#------------------------------------------------------------------------------
#$Date: 2020-06-06 08:30:26 +0300 (Sat, 06 Jun 2020) $
#$Revision: 252982 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/34/2243425.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2243425
_cell_angle_alpha                90.534
_cell_angle_beta                 104.376
_cell_angle_gamma                101.135
_cell_length_a                   8.3146
_cell_length_b                   8.6714
_cell_length_c                   14.5827
_exptl_crystal_F_000             556.00
_reflns_d_resolution_high        0.8000
_cod_data_source_file            mw2159Isup2.hkl
_cod_data_source_block           I
_shelx_title                     ' Chi25 in P-1 No.2'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            220.99
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 3934.77 3822.68 46.49 o
3 0 0 19969.84 20304.73 233.38 o
4 0 0 21405.16 21610.31 254.70 o
5 0 0 9122.86 9044.97 190.84 o
6 0 0 6848.95 6827.94 140.63 o
7 0 0 5930.33 6073.32 175.20 o
8 0 0 7998.95 7957.13 194.35 o
9 0 0 5422.60 5317.28 163.48 o
-10 1 0 1633.30 1537.06 103.19 o
-9 1 0 2428.65 2293.01 139.84 o
-8 1 0 7333.94 7025.27 253.23 o
-7 1 0 2680.32 2697.26 169.63 o
-6 1 0 4584.93 4464.14 92.85 o
-5 1 0 7498.87 7331.12 116.83 o
-4 1 0 20961.35 21073.23 246.13 o
-3 1 0 22360.13 22545.13 226.20 o
-2 1 0 16529.25 16790.58 186.54 o
-1 1 0 18372.46 18370.73 290.04 o
1 1 0 7672.98 7810.76 75.69 o
2 1 0 9058.46 8883.09 87.91 o
3 1 0 10900.11 10967.53 118.46 o
4 1 0 8235.83 7830.69 147.40 o
5 1 0 9327.93 9518.21 184.03 o
6 1 0 2536.48 2643.14 73.19 o
7 1 0 10942.49 10578.08 259.13 o
8 1 0 8669.11 8545.83 328.99 o
9 1 0 2191.50 2058.57 97.40 o
-10 2 0 973.78 912.28 97.27 o
-9 2 0 1890.26 1773.56 124.96 o
-8 2 0 3337.29 3432.58 230.01 o
-7 2 0 5477.30 5757.16 174.96 o
-6 2 0 3068.78 2988.62 77.99 o
-5 2 0 5123.35 5103.81 102.23 o
-4 2 0 14653.01 14562.22 185.14 o
-3 2 0 10621.58 10670.33 130.23 o
-2 2 0 243.86 295.55 15.65 o
-1 2 0 17713.49 17879.59 191.58 o
0 2 0 10090.42 10310.49 92.61 o
1 2 0 4730.44 4653.81 50.31 o
2 2 0 5701.37 5673.71 59.64 o
3 2 0 8744.20 8905.63 107.22 o
4 2 0 9177.10 9241.88 161.98 o
5 2 0 6073.78 5942.45 128.69 o
6 2 0 2586.56 2539.72 66.09 o
7 2 0 2676.81 2736.26 150.65 o
8 2 0 3292.24 3320.05 144.46 o
