#------------------------------------------------------------------------------ #$Date: 2021-06-26 08:53:12 +0300 (Sat, 26 Jun 2021) $ #$Revision: 266715 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/38/2243855.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243855 loop_ _publ_author_name 'Naghiyev, Farid N.' 'Grishina, Maria M.' 'Khrustalev, Victor N.' 'Akkurt, Mehmet' 'Huseynova, Afet T.' 'Akobirshoeva, Anzurat A.' 'Mamedov, \.Ibrahim G.' _publ_section_title ; Crystal structure and Hirshfeld surface analysis of ethyl 6'-amino-2'-(chloromethyl)-5'-cyano-2-oxo-1,2-dihydrospiro[indoline-3,4'-pyran]-3'-carboxylate ; _journal_coeditor_code VM2250 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 739 _journal_page_last 743 _journal_paper_doi 10.1107/S2056989021006459 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac 'C17 H14 Cl N3 O4' _chemical_formula_moiety 'C17 H14 Cl N3 O4' _chemical_formula_sum 'C17 H14 Cl N3 O4' _chemical_formula_weight 359.76 _chemical_name_systematic 'Ethyl 6'-amino-2'-(chloromethyl)-5'-cyano-2-oxo-1,2-dihydrospiro[indoline-3,4'-pyran]-3'-carboxylate' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary difmap _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2013 _cell_angle_alpha 98.8503(7) _cell_angle_beta 108.0048(7) _cell_angle_gamma 96.3852(6) _cell_formula_units_Z 2 _cell_length_a 8.0218(2) _cell_length_b 10.2278(3) _cell_length_c 10.6714(3) _cell_measurement_reflns_used 6340 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 32.51 _cell_measurement_theta_min 2.59 _cell_volume 810.92(4) _computing_cell_refinement ; SAINT (Bruker, 2013) ; _computing_data_collection ; APEX3 (Bruker, 2018) ; _computing_data_reduction ; SAINT (Bruker, 2013) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; PLATON (Spek, 2020) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker D8 QUEST PHOTON-III CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0388 _diffrn_reflns_av_unetI/netI 0.0433 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 18865 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 32.589 _diffrn_reflns_theta_min 2.590 _exptl_absorpt_coefficient_mu 0.264 _exptl_absorpt_correction_T_max 0.949 _exptl_absorpt_correction_T_min 0.903 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.473 _exptl_crystal_description prism _exptl_crystal_F_000 372 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.20 _exptl_crystal_size_min 0.15 _refine_diff_density_max 0.435 _refine_diff_density_min -0.628 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 236 _refine_ls_number_reflns 5899 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0612 _refine_ls_R_factor_gt 0.0444 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0366P)^2^+0.4187P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0955 _refine_ls_wR_factor_ref 