#------------------------------------------------------------------------------ #$Date: 2020-06-06 08:31:45 +0300 (Sat, 06 Jun 2020) $ #$Revision: 252984 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/34/2243428.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243428 _cell_angle_alpha 90.000 _cell_angle_beta 108.151 _cell_angle_gamma 90.000 _cell_length_a 12.8783 _cell_length_b 6.8842 _cell_length_c 16.2080 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8102 _cod_data_source_file pk2628Isup2.hkl _cod_data_source_block I _shelx_title ' GVSU919C in Pc # 7' _shelx_refln_list_code 4 _shelx_f_calc_maximum 157.32 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 0 -20 47.96 59.23 5.89 o 1 1 -19 115.05 131.96 11.79 o 2 1 -19 167.69 165.08 10.67 o 3 1 -19 32.75 40.63 4.91 o 4 1 -19 86.48 82.91 4.65 o 5 1 -19 20.95 18.67 3.54 o 6 1 -19 45.61 41.38 3.22 o 7 1 -19 171.26 186.85 6.77 o 8 1 -19 51.52 61.51 4.37 o 9 1 -19 180.58 224.01 11.51 o 3 2 -19 93.11 96.39 4.86 o 4 2 -19 15.49 17.29 2.98 o 5 2 -19 4.32 1.02 2.20 o 6 2 -19 85.58 97.94 5.12 o 7 2 -19 18.20 19.37 3.65 o -2 0 -18 132.10 136.99 7.86 o -1 0 -18 316.09 357.07 14.60 o 0 0 -18 117.86 144.29 9.26 o 1 0 -18 352.71 340.23 14.60 o 2 0 -18 153.06 148.22 9.26 o 3 0 -18 203.55 193.13 10.67 o 4 0 -18 54.71 57.83 7.86 o 5 0 -18 78.57 87.02 7.58 o 6 0 -18 198.35 232.15 12.35 o 7 0 -18 183.79 200.71 11.23 o 8 0 -18 376.01 383.46 16.00 o 9 0 -18 141.49 158.04 9.26 o 10 0 -18 371.92 406.19 16.00 o -1 1 -18 53.34 52.10 4.07 o 0 1 -18 17.77 26.34 3.65 o 1 1 -18 16.01 15.58 2.87 o 2 1 -18 86.40 94.04 4.90 o 3 1 -18 43.36 46.88 5.36 o 4 1 -18 156.29 162.11 5.82 o 5 1 -18 168.72 195.59 8.82 o 6 1 -18 39.92 39.49 3.51 o 7 1 -18 85.81 97.88 4.68 o 8 1 -18 17.12 24.30 2.62 o 9 1 -18 23.81 28.69 2.62 o 10 1 -18 56.33 69.33 3.72 o -1 2 -18 10.75 14.88 5.89 o 0 2 -18 28.98 40.09 3.23 o 1 2 -18 14.99 18.24 2.42 o 2 2 -18 35.77 40.94 3.16 o 3 2 -18 119.86 128.11 4.50 o 4 2 -18 26.73 29.45 2.55 o 5 2 -18 20.62 20.16 2.23 o 6 2 -18 141.64 148.19 4.45 o 7 2 -18 40.08 47.34 3.18 o 8 2 -18 7.05 10.42 2.13 o 9 2 -18 12.71 18.32 2.35 o 10 2 -18 17.83 28.07 4.21 o 1 3 -18 7.33 11.85 2.18 o 2 3 -18 88.11 79.79 4.77 o 3 3 -18 3.11 0.33 2.81 o 4 3 -18 35.29 34.23 3.65 o 5 3 -18 41.12 37.09 3.56 o 6 3 -18 4.52 1.04 2.67 o 7 3 -18 85.24 