#------------------------------------------------------------------------------
#$Date: 2020-06-06 08:30:26 +0300 (Sat, 06 Jun 2020) $
#$Revision: 252982 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/34/2243427.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2243427
_cell_angle_alpha                95.782
_cell_angle_beta                 102.874
_cell_angle_gamma                93.843
_cell_length_a                   7.8746
_cell_length_b                   9.7566
_cell_length_c                   15.0004
_exptl_crystal_F_000             600.00
_reflns_d_resolution_high        0.8001
_cod_data_source_file            mw2159IIIsup4.hkl
_cod_data_source_block           III
_shelx_title                     ' CHI32 in P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            300.29
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 12917.46 12951.77 172.57 o
2 0 0 185.86 224.71 10.69 o
3 0 0 63.19 82.98 7.67 o
4 0 0 3898.36 3997.39 116.12 o
5 0 0 1800.22 1733.97 72.08 o
6 0 0 4351.08 4477.69 136.32 o
7 0 0 3668.38 3806.64 204.10 o
8 0 0 2276.87 2551.11 143.32 o
9 0 0 19.20 6.71 19.90 o
-9 1 0 2346.86 2266.69 188.91 o
-8 1 0 1441.78 1416.90 93.95 o
-7 1 0 34.44 26.94 13.14 o
-6 1 0 2589.30 2464.85 79.67 o
-5 1 0 8157.41 8204.01 317.26 o
-4 1 0 10549.35 10348.83 242.17 o
-3 1 0 11646.46 11845.95 256.51 o
-2 1 0 90.01 102.64 6.75 o
-1 1 0 347.23 449.21 10.96 o
1 1 0 33866.52 32022.70 502.32 o
2 1 0 5236.47 4828.70 91.18 o
3 1 0 9807.68 9998.79 176.68 o
4 1 0 5398.12 5475.02 200.37 o
5 1 0 259.20 286.34 32.39 o
6 1 0 1590.37 1384.65 91.04 o
7 1 0 5543.40 5693.21 196.99 o
8 1 0 4886.97 4797.67 190.21 o
9 1 0 2594.45 2781.61 306.99 o
-9 2 0 2760.87 2857.73 159.57 o
-8 2 0 4581.48 4832.92 270.61 o
-7 2 0 2025.41 2050.31 90.28 o
-6 2 0 515.44 506.84 32.78 o
-5 2 0 765.85 802.81 40.26 o
-4 2 0 1721.61 1718.88 43.13 o
-3 2 0 5697.24 5854.27 128.35 o
-2 2 0 21324.81 21325.48 443.63 o
-1 2 0 1307.21 1334.42 18.54 o
0 2 0 4440.05 4384.24 55.89 o
1 2 0 2420.96 2487.19 49.65 o
2 2 0 6802.73 7081.01 96.50 o
3 2 0 24713.03 23706.65 390.06 o
4 2 0 20308.40 20373.34 376.10 o
5 2 0 2050.36 2150.04 73.83 o
6 2 0 354.28 349.82 45.10 o
7 2 0 175.61 174.74 32.95 o
8 2 0 645.57 672.54 68.81 o
9 2 0 2936.17 3026.71 431.65 o
-9 3 0 10.09 27.98 13.50 o
-8 3 0 1800.88 1944.58 117.67 o
-7 3 0 4933.44 4908.77 448.21 o
-6 3 0 4771.29 4561.75 219.45 o
-5 3 0 9404.37 9086.40 352.10 o
-4 3 0 256.01 248.26 16.56 o
-3 3 0 716.79 696.33 22.00 o
-2 3 0 8781.27 8428.05 180.90 o
-1 3 0 25213.76 24485.38 289.68 o
0 3 0 16140.39 16479.99 166.03 o
1 3 0 2120.41 2242.18 46.90 o
2 3 0 2519.84 2592.38 55.37 o
3 3 0 12.88 72.13 14.42 o
4 3 0 8220.82 8246.88 308.14 o
5 3 0 3800.77 3770.55 185.44 o
6 3 0 6081.64 5945.01 175.00 o
7 3 0 4521.32 4477.07 193.90 o
8 3 0 499.88 486.76 83.69 o
9 3 0 270.45 273.66 55.33 o