0.1064 _reflns_number_gt 4685 _reflns_number_total 5899 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file vm2250sup1.cif _cod_data_source_block I _cod_database_code 2243855 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.937 _shelx_estimated_absorpt_t_max 0.961 _shelx_hkl_file ; -1 0 0 7.20 1.20 -1 0 0 5.00 1.10 -1 0 0 8.40 1.40 1 0 0 5.40 1.10 1 0 0 6.60 1.30 1 0 0 4.70 0.90 -3 0 0 1956.40 54.19 3 0 0 1987.40 53.69 3 0 0 1988.00 52.99 -4 0 0 7769.92 185.18 4 0 0 7683.43 184.08 4 0 0 7679.13 182.88 -5 0 0 1127.69 40.70 5 0 0 1134.09 39.60 5 0 0 954.80 43.60 -6 0 0 30.30 7.30 6 0 0 22.70 5.90 6 0 0 28.60 6.90 -7 0 0 77.09 12.90 7 0 0 80.39 10.80 7 0 0 78.39 12.90 -8 0 0 405.06 28.30 8 0 0 420.26 27.00 8 0 0 385.86 27.20 -9 0 0 350.36 28.60 9 0 0 350.16 26.10 9 0 0 369.06 27.60 -10 0 0 15.90 8.70 10 0 0 17.50 8.10 10 0 0 13.90 8.10 -11 0 0 30.70 11.40 11 0 0 17.90 8.50 11 0 0 24.20 10.60 11 -1 0 17.30 9.60 11 -1 0 38.90 11.10 -11 1 0 29.00 11.90 10 -1 0 152.68 19.10 10 -1 0 96.59 15.90 -10 1 0 120.99 19.80 9 -1 0 51.39 10.90 9 -1 0 32.40 9.50 -9 1 0 59.19 12.90 8 -1 0 72.69 16.30 -8 1 0 63.49 12.90 7 -1 0 70.79 11.10 7 -1 0 59.69 10.30 -7 1 0 72.59 11.80 6 -1 0 1624.14 52.19 6 -1 0 1578.04 54.59 -6 1 0 1528.65 54.79 5 -1 0 192.58 13.80 5 -1 0 170.88 12.10 -5 1 0 163.68 13.20 4 -1 0 76.19 7.60 4 -1 0 74.79 6.80 -4 1 0 78.59 8.10 3 -1 0 1430.46 42.00 3 -1 0 1473.25 40.00 -3 1 0 1493.15 42.50 2 -1 0 150.58 6.90 2 -1 0 161.18 8.20 -2 1 0 157.88 5.00 -2 1 0 153.18 8.10 1 -1 0 899.81 22.50 1 -1 0 887.71 20.80 1 -1 0 875.41 22.30 1 -1 0 912.11 20.30 -1 1 0 760.22 21.90 -1 1 0 743.93 21.70 -1 1 0 846.62 20.20 0 -1 0 2361.16 53.79 -1 -1 0 6904.31 154.28 -1 -1 0 6824.92 152.18 -1 -1 0 6464.95 152.38 1 1 0 6976.30 152.28 1 1 0 6950.00 154.08 1 1 0 6681.23 153.88 -2 -1 0 5966.30 142.69 2 1 0 6094.59 137.79 2 1 0 6211.18 142.69 2 1 0 6200.08 137.99 2 1 0 6114.09 141.09 -3 -1 0 973.00 32.20 3 1 0 962.10 30.70 3 1 0 970.90 25.60 3 1 0 970.40 25.40 3 1 0 975.00 31.60 -4 -1 0 1156.68 39.90 4 1 0 1188.78 38.80 4 1 0 1154.18 30.20 4 1 0 1188.88 30.20 -5 -1 0 272.37 17.90 5 1 0 283.07 17.40 5 1 0 295.07 17.90 -6 -1 0 50.99 10.00 6 1 0 47.10 9.30 6 1 0 52.69 9.60 -7 -1 0 0.70 2.50 7 1 0 -4.20 2.80 7 1 0 2.20 3.70 -8 -1 0 216.88 21.20 8 1 0 265.97 21.20 8 1 0 236.68 20.20 -9 -1 0 82.39 16.10 9 1 0 87.49 16.00 9 1 0 56.79 12.60 -10 -1 0 9.10 8.80 10 1 0 25.00 9.80 10 1 0 22.50 10.10 -11 -1 0 28.70 12.00 11 1 0 23.40 9.60 11 1 0 28.20 12.30 11 -2 0 159.48 18.80 11 -2 0 120.29 20.00 -11 2 0 136.49 21.40 10 -2 0 65.49 11.70 10 -2 0 78.29 15.40 -10 2 0 85.79 17.20 9 -2 0 1.40 4.80 9 -2 0 3.60 3.20 -9 2 0 -7.60 3.60 8 -2 0 513.95 27.60 8 -2 0 512.55 31.30 -8 2 0 542.85 32.90 7 -2 0 796.02 37.60 7 -2 0 782.82 33.70 -7 2 0 833.42 38.90 6 -2 0 93.89 10.80 6 -2 0 97.79 9.40 -6 