75.59 6.04 o 8 3 -18 16.62 16.39 2.67 o -3 1 -17 14.00 19.09 4.21 o -2 1 -17 165.69 170.12 5.34 o -1 1 -17 50.70 56.38 4.17 o 0 1 -17 114.33 129.06 4.62 o 1 1 -17 95.17 93.31 4.22 o 2 1 -17 234.71 230.81 7.17 o 3 1 -17 111.97 107.60 4.42 o 4 1 -17 52.48 53.74 5.79 o 5 1 -17 228.90 230.45 6.44 o 6 1 -17 25.53 31.52 2.89 o 7 1 -17 251.91 260.73 7.74 o 8 1 -17 67.31 73.04 4.46 o 9 1 -17 29.81 30.64 2.91 o 10 1 -17 172.75 182.46 7.81 o 11 1 -17 40.58 43.95 3.73 o -2 2 -17 33.17 35.13 2.84 o -1 2 -17 306.08 319.36 7.94 o 0 2 -17 48.98 47.07 5.21 o 1 2 -17 172.04 157.44 4.96 o 2 2 -17 30.45 29.14 2.67 o 3 2 -17 62.97 63.48 3.92 o 4 2 -17 73.16 76.94 4.15 o 5 2 -17 17.54 20.88 2.56 o 6 2 -17 96.29 104.77 4.34 o 7 2 -17 12.21 14.82 2.81 o 8 2 -17 200.83 190.44 5.33 o 9 2 -17 177.11 186.79 5.67 o 10 2 -17 225.34 242.29 6.58 o 11 2 -17 231.96 239.72 7.53 o -1 3 -17 31.85 32.22 3.37 o 0 3 -17 18.69 23.81 2.70 o 1 3 -17 16.68 18.26 2.56 o 2 3 -17 33.45 30.55 3.56 o 3 3 -17 110.74 123.45 6.12 o 4 3 -17 13.81 11.21 2.78 o 5 3 -17 85.88 87.95 5.19 o 6 3 -17 68.62 65.12 4.77 o 7 3 -17 22.07 19.79 3.27 o 8 3 -17 5.68 4.05 2.76 o 9 3 -17 7.99 7.67 2.95 o 10 3 -17 54.80 56.71 3.67 o 1 4 -17 37.27 37.19 3.93 o 2 4 -17 78.50 80.37 4.77 o 3 4 -17 98.61 99.25 3.91 o 4 4 -17 4.86 6.04 3.65 o 5 4 -17 72.54 72.44 4.46 o 6 4 -17 153.08 142.89 6.02 o 7 4 -17 11.39 7.12 2.08 o -4 0 -16 14.55 9.54 3.65 o -3 0 -16 154.13 153.27 8.98 o -2 0 -16 18.70 13.75 4.49 o -1 0 -16 375.17 374.47 17.12 o 0 0 -16 182.16 160.29 11.51 o 1 0 -16 684.71 592.87 23.58 o 2 0 -16 301.79 271.45 14.32 o 3 0 -16 364.47 350.89 16.56 o 4 0 -16 234.21 205.76 12.35 o 5 0 -16 302.89 284.97 10.70 o 6 0 -16 305.00 283.19 10.22 o 7 0 -16 660.66 623.00 17.46 o 8 0 -16 176.53 162.20 7.54 o 9 0 -16 411.10 403.78 23.16 o 10 0 -16 21.49 15.79 3.47 o 11 0 -16 186.19 204.83 15.58 o 12 0 -16 22.53 20.07 5.47 o -4 1 -16 105.22 103.72 4.03 o -3 1 -16 4.51 4.15 2.51 o -2 1 -16 140.47 135.82 4.60 o -1 1 -16 17.26 17.05 3.53 o 0 1 -16 97.39 96.07 4.20 o 1 1 -16 113.31 111.23 4.64 o 2 1 -16 4.95 6.93 2.58 o 3 1 -16 55.09 64.50 4.13 o 4 1 -16 0.23 1.20 2.39 o 5 1 -16 55.09 66.12 4.49 o 6 1 -16 3.95 5.54 2.71 o 7 1 -16 160.91 164.41 5.48 o 8 1 -16 131.53 144.47 5.05 o 9 1 -16 34.69 37.01 2.68 o 10 1 -16 137.29 150.91 5.01 o 11 1 -16 12.01 10.60 2.37 