-9 4 0 1497.27 1483.18 153.58 o
-8 4 0 56.89 27.43 18.14 o
-7 4 0 1120.80 1265.87 93.10 o
-6 4 0 3343.26 3324.87 167.99 o
-5 4 0 5698.84 5199.57 335.92 o
-4 4 0 5217.54 5041.51 218.54 o
-3 4 0 2905.01 2848.37 112.54 o
-2 4 0 1250.24 1195.32 28.37 o
-1 4 0 214.51 218.15 11.22 o
0 4 0 7833.33 7980.53 136.36 o
1 4 0 13460.40 13094.36 288.27 o
2 4 0 18049.60 17654.84 248.37 o
3 4 0 4794.65 4672.52 138.01 o
4 4 0 21.48 24.38 6.50 o
5 4 0 1527.19 1420.40 74.67 o
6 4 0 2945.61 2720.75 114.35 o
7 4 0 3544.81 3826.27 238.41 o
8 4 0 2532.78 2629.22 212.32 o
-9 5 0 1529.97 1387.60 117.23 o
-8 5 0 1312.38 1045.11 106.03 o
-7 5 0 2035.65 2057.99 182.46 o
-6 5 0 209.93 183.77 20.84 o
-5 5 0 329.61 330.76 21.88 o
-4 5 0 5797.04 5469.62 235.83 o
-3 5 0 8997.01 8053.99 280.12 o
-2 5 0 12620.87 12482.70 369.31 o
-1 5 0 2387.55 2452.28 77.22 o
0 5 0 84.13 82.96 10.40 o
1 5 0 3781.49 3646.65 132.65 o
2 5 0 11005.23 10942.27 245.02 o
3 5 0 7529.37 7375.04 177.38 o
4 5 0 7310.84 7039.32 196.62 o
5 5 0 1439.58 1379.22 84.92 o
6 5 0 804.29 728.41 64.94 o
7 5 0 315.26 358.14 90.70 o
8 5 0 2036.07 2102.13 191.86 o
-8 6 0 2590.60 2169.76 179.46 o
-7 6 0 3416.94 3294.37 349.83 o
-6 6 0 5682.42 5821.21 464.11 o
-5 6 0 1422.90 1357.01 77.24 o
-4 6 0 834.87 765.05 53.75 o
-3 6 0 379.59 347.48 19.25 o
-2 6 0 4112.72 4284.15 134.31 o
-1 6 0 9684.83 10230.76 173.85 o
0 6 0 10837.47 11386.47 234.31 o
1 6 0 3186.19 3053.28 150.68 o
2 6 0 275.81 241.92 31.39 o
3 6 0 3580.85 3552.06 185.20 o
4 6 0 6009.50 5584.90 213.89 o
5 6 0 4470.37 4259.87 167.34 o
6 6 0 4671.04 4519.73 183.65 o
7 6 0 522.41 446.43 67.83 o
-8 7 0 69.53 28.35 20.08 o
-7 7 0 1085.09 910.95 77.76 o
-6 7 0 2810.46 2805.10 256.95 o
-5 7 0 4561.27 4667.66 346.82 o
-4 7 0 2745.39 2661.49 122.72 o
-3 7 0 2333.72 2305.80 64.85 o
-2 7 0 114.62 101.58 11.02 o
-1 7 0 4872.57 5212.76 107.83 o
0 7 0 8454.94 8645.96 256.83 o
1 7 0 10671.97 10550.51 494.75 o
2 7 0 3392.55 3370.45 133.93 o
3 7 0 40.17 64.30 17.81 o
4 7 0 18.55 15.88 11.88 o
5 7 0 710.68 589.92 61.87 o
6 7 0 1733.20 1568.02 124.35 o
7 7 0 3175.97 2978.33 199.04 o
-7 8 0 197.08 83.16 47.27 o
-6 8 0 279.03 200.85 39.12 o
-5 8 0 1928.38 1703.52 95.36 o
-4 8 0 4361.69 4659.45 193.16 o
-3 8 0 4119.60 4207.74 155.93 o
-2 8 0 3138.65 3254.46 82.54 o
-1 8 0 23.63 22.18 5.78 o
0 8 0 41.25 86.79 16.49 o
1 8 0 649.08 632.80 54.89 o
2 8 0 6219.50 6226.36 234.77 o
3 8 0 6792.65 6826.61 298.41 o
4 8 0 3991.13 3714.61 265.44 o
5 8 0 620.04 615.29 73.78 o
6 8 0 83.16 105.35 34.11 o
-7 9 0 1294.17 1273.75 111.69 o
-6 9 0 1081.74 1102.63 98.47 o
-5 9 0 765.80 731.12 64.99 o
-4 9 0 269.73 253.06 39.11 o
-3 9 0 952.71 1018.48 65.74 o
-2 9 0 5153.76 5429.32 201.51 o
-1 9 0 5659.75 6245.76 141.96 o
0 9 0 862.77 876.04 55.67 o
1 9 0 1356.19 1268.97 83.87 o
2 9 0 283.54 208.22 36.50 o
3 9 0 3928.99 3798.35 288.08 o