2 0 96.19 11.20 5 -2 0 335.47 16.60 5 -2 0 340.77 19.10 -5 2 0 321.37 18.90 4 -2 0 2494.75 63.89 4 -2 0 2442.16 68.19 -4 2 0 2449.85 68.39 3 -2 0 2476.45 64.99 3 -2 0 2458.75 60.69 3 -2 0 2472.95 57.99 -3 2 0 2498.55 58.09 -3 2 0 2468.55 65.39 2 -2 0 411.36 15.60 2 -2 0 445.56 12.40 2 -2 0 420.76 15.40 2 -2 0 435.96 13.30 -2 2 0 431.16 13.20 1 -2 0 316.57 11.40 1 -2 0 318.07 10.80 1 -2 0 315.47 11.00 -1 2 0 310.87 10.90 -1 2 0 314.27 10.60 0 -2 0 1.90 1.10 0 -2 0 2.20 0.70 0 -2 0 0.20 0.80 0 2 0 0.60 0.70 0 2 0 1.60 0.80 0 2 0 0.40 0.70 -1 -2 0 6.20 1.50 -1 -2 0 3.40 1.60 -1 -2 0 4.90 2.30 -1 -2 0 3.30 1.60 1 2 0 14.90 2.90 1 2 0 8.80 1.80 -2 -2 0 5218.08 123.99 -2 -2 0 5018.80 123.99 2 2 0 5379.46 124.49 2 2 0 5179.68 121.49 -3 -2 0 662.43 25.80 3 2 0 665.53 23.60 3 2 0 668.43 21.00 3 2 0 674.33 25.50 -4 -2 0 5936.71 148.29 4 2 0 5851.11 144.49 4 2 0 5849.41 137.29 4 2 0 6009.00 147.59 -5 -2 0 83.89 10.60 5 2 0 93.19 10.30 5 2 0 83.99 9.40 5 2 0 79.29 5.90 -6 -2 0 936.91 41.80 6 2 0 991.30 41.10 6 2 0 977.10 39.60 6 2 0 946.71 27.60 -7 -2 0 5.60 4.80 7 2 0 13.70 4.90 7 2 0 9.10 4.70 -8 -2 0 239.28 22.50 8 2 0 206.48 19.90 8 2 0 209.88 19.30 -9 -2 0 44.80 12.20 9 2 0 47.10 13.20 9 2 0 59.69 12.90 -10 -2 0 -1.30 7.10 10 2 0 8.30 6.30 10 2 0 7.70 6.10 -11 -2 0 10.70 9.10 11 2 0 18.30 7.70 11 2 0 6.90 8.60 11 -3 0 67.59 12.70 11 -3 0 63.79 15.30 -11 3 0 72.79 17.00 10 -3 0 272.67 25.20 10 -3 0 213.38 19.30 -10 3 0 220.98 24.50 9 -3 0 29.70 7.00 9 -3 0 40.60 11.10 -9 3 0 41.90 10.70 8 -3 0 46.70 10.60 8 -3 0 49.80 8.80 -8 3 0 65.69 12.40 7 -3 0 -3.10 1.80 7 -3 0 2.00 2.80 -7 3 0 3.20 3.70 6 -3 0 504.75 26.60 6 -3 0 547.85 23.30 -6 3 0 552.04 28.20 5 -3 0 299.87 18.00 5 -3 0 293.77 14.40 -5 3 0 325.37 18.90 4 -3 0 485.25 17.40 4 -3 0 491.15 21.70 4 -3 0 479.25 15.60 -4 3 0 493.55 22.10 3 -3 0 3867.91 89.39 3 -3 0 3881.81 96.39 3 -3 0 3847.82 91.29 3 -3 0 3854.71 96.79 2 -3 0 433.56 16.90 2 -3 0 447.96 15.60 2 -3 0 465.05 16.70 1 -3 0 2316.97 57.39 1 -3 0 2383.36 54.09 1 -3 0 2388.66 59.39 1 -3 0 2415.96 59.69 0 -3 0 1530.65 40.70 0 -3 0 1522.45 37.90 0 -3 0 1482.45 39.70 0 3 0 1403.06 40.20 0 3 0 1519.45 36.90 -1 -3 0 93.09 6.90 1 3 0 89.19 6.50 1 3 0 98.99 5.40 -2 -3 0 558.94 22.20 -2 -3 0 595.84 22.20 -2 -3 0 571.34 20.30 2 3 0 594.24 22.50 2 3 0 591.74 19.60 -3 -3 0 579.54 24.50 3 3 0 535.45 23.60 3 3 0 565.94 21.30 3 3 0 570.34 20.60 -4 -3 0 758.32 32.00 4 3 0 772.12 31.60 4 3 0 798.12 29.50 4 3 0 775.02 26.00 -5 -3 0 127.59 13.50 5 3 0 135.59 13.00 5 3 0 131.49 11.80 5 3 0 118.59 8.60 -6 -3 0 334.87 23.30 6 3 0 296.87 14.10 6 3 0 305.87 21.70 6 3 0 322.47 20.50 -7 -3 0 186.98 30.60 7 3 0 170.88 16.40 7 3 0 173.68 9.60 7 3 0 167.58 17.10 -8 -3 0 284.57 25.10 8 3 0 274.17 23.40 8 3 0 257.27 21.30 -9 -3 0 33.40 10.80 9 3 0 38.60 10.00 9 3 0 36.60 9.00 -10 -3 0 55.89 15.40 