7 12423.7 1421.33 18 -2 -15 7 13243.5 1496.70 11 -2 15 -7 13672.5 1288.80 5 2 -15 -8 4080.31 996.434 25 -2 -15 8 4000.46 1080.18 10 -2 15 -8 4032.04 1092.55 19 2 -15 -8 3475.20 765.257 3 -2 -15 8 4669.02 1038.39 18 -2 -15 8 3986.30 1006.95 11 -2 15 -8 3835.61 832.102 5 -2 15 -8 5046.11 1091.85 22 -2 -15 9 9773.76 1348.59 18 -2 15 -9 10116.5 1213.80 5 -2 -15 9 7432.95 1231.34 10 -2 15 -9 8265.47 1304.85 21 -2 15 -9 9408.62 1283.04 20 2 -15 -9 8526.22 1103.05 3 2 -15 -9 8341.38 1304.33 25 -2 15 -9 8991.15 1399.84 22 -2 -15 10 8795.33 1434.08 10 -2 15 -10 10462.6 1390.82 20 -2 15 -10 9265.00 1364.40 22 -2 15 -10 9926.22 1190.53 5 -2 15 -10 6750.52 1286.73 21 -2 -15 10 8530.35 1338.30 18 2 -15 -10 9523.03 1127.93 3 2 -15 -10 7506.15 1244.63 25 2 -15 -11 3896.31 992.849 25 -2 15 -11 6313.12 1132.86 22 2 -15 -11 4973.65 936.387 26 -2 -15 11 5813.86 1134.82 18 -2 -15 11 7302.58 1252.39 10 -2 15 -11 5289.85 1074.41 20 -2 15 -11 4311.44 1002.70 21 2 -15 -12 433.370 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9753.24 1284.04 20 -2 19 -11 10531.7 1210.76 12 -2 -19 11 11220.5 1273.00 18 2 -19 -11 10977.0 1344.06 25 -2 -19 11 9823.74 1282.91 10 -2 -19 12 1060.75 635.910 10 2 -19 -12 1228.37 622.730 25 -2 19 -12 1356.42 655.877 12 -2 19 -12 852.351 572.237 20 -2 -19 12 1956.05 698.690 18 -2 19 -12 1541.34 696.788 21 2 -19 -13 1106.44 643.297 25 -2 19 -13 987.289 628.821 21 -2 19 -13 163.898 521.172 20 -2 19 -13 328.769 525.180 12 -2 -19 13 641.525 618.530 18 -2 -19 13 949.561 566.944 10 2 -19 -14 26.4252 544.610 25 -2 -19 14 295.811 553.456 18 -2 19 -14 95.9421 411.934 12 2 -19 -15 2026.30 686.048 25 -2 19 -15 1473.64 563.522 14 -2 -19 15 1950.78 678.645 18 -2 19 -15 1457.12 539.079 12 -2 -19 16 483.815 491.048 18 -2 19 -16 205.161 433.674 14 -2 19 -16 657.440 408.649 13 2 -19 -16 154.340 468.660 25 -2 19 -16 1367.42 513.210 12 2 -19 -17 1735.30 631.742 25 -2 19 -17 894.739 495.658 14 -2 19 -17 1903.95 478.601 12 -2 -19 17 1952.78 589.805 18 -2 19 -17 116.206 215.863 13 2 -19 -18 1805.77 606.825 25 -2 19 -18 2802.03 461.726 12 -2 -19 18 2312.07 568.399 18 2 -19 -19-537.061 425.062 25 -2 -19 19 263.231 330.821 18 -2 19 -19-110.077 334.225 14 -2 -19 20 309.665 309.149 18 2 20 -18 1577.65 421.209 13 2 -20 18 1163.63 322.589 18 2 20 -17 836.855 436.925 13 2 -20 17 154.182 328.105 18 2 20 -17 759.180 329.722 23 2 20 -16-51.2707 307.273 23 2 20 -16 597.458 451.319 13 2 -20 16 705.396 397.101 18 2 -20 15 1326.80 450.828 18 2 20 -15 1222.41 525.280 13 2 20 -15 1131.13 392.022 23 2 -20 15 860.759 498.612 16 2 -20 14 618.086 494.233 10 2 20 -14 385.989 398.071 23 2 -20 14 1190.59 506.034 18 2 20 -14 1046.41 514.980 13 2 -20 14 1089.64 532.381 11 2 -20 14 865.575 499.695 16 2 20 -13 287.126 400.206 23 2 -20 13 543.609 519.219 16 2 -20 13 359.160 436.007 18 2 -20 13 1471.20 569.323 11 2 20 -12 1385.72 539.860 23 2 20 -12 2217.86 703.133 12 2 -20 12 2011.06 627.001 18 2 -20 12 1812.53 667.706 11 2 -20 12 2373.97 691.234 16 2 20 -11-583.225 565.749 12 2 -20 11 760.843 509.212 18 2 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629.241 9 2 -20 4-1030.93 618.593 16 2 -20 3 657.850 652.813 9 2 20 -3 11.5649 636.422 21 2 20 -3 841.443 557.680 12 2 -20 3 937.649 631.829 11 -2 -20 -3-97.0765 578.556 10 2 -20 3 415.394 562.013 16 2 20 -2 859.793 714.802 21 -2 -20 -2 1215.12 534.449 18 2 -20 2 2168.59 756.424 11 2 -20 2 1741.42 713.954 9 -2 -20 -2 1730.11 802.260 10 2 -20 2 1990.92 731.221 16 2 20 -1 775.303 711.043 21 2 -20 1 1923.62 728.070 9 -2 -20 -1 756.437 589.997 18 2 -20 1 1602.53 743.569 11 -2 -20 -1 1569.54 625.596 10 2 -20 1 1610.05 640.759 16 -2 20 1 1515.25 708.523 22 -2 20 0 6072.44 1047.36 22 2 20 0 4641.28 1012.22 21 -2 -20 0 6283.05 962.303 18 2 -20 0 3881.73 904.354 11 -2 -20 0 5064.65 998.679 10 2 -20 0 5530.25 1013.25 9 -2 20 -1 1270.19 755.556 22 2 20 1 1168.49 746.263 21 -2 -20 1 1407.34 685.760 18 2 -20 -1 1208.51 687.106 11 -2 -20 1 1844.86 696.711 10 2 -20 -1 982.600 602.737 9 -2 20 -2 2710.12 1251.28 19 -2 20 -2 666.158 643.209 22 2 20 2 2399.81 826.718 21 2 -20 -2 2009.22 774.026 9 -2 -20 2 585.840 595.287 18 2 -20 -2 2211.12 725.281 11 -2 -20 2 1278.31 730.793 10 -2 20 -3 1558.59 793.391 19 -2 -20 3-44.3746 578.318 18 2 -20 -3 875.858 503.529 11 -2 -20 3 421.824 600.582 10 2 -20 -3 787.131 684.649 9 -2 20 -3 93.7076 641.378 22 -2 20 -4-320.871 630.372 20 -2 -20 4 190.136 554.698 18 2 -20 -4 2342.87 703.926 11 -2 -20 4 984.678 732.981 10 2 -20 -4 465.750 509.112 9 -2 20 -4 534.832 641.826 22 2 -20 -5 4438.70 881.727 9 -2 20 -5 5742.31 1121.72 22 -2 -20 5 4978.01 940.048 18 -2 20 -5 5311.11 1029.33 20 -2 -20 5 4483.94 1051.13 10 2 -20 -6 1521.70 644.975 25 -2 20 -6 1438.71 704.130 22 -2 20 -6-344.352 674.250 21 -2 -20 6 499.420 556.012 18 -2 20 -6 1827.72 643.017 12 -2 -20 6 1351.67 775.022 10 -2 20 -6 1194.80 630.054 20 -2 20 -7-214.926 569.519 20 2 -20 -7-343.229 572.519 25 -2 20 -7-993.896 736.558 21 -2 -20 7-278.386 573.286 18 -2 20 -7 265.013 652.870 22 -2 20 -7 964.972 609.684 12 -2 -20 7 517.471 589.519 10 -2 20 -8 6065.84 1097.16 22 -2 20 -8 6649.74 1106.99 21 -2 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554.071 22 -2 22 4 237.833 418.937 22 2 22 -4 52.1538 574.843 21 2 -22 4 1401.96 626.008 11 -2 22 3 5615.87 1003.19 22 2 22 -3 6229.36 986.284 21 2 -22 3 4518.26 851.646 11 -2 -22 -3 6190.29 951.978 10 -2 22 2 1740.21 747.154 22 2 22 -2 1005.40 674.126 21 2 -22 2 552.243 591.443 11 -2 -22 -2 1641.84 735.388 10 -2 22 1 5390.08 1049.85 22 2 22 -1 6187.90 1041.95 21 -2 22 1 5269.46 778.824 12 2 -22 1 4338.40 855.094 11 -2 -22 -1 4748.79 901.463 10 2 22 0 525.662 394.561 23 2 22 0-60.0528 577.197 21 -2 -22 0 156.614 509.300 18 -2 22 0 1352.55 559.545 12 2 -22 0 482.325 566.418 11 -2 -22 0 424.424 662.214 10 -2 22 -1 4990.89 956.551 20 -2 22 -1 3679.24 934.756 22 2 22 1 5436.02 962.701 21 -2 -22 1 5449.35 826.723 18 -2 22 -1 4884.70 862.320 12 2 -22 -1 4802.53 841.506 11 -2 -22 1 4438.33 885.482 10 -2 22 -2-311.615 649.325 22 2 22 2 759.895 609.148 21 -2 22 -2 1582.38 711.172 20 -2 -22 2 1686.22 557.758 18 -2 22 -2 1660.26 611.411 12 2 -22 -2 583.364 522.649 11 -2 -22 2 1703.00 772.351 10 2 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2333.61 29 3 -10 -1 41868.9 1855.95 3 3 -10 -1 45947.0 1925.34 1 3 10 1 44700.2 1820.78 29 -3 10 -2 8665.75 945.821 5 3 -10 -2 9853.39 1013.10 1 3 10 2 8475.22 860.180 29 3 -10 -2 7218.46 913.542 3 3 -10 -3 32341.3 1672.86 3 3 10 3 36494.1 1611.17 29 -3 10 -3 33498.4 1732.60 5 3 10 4 19765.9 1194.49 29 -3 10 -4 18204.7 1312.57 5 3 -10 -4 18456.3 1272.02 3 -3 10 -5 30384.8 1713.30 5 3 -10 -5 27988.0 1542.78 3 3 10 5 30189.8 1429.99 29 -3 10 -6 16503.6 1279.60 5 3 -10 -6 14761.1 1193.12 3 3 -10 -7 63459.9 2400.86 3 -3 10 -7 69496.9 2530.85 5 3 -10 -8 19511.6 1403.05 3 -3 10 -8 19749.7 1402.33 5 -3 10 -9 39952.0 1967.64 5 3 -10 -9 37050.9 1898.19 3 -3 10 -10 3488.79 754.200 5 3 -10 -10 4493.45 775.990 3 3 -10 -11 5443.78 1055.98 25 -3 10 -11 4857.76 951.305 6 -3 10 -11 5347.05 1085.59 22 -3 10 -11 5623.91 825.642 5 -3 10 -11 5617.39 1081.23 19 -3 -10 11 4761.88 1017.67 18 3 -10 -11 5736.69 865.237 3 -3 10 -11 4041.34 949.822 17 3 -10 -11 3968.45 857.112 26 -3 10 -12 13364.0 1392.68 24 3 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14 -3 -10 17 6667.21 1205.88 18 -3 10 -17 3691.91 804.689 17 3 -10 -17 3409.24 853.852 26 3 -10 -18 4180.99 1017.29 25 -3 10 -18 2689.48 787.447 14 -3 -10 18 3383.66 933.482 18 -3 10 -18 5031.29 987.704 17 3 -10 -18 4984.57 980.394 26 3 -10 -19 1966.73 709.255 26 3 -10 -19 1517.73 701.965 25 -3 10 -19 2763.48 793.770 14 -3 10 -19 1400.40 625.950 17 3 -10 -20 2247.51 809.704 25 -3 10 -20 1764.03 701.456 14 -3 -10 20 2245.30 764.554 18 -3 10 -20 2805.18 809.805 17 3 -10 -20 2924.33 823.255 26 3 -10 -21-2.52558 646.806 26 -3 10 -21 55.7772 476.400 14 3 -10 -21-284.077 574.181 25 -3 10 -21-432.378 534.953 17 -3 10 -22 3947.66 770.173 14 -3 10 -22 4192.64 821.817 17 3 -10 -22 4301.64 800.217 25 3 -10 -22 4998.31 874.933 26 -3 10 -23 609.474 550.866 26 -3 10 -23-458.741 478.743 14 -3 10 -23 496.107 520.592 17 3 -10 -23 410.626 559.532 26 3 -10 -24-213.336 515.060 26 -3 10 -24 25.1624 447.078 26 3 -10 -24 381.229 466.566 27 -3 10 -25 348.889 442.467 26 3 -10 -25 663.394 448.581 27 3 -10 -25 691.334 460.286 26 -3 10 -26 877.784 349.881 26 3 -10 -26 1097.77 377.255 27 3 -10 -26 271.137 389.309 26 3 11 -26 6.12578 268.176 13 3 -11 26 92.1746 328.149 18 3 11 -25 5093.44 624.303 13 3 -11 25 3938.43 671.490 18 3 11 -24 1272.96 482.591 13 3 -11 24-89.2150 477.284 18 3 11 -23 408.215 447.153 13 3 -11 23-174.426 525.263 18 3 11 -22 1752.46 620.559 13 3 -11 22 1262.01 656.078 18 3 11 -21 696.673 570.137 13 3 -11 21 711.959 637.264 18 3 11 -20 897.569 594.586 13 3 -11 20-170.029 588.015 18 3 -11 20 1101.31 616.712 16 3 11 -19 2087.96 541.354 23 3 11 -19 2140.59 769.255 13 3 -11 19 2560.29 807.842 18 3 -11 19 2808.25 785.802 16 3 -11 18 3184.30 814.019 16 3 11 -18 2618.09 609.321 23 3 11 -18 2048.21 752.079 13 3 -11 18 862.510 665.318 18 -3 -11 -18 2692.80 817.273 15 3 11 -17 2204.36 747.008 13 3 -11 17 5168.33 962.630 16 3 -11 17 3078.52 928.413 18 3 11 -17 5154.05 829.607 23 -3 -11 -17 3668.30 930.244 15 3 -11 16 5872.17 1009.03 16 3 11 -16 8471.53 1037.08 23 3 11 -16 7634.51 1093.64 13 3 -11 16 4560.24 1009.94 18 -3 -11 -16 6364.59 1172.23 15 3 11 -15 15972.7 1385.65 23 3 11 -15 13756.6 1429.60 13 -3 -11 -15 13924.5 1520.87 15 -3 -11 -14 9641.02 1385.45 15 3 -11 14 10497.6 1435.12 2 3 11 -14 10395.7 1170.60 23 3 11 -14 10903.9 1370.67 29 3 -11 13 191.760 715.094 2 3 11 -13 1312.99 684.491 12 3 11 -13 1333.91 721.562 29 3 11 -13 1376.93 649.648 23 -3 -11 -13 2066.71 833.682 15 3 11 -12 5607.98 968.355 29 3 11 -12 4652.47 810.602 23 3 -11 12 5595.18 1079.50 2 3 11 -12 4800.60 957.574 12 -3 -11 -12 4756.68 1070.88 15 -3 -11 -11 7496.83 1156.75 15 -3 -11 -11 5918.29 1129.35 25 3 -11 11 7001.29 1177.29 2 3 11 -11 6367.65 984.422 12 3 11 -11 6737.86 1046.80 29 -3 -11 -10 15174.4 1587.85 25 3 11 -10 13345.6 1286.17 29 3 11 -10 12759.6 1313.08 12 3 11 -10 12937.7 1250.97 6 3 -11 10 12101.4 1413.61 2 3 -11 9 6828.13 1148.58 2 3 11 -9 7777.35 1014.40 29 3 -11 8 3401.26 868.617 2 3 11 -8 2203.95 673.619 29 3 11 -7 2152.80 625.105 29 -3 11 7 2022.95 631.459 5 3 -11 7 2385.08 747.485 2 3 -11 6 7063.44 1080.41 2 -3 11 6 7656.83 883.898 5 3 11 -6 6894.24 930.205 29 -3 11 5 9908.43 1032.89 5 3 -11 5 10307.4 1133.38 2 3 11 -5 9638.21 1055.29 29 -3 11 4 5551.83 774.519 5 3 11 -4 5700.50 875.920 29 3 -11 4 5697.17 905.852 1 3 -11 4 4620.30 835.015 2 3 -11 3 81284.7 2743.68 1 -3 11 3 79814.4 2674.63 5 3 11 -3 85038.6 2729.82 29 3 -11 3 81380.7 2806.86 2 3 -11 2 5742.45 858.201 1 3 -11 2 7372.58 954.245 2 3 11 -2 5840.88 809.754 29 -3 11 2 6037.11 836.114 5 3 11 -1 922.603 521.475 29 3 -11 1 1132.90 617.258 1 -3 11 1 1111.58 497.556 5 -3 11 0 505.216 434.966 5 3 -11 0-163.055 516.978 1 3 -11 0-57.4686 496.105 3 3 11 0 461.135 420.704 29 -3 11 -1-21.1327 435.472 5 3 -11 -1 532.029 530.309 3 3 -11 -1 482.753 440.308 1 3 11 1 759.777 450.304 29 -3 11 -2 5028.18 823.043 5 3 -11 -2 5395.29 797.434 3 3 -11 -2 5656.64 850.068 1 3 11 2 5280.67 783.187 29 3 11 3 86585.4 2521.65 29 -3 11 -3 77375.3 2720.20 5 3 -11 -3 83492.4 2708.01 3 3 11 4 5400.60 770.692 29 3 -11 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1170.24 18 3 -11 -12 4874.53 885.077 4 3 -11 -12 6218.34 956.873 3 -3 11 -12 5801.42 1049.23 17 -3 11 -13 546.105 632.324 6 3 -11 -13 252.879 708.681 25 -3 11 -13 2452.04 965.509 22 -3 11 -13 1684.84 741.939 20 3 -11 -13 781.299 730.259 26 -3 -11 13 1297.78 854.319 18 3 -11 -13 2549.27 723.527 4 3 -11 -13 645.938 628.213 3 -3 11 -13 1539.23 772.496 17 3 -11 -14 11358.3 1427.84 25 -3 11 -14 6188.08 1097.85 6 -3 11 -14 10563.2 1372.66 20 3 -11 -14 11608.0 1271.61 4 -3 -11 14 11076.4 1459.36 18 -3 11 -14 10151.7 1290.08 17 3 -11 -14 9612.40 1170.97 26 3 -11 -15 15355.9 1455.93 26 3 -11 -15 14384.8 1620.28 25 -3 11 -15 14517.9 1546.43 20 -3 11 -15 13369.0 1320.37 12 -3 -11 15 14600.5 1574.88 18 -3 11 -15 17061.8 1590.60 17 3 -11 -16 7068.76 1203.55 25 3 -11 -16 7099.28 1137.99 26 -3 -11 16 8102.77 1264.08 18 -3 11 -16 5832.98 1088.82 17 3 -11 -17 3782.94 936.585 26 3 -11 -17 2534.38 848.648 25 -3 -11 17 4351.42 1052.01 18 -3 11 -17 3420.22 797.188 17 3 -11 -18 2843.98 926.508 25 -3 11 -18 3979.98 868.991 14 -3 -11 18 4526.13 1024.60 18 -3 11 -18 2528.93 769.923 17 3 -11 -18 3185.06 833.028 26 3 -11 -19 2430.44 805.176 25 3 -11 -19 2279.88 807.669 26 -3 11 -19 2667.01 785.489 14 -3 -11 19 1766.71 749.362 18 -3 11 -19 2388.04 750.670 17 3 -11 -20 429.543 618.607 25 -3 11 -20 474.898 509.011 14 -3 -11 20 1429.23 693.442 18 -3 11 -20 851.526 631.904 17 3 -11 -20 812.748 669.405 26 -3 11 -21-70.4535 483.972 14 3 -11 -21 333.508 589.646 25 -3 -11 21 132.671 555.978 18 -3 11 -21 465.631 534.920 17 3 -11 -21-7.21156 571.758 26 3 -11 -22 1748.19 612.379 25 -3 11 -22 1576.43 584.065 14 -3 11 -22 1588.64 620.672 17 3 -11 -22 2001.77 648.575 26 -3 11 -23 827.385 529.991 26 3 -11 -23 1008.91 492.709 27 -3 11 -23 213.181 400.176 14 -3 11 -23 825.278 500.543 17 3 -11 -23 576.590 538.129 26 3 -11 -24 1262.87 510.855 26 3 -11 -24 1192.42 555.852 27 -3 11 -24 1579.85 530.469 26 3 -11 -25 4482.82 619.619 27 3 -11 -25 5410.29 678.403 26 -3 11 -25 4316.86 595.343 26 -3 11 -26 371.980 299.466 26 3 12 -25 641.593 349.078 13 3 -12 25-47.6515 390.355 18 3 12 -24-159.427 389.064 13 3 -12 24 656.238 493.283 18 3 12 -23 1369.64 549.144 13 3 -12 23 2357.18 649.749 18 3 12 -22 1173.50 553.412 13 3 -12 22-2.57147 530.033 18 3 12 -21 516.634 518.058 13 3 -12 21 940.084 635.656 18 3 -12 20 555.258 422.512 16 3 12 -20 280.701 574.263 13 3 -12 20 561.018 612.795 18 3 12 -19 363.294 569.165 13 3 12 -19 620.947 408.844 23 3 -12 19 210.141 547.845 18 3 12 -18 5354.78 974.915 13 3 -12 18 3863.15 900.585 18 3 -12 18 4579.44 927.653 16 3 12 -18 5454.64 851.810 23 3 -12 17 2597.12 796.686 16 3 12 -17 1970.95 593.035 23 3 12 -17 1805.10 747.493 13 3 -12 17 2154.43 757.000 18 -3 -12 -17 2010.36 727.834 15 3 12 -16 2574.06 688.543 23 3 12 -16 3206.01 829.684 13 3 -12 16 1447.75 819.811 18 3 -12 16 3394.77 839.294 16 -3 -12 -16 3246.15 899.774 15 3 12 -15-862.921 529.478 23 3 -12 15-680.104 720.976 18 3 12 -15-690.055 654.125 13 -3 -12 -15 33.5084 464.158 15 3 -12 15-218.749 525.203 16 3 12 -14 3033.44 747.645 23 3 -12 14 841.305 614.690 18 3 -12 14 3170.88 811.320 16 -3 -12 -14 3675.57 952.865 15 -3 -12 -13 27955.7 2103.86 15 3 12 -13 26014.2 1785.84 23 3 12 -13 25834.7 1862.18 12 3 -12 13 28298.2 2146.94 2 3 12 -13 29907.7 2008.20 29 3 