4 9 0 2921.01 2866.17 157.30 o
5 9 0 1701.26 1854.28 160.26 o
-6 10 0 2452.35 2718.07 185.91 o
-5 10 0 2843.47 3254.74 205.54 o
-4 10 0 1583.93 1590.44 107.93 o
-3 10 0 3.73 1.53 17.82 o
-2 10 0 872.99 955.45 62.06 o
-1 10 0 1858.67 2061.28 117.32 o
0 10 0 2475.47 2587.02 111.52 o
1 10 0 1643.78 1634.46 121.48 o
2 10 0 2028.33 2024.58 120.30 o
3 10 0 368.43 387.23 52.74 o
4 10 0 11.83 19.44 20.17 o
-4 11 0 2236.11 2557.70 162.56 o
-3 11 0 1715.75 1913.46 146.44 o
-2 11 0 970.84 1035.73 105.55 o
-1 11 0 556.65 612.80 67.67 o
0 11 0 282.01 286.58 49.32 o
1 11 0 2821.30 3228.43 167.22 o
2 11 0 4570.75 4671.31 357.62 o
3 11 0 2292.04 2457.66 206.16 o
-2 12 0 2689.49 3159.26 199.46 o
-1 12 0 1012.16 1101.68 95.17 o
0 12 0 604.07 644.79 72.51 o
0 -12 1 3.04 -4.98 21.23 o
1 -12 1 955.50 888.55 99.92 o
2 -12 1 2171.91 2613.37 180.41 o
-3 -11 1 840.41 772.06 110.04 o
-2 -11 1 3134.29 3065.24 255.18 o
-1 -11 1 3443.69 3890.35 190.66 o
0 -11 1 603.04 639.66 68.61 o
1 -11 1 358.90 431.88 53.00 o
2 -11 1 160.65 128.48 33.04 o
3 -11 1 455.23 403.81 63.65 o
4 -11 1 1338.63 1272.45 175.08 o
-4 -10 1 1232.05 1266.86 102.14 o
-3 -10 1 167.58 134.37 33.86 o
-2 -10 1 5.37 3.16 12.05 o
-1 -10 1 1849.40 1892.66 110.43 o
0 -10 1 1406.58 1385.15 70.45 o
1 -10 1 3922.06 4304.11 173.27 o
2 -10 1 2517.54 2877.79 110.22 o
3 -10 1 452.22 484.00 55.14 o
4 -10 1 78.27 81.40 19.22 o
5 -10 1 2835.10 3065.05 261.45 o
6 -10 1 1682.36 1661.45 143.65 o
-5 -9 1 1082.39 943.10 87.07 o
-4 -9 1 5628.81 5319.74 340.31 o
-3 -9 1 6242.13 6280.50 358.91 o
-2 -9 1 1585.33 1538.97 99.74 o
-1 -9 1 267.07 281.41 34.95 o
0 -9 1 2110.25 2233.78 76.06 o
1 -9 1 1514.52 1549.18 55.49 o
2 -9 1 3730.49 4088.86 112.28 o
3 -9 1 3449.62 3663.78 184.51 o
4 -9 1 963.76 969.59 68.84 o
5 -9 1 367.74 337.80 44.27 o
6 -9 1 150.52 99.52 34.84 o
-6 -8 1 959.68 973.77 89.28 o
-5 -8 1 17.42 -3.38 17.42 o
-4 -8 1 206.66 185.86 37.92 o
-3 -8 1 6362.57 6116.63 309.86 o
-2 -8 1 2679.98 2476.33 118.42 o
-1 -8 1 3244.19 3115.04 117.93 o
0 -8 1 2044.76 2111.57 90.52 o
1 -8 1 649.77 641.34 32.62 o
2 -8 1 247.01 259.07 20.01 o
3 -8 1 3178.46 3145.64 192.40 o
4 -8 1 4531.80 4725.07 270.27 o
5 -8 1 4472.77 4462.95 400.22 o
6 -8 1 1008.32 889.64 77.02 o
7 -8 1 39.39 20.74 16.73 o
-7 -7 1 1258.51 1172.63 155.61 o
-6 -7 1 3051.64 3000.01 171.35 o
-5 -7 1 2979.10 2770.78 138.31 o
-4 -7 1 7818.36 7630.48 284.27 o
-3 -7 1 292.60 331.18 45.78 o
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0 -7 1 9869.37 10377.62 437.46 o
1 -7 1 5360.81 5271.03 194.02 o
2 -7 1 548.82 542.76 27.79 o
3 -7 1 1.46 4.86 4.49 o
4 -7 1 951.84 915.87 49.15 o
5 -7 1 2652.11 2616.93 288.02 o
6 -7 1 2481.14 2616.41 188.43 o
7 -7 1 2079.32 1972.48 189.24 o
8 -7 1 1062.42 847.39 115.19 o
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0 -6 1 563.60 513.97 44.81 o
1 -6 1 3274.19 3241.97 66.38 o