10 3 0 32.50 14.40 10 3 0 69.09 14.40 11 -4 0 -5.30 5.50 11 -4 0 6.40 4.80 -11 4 0 10.80 7.90 10 -4 0 24.80 7.60 10 -4 0 12.10 8.90 -10 4 0 12.50 8.00 9 -4 0 96.69 16.00 9 -4 0 76.99 10.10 -9 4 0 83.59 15.90 8 -4 0 115.69 11.40 8 -4 0 129.59 15.00 -8 4 0 105.99 16.60 7 -4 0 341.57 18.30 7 -4 0 340.77 23.40 -7 4 0 366.16 24.10 6 -4 0 1.60 2.00 -6 4 0 2.80 3.00 5 -4 0 2.70 1.70 5 -4 0 -0.80 2.40 -5 4 0 4.70 2.90 4 -4 0 401.06 19.80 4 -4 0 402.56 13.80 4 -4 0 408.46 15.70 3 -4 0 4713.93 113.19 3 -4 0 4803.72 116.39 3 -4 0 4669.73 116.99 2 -4 0 38.90 4.90 2 -4 0 47.60 5.10 2 -4 0 50.99 5.20 1 -4 0 49.50 4.20 1 -4 0 58.09 5.40 1 -4 0 56.59 5.60 1 -4 0 53.69 3.30 0 -4 0 2097.29 53.29 0 -4 0 2185.08 57.49 0 -4 0 2084.89 55.69 0 4 0 2167.98 53.39 0 4 0 2058.99 51.59 -1 -4 0 2261.07 60.39 -1 -4 0 2281.37 60.69 1 4 0 2139.29 58.09 1 4 0 2275.57 59.29 -2 -4 0 25.60 4.90 -2 -4 0 32.70 5.30 -2 -4 0 35.50 5.70 2 4 0 18.90 3.60 2 4 0 27.40 4.10 -3 -4 0 549.54 24.90 3 4 0 538.55 21.90 3 4 0 519.15 21.00 3 4 0 557.54 24.60 -4 -4 0 42.70 8.40 4 4 0 44.10 7.00 4 4 0 47.30 8.70 4 4 0 46.50 5.80 -5 -4 0 377.46 23.60 5 4 0 348.67 19.90 5 4 0 341.27 22.00 5 4 0 331.77 16.70 -6 -4 0 800.12 39.30 6 4 0 810.32 35.50 6 4 0 841.62 29.60 6 4 0 797.32 38.80 -7 -4 0 672.33 37.50 7 4 0 614.74 24.10 7 4 0 607.14 34.90 7 4 0 647.74 33.30 -8 -4 0 -0.10 3.70 8 4 0 0.90 5.30 8 4 0 8.90 5.70 -9 -4 0 124.09 20.00 9 4 0 165.18 18.10 9 4 0 172.68 20.50 -10 -4 0 632.24 44.90 10 4 0 694.03 41.50 10 4 0 591.84 40.50 11 -5 0 32.80 9.00 11 -5 0 25.30 10.80 -11 5 0 28.30 10.60 10 -5 0 1.40 4.80 10 -5 0 0.20 3.20 -10 5 0 -6.80 5.20 9 -5 0 239.58 16.90 9 -5 0 224.58 21.90 -9 5 0 252.77 24.10 8 -5 0 -3.20 2.00 8 -5 0 11.60 5.30 -8 5 0 -1.00 4.90 7 -5 0 9.90 5.00 7 -5 0 24.80 5.20 -7 5 0 23.40 7.60 6 -5 0 446.66 17.60 6 -5 0 412.76 24.50 -6 5 0 416.26 25.00 -6 5 0 445.06 16.80 5 -5 0 402.96 21.80 5 -5 0 382.86 13.90 -5 5 0 379.26 22.10 4 -5 0 888.71 29.50 4 -5 0 868.51 32.80 3 -5 0 249.48 14.50 3 -5 0 251.87 13.90 3 -5 0 274.37 13.90 2 -5 0 25.90 5.10 2 -5 0 37.50 6.00 2 -5 0 30.00 4.70 1 -5 0 40.90 3.50 1 -5 0 43.10 5.40 1 -5 0 37.90 6.10 -1 5 0 51.49 4.60 0 -5 0 2160.48 59.89 0 -5 0 2167.68 56.69 0 -5 0 2269.87 61.99 0 5 0 2180.28 54.89 0 5 0 2241.98 56.99 -1 -5 0 6493.35 152.78 -1 -5 0 6244.58 154.88 -1 -5 0 6410.06 154.48 1 5 0 6484.85 153.08 1 5 0 6387.86 147.99 -2 -5 0 58.89 6.80 -2 -5 0 65.59 7.50 2 5 0 60.39 5.60 2 5 0 65.99 7.40 -3 -5 0 462.45 23.80 3 5 0 471.95 20.00 3 5 0 496.45 22.30 -4 -5 0 1013.70 41.50 4 5 0 1052.39 41.20 4 5 0 1030.00 37.20 4 5 0 1052.19 36.40 -5 -5 0 465.45 27.60 5 5 0 450.45 23.40 5 5 0 454.15 22.20 5 5 0 457.55 26.80 -6 -5 0 116.99 14.90 6 5 0 117.29 14.40 6 5 0 113.19 12.40 6 5 0 110.69 10.50 -7 -5 0 14.70 7.60 7 5 0 40.70 7.20 7 5 0 33.80 9.00 7 5 0 41.50 10.60 -8 -5 0 213.98 23.50 