12 -12 12093.5 1347.99 29 3 -12 12 10396.2 1409.35 2 3 12 -12 9341.38 1207.17 12 3 -12 12 7149.87 1089.75 18 3 12 -12 10504.2 1173.65 23 3 -12 12 9306.53 1290.48 9 -3 -12 -12 10727.2 1404.34 15 3 12 -11 6464.31 1056.73 12 3 -12 11 5060.03 1031.22 2 3 -12 11 3994.55 928.625 18 3 12 -11 6365.73 987.055 29 -3 -12 -11 5373.23 1052.64 15 -3 -12 -10 6073.36 1060.12 15 -3 -12 -10 8436.12 1299.53 25 3 -12 10 8431.57 1256.59 9 3 12 -10 9152.08 1165.53 12 3 -12 10 7251.07 1162.39 2 3 -12 10 7166.14 996.579 18 3 12 -10 7940.42 1074.70 29 -3 -12 -9 778.408 819.627 25 3 -12 9 1101.48 696.197 9 3 12 -9 2003.66 671.921 29 3 12 -9 1801.92 850.144 21 3 12 -9 1443.40 702.366 12 3 -12 9 866.576 690.586 2 3 -12 9 2748.64 637.892 18 3 -12 8 9182.32 1219.04 2 3 12 -8 9463.41 1096.18 12 -3 -12 -8 10885.9 1415.70 25 3 -12 8 9874.62 1243.83 9 3 12 -8 9890.12 1161.78 29 3 12 -8 12379.9 1422.14 21 3 12 -7 2805.08 727.135 29 -3 12 7 3107.09 659.278 5 3 -12 7 2368.53 752.993 2 3 12 -6 3939.16 818.180 29 -3 12 6 3902.85 689.069 5 3 -12 6 5082.16 955.085 2 3 -12 5 8926.97 1184.40 2 -3 12 5 7892.57 965.010 5 3 12 -5 7917.13 1009.51 29 3 -12 5 8122.17 1011.81 1 3 12 -4 912.969 576.865 29 -3 12 4 1119.68 511.479 5 3 -12 4 1822.24 639.317 1 3 -12 4 1813.69 720.132 2 -3 12 3 2997.49 678.961 5 3 -12 3 4461.06 834.142 2 3 -12 3 3595.53 755.154 1 3 12 -3 3108.30 639.701 29 3 -12 2 4893.02 840.287 1 -3 12 2 5073.62 813.699 5 3 12 -2 6016.56 861.418 29 3 12 -1 21753.4 1431.43 29 3 -12 1 19880.4 1485.63 1 -3 12 1 19448.6 1432.90 5 3 12 0 1727.80 585.591 29 3 -12 0 2054.37 618.671 1 3 -12 0 1571.61 612.878 3 -3 12 0 1989.44 617.251 5 3 -12 -1 20881.3 1468.81 3 -3 12 -1 20339.8 1459.64 5 3 12 1 22209.5 1416.26 29 3 -12 -1 21276.6 1470.38 1 3 12 2 5072.73 792.430 29 -3 12 -2 4392.03 823.601 5 3 -12 -2 5573.67 857.633 3 3 -12 -2 5333.50 849.944 1 -3 12 -3 2851.91 711.984 5 3 -12 -3 3481.17 711.981 3 3 12 3 3186.79 636.269 29 -3 12 -4 1038.01 487.465 5 3 -12 -4 1448.92 601.159 3 3 -12 -5 7559.50 973.068 3 -3 12 -5 6541.99 922.969 5 -3 12 -6 4169.36 804.165 5 3 -12 -6 3681.76 751.247 3 -3 12 -7 2126.91 658.017 5 3 -12 -7 2330.79 676.116 3 3 -12 -8 9390.53 1083.89 3 -3 12 -8 8381.11 1213.55 22 -3 12 -8 9655.20 1096.30 5 -3 12 -8 8382.78 1369.51 19 -3 -12 8 11291.0 1414.55 18 3 -12 -8 9269.89 1308.78 25 3 -12 -8 10388.7 1193.36 26 3 -12 -9 1530.68 696.217 25 -3 12 -9 961.441 735.978 22 -3 12 -9 1544.55 791.855 19 -3 -12 9 2116.35 664.623 18 3 -12 -9 1206.44 553.053 3 -3 12 -9-182.019 629.115 17 3 -12 -9 742.538 645.594 26 -3 12 -9 1703.26 613.124 5 3 -12 -10 8225.37 1240.08 25 -3 12 -10 6386.94 1105.40 20 -3 12 -10 6851.97 1203.18 19 -3 12 -10 7638.49 1248.95 22 -3 12 -10 7498.21 972.747 5 -3 -12 10 6977.63 1139.36 18 3 -12 -10 7321.37 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2233.22 1005.06 19 3 -13 -5 2697.90 709.183 3 -3 -13 5 1504.07 809.501 18 3 -13 -6 9031.22 1227.99 25 -3 13 -6 8048.43 1262.66 22 -3 13 -6 8718.40 1233.65 19 -3 13 -6 9299.46 1080.08 5 -3 -13 6 10247.5 1394.91 10 -3 -13 6 9295.81 1216.77 18 3 -13 -6 9857.81 1110.47 3 3 -13 -7 3470.58 929.144 25 -3 13 -7 5672.88 1107.44 22 -3 13 -7 5928.38 894.920 5 -3 13 -7 4245.11 1022.60 19 3 -13 -7 4469.82 824.627 3 -3 -13 7 5770.75 985.448 18 -3 -13 7 6612.86 1251.71 10 -3 13 -8 1326.57 616.459 5 -3 13 -8 885.388 700.751 19 3 -13 -8 1608.99 614.230 3 -3 -13 8 2201.53 832.476 18 -3 13 -8 1724.92 778.942 22 -3 -13 8-57.9778 596.607 10 -3 13 -8 2676.90 722.464 17 3 -13 -8 554.652 676.682 25 3 -13 -8 1305.57 673.278 26 3 -13 -9 13034.5 1335.77 3 -3 13 -9 10634.2 1236.59 5 -3 13 -9 10650.4 1429.44 22 -3 13 -9 11501.8 1474.07 19 -3 -13 9 10924.3 1354.10 18 -3 13 -9 11962.9 1339.50 17 -3 -13 9 11952.7 1588.41 10 3 -13 -9 10102.1 1347.73 25 3 -13 -9 13056.7 1290.10 26 3 -13 -10 4987.85 1121.79 25 -3 13 -10 5369.25 892.604 5 -3 13 -10 3741.35 986.803 21 -3 13 -10 4940.49 944.479 20 -3 13 -10 4668.41 1080.92 19 -3 -13 10 6295.10 1117.93 18 3 -13 -10 3699.56 798.222 3 -3 -13 10 4442.18 988.932 10 -3 13 -10 4203.69 917.886 17 3 -13 -10 4180.31 960.162 26 -3 13 -10 5551.99 1062.99 22 3 -13 -11 1438.16 842.566 25 3 -13 -11 2186.57 736.188 26 -3 13 -11 2749.15 908.525 22 -3 13 -11 1692.89 454.523 5 3 -13 -11 1369.33 430.293 4 -3 -13 11 1460.92 837.769 18 3 -13 -11 2253.13 670.422 3 -3 13 -11 2366.47 798.078 17 -3 13 -11 2348.90 863.712 20 -3 13 -11 2160.22 870.584 6 3 -13 -12 3595.68 997.045 25 -3 13 -12 2710.54 836.959 22 -3 13 -12 1476.94 743.950 20 -3 -13 12 2752.16 881.206 18 3 -13 -12 1358.01 597.472 4 3 -13 -12 1598.57 594.773 3 -3 13 -12 2248.72 775.454 17 -3 13 -12 970.035 715.200 6 3 -13 -12 2526.25 789.631 26 3 -13 -13 12484.0 1560.19 25 -3 13 -13 9477.85 1397.39 22 -3 13 -13 11541.7 1435.13 20 -3 -13 13 11580.7 1435.85 18 -3 13 -13 13663.7 1417.53 17 3 -13 -13 12713.5 1373.42 26 3 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1926.79 682.529 17 3 -13 -19 2323.53 677.252 27 3 -13 -19 2017.73 754.030 26 3 -13 -20-550.716 541.353 25 3 -13 -20 1218.02 606.311 27 -3 13 -20-781.461 496.365 14 3 -13 -20 6.87447 651.737 26 -3 -13 20-33.3471 512.024 18 -3 13 -20 201.472 474.786 17 3 -13 -21 244.540 496.614 25 -3 13 -21 363.131 463.583 14 3 -13 -21 53.0978 434.504 27 -3 -13 21 520.447 553.166 18 -3 13 -21 186.158 477.548 17 3 -13 -21-460.939 577.715 26 3 -13 -22 938.400 513.613 25 3 -13 -22 920.685 342.367 27 -3 13 -22 257.692 401.845 14 -3 -13 22-426.987 447.950 18 -3 13 -22-263.870 411.179 17 3 -13 -22-414.145 541.269 26 3 -13 -23 501.601 267.521 25 -3 13 -23 5553.76 726.492 26 -3 13 -24 706.770 354.021 26 3 14 -24 516.431 319.821 13 3 -14 24-273.013 334.336 18 3 14 -23 254.611 407.620 13 3 -14 23 250.436 452.138 18 3 14 -22 78.3597 403.875 13 3 -14 22-329.360 473.909 18 3 14 -21 257.001 505.789 13 3 -14 21 1500.68 597.196 18 3 14 -20 1901.05 615.645 13 3 -14 20 1637.16 636.877 18 3 -14 20 481.099 539.372 16 3 14 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497.195 18 3 -20 -15 602.745 454.106 25 -3 20 -15-182.920 387.723 14 -3 20 -15 263.609 330.231 12 -3 -20 15 356.311 440.251 18 3 -20 -16 720.820 452.960 25 -3 20 -16 1731.08 411.183 12 -3 -20 16 1758.27 471.790 18 3 -20 -17 633.748 392.648 25 -3 20 -17 25.3980 307.281 14 -3 -20 17 119.430 327.184 18 3 21 -16 700.815 315.294 13 3 21 -15 904.078 317.143 23 3 21 -15 961.936 403.484 13 3 -21 14 9.60440 330.199 10 3 -21 14 344.869 420.142 16 3 21 -14 1073.40 371.935 23 3 21 -14-65.1820 402.903 13 3 21 -13 1649.63 525.049 13 3 -21 13 1183.31 469.369 11 3 -21 13 1304.27 572.948 16 3 21 -13 1847.10 483.669 23 3 21 -12-168.277 361.940 23 3 21 -12-828.579 480.229 13 3 -21 12-137.193 478.207 11 3 -21 12 196.611 438.558 16 3 21 -11-35.2668 358.752 23 3 21 -11 834.474 545.416 13 3 -21 11 314.980 468.301 11 3 -21 11 554.609 490.756 16 3 21 -10 766.504 445.211 23 3 -21 10 399.259 510.966 11 3 -21 10 956.573 583.763 16 3 21 -9 803.660 458.384 23 3 -21 9 45.7791 422.030 11 3 -21 9 392.956 487.732 16 3 21 -8 600.082 491.580 23 3 -21 8 1283.51 635.838 11 3 -21 8 633.312 503.869 16 3 21 -7 6884.31 909.297 23 3 -21 7 4679.13 863.775 11 3 -21 7 6383.18 919.508 16 3 21 -6 1209.27 526.433 23 3 -21 6 1092.48 619.999 11 3 -21 6 1399.49 629.236 16 3 21 -5 948.772 487.801 23 3 -21 5 1060.38 599.453 11 3 -21 5 666.306 569.252 16 3 21 -4 5909.48 820.318 23 3 21 -4 6803.83 1024.87 21 3 -21 4 5829.62 986.212 11 3 -21 4 5962.99 925.575 9 3 -21 4 6205.39 954.626 16 3 -21 3 1054.37 567.111 9 3 21 -3 1092.82 531.741 23 -3 21 3 1878.12 819.360 22 3 21 -3 159.184 583.290 21 -3 -21 -3 501.962 449.349 18 3 -21 3 900.662 646.444 11 3 -21 3 2299.21 723.275 16 3 -21 2 3383.24 794.723 9 3 21 -2 4094.76 684.456 23 -3 21 2 3130.79 897.639 22 3 21 -2 3974.53 813.170 21 -3 21 2 4176.13 916.646 19 -3 -21 -2 4934.08 806.463 18 3 -21 2 4064.52 787.015 11 3 -21 2 4211.79 783.020 16 3 -21 1 3707.65 831.971 9 3 21 -1 3969.42 687.615 23 -3 21 1 2790.39 878.645 22 -3 21 1 4132.98 824.814 19 -3 -21 -1 4228.67 798.945 18 3 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21 -6 2659.96 833.616 22 -3 21 -6 1441.40 647.394 21 -3 21 -6 1589.63 676.041 20 -3 -21 6 1956.84 637.548 18 -3 21 -6 1765.94 683.769 12 -3 -21 6 1464.32 667.793 10 3 -21 -7 4876.80 850.680 25 -3 21 -7 6795.04 1079.53 22 -3 21 -7 5776.07 977.998 21 -3 21 -7 6236.78 1005.33 20 -3 -21 7 7279.20 965.835 18 -3 21 -7 6465.05 930.546 12 -3 -21 7 7181.34 1059.96 10 3 -21 -8 864.197 594.118 25 -3 21 -8 676.951 617.068 22 -3 21 -8 1181.33 592.342 21 -3 21 -8 966.258 624.927 20 -3 -21 8 1166.70 560.621 18 -3 21 -8 1548.27 661.825 12 3 -21 -9 142.175 503.426 25 -3 21 -9 135.761 473.659 22 -3 21 -9 975.620 476.877 21 -3 21 -9 1088.08 677.825 20 -3 -21 9 368.876 540.147 18 -3 21 -9 1689.51 583.990 12 3 -21 -10 412.862 500.755 25 -3 21 -10 1763.49 632.726 21 -3 21 -10 2011.17 614.173 20 -3 -21 10 1123.50 532.709 18 -3 21 -10 809.329 542.348 12 3 -21 -11 732.494 438.624 25 -3 21 -11 750.707 530.775 20 -3 -21 11 560.411 464.417 18 -3 21 -11 418.707 438.278 12 3 -21 -12 599.781 473.628 25 -3 -21 12-115.713 411.658 18 -3 21 -12-194.404 424.750 12 3 -21 -13 992.802 498.797 25 -3 21 -13 873.845 433.284 14 -3 21 -13 1401.87 470.147 12 -3 -21 13 2026.94 554.779 18 3 -21 -14-73.9277 368.442 25 -3 21 -14 46.0103 370.311 14 -3 21 -14 166.450 332.567 12 -3 -21 14 425.474 390.362 18 3 -21 -15 415.650 360.394 25 -3 21 -15 245.508 325.669 14 -3 21 -15 970.277 354.121 12 -3 -21 15 476.093 315.508 18 3 -21 -16 748.207 342.909 25 -3 -21 16 87.1957 272.616 18 3 22 -14 2094.64 365.812 23 3 22 -13 1442.40 362.872 23 3 22 -13 913.264 362.246 13 3 22 -12 364.574 350.169 23 3 22 -12 390.512 405.316 13 3 -22 12 91.6054 358.373 11 3 22 -11 1516.70 468.501 23 -3 22 11 1999.90 494.569 22 3 22 -11 1333.71 515.714 13 3 -22 11 1108.57 470.521 11 3 -22 11 1300.43 485.737 16 -3 22 10 2192.25 599.412 22 3 22 -10 2161.74 540.992 23 3 22 -10 1839.68 542.276 13 3 -22 10 1997.42 545.900 11 3 -22 10 1654.02 511.094 16 3 22 -9-520.240 387.237 23 3 -22 9-303.673 475.153 11 3 -22 9-105.729 423.258 16 3 22 -8 624.288 381.346 23 -3 22 8 514.823 504.227 22 3 -22 8 185.480 489.553 11 3 -22 8 607.511 487.484 16 3 22 -7 626.595 424.009 23 -3 22 7 117.473 480.024 22 3 -22 7 544.608 460.888 11 3 -22 7 440.962 519.111 16 3 22 -6 3388.63 622.723 23 -3 22 6 4101.99 796.213 22 3 -22 6 3012.37 705.466 11 3 -22 6 3025.42 682.702 16 3 22 -5 623.998 415.098 23 3 -22 5 736.199 544.545 11 3 -22 5 1058.93 544.723 16 3 22 -4 586.639 426.756 23 3 -22 4 602.737 517.089 16 -3 22 4-95.5891 458.250 22 3 -22 4-136.175 505.386 11 3 22 -3-97.7737 315.684 23 -3 22 3-409.783 573.576 22 -3 22 3-173.327 407.117 12 3 -22 3 507.579 568.963 11 3 22 -2 1301.67 511.499 23 -3 22 2 524.548 545.386 22 -3 -22 -2 484.838 444.941 18 3 -22 2 906.906 512.971 11 3 22 -1 1178.74 414.465 23 -3 22 1 93.5223 549.506 22 -3 -22 -1-153.426 406.344 18 3 -22 1 177.225 462.320 11 -3 22 0 2512.41 760.840 22 -3 -22 0 2324.64 610.175 18 3 -22 0 2061.05 643.988 11 -3 22 -1 305.310 571.735 22 -3 -22 1 410.056 465.273 18 -3 22 -1 750.289 516.679 12 3 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22 -4 11 -10 9104.10 1024.87 5 -4 11 -10 6754.05 1209.58 19 -4 -11 10 4696.00 1100.38 18 4 -11 -10 4781.76 888.898 3 -4 11 -10 5073.53 1030.50 17 -4 11 -10 4287.89 963.509 6 4 -11 -10 6306.57 1019.03 26 -4 11 -11 6345.02 1025.27 6 4 -11 -11 6265.16 1261.36 25 4 -11 -11 8012.21 1082.81 3 -4 11 -11 7433.89 1274.90 22 -4 11 -11 7966.34 1318.30 19 -4 -11 11 10149.8 1326.28 18 -4 11 -11 7047.52 1182.57 17 4 -11 -11 8779.82 1208.76 27 4 -11 -11 8039.94 1160.10 26 4 -11 -12 3003.36 985.095 25 -4 11 -12 4271.54 1088.21 22 -4 -11 12 4008.17 989.764 18 4 -11 -12 2825.34 793.947 4 4 -11 -12 2644.23 732.713 3 -4 11 -12 3137.92 813.216 17 4 -11 -12 4103.27 935.764 26 -4 11 -12 3037.82 1018.18 6 4 -11 -12 4434.27 985.667 27 -4 11 -13 4984.41 859.521 24 -4 11 -13 5535.92 1180.40 22 4 -11 -13 4307.73 1102.54 25 -4 -11 13 3817.19 1034.89 18 -4 11 -13 5138.63 1021.69 17 4 -11 -13 5266.58 1046.68 27 4 -11 -13 5281.21 983.784 26 4 -11 -14 6089.72 1134.54 25 -4 11 -14 7867.55 1082.23 24 4 -11 -14 6392.19 1072.65 27 -4 -11 14 6638.24 1125.61 18 4 -11 -14 4468.79 920.418 26 -4 11 -14 6320.51 1066.47 17 4 -11 -15 7023.16 1261.41 25 4 -11 -15 8112.79 1177.39 27 -4 -11 15 9723.20 1371.68 18 -4 11 -15 9197.37 1247.17 17 4 -11 -15 6728.86 1023.30 26 4 -11 -16 907.005 764.159 25 -4 -11 16 928.518 742.200 18 -4 11 -16 3.46133 487.597 17 4 -11 -16 1007.45 698.880 27 4 -11 -16-586.568 623.281 26 -4 11 -17 5202.79 923.702 14 4 -11 -17 4487.39 1053.07 25 -4 -11 17 6327.70 1115.80 18 -4 11 -17 4092.77 898.797 17 4 -11 -17 4461.17 878.710 27 4 -11 -17 4377.43 945.477 26 4 -11 -18 803.606 691.880 25 -4 11 -18-534.842 543.270 14 -4 -11 18 230.643 608.428 18 -4 11 -18-528.953 584.172 17 4 -11 -18 516.004 538.224 26 4 -11 -18 746.989 637.487 27 4 -11 -19 2049.84 755.654 25 -4 11 -19 1225.00 681.788 14 -4 11 -19 1053.54 614.546 17 4 -11 -19 1109.16 676.200 26 4 -11 -19 1511.73 727.234 27 4 -11 -20 1842.35 736.290 25 -4 11 -20 1980.81 662.622 14 -4 11 -20 1243.50 614.684 17 4 -11 -20 1190.47 733.914 27 4 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6553.88 1062.40 29 -4 -12 -10 4262.62 1030.23 15 4 -12 10 4617.03 1029.55 9 4 12 -10 3331.80 712.829 23 4 -12 10 4000.53 929.951 2 4 -12 10 2964.27 870.307 18 4 12 -10 3372.45 934.288 29 4 -12 10 4144.29 918.728 1 -4 -12 -9 193.402 645.589 15 4 12 -9 668.464 518.384 23 4 -12 9 295.394 626.440 2 4 -12 9 2030.34 833.260 9 4 -12 9 1381.14 690.255 1 4 12 -9 1506.24 643.648 29 -4 -12 -8 7342.45 1055.00 15 4 -12 8 9088.40 1255.37 2 4 -12 8 7784.81 1113.92 1 4 12 -8 9422.66 1146.92 23 4 12 -8 6825.41 1118.93 29 4 -12 8 8241.78 1195.90 9 -4 -12 -7 3019.00 1086.77 15 4 12 -7 1558.48 628.670 23 -4 -12 -7 3129.19 740.217 18 4 -12 7 3053.72 815.312 1 4 -12 7 2534.83 794.781 2 4 12 -7 3370.08 800.353 29 4 -12 7 3866.79 893.826 9 4 -12 7 2937.86 818.870 8 4 -12 6 9074.71 1120.72 8 4 -12 6 8484.19 1141.57 1 4 12 -6 7959.21 1083.46 29 4 12 -6 8640.07 1103.62 23 -4 -12 -6 10063.1 1186.49 18 4 -12 6 8020.07 1156.34 2 4 -12 5 4522.71 917.298 8 4 -12 5 7053.09 992.778 1 4 12 -5 4055.01 920.666 29 4 12 -5 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1795.38 736.370 22 -4 16 -6 2540.53 928.954 19 -4 -16 6 1531.09 741.743 18 -4 -16 6 1898.27 888.061 10 4 -16 -6 1213.70 722.786 9 4 -16 -7 1840.29 700.830 8 4 -16 -7 38.4049 690.224 25 -4 16 -7-117.202 499.602 22 -4 16 -7 971.437 843.676 19 -4 -16 7 753.090 628.506 18 -4 -16 7 956.704 739.770 10 -4 16 -7 1367.68 652.351 17 4 -16 -7-146.803 557.527 9 4 -16 -8 747.324 603.248 8 4 -16 -8-549.833 710.598 25 -4 16 -8-436.740 630.060 