o 12 1 -16 96.57 104.68 5.02 o -4 2 -16 15.35 13.77 3.09 o -3 2 -16 18.45 20.41 2.56 o -2 2 -16 23.28 27.23 2.64 o -1 2 -16 33.87 39.83 3.63 o 0 2 -16 73.63 71.12 4.85 o 1 2 -16 35.97 25.80 3.00 o 2 2 -16 97.14 103.51 4.50 o 3 2 -16 73.48 71.51 6.97 o 4 2 -16 106.42 118.37 4.79 o 5 2 -16 107.32 98.44 4.48 o 6 2 -16 100.10 104.16 4.45 o 7 2 -16 59.93 47.91 3.36 o 8 2 -16 104.20 103.02 4.49 o 9 2 -16 20.29 21.57 2.44 o 10 2 -16 9.58 9.23 2.20 o 11 2 -16 11.83 14.72 2.35 o 12 2 -16 8.72 9.40 2.19 o -3 3 -16 43.23 35.64 3.27 o -2 3 -16 240.84 261.48 6.64 o -1 3 -16 72.95 76.82 4.14 o 0 3 -16 58.71 58.73 4.17 o 1 3 -16 223.81 218.34 6.64 o 2 3 -16 89.95 83.68 4.99 o 3 3 -16 236.21 212.86 6.59 o 4 3 -16 1.28 2.25 2.31 o 5 3 -16 223.07 223.08 11.27 o 6 3 -16 62.85 66.78 4.71 o 7 3 -16 222.14 226.62 6.97 o 8 3 -16 38.84 42.81 3.16 o 9 3 -16 105.54 117.91 3.84 o 10 3 -16 258.66 295.26 6.49 o 11 3 -16 41.89 38.90 2.97 o -1 4 -16 143.51 145.78 6.24 o 0 4 -16 36.63 40.14 2.84 o 1 4 -16 79.60 91.13 4.34 o 2 4 -16 163.56 171.56 5.23 o 3 4 -16 101.87 107.30 4.81 o 4 4 -16 102.22 117.25 4.40 o 5 4 -16 92.43 105.43 4.52 o 6 4 -16 146.52 164.45 5.34 o 7 4 -16 59.08 71.85 3.64 o 8 4 -16 32.96 32.35 3.06 o 9 4 -16 159.75 149.45 4.80 o 4 5 -16 11.65 15.16 3.93 o 5 5 -16 25.50 29.87 2.96 o -6 1 -15 42.26 39.86 4.77 o -5 1 -15 15.44 18.41 2.79 o -4 1 -15 87.54 94.10 5.64 o -3 1 -15 20.81 19.24 3.00 o -2 1 -15 68.36 64.63 4.73 o -1 1 -15 120.19 106.67 5.34 o 0 1 -15 103.38 84.03 4.53 o 1 1 -15 263.42 242.86 7.54 o 2 1 -15 10.76 8.43 2.60 o 3 1 -15 595.35 533.71 13.57 o 4 1 -15 107.64 98.80 7.94 o 5 1 -15 351.27 306.89 7.75 o 6 1 -15 223.09 203.04 6.29 o 7 1 -15 81.47 78.92 4.52 o 8 1 -15 206.80 184.99 5.36 o 9 1 -15 17.62 16.29 2.81 o 10 1 -15 114.35 106.55 4.12 o 11 1 -15 41.85 45.48 2.98 o 12 1 -15 25.16 20.66 2.47 o 13 1 -15 64.27 77.79 4.46 o -5 2 -15 116.53 114.27 9.93 o -4 2 -15 70.62 63.14 4.46 o -3 2 -15 43.88 50.01 4.86 o -2 2 -15 216.85 189.25 7.93 o -1 2 -15 166.29 148.22 7.31 o 0 2 -15 391.50 343.99 8.03 o 1 2 -15 2.77 -2.43 2.43 o 2 2 -15 268.90 235.57 6.49 o 3 2 -15 174.13 176.84 6.02 o 4 2 -15 231.84 208.78 6.14 o 5 2 -15 171.83 164.58 5.76 o 6 2 -15 147.89 147.89 5.74 o 7 2 -15 274.00 262.23 7.05 o 8 2 -15 36.83 36.16 3.08 o 9 2 -15 410.48 385.14 10.72 o 10 2 -15 30.02 32.04 4.09 