8 5 0 212.58 21.80 8 5 0 236.58 21.00 -9 -5 0 24.00 18.80 9 5 0 45.90 13.30 9 5 0 28.80 9.10 -10 -5 0 12.30 9.20 11 -6 0 34.10 7.50 11 -6 0 25.60 10.30 -11 6 0 11.60 10.00 10 -6 0 12.60 8.90 10 -6 0 17.20 5.10 -10 6 0 49.50 14.10 9 -6 0 85.89 9.10 9 -6 0 86.49 15.10 -9 6 0 46.40 12.30 8 -6 0 54.09 12.50 8 -6 0 80.09 7.70 -8 6 0 46.50 11.00 7 -6 0 84.99 13.80 7 -6 0 75.19 6.50 -7 6 0 90.19 14.20 -7 6 0 78.69 6.80 6 -6 0 120.69 13.00 6 -6 0 121.69 6.60 -6 6 0 118.19 9.00 -6 6 0 119.39 13.30 5 -6 0 91.19 9.90 5 -6 0 108.09 11.60 4 -6 0 23.40 5.40 4 -6 0 14.90 6.20 4 -6 0 27.50 5.40 3 -6 0 34.60 5.60 3 -6 0 40.60 6.70 3 -6 0 39.60 7.10 2 -6 0 241.18 12.60 2 -6 0 250.77 14.80 2 -6 0 245.68 14.80 1 -6 0 390.66 14.20 1 -6 0 394.46 18.80 1 -6 0 393.26 19.70 -1 6 0 389.56 15.50 0 -6 0 58.39 6.80 0 -6 0 35.60 6.20 0 -6 0 58.99 5.70 0 6 0 55.69 5.00 -1 -6 0 1.80 2.30 -1 -6 0 4.90 2.40 -1 -6 0 0.20 1.50 1 6 0 0.90 1.50 1 6 0 -1.10 1.30 -2 -6 0 30.80 6.20 -2 -6 0 32.20 6.40 2 6 0 26.70 4.40 2 6 0 28.30 5.20 -3 -6 0 235.68 24.80 -3 -6 0 241.48 17.60 3 6 0 281.97 17.50 3 6 0 305.17 19.00 3 6 0 283.77 14.70 -4 -6 0 19.20 6.20 4 6 0 22.60 6.80 4 6 0 29.70 6.70 -5 -6 0 39.20 9.30 5 6 0 54.19 9.10 5 6 0 42.80 8.40 5 6 0 45.50 8.40 -6 -6 0 -4.30 3.80 6 6 0 0.70 3.80 6 6 0 4.80 4.10 -7 -6 0 49.90 12.20 7 6 0 55.09 14.10 7 6 0 77.99 10.20 7 6 0 59.49 11.30 -8 -6 0 26.50 8.90 8 6 0 20.80 7.50 8 6 0 30.70 9.60 8 6 0 32.70 11.00 -9 -6 0 55.89 14.90 9 6 0 69.49 13.40 9 6 0 95.89 17.60 11 -7 0 30.10 11.80 11 -7 0 35.10 6.00 -11 7 0 38.50 10.50 10 -7 0 5.40 3.10 10 -7 0 0.70 5.70 9 -7 0 572.74 36.20 9 -7 0 606.24 21.30 -9 7 0 527.05 36.60 8 -7 0 165.38 17.80 -8 7 0 200.18 20.60 7 -7 0 101.09 13.20 -7 7 0 110.49 9.30 6 -7 0 -3.70 2.60 -6 7 0 2.60 2.40 -6 7 0 5.50 2.90 5 -7 0 293.77 19.10 5 -7 0 299.47 19.90 4 -7 0 701.53 29.10 4 -7 0 715.83 31.50 4 -7 0 756.82 30.50 3 -7 0 607.84 26.70 3 -7 0 598.24 24.50 3 -7 0 580.54 26.50 2 -7 0 286.87 17.80 2 -7 0 308.67 10.20 2 -7 0 316.07 10.10 1 -7 0 343.37 19.80 1 -7 0 351.76 14.10 1 -7 0 365.66 19.30 -1 7 0 344.27 15.10 0 -7 0 148.59 9.80 0 -7 0 143.19 12.40 0 -7 0 136.79 17.20 0 7 0 145.79 8.60 -1 -7 0 68.99 7.50 -1 -7 0 62.29 9.30 -1 -7 0 70.19 8.70 1 7 0 81.19 6.40 1 7 0 68.59 7.70 -2 -7 0 198.88 15.10 2 7 0 196.78 14.30 2 7 0 194.98 11.10 -3 -7 0 2.40 4.40 -3 -7 0 10.60 4.70 3 7 0 7.90 4.10 3 7 0 6.90 3.70 3 7 0 14.70 4.30 -4 -7 0 455.35 27.30 4 7 0 448.26 21.70 4 7 0 446.36 26.20 4 7 0 460.65 25.00 -5 -7 0 73.69 13.70 5 7 0 62.59 9.90 5 7 0 56.59 10.70 5 7 0 75.19 11.40 -6 -7 0 75.79 13.70 6 7 0 85.19 15.80 6 7 0 84.99 11.10 6 7 0 69.39 11.10 -7 -7 0 29.90 11.10 7 7 0 30.00 9.00 7 7 0 37.10 8.90 7 7 0 32.80 7.70 -8 -7 0 58.49 14.40 8 7 0 78.19 18.40 8 7 0 88.29 15.00 8 7 0 70.79 11.50 -9 -7 0 8.90 8.60 9 7 0 2.30 8.00 9 7 0 -13.70 6.90 10 -8 0 38.00 