22 -4 16 -8-29.1121 506.163 21 -4 16 -8 33.2391 646.303 19 -4 -16 8-315.934 631.208 18 -4 -16 8 911.943 648.578 10 -4 16 -8 52.4378 529.773 17 4 -16 -8 1601.20 701.197 9 4 -16 -9 850.572 626.318 25 -4 16 -9 298.424 634.104 22 -4 16 -9 299.707 603.923 20 -4 16 -9 523.762 589.739 19 -4 -16 9 828.002 688.474 18 -4 16 -9 1299.26 721.533 17 4 -16 -10 5163.13 1081.49 25 -4 16 -10 7885.32 1279.35 22 -4 16 -10 7556.54 1151.01 20 -4 -16 10 6661.98 1108.48 18 -4 16 -10 7752.81 1071.29 17 4 -16 -11 3420.55 1013.53 25 -4 16 -11 2913.69 913.176 22 -4 16 -11 2991.05 905.587 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1014.33 537.507 9 4 -19 -7 15055.0 1442.95 25 -4 19 -7 13989.9 1516.55 22 -4 19 -7 14181.2 1416.10 21 -4 19 -7 13825.4 1442.36 20 -4 -19 7 15084.2 1388.39 18 4 -19 -7 16273.4 1361.26 9 4 -19 -8-324.538 618.597 25 -4 19 -8 670.208 617.994 22 -4 19 -8-771.870 618.188 21 -4 19 -8-560.339 633.280 20 -4 -19 8-134.233 579.640 18 4 -19 -9 32.6515 529.867 25 -4 19 -9-48.3972 550.613 22 -4 19 -9 417.400 497.658 21 -4 19 -9-384.877 546.572 20 -4 -19 9 231.024 537.006 18 4 -19 -10 2392.02 691.870 25 -4 19 -10 2253.75 828.409 22 -4 19 -10 2534.82 723.595 20 -4 -19 10 1881.56 695.084 18 -4 19 -10 1203.37 641.647 12 4 -19 -11-128.638 527.971 25 -4 19 -11 317.779 462.116 20 -4 -19 11 1046.60 576.996 18 -4 19 -11-32.4549 475.744 12 4 -19 -12-125.769 541.030 25 -4 19 -12 161.264 501.427 20 -4 -19 12 308.145 489.768 18 -4 19 -12-17.0526 434.977 12 4 -19 -13 674.936 569.040 25 -4 -19 13 867.184 512.772 18 -4 19 -13 1231.62 492.136 12 4 -19 -14 296.014 495.636 25 -4 -19 14 109.150 444.781 18 -4 19 -14 147.429 349.015 12 4 -19 -15-82.1535 441.463 25 -4 19 -15 486.550 436.538 14 -4 19 -15 472.185 343.430 12 -4 -19 15-161.325 412.017 18 4 -19 -16 398.450 475.588 25 -4 19 -16-9.67789 333.087 14 -4 19 -16 494.137 301.823 12 -4 -19 16 597.810 456.498 18 4 -19 -17 1290.98 442.163 25 -4 19 -17 497.607 323.060 14 -4 -19 17 300.849 320.427 18 4 -20 16 463.633 345.338 16 4 20 -16 115.361 265.994 23 4 20 -15 651.096 333.597 23 4 20 -15-126.314 338.745 13 4 -20 15-136.870 351.154 16 4 20 -14 336.197 353.539 23 4 20 -14 205.364 385.974 13 4 -20 14 573.122 383.884 11 4 -20 14-389.633 450.508 16 4 20 -13 1166.26 434.357 23 4 20 -13 770.245 436.819 13 4 -20 13-68.2640 386.126 11 4 -20 13 53.3850 449.828 16 4 20 -12-75.0576 368.256 23 4 20 -12 319.031 446.402 13 4 -20 12 485.264 470.230 11 4 -20 12-40.7874 405.858 16 4 20 -11 336.659 424.917 23 4 20 -11 583.247 509.093 13 4 -20 11 618.587 525.965 11 4 -20 11 382.606 465.253 16 4 20 -10 1301.90 519.389 23 4 20 -10 441.400 513.094 13 -4 20 10-712.144 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540.054 18 4 -20 2-380.861 538.552 9 4 20 -1 5196.83 723.963 23 -4 20 1 5967.50 1115.11 22 -4 20 1 5587.23 1076.21 19 -4 -20 -1 5694.69 887.970 18 4 -20 1 6168.33 1007.16 9 -4 20 0 889.738 696.250 22 -4 20 0-226.283 630.255 19 -4 -20 0 159.516 422.069 18 4 -20 0 507.563 546.562 9 -4 20 -1 5529.13 1109.65 22 -4 20 -1 5171.94 1025.95 19 -4 -20 1 7152.47 967.288 18 4 -20 -1 5653.82 990.333 9 -4 20 -2-1522.04 816.461 22 -4 20 -2 650.680 717.068 19 -4 -20 2-228.169 472.926 18 4 -20 -2-975.752 579.722 9 -4 20 -3 329.854 630.043 22 -4 20 -3 1229.26 724.423 19 -4 -20 3 50.9395 491.045 18 4 -20 -3 497.700 518.297 9 -4 20 -4 1619.63 722.480 22 -4 20 -4 257.319 548.270 19 -4 -20 4 969.079 611.775 18 4 -20 -4 515.392 558.118 11 4 -20 -4 680.028 538.759 9 -4 20 -5 336.728 658.110 22 -4 20 -5 579.096 653.041 21 -4 20 -5 2439.53 754.876 20 -4 20 -5 1146.54 702.401 19 -4 -20 5 672.023 504.344 18 4 -20 -5 773.249 532.036 9 -4 20 -6 2085.27 715.677 22 -4 20 -6 861.358 596.708 21 -4 20 -6 1485.23 657.355 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20 -14 334.825 381.128 14 -4 20 -14 332.704 317.735 12 -4 -20 14 304.736 412.273 18 4 -20 -15-275.777 392.157 25 -4 20 -15 81.6781 315.869 14 -4 20 -15-791.591 313.826 12 -4 -20 15-563.722 363.338 18 4 -20 -16-43.8371 330.502 25 -4 20 -16-145.805 279.987 14 -4 -20 16-47.1320 274.542 18 4 -21 14 618.842 388.608 16 4 21 -14 463.660 326.089 23 4 21 -13-92.2382 295.872 23 4 -21 13 937.743 364.196 11 4 -21 13 392.009 358.752 16 4 21 -12 2690.30 527.598 23 4 21 -12 2623.39 514.254 13 4 -21 12 1067.23 435.866 11 4 -21 12 1801.06 530.192 16 4 21 -11 751.352 389.781 23 4 21 -11 1051.03 438.233 13 4 -21 11 585.981 436.515 11 4 -21 11 785.363 468.526 16 4 21 -10 1773.86 500.790 23 4 21 -10 2185.60 541.297 13 4 -21 10 1309.33 557.638 11 4 -21 10 1233.76 520.139 16 4 21 -9 3372.33 613.428 23 4 21 -9 3391.79 606.168 13 4 -21 9 3260.53 674.346 11 4 -21 9 2100.73 603.727 16 4 21 -8 511.022 419.610 23 4 21 -8 1563.43 525.183 13 4 -21 8 516.174 552.221 11 4 -21 8 486.901 481.473 16 4 21 -7 2155.78 586.631 23 -4 21 7 2037.17 639.489 19 4 -21 7 1914.99 634.724 11 4 -21 7 3164.71 640.291 16 4 21 -6 1042.19 494.025 23 -4 21 6 943.947 582.055 19 4 -21 6 1308.68 578.257 11 4 -21 6 644.948 556.573 9 4 -21 6 312.450 466.684 16 4 -21 5 2274.45 665.225 9 4 21 -5 2705.89 572.605 23 -4 21 5 2716.32 682.415 19 4 -21 5 2135.34 692.323 11 4 -21 5 3051.52 726.776 16 4 -21 4 355.409 543.493 9 4 21 -4 726.295 467.951 23 -4 21 4 1412.37 647.495 22 -4 21 4-191.995 506.189 19 4 -21 4 1058.84 559.291 11 4 -21 4-30.2595 501.503 16 4 -21 3 1386.05 618.288 9 4 21 -3 984.380 399.441 23 -4 21 3 1886.04 707.186 22 -4 21 3 826.410 585.738 19 4 -21 3 1775.26 566.852 11 4 -21 3 440.067 484.521 16 -4 21 2 1498.39 646.652 22 4 21 -2 660.686 422.910 23 -4 21 2 531.320 549.143 19 -4 -21 -2 543.026 471.852 18 4 -21 2-355.028 522.704 11 4 -21 2 462.945 497.931 9 -4 21 1-484.471 600.619 22 -4 21 1-273.272 589.256 19 -4 -21 -1-86.7187 419.204 18 4 -21 1 425.663 513.939 11 4 -21 1-40.2336 492.756 9 4 -21 0 3340.15 730.231 9 -4 21 0 3490.03 860.907 22 -4 21 0 4612.73 871.198 19 -4 -21 0 3914.09 710.599 18 4 -21 0 3941.87 757.732 11 4 -21 -1-345.657 483.709 9 -4 21 -1 685.070 593.743 22 -4 21 -1 261.255 616.028 19 -4 -21 1 461.923 522.383 18 4 -21 -1 171.409 482.657 11 -4 21 -2 383.778 455.090 22 -4 21 -2 284.393 554.116 19 -4 -21 2 603.129 453.587 18 4 -21 -2-199.378 481.508 11 4 -21 -2 764.502 501.671 9 4 -21 -3 765.928 513.942 9 -4 21 -3 790.368 559.861 22 -4 21 -3 2212.30 693.597 19 -4 -21 3 792.347 529.710 18 4 -21 -3 875.791 555.885 11 4 -21 -4 635.496 521.838 9 -4 21 -4-38.7487 532.646 22 -4 21 -4-619.667 528.495 21 -4 21 -4 1157.08 603.148 20 -4 -21 4 369.617 452.538 18 -4 21 -5 2242.46 752.936 22 -4 21 -5 1205.75 617.395 21 -4 21 -5 2794.60 763.667 20 -4 -21 5 1836.43 611.866 18 4 -21 -5 3081.59 680.324 9 -4 21 -6 1216.76 612.429 22 -4 21 -6 204.051 484.768 21 -4 21 -6 1222.26 598.540 20 -4 -21 6 1120.63 550.841 18 4 -21 -7 1690.21 593.000 25 -4 21 -7 2277.10 736.606 22 -4 21 -7 1489.16 577.684 21 -4 21 -7 1622.14 702.868 20 -4 -21 7 2400.92 643.038 18 -4 21 -7 3257.27 661.523 12 4 -21 -8 706.173 465.276 25 -4 21 -8-142.549 493.458 22 -4 21 -8 934.598 441.584 21 -4 21 -8 475.535 513.477 20 -4 -21 8-406.438 488.715 18 -4 21 -8 121.732 463.245 12 4 -21 -9 2020.19 626.920 25 -4 21 -9 3517.49 708.025 20 -4 -21 9 2693.49 607.249 18 -4 21 -9 2775.72 573.241 12 4 -21 -10 1774.83 553.497 25 -4 21 -10 856.813 466.653 20 -4 -21 10 2507.59 604.329 18 -4 21 -10 2474.91 582.703 12 4 -21 -11 1146.39 476.217 25 -4 21 -11 1010.49 471.661 20 -4 -21 11 390.416 433.648 18 -4 21 -11 522.315 417.988 12 4 -21 -12 2809.68 560.018 25 -4 -21 12 2167.61 536.767 18 -4 21 -12 2125.55 497.878 12 4 -21 -13 394.747 385.395 25 -4 21 -13 138.526 325.995 14 -4 -21 13 463.137 340.766 18 -4 21 -13 945.805 357.215 12 4 -21 -14 490.114 325.056 25 -4 21 -14-349.613 297.428 14 -4 -21 14 233.778 296.963 18 4 22 -12 1364.17 350.558 23 -4 22 11 1102.40 399.742 22 4 -22 11 415.047 339.527 11 4 -22 11 233.301 343.114 16 4 22 -10 793.715 361.630 23 -4 22 10 854.672 379.093 22 4 -22 10 380.344 364.529 11 4 -22 10 1251.25 397.170 16 4 22 -9 930.688 403.079 23 4 -22 9 421.071 414.692 11 4 -22 9 918.836 437.285 16 4 22 -8 1317.31 459.952 23 -4 22 8 768.347 475.483 22 4 -22 8 1157.32 499.851 11 4 -22 8 1144.37 438.280 16 4 22 -7 337.111 360.683 23 -4 22 7 555.533 519.704 22 4 -22 7 204.749 416.084 11 4 -22 7-501.907 404.360 16 4 22 -6 2159.72 460.092 23 -4 22 6 1939.92 623.644 22 4 -22 6 991.369 495.912 11 4 -22 6 2155.19 560.303 16 4 22 -5 186.384 293.696 23 -4 22 5 915.251 543.865 22 4 -22 5 576.999 479.479 11 4 -22 5 618.080 425.330 16 4 22 -4-287.681 404.192 23 -4 22 4-507.109 558.857 22 -4 22 4 1283.71 523.934 19 4 -22 4 237.164 423.751 11 4 22 -3 1405.11 441.511 23 -4 22 3 1040.89 569.274 22 -4 22 3 441.852 533.335 19 4 -22 3 816.593 462.429 11 -4 22 2 762.821 590.153 22 -4 22 2 1503.76 673.695 19 4 -22 2 875.796 511.181 11 4 -22 2 1580.23 584.302 9 -4 22 1 701.623 550.234 22 -4 22 1-174.393 473.098 19 4 -22 1 408.722 439.735 11 4 -22 1 31.8917 451.108 9 -4 22 0-301.514 511.624 22 -4 22 0 461.038 558.214 19 -4 -22 0 457.966 443.868 18 4 -22 0-224.794 472.412 11 4 -22 0 262.329 465.379 9 -4 22 -1 359.917 563.742 22 -4 -22 1 44.2605 411.061 18 4 -22 -1 368.647 469.881 11 4 -22 -1-260.151 433.154 9 -4 22 -2 1232.30 610.266 22 -4 22 -2 261.611 510.087 21 -4 22 -2 963.503 620.645 20 -4 -22 2 1055.05 480.584 18 4 -22 -2 1040.43 472.791 11 -4 22 -3 1251.37 551.870 22 -4 22 -3-279.913 509.944 21 -4 22 -3 1313.86 581.585 20 -4 -22 3 586.988 461.073 18 -4 22 -3 713.773 533.614 12 4 -22 -3-442.489 313.786 11 -4 22 -4 1054.43 562.476 22 -4 22 -4-377.396 492.120 21 -4 22 -4 297.809 522.938 20 -4 -22 4 64.6476 396.789 18 -4 22 -4 761.108 485.973 12 -4 22 -5 583.931 523.247 22 -4 22 -5-400.424 482.189 21 -4 22 -5 864.120 546.430 20 -4 -22 5 517.712 418.144 18 -4 22 -5 1111.77 466.329 12 -4 22 -6 1351.44 622.678 22 -4 22 -6 255.427 405.818 21 -4 22 -6 1633.75 570.462 20 -4 -22 6 1700.19 523.160 18 -4 22 -6 1273.39 513.111 12 -4 22 -7 118.091 524.826 22 -4 22 -7 1103.35 413.230 21 -4 22 -7-191.213 414.214 20 -4 -22 7 533.276 390.638 18 -4 22 -7-139.734 363.239 12 -4 22 -8 281.575 287.327 21 -4 22 -8 1113.97 488.059 20 -4 -22 8 1892.55 500.938 18 -4 22 -8 1386.15 484.093 12 -4 22 -9 1148.59 508.366 20 -4 -22 9 1508.58 499.453 18 -4 22 -9 1268.13 457.682 12 4 -22 -10-109.589 379.185 25 -4 -22 10-15.5658 331.609 18 -4 22 -10 717.799 378.436 12 -4 -22 11 703.872 379.196 18 -4 22 -11 1381.15 375.254 12 -4 -22 12 819.384 326.536 18 -4 22 -12 1282.41 328.390 12 4 23 -9 2061.87 344.837 23 4 -23 9 750.271 365.958 11 4 23 -8 558.945 304.858 23 4 -23 8 759.690 330.620 11 -4 23 7 1338.78 444.307 22 4 -23 7 1202.64 420.528 11 4 23 -6 2707.43 421.000 23 -4 23 6 1905.94 533.672 22 4 23 -5 232.349 293.414 23 -4 23 5-132.875 430.110 22 4 -23 5 350.107 406.498 11 4 23 -4 857.059 311.198 23 -4 23 4 482.659 520.234 22 4 -23 4 222.158 401.921 11 -4 23 3 1978.47 593.468 22 4 -23 3 859.972 453.675 11 -4 23 2-251.545 435.926 22 -4 23 2 305.982 472.636 20 -4 23 2 191.863 339.021 12 4 -23 2 541.698 423.966 11 -4 23 1 978.267 526.728 22 -4 23 1 718.854 510.941 20 -4 23 1-173.113 343.195 12 4 -23 1 115.455 374.646 11 -4 23 0 2663.20 665.175 22 -4 23 0 995.248 523.378 21 -4 23 0 2380.20 600.262 20 -4 23 0 1788.14 450.367 12 4 -23 0 949.490 482.100 11 -4 23 -1 946.654 487.430 22 -4 23 -1 354.495 467.629 21 -4 23 -1 102.809 431.920 20 -4 23 -1 1.55340 407.990 12 4 -23 -1-45.3618 373.665 11 -4 23 -2 695.294 488.590 22 -4 23 -2-13.7473 434.051 21 -4 23 -2 242.807 458.489 20 -4 -23 2 313.394 343.777 18 -4 23 -2 457.402 400.743 12 4 -23 -2 6.21567 228.815 11 4 -23 -2 110.423 290.849 10 -4 23 -3 1478.04 552.073 22 -4 23 -3 608.230 463.895 21 -4 23 -3 1476.66 557.198 20 -4 -23 3 2259.18 484.251 18 -4 23 -3 1839.41 505.149 12 -4 23 -4 585.435 462.541 22 -4 23 -4 182.538 398.695 21 -4 23 -4 656.067 498.883 20 -4 -23 4 868.225 412.274 18 -4 23 -4 391.848 389.810 12 -4 23 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397.120 312.321 11 4 -24 2 1807.53 419.631 10 -4 24 1 903.466 371.255 22 -4 24 1-417.783 341.206 21 -4 24 1 89.2996 349.755 20 4 -24 1 908.690 316.666 10 -4 24 0 692.875 363.583 22 -4 24 0 150.736 346.787 21 -4 24 0 711.179 422.086 20 -4 24 -1 53.1598 300.097 22 -4 24 -1-566.635 306.295 21 -4 24 -1 437.881 373.147 20 -4 24 -2 2577.15 529.119 22 -4 24 -2 1528.92 464.113 20 -4 24 -2 1636.98 357.728 12 -4 24 -3 800.581 362.265 22 -4 24 -3 424.273 334.070 20 -4 24 -3 484.742 283.163 12 -4 24 -4 328.280 334.607 20 -4 24 -4 203.601 252.267 12 -4 24 -5 198.071 299.729 20 -4 24 -5 282.609 261.590 12 -4 24 -6-118.500 241.768 20 5 0 0-192.030 515.687 29 5 0 1 109679. 2909.62 29 5 0 -1 116126. 