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Information card for entry 2243362
Preview
Coordinates | 2243362.cif |
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Structure factors | 2243362.hkl |
Original IUCr paper | HTML |
Chemical name | Poly[bis[μ~3~-2-(4,4-dimethyl-2-oxazolin-2-yl)anilinido][μ~2~-2-(4,4-dimethyl-2-oxazolin-2-yl)aniline]tetrasodium(I)] |
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Formula | C44 H52 N8 Na4 O4 |
Calculated formula | C44 H52 N8 Na4 O4 |
Title of publication | Synthesis and crystal structures of tetrameric [2-(4,4-dimethyl-2-oxazolin-2-yl)anilido]sodium and tris[2-(4,4-dimethyl-2-oxazolin-2-yl)anilido]ytterbium(III) |
Authors of publication | Gajecki, Leah; Twamley, Brendan; Berg, David J. |
Journal of publication | Acta Crystallographica Section E |
Year of publication | 2020 |
Journal volume | 76 |
Journal issue | 5 |
Pages of publication | 703 - 709 |
a | 10.9545 ± 0.0005 Å |
b | 11.8785 ± 0.0005 Å |
c | 18.8415 ± 0.0008 Å |
α | 105.266 ± 0.001° |
β | 97.446 ± 0.001° |
γ | 106.12 ± 0.001° |
Cell volume | 2217.2 ± 0.17 Å3 |
Cell temperature | 87 ± 2 K |
Ambient diffraction temperature | 87 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.097 |
Residual factor for significantly intense reflections | 0.0659 |
Weighted residual factors for significantly intense reflections | 0.1443 |
Weighted residual factors for all reflections included in the refinement | 0.1577 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | Yes |
Revision | Date | Message | Files |
---|---|---|---|
251009 (current) | 2020-04-22 | cif/ hkl/ Adding structures of 2243362, 2243363 via cif-deposit CGI script. |
2243362.cif 2243362.hkl |
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Users of the data should acknowledge the original authors of the
structural data.