11.10 -10 8 0 35.90 11.10 9 -8 0 218.48 22.80 -9 8 0 248.68 24.60 8 -8 0 173.88 19.30 -8 8 0 212.48 13.10 -8 8 0 187.08 20.60 7 -8 0 11.80 6.60 -7 8 0 0.50 3.90 -7 8 0 6.10 3.50 6 -8 0 78.29 12.20 -6 8 0 80.19 9.20 5 -8 0 1.60 2.80 5 -8 0 4.80 3.70 4 -8 0 930.61 36.90 4 -8 0 929.31 38.40 4 -8 0 919.21 35.40 3 -8 0 12.90 5.20 3 -8 0 10.20 4.30 3 -8 0 13.20 3.90 2 -8 0 164.78 7.50 2 -8 0 171.38 7.50 2 -8 0 167.88 14.10 2 -8 0 174.88 14.10 -2 8 0 161.78 10.90 1 -8 0 35.30 8.10 1 -8 0 36.20 4.60 1 -8 0 34.80 7.10 -1 8 0 44.30 6.30 0 -8 0 13.30 4.40 0 -8 0 9.30 3.80 0 -8 0 9.30 4.00 0 8 0 8.70 2.80 -1 -8 0 -2.80 1.80 -1 -8 0 12.00 4.70 1 8 0 3.00 2.00 1 8 0 -1.20 3.10 -2 -8 0 248.88 17.30 -2 -8 0 286.27 19.30 2 8 0 269.47 19.50 2 8 0 263.37 17.70 2 8 0 288.67 14.40 -3 -8 0 68.79 11.30 -3 -8 0 25.30 7.90 3 8 0 48.90 10.00 3 8 0 49.30 6.50 3 8 0 51.89 8.80 -4 -8 0 1.90 4.30 4 8 0 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247.08 18.30 -1 -8 3 263.97 16.00 0 8 -3 7.90 3.70 0 -8 3 6.70 3.10 0 -8 3 12.10 4.80 -1 8 -3 262.17 18.20 1 -8 3 249.58 18.30 1 -8 3 259.37 13.70 1 -8 3 265.57 14.30 -2 8 -3 5.00 3.50 2 -8 3 -2.40 3.00 2 -8 3 10.30 2.70 2 -8 3 3.20 2.30 2 -8 3 2.10 2.20 -3 8 -3 44.70 7.80 3 -8 3 44.10 6.80 3 -8 3 41.40 4.70 3 -8 3 65.59 11.20 3 -8 3 53.39 5.20 -4 8 -3 31.90 7.00 4 -8 3 36.80 4.40 4 -8 3 38.40 9.30 4 -8 3 47.00 8.20 4 -8 3 42.50 4.40 -5 8 -3 128.19 11.30 5 -8 3 119.29 7.60 5 -8 3 113.19 12.00 5 -8 3 105.29 7.30 5 -8 3 109.49 16.80 -6 8 -3 -0.90 3.50 6 -8 3 6.60 4.80 6 -8 3 6.20 2.40 6 -8 3 4.90 2.10 -7 8 -3 -3.70 3.50 -7 8 -3 13.80 5.40 7 -8 3 12.10 6.60 7 -8 3 5.60 2.80 8 -8 3 -0.30 5.20 8 -8 3 4.60 2.20 -9 8 -3 47.30 13.60 9 -8 3 43.60 7.00 9 -8 3 32.80 12.00 9 7 -3 -1.40 5.70 9 7 -3 10.50 9.80 9 7 -3 -1.00 6.00 -9 -7 3 6.90 6.90 8 7 -3 179.08 16.00 8 7 -3 186.68 16.90 8 7 -3 195.38 21.00 -8 -7 3 200.88 22.70 7 7 -3 192.88 20.80 7 7 -3 171.68 15.50 7 7 -3 194.88 15.20 -7 -7 3 173.28 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5.30 -6 7 -3 21.20 7.60 6 -7 3 31.10 5.50 6 -7 3 37.70 9.00 -7 7 -3 63.79 12.90 7 -7 3 63.79 7.70 7 -7 3 63.59 12.40 -8 7 -3 165.08 20.90 8 -7 3 174.78 13.50 8 -7 3 181.78 19.50 -9 7 -3 58.09 17.10 9 -7 3 36.90 10.80 -10 7 -3 8.50 10.20 10 -7 3 2.00 3.00 10 -7 3 2.30 7.90 10 6 -3 95.79 20.60 10 6 -3 45.10 11.10 -10 -6 3 54.09 15.30 9 6 -3 -1.80 5.30 9 6 -3 4.10 6.50 9 6 -3 12.70 6.30 -9 -6 3 4.20 7.30 8 6 -3 78.29 15.70 8 6 -3 71.19 11.00 8 6 -3 63.49 10.70 -8 -6 3 78.79 16.10 7 6 -3 11.60 5.20 7 6 -3 24.50 7.10 -7 -6 3 2.10 5.00 6 6 -3 18.60 5.10 6 6 -3 19.30 5.90 -6 -6 3 2.70 5.40 5 6 -3 196.38 17.30 5 6 -3 235.48 16.60 5 6 -3 205.68 12.70 -5 -6 3 217.38 18.90 4 6 -3 504.15 26.30 4 6 -3 505.85 25.30 4 6 -3 498.85 18.70 -4 -6 3 492.65 27.40 3 6 -3 144.99 12.40 3 6 -3 120.29 11.70 3 6 -3 124.59 6.60 -3 -6 3 148.79 