2938.80 29 5 0 2 241.637 484.981 29 5 0 -3 488.178 455.238 29 5 0 -4 8694.32 881.048 29 5 0 -5 10559.6 976.618 29 5 0 -6 42779.0 1760.11 4 5 0 -6 36773.2 1697.70 29 5 0 -7 26800.2 1446.91 4 5 0 -7 25738.0 1451.39 29 5 0 -8 49467.5 2033.18 4 5 0 -8 46704.0 1945.05 29 5 0 -9 11470.3 1069.60 4 5 0 -9 12149.6 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569.723 24 -5 6 -20 1199.05 607.624 17 5 -6 -20-133.018 552.592 26 -5 6 -21 1899.16 619.968 26 -5 6 -21 625.977 468.606 17 5 -6 -21 709.582 717.317 27 5 -6 -21 1155.91 618.689 26 -5 6 -22 193.399 401.373 26 5 -6 -22 956.628 526.738 26 -5 6 -22 570.294 466.661 17 5 -6 -22 1546.08 712.458 27 -5 6 -23 3407.28 691.302 17 -5 6 -23 4004.75 697.039 28 5 -6 -23 4075.12 840.219 27 5 -6 -23 4200.62 655.492 26 -5 6 -24 5120.98 738.572 28 -5 6 -24 5555.79 756.677 17 5 -6 -24 5388.74 833.092 27 5 -6 -24 4871.33 626.349 26 -5 6 -25 46.5368 346.136 28 5 -6 -25 534.640 473.227 27 5 -6 -26 455.797 319.254 27 5 7 -25-638.757 398.746 13 5 -7 25-156.441 420.015 18 5 7 -24 448.669 450.456 13 5 -7 24-28.6737 496.718 18 5 7 -23 1097.83 540.974 13 5 -7 23 1080.91 583.284 18 -5 -7 -23 479.941 270.640 28 5 7 -22-14.7683 544.756 13 -5 -7 -22 303.656 424.550 28 5 7 -21 2070.40 703.292 13 -5 -7 -21 1451.95 613.626 28 -5 -7 -21 1673.79 699.852 15 5 7 -20 1238.40 637.210 13 -5 -7 -20 836.798 553.368 28 -5 -7 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29767.8 2211.26 15 -5 -7 -10 1565.25 713.040 15 5 7 -10 2092.68 689.890 23 5 -7 10 1220.50 598.782 1 5 -7 10 2422.82 717.291 2 5 7 -10 2001.50 732.893 29 -5 -7 -9 3834.86 913.695 15 5 7 -9 3676.07 773.129 23 5 -7 9 1873.99 604.919 1 5 -7 9 2788.22 798.673 2 5 7 -9 2322.57 787.057 29 5 -7 8 5698.29 849.274 2 5 -7 8 4642.09 846.975 1 5 7 -8 5449.99 899.736 29 5 -7 7 1271.56 560.484 2 5 -7 7 1782.21 674.682 1 5 7 -7 2423.22 710.655 29 5 -7 6 531.385 426.330 2 5 7 -6 95.9035 507.662 29 5 -7 6 611.028 515.266 1 5 -7 5 2783.60 693.980 1 5 7 -5 2888.91 738.735 29 5 7 -4 8624.81 1083.95 29 5 -7 4 8314.41 1014.28 1 5 7 -3 6623.46 946.633 29 5 -7 3 8042.79 913.565 3 5 -7 3 5455.27 862.726 1 5 -7 2 5415.47 813.976 3 5 7 -2 7309.53 1000.96 29 5 -7 2 6574.93 912.267 1 5 -7 1 45795.0 2044.01 1 5 7 -1 45278.7 2110.68 29 5 -7 1 48174.5 1985.96 3 5 -7 0-341.835 436.884 3 5 7 0-345.035 565.483 29 5 7 1 42822.0 2063.51 29 5 -7 -1 45829.0 1917.46 3 5 -7 -2 6353.64 843.201 3 5 7 2 5945.09 904.758 29 5 -7 -3 6927.76 788.073 29 5 7 3 6414.47 919.387 29 5 -7 -3 6927.70 862.028 3 5 -7 -4 8305.92 913.371 3 5 -7 -4 11212.5 943.585 29 5 7 4 8404.16 997.482 29 5 -7 -5 3560.71 653.508 3 5 7 5 3006.85 683.418 29 5 -7 -6 526.277 438.382 3 5 7 6 464.807 509.551 29 5 7 7 3214.76 663.938 29 5 -7 -7 2182.74 624.081 3 5 7 8 5168.80 879.907 29 5 -7 -8 5039.28 814.676 3 5 7 9 1930.90 650.732 29 5 -7 -9 1905.69 783.570 7 5 -7 -9 2070.74 582.606 3 -5 7 -9 1935.02 770.545 17 5 -7 -9 952.909 632.316 27 5 -7 -10 507.055 658.258 7 -5 7 -10 2286.93 889.539 19 5 -7 -10 2124.50 633.773 3 -5 7 -10 2171.80 758.765 17 5 -7 -10 955.349 720.959 27 5 -7 -11 26395.5 1637.15 7 5 -7 -11 27328.2 1765.37 3 5 -7 -11 28521.8 1851.75 4 -5 7 -11 29146.1 2132.89 19 -5 7 -11 24966.8 1934.57 17 5 -7 -11 30822.2 2176.35 27 5 -7 -11 29575.5 1880.24 26 -5 7 -12 1796.44 695.157 24 5 -7 -12 1526.50 642.099 7 5 -7 -12 2817.70 764.003 4 -5 7 -12 1902.92 794.215 17 5 -7 -12 2134.02 826.509 27 5 -7 -12 2208.19 825.035 26 -5 7 -13 8241.04 1212.69 24 5 -7 -13 7044.69 1008.85 7 5 -7 -13 7644.39 1044.11 4 -5 7 -13 8974.82 1279.83 17 5 -7 -13 8276.70 1258.23 27 5 -7 -13 8899.31 1174.64 26 5 -7 -14 8254.32 1327.06 25 -5 7 -14 11289.8 1331.39 24 5 -7 -14 9286.65 1087.68 7 -5 7 -14 9431.67 1337.26 17 5 -7 -14 11462.1 1398.63 27 5 -7 -14 10019.3 1277.18 26 5 -7 -15 822.506 693.632 25 -5 7 -15 1309.70 612.122 24 5 -7 -15 1527.41 652.548 7 -5 7 -15 1907.40 731.168 17 5 -7 -15 1879.26 736.466 26 5 -7 -16 1601.66 775.044 25 -5 7 -16 1880.34 826.350 24 5 -7 -16 3026.00 708.813 7 -5 7 -16 1419.32 686.179 17 5 -7 -16 1852.05 735.746 26 5 -7 -17 7487.32 1246.93 25 -5 7 -17 10217.3 1237.78 24 5 -7 -17 7303.88 955.433 7 -5 7 -17 7609.53 1137.37 17 5 -7 -17 9741.02 1345.29 27 5 -7 -17 7706.94 1103.42 26 5 -7 -18 5607.45 1064.33 25 -5 7 -18 3682.26 866.912 24 -5 7 -18 4937.69 991.070 17 5 -7 -18 5055.60 1039.06 27 5 -7 -18 5243.02 935.813 26 5 -7 -19 1315.09 697.676 25 -5 7 -19 1556.49 626.675 24 -5 7 -19 1091.98 614.727 17 5 -7 -19 2128.16 882.826 27 5 -7 -19 288.794 647.299 26 -5 7 -20-15.2867 536.502 17 5 -7 -20 1174.71 727.298 27 5 -7 -20 677.140 604.337 26 -5 7 -21 1748.02 575.736 26 -5 7 -21 1583.70 589.975 17 5 -7 -21 2549.62 824.312 27 5 -7 -21 2033.67 664.793 26 -5 7 -22 1413.68 538.965 26 5 -7 -22 494.216 526.072 26 -5 7 -22 159.861 450.517 17 5 -7 -22 1044.21 669.694 27 -5 7 -23 321.385 219.946 26 -5 7 -23 1437.17 515.358 17 5 -7 -23 1675.86 669.191 27 -5 7 -23 1202.38 502.301 28 5 -7 -23 747.765 478.182 26 -5 7 -24 943.855 436.004 17 -5 7 -24-9.39874 374.395 28 5 -7 -24 1110.42 560.217 27 5 -7 -24 1008.41 455.657 26 5 -7 -25 293.114 451.211 27 -5 7 -25 194.796 314.623 28 5 8 -25 898.807 388.956 13 5 -8 25 1469.63 433.785 18 5 8 -24 756.649 448.520 13 5 -8 24 1281.71 534.129 18 5 8 -23 2592.66 604.446 13 5 -8 23 1877.08 658.779 18 5 8 -22 703.230 556.979 13 5 -8 22 923.766 575.339 18 5 8 -21 1059.60 571.981 13 -5 -8 -21 1198.50 590.364 15 5 8 -20 567.284 568.848 13 -5 -8 -20 192.385 490.318 15 5 8 -19 755.761 471.622 23 5 8 -19 1556.72 735.806 13 -5 -8 -19 1198.82 714.773 15 5 8 -18 11483.2 1141.85 23 5 8 -18 10065.0 1132.59 13 -5 -8 -18 10613.9 1351.45 15 5 8 -17 1642.32 702.415 23 5 8 -17 1818.81 728.224 13 -5 -8 -17 1396.54 808.640 15 -5 -8 -16 2875.43 922.818 15 5 8 -16 1386.57 645.826 23 5 8 -16 1397.56 641.893 13 -5 -8 -15-312.635 668.307 15 5 8 -15 866.081 551.297 23 -5 -8 -14 2871.12 913.321 15 5 8 -14 5178.66 922.870 23 5 8 -14 6116.35 1013.72 13 -5 -8 -13 3734.67 943.802 15 5 8 -13 4189.08 853.243 23 5 8 -13 4219.36 940.709 13 5 8 -13 6008.58 968.175 29 5 -8 13 3046.06 830.074 1 5 -8 12 15643.1 1567.39 2 5 -8 12 16847.4 1613.11 1 5 8 -12 17270.7 1427.09 23 5 8 -12 18744.4 1607.05 13 5 8 -12 15787.2 1487.53 29 -5 -8 -12 18535.2 1771.78 15 5 -8 11 14968.1 1471.19 2 5 8 -11 15459.0 1434.14 23 5 8 -11 15803.1 1452.92 13 5 8 -11 14298.0 1430.91 29 5 -8 11 13774.1 1369.12 1 -5 -8 -11 14092.4 1568.05 15 -5 -8 -10 7855.09 1285.82 15 5 8 -10 6937.43 985.891 23 5 8 -10 8051.53 1151.74 13 5 -8 10 6277.85 1004.03 1 5 -8 10 7456.79 1088.71 2 5 8 -10 8431.78 1155.93 29 -5 -8 -9 6065.17 1082.28 15 5 8 -9 6390.97 945.954 23 5 -8 9 7011.53 1046.54 1 5 -8 9 6803.55 1066.86 2 5 8 -9 7393.09 1071.35 29 -5 -8 -8 1285.17 665.276 15 5 8 -8 2103.64 596.420 23 5 -8 8 1503.09 585.105 2 5 -8 8 1506.93 608.809 1 5 8 -8 1366.49 715.569 29 5 -8 7 10579.7 1218.46 1 5 -8 7 9756.49 1123.16 2 5 8 -7 10890.2 1133.31 23 5 8 -7 9755.09 1161.92 29 5 -8 6 5466.82 889.693 1 5 -8 6 6548.93 912.617 2 5 8 -6 7020.97 1039.46 29 5 8 -5 3860.61 848.485 29 5 -8 5 5335.34 888.132 1 5 8 -4 806.804 578.768 29 5 -8 4 441.933 538.827 1 5 8 -3 5716.90 968.534 29 5 -8 3 6213.83 930.821 1 5 -8 3 5709.47 833.241 3 5 -8 2 305.619 455.632 3 5 -8 2 358.241 556.967 1 5 8 -2 721.402 593.169 29 5 -8 1 2499.04 650.021 3 5 8 -1 3305.43 773.565 29 5 -8 1 3602.72 740.870 1 5 -8 0 5293.10 834.003 3 5 8 0 7441.64 965.580 29 5 8 1 2771.16 704.015 29 5 -8 -1 2693.93 645.381 3 5 -8 -2 442.460 421.278 3 5 8 2 1047.30 627.516 29 5 -8 -3 7458.94 851.181 29 5 8 3 6129.15 929.323 29 5 -8 -3 5938.50 909.936 3 5 8 4 484.522 555.595 29 5 -8 -4 653.162 491.091 3 5 8 5 4995.94 872.051 29 5 -8 -5 4849.50 775.989 3 5 -8 -6 6670.49 864.552 3 5 8 6 5800.34 870.631 29 5 -8 -7 12141.2 1158.08 3 5 8 7 10302.7 1142.37 29 -5 8 -7 8198.92 1195.46 17 5 8 8 838.949 578.820 29 5 -8 -8 787.819 590.814 7 5 -8 -8 1027.45 540.466 3 -5 8 -8-196.671 537.077 17 5 -8 -8 777.367 629.282 27 5 -8 -9 6434.72 920.779 7 5 -8 -9 7045.90 1186.16 27 -5 8 -9 4785.76 1126.79 19 5 -8 -9 6604.29 941.438 3 -5 8 -9 5377.68 988.368 17 5 -8 -9 8530.85 1093.28 26 5 -8 -10 6477.31 931.234 7 -5 8 -10 8258.95 1153.72 22 5 -8 -10 7782.39 1139.11 26 -5 8 -10 8727.95 1310.48 19 5 -8 -10 7258.76 1011.27 3 -5 8 -10 7457.23 1175.92 17 5 -8 -10 7911.67 1215.84 27 -5 8 -11 19596.5 1579.93 24 5 -8 -11 15464.1 1332.93 7 5 -8 -11 16252.2 1690.82 27 -5 8 -11 16460.0 1657.05 22 5 -8 -11 16093.0 1409.15 3 5 -8 -11 16092.3 1474.40 4 -5 8 -11 17801.7 1821.53 19 -5 8 -11 15214.9 1605.35 17 5 -8 -11 13945.3 1470.96 26 5 -8 -12 17706.7 1757.16 27 -5 8 -12 15926.7 1549.88 24 5 -8 -12 13834.9 1301.27 7 -5 8 -12 19506.7 1798.49 22 5 -8 -12 17411.0 1501.99 3 5 -8 -12 17473.6 1506.50 4 -5 8 -12 16331.9 1673.67 17 5 -8 -12 16931.4 1554.73 26 5 -8 -13 5365.48 1123.69 25 -5 8 -13 4518.09 907.520 24 5 -8 -13 3415.06 827.677 7 -5 8 -13 4582.83 1042.59 17 5 -8 -13 4466.25 1049.72 27 5 -8 -13 3937.76 952.724 26 5 -8 -14 3623.28 1081.15 25 -5 8 -14 4228.75 960.863 24 5 -8 -14 4592.66 864.206 7 5 -8 -14 4046.53 869.594 26 -5 8 -14 6172.58 1056.41 17 5 -8 -14 5804.43 1065.02 27 5 -8 -15 987.825 669.627 25 -5 8 -15 1273.29 610.758 24 5 -8 -15 250.072 486.064 7 -5 8 -15 286.132 498.943 17 5 -8 -15-189.450 618.338 26 5 -8 -15 1182.94 710.695 27 5 -8 -16 1449.95 782.066 25 -5 8 -16 1467.72 660.776 24 -5 8 -16 2596.83 789.768 14 5 -8 -16 612.659 429.677 7 -5 8 -16 949.744 667.598 17 5 -8 -16 2082.12 812.276 27 5 -8 -16 999.604 753.045 26 5 -8 -17 995.606 711.987 25 -5 8 -17 653.061 567.207 24 -5 8 -17 1960.81 721.475 14 -5 8 -17 1521.05 746.042 17 5 -8 -17 2561.33 850.795 27 5 -8 -17 2221.37 755.408 26 5 -8 -18 11366.4 1354.64 25 -5 8 -18 10414.6 1217.31 24 -5 8 -18 11496.8 1199.00 14 -5 8 -18 9545.11 1246.84 17 5 -8 -18 12652.0 1499.32 27 5 -8 -18 10486.6 1226.53 26 5 -8 -19 2364.34 726.030 25 -5 8 -19 1400.36 644.711 14 -5 8 -19 1253.99 641.042 17 5 -8 -19 1647.75 762.789 27 5 -8 -19 573.950 634.544 26 5 -8 -20 393.712 578.574 25 -5 8 -20-243.992 503.698 17 5 -8 -20 1188.41 774.357 27 5 -8 -20 920.029 632.645 26 -5 8 -21 1165.70 557.770 26 5 -8 -21 1679.84 723.253 27 -5 8 -21 1591.04 686.884 17 5 -8 -21 1892.83 649.858 26 -5 8 -22 1066.47 476.874 26 -5 8 -22 798.536 519.251 17 -5 8 -22 354.651 472.259 28 5 -8 -22 949.036 689.712 27 5 -8 -22-215.729 499.610 26 -5 8 -23 1470.10 364.992 26 -5 8 -23 2368.63 593.355 17 -5 8 -23 890.671 448.604 28 5 -8 -23 2442.66 667.569 27 5 -8 -23 2208.89 564.633 26 5 -8 -24 795.393 530.411 27 -5 8 -24 394.930 346.230 28 5 -8 -25 426.000 386.016 27 5 -9 25 274.129 300.871 18 5 9 -24 867.265 393.831 13 5 -9 24 1058.90 447.972 18 5 9 -23 2149.04 554.623 13 5 -9 23 1111.01 546.675 18 5 9 -22 692.432 515.617 13 5 -9 22 35.8736 512.201 18 5 9 -21 904.708 549.994 13 5 -9 21 945.397 589.849 18 -5 -9 -21 664.482 509.435 15 5 9 -20 1314.04 594.872 13 5 -9 20 427.858 560.689 16 -5 -9 -20 1435.90 601.029 15 5 9 -19 3101.25 606.224 23 5 9 -19 2875.01 791.264 13 5 -9 19 1583.18 710.331 16 -5 -9 -19 1431.07 710.238 15 5 9 -18 1300.67 526.085 23 5 9 -18 644.292 587.413 13 -5 -9 -18 619.022 652.580 15 5 9 -17 4984.01 854.820 23 5 9 -17 3809.80 859.544 13 -5 -9 -17 5441.89 1147.39 15 5 9 -16 7761.53 1068.13 23 5 9 -16 8538.63 1105.54 13 -5 -9 -16 9956.93 1375.32 15 -5 -9 -15 7534.04 1180.45 15 5 9 -15 7518.41 975.281 23 5 9 -15 5924.80 1022.39 13 -5 -9 -14-118.486 626.944 15 5 9 -14 734.627 514.072 23 5 9 -14 1284.97 739.246 13 -5 -9 -13 1098.30 788.384 15 5 9 -13 436.412 606.075 23 5 9 -13 1125.42 739.230 13 5 9 -12 13979.6 1380.07 23 5 9 -12 12113.6 1369.64 13 5 9 -12 15038.9 1462.49 29 -5 -9 -12 15072.1 1649.12 15 5 -9 12 13113.8 1457.87 1 5 -9 11 11771.0 1344.74 2 5 9 -11 13591.7 1336.34 23 5 9 -11 13325.2 1425.79 13 5 -9 11 9664.08 1281.07 1 5 9 -11 14745.0 1414.96 29 -5 -9 -11 13828.2 1583.49 15 5 -9 10 16846.5 1543.30 1 5 9 -10 19125.3 1511.91 23 5 -9 10 18351.6 1619.26 2 5 9 -10 17196.1 1435.49 13 5 9 -10 18950.6 1610.23 29 -5 -9 -10 20869.5 1873.81 15 5 -9 9 17234.1 1513.23 1 5 9 -9 17297.6 1457.32 23 5 -9 9 18886.6 1610.25 2 5 9 -9 19502.8 1628.09 29 -5 -9 -9 18655.6 1728.98 15 5 -9 9 20826.0 1645.83 8 -5 -9 -8 7235.19 1212.74 15 5 9 -8 7962.85 1069.51 23 5 -9 8 8789.02 1120.09 8 5 9 -8 9695.19 1197.74 29 5 -9 8 6530.90 978.991 2 5 -9 8 5770.69 993.265 1 5 -9 7 3054.29 766.749 8 -5 -9 -7 2672.48 792.157 15 5 9 -7 2778.83 814.357 29 5 -9 7 3512.79 798.472 1 5 9 -7 3533.97 698.912 23 5 -9 7 2492.57 692.774 2 5 -9 6 1929.16 704.229 1 5 9 -6 1231.14 532.040 23 5 -9 6 1636.75 566.785 2 5 9 -6 1671.64 708.514 29 5 9 -5 5962.71 935.997 29 5 -9 5 4802.67 883.968 1 -5 -9 -5 5522.35 956.666 18 5 -9 4 1278.55 595.575 1 5 9 -4 1644.65 664.271 29 5 9 -3 32686.0 1920.39 29 5 -9 3 30371.1 1836.65 1 5 -9 3 36511.8 1912.00 3 5 -9 2 7769.67 945.788 3 5 -9 2 8353.55 1040.26 1 5 9 -2 6830.18 969.783 29 5 -9 1 7348.36 958.936 1 5 9 -1 8329.65 1073.93 29 5 -9 1 7760.74 947.406 3 5 -9 0 2994.46 746.586 3 5 9 0 4360.63 869.828 29 5 9 1 8542.35 1044.63 29 5 -9 -1 8240.16 1007.46 3 5 -9 -2 7689.82 950.906 3 5 9 2 7825.24 1001.45 29 5 9 3 33476.4 1872.76 29 5 -9 -3 31668.7 1773.32 3 5 -9 -4 459.176 515.263 3 5 9 4 56.0564 498.770 29 5 9 5 5383.89 903.541 29 5 -9 -5 4964.46 851.757 3 -5 9 -5 5616.71 1016.35 17 5 -9 -6 1859.35 792.726 27 5 9 6 1944.48 655.003 29 5 -9 -6 307.743 509.188 7 -5 9 -6 1913.06 760.013 19 5 -9 -6 1275.70 565.289 3 -5 9 -6 1170.83 716.558 17 -5 9 -7 2668.76 899.670 17 5 -9 -7 4441.61 924.624 27 5 -9 -7 3439.99 759.560 7 -5 9 -7 2823.22 668.893 22 -5 9 -7 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912.614 8 -7 10 -3 5515.66 1142.80 19 -7 -10 3 3433.88 817.558 18 -7 10 -3 4729.49 1029.21 17 7 -10 -4 1406.07 604.916 8 -7 10 -4 1694.24 755.968 19 -7 -10 4 748.160 598.473 18 -7 10 -4 932.689 691.691 17 7 -10 -5 1044.37 659.429 8 -7 10 -5 2301.97 918.696 19 -7 -10 5 1903.33 833.290 18 -7 10 -5 1401.82 757.131 17 7 -10 -6 6853.13 1016.53 8 -7 10 -6 5563.79 1084.58 19 -7 -10 6 5570.40 975.190 18 -7 10 -6 4922.42 1018.18 17 7 -10 -6 6435.94 1132.84 27 7 -10 -7 405.879 564.090 8 7 -10 -7 561.437 509.828 7 -7 10 -7-307.229 603.083 19 -7 -10 7-405.478 576.694 18 -7 10 -7 1116.01 749.923 17 7 -10 -7 522.854 627.917 27 7 -10 -8 449.122 591.033 8 7 -10 -8-172.705 620.377 7 -7 10 -8 141.869 643.481 19 -7 10 -8 304.852 571.794 17 7 -10 -8 69.2871 667.598 27 7 -10 -9 1268.20 656.151 8 7 -10 -9 145.789 515.200 7 -7 10 -9 904.903 604.291 19 -7 10 -9 573.526 628.795 17 7 -10 -9 93.5096 751.996 27 7 -10 -10-143.219 524.978 8 7 -10 -10-687.129 619.351 7 -7 10 -10 307.820 610.501 17 7 -10 -10 426.832 753.229 27 7 -10 -11 4399.88 1012.94 25 7 -10 -11 4722.90 902.076 8 7 -10 -11 4601.77 849.050 7 -7 10 -11 4758.49 982.351 17 7 -10 -11 6979.24 1225.05 27 7 -10 -12 3592.47 989.833 25 7 -10 -12 3400.78 802.467 8 -7 10 -12 2574.00 687.213 24 7 -10 -12 2832.12 656.672 7 -7 10 -12 2230.19 799.363 17 7 -10 -12 3861.86 970.804 27 7 -10 -13 675.278 651.071 25 7 -10 -13-131.984 540.486 8 -7 10 -13 32.8212 457.702 24 -7 10 -13 273.382 559.296 17 7 -10 -13 788.031 691.943 27 7 -10 -14 1628.36 597.417 8 7 -10 -14 2172.66 832.196 25 -7 10 -14 756.806 532.638 24 -7 10 -14 2418.21 717.078 17 7 -10 -14 3808.68 896.709 27 7 -10 -15 3293.49 696.863 8 7 -10 -15 1592.77 675.242 25 -7 10 -15 423.293 430.697 24 -7 10 -15 1676.38 591.963 17 7 -10 -15 3417.19 789.122 27 7 -10 -16 891.136 549.144 25 -7 10 -16 1567.41 574.963 17 7 -10 -16 1161.89 625.479 27 7 -10 -17 4064.97 758.344 25 -7 10 -17 4783.29 765.933 17 7 -10 -17 5014.72 881.242 27 7 -10 -18 1739.53 599.708 25 -7 10 -18 1342.13 526.578 17 7 -10 -18 3146.17 672.054 27 7 -10 -19 2016.89 437.908 25 -7 10 -19 2132.08 512.562 17 7 -10 -19 1964.20 551.304 27 7 -10 -20 1849.32 450.459 27 -7 10 -20 969.919 374.723 17 7 11 -18 337.235 323.115 23 -7 -11 -18 318.972 441.447 15 7 11 -17 617.356 406.001 23 7 -11 17 752.897 527.395 16 -7 -11 -17 1556.75 567.148 15 7 11 -16 2431.58 582.913 23 -7 -11 -16 2051.21 630.107 15 7 11 -15 2871.66 647.133 23 -7 -11 -15 2100.07 693.705 15 7 11 -14 2383.49 607.959 23 -7 -11 -14 1408.48 639.839 15 -7 -11 -13 1263.69 665.199 15 7 11 -13 406.449 548.076 23 -7 -11 -12 2084.28 714.309 15 7 11 -12 2470.60 704.411 23 -7 -11 -11 793.028 620.851 15 7 11 -11 1080.80 593.625 23 -7 -11 -10 1139.18 609.727 15 7 11 -10 2225.24 664.557 23 7 -11 10 2489.53 756.527 9 -7 -11 -9 3102.44 846.244 15 7 11 -9 1830.32 704.605 23 7 -11 9 2797.69 741.263 9 -7 -11 -8 1733.57 745.876 15 7 11 -8 1154.50 609.301 23 7 -11 8 2197.32 749.792 9 7 -11 7 1046.69 558.869 8 -7 -11 -7 941.794 540.017 15 7 11 -7 1189.02 615.682 23 7 -11 6 1936.60 654.443 8 -7 -11 -6 1279.07 639.627 15 7 11 -6 2579.09 738.542 23 7 -11 5 1942.39 693.523 8 -7 -11 -5 1673.48 683.423 15 7 11 -5 2417.15 762.982 23 7 -11 4-226.513 610.867 8 -7 -11 -4 112.132 562.002 15 7 11 -4 916.430 502.668 23 7 -11 3 4922.40 951.887 8 -7 -11 -3 5623.35 1064.69 15 7 11 -3 4140.88 874.942 23 -7 -11 -2 4169.33 893.045 15 7 -11 2 4178.34 926.606 8 7 11 -2 5476.46 873.960 23 -7 11 2 2721.23 842.989 17 7 -11 1 1691.46 802.928 8 7 11 -1 2812.83 667.715 23 -7 11 1 1070.53 741.464 17 7 11 0 7922.24 1028.28 23 -7 -11 0 9749.63 1259.38 18 -7 11 0 8222.79 1279.22 17 7 -11 0 9413.57 1232.52 8 7 -11 -1 1381.92 664.570 8 -7 -11 1 2322.30 777.132 18 -7 11 -1 2174.70 813.367 17 7 -11 -2 2989.57 836.741 8 -7 11 -2 5977.73 1068.80 22 -7 11 -2 5069.64 1086.71 19 -7 -11 2 4746.70 928.489 18 -7 11 -2 2634.32 860.679 17 7 -11 -3 3888.05 898.290 8 -7 11 -3 4975.26 1040.35 22 -7 11 -3 2106.78 870.771 19 -7 -11 3 4588.48 1023.66 18 -7 11 -3 3907.28 987.017 17 7 -11 -4-537.297 548.733 8 -7 11 -4-389.711 544.094 22 -7 11 -4-177.733 702.925 19 -7 -11 4 663.246 622.336 18 -7 11 -4-613.373 629.986 17 7 -11 -5 588.554 626.815 8 -7 11 -5-252.400 630.077 19 -7 -11 5-18.5241 668.040 18 -7 11 -5 530.735 619.822 17 7 -11 -6 2007.24 713.259 8 -7 11 -6 2260.16 821.112 19 -7 -11 6 1324.79 684.813 18 -7 11 -6 2569.02 871.651 17 7 -11 -7 1055.67 735.246 8 -7 11 -7-381.923 571.090 19 -7 -11 7 1368.69 650.549 18 -7 11 -7 1342.40 706.251 17 7 -11 -7-648.938 689.793 27 7 -11 -8 1624.91 665.854 8 -7 11 -8 745.306 737.279 19 -7 -11 8 1011.15 672.278 18 -7 11 -8 466.367 640.742 17 7 -11 -8 1992.89 757.435 27 7 -11 -9 1924.46 720.969 8 -7 11 -9 998.824 760.551 19 -7 -11 9 2963.68 797.310 18 -7 11 -9 2656.36 765.143 17 7 -11 -9 2153.13 828.194 27 7 -11 -10 2224.97 652.047 8 7 -11 -10 1374.55 783.021 25 -7 11 -10 1625.00 719.008 17 7 -11 -10 1015.75 701.681 27 7 -11 -11-172.329 458.821 8 7 -11 -11 512.339 647.282 25 7 -11 -11-297.396 626.257 27 -7 11 -11 387.817 588.553 17 7 -11 -12 2632.65 735.025 8 7 -11 -12 2323.94 862.913 25 -7 11 -12 2508.30 769.369 17 7 -11 -12 2275.04 738.695 27 7 -11 -13-242.834 476.791 8 7 -11 -13-392.629 619.700 25 -7 11 -13-274.794 530.608 17 7 -11 -13 79.3949 586.438 27 7 -11 -14 2595.64 677.829 8 7 -11 -14 733.752 602.878 25 -7 11 -14 1936.59 647.196 17 7 -11 -14 1691.51 711.565 27 7 -11 -15 2704.55 745.261 25 -7 11 -15 2222.37 641.915 17 7 -11 -15 2908.01 772.435 27 7 -11 -16 2240.75 672.630 25 -7 11 -16 2559.89 637.745 17 7 -11 -16 2766.99 729.951 27 7 -11 -17 279.320 456.010 25 -7 11 -17 608.981 469.809 17 7 -11 -17 1212.51 559.969 27 7 -11 -18 272.919 361.247 25 -7 11 -18 3.48127 385.133 17 7 -11 -18 126.808 424.858 27 7 -11 -19-114.864 344.629 27 -7 11 -19 48.5630 303.190 17 -7 11 -20 728.509 282.820 17 7 12 -18 380.790 288.157 23 7 -12 18 344.045 381.533 16 7 12 -17-44.3057 381.178 23 7 -12 17-16.9339 412.719 16 -7 -12 -17 535.433 398.232 15 7 12 -16 984.422 453.559 23 7 -12 16 587.686 523.253 16 -7 -12 -16 1199.37 475.785 15 7 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1864.82 612.643 17 7 -12 -14 1318.11 654.866 27 7 -12 -15 757.453 551.029 25 -7 12 -15 1036.23 505.895 17 7 -12 -15-442.864 548.118 27 7 -12 -16 1825.24 626.736 25 -7 12 -16 251.093 406.994 17 7 -12 -16 860.802 471.205 27 7 -12 -17 493.031 496.739 25 -7 12 -17-254.085 405.224 17 7 -12 -17-463.664 472.545 27 7 -12 -18 1175.09 425.523 25 -7 12 -18 389.192 352.553 17 -7 12 -19 1557.29 357.248 17 7 13 -17-464.114 320.950 23 7 -13 17 298.512 375.121 16 7 13 -16 1247.65 479.887 23 7 -13 16 1675.34 565.862 16 -7 -13 -16 1801.79 495.601 15 7 13 -15 4749.01 696.703 23 7 -13 15 4507.06 776.806 16 -7 -13 -15 5477.09 757.311 15 7 13 -14 221.494 425.610 23 7 -13 14 307.635 518.071 16 -7 -13 -14 213.328 453.740 15 7 13 -13 719.415 482.757 23 -7 -13 -13 936.095 504.010 15 7 13 -12 206.761 501.875 23 -7 -13 -12 146.980 449.107 15 7 13 -11-72.2106 491.940 23 -7 -13 -11 1025.68 582.915 15 -7 -13 -10 2565.71 718.882 15 7 13 -10 1640.11 614.281 23 7 -13 10 1849.27 639.619 9 -7 -13 -9 1124.95 661.245 15 7 13 -9 1390.17 626.997 23 7 -13 9 1391.64 685.486 9 -7 -13 -8 732.941 537.193 15 7 13 -8 796.679 548.304 23 7 -13 8 1382.96 701.315 9 -7 -13 -7 1888.40 710.150 15 7 13 -7 1275.78 593.052 23 7 -13 7 1521.69 791.130 9 -7 -13 -6 1988.02 660.546 15 7 13 -6 1156.33 575.469 23 7 -13 6 1949.56 720.477 9 7 -13 5 1113.33 715.956 8 -7 -13 -5 2279.56 642.775 15 7 13 -5 907.741 549.853 23 7 -13 4 2523.87 726.554 8 7 13 -4 2258.71 725.958 23 -7 13 4 760.728 676.844 17 7 13 -3 9144.49 1067.73 23 -7 13 3 7646.91 1215.07 17 7 -13 3 8280.80 1122.37 8 7 -13 2 1382.63 689.547 8 7 13 -2 2300.75 646.042 23 -7 13 2 2574.93 847.018 17 7 -13 1 1012.77 630.121 8 7 13 -1 512.030 471.952 23 -7 13 1 600.233 624.782 17 -7 -13 0 5855.62 992.737 18 -7 13 0 7193.98 1199.73 17 7 -13 0 7158.15 1073.39 8 7 -13 -1 898.825 719.701 8 -7 13 -1 3029.20 766.588 22 -7 13 -1 926.345 790.461 19 -7 -13 1 1656.62 566.387 18 -7 13 -1 51.7728 683.812 17 7 -13 -2 2163.46 841.563 8 -7 13 -2 833.077 650.591 22 -7 13 -2 1854.24 836.770 19 -7 -13 2 3326.41 820.474 18 -7 13 -2 1879.85 804.960 17 -7 13 -3 9085.82 1319.24 22 -7 13 -3 9599.21 1437.60 19 -7 -13 3 9185.95 1184.93 18 -7 13 -3 9291.75 1284.27 17 7 -13 -3 10220.2 1200.85 8 7 -13 -4 2010.10 744.774 8 -7 13 -4 428.900 479.017 22 -7 13 -4 1925.41 797.183 19 -7 -13 4 2880.39 765.017 18 -7 13 -4 1129.15 735.713 17 7 -13 -5 1081.73 606.573 8 7 -13 -5 557.228 645.399 25 -7 13 -5 1976.62 675.996 22 -7 13 -5 1413.40 730.791 19 -7 -13 5 2213.76 700.440 18 -7 13 -5 2233.75 803.728 17 7 -13 -6 737.529 568.882 8 7 -13 -6 2182.09 792.618 25 -7 13 -6 1365.33 495.917 22 -7 13 -6 1102.35 674.189 19 -7 -13 6 960.596 630.366 18 -7 13 -6 1546.77 737.675 17 7 -13 -7 1438.20 685.352 8 7 -13 -7 1465.23 760.666 25 -7 13 -7 3574.70 863.312 22 -7 13 -7 2562.85 873.562 19 -7 -13 7 832.275 613.139 18 -7 13 -7 2089.44 768.698 17 7 -13 -8 775.385 549.240 8 7 -13 -8 1304.06 731.552 25 -7 13 -8 1557.91 681.400 22 -7 13 -8 953.126 634.270 19 -7 -13 8 797.584 639.762 18 -7 13 -8 1178.29 663.269 17 7 -13 -9 919.555 537.585 8 7 -13 -9 1210.84 747.153 25 -7 13 -9 1204.68 667.323 22 -7 -13 9 1091.64 631.226 18 -7 13 -9 679.127 613.297 17 7 -13 -10 1888.21 619.155 8 7 -13 -10 1511.90 722.489 25 -7 -13 10 1930.13 649.150 18 -7 13 -10 1124.11 617.546 17 7 -13 -11-312.949 475.355 8 7 -13 -11 1723.35 757.952 25 -7 -13 11 1262.53 590.334 18 -7 13 -11 1532.23 655.203 17 7 -13 -12 942.210 497.161 8 7 -13 -12 1325.42 719.607 25 -7 13 -12 69.2508 458.857 17 7 -13 -13 561.187 483.306 8 7 -13 -13 1787.18 661.384 25 -7 13 -13 697.224 527.851 17 7 -13 -14 240.690 559.784 25 -7 13 -14 217.807 420.137 17 7 -13 -15 3920.76 808.679 25 -7 13 -15 4288.76 709.708 17 7 -13 -16 1812.60 581.247 25 -7 13 -16 2091.30 534.439 17 7 -13 -17-286.271 395.503 25 -7 13 -17-8.92480 296.241 17 -7 13 -18 1411.51 359.551 17 7 -14 17 913.795 377.475 16 7 14 -16 313.726 322.839 23 7 -14 16-300.072 432.800 16 7 14 -15 1824.18 486.860 23 7 -14 15 737.330 491.659 16 7 14 -14 320.799 409.337 23 7 -14 14 697.275 525.255 16 -7 -14 -14-85.6286 366.219 15 7 14 -13 860.282 464.834 23 7 -14 13 574.379 450.000 16 -7 -14 -13 1086.91 468.415 15 7 14 -12 535.155 469.473 23 7 -14 12 681.327 564.400 16 -7 -14 -12 1550.33 540.348 15 7 14 -11 981.826 500.848 23 7 -14 11 204.791 496.582 9 -7 -14 -11-68.8243 411.687 15 7 14 -10 3305.88 717.866 23 7 -14 10 2802.13 710.039 9 -7 -14 -10 2708.54 677.012 15 7 14 -9 1949.57 622.315 23 7 -14 9 2245.21 631.823 9 -7 -14 -9 2107.60 631.666 15 -7 -14 -8 937.310 590.572 15 7 14 -8 1507.74 571.080 23 7 -14 8 2369.84 726.177 9 7 14 -7 4024.60 784.674 23 -7 14 7 4658.87 949.179 17 7 -14 7 4899.39 936.339 9 7 14 -6 1284.83 599.105 23 7 -14 6 1829.95 724.749 9 7 14 -5 2251.58 631.580 23 -7 14 5 2416.31 787.958 17 7 -14 5 1710.42 718.495 9 7 14 -4 999.712 548.815 23 -7 14 4 620.351 641.100 17 7 -14 4-620.750 578.117 9 7 -14 4 719.276 595.128 8 7 -14 3 389.150 573.149 8 7 14 -3 285.827 372.569 23 -7 14 3-745.068 687.717 17 7 -14 2 424.565 568.103 8 7 14 -2 313.664 432.316 23 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1593.20 590.477 8 7 -15 -7 145.021 515.424 25 -7 15 -7 816.550 549.974 22 -7 15 -7 140.372 547.011 19 -7 -15 7-758.323 545.388 18 -7 15 -7 53.0435 520.130 17 7 -15 -7-489.939 507.628 9 7 -15 -8 248.555 497.286 8 7 -15 -8 184.713 521.954 25 -7 15 -8 1031.99 606.409 22 -7 -15 8 1117.44 587.583 18 -7 15 -8 69.2704 448.857 17 7 -15 -8 221.271 474.765 9 7 -15 -9 3118.21 659.190 8 7 -15 -9 2223.34 708.182 25 -7 -15 9 3345.58 688.444 18 -7 15 -9 3850.11 814.319 17 7 -15 -9 3278.24 670.660 9 7 -15 -10 750.740 514.848 8 7 -15 -10 753.662 597.643 25 -7 -15 10 84.0705 481.172 18 -7 15 -10-372.422 484.561 17 7 -15 -10-146.852 342.115 9 7 -15 -11 539.925 437.636 8 7 -15 -11 313.524 489.166 25 -7 -15 11 1652.68 529.885 18 -7 15 -11 790.379 478.967 17 7 -15 -12 574.732 510.948 25 -7 15 -12 503.876 454.579 17 7 -15 -12-666.931 275.097 8 7 -15 -13 2010.87 628.769 25 -7 15 -13 1806.65 563.157 17 7 -15 -14 705.769 460.999 25 -7 15 -14 718.799 414.686 17 7 -15 -15 1476.50 518.412 25 -7 15 -15 1320.63 386.643 17 7 -15 -16 289.920 320.201 25 7 -16 15 787.973 356.132 16 7 16 -14 1344.71 370.943 23 7 -16 14 671.373 408.987 16 7 16 -13-400.665 369.113 23 7 -16 13 43.2976 369.057 16 7 16 -12-327.503 408.557 23 7 -16 12-54.9896 439.109 16 7 16 -11 2196.48 556.079 23 -7 16 11 1957.03 559.740 17 7 -16 11 2575.97 578.298 16 7 16 -10 1169.68 483.699 23 -7 16 10 915.528 485.425 17 7 -16 10 772.226 456.894 9 7 -16 10 641.016 490.883 16 7 16 -9 1044.55 433.290 23 -7 16 9-166.315 482.584 17 7 -16 9 198.645 452.425 9 7 -16 9 57.9923 423.942 16 7 16 -8 233.126 395.845 23 -7 16 8 1338.86 548.897 17 7 -16 8 245.021 526.792 9 7 -16 8 625.829 472.040 16 7 16 -7 1764.40 534.498 23 -7 16 7 2817.92 700.851 17 7 -16 7 2007.21 657.727 9 7 -16 7 2475.97 661.566 16 7 16 -6 665.091 449.005 23 -7 16 6 331.722 508.909 17 7 -16 6 268.956 557.798 9 7 -16 6-626.541 507.162 16 7 16 -5 1147.31 495.582 23 -7 16 5 775.268 518.249 17 7 -16 5 594.213 548.630 9 7 -16 5 365.486 535.614 16 7 16 -4 273.218 396.767 23 -7 16 4-30.3143 687.772 19 -7 16 4 1467.71 611.545 17 7 -16 4 959.784 557.750 16 7 -16 4 289.331 552.470 9 7 16 -3 18.2718 375.158 23 -7 16 3 901.629 680.450 19 -7 16 3 445.241 566.763 17 7 -16 3-45.5022 463.104 16 7 -16 3 508.979 566.889 9 7 16 -2 358.795 450.189 23 -7 16 2-50.2557 535.282 22 -7 16 2-406.480 621.403 19 -7 16 2 370.229 607.093 17 7 -16 2 704.249 601.096 9 -7 16 1 1298.78 631.155 22 -7 16 1 898.337 666.846 19 -7 16 1 1164.64 676.756 17 7 -16 1 1128.81 529.333 9 -7 16 0 6895.81 1124.61 22 -7 16 0 6573.81 1161.12 19 -7 16 0 7001.55 1048.86 17 7 -16 0 7858.74 1050.25 9 7 -16 0 7261.75 1021.88 8 7 -16 -1 929.495 587.870 8 -7 16 -1 1066.42 659.835 22 -7 16 -1 876.055 663.616 19 -7 16 -1-332.988 623.523 17 7 -16 -1 423.432 571.341 9 7 -16 -2 1361.13 551.060 8 7 -16 -2 761.617 469.897 25 -7 16 -2 189.885 519.117 22 -7 16 -2 628.433 667.674 19 -7 -16 2-133.226 481.362 18 -7 16 -2 642.990 538.830 17 7 -16 -2-61.2314 508.154 9 7 -16 -3 1214.74 565.594 8 7 -16 -3 1406.25 618.604 25 -7 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555.664 19 -7 17 8-236.885 343.347 17 7 -17 8 179.313 423.770 9 7 -17 8 16.2619 417.638 16 7 17 -7 2293.80 552.348 23 -7 17 7 1695.68 648.037 19 -7 17 7 2051.44 552.524 17 7 -17 7 2925.16 648.339 9 7 -17 7 2451.17 627.360 16 7 17 -6-264.864 363.682 23 -7 17 6 371.936 531.683 19 -7 17 6-628.473 459.019 17 7 -17 6 791.803 475.701 9 7 -17 6-9.39971 415.718 16 7 17 -5 81.8130 342.882 23 -7 17 5 512.995 583.616 19 -7 17 5 653.654 468.457 17 7 -17 5 629.217 511.602 9 7 -17 5 24.4154 490.413 16 7 17 -4-134.747 337.433 23 -7 17 4-102.597 501.654 22 -7 17 4 384.494 589.278 19 -7 17 4-353.716 480.091 17 7 -17 4 173.741 470.777 9 7 -17 4 869.554 472.415 16 7 17 -3 868.474 443.559 23 -7 17 3 1469.69 667.039 19 -7 17 3-82.0580 423.532 17 7 -17 3 799.671 562.200 9 -7 17 2-404.007 567.341 22 -7 17 2 55.6001 637.244 19 -7 17 2-104.756 468.237 17 7 -17 2 236.136 527.000 9 -7 17 1 1080.05 541.252 22 -7 17 1 1076.28 663.213 19 -7 17 1-4.72685 473.635 17 7 -17 1 350.017 543.665 9 -7 17 0 6620.66 1055.17 22 -7 17 0 6235.42 1077.35 19 -7 17 0 6810.47 888.275 17 7 -17 0 6354.23 966.565 9 -7 17 -1-99.5430 503.142 22 -7 17 -1 540.525 631.201 19 -7 17 -1-239.130 530.689 17 7 -17 -1 564.575 521.369 9 -7 17 -2 552.864 513.797 22 -7 17 -2 121.040 544.420 19 -7 17 -2-413.674 580.443 17 7 -17 -2-226.429 517.565 9 7 -17 -3 630.965 450.741 25 -7 17 -3 1105.99 606.707 22 -7 17 -3 1454.85 621.644 19 -7 17 -3 1211.72 631.052 17 7 -17 -3 1313.53 592.203 9 7 -17 -4 667.320 450.111 25 -7 17 -4-275.508 531.280 22 -7 17 -4-397.368 226.554 20 -7 17 -4 492.648 570.334 19 -7 -17 4 536.458 426.784 18 -7 17 -4 853.926 473.859 17 7 -17 -4 525.323 485.535 9 7 -17 -5 344.679 476.788 25 -7 17 -5 728.815 524.519 22 -7 17 -5 945.191 588.166 19 -7 -17 5 1210.51 526.520 18 -7 17 -5 828.998 501.009 17 7 -17 -5 1650.19 576.026 9 7 -17 -6 115.100 458.175 25 -7 17 -6-206.630 411.801 22 -7 -17 6 997.876 519.996 18 -7 17 -6 375.083 412.857 17 7 -17 -6 384.775 411.075 9 7 -17 -7 2296.36 584.531 25 -7 17 -7 2336.26 556.667 22 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585.552 15 9 7 -7 542.553 514.152 23 -9 -7 -6 512.300 651.481 15 9 7 -6 738.722 461.767 23 -9 7 6 441.050 561.342 17 -9 -7 -5 6311.91 1014.02 15 9 7 -5 7627.28 952.689 23 -9 7 5 7623.79 1158.83 17 9 -7 4 1955.14 699.739 8 -9 -7 -4 1230.38 605.030 15 9 7 -4 2064.88 694.898 23 -9 7 4 2121.23 708.900 17 9 -7 3 106.664 575.145 8 -9 -7 -3 681.001 538.927 15 9 7 -3 1279.50 563.987 23 -9 7 3 491.343 586.351 17 9 -7 2 1993.74 708.545 8 -9 -7 -2 1089.89 659.412 15 -9 7 2 734.033 720.701 15 9 7 -2 2733.18 667.494 23 -9 7 2 2616.22 788.382 17 -9 -7 -1 2388.15 780.164 15 9 -7 1 3541.18 846.717 8 -9 7 1 1527.69 765.523 15 9 7 -1 1950.89 635.582 23 -9 7 1 1954.20 820.380 17 -9 -7 0 849.839 652.581 15 9 -7 0 577.900 541.193 8 -9 7 0 414.742 650.754 15 9 7 0 1082.88 592.234 23 -9 7 0 939.132 704.302 17 -9 -7 1 913.619 672.639 15 9 -7 -1 3085.75 826.215 8 -9 7 -1 1362.92 796.377 15 -9 7 -1 1696.07 744.224 17 -9 -7 2 1741.78 785.237 15 9 -7 -2 2297.46 743.810 8 -9 7 -2 2160.42 792.279 15 -9 7 -2 1149.26 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15 9 -8 -4 2725.65 686.169 8 -9 8 -4 1212.20 583.716 17 -9 -8 5 1130.15 571.431 15 9 -8 -5 1343.71 664.059 8 -9 8 -5 1304.88 698.237 17 9 -8 -6 1614.81 659.530 8 -9 8 -6 2521.90 725.011 17 9 -8 -7 3430.58 759.177 8 -9 8 -7 2727.40 761.992 17 9 -8 -8 5105.37 867.865 8 -9 8 -8 5293.01 897.433 17 9 -8 -9 2826.36 696.324 8 -9 8 -9 3233.49 741.551 17 9 -8 -10 531.521 545.573 25 -9 8 -10 1241.95 532.052 17 9 -8 -11 2732.65 636.430 8 9 -8 -11 1315.59 599.498 25 -9 