#------------------------------------------------------------------------------ #$Date: 2020-05-16 08:31:48 +0300 (Sat, 16 May 2020) $ #$Revision: 252095 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/33/2243393.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243393 _cell_angle_alpha 90.000 _cell_angle_beta 102.761 _cell_angle_gamma 90.000 _cell_length_a 17.0606 _cell_length_b 5.7820 _cell_length_c 12.5815 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.7623 _cod_data_source_file wm5557IIsup3.hkl _cod_data_source_block II _shelx_title ' hc2cg' _shelx_refln_list_code 4 _shelx_f_calc_maximum 245.86 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 377.46 407.67 0.95 o 4 0 0 1307.92 1205.91 5.07 o 5 0 0 1002.72 908.59 5.83 o 6 0 0 164.69 175.13 13.02 o 7 0 0 37.78 75.58 26.10 o 8 0 0 4.69 9.13 0.99 o 9 0 0 453.50 460.65 2.12 o 10 0 0 515.46 530.77 2.40 o 11 0 0 484.56 471.32 2.41 o 12 0 0 0.19 3.52 1.06 o 13 0 0 103.30 84.21 2.04 o 14 0 0 605.14 524.47 4.69 o 15 0 0 202.02 192.90 3.13 o 16 0 0 46.77 43.42 1.98 o 17 0 0 147.04 134.51 2.95 o 18 0 0 574.87 564.13 5.83 o 19 0 0 211.31 219.71 4.05 o 20 0 0 11.78 13.91 1.72 o 1 1 0 9918.15 9864.66 37.40 o 2 1 0 3329.97 3593.76 23.26 o 3 1 0 7.92 9.93 0.47 o 4 1 0 1077.08 965.68 2.37 o 5 1 0 172.46 202.09 2.00 o 6 1 0 213.57 189.25 1.07 o 7 1 0 533.97 555.97 1.59 o 8 1 0 255.16 251.52 3.46 o 9 1 0 220.37 234.69 1.62 o 10 1 0 595.33 584.06 4.66 o 11 1 0 202.60 216.71 2.27 o 12 1 0 0.04 0.15 0.41 o 13 1 0 15.66 14.88 0.97 o 14 1 0 199.56 180.36 3.52 o 15 1 0 225.40 210.37 2.36 o 16 1 0 44.98 39.97 1.34 o 17 1 0 196.10 188.79 2.41 o 18 1 0 6.00 5.87 1.21 o 19 1 0 22.03 21.74 1.47 o 20 1 0 43.73 41.34 3.65 o 0 2 0 1132.80 1215.84 4.44 o 1 2 0 388.37 416.76 4.90 o 2 2 0 2485.74 2503.75 23.24 o 3 2 0 712.83 648.74 2.22 o 4 2 0 39.51 37.42 1.10 o 5 2 0 4771.24 4966.26 129.74 o 6 2 0 1470.24 1496.68 7.15 o 7 2 0 254.68 276.77 1.79 o 8 2 0 66.76 81.99 2.85 o 9 2 0 100.50 95.67 1.27 o 10 2 0 26.19 28.48 0.71 o 11 2 0 4.27 3.07 0.60 o 12 2 0 41.90 44.66 1.76 o 13 2 0 87.91 86.57 3.23 o 14 2 0 809.21 777.69 6.02 o 15 2 0 0.00 1.16 1.54 o 16 2 0 21.55 23.27 1.68 o 17 2 0 52.44 51.14 2.18 o 18 2 0 0.00 1.54 1.75 o 19 2 0 0.06 -0.63 1.81 o 1 3 0 3.06 3.31 0.22 o 2 3 0 471.53 491.02 1.19 o 3 3 0 718.23 697.39 2.67 o 