9 2 0 880.78 808.74 85.28 o
-10 3 0 57.07 98.78 36.00 o
-9 3 0 425.84 539.47 72.44 o
-8 3 0 346.76 401.14 75.16 o
-7 3 0 1834.92 1754.08 92.36 o
-6 3 0 731.42 710.50 46.23 o
-5 3 0 91.72 107.83 14.43 o
-4 3 0 615.27 530.25 26.30 o
-3 3 0 5530.92 5627.25 119.81 o
-2 3 0 1284.62 1373.47 40.08 o
-1 3 0 51.27 44.81 5.19 o
0 3 0 5316.25 5380.15 60.77 o
1 3 0 3816.95 3913.48 49.78 o
2 3 0 1138.62 1160.98 25.12 o
3 3 0 498.64 462.10 19.62 o
4 3 0 3034.27 3099.56 62.99 o
5 3 0 424.44 430.81 23.54 o
6 3 0 684.75 718.21 38.65 o
7 3 0 907.68 845.90 66.72 o
8 3 0 947.12 863.06 88.72 o
-9 4 0 298.45 282.92 42.07 o
-8 4 0 325.81 338.30 44.23 o
-7 4 0 771.74 777.21 61.68 o
-6 4 0 290.04 280.77 35.19 o
-5 4 0 191.31 164.19 19.38 o
-4 4 0 2005.24 2251.78 128.48 o
-3 4 0 10.89 59.36 15.75 o
-2 4 0 70.57 160.95 19.91 o
-1 4 0 2.73 28.89 5.96 o
0 4 0 185.82 257.26 14.57 o
1 4 0 3.14 18.56 5.86 o
2 4 0 22.93 26.08 4.64 o
3 4 0 338.19 356.32 16.06 o
4 4 0 39.10 37.45 7.19 o
5 4 0 0.79 7.50 8.88 o
6 4 0 821.35 789.74 47.64 o
7 4 0 16.71 -12.41 23.33 o
8 4 0 280.45 293.87 47.42 o
-9 5 0 983.36 938.00 79.36 o
-8 5 0 434.60 441.30 50.79 o
-7 5 0 681.41 609.08 55.52 o
-6 5 0 2045.11 2141.16 98.57 o
-5 5 0 2381.89 2395.38 190.94 o
-4 5 0 543.57 527.14 34.28 o
-3 5 0 1375.74 1419.17 55.44 o
-2 5 0 4564.54 4609.79 135.65 o
-1 5 0 2103.21 2155.02 46.32 o
0 5 0 67.07 107.28 10.77 o
1 5 0 1099.05 1117.99 32.24 o
2 5 0 5500.10 5589.00 74.40 o
3 5 0 1086.02 1096.73 35.60 o
4 5 0 167.93 156.56 16.17 o
5 5 0 189.22 161.52 19.59 o
6 5 0 1585.80 1592.87 72.99 o
7 5 0 217.56 208.59 65.61 o
-9 6 0 3173.52 3073.96 245.29 o
-8 6 0 2107.47 2173.34 115.58 o
-7 6 0 2340.44 2357.46 113.09 o
-6 6 0 4067.38 4070.95 142.90 o
-5 6 0 4145.84 4160.79 116.40 o
-4 6 0 4269.02 4241.50 114.59 o
-3 6 0 7597.58 7698.71 165.79 o
-2 6 0 7585.07 7616.95 170.91 o
-1 6 0 5591.02 5477.23 101.99 o
0 6 0 6893.03 7139.21 151.91 o
1 6 0 4776.30 4894.48 103.17 o
2 6 0 5650.42 5676.37 112.08 o
3 6 0 2245.95 2296.35 72.17 o
4 6 0 2336.50 2388.05 77.43 o
5 6 0 4841.39 4937.43 136.57 o
6 6 0 4055.66 3999.43 143.28 o
7 6 0 1865.18 1836.30 148.15 o
-8 7 0 3001.98 2917.16 171.66 o
-7 7 0 4043.27 4133.63 196.15 o
-6 7 0 8770.81 8460.57 256.71 o
-5 7 0 5735.74 5794.09 196.47 o
-4 7 0 5383.85 5399.04 139.77 o