8 -11 2112.48 577.166 17 9 -8 -12 2342.96 607.352 8 9 -8 -12 2535.15 652.345 25 -9 8 -12 3079.31 612.996 17 9 -8 -13 710.651 498.890 8 9 -8 -13 166.510 435.128 25 -9 8 -13 1028.12 426.121 17 9 -8 -14-256.909 369.230 8 9 -8 -14 227.301 472.086 25 -9 8 -14 896.758 374.676 17 -9 -9 -15 544.701 316.783 15 9 9 -14 421.598 312.836 23 -9 9 14-62.4244 339.867 17 -9 -9 -14 44.8709 345.643 15 9 9 -13 884.821 385.934 23 -9 9 13 928.505 473.259 17 -9 -9 -13 806.366 434.496 15 -9 -9 -12 474.641 464.897 15 9 9 -12 937.961 472.579 23 9 9 -12 601.772 277.914 7 -9 9 12 985.944 538.755 17 -9 -9 -11 941.895 486.428 15 9 9 -11 529.560 416.757 23 -9 9 11 1653.39 576.754 17 -9 -9 -10 1059.47 532.086 15 9 9 -10-233.116 446.682 23 -9 9 10 306.621 484.865 17 -9 -9 -9 849.496 543.475 15 9 9 -9 523.440 464.709 23 -9 -9 -8 918.659 511.567 15 9 9 -8 1186.12 507.666 23 -9 9 8 1701.82 634.410 17 -9 -9 -7 1521.56 637.021 15 9 9 -7 2534.20 599.509 23 -9 9 7 2105.71 723.753 17 9 -9 7 2118.61 685.778 9 -9 -9 -6 2864.73 686.550 15 9 9 -6 4097.86 728.119 23 -9 9 6 2773.19 798.380 17 9 -9 5 4187.35 759.901 8 -9 -9 -5 2240.81 670.832 15 9 9 -5 3168.41 691.944 23 -9 9 5 3173.52 820.903 17 9 -9 4 2122.03 655.717 8 -9 -9 -4 1896.92 690.911 15 9 9 -4 2627.77 626.138 23 -9 9 4 3524.46 817.773 19 -9 9 4 1811.99 720.760 17 9 -9 3 1023.89 564.969 8 -9 -9 -3 1937.76 683.387 15 -9 9 3 1158.39 660.134 15 9 9 -3 1694.87 573.418 23 -9 9 3 1555.13 676.656 19 -9 9 3 2145.61 806.589 17 9 -9 2 4073.63 839.927 8 -9 -9 -2 3520.60 789.975 15 -9 9 2 1946.13 682.155 15 9 9 -2 4104.45 735.565 23 -9 9 2 3100.93 755.774 19 -9 9 2 3614.07 896.371 17 9 -9 1 1416.94 621.880 8 -9 -9 -1 995.213 554.378 15 -9 9 1 181.312 615.626 15 9 9 -1 1290.77 476.649 23 -9 9 1-942.286 614.276 19 -9 9 1 992.074 646.137 17 -9 -9 0 326.451 511.231 15 9 -9 0 441.889 539.506 8 -9 9 0 148.657 610.193 15 -9 9 0-555.292 592.348 17 -9 -9 1 1932.40 674.290 15 9 -9 -1 741.453 559.251 8 -9 9 -1 1104.10 540.919 15 -9 9 -1 1668.53 728.222 17 -9 -9 2 2434.33 678.090 15 9 -9 -2 3663.48 852.120 8 -9 9 -2 4168.47 902.487 17 -9 -9 3-78.6995 396.025 15 9 -9 -3 1642.75 671.374 8 -9 9 -3 1624.78 682.884 17 9 -9 -4 2923.28 750.220 8 -9 9 -4 2054.73 733.547 17 9 -9 -5 3753.48 774.242 8 -9 9 -5 2942.73 788.742 17 9 -9 -6 4468.91 858.765 8 -9 9 -6 3110.69 780.318 17 9 -9 -7 2117.55 674.792 8 -9 9 -7 1475.17 671.325 17 9 -9 -8-18.2623 518.514 8 -9 9 -8 684.803 551.703 17 9 -9 -9 450.995 543.247 8 9 -9 -9 884.647 542.878 25 -9 9 -9 1399.81 613.190 17 9 -9 -10 774.313 496.520 8 9 -9 -10 340.748 535.499 25 -9 9 -10 2.16925 473.383 17 9 -9 -11 1274.93 514.809 8 9 -9 -11 337.710 541.655 25 -9 9 -11 1591.65 507.347 17 9 -9 -12 1298.50 546.833 8 9 -9 -12 1661.57 549.061 25 -9 9 -12 416.354 407.264 17 9 -9 -13-29.0135 316.890 8 9 -9 -13 334.815 379.595 25 -9 9 -13 740.206 398.218 17 9 -9 -14-145.881 342.149 25 -9 9 -14-255.596 322.161 17 9 10 -14 1736.43 352.832 23 9 -10 14 1486.28 382.369 16 9 10 -13 328.029 309.095 23 -9 10 13-50.0620 357.855 17 -9 -10 -13 662.429 364.801 15 9 10 -12 653.874 382.366 23 -9 10 12 275.873 440.014 17 -9 -10 -12 1147.44 431.367 15 -9 -10 -11 515.579 430.925 15 9 10 -11 554.756 439.888 23 -9 10 11 1049.75 550.504 17 -9 -10 -10-152.703 375.938 15 9 10 -10 3.22849 339.706 23 -9 10 10-106.507 455.689 17 -9 -10 -9 239.135 422.851 15 9 10 -9 592.002 434.764 23 -9 10 9 320.690 492.647 17 -9 -10 -8 2365.13 607.494 15 9 10 -8 2402.27 604.998 23 -9 10 8 1521.25 667.998 17 -9 -10 -7 139.580 420.277 15 9 10 -7 889.039 430.788 23 -9 10 7 634.926 596.842 17 9 -10 7 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216.658 410.207 17 -10 -9 -5 30.2032 381.957 15 -10 9 5-318.308 412.182 15 -10 9 5-961.527 475.553 17 10 -9 5-549.368 407.305 9 -10 -9 -4 727.781 412.868 15 -10 9 4 1079.29 472.614 15 -10 9 4 658.549 507.988 17 10 -9 4 709.792 446.893 9 -10 -9 -3 788.981 458.204 15 -10 9 3 1262.53 457.970 15 -10 9 3 931.283 514.040 17 -10 -9 -2 137.274 402.215 15 -10 9 2-677.355 423.192 15 10 -9 2 149.747 366.605 8 10 -9 1 45.1903 374.821 8 -10 -9 -1-917.806 327.964 15 -10 9 1 459.449 433.271 17 10 -9 0 32.0901 400.288 8 -10 -9 0 47.9410 184.951 15 -10 9 0 507.431 456.274 17 10 -9 -1 1263.22 432.354 8 -10 9 -1 664.553 504.403 17 10 -9 -2-1009.26 505.688 8 -10 9 -2 104.505 427.880 17 10 -9 -3 1265.85 524.649 8 -10 9 -3 1186.05 509.940 17 10 -9 -4 885.374 490.474 8 -10 9 -4 157.947 456.992 17 10 -9 -5 907.033 470.540 8 10 -9 -5 68.8966 435.366 25 -10 9 -5-115.085 334.586 17 10 -9 -6 133.379 372.386 8 10 -9 -6 566.037 469.265 25 -10 9 -6 564.166 368.959 17 10 -9 -7 410.204 426.824 8 10 -9 -7-43.9468 414.111 25 -10 9 -7 76.1636 327.441 17 10 -9 -8 1230.10 422.503 8 10 -9 -8 827.483 423.967 25 -10 9 -8 1395.87 379.023 17 10 -9 -9 571.318 342.707 8 10 -9 -9 490.958 368.415 25 -10 10 7 1245.87 425.313 17 -10 10 6 292.125 365.442 17 -10 10 5 60.4854 356.754 17 -10 10 4 92.4320 408.608 17 10 -10 4 628.539 354.373 9 -10 10 3 577.501 410.949 17 10 -10 3 1085.07 452.765 9 -10 10 2 211.042 416.756 17 10 -10 2 842.494 472.193 9 10 -10 1 2548.26 492.278 25 -10 10 1 1465.97 530.996 17 10 -10 0 2780.31 538.460 8 10 -10 0 1231.81 462.120 25 -10 10 0 1955.77 537.288 17 10 -10 -1 1699.70 494.481 8 10 -10 -1 1320.65 499.352 25 -10 10 -1 1164.16 523.993 17 10 -10 -2 825.359 449.949 8 10 -10 -2 1084.58 453.303 25 -10 10 -2 658.295 444.148 17 10 -10 -3 1455.48 475.688 8 10 -10 -3 28.9619 435.807 25 -10 10 -3 1524.38 484.428 17 10 -10 -4 635.462 398.956 8 10 -10 -4 210.004 385.810 25 -10 10 -4 37.9421 314.801 17 10 -10 -5-581.273 381.357 8 10 -10 -5-34.9788 399.682 25 -10 10 -5 249.370 350.637 17 10 -10 -6 271.964 378.401 8 10 -10 -6-211.914 351.968 25 -10 10 -6-261.133 311.758 17 10 -10 -7 2351.31 451.213 8 10 -10 -7 2050.42 496.123 25 -10 10 -7 729.977 369.427 17 10 -10 -8 236.010 275.891 8 10 -10 -8-279.981 319.882 25 -10 11 5 469.662 311.027 17 -10 11 4 321.899 336.578 17 -10 11 3 299.491 353.129 17 10 -11 3 1515.71 405.669 9 -10 11 2-572.602 389.652 17 10 -11 2-592.704 382.347 9 -10 11 1 237.857 406.279 17 10 -11 1 331.443 395.587 9 -10 11 0 512.206 404.020 17 10 -11 0 63.7586 367.847 9 -10 11 -1 461.419 411.655 17 10 -11 -1 199.268 370.410 9 10 -11 -2 355.839 366.587 8 10 -11 -2 401.180 323.633 25 -10 11 -2 44.6814 334.332 17 10 -11 -2 170.717 392.668 9 10 -11 -3 973.726 396.806 8 10 -11 -3 503.883 334.607 25 -10 11 -3 28.5082 320.599 17 10 -11 -4 1688.12 443.375 8 10 -11 -4 1363.94 400.821 25 -10 11 -4 1253.59 370.685 17 10 -11 -4 1560.74 447.815 9 10 -11 -5-55.3207 299.000 8 10 -11 -5 611.240 378.303 25 -10 11 -5 429.899 302.037 17 10 -11 -5 466.852 340.691 9 10 -11 -6 255.919 326.861 8 -10 12 2 248.444 282.038 17 -10 12 1 675.987 360.721 17 -10 12 0 541.012 383.169 17 10 -12 0 549.263 331.765 9 -10 12 -1 967.725 371.600 17 10 -12 -1 769.497 394.347 9 -10 12 -2 272.895 291.379 17 10 -12 -2 838.349 374.689 9 10 -12 -3 646.975 349.772 9 -11 0 0 471.465 405.839 15 -11 0 -1 283.694 390.413 15 -11 0 1 1293.46 478.992 15 -11 0 -2 889.250 432.825 15 -11 0 2 571.300 454.659 15 -11 0 3 3900.03 711.604 15 -11 0 -3 4972.11 664.505 15 -11 0 -4 327.844 393.196 15 -11 0 4 299.233 405.675 15 -11 0 -5-109.446 360.548 15 -11 0 5-40.6721 388.673 15 -11 0 -6 3449.49 517.121 15 -11 0 6 3133.67 551.244 15 -11 -1 -6 302.091 332.772 15 -11 1 6-185.160 385.219 15 -11 -1 -5 1637.16 425.867 15 -11 1 5 683.095 443.641 15 -11 -1 -4 2529.07 511.110 15 -11 1 4 2166.53 573.117 15 -11 -1 -3 3540.52 594.291 15 -11 1 3 2101.69 561.549 15 -11 -1 -2 4309.86 645.220 15 -11 1 2 3867.49 663.977 15 -11 -1 -1 785.815 411.478 15 -11 1 1 935.313 486.353 15 -11 -1 0 1802.74 542.766 15 -11 1 0 3188.83 576.442 15 -11 1 -1 5.20642 420.449 15 -11 -1 1 609.635 458.496 15 -11 1 -2 3229.07 621.648 15 -11 -1 2 4596.79 696.702 15 -11 1 -3 2280.87 511.586 15 -11 -1 3 2265.56 570.386 15 -11 1 -4 2315.55 517.919 15 -11 -1 4 2077.72 522.322 15 -11 1 -5 1526.89 429.465 15 -11 -1 5 1248.53 485.198 15 -11 -1 6-52.5021 331.683 15 -11 -2 -6 949.016 385.678 15 -11 2 6 390.359 390.922 15 -11 -2 -5 662.470 360.189 15 -11 2 5 970.121 452.386 15 -11 -2 -4-500.021 401.159 15 -11 2 4 303.381 399.883 15 -11 -2 -3 538.100 414.538 15 -11 2 3 659.497 445.295 15 -11 -2 -2 1747.56 490.594 15 -11 2 2 1640.18 486.887 15 -11 -2 -1 1185.58 486.300 15 -11 2 1 877.527 476.303 15 -11 -2 0 1941.44 537.618 15 -11 2 0 2907.47 594.018 15 -11 -2 1 889.753 416.844 15 -11 2 -1 695.358 426.525 15 -11 2 -2 1001.01 507.835 15 -11 -2 2 1273.13 482.969 15 -11 2 -3 1048.74 423.092 15 -11 -2 3 1534.11 444.827 15 -11 2 -4 1078.99 402.575 15 -11 -2 4 906.413 410.746 15 -11 -2 5 268.905 319.688 15 -11 -3 -6 433.379 356.839 15 -11 3 6 190.542 345.227 15 -11 -3 -5 901.275 410.550 15 -11 3 5-128.886 345.960 15 -11 -3 -4 1264.61 390.379 15 -11 3 4 930.565 434.261 15 -11 -3 -3 1431.28 494.610 15 -11 3 3 1252.47 447.202 15 -11 -3 -2 157.222 379.154 15 -11 3 2 220.915 364.882 15 -11 -3 -1 836.607 479.737 15 -11 3 1 231.571 405.477 15 -11 -3 0 446.763 405.856 15 -11 3 0 420.439 405.083 15 -11 -3 1 601.456 393.812 15 -11 3 -1-181.887 396.744 15 -11 3 -2 274.085 309.999 15 -11 -3 2 547.778 384.450 15 -11 3 -3 1262.63 418.702 15 -11 -3 3 403.326 365.966 15 -11 -3 4-508.854 366.302 15 -11 -4 -5 1630.22 401.922 15 -11 -4 -4 719.912 380.301 15 -11 4 4 481.485 409.618 15 -11 -4 -3 618.614 364.243 15 -11 4 3 1.41490 367.910 15 -11 -4 -2 2510.98 491.947 15 -11 4 2 2447.64 510.693 15 -11 -4 -1 58.4983 330.306 15 -11 4 1-69.6876 352.736 15 -11 -4 0 181.902 380.365 15 -11 4 0 698.236 335.896 15 -11 -4 1 471.728 371.367 15 -11 4 -1 376.155 294.611 15 -11 -4 2 1536.09 420.098 15 -11 -5 -2 364.845 308.859 15 -11 -5 -1 74.0634 288.490 15 0 0 0 0.00 0.00 0 TITL exp_0232(ChinaLow4) in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 8.972983 20.917072 23.920065 90.0000 90.0000 90.0000 ZERR 20.00 0.000485 0.000897 0.001080 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 220.00 200.00 20.00 20.00 TREF HKLF 4 END ; _shelx_hkl_checksum 24620 _shelx_res_file ; TITL exp_0232(chinalow4)_a.res in P2(1)2(1)2(1) 0232.res created by SHELXL-2018/3 at 15:18:13 on 24-Oct-2019 REM Old TITL exp_0232(ChinaLow4) in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1): R1 0.157, Rweak 0.060, Alpha 0.005 REM 0.510 for 31 systematic absences, Orientation as input REM Flack x = -0.077 ( 0.103 ) from 2514 Parsons' quotients REM Formula found by SHELXT: C44 N2 O15 CELL 1.54184 8.972983 20.917072 23.920065 90 90 90 ZERR 4 0.000485 0.000897 0.00108 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H O UNIT 184 224 60 L.S. 8 DFIX 1.4 0.01 c21b c22b PLAN 20 BOND $H CONF list 4 fmap 2 53 acta HTAB REM REM REM HTAB O3 O5 HTAB C1 O15B HTAB C3 O11 HTAB C4 O15B HTAB C16 O3 HTAB C16 O15A EQIV $1 x+1/2, -y+3/2, -z+1 HTAB C37 O9_$1 EQIV $2 x+1, y, z HTAB C37 O15B_$2 WGHT 0.071000 1.458300 FVAR 4.97945 0.82646 O1 3 0.000607 0.693000 0.897657 11.00000 0.07079 0.06127 = 0.05334 -0.01409 0.02318 -0.01568 O2 3 0.129518 0.674824 0.818771 11.00000 0.05011 0.04857 = 0.04220 -0.01160 0.00977 -0.01405 O3 3 0.082932 0.547585 0.834735 11.00000 0.04537 0.04865 = 0.04987 -0.00437 0.00906 -0.00674 AFIX 83 H3A 2 0.173963 0.544145 0.834484 11.00000 -1.50000 AFIX 0 O4 3 0.530621 0.641540 0.780210 11.00000 0.04950 0.07143 = 0.04674 0.00362 0.00174 -0.02137 O5 3 0.369385 0.559432 0.787286 11.00000 0.03855 0.05164 = 0.04306 -0.00312 -0.00445 -0.00531 O6 3 0.560565 0.627268 0.588455 11.00000 0.03778 0.08047 = 0.04553 -0.01707 0.00208 -0.00678 O7 3 0.706220 0.696645 0.633302 11.00000 0.05285 0.09620 = 0.06708 -0.02259 0.00495 -0.02128 O8 3 0.260976 0.674363 0.546979 11.00000 0.05081 0.05293 = 0.04103 -0.00882 -0.00019 -0.00418 O9 3 0.375861 0.735076 0.481286 11.00000 0.07793 0.11793 = 0.05623 -0.00018 0.01207 -0.02614 O10 3 0.357894 0.543613 0.585918 11.00000 0.05030 0.05543 = 0.04524 -0.01687 0.00436 -0.00087 O11 3 0.113179 0.520490 0.587296 11.00000 0.05118 0.05019 = 0.07176 -0.01633 -0.01544 -0.00224 O12 3 0.213615 0.445492 0.753431 11.00000 0.04556 0.04351 = 0.05294 -0.00924 -0.00954 0.00663 O13 3 0.286158 0.397089 0.673607 11.00000 0.09151 0.10715 = 0.07541 -0.04413 -0.03256 0.06191 C1 1 -0.106854 0.537931 0.766728 11.00000 0.04295 0.03877 = 0.06427 -0.01334 0.00542 -0.00494 AFIX 23 H1A 2 -0.162596 0.561225 0.738581 11.00000 -1.20000 H1B 2 -0.170118 0.531620 0.799144 11.00000 -1.20000 AFIX 0 C2 1 -0.052735 0.472766 0.743316 11.00000 0.04050 0.03615 = 0.06938 -0.01429 -0.00501 -0.00221 C3 1 0.108625 0.484717 0.722937 11.00000 0.03924 0.04409 = 0.04873 -0.00431 -0.00422 0.00615 AFIX 13 H3B 2 0.116083 0.475813 0.682811 11.00000 -1.20000 AFIX 0 C4 1 0.136777 0.556344 0.734007 11.00000 0.03896 0.04085 = 0.04352 -0.00910 0.00069 -0.00291 AFIX 13 H4A 2 0.093509 0.578117 0.701564 11.00000 -1.20000 AFIX 0 C5 1 0.299456 0.579619 0.735788 11.00000 0.03682 0.05075 = 0.04026 -0.00460 0.00127 -0.00100 AFIX 13 H5A 2 0.298412 0.626464 0.735278 11.00000 -1.20000 AFIX 0 C6 1 0.388033 0.557023 0.685552 11.00000 0.03443 0.06101 = 0.04860 -0.00679 -0.00077 0.00070 C7 1 0.338876 0.587842 0.631248 11.00000 0.03924 0.05263 = 0.03982 -0.01503 0.00453 -0.00275 AFIX 13 H7A 2 0.233527 0.599777 0.634048 11.00000 -1.20000 AFIX 0 C8 1 0.432321 0.647910 0.620112 11.00000 0.04204 0.06223 = 0.03929 -0.01720 0.00381 -0.00754 AFIX 13 H8A 2 0.467627 0.664157 0.656185 11.00000 -1.20000 AFIX 0 C9 1 0.353428 0.702215 0.590065 11.00000 0.04438 0.05745 = 0.04193 -0.01088 0.00431 -0.01294 AFIX 13 H9A 2 0.429542 0.728441 0.571698 11.00000 -1.20000 AFIX 0 C10 1 0.257571 0.747072 0.627561 11.00000 0.04905 0.04868 = 0.04593 -0.01166 0.00635 -0.00750 C11 1 0.131547 0.712800 0.656841 11.00000 0.04407 0.04282 = 0.05213 -0.01472 0.00124 -0.00852 AFIX 43 H11A 2 0.069291 0.687982 0.634587 11.00000 -1.20000 AFIX 0 C12 1 0.100866 0.714494 0.710693 11.00000 0.04182 0.04365 = 0.04784 -0.01033 0.00101 -0.00319 AFIX 43 H12A 2 0.169386 0.735170 0.733586 11.00000 -1.20000 AFIX 0 C13 1 -0.034641 0.686175 0.739001 11.00000 0.03913 0.04109 = 0.05470 -0.01289 0.00854 -0.00513 AFIX 13 H13A 2 -0.085897 0.658635 0.712004 11.00000 -1.20000 AFIX 0 C14 1 0.002201 0.646040 0.790880 11.00000 0.04125 0.04464 = 0.04833 -0.01534 0.01174 -0.00960 AFIX 13 H14A 2 -0.082849 0.649530 0.816401 11.00000 -1.20000 AFIX 0 C15 1 0.033996 0.574230 0.782758 11.00000 0.03894 0.04496 = 0.04556 -0.00572 0.00456 -0.00567 C16 1 -0.071703 0.420217 0.786007 11.00000 0.05908 0.04436 = 0.08877 -0.00172 0.01262 -0.00365 AFIX 33 H16A 2 -0.018193 0.431146 0.819420 11.00000 -1.50000 H16B 2 -0.175563 0.415222 0.794593 11.00000 -1.50000 H16C 2 -0.033412 0.380874 0.771149 11.00000 -1.50000 AFIX 0 C17 1 0.501988 0.518013 0.687818 