4 3 0 1983.63 2109.59 4.80 o 5 3 0 81.36 78.41 2.37 o 6 3 0 412.91 447.50 2.34 o 7 3 0 1363.52 1430.84 19.75 o 8 3 0 21.23 25.40 0.86 o 9 3 0 69.46 61.52 2.76 o 10 3 0 692.42 671.05 3.37 o 11 3 0 449.68 441.22 2.91 o 12 3 0 219.27 224.92 2.23 o 13 3 0 280.58 275.42 2.54 o 14 3 0 90.28 91.18 1.67 o 15 3 0 0.69 0.65 1.57 o 16 3 0 169.50 167.84 3.49 o 17 3 0 0.01 -0.75 1.45 o 18 3 0 19.29 18.10 2.02 o 0 4 0 943.53 951.16 5.74 o 1 4 0 584.21 563.57 3.18 o 2 4 0 115.98 111.71 1.61 o 3 4 0 107.96 106.32 1.55 o 4 4 0 80.01 74.54 1.90 o 5 4 0 693.20 711.71 5.19 o 6 4 0 106.79 109.49 2.27 o 7 4 0 0.01 -0.34 1.27 o 8 4 0 64.01 63.98 2.03 o 9 4 0 258.16 252.63 3.48 o 10 4 0 28.99 27.02 1.64 o 11 4 0 127.81 105.60 2.61 o 12 4 0 82.55 80.20 2.42 o 13 4 0 27.57 22.87 1.68 o 14 4 0 21.58 17.71 1.74 o 15 4 0 0.60 0.18 1.70 o 16 4 0 4.79 5.23 1.76 o 17 4 0 0.31 2.53 1.45 o 1 5 0 1692.85 1655.13 6.06 o 2 5 0 4.74 7.93 1.42 o 3 5 0 276.76 275.19 5.33 o 4 5 0 25.39 22.89 1.33 o 5 5 0 37.20 31.94 1.23 o 6 5 0 13.84 8.15 1.06 o 7 5 0 130.01 111.44 3.62 o 8 5 0 57.76 47.52 1.99 o 9 5 0 16.36 14.35 1.64 o 10 5 0 30.10 28.17 1.77 o 11 5 0 44.70 49.09 2.23 o 12 5 0 1.50 -0.46 1.57 o 13 5 0 0.98 2.95 1.72 o 14 5 0 3.32 6.60 1.82 o 15 5 0 45.50 46.63 2.51 o 0 6 0 837.31 823.90 6.82 o 1 6 0 67.49 66.82 1.79 o 2 6 0 0.55 1.87 1.04 o 3 6 0 0.06 -0.19 1.01 o 4 6 0 5.99 10.65 2.61 o 5 6 0 1.52 2.11 1.09 o 6 6 0 28.00 20.74 1.25 o 7 6 0 83.21 75.60 1.91 o 8 6 0 143.32 141.34 2.34 o 9 6 0 21.01 17.64 1.29 o 10 6 0 25.22 23.49 1.62 o 11 6 0 46.35 49.81 1.69 o 1 7 0 43.24 41.97 1.70 o 2 7 0 50.57 59.53 1.80 o 3 7 0 36.92 41.35 1.71 o 4 7 0 13.61 18.18 1.54 o 5 7 0 18.71 16.43 1.44 o 6 7 0 6.65 7.88 1.31 o 7 7 0 17.20 23.24 2.36 o -21 1 1 6.14 7.21 2.01 o -20 1 1 0.04 3.97 3.89 o -19 1 1 6.94 6.40 1.48 o -18 1 1 66.40 54.54 1.60 o -17 1 1 17.21 15.71 1.27 o -16 1 1 24.76 21.40 1.14 o -15 1 1 56.49 54.23 2.45 o -14 1 1 43.00 44.90 1.02 o -13 1 1 7.04 10.35 0.73 o -12 1 1 4.61 5.82 1.06 o -11 1 1 75.10 71.10 1.02 o -10 1 1 998.24 1031.53 7.47 o -9 1 1 9.55 10.18 0.42 o -8 1 1 32.21 34.04 0.54 o -7 1 1 48.32 44.28 0.53 o -6 1 1 564.44 595.50 3.17 o -5 1 1 8680.60 8435.64 54.60 o -4 1 1 2984.85 2839.45 58.95 o -3 1 1 1419.68 1362.05 9.62 o -2 1 1 91.45 102.63 1.06 o -1 1 1 1030.00 1080.83 4.76 o 0 1 1 