-3 7 0 8582.20 8658.18 188.72 o
-2 7 0 11115.79 11381.87 224.99 o
-1 7 0 6702.77 6868.76 149.33 o
0 7 0 3245.99 3359.38 101.57 o
1 7 0 3449.80 3706.55 100.28 o
2 7 0 9237.48 8411.15 844.96 o
3 7 0 6991.64 7143.74 148.03 o
4 7 0 3447.08 3669.31 116.63 o
5 7 0 5005.38 4801.19 141.20 o
6 7 0 4267.09 4285.96 184.71 o
-8 8 0 3507.69 3584.55 197.46 o
-7 8 0 4973.59 4933.44 182.77 o
-6 8 0 7780.38 7800.99 304.36 o
-5 8 0 6905.33 6570.29 221.67 o
-4 8 0 7806.58 7834.08 237.56 o
-3 8 0 4761.10 4661.31 174.50 o
-2 8 0 3480.13 3360.68 100.32 o
-1 8 0 9904.55 9982.19 218.49 o
0 8 0 6567.47 6584.18 201.37 o
1 8 0 7653.24 8287.60 231.28 o
2 8 0 7323.69 7348.42 403.24 o
3 8 0 5967.24 5995.84 204.33 o
4 8 0 4167.41 4146.08 151.17 o
5 8 0 4466.69 4292.19 186.22 o
-7 9 0 2556.50 2733.19 162.07 o
-6 9 0 2645.20 2457.01 138.49 o
-5 9 0 3564.42 3438.49 161.13 o
-4 9 0 1236.40 1357.33 94.52 o
-3 9 0 2423.16 2304.52 152.20 o
-2 9 0 7828.84 8011.10 204.59 o
-1 9 0 6134.92 6197.91 207.14 o
0 9 0 1338.13 1435.37 122.11 o
1 9 0 3397.21 3731.48 192.33 o
2 9 0 5457.87 5392.48 203.33 o
3 9 0 2824.92 2958.07 189.52 o
-5 10 0 2319.05 2205.57 132.69 o
-4 10 0 2078.51 1848.94 198.51 o
-3 10 0 1354.87 1222.76 150.19 o
-2 10 0 3302.42 3392.44 157.34 o
-1 10 0 2063.93 1968.02 141.90 o
0 10 0 2045.46 2235.51 152.47 o
1 10 0 1660.12 1625.47 190.24 o
-2 -10 1 3167.64 3026.75 237.51 o
-1 -10 1 2765.69 2534.23 288.48 o
0 -10 1 4523.12 4512.15 332.28 o
1 -10 1 6739.13 6886.68 278.74 o
2 -10 1 4328.12 4283.68 179.61 o
3 -10 1 4322.27 3783.20 145.95 o
4 -10 1 5332.48 5314.08 224.70 o
5 -10 1 7290.46 6953.11 251.86 o
-3 -9 1 4796.93 4934.69 195.79 o
-2 -9 1 3164.89 3220.27 151.39 o
-1 -9 1 3884.61 3777.08 221.21 o
0 -9 1 4098.03 4045.46 160.70 o
1 -9 1 6019.92 6176.98 225.06 o
2 -9 1 6883.75 7153.88 193.33 o
3 -9 1 3079.86 2677.61 307.86 o
4 -9 1 1689.20 1702.49 108.06 o
5 -9 1 2716.41 2534.28 138.38 o
6 -9 1 3128.11 2995.61 157.48 o
7 -9 1 2083.35 2161.47 123.45 o
-5 -8 1 611.12 554.22 76.93 o
-4 -8 1 1090.38 1147.65 96.23 o
-3 -8 1 2725.57 2655.29 130.25 o
-2 -8 1 2919.69 2906.44 113.25 o
-1 -8 1 694.24 739.23 61.20 o
0 -8 1 1253.01 1392.18 67.66 o
1 -8 1 1740.04 1826.32 81.40 o
2 -8 1 1312.35 1333.65 75.20 o
3 -8 1 114.10 113.14 27.58 o
4 -8 1 1744.96 1634.70 101.10 o
5 -8 1 3221.68 3226.43 150.53 o
6 -8 1 743.88 729.66 73.00 o