11.00000 0.04845 0.08756 = 0.05862 -0.00691 0.00945 0.01331 AFIX 93 H17A 2 0.555265 0.508527 0.655517 11.00000 -1.50000 H17B 2 0.529653 0.499790 0.721730 11.00000 -1.50000 AFIX 0 C18 1 0.363867 0.780221 0.668833 11.00000 0.05162 0.05725 = 0.05577 -0.01820 0.00857 -0.01966 AFIX 33 H18A 2 0.441873 0.801291 0.648462 11.00000 -1.50000 H18B 2 0.309531 0.811149 0.690370 11.00000 -1.50000 H18C 2 0.406548 0.748918 0.693431 11.00000 -1.50000 AFIX 0 C19 1 0.188172 0.798639 0.589324 11.00000 0.06341 0.05173 = 0.06029 -0.01007 0.01188 -0.00766 AFIX 33 H19A 2 0.266006 0.821231 0.570141 11.00000 -1.50000 H19B 2 0.123781 0.778591 0.562493 11.00000 -1.50000 H19C 2 0.131616 0.828133 0.611582 11.00000 -1.50000 AFIX 0 C20 1 -0.139928 0.740840 0.754834 11.00000 0.05014 0.04989 = 0.06478 -0.01014 0.01317 -0.00240 AFIX 33 H20A 2 -0.226740 0.723714 0.772888 11.00000 -1.50000 H20B 2 -0.089849 0.769599 0.779842 11.00000 -1.50000 H20C 2 -0.169221 0.763488 0.721702 11.00000 -1.50000 AFIX 0 C23 1 0.294329 0.403039 0.722920 11.00000 0.05212 0.06786 = 0.06790 -0.01856 -0.02246 0.01602 C24 1 0.400524 0.368618 0.760339 11.00000 0.05972 0.06368 = 0.09030 -0.01543 -0.02971 0.02100 AFIX 33 H24A 2 0.384613 0.381844 0.798304 11.00000 -1.50000 H24B 2 0.384338 0.323385 0.757292 11.00000 -1.50000 H24C 2 0.500928 0.378485 0.749489 11.00000 -1.50000 AFIX 0 C25 1 0.486599 0.594344 0.804707 11.00000 0.03386 0.06308 = 0.04028 -0.00920 0.00440 -0.00788 C26 1 0.557355 0.567897 0.855501 11.00000 0.03802 0.05508 = 0.04748 -0.00461 0.00101 -0.00155 C27 1 0.530254 0.504565 0.872392 11.00000 0.04896 0.06374 = 0.05174 -0.00777 -0.00272 -0.00783 AFIX 43 H27A 2 0.460643 0.479562 0.853638 11.00000 -1.20000 AFIX 0 C28 1 0.607396 0.480394 0.916592 11.00000 0.06695 0.05775 = 0.07084 0.00255 -0.01225 -0.00374 AFIX 43 H28A 2 0.589648 0.438648 0.928197 11.00000 -1.20000 AFIX 0 C29 1 0.711788 0.517097 0.944455 11.00000 0.06028 0.07994 = 0.05747 0.00543 -0.01476 -0.00294 AFIX 43 H29A 2 0.765091 0.499456 0.974015 11.00000 -1.20000 AFIX 0 C30 1 0.737850 0.579892 0.928806 11.00000 0.04981 0.07196 = 0.05222 -0.00300 -0.00835 -0.01314 AFIX 43 H30A 2 0.805632 0.605031 0.948348 11.00000 -1.20000 AFIX 0 C31 1 0.662096 0.604027 0.884197 11.00000 0.04548 0.05999 = 0.04529 -0.00539 0.00453 -0.00955 AFIX 43 H31A 2 0.681026 0.645716 0.872697 11.00000 -1.20000 AFIX 0 C32 1 0.236766 0.510187 0.569647 11.00000 0.05608 0.04878 = 0.05221 -0.01260 -0.00755 0.00536 C33 1 0.284357 0.457358 0.529532 11.00000 0.09312 0.06145 = 0.07298 -0.02817 -0.01554 0.01194 AFIX 13 H33A 2 0.364841 0.433760 0.548003 11.00000 -1.20000 AFIX 0 C34 1 0.157484 0.410805 0.521555 11.00000 0.10139 0.06734 = 0.12215 -0.04630 -0.03039 0.00823 AFIX 33 H34A 2 0.123433 0.396131 0.557373 11.00000 -1.50000 H34B 2 0.077123 0.431684 0.502355 11.00000 -1.50000 H34C 2 0.191245 0.375006 0.499867 11.00000 -1.50000 AFIX 0 C35 1 0.346599 0.483395 0.477748 11.00000 0.14211 0.13216 = 0.09986 -0.06924 0.02424 0.00651 AFIX 33 H35A 2 0.426177 0.512376 0.486541 11.00000 -1.50000 H35B 2 0.384281 0.449103 0.455127 11.00000 -1.50000 H35C 2 0.270159 0.505780 0.457616 11.00000 -1.50000 AFIX 0 C36 1 0.692938 0.653363 0.600532 11.00000 0.04209 0.07665 = 0.04428 -0.00276 -0.00379 -0.00950 C37 1 0.814523 0.623097 0.567936 11.00000 0.04492 0.08998 = 0.06891 -0.00872 0.00682 -0.01101 AFIX 33 H37A 2 0.774040 0.589746 0.544923 11.00000 -1.50000 H37B 2 0.861401 0.654651 0.544694 11.00000 -1.50000 H37C 2 0.886841 0.605300 0.593087 11.00000 -1.50000 AFIX 0 C38 1 0.283205 0.694625 0.494093 11.00000 0.05943 0.07514 = 0.04545 -0.00997 0.00256 0.00480 C39 1 0.178679 0.662444 0.454980 11.00000 0.09217 0.07358 = 0.05579 -0.01010 -0.02548 0.01001 AFIX 33 H39A 2 0.117637 0.632800 0.475338 11.00000 -1.50000 H39B 2 0.116467 0.693873 0.437353 11.00000 -1.50000 H39C 2 0.234405 0.639867 0.426981 11.00000 -1.50000 AFIX 0 C40 1 0.112651 0.698463 0.870952 11.00000 0.06666 0.03813 = 0.03665 -0.00325 0.00902 -0.00817 C41 1 0.251998 0.730574 0.890483 11.00000 0.07116 0.03006 = 0.03776 0.00012 -0.00526 -0.00584 C42 1 0.370220 0.744220 0.855173 11.00000 0.06858 0.05149 = 0.04103 -0.00026 -0.00418 -0.01485 AFIX 43 H42A 2 0.364942 0.733140 0.817572 11.00000 -1.20000 AFIX 0 C43 1 0.495656 0.774196 0.875690 11.00000 0.06981 0.05375 = 0.05316 0.00710 -0.01541 -0.01951 AFIX 43 H43A 2 0.574525 0.783603 0.851844 11.00000 -1.20000 AFIX 0 C44 1 0.504307 0.790125 0.931064 11.00000 0.07879 0.03948 = 0.06620 0.00498 -0.02935 -0.01409 AFIX 43 H44A 2 0.589471 0.810125 0.944670 11.00000 -1.20000 AFIX 0 C45 1 0.387789 0.776796 0.966976 11.00000 0.09939 0.05301 = 0.04251 -0.00730 -0.02330 -0.00086 AFIX 43 H45A 2 0.394730 0.787287 1.004668 11.00000 -1.20000 AFIX 0 C46 1 0.262110 0.748026 0.946594 11.00000 0.08030 0.04341 = 0.04305 -0.00229 -0.00084 -0.00159 AFIX 43 H46A 2 0.182458 0.740016 0.970464 11.00000 -1.20000 AFIX 0 PART 1 O14A 3 -0.148718 0.464278 0.692236 21.00000 0.04297 0.03117 = 0.07662 -0.01298 -0.02133 0.00359 O15A 3 -0.038497 0.370187 0.671555 21.00000 0.07728 0.03910 = 0.09158 -0.02084 -0.02797 0.01904 C21A 1 -0.125121 0.411673 0.660391 21.00000 0.05471 0.03657 = 0.09128 -0.01842 -0.02097 -0.00005 C22A 1 -0.226328 0.413324 0.610532 21.00000 0.08549 0.04003 = 0.10687 -0.02521 -0.05154 0.00139 AFIX 33 H22A 2 -0.284604 0.451803 0.611333 21.00000 -1.50000 H22B 2 -0.167759 0.412314 0.576958 21.00000 -1.50000 H22C 2 -0.291418 0.376913 0.611383 21.00000 -1.50000 AFIX 0 PART 2 O15B 3 -0.122380 0.524879 0.651292 -21.00000 0.04674 0.08716 = 0.05284 0.00275 -0.01131 0.00669 O14B 3 -0.139308 0.438280 0.708084 -21.00000 0.03631 0.04355 = 0.07012 -0.01869 0.00251 0.00549 C21B 1 -0.159617 0.470066 0.657657 -21.00000 0.03176 0.06898 = 0.06029 0.00342 -0.02531 0.00506 C22B 1 -0.207219 0.433897 0.611378 -21.00000 0.04001 0.09419 = 0.16850 -0.09994 0.03311 -0.02797 AFIX 33 H22D 2 -0.232776 0.391506 0.623405 -21.00000 -1.50000 H22E 2 -0.292928 0.453841 0.594859 -21.00000 -1.50000 H22F 2 -0.128428 0.431672 0.584298 -21.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM exp_0232(chinalow4)_a.res in P2(1)2(1)2(1) REM wR2 = 0.1534, GooF = S = 1.016, Restrained GooF = 1.016 for all data REM R1 = 0.0563 for 7007 Fo > 4sig(Fo) and 0.0793 for all 9301 data REM 587 parameters refined using 1 restraints END WGHT 0.0700 1.2709 REM Instructions for potential hydrogen bonds HTAB O3 O5 HTAB C1 O15B HTAB C3 O11 HTAB C4 O15B HTAB C16 O3 HTAB C16 O15A HTAB C37 O9_$1 HTAB C37 O15B_$2 REM Highest difference peak 0.258, deepest hole -0.186, 1-sigma level 0.044 Q1 1 0.8122 0.8016 0.9057 11.00000 0.05 0.26 Q2 1 0.1535 0.3148 0.5856 11.00000 0.05 0.25 Q3 1 0.4177 0.4529 0.5067 11.00000 0.05 0.24 Q4 1 0.4271 0.6848 0.4794 11.00000 0.05 0.22 Q5 1 0.4803 0.3998 0.7824 11.00000 0.05 0.20 Q6 1 0.7760 0.6187 0.5344 11.00000 0.05 0.19 Q7 1 0.0732 0.6740 0.4781 11.00000 0.05 0.18 Q8 1 0.2239 0.3620 0.6766 11.00000 0.05 0.18 Q9 1 0.2261 0.4740 0.5047 11.00000 0.05 0.18 Q10 1 0.0998 0.5552 0.5580 11.00000 0.05 0.17 Q11 1 0.9183 0.6515 0.5655 11.00000 0.05 0.17 Q12 1 0.1945 0.6142 0.4593 11.00000 0.05 0.17 Q13 1 0.0921 0.4401 0.4932 11.00000 0.05 0.17 Q14 1 0.3438 0.3426 0.8029 11.00000 0.05 0.16 Q15 1 0.1996 0.6802 0.4177 11.00000 0.05 0.16 Q16 1 0.1724 0.5447 0.8578 11.00000 0.05 0.16 Q17 1 0.2366 0.5600 0.7534 11.00000 0.05 0.15 Q18 1 0.2857 0.7411 0.8197 11.00000 0.05 0.15 Q19 1 -0.1388 0.6786 0.6967 11.00000 0.05 0.15 Q20 1 0.6550 0.7404 0.6271 11.00000 0.05 0.15 ; _shelx_res_checksum 94960 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.0006(4) 0.69300(16) 0.89766(13) 0.0618(9) Uani d 1 . . O O2 0.1295(3) 0.67482(14) 0.81877(12) 0.0470(7) Uani d 1 . . O O3 0.0829(3) 0.54758(14) 0.83474(12) 0.0480(7) Uani d 1 . . H H3A 0.173963 0.544145 0.834484 0.072 Uiso calc 1 . . O O4 0.5306(4) 0.64154(17) 0.78021(13) 0.0559(8) Uani d 1 . . O O5 0.3694(3) 0.55943(14) 0.78729(12) 0.0444(6) Uani d 1 . . O O6 0.5606(3) 0.62727(17) 0.58845(13) 0.0546(8) Uani d 1 . . O O7 0.7062(4) 0.6966(2) 0.63330(16) 0.0720(11) Uani d 1 . . O O8 0.2610(4) 0.67436(14) 0.54698(12) 0.0483(7) Uani d 1 . . O O9 0.3759(5) 0.7351(2) 0.48129(16) 0.0840(13) Uani d 1 . . O O10 0.3579(4) 0.54361(15) 0.58592(12) 0.0503(7) Uani d 1 . . O O11 0.1132(4) 0.52049(15) 0.58730(15) 0.0577(8) Uani d 1 . . O O12 0.2136(3) 0.44549(13) 0.75343(12) 0.0473(7) Uani d 1 . . O O13 0.2862(5) 0.3971(2) 0.67361(18) 0.0914(15) Uani d 1 . . C C1 -0.1069(5) 0.5379(2) 0.7667(2) 0.0487(11) Uani d 1 . . H H1A -0.162596 0.561225 0.738581 0.058 Uiso calc 1 . . H H1B -0.170118 0.531620 0.799144 0.058 Uiso calc 1 . . C C2 -0.0527(5) 0.47277(19) 0.7433(2) 0.0487(11) Uani d 1 . . C C3 0.1086(5) 0.4847(2) 0.72294(18) 0.0440(9) Uani d 1 . . H H3B 0.116083 0.475813 0.682811 0.053 Uiso calc 1 . . C C4 0.1368(5) 0.55634(19) 0.73401(17) 0.0411(9) Uani d 1 . . H H4A 0.093509 0.578117 0.701564 0.049 Uiso calc 1 . . C C5 0.2995(5) 0.5796(2) 0.73579(17) 0.0426(9) Uani d 1 . . H H5A 0.298412 0.626464 0.735278 0.051 Uiso calc 1 . . C C6 0.3880(5) 0.5570(2) 0.68555(18) 0.0480(10) Uani d 1 . . C C7 0.3389(5) 0.5878(2) 0.63125(17) 0.0439(10) Uani d 1 . . H H7A 0.233527 0.599777 0.634048 0.053 Uiso calc 1 . . C C8 0.4323(5) 0.6479(2) 0.62011(18) 0.0479(10) Uani d 1 . . H H8A 0.467627 0.664157 0.656185 0.057 Uiso calc 1 . . C C9 0.3534(5) 0.7022(2) 0.59007(18) 0.0479(10) Uani d 1 . . H H9A 0.429542 0.728441 0.571698 0.058 Uiso calc 1 . . C C10 0.2576(5) 0.7471(2) 0.62756(18) 0.0479(10) Uani d 1 . . C C11 0.1315(5) 0.7128(2) 0.65684(18) 0.0463(10) Uani d 1 . . H H11A 0.069291 0.687982 0.634587 0.056 Uiso calc 1 . . C C12 0.1009(5) 0.7145(2) 0.71069(18) 0.0444(10) Uani d 1 . . H H12A 0.169386 0.735170 0.733586 0.053 Uiso calc 1 . . C C13 -0.0346(5) 0.68617(19) 0.73900(19) 0.0450(10) Uani d 1 . . H H13A -0.085897 0.658635 0.712004 0.054 Uiso calc 1 . . C C14 0.0022(5) 0.64604(19) 0.79088(18) 0.0447(10) Uani d 1 . . H H14A -0.082849 0.649530 0.816401 0.054 Uiso calc 1 . . C C15 0.0340(5) 0.5742(2) 0.78276(18) 0.0432(9) Uani d 1 . . C C16 -0.0717(6) 0.4202(2) 0.7860(2) 0.0641(14) Uani d 1 . . H H16A -0.018193 0.431146 0.819420 0.096 Uiso calc 1 . . H H16B -0.175563 0.415222 0.794593 0.096 Uiso calc 1 . . H H16C -0.033412 0.380874 0.771149 0.096 Uiso calc 1 . . C C17 0.5020(6) 0.5180(3) 0.6878(2) 0.0649(14) Uani d 1 . . H H17A 0.555265 0.508527 0.655517 0.097 Uiso calc 1 . . H H17B 0.529653 0.499790 0.721730 0.097 Uiso calc 1 . . C C18 0.3639(6) 0.7802(2) 0.6688(2) 0.0549(12) Uani d 1 . . H H18A 0.441873 0.801291 0.648462 0.082 Uiso calc 1 . . H H18B 0.309531 0.811149 0.690370 0.082 Uiso calc 1 . . H H18C 0.406548 0.748918 0.693431 0.082 Uiso calc 1 . . C C19 0.1882(6) 0.7986(2) 0.5893(2) 0.0585(12) Uani d 1 . . H H19A 0.266006 0.821231 0.570141 0.088 Uiso calc 1 . . H H19B 0.123781 0.778591 0.562493 0.088 Uiso calc 1 . . H H19C 0.131616 0.828133 0.611582 0.088 Uiso calc 1 . . C C20 -0.1399(6) 0.7408(2) 0.7548(2) 0.0549(11) Uani d 1 . . H H20A -0.226740 0.723714 0.772888 0.082 Uiso calc 1 . . H H20B -0.089849 0.769599 0.779842 0.082 Uiso calc 1 . . H H20C -0.169221 0.763488 0.721702 0.082 Uiso calc 1 . . C C23 0.2943(6) 0.4030(3) 0.7229(2) 0.0626(14) Uani d 1 . . C C24 0.4005(6) 0.3686(3) 0.7603(3) 0.0712(16) Uani d 1 . . H H24A 0.384613 0.381844 0.798304 0.107 Uiso calc 1 . . H H24B 0.384338 0.323385 0.757292 0.107 Uiso calc 1 . . H H24C 0.500928 0.378485 0.749489 0.107 Uiso calc 1 . . C C25 0.4866(5) 0.5943(2) 0.80471(18) 0.0457(10) Uani d 1 . . C C26 0.5574(5) 0.5679(2) 0.85550(18) 0.0469(10) Uani d 1 . . C C27 0.5303(6) 0.5046(2) 0.8724(2) 0.0548(12) Uani d 1 . . H H27A 0.460643 0.479562 0.853638 0.066 Uiso calc 1 . . C C28 0.6074(7) 0.4804(3) 0.9166(2) 0.0652(14) Uani d 1 . . H H28A 0.589648 0.438648 0.928197 0.078 Uiso calc 1 . . C C29 0.7118(7) 0.5171(3) 0.9445(2) 0.0659(14) Uani d 1 . . H H29A 0.765091 0.499456 0.974015 0.079 Uiso calc 1 . . C C30 0.7379(6) 0.5799(3) 0.9288(2) 0.0580(12) Uani d 1 . . H H30A 0.805632 0.605031 0.948348 0.070 Uiso calc 1 . . C C31 0.6621(5) 0.6040(2) 0.88420(19) 0.0503(11) Uani d 1 . . H H31A 0.681026 0.645716 0.872697 0.060 Uiso calc 1 . . C C32 0.2368(6) 0.5102(2) 0.5696(2) 0.0524(11) Uani d 1 . . C C33 0.2844(8) 0.4574(3) 0.5295(3) 0.0758(17) Uani d 1 . . H H33A 0.364841 0.433760 0.548003 0.091 Uiso calc 1 . . C C34 0.1575(8) 0.4108(3) 0.5216(3) 0.097(2) Uani d 1 . . H H34A 0.123433 0.396131 0.557373 0.145 Uiso calc 1 . . H H34B 0.077123 0.431684 0.502355 0.145 Uiso calc 1 . . H H34C 0.191245 0.375006 0.499867 0.145 Uiso calc 1 . . C C35 0.3466(11) 0.4834(4) 0.4777(3) 0.125(3) Uani d 1 . . H H35A 0.426177 0.512376 0.486541 0.187 Uiso calc 1 . . H H35B 0.384281 0.449103 0.455127 0.187 Uiso calc 1 . . H H35C 0.270159 0.505780 0.457616 0.187 Uiso calc 1 . . C C36 0.6929(5) 0.6534(3) 0.60053(19) 0.0543(12) Uani d 1 . . C C37 0.8145(6) 0.6231(3) 0.5679(2) 0.0679(14) Uani d 1 . . H H37A 0.774040 0.589746 0.544923 0.102 Uiso calc 1 . . H H37B 0.861401 0.654651 0.544694 0.102 Uiso calc 1 . . H H37C 0.886841 0.605300 0.593087 0.102 Uiso calc 1 . . C C38 0.2832(6) 0.6946(3) 0.4941(2) 0.0600(13) Uani d 1 . . C C39 0.1787(8) 0.6624(3) 0.4550(2) 0.0738(17) Uani d 1 . . H H39A 0.117637 0.632800 0.475338 0.111 Uiso calc 1 . . H H39B 0.116467 0.693873 0.437353 0.111 Uiso calc 1 . . H H39C 0.234405 0.639867 0.426981 0.111 Uiso calc 1 . . C C40 0.1127(6) 0.69846(19) 0.87095(17) 0.0471(10) Uani d 1 . . C C41 0.2520(6) 0.73057(18) 0.89048(17) 0.0463(11) Uani d 1 . . C C42 0.3702(6) 0.7442(2) 0.85517(19) 0.0537(12) Uani d 1 . . H H42A 0.364942 0.733140 0.817572 0.064 Uiso calc 1 . . C C43 0.4957(6) 0.7742(2) 0.8757(2) 0.0589(13) Uani d 1 . . H H43A 0.574525 0.783603 0.851844 0.071 Uiso calc 1 . . C C44 0.5043(7) 0.7901(2) 0.9311(2) 0.0615(14) Uani d 1 . . H H44A 0.589471 0.810125 0.944670 0.074 Uiso calc 1 . . C C45 0.3878(7) 0.7768(2) 0.9670(2) 0.0650(15) Uani d 1 . . H H45A 0.394730 0.787287 1.004668 0.078 Uiso calc 1 . . C C46 0.2621(7) 0.7480(2) 0.94659(19) 0.0556(12) Uani d 1 . . H H46A 0.182458 0.740016 0.970464 0.067 Uiso calc 1 . . O O14A -0.1487(7) 0.4643(3) 0.6922(3) 0.0503(15) Uani d 0.826(8) A 1 O O15A -0.0385(5) 0.37019(18) 0.6716(2) 0.0693(15) Uani d 0.826(8) A 1 C C21A -0.1251(7) 0.4117(3) 0.6604(3) 0.0609(18) Uani d 0.826(8) A 1 C C22A -0.2263(13) 0.4133(4) 0.6105(5) 0.077(3) Uani d 0.826(8) A 1 H H22A -0.284604 0.451803 0.611333 0.116 Uiso calc 0.826(8) A 1 H H22B -0.167759 0.412314 0.576958 0.116 Uiso calc 0.826(8) A 1 H H22C -0.291418 0.376913 0.611383 0.116 Uiso calc 0.826(8) A 1 O O15B -0.122(2) 0.5249(12) 0.6513(8) 0.062(6) Uani d 0.174(8) A 2 O O14B -0.139(3) 0.4383(12) 0.7081(13) 0.050(7) Uani d 0.174(8) A 