464.64 477.07 4.66 o 1 1 1 329.42 348.40 1.22 o 2 1 1 65.57 77.37 2.81 o 3 1 1 449.32 458.97 1.48 o 4 1 1 2.59 4.19 1.10 o 5 1 1 65.07 70.00 0.66 o 6 1 1 249.19 240.29 2.09 o 7 1 1 28.50 33.25 0.70 o 8 1 1 50.40 54.86 0.69 o 9 1 1 114.37 126.13 1.21 o 10 1 1 771.48 766.02 2.78 o 11 1 1 38.53 38.58 1.08 o 12 1 1 138.83 140.63 3.55 o 13 1 1 222.33 220.45 6.23 o 14 1 1 221.75 220.79 10.65 o 15 1 1 14.53 12.67 1.13 o 16 1 1 10.82 9.00 1.10 o 17 1 1 69.53 61.44 1.63 o 18 1 1 20.63 18.60 1.37 o 19 1 1 82.28 79.62 1.94 o 20 1 1 3.10 5.15 1.21 o -20 2 1 0.82 1.81 1.55 o -19 2 1 1.99 3.00 1.64 o -18 2 1 23.71 20.30 1.95 o -17 2 1 5.00 6.99 1.61 o -16 2 1 181.32 183.75 2.31 o -15 2 1 141.00 146.09 2.06 o -14 2 1 318.28 323.35 2.74 o -13 2 1 558.52 520.94 19.98 o -12 2 1 95.34 103.90 8.63 o -11 2 1 90.99 102.66 1.45 o -10 2 1 5.48 4.89 0.54 o -9 2 1 148.39 156.05 1.56 o -8 2 1 12.83 11.62 0.67 o -7 2 1 20.07 23.85 1.47 o -6 2 1 2156.42 2242.11 7.09 o -5 2 1 388.83 378.13 2.86 o -4 2 1 536.66 528.38 2.07 o -3 2 1 4252.73 4367.21 20.61 o -2 2 1 2102.34 2174.41 5.57 o -1 2 1 1069.73 1124.28 4.77 o 0 2 1 94.01 95.64 1.29 o 1 2 1 0.08 0.75 0.32 o 2 2 1 76.93 65.27 0.93 o 3 2 1 650.53 661.56 1.73 o 4 2 1 562.56 548.09 2.01 o 5 2 1 111.28 106.84 4.38 o 6 2 1 197.14 205.73 1.79 o 7 2 1 70.22 87.88 1.09 o 8 2 1 22.44 28.04 0.79 o 9 2 1 182.40 191.18 1.71 o 10 2 1 284.67 278.94 2.14 o 11 2 1 317.48 304.60 3.43 o 12 2 1 1029.72 1053.80 6.51 o 13 2 1 29.56 30.08 1.71 o 14 2 1 105.10 106.11 2.61 o 15 2 1 126.51 121.03 2.73 o 16 2 1 13.86 13.73 1.56 o 17 2 1 44.68 44.30 2.20 o 18 2 1 2.24 0.68 1.68 o 19 2 1 17.43 13.32 1.94 o -19 3 1 23.00 25.55 2.04 o -18 3 1 2.54 1.93 1.76 o -17 3 1 54.39 52.23 1.59 o -16 3 1 6.34 6.93 1.19 o -15 3 1 11.09 10.47 1.05 o -14 3 1 123.75 117.25 1.87 o -13 3 1 254.41 239.88 3.04 o -12 3 1 294.40 291.31 2.50 o -11 3 1 224.30 220.67 5.80 o -10 3 1 4.63 4.77 0.82 o -9 3 1 110.94 117.61 1.49 o -8 3 1 228.67 241.77 1.97 o -7 3 1 272.53 269.28 3.02 o -6 3 1 331.71 378.35 3.44 o -5 3 1 13.91 19.92 0.52 o -4 3 1 832.18 813.09 10.01 o -3 3 1 3.44 8.29 0.35 o -2 3 1 160.20 144.99 1.00 o -1 3 1 39.10 32.75 0.54 o 0 3 1 4.61 8.12 1.08 o 1 3 1 3.47 2.29 0.37 o 2 3 1 438.10 457.05 3.25 o 3 3 1 687.59 705.97 2.85 o 4 3 1 1026.25 1072.21 2.65 o 5 3 1 64.01 67.64 0.99 o 6 3 