2 -6 1 5440.34 5187.70 112.11 o
3 -6 1 7008.36 6962.62 220.60 o
4 -6 1 3105.76 2777.22 111.17 o
5 -6 1 431.34 477.27 43.69 o
6 -6 1 1421.68 1428.86 156.14 o
7 -6 1 3189.28 3134.71 301.54 o
8 -6 1 2961.95 2612.31 206.67 o
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-1 -5 1 13387.09 13110.78 384.53 o
0 -5 1 5802.28 6236.49 135.20 o
1 -5 1 279.62 285.24 13.87 o
2 -5 1 3696.25 3555.50 74.22 o
3 -5 1 8102.88 7318.89 213.84 o
4 -5 1 6121.15 5276.59 136.77 o
5 -5 1 5956.91 5322.16 474.20 o
6 -5 1 536.04 417.79 38.79 o
7 -5 1 0.58 5.73 11.49 o
8 -5 1 593.82 457.34 64.54 o
-8 -4 1 737.54 931.06 121.18 o
-7 -4 1 5590.35 6039.51 499.41 o
-6 -4 1 4619.55 4320.34 232.01 o
-5 -4 1 2798.87 2567.53 128.99 o
-4 -4 1 553.10 525.90 38.55 o
-3 -4 1 3258.30 3081.88 165.18 o
-2 -4 1 3738.01 3624.43 118.38 o
-1 -4 1 15528.73 15791.96 244.20 o
0 -4 1 22163.71 22725.09 383.55 o
1 -4 1 4995.04 5036.44 76.97 o
2 -4 1 125.05 123.77 7.21 o
3 -4 1 132.90 138.79 10.14 o
4 -4 1 3445.30 3117.43 153.17 o
5 -4 1 8124.58 6641.41 138.09 o
6 -4 1 7913.44 7704.88 581.52 o
7 -4 1 3473.74 3466.13 358.97 o
8 -4 1 449.32 500.38 49.71 o
9 -4 1 51.97 11.30 19.84 o
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-8 -3 1 21.50 22.11 74.78 o
-7 -3 1 747.39 582.94 64.89 o
-6 -3 1 2544.89 2339.91 135.22 o
-5 -3 1 7379.33 7446.73 272.58 o
-4 -3 1 6415.05 5761.41 175.59 o
-3 -3 1 8921.19 8778.19 195.42 o
-2 -3 1 82.95 74.24 9.54 o
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0 -3 1 8138.33 8514.78 100.78 o
1 -3 1 23771.48 23707.30 283.04 o
2 -3 1 14977.00 14468.09 272.02 o
3 -3 1 7769.60 7285.83 235.78 o
4 -3 1 66.41 63.63 7.35 o
5 -3 1 218.87 205.19 15.18 o
6 -3 1 6410.63 6644.78 604.20 o
7 -3 1 3533.43 3598.20 290.90 o
8 -3 1 2296.70 2420.62 270.60 o
9 -3 1 2055.99 2066.14 170.21 o
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-8 -2 1 3066.79 3002.58 150.36 o
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-6 -2 1 1544.72 1444.38 69.30 o
-5 -2 1 432.46 502.43 33.22 o
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1 -2 1 3320.41 3421.57 54.69 o
2 -2 1 2212.05 2253.96 47.39 o
3 -2 1 8016.95 7849.98 161.59 o
4 -2 1 8611.04 8196.28 141.57 o
5 -2 1 6020.39 5837.67 175.91 o
6 -2 1 674.98 648.25 70.47 o
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1 -1 1 1565.20 1797.17 33.39 o
2 -1 1 2115.91 2306.97 48.03 o
3 -1 1 481.66 501.97 19.11 o
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5 -1 1 11776.02 12055.36 556.95 o
6 -1 1 6746.03 6798.71 385.45 o
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8 2 1 214.12 200.31 37.19 o
9 2 1 728.70 527.06 123.63 o
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0 3 1 9377.40 9299.18 123.46 o
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4 3 1 469.44 463.06 44.96 o
5 3 1 4004.55 3839.30 97.57 o
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