7 -8 1 627.32 722.76 118.08 o
-6 -7 1 475.13 465.30 56.14 o
-5 -7 1 61.18 53.85 19.73 o
-4 -7 1 322.96 311.84 28.52 o
-3 -7 1 441.41 437.36 32.99 o
-2 -7 1 695.89 682.01 61.63 o
-1 -7 1 14.77 15.94 11.59 o
0 -7 1 169.78 139.59 22.01 o
1 -7 1 1097.08 1128.78 59.83 o
2 -7 1 848.00 832.65 61.47 o
3 -7 1 303.41 332.05 29.98 o
4 -7 1 552.23 623.61 61.12 o
5 -7 1 916.09 823.64 70.57 o
6 -7 1 61.64 48.13 21.32 o
7 -7 1 232.41 199.53 49.02 o
8 -7 1 33.28 126.41 39.94 o
-7 -6 1 44.10 26.31 25.96 o
-6 -6 1 30.10 69.38 18.32 o
-5 -6 1 996.95 1031.33 52.14 o
-4 -6 1 1062.36 989.18 43.47 o
-3 -6 1 69.11 49.63 9.63 o
-2 -6 1 685.19 688.51 33.74 o
-1 -6 1 474.58 457.57 31.91 o
0 -6 1 537.23 514.49 35.34 o
1 -6 1 125.94 128.17 20.58 o
2 -6 1 1452.94 1433.73 72.00 o
3 -6 1 1993.30 1949.19 115.42 o
4 -6 1 405.91 396.28 30.37 o
5 -6 1 45.42 74.29 31.44 o
6 -6 1 420.13 412.07 76.30 o
7 -6 1 1583.53 1477.00 91.09 o
8 -6 1 167.74 160.23 32.82 o
9 -6 1 6.96 14.29 19.72 o
-7 -5 1 1105.18 1036.36 74.33 o
-6 -5 1 1994.19 2011.17 73.57 o
-5 -5 1 569.21 631.13 37.10 o
-4 -5 1 2646.37 2623.50 69.41 o
-3 -5 1 2056.95 2068.58 45.97 o
-2 -5 1 1017.10 994.10 33.66 o
-1 -5 1 7218.03 7384.06 111.45 o
0 -5 1 4714.66 4761.42 104.48 o
1 -5 1 1109.57 1123.85 36.85 o
2 -5 1 3774.22 3783.59 96.09 o
3 -5 1 6869.44 7066.15 146.31 o
4 -5 1 2336.91 2297.97 72.04 o
5 -5 1 1753.28 1819.65 71.86 o
6 -5 1 1114.70 1082.03 86.06 o
7 -5 1 3268.80 3339.03 136.52 o
8 -5 1 1262.57 1290.14 88.61 o
9 -5 1 214.05 150.41 35.45 o
-8 -4 1 4230.57 4382.98 247.59 o
-7 -4 1 3570.26 3623.91 145.19 o
-6 -4 1 3586.70 3583.44 99.66 o
-5 -4 1 9913.25 10086.02 171.70 o
-4 -4 1 11799.51 12075.95 167.93 o
-3 -4 1 7709.41 7608.55 114.75 o
-2 -4 1 6815.06 6650.81 91.77 o
-1 -4 1 23190.60 23391.04 238.04 o
0 -4 1 15851.84 15935.70 209.67 o
1 -4 1 10428.73 10621.34 154.28 o
2 -4 1 9250.13 9105.76 322.20 o
3 -4 1 11460.98 11077.40 194.93 o
4 -4 1 8296.35 8449.29 212.52 o
5 -4 1 3149.01 3317.64 106.89 o
6 -4 1 4325.59 4389.33 146.24 o
7 -4 1 5819.83 5933.11 185.97 o
8 -4 1 3999.95 3983.16 159.47 o
9 -4 1 2265.24 2134.57 125.95 o
-9 -3 1 3223.51 3374.01 155.23 o
-8 -3 1 6084.75 5939.97 199.77 o
-7 -3 1 5680.28 5672.40 259.16 o
-6 -3 1 3181.62 3155.38 81.46 o
-5 -3 1 10073.13 9904.93 166.62 o
-4 -3 1 13834.10 13797.34 172.14 o