1 192.17 187.36 1.45 o 7 3 1 11.77 10.56 0.66 o 8 3 1 132.46 120.38 1.83 o 9 3 1 189.54 164.56 1.69 o 10 3 1 64.59 61.99 1.23 o 11 3 1 2.91 2.78 0.85 o 12 3 1 16.70 16.37 1.00 o 13 3 1 153.89 149.84 3.01 o 14 3 1 11.19 11.76 1.72 o 15 3 1 21.67 20.52 1.72 o 16 3 1 9.78 9.23 1.76 o 17 3 1 0.07 -0.38 1.37 o 18 3 1 0.00 2.65 1.65 o -17 4 1 0.08 0.28 1.12 o -16 4 1 2.84 1.16 1.05 o -15 4 1 10.88 12.28 1.17 o -14 4 1 2.24 2.02 1.02 o -13 4 1 25.61 28.60 1.21 o -12 4 1 46.75 46.71 1.31 o -11 4 1 14.00 9.76 0.86 o -10 4 1 175.86 159.84 2.65 o -9 4 1 505.78 506.83 6.18 o -8 4 1 0.95 3.29 0.77 o -7 4 1 6.42 7.21 1.46 o -6 4 1 525.11 534.22 4.64 o -5 4 1 288.21 288.50 2.43 o -4 4 1 270.36 275.00 4.20 o -3 4 1 2.70 3.16 0.82 o -2 4 1 4.58 5.71 0.85 o -1 4 1 358.97 341.39 7.43 o 0 4 1 127.13 118.72 2.91 o 1 4 1 283.63 258.93 2.42 o 2 4 1 1.33 2.24 1.29 o 3 4 1 32.59 33.16 1.09 o 4 4 1 253.29 254.32 1.74 o 5 4 1 21.47 19.35 0.87 o 6 4 1 56.30 57.50 1.21 o 7 4 1 147.28 172.73 4.30 o 8 4 1 26.01 22.16 1.03 o 9 4 1 29.65 24.10 1.12 o 10 4 1 23.14 24.29 1.08 o 11 4 1 97.78 92.53 2.14 o 12 4 1 7.86 10.03 1.74 o 13 4 1 156.15 139.42 3.11 o 14 4 1 2.12 1.34 1.58 o 15 4 1 117.78 116.11 2.92 o 16 4 1 15.65 24.35 2.02 o -15 5 1 4.73 8.05 1.83 o -14 5 1 28.63 29.80 2.11 o -13 5 1 88.94 87.31 2.79 o -12 5 1 43.10 49.83 2.25 o -11 5 1 28.56 27.06 1.78 o -10 5 1 3.72 4.32 1.47 o -9 5 1 0.03 1.07 1.49 o -8 5 1 0.10 0.36 1.03 o -7 5 1 33.05 32.96 1.92 o -6 5 1 19.33 15.95 1.34 o -5 5 1 13.37 12.99 1.13 o -4 5 1 122.79 117.74 1.94 o -3 5 1 1.63 5.47 2.52 o -2 5 1 316.55 308.56 2.80 o -1 5 1 45.81 45.88 1.48 o 0 5 1 23.57 22.45 1.31 o 1 5 1 433.37 427.30 3.23 o 2 5 1 266.38 265.90 2.61 o 3 5 1 245.30 256.53 2.56 o 4 5 1 27.31 33.10 1.85 o 5 5 1 45.33 49.52 1.40 o 6 5 1 26.72 26.66 1.24 o 7 5 1 18.29 14.89 0.95 o 8 5 1 106.80 87.68 2.37 o 9 5 1 0.07 1.10 1.47 o 10 5 1 11.32 12.74 1.63 o 11 5 1 14.15 13.70 1.56 o 12 5 1 86.70 84.69 2.65 o 13 5 1 108.21 103.02 2.88 o 14 5 1 51.60 64.75 2.54 o -12 6 1 14.12 18.60 2.26 o -11 6 1 43.06 53.14 1.98 o -10 6 1 1.57 2.37 1.20 o -9 6 1 8.46 6.76 1.91 o -8 6 1 1.17 0.54 1.19 o -7 6 1 10.89 9.92 1.17 o -6 6 1 6.18 7.53 1.15 o -5 6 1 6.18 5.63 2.08 o -4 6 1 76.41 76.44 1.78 o -3 6 1 167.10 164.81 2.35 o -2 6 1 0.57 2.26 1.11 o -1 6 1 79.59 82.11 2.30 o 0 6 1 