o 11 2 -15 186.49 198.20 4.79 o 12 2 -15 39.09 40.33 2.59 o 13 2 -15 81.74 71.08 3.49 o -4 3 -15 47.59 45.18 3.34 o -3 3 -15 0.60 0.12 2.07 o -2 3 -15 35.42 31.48 2.89 o -1 3 -15 12.56 13.79 2.72 o 0 3 -15 27.47 26.55 3.02 o 1 3 -15 30.01 32.90 4.12 o 2 3 -15 29.66 31.74 3.32 o 3 3 -15 64.61 46.97 4.79 o 4 3 -15 30.64 25.90 3.12 o 5 3 -15 33.81 32.22 4.51 o 6 3 -15 71.03 66.81 4.43 o 7 3 -15 6.13 10.57 2.24 o 8 3 -15 45.77 40.02 2.68 o 9 3 -15 20.04 24.49 2.12 o 10 3 -15 35.63 33.35 2.03 o 11 3 -15 51.46 51.57 2.43 o 12 3 -15 2.94 2.13 1.93 o -3 4 -15 125.02 129.97 5.15 o -2 4 -15 65.12 73.02 4.26 o -1 4 -15 9.78 12.43 3.23 o 0 4 -15 99.34 94.38 5.36 o 1 4 -15 47.35 40.54 4.07 o 2 4 -15 128.01 126.35 6.63 o 3 4 -15 188.69 189.81 6.96 o 4 4 -15 435.72 423.57 10.14 o 5 4 -15 61.73 76.32 4.46 o 6 4 -15 172.61 167.02 5.70 o 7 4 -15 22.59 28.31 2.21 o 8 4 -15 131.26 136.84 3.93 o 9 4 -15 47.03 43.66 2.67 o 10 4 -15 7.42 5.35 1.53 o 0 5 -15 99.15 89.98 6.12 o 1 5 -15 216.84 217.69 5.77 o 2 5 -15 3.34 6.93 2.31 o 3 5 -15 694.05 696.49 17.57 o 4 5 -15 135.76 140.22 5.94 o 5 5 -15 360.39 369.70 8.53 o 6 5 -15 163.17 164.74 6.83 o 7 5 -15 62.71 67.31 4.90 o 8 5 -15 183.65 175.45 7.86 o -7 0 -14 46.07 38.74 5.33 o -6 0 -14 12.33 11.09 3.18 o -5 0 -14 9.18 16.70 3.77 o -4 0 -14 45.25 40.30 4.35 o -3 0 -14 13.57 17.53 7.02 o -2 0 -14 97.71 97.19 6.74 o -1 0 -14 2.19 7.05 3.93 o 0 0 -14 492.99 445.49 21.47 o 1 0 -14 213.63 177.97 11.51 o 2 0 -14 885.03 709.64 27.23 o 3 0 -14 2290.88 1949.14 46.35 o 4 0 -14 2521.18 2251.53 72.28 o 5 0 -14 695.73 606.67 17.27 o 6 0 -14 208.99 186.66 8.63 o 7 0 -14 440.80 399.27 13.00 o 8 0 -14 2.66 4.26 3.63 o 9 0 -14 124.50 118.25 6.34 o 10 0 -14 16.26 24.24 3.48 o 11 0 -14 73.86 73.14 4.99 o 12 0 -14 11.24 16.65 3.49 o 13 0 -14 43.20 42.93 4.26 o 14 0 -14 73.13 87.41 4.55 o -7 1 -14 47.98 64.22 5.61 o -6 1 -14 207.02 216.76 9.58 o -5 1 -14 32.85 35.02 3.02 o -4 1 -14 104.98 107.16 5.01 o -3 1 -14 46.67 46.64 3.93 o -2 1 -14 55.73 51.83 4.03 o -1 1 -14 337.93 313.04 9.98 o 0 1 -14 247.51 210.95 10.22 o 1 1 -14 42.87 41.46 3.81 o 2 1 -14 419.71 374.32 8.66 o 3 1 -14 231.83 218.17 6.35 o 4 1 -14 181.85 161.76 5.58 o 5 1 -14 478.06 443.14 9.92 o 6 1 -14 53.58 48.89 5.32 o 7 1 -14 282.86 265.24 7.50 o 8 1 -14 375.26 348.05 7.11 o 9 1 -14 39.84 29.94 2.42 o 