-3 -3 1 7966.62 8387.37 110.02 o
-2 -3 1 15790.77 15666.29 156.87 o
-1 -3 1 26264.43 25957.22 213.23 o
0 -3 1 13029.01 12896.50 135.93 o
1 -3 1 9505.58 9750.98 113.57 o
2 -3 1 11202.32 11259.35 142.88 o
3 -3 1 20231.76 20586.62 322.55 o
4 -3 1 18237.64 17682.81 262.56 o
5 -3 1 3839.28 3777.60 144.73 o
6 -3 1 7383.74 7299.30 214.36 o
7 -3 1 17292.94 16515.04 346.98 o
8 -3 1 9003.08 8574.76 257.34 o
9 -3 1 2992.27 2951.69 140.73 o
-9 -2 1 4942.89 4922.45 219.34 o
-8 -2 1 4647.96 4597.50 164.91 o
-7 -2 1 4389.93 4560.44 152.89 o
-6 -2 1 6997.78 7066.96 135.40 o
-5 -2 1 14305.28 14160.89 209.81 o
-4 -2 1 18295.92 18047.40 236.85 o
-3 -2 1 9296.45 9214.94 105.32 o
-2 -2 1 5719.96 5514.34 61.70 o
-1 -2 1 31105.48 29608.87 254.88 o
0 -2 1 34066.87 31669.48 354.62 o
1 -2 1 3309.10 3228.72 61.92 o
2 -2 1 5529.19 5938.37 94.93 o
3 -2 1 15903.94 15826.75 224.69 o
4 -2 1 19347.91 19249.49 318.38 o
5 -2 1 15084.58 14595.59 214.17 o
6 -2 1 9466.54 8954.24 158.04 o
7 -2 1 4614.10 4704.14 158.45 o
8 -2 1 4063.96 3941.28 153.60 o
9 -2 1 2817.34 2826.16 199.77 o
-9 -1 1 2540.80 2640.02 128.35 o
-8 -1 1 5120.33 5131.19 150.71 o
-7 -1 1 3385.26 3390.81 93.03 o
-6 -1 1 4484.32 4458.99 80.90 o
-5 -1 1 9046.18 8899.14 154.66 o
-4 -1 1 11617.85 11461.58 132.70 o
-3 -1 1 1576.71 1470.89 27.92 o
-2 -1 1 6196.36 6128.61 63.12 o
-1 -1 1 7560.20 7634.82 63.04 o
0 -1 1 11279.85 10913.45 319.05 o
1 -1 1 14393.10 13977.03 180.63 o
2 -1 1 18574.36 18769.20 230.99 o
3 -1 1 23022.49 23194.03 245.60 o
4 -1 1 11449.60 11329.11 167.00 o
5 -1 1 1347.38 1333.48 41.39 o
6 -1 1 3610.00 3578.62 76.69 o
7 -1 1 9999.10 10275.91 227.27 o
8 -1 1 2484.16 2398.76 184.29 o
9 -1 1 1488.68 1332.28 123.30 o
-9 0 1 1611.16 1542.28 95.25 o
-8 0 1 2865.57 2813.33 107.77 o
-7 0 1 1053.20 1075.86 60.21 o
-6 0 1 468.91 471.56 28.95 o
-5 0 1 1949.33 1899.76 55.98 o
-4 0 1 4069.01 3934.96 80.21 o
-3 0 1 631.01 744.00 27.71 o
-2 0 1 3311.31 3285.79 42.88 o
1 0 1 14376.92 13917.12 205.39 o
2 0 1 65.68 94.49 7.15 o
3 0 1 1519.25 1622.62 55.97 o
4 0 1 3389.91 3447.40 90.07 o
5 0 1 2272.63 2148.77 85.91 o
6 0 1 623.79 674.77 62.16 o
7 0 1 2082.76 2036.97 95.46 o
8 0 1 1316.47 1289.37 95.34 o
9 0 1 605.85 624.74 68.44 o
-10 1 1 70.87 63.07 25.19 o
-9 1 1 67.68 64.59 21.40 o
-8 1 1 357.66 355.19 52.20 o
-7 1 1 307.85 284.35 42.48 o