39.32 34.81 2.48 o 1 6 1 2.38 3.32 1.08 o 2 6 1 3.06 3.97 0.95 o 3 6 1 2.12 0.99 1.02 o 4 6 1 18.61 17.22 1.18 o 5 6 1 63.63 62.76 1.74 o 6 6 1 9.62 10.78 1.25 o 7 6 1 74.14 79.47 1.81 o 8 6 1 7.67 9.88 1.48 o 9 6 1 35.50 36.30 1.55 o 10 6 1 4.72 4.06 1.19 o 11 6 1 2.28 2.15 1.32 o -8 7 1 0.76 1.40 1.60 o -7 7 1 11.40 16.11 1.97 o -6 7 1 5.60 4.98 1.87 o -5 7 1 10.11 8.84 1.64 o -4 7 1 39.43 38.79 1.70 o -3 7 1 9.94 8.49 1.34 o -2 7 1 0.74 1.72 1.12 o -1 7 1 14.74 17.99 1.40 o 0 7 1 17.60 23.59 1.45 o 1 7 1 54.80 65.79 2.72 o 2 7 1 21.75 23.25 1.51 o 3 7 1 27.76 31.76 2.11 o 4 7 1 0.00 2.14 2.78 o 5 7 1 47.86 51.78 1.82 o 6 7 1 32.15 37.65 1.69 o -21 0 2 54.81 55.37 2.51 o -20 0 2 3.72 5.93 1.70 o -19 0 2 252.51 250.31 4.10 o -18 0 2 505.36 482.33 5.20 o -17 0 2 436.09 434.86 4.73 o -16 0 2 255.75 245.61 3.47 o -15 0 2 33.25 37.96 1.69 o -14 0 2 37.75 40.85 1.57 o -13 0 2 10.56 8.15 0.86 o -12 0 2 4.81 5.35 0.78 o -11 0 2 358.69 380.68 5.82 o -10 0 2 1610.95 1608.67 3.60 o -9 0 2 218.38 203.84 3.07 o -8 0 2 6.30 3.84 0.38 o -7 0 2 162.01 180.45 1.61 o -6 0 2 966.21 888.54 5.57 o -5 0 2 1068.68 1279.70 7.17 o -4 0 2 60446.25 59748.17 164.95 o -3 0 2 869.91 833.65 12.70 o -2 0 2 2308.42 2132.82 19.76 o -1 0 2 70.70 112.91 3.44 o 0 0 2 4.64 16.27 2.56 o 1 0 2 103.59 66.49 0.90 o 2 0 2 2335.02 2317.55 16.75 o 3 0 2 2429.72 2170.29 4.67 o 4 0 2 14.99 6.84 0.57 o 5 0 2 361.91 317.72 1.27 o 6 0 2 89.21 70.41 0.61 o 7 0 2 73.00 68.98 0.68 o 8 0 2 7.57 6.30 0.37 o 9 0 2 1137.36 1172.19 3.08 o 10 0 2 105.62 104.38 1.95 o 11 0 2 184.51 196.32 2.72 o 12 0 2 17.55 18.80 1.29 o 13 0 2 32.07 31.18 1.56 o 14 0 2 31.57 40.64 1.83 o 15 0 2 1207.09 1184.97 7.64 o 16 0 2 361.13 345.42 4.52 o 17 0 2 139.78 136.30 3.29 o 18 0 2 544.23 555.51 6.06 o 19 0 2 26.51 35.49 2.27 o -21 1 2 33.00 29.20 2.07 o -20 1 2 7.99 14.47 6.37 o -19 1 2 29.01 29.41 1.78 o -18 1 2 20.48 19.64 1.22 o -17 1 2 0.85 1.24 0.94 o -16 1 2 11.71 8.89 0.86 o -15 1 2 2.12 1.30 0.73 o -14 1 2 4.31 3.87 0.70 o -13 1 2 26.45 26.43 0.84 o -12 1 2 4.50 3.10 0.60 o -11 1 2 707.55 721.80 2.28 o -10 1 2 7.65 11.92 1.27 o -9 1 2 502.20 484.40 1.70 o -8 1 2 1137.37 1197.97 2.21 o -7 1 2 2915.30 2946.92 8.11 o -6 1 2 96.79 103.23 0.61 o -5 1 2 621.07 645.93 15.37 o -4 1 2 49.69 37.68 0.79 o -3 1 2 12174.13 12035.57 52.01 o -2 1 2 2704.35 2653.05 11.07 o -1 1 2 523.22 469.97 1.61 o 0 1 2 1810.87 1706.41 15.91 o 1 1 2 302.12 363.44 1.32 o 2 1 2 38.88 26.87 0.50 o 3 1 2 1465.57 1378.54 3.93 o 4 1 2 183.84 223.82 1.81 o 5 1 2 478.09 574.25 3.08 o 6 1 2 3548.42 3642.58 18.92 o 7 1 2 2293.42 2382.77 3.56 o 8 1 2 621.15 595.74 5.58 o 9 1 2 52.67 58.92 0.71 o 10 1 2 0.30 0.58 0.73 o 11 1 2 396.05 411.95 2.75 o 12 1 2 265.49 263.04 5.86 o 13 1 2 162.35 154.56 1.96 o 14 1 2 23.89 22.61 1.17 o 15 1 2 110.65 111.69 1.96 o 16 1 2 234.60 223.14 2.62 o 17 1 2 168.91 164.50 3.29 o 18 1 2 9.71 12.73 2.26 o 19 1 2 20.84 24.39 1.35 o -20 2 2 8.06 4.67 1.76 o -19 2 2 4.95 5.02 1.70 o -18 2 2 313.64 306.25 3.09 o -17 2 2 28.62 31.36 1.39 o -16 2 2 51.56 51.16 1.47 o -15 2 2 192.66 196.80 5.85 o -14 2 2 249.40 245.51 3.45 o -13 2 2 125.95 120.50 1.71 o -12 2 2 123.69 129.47 1.71 o -11 2 2 1.22 1.09 0.77 o -10 2 2 280.65 293.98 5.33 o -9 2 2 303.22 329.85 1.83 o -8 2 2 2.95 5.07 0.66 o -7 2 2 0.00 1.18 0.94 o -6 2 2 2077.72 2040.15 6.38 o -5 2 2 44.44 44.71 0.81 o -4 2 2 2847.60 2927.25 5.03 o -3 2 2 463.26 493.52 2.02 o -2 2 2 1815.67 1815.02 3.76 o -1 2 2 947.72 885.15 4.62 o 0 2 2 17.70 18.03 0.47 o 1 2 2 10051.19 10326.34 36.32 o 2 2 2 234.73 219.03 0.93 o 3 2 2 33.27 32.12 0.48 o 4 2 2 1203.51 1285.40 8.28 o 5 2 2 641.70 621.83 3.58 o 6 2 2 3.22 3.31 0.72 o 7 2 2 4.49 2.10 0.77 o 8 2 2 172.59 192.04 2.44 o 9 2 2 81.45 68.82 1.69 o 10 2 2 687.77 651.75 4.68 o 11 2 2 1.85 2.72 1.15 o 12 2 2 57.30 57.31 2.01 o 13 2 2 284.38 274.59 3.66 o 14 2 2 282.87 275.85 3.86 o 15 2 2 51.47 47.62 2.18 o 16 2 2 37.21 36.59 2.15 o 17 2 2 31.75 37.87 2.37 o 18 2 2 201.26 205.40 3.95 o 19 2 2 54.04 63.84 2.70 o -19 3 2 31.47 32.17 1.52 o -18 3 2 14.51 16.77 1.34 o -17 3 2 131.61 127.37 2.13 o -16 3 2 24.68 26.39 1.24 o -15 3 2 51.30 50.67 1.50 o -14 3 2 28.22 25.05 1.18 o -13 3 2 15.76 14.34 1.39 o -12 3 2 60.09 59.36 1.35 o -11 3 2 8.67 10.62 0.93 o -10 3 2 71.87 63.37 1.79 o -9 3 2 3.96 3.45 0.78 o -8 3 2 520.38 524.90 4.28 o -7 3 2 434.91 431.59 3.80 o -6 3 2 33.65 42.82 0.91 o -5 3 2 157.03 150.14 1.41 o -4 3 2 57.60 59.53 0.92 o -3 3 2 28.92 33.49 0.63 o -2 3 2 13.05 7.36 0.45 o -1 3 2 337.36 344.31 2.09 o 0 3 2 104.79 82.70 1.33 o 1 3 2 25.24 23.68 1.04 o 2 3 2 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