10 1 -14 53.21 47.81 2.91 o 11 1 -14 108.69 109.24 3.54 o 12 1 -14 24.91 25.96 1.97 o 13 1 -14 204.93 228.86 4.58 o 14 1 -14 56.78 71.64 3.97 o -6 2 -14 25.38 37.93 7.30 o -5 2 -14 72.69 74.96 4.95 o -4 2 -14 24.77 20.56 2.32 o -3 2 -14 14.32 19.01 3.06 o -2 2 -14 90.94 86.72 4.05 o -1 2 -14 2.19 3.83 2.07 o 0 2 -14 104.43 90.49 5.30 o 1 2 -14 106.25 91.36 5.33 o 2 2 -14 130.45 105.66 4.92 o 3 2 -14 137.12 133.13 6.64 o 4 2 -14 105.11 99.97 4.73 o 5 2 -14 166.67 148.33 5.95 o 6 2 -14 118.49 106.79 5.06 o 7 2 -14 154.19 143.24 4.66 o 8 2 -14 10.27 10.87 2.40 o 9 2 -14 111.12 105.66 3.66 o 10 2 -14 22.54 24.79 2.37 o 11 2 -14 22.21 24.16 2.17 o 12 2 -14 82.26 88.25 3.51 o 13 2 -14 37.90 43.41 2.46 o -5 3 -14 74.38 67.67 4.31 o -4 3 -14 107.94 107.12 5.32 o -3 3 -14 66.45 53.88 3.49 o -2 3 -14 14.73 18.64 3.47 o -1 3 -14 381.13 355.64 8.67 o 0 3 -14 1.57 3.81 2.17 o 1 3 -14 197.81 178.07 7.21 o 2 3 -14 396.78 372.80 9.98 o 3 3 -14 225.58 235.96 11.51 o 4 3 -14 227.28 230.16 7.34 o 5 3 -14 378.68 372.88 11.14 o 6 3 -14 217.69 214.67 7.02 o 7 3 -14 1.60 0.92 2.00 o 8 3 -14 377.06 367.65 6.87 o 9 3 -14 30.01 31.07 2.38 o 10 3 -14 99.98 101.36 3.35 o 11 3 -14 108.61 111.64 3.42 o 12 3 -14 69.69 69.36 2.55 o -4 4 -14 36.71 37.36 6.04 o -3 4 -14 19.90 22.98 2.99 o -2 4 -14 139.22 142.28 5.68 o -1 4 -14 47.99 47.41 3.32 o 0 4 -14 299.29 285.59 13.67 o 1 4 -14 15.52 17.41 3.44 o 2 4 -14 153.93 152.85 7.24 o 3 4 -14 361.81 367.63 11.71 o 4 4 -14 327.55 345.86 9.16 o 5 4 -14 139.78 141.58 5.11 o 6 4 -14 6.99 3.69 2.24 o 7 4 -14 329.43 320.89 9.60 o 8 4 -14 43.83 45.96 2.93 o 9 4 -14 155.42 160.33 4.33 o 10 4 -14 26.70 31.46 3.68 o 11 4 -14 44.64 41.90 2.76 o -2 5 -14 3.52 2.81 3.37 o -1 5 -14 18.38 20.32 3.07 o 0 5 -14 71.50 66.61 4.96 o 1 5 -14 7.29 10.59 2.96 o 2 5 -14 157.46 147.47 5.05 o 3 5 -14 9.73 10.15 3.04 o 4 5 -14 15.24 19.83 2.14 o 5 5 -14 56.61 50.85 3.30 o 6 5 -14 22.19 25.32 2.56 o 7 5 -14 36.87 36.91 5.39 o 8 5 -14 6.09 9.90 2.12 o 9 5 -14 5.20 4.94 2.71 o 2 6 -14 199.09 199.59 10.67 o 5 6 -14 173.71 164.22 7.86 o -8 1 -13 46.97 53.80 3.76 o -7 1 -13 13.45 14.56 3.16 o -6 1 -13 117.26 138.32 5.55 o -5 1 -13 19.65 16.15 2.64 o -4 1 -13 51.75 44.22 3.26 o -3 1 -13 41.23 38.87 2.77 o -2 1 -13 38.80 28.52 2.42 o -1 1 -13 168.49 143.65 4.53 o 0 1 -13 40.98 32.02 3.66 o 1 1 -13 190.24 165.11 11.83 o 2 1 -13 1425.18 1160.96 20.53 o 3 1 -13 404.19 356.12 11.42 o 4 1 -13 1829.13 1626.32 27.90 o 5 1 -13 130.87 126.37 5.56 o 6 1 -13 337.26 296.44 7.88 o 7 1 -13 35.07 30.78 3.11 o 8 1 -13 217.31 182.05 5.03 o 9 1 -13 10.37 12.25 2.08 o 10 1 -13 7.73 8.24 2.06 o 11 1 -13 91.39 87.19 3.44 o 12 1 -13 39.77 48.04 2.69 o 13 1 -13 113.02 121.20 3.19 o 14 1 -13 8.50 11.77 2.05 o -7 2 -13 166.87 172.86 11.93 o -6 2 -13 74.06 66.85 3.58 o -5 2 -13 41.22 43.34 3.88 o -4 2 -13 84.74 77.24 5.08 o -3 2 -13 38.03 29.87 2.69 o -2 2 -13 254.88 215.51 6.26 o -1 2 -13 385.58 304.17 10.68 o 0 2 -13 280.24 249.60 7.02 o 1 2 -13 728.68 598.54 11.49 o 2 2 -13 110.05 102.32 4.93 o 3 2 -13 1172.65 962.78 17.54 o 4 2 -13 700.56 615.41 12.45 o 5 2 -13 273.89 235.62 5.99 o 6 2 -13 292.55 267.76 9.99 o 7 2 -13 805.32 686.30 11.09 o 8 2 -13 2.32 5.08 1.95 o 9 2 -13 177.34 169.45 4.82 o 10 2 -13 28.73 24.05 2.34 o 11 2 -13 53.71 54.01 3.05 o 12 2 -13 189.17 202.23 5.59 o 13 2 -13 41.25 43.64 2.30 o 14 2 -13 206.86 211.57 5.51 o -6 3 -13 39.50 38.33 3.98 o -5 3 -13 0.32 -2.11 2.11 o -4 3 -13 74.41 79.19 3.79 o -3 3 -13 43.25 37.77 3.28 o -2 3 -13 22.03 22.19 2.56 o -1 3 -13 50.45 39.30 2.96 o 0 3 -13 28.65 25.05 2.82 o 1 3 -13 73.35 64.98 3.75 o 2 3 -13 674.26 603.06 13.23 o 3 3 -13 168.30 147.68 7.91 o 4 3 -13 872.16 802.15 42.67 o 5 3 -13 63.32 63.77 4.81 o 6 3 -13 126.58 111.14 5.00 o 7 3 -13 35.41 25.18 2.60 o 8 3 -13 14.20 11.91 2.52 o 9 3 -13 27.90 30.84 2.46 o 10 3 -13 22.45 22.70 2.27 o 11 3 -13 60.98 64.19 3.03 o 12 3 -13 36.20 38.00 2.30 o 13 3 -13 15.50 16.21 1.53 o -5 4 -13 81.33 83.65 6.46 o -4 4 -13 54.29 52.05 3.43 o -3 4 -13 2.48 3.10 2.23 o -2 4 -13 148.63 145.89 5.76 o -1 4 -13 32.54 36.28 3.51 o 0 4 -13 81.23 82.99 4.14 o 1 4 -13 17.82 16.31 2.28 o 2 4 -13 22.56 25.58 2.72 o 3 4 -13 177.55 166.78 5.92 o 4 4 -13 68.57 67.95 4.11 o 5 4 -13 153.19 140.90 5.15 o 6 4 -13 49.83 49.60 3.67 o 7 4 -13 132.42 126.86 4.83 o 8 4 -13 26.53 23.60 2.79 o 9 4 -13 178.95 176.20 4.66 o 10 4 -13 100.08 105.06 3.62 o 11 4 -13 12.07 14.11 1.92 o 12 4 -13 93.54 90.38 3.69 o -3 5 -13 35.22 31.52 5.61 o -2 5 -13 23.55 23.60 2.13 o -1 5 -13 338.67 316.06 11.04 o 0 5 -13 69.48 64.01 3.30 o 1 5 -13 106.07 96.87 3.75 o 2 5 -13 193.55 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