-6 1 1 147.22 139.31 15.23 o
-5 1 1 820.27 809.26 31.93 o
-4 1 1 1249.52 1235.60 38.09 o
-3 1 1 6737.76 7009.96 83.40 o
-2 1 1 205.39 238.56 9.66 o
-1 1 1 1572.73 1720.24 43.09 o
0 1 1 6345.44 6524.71 128.24 o
1 1 1 15.09 23.65 3.24 o
2 1 1 171.42 188.37 8.28 o
3 1 1 5890.17 6395.03 95.75 o
4 1 1 449.69 475.80 25.02 o
5 1 1 77.29 110.15 14.80 o
6 1 1 2129.48 2225.67 132.20 o
7 1 1 97.14 135.67 22.37 o
8 1 1 104.67 103.64 21.21 o
9 1 1 5.77 7.56 35.77 o
-10 2 1 849.78 867.49 93.35 o
-9 2 1 307.08 300.37 52.05 o
-8 2 1 62.91 90.98 48.35 o
-7 2 1 837.59 832.33 73.12 o
-6 2 1 1307.93 1257.59 46.35 o
-5 2 1 277.74 275.44 19.70 o
-4 2 1 1026.08 1143.41 35.24 o
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-1 2 1 8678.94 8759.20 112.94 o
0 2 1 45.98 60.68 4.42 o
1 2 1 2768.53 2875.80 41.03 o
2 2 1 879.86 856.72 18.29 o
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4 2 1 202.81 196.90 14.27 o
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6 2 1 1529.53 1613.15 57.53 o
7 2 1 12.44 25.22 9.70 o
8 2 1 59.40 30.50 25.01 o
9 2 1 742.76 732.00 101.10 o
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5 3 1 2482.52 2494.62 59.87 o
6 3 1 4329.78 4611.49 135.74 o
7 3 1 1759.98 1643.54 94.19 o
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-1 4 1 4811.56 4580.59 80.68 o
0 4 1 11884.62 12313.42 125.41 o
1 4 1 15855.58 16125.97 180.08 o
2 4 1 16030.07 15475.95 198.45 o
3 4 1 6107.22 6048.94 100.64 o
4 4 1 7367.03 7378.70 108.64 o
5 4 1 10858.78 10809.96 201.86 o
6 4 1 4652.93 4577.29 154.42 o
7 4 1 2128.64 2038.16 105.22 o
8 4 1 1950.69 2090.71 119.96 o
-9 5 1 2925.99 3049.71 142.18 o
-8 5 1 4495.04 4421.59 163.65 o
-7 5 1 5890.67 5920.06 181.35 o
-6 5 1 8660.02 8773.62 185.66 o
-5 5 1 3027.78 3090.42 150.35 o
-4 5 1 4392.41 4507.35 144.46 o
-3 5 1 14296.45 14098.85 246.21 o
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-1 5 1 11450.86 11358.19 147.79 o
0 5 1 14425.66 14648.30 169.96 o
1 5 1 14817.34 14781.89 169.69 o
2 5 1 11910.97 11988.35 186.33 o
3 5 1 13008.26 13006.76 220.43 o
4 5 1 4775.62 4827.13 95.45 o
5 5 1 4579.36 4975.12 133.13 o
6 5 1 4510.18 4432.31 162.36 o
7 5 1 3893.08 3873.66 450.84 o
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-7 6 1 5372.95 5632.50 178.84 o
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