2 C C21B -0.160(3) 0.4701(18) 0.6577(16) 0.054(8) Uani d 0.174(8) A 2 C C22B -0.207(5) 0.434(3) 0.611(2) 0.10(2) Uani d 0.174(8) A 2 H H22D -0.232776 0.391506 0.623405 0.151 Uiso calc 0.174(8) A 2 H H22E -0.292928 0.453841 0.594859 0.151 Uiso calc 0.174(8) A 2 H H22F -0.128428 0.431672 0.584298 0.151 Uiso calc 0.174(8) A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.071(2) 0.061(2) 0.0533(19) -0.0157(18) 0.0232(18) -0.0141(15) O2 0.0501(17) 0.0486(15) 0.0422(15) -0.0141(14) 0.0098(14) -0.0116(13) O3 0.0454(17) 0.0487(16) 0.0499(17) -0.0067(13) 0.0091(14) -0.0044(13) O4 0.0495(19) 0.071(2) 0.0467(17) -0.0214(17) 0.0017(15) 0.0036(15) O5 0.0385(15) 0.0516(16) 0.0431(15) -0.0053(13) -0.0045(13) -0.0031(13) O6 0.0378(16) 0.080(2) 0.0455(17) -0.0068(16) 0.0021(14) -0.0171(16) O7 0.053(2) 0.096(3) 0.067(2) -0.021(2) 0.0049(18) -0.023(2) O8 0.0508(18) 0.0529(16) 0.0410(15) -0.0042(14) -0.0002(14) -0.0088(13) O9 0.078(3) 0.118(3) 0.056(2) -0.026(3) 0.012(2) 0.000(2) O10 0.0503(18) 0.0554(17) 0.0452(16) -0.0009(15) 0.0044(15) -0.0169(13) O11 0.051(2) 0.0502(18) 0.072(2) -0.0022(15) -0.0154(17) -0.0163(16) O12 0.0456(17) 0.0435(15) 0.0529(17) 0.0066(13) -0.0095(14) -0.0092(13) O13 0.092(3) 0.107(3) 0.075(3) 0.062(3) -0.033(2) -0.044(2) C1 0.043(2) 0.039(2) 0.064(3) -0.0049(18) 0.005(2) -0.0133(19) C2 0.041(2) 0.036(2) 0.069(3) -0.0022(17) -0.005(2) -0.014(2) C3 0.039(2) 0.044(2) 0.049(2) 0.0061(18) -0.0042(19) -0.0043(18) C4 0.039(2) 0.041(2) 0.044(2) -0.0029(18) 0.0007(18) -0.0091(17) C5 0.037(2) 0.051(2) 0.040(2) -0.0010(18) 0.0013(17) -0.0046(17) C6 0.034(2) 0.061(3) 0.049(2) 0.001(2) -0.0008(19) -0.007(2) C7 0.039(2) 0.053(2) 0.040(2) -0.0027(19) 0.0045(18) -0.0150(18) C8 0.042(2) 0.062(3) 0.039(2) -0.008(2) 0.0038(19) -0.017(2) C9 0.044(2) 0.057(2) 0.042(2) -0.013(2) 0.0043(19) -0.0109(19) C10 0.049(3) 0.049(2) 0.046(2) -0.008(2) 0.006(2) -0.0117(19) C11 0.044(2) 0.043(2) 0.052(2) -0.0085(19) 0.001(2) -0.0147(18) C12 0.042(2) 0.044(2) 0.048(2) -0.0032(18) 0.001(2) -0.0103(18) C13 0.039(2) 0.041(2) 0.055(2) -0.0051(18) 0.0085(19) -0.0129(18) C14 0.041(2) 0.045(2) 0.048(2) -0.0096(18) 0.012(2) -0.0153(18) C15 0.039(2) 0.045(2) 0.046(2) -0.0057(18) 0.0046(18) -0.0057(18) C16 0.059(3) 0.044(2) 0.089(4) -0.004(2) 0.013(3) -0.002(2) C17 0.048(3) 0.088(4) 0.059(3) 0.013(3) 0.009(2) -0.007(3) C18 0.052(3) 0.057(3) 0.056(3) -0.020(2) 0.009(2) -0.018(2) C19 0.063(3) 0.052(2) 0.060(3) -0.008(2) 0.012(2) -0.010(2) C20 0.050(3) 0.050(2) 0.065(3) -0.002(2) 0.013(2) -0.010(2) C23 0.052(3) 0.068(3) 0.068(3) 0.016(2) -0.022(2) -0.019(3) C24 0.060(3) 0.064(3) 0.090(4) 0.021(3) -0.030(3) -0.015(3) C25 0.034(2) 0.063(3) 0.040(2) -0.008(2) 0.0044(17) -0.0092(19) C26 0.038(2) 0.055(3) 0.047(2) -0.0015(19) 0.0010(19) -0.0046(19) C27 0.049(3) 0.064(3) 0.052(3) -0.008(2) -0.003(2) -0.008(2) C28 0.067(4) 0.058(3) 0.071(3) -0.004(3) -0.012(3) 0.003(2) C29 0.060(3) 0.080(3) 0.057(3) -0.003(3) -0.015(3) 0.005(3) C30 0.050(3) 0.072(3) 0.052(3) -0.013(3) -0.008(2) -0.003(2) C31 0.045(3) 0.060(3) 0.045(2) -0.010(2) 0.005(2) -0.005(2) C32 0.056(3) 0.049(2) 0.052(3) 0.005(2) -0.008(2) -0.013(2) C33 0.093(5) 0.061(3) 0.073(4) 0.012(3) -0.016(3) -0.028(3) C34 0.101(5) 0.067(4) 0.122(6) 0.008(4) -0.030(5) -0.046(4) C35 0.142(8) 0.132(7) 0.100(6) 0.007(6) 0.024(6) -0.069(5) C36 0.042(3) 0.077(3) 0.044(2) -0.009(2) -0.004(2) -0.003(2) C37 0.045(3) 0.090(4) 0.069(3) -0.011(3) 0.007(3) -0.009(3) C38 0.059(3) 0.075(3) 0.045(3) 0.005(3) 0.003(2) -0.010(2) C39 0.092(5) 0.074(3) 0.056(3) 0.010(3) -0.025(3) -0.010(3) C40 0.067(3) 0.038(2) 0.037(2) -0.008(2) 0.009(2) -0.0032(16) C41 0.071(3) 0.0301(18) 0.038(2) -0.006(2) -0.005(2) 0.0001(16) C42 0.069(3) 0.051(2) 0.041(2) -0.015(2) -0.004(2) -0.0003(19) C43 0.070(3) 0.054(3) 0.053(3) -0.020(2) -0.015(3) 0.007(2) C44 0.079(4) 0.039(2) 0.066(3) -0.014(2) -0.029(3) 0.005(2) C45 0.099(5) 0.053(3) 0.043(3) -0.001(3) -0.023(3) -0.007(2) C46 0.080(4) 0.043(2) 0.043(2) -0.002(2) -0.001(2) -0.0023(19) O14A 0.043(3) 0.031(3) 0.077(5) 0.004(2) -0.021(3) -0.013(3) O15A 0.077(3) 0.039(2) 0.092(3) 0.019(2) -0.028(3) -0.021(2) C21A 0.055(4) 0.037(3) 0.091(5) 0.000(3) -0.021(4) -0.018(3) C22A 0.085(7) 0.040(4) 0.107(6) 0.001(4) -0.052(5) -0.025(4) O15B 0.047(11) 0.087(17) 0.053(12) 0.007(11) -0.011(9) 0.003(10) O14B 0.036(11) 0.044(15) 0.070(19) 0.005(12) 0.003(11) -0.019(12) C21B 0.032(14) 0.07(2) 0.06(2) 0.005(13) -0.025(15) 0.003(18) C22B 0.040(19) 0.09(4) 0.17(5) -0.03(2) 0.03(3) -0.10(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C40 O2 C14 119.2(3) C15 O3 H3A 109.5 C25 O5 C5 116.4(3) C36 O6 C8 118.2(3) C38 O8 C9 117.2(4) C32 O10 C7 117.1(3) C23 O12 C3 116.6(3) C15 C1 C2 105.6(4) C15 C1 H1A 110.6 C2 C1 H1A 110.6 C15 C1 H1B 110.6 C2 C1 H1B 110.6 H1A C1 H1B 108.7 O14B C2 C16 88.2(13) O14A C2 C16 113.5(4) O14B C2 C3 115.2(12) O14A C2 C3 107.4(4) C16 C2 C3 115.8(4) O14B C2 C1 120.9(11) O14A C2 C1 102.6(4) C16 C2 C1 111.1(4) C3 C2 C1 105.3(3) O12 C3 C4 111.0(3) O12 C3 C2 111.0(4) C4 C3 C2 104.8(3) O12 C3 H3B 110.0 C4 C3 H3B 110.0 C2 C3 H3B 110.0 C15 C4 C5 118.2(3) C15 C4 C3 105.6(3) C5 C4 C3 117.9(4) C15 C4 H4A 104.5 C5 C4 H4A 104.5 C3 C4 H4A 104.5 O5 C5 C6 110.9(3) O5 C5 C4 110.0(3) C6 C5 C4 112.1(3) O5 C5 H5A 107.9 C6 C5 H5A 107.9 C4 C5 H5A 107.9 C17 C6 C7 121.9(4) C17 C6 C5 124.8(5) C7 C6 C5 113.2(4) O10 C7 C6 109.8(4) O10 C7 C8 109.4(3) C6 C7 C8 109.8(4) O10 C7 H7A 109.3 C6 C7 H7A 109.3 C8 C7 H7A 109.3 O6 C8 C9 110.3(4) O6 C8 C7 106.4(3) C9 C8 C7 116.1(4) O6 C8 H8A 107.9 C9 C8 H8A 107.9 C7 C8 H8A 107.9 O8 C9 C8 107.7(3) O8 C9 C10 109.7(4) C8 C9 C10 115.8(4) O8 C9 H9A 107.8 C8 C9 H9A 107.8 C10 C9 H9A 107.8 C11 C10 C18 112.4(4) C11 C10 C19 107.7(4) C18 C10 C19 108.4(4) C11 C10 C9 113.2(4) C18 C10 C9 107.4(4) C19 C10 C9 107.6(4) C12 C11 C10 126.6(4) C12 C11 H11A 116.7 C10 C11 H11A 116.7 C11 C12 C13 126.5(4) C11 C12 H12A 116.7 C13 C12 H12A 116.7 C12 C13 C20 108.3(3) C12 C13 C14 113.8(4) C20 C13 C14 110.0(4) C12 C13 H13A 108.2 C20 C13 H13A 108.2 C14 C13 H13A 108.2 O2 C14 C13 108.3(3) O2 C14 C15 108.4(4) C13 C14 C15 118.1(3) O2 C14 H14A 107.2 C13 C14 H14A 107.2 C15 C14 H14A 107.2 O3 C15 C1 106.2(3) O3 C15 C4 112.4(4) C1 C15 C4 100.7(3) O3 C15 C14 109.1(3) C1 C15 C14 111.3(4) C4 C15 C14 116.4(3) C2 C16 H16A 109.5 C2 C16 H16B 109.5 H16A C16 H16B 109.5 C2 C16 H16C 109.5 H16A C16 H16C 109.5 H16B C16 H16C 109.5 C6 C17 H17A 120.0 C6 C17 H17B 120.0 H17A C17 H17B 120.0 C10 C18 H18A 109.5 C10 C18 H18B 109.5 H18A C18 H18B 109.5 C10 C18 H18C 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 C10 C19 H19A 109.5 C10 C19 H19B 109.5 H19A C19 H19B 109.5 C10 C19 H19C 109.5 H19A C19 H19C 109.5 H19B C19 H19C 109.5 C13 C20 H20A 109.5 C13 C20 H20B 109.5 H20A C20 H20B 109.5 C13 C20 H20C 109.5 H20A C20 H20C 109.5 H20B C20 H20C 109.5 O13 C23 O12 124.7(5) O13 C23 C24 125.7(5) O12 C23 C24 109.5(4) C23 C24 H24A 109.5 C23 C24 H24B 109.5 H24A C24 H24B 109.5 C23 C24 H24C 109.5 H24A C24 H24C 109.5 H24B C24 H24C 109.5 O4 C25 O5 123.1(4) O4 C25 C26 124.1(4) O5 C25 C26 112.8(4) C31 C26 C27 119.2(4) C31 C26 C25 119.6(4) C27 C26 C25 121.0(4) C28 C27 C26 119.0(5) C28 C27 H27A 120.5 C26 C27 H27A 120.5 C27 C28 C29 120.9(5) C27 C28 H28A 119.6 C29 C28 H28A 119.6 C28 C29 C30 120.7(5) C28 C29 H29A 119.6 C30 C29 H29A 119.7 C31 C30 C29 118.6(5) C31 C30 H30A 120.7 C29 C30 H30A 120.7 C30 C31 C26 121.6(5) C30 C31 H31A 119.2 C26 C31 H31A 119.2 O11 C32 O10 123.2(4) O11 C32 C33 127.4(5) O10 C32 C33 109.4(5) C35 C33 C34 114.9(6) C35 C33 C32 111.7(5) C34 C33 C32 109.6(6) C35 C33 H33A 106.7 C34 C33 H33A 106.7 C32 C33 H33A 106.7 C33 C34 H34A 109.5 C33 C34 H34B 109.5 H34A C34 H34B 109.5 C33 C34 H34C 109.5 H34A C34 H34C 109.5 H34B C34 H34C 109.5 C33 C35 H35A 109.5 C33 C35 H35B 109.5 H35A C35 H35B 109.5 C33 C35 H35C 109.5 H35A C35 H35C 109.5 H35B C35 H35C 109.5 O7 C36 O6 122.4(5) O7 C36 C37 126.2(5) O6 C36 C37 111.4(4) C36 C37 H37A 109.5 C36 C37 H37B 109.5 H37A C37 H37B 109.5 C36 C37 H37C 109.5 H37A C37 H37C 109.5 H37B C37 H37C 109.5 O9 C38 O8 123.5(5) O9 C38 C39 125.7(5) O8 C38 C39 110.8(5) C38 C39 H39A 109.5 C38 C39 H39B 109.5 H39A C39 H39B 109.5 C38 C39 H39C 109.5 H39A C39 H39C 109.5 H39B C39 H39C 109.5 O1 C40 O2 123.5(4) O1 C40 C41 125.4(4) O2 C40 C41 111.1(4) C42 C41 C46 118.9(5) C42 C41 C40 122.9(4) C46 C41 C40 118.2(4) C43 C42 C41 120.1(4) C43 C42 H42A 119.9 C41 C42 H42A 119.9 C44 C43 C42 120.1(5) C44 C43 H43A 119.9 C42 C43 H43A 119.9 C43 C44 C45 120.7(5) C43 C44 H44A 119.7 C45 C44 H44A 119.7 C46 C45 C44 119.4(4) C46 C45 H45A 120.3 C44 C45 H45A 120.3 C45 C46 C41 120.8(5) C45 C46 H46A 119.6 C41 C46 H46A 119.6 C21A O14A C2 117.6(5) O15A C21A O14A 124.4(6) O15A C21A C22A 126.0(6) O14A C21A C22A 109.5(6) C21A C22A H22A 109.5 C21A C22A H22B 109.5 H22A C22A H22B 109.5 C21A C22A H22C 109.5 H22A C22A H22C 109.5 H22B C22A H22C 109.5 C2 O14B C21B 111(2) O15B C21B O14B 122(3) O15B C21B C22B 120(4) O14B C21B C22B 118(4) C21B C22B H22D 109.5 C21B C22B H22E 109.5 H22D C22B H22E 109.5 C21B C22B H22F 109.5 H22D C22B H22F 109.5 H22E C22B H22F 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C40 1.197(5) O2 C40 1.351(5) O2 C14 1.454(5) O3 C15 1.432(5) O3 H3A 0.8200 O4 C25 1.214(5) O5 C25 1.347(5) O5 C5 1.445(5) O6 C36 1.339(6) O6 C8 1.444(5) O7 C36 1.203(6) O8 C38 1.349(6) O8 C9 1.446(5) O9 C38 1.225(7) O10 C32 1.350(6) O10 C7 1.435(5) O11 C32 1.206(6) O12 C23 1.359(6) O12 C3 1.447(5) O13 C23 1.188(7) C1 C15 1.523(6) C1 C2 1.552(6) C1 H1A 0.9700 C1 H1B 0.9700 C2 O14B 1.35(3) C2 O14A 1.505(8) C2 C16 1.510(7) C2 C3 1.548(6) C3 C4 1.542(6) C3 H3B 0.9800 C4 C15 1.533(6) C4 C5 1.539(6) C4 H4A 0.9800 C5 C6 1.516(6) C5 H5A 0.9800 C6 C17 1.309(7) C6 C7 1.516(6) C7 C8 1.534(6) C7 H7A 0.9800 C8 C9 1.519(7) C8 H8A 0.9800 C9 C10 1.557(6) C9 H9A 0.9800 C10 C11 1.511(6) C10 C18 1.538(6) C10 C19 1.545(7) C11 C12 1.318(6) C11 H11A 0.9300 C12 C13 1.513(6) C12 H12A 0.9300 C13 C20 1.531(6) C13 C14 1.534(6) C13 H13A 0.9800 C14 C15 1.541(6) C14 H14A 0.9800 C16 H16A 0.9600 C16 H16B 0.9600 C16 H16C 0.9600 C17 H17A 0.9300 C17 H17B 0.9300 C18 H18A 0.9600 C18 H18B 0.9600 C18 H18C 0.9600 C19 H19A 0.9600 C19 H19B 0.9600 C19 H19C 0.9600 C20 H20A 0.9600 C20 H20B 0.9600 C20 H20C 0.9600 C23 C24 1.492(7) C24 H24A 0.9600 C24 H24B 0.9600 C24 H24C 0.9600 C25 C26 1.478(6) C26 C31 1.388(6) C26 C27 1.406(7) C27 C28 1.361(7) C27 H27A 0.9300 C28 C29 1.382(8) C28 H28A 0.9300 C29 C30 1.386(8) C29 H29A 0.9300 C30 C31 1.362(7) C30 H30A 0.9300 C31 H31A 0.9300 C32 C33 1.525(7) C33 C35 1.464(10) C33 C34 1.510(9) C33 H33A 0.9800 C34 H34A 0.9600 C34 H34B 0.9600 C34 H34C 0.9600 C35 H35A 0.9600 C35 H35B 0.9600 C35 H35C 0.9600 C36 C37 1.483(7) C37 H37A 0.9600 C37 H37B 0.9600 C37 H37C 0.9600 C38 C39 1.486(8) C39 H39A 0.9600 C39 H39B 0.9600 C39 H39C 0.9600 C40 C41 1.494(7) C41 C42 1.386(7) C41 C46 1.394(6) C42 C43 1.379(7) C42 H42A 0.9300 C43 C44 1.368(7) C43 H43A 0.9300 C44 C45 1.382(8) C44 H44A 0.9300 C45 C46 1.368(8) C45 H45A 0.9300 C46 H46A 0.9300 O14A C21A 1.355(9) O15A C21A 1.195(7) C21A C22A 1.499(11) C22A H22A 0.9600 C22A H22B 0.9600 C22A H22C 0.9600 O15B C21B 1.20(4) O14B C21B 1.39(5) C21B C22B 1.407(14) C22B H22D 0.9600 C22B H22E 0.9600 C22B H22F 0.9600 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O3 H3A O5 . 0.82 2.11 2.821(4) 144.9 yes C1 H1A O15B . 0.97 2.25 2.78(2) 113.0 yes C3 H3B O11 . 0.98 2.47 3.330(6) 146.5 yes C4 H4A O15B . 0.98 2.54 3.12(2) 118.3 yes C16 H16A O3 . 0.96 2.62 3.222(6) 120.7 yes C16 H16C O15A . 0.96 2.39 2.946(7) 116.2 yes C37 H37B O9 4_566 0.96 2.39 3.239(8) 146.8 yes C37 H37C O15B 1_655 0.96 2.19 2.92(2) 132.2 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C15 C1 C2 O14B -156.8(15) C15 C1 C2 O14A -136.3(4) C15 C1 C2 C16 102.2(5) C15 C1 C2 C3 -24.0(5) C23 O12 C3 C4 -125.1(4) C23 O12 C3 C2 118.8(4) O14B C2 C3 O12 -106.0(13) O14A C2 C3 O12 -133.0(4) C16 C2 C3 O12 -5.0(5) C1 C2 C3 O12 118.2(4) O14B C2 C3 C4 134.2(13) O14A C2 C3 C4 107.1(4) C16 C2 C3 C4 -124.9(4) C1 C2 C3 C4 -1.7(5) O12 C3 C4 C15 -93.2(4) C2 C3 C4 C15 26.7(4) O12 C3 C4 C5 41.4(5) C2 C3 C4 C5 161.3(4) C25 O5 C5 C6 79.4(4) C25 O5 C5 C4 -155.9(3) C15 C4 C5 O5 54.8(5) C3 C4 C5 O5 -74.2(5) C15 C4 C5 C6 178.7(4) C3 C4 C5 C6 49.8(5) O5 C5 C6 C17 7.8(6) C4 C5 C6 C17 -115.7(5) O5 C5 C6 C7 -168.1(3) C4 C5 C6 C7 68.4(5) C32 O10 C7 C6 97.3(4) C32 O10 C7 C8 -142.2(4) C17 C6 C7 O10 36.6(6) C5 C6 C7 O10 -147.4(4) C17 C6 C7 C8 -83.7(5) C5 C6 C7 C8 92.4(4) C36 O6 C8 C9 93.3(5) C36 O6 C8 C7 -140.1(4) O10 C7 C8 O6 -30.8(5) C6 C7 C8 O6 89.7(4) O10 C7 C8 C9 92.3(4) C6 C7 C8 C9 -147.2(4) C38 O8 C9 C8 -123.8(4) C38 O8 C9 C10 109.4(4) O6 C8 C9 O8 80.8(4) C7 C8 C9 O8 -40.2(5) O6 C8 C9 C10 -156.1(4) C7 C8 C9 C10 82.9(4) O8 C9 C10 C11 60.7(5) C8 C9 C10 C11 -61.3(5) O8 C9 C10 C18 -174.6(4) C8 C9 C10 C18 63.3(5) O8 C9 C10 C19 -58.2(5) C8 C9 C10 C19 179.8(4) C18 C10 C11 C12 6.6(7) C19 C10 C11 C12 -112.6(5) C9 C10 C11 C12 128.5(5) C10 C11 C12 C13 172.8(4) C11 C12 C13 C20 -105.5(5) C11 C12 C13 C14 131.9(5) C40 O2 C14 C13 116.5(4) C40 O2 C14 C15 -114.2(4) C12 C13 C14 O2 34.6(4) C20 C13 C14 O2 -87.1(4) C12 C13 C14 C15 -89.0(4) C20 C13 C14 C15 149.3(4) C2 C1 C15 O3 -77.5(4) C2 C1 C15 C4 39.8(5) C2 C1 C15 C14 163.9(4) C5 C4 C15 O3 -62.9(5) C3 C4 C15 O3 71.6(4) C5 C4 C15 C1 -175.5(4) C3 C4 C15 C1 -41.1(4) C5 C4 C15 C14 64.0(5) C3 C4 C15 C14 -161.6(4) O2 C14 C15 O3 49.6(4) C13 C14 C15 O3 173.1(3) O2 C14 C15 C1 166.4(3) C13 C14 C15 C1 -70.0(5) O2 C14 C15 C4 -78.9(4) C13 C14 C15 C4 44.7(5) C3 O12 C23 O13 1.4(8) C3 O12 C23 C24 177.8(4) C5 O5 C25 O4 2.2(6) C5 O5 C25 C26 -176.2(3) O4 C25 C26 C31 12.9(7) O5 C25 C26 C31 -168.7(4) O4 C25 C26 C27 -161.3(5) O5 C25 C26 C27 17.0(6) C31 C26 C27 C28 0.1(7) C25 C26 C27 C28 174.4(5) C26 C27 C28 C29 -0.4(8) C27 C28 C29 C30 1.5(9) C28 C29 C30 C31 -2.2(9) C29 C30 C31 C26 1.9(8) C27 C26 C31 C30 -0.9(7) C25 C26 C31 C30 -175.2(4) C7 O10 C32 O11 7.8(7) C7 O10 C32 C33 -169.2(4) O11 C32 C33 C35 118.8(7) O10 C32 C33 C35 -64.4(7) O11 C32 C33 C34 -9.7(8) O10 C32 C33 C34 167.1(5) C8 O6 C36 O7 -6.2(7) C8 O6 C36 C37 175.0(4) C9 O8 C38 O9 -0.4(7) C9 O8 C38 C39 -179.1(4) C14 O2 C40 O1 5.7(7) C14 O2 C40 C41 -175.4(3) O1 C40 C41 C42 -169.8(5) O2 C40 C41 C42 11.3(6) O1 C40 C41 C46 9.5(7) O2 C40 C41 C46 -169.4(4) C46 C41 C42 C43 0.4(7) C40 C41 C42 C43 179.7(4) C41 C42 C43 C44 0.5(8) C42 C43 C44 C45 -0.4(8) C43 C44 C45 C46 -0.7(8) C44 C45 C46 C41 1.7(7) C42 C41 C46 C45 -1.5(7) C40 C41 C46 C45 179.1(4) C16 C2 O14A C21A -62.3(7) C3 C2 O14A C21A 67.0(7) C1 C2 O14A C21A 177.7(6) C2 O14A C21A O15A 3.8(11) C2 O14A C21A C22A -177.6(7) C16 C2 O14B C21B 179(2) C3 C2 O14B C21B -63(2) C1 C2 O14B C21B 65(3) C2 O14B C21B O15B -10(4) C2 O14B C21B C22B 161(3) _cod_database_fobs_code 2243205