13.30 2 6 -3 184.78 13.60 2 6 -3 167.08 12.20 -2 -6 3 169.88 13.50 -2 -6 3 153.48 12.70 1 6 -3 702.33 26.80 1 6 -3 761.12 30.10 -1 -6 3 674.03 29.00 -1 -6 3 702.03 26.80 0 6 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47.50 8.60 7 5 -3 54.99 9.50 -7 -5 3 30.20 9.10 6 5 -3 28.00 6.50 6 5 -3 24.40 7.40 6 5 -3 28.90 6.50 -6 -5 3 27.10 8.50 5 5 -3 268.67 19.30 5 5 -3 280.67 15.30 5 5 -3 276.67 17.20 -5 -5 3 263.97 19.80 4 5 -3 330.27 19.80 4 5 -3 312.17 18.00 4 5 -3 330.27 14.60 -4 -5 3 356.26 21.30 3 5 -3 374.06 13.30 3 5 -3 369.76 20.10 3 5 -3 335.47 24.20 -3 -5 3 375.06 20.80 2 5 -3 52.39 6.40 2 5 -3 38.50 6.80 -2 -5 3 46.90 7.50 -2 -5 3 35.40 5.60 1 5 -3 200.98 12.00 1 5 -3 210.28 13.40 -1 -5 3 225.08 14.00 0 -5 3 897.31 32.80 0 -5 3 895.61 29.80 0 -5 3 954.80 30.00 -1 5 -3 525.65 21.70 1 -5 3 502.05 16.70 1 -5 3 501.45 19.20 1 -5 3 520.65 22.90 1 -5 3 504.25 19.00 -2 5 -3 152.18 10.50 2 -5 3 152.58 12.00 2 -5 3 158.88 9.40 2 -5 3 156.28 9.60 -3 5 -3 788.82 27.30 3 -5 3 785.72 29.00 3 -5 3 778.42 26.60 3 -5 3 778.22 32.30 -4 5 -3 508.45 19.90 4 -5 3 520.05 26.90 4 -5 3 528.25 21.60 4 -5 3 562.44 25.40 -5 5 -3 369.26 15.00 -5 5 -3 392.76 25.00 5 -5 3 394.66 19.20 5 -5 3 393.56 22.70 -6 5 -3 20.40 7.10 6 -5 3 15.00 5.90 6 -5 3 27.40 6.10 -7 5 -3 88.19 15.00 7 -5 3 76.79 13.90 7 -5 3 90.29 9.90 -8 5 -3 258.97 24.00 8 -5 3 250.97 18.60 8 -5 3 224.08 21.90 -9 5 -3 8.50 7.40 9 -5 3 11.30 6.60 9 -5 3 5.80 3.80 -10 5 -3 20.10 8.20 10 -5 3 28.30 8.30 10 -5 3 10.00 8.50 11 4 -3 200.18 23.40 11 4 -3 173.08 21.20 -11 -4 3 148.99 23.80 10 4 -3 -12.40 4.90 -10 -4 3 1.50 11.30 9 4 -3 4.80 4.60 9 4 -3 11.50 7.30 -9 -4 3 1.20 6.50 8 4 -3 7.90 5.30 8 4 -3 24.80 5.90 8 4 -3 7.90 5.40 -8 -4 3 9.70 6.50 7 4 -3 454.65 24.70 7 4 -3 425.86 21.50 7 4 -3 437.86 27.80 -7 -4 3 455.55 29.60 6 4 -3 280.57 20.10 6 4 -3 250.37 16.30 -6 -4 3 238.68 19.70 5 4 -3 15.40 4.40 5 4 -3 15.90 4.40 5 4 -3 8.40 3.70 -5 -4 3 14.00 5.40 4 4 -3 112.99 9.50 4 4 -3 105.69 7.90 4 4 -3 107.09 10.50 -4 -4 3 96.29 10.40 3 4 -3 805.72 24.00 3 4 -3 776.52 29.10 3 4 -3 822.02 31.00 -3 -4 3 799.02 31.30 2 4 -3 1025.50 34.30 2 4 -3 1062.49 26.10 2 4 -3 1009.10 34.10 -2 -4 3 1011.20 25.80 -2 -4 3 1048.90 35.30 1 4 -3 8.60 2.90 1 4 -3 17.40 3.90 -1 -4 3 12.20 2.80 -1 -4 3 7.60 3.00 0 4 -3 1518.65 37.20 0 4 -3 1542.45 45.20 0 -4 3 1607.44 43.60 0 -4 3 1577.94 37.30 0 -4 3 1495.35 43.20 0 -4 3 1549.05 45.80 -1 4 -3 1454.35 42.80 1 -4 3 1508.95 41.70 1 -4 3 1483.45 41.60 1 -4 3 1479.85 39.30 1 -4 3 1492.25 44.90 -2 4 -3 1239.18 36.70 2 -4 3 1263.37 36.70 2 -4 3 1213.98 40.60 2 -4 3 1239.18 37.10 -3 4 -3 38.30 4.50 3 -4 3 32.20 5.60 3 -4 3 33.50 6.90 3 -4 3 29.50 4.90 -4 4 -3 129.69 7.50 4 -4 3 121.39 9.60 4 -4 3 98.19 10.50 -5 4 -3 5.20 3.90 5 -4 3 6.20 2.70 5 -4 3 7.80 4.10 -6 4 -3 1445.26 57.09 6 -4 3 1533.15 56.19 6 -4 3 1501.35 50.69 -7 4 -3 84.09 14.50 7 -4 3 87.89 10.50 7 -4 3 84.29 14.10 -8 4 -3 8.50 6.20 8 -4 3 20.10 4.30 8 -4 3 7.30 4.80 -9 4 -3 11.00 7.40 9 -4 3 1.60 5.00 9 -4 3 6.90 4.50 -10 4 -3 19.90 10.10 10 -4 3 15.60 10.00 10 -4 3 5.90 5.10 11 3 -3 14.30 8.90 11 3 -3 12.00 6.40 -11 -3 3 2.50 8.10 10 3 -3 3.20 4.80 10 3 -3 2.20 5.70 -10 -3 3 6.40 7.30 9 3 -3 54.89 11.80 9 3 -3 56.79 11.80 9 3 -3 60.39 7.70 -9 -3 3 46.40 10.70 8 3 -3 93.09 13.90 8 3 -3 84.59 8.60 8 3 -3 71.99 12.60 -8 -3 3 79.69 14.80 7 3 -3 130.19 14.30 7 3 -3 124.09 12.30 7 3 -3 120.99 10.30 -7 -3 3 116.49 14.40 6 3 -3 47.20 8.10 6 3 -3 50.39 9.60 6 3 -3 50.69 6.60 -6 -3 3 50.39 10.40 5 3 -3 5.80 2.90 5 3 -3 -0.90 2.00 5 3 -3 2.70 2.40 -5 -3 3 5.80 3.60 4 3 -3 191.98 11.70 4 3 -3 161.18 10.30 4 3 -3 170.78 12.70 -4 -3 3 189.98 13.90 3 3 -3 378.96 17.00 3 3 -3 354.86 17.80 3 3 -3 375.56 14.40 2 3 -3 152.48 9.80 2 3 -3 149.79 9.90 2 3 -3 154.08 6.70 -2 -3 3 163.28 10.40 -2 -3 3 152.98 9.90 -2 -3 3 150.98 6.60 1 3 -3 20.00 3.90 1 3 -3 20.30 3.80 -1 -3 3 28.60 2.10 -1 -3 3 25.60 2.00 -1 -3 3 24.60 4.20 -1 -3 3 22.50 3.80 0 3 -3 209.98 8.20 0 3 -3 221.18 11.20 0 -3 3 217.98 11.50 0 -3 3 219.38 8.30 0 -3 3 229.88 11.10 -1 3 -3 1.60 1.40 1 -3 3 1.50 1.30 1 -3 3 1.60 1.30 1 -3 3 3.70 1.60 -2 3 -3 36.20 4.10 2 -3 3 40.60 4.80 2 -3 3 41.80 4.70 2 -3 3 30.60 5.40 -3 3 -3 193.18 9.30 3 -3 3 192.48 11.70 3 -3 3 193.88 13.30 3 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13.00 9 8 -4 78.59 19.40 9 8 -4 54.39 12.00 -9 -8 4 67.49 17.50 8 8 -4 3.10 7.30 -8 -8 4 3.80 6.50 7 8 -4 54.59 12.00 7 8 -4 51.89 12.00 7 8 -4 65.29 9.50 -7 -8 4 82.49 16.70 6 8 -4 17.00 6.10 6 8 -4 13.30 4.50 6 8 -4 36.10 11.30 -6 -8 4 19.20 8.40 5 8 -4 537.95 30.00 5 8 -4 523.35 19.30 5 8 -4 524.55 30.80 -5 -8 4 510.45 32.30 4 8 -4 145.59 14.60 4 8 -4 141.69 15.00 -4 -8 4 143.79 16.10 3 8 -4 12.50 4.50 3 8 -4 13.90 5.40 -3 -8 4 29.00 6.60 -3 -8 4 17.80 6.80 2 8 -4 1639.04 58.19 2 8 -4 1600.54 54.09 -2 -8 4 1644.84 58.49 1 8 -4 601.34 30.40 1 8 -4 597.74 26.80 -1 -8 4 618.24 30.80 -1 -8 4 622.24 27.20 0 8 -4 1216.88 45.60 0 -8 4 1168.78 41.00 0 -8 4 1112.49 45.20 0 -8 4 1202.78 40.90 -1 8 -4 32.40 7.70 1 -8 4 41.80 8.20 1 -8 4 47.00 6.30 1 -8 4 46.00 6.20 -2 8 -4 2075.19 65.39 2 -8 4 2000.90 67.69 2 -8 4 2041.10 57.39 2 -8 4 2018.90 54.79 2 -8 4 2049.49 57.89 -3 8 -4 86.09 10.50 3 -8 4 97.19 8.90 3 -8 4 68.39 11.60 3 -8 4 99.59 8.20 3 -8 4 95.49 8.20 -4 8 -4 28.70 6.20 4 -8 4 36.70 7.20 4 -8 4 27.40 5.10 4 -8 4 35.00 5.60 4 -8 4 30.40 7.60 -5 8 -4 7.70 4.40 5 -8 4 16.80 5.50 5 -8 4 15.80 7.30 5 -8 4 13.90 3.90 5 -8 4 11.10 3.70 -6 8 -4 140.29 12.60 6 -8 4 154.28 15.10 6 -8 4 135.29 10.50 -7 8 -4 172.78 20.70 7 -8 4 155.18 12.10 7 -8 4 184.18 18.40 -8 8 -4 38.90 11.30 8 -8 4 44.00 11.50 8 -8 4 30.00 6.50 -9 8 -4 8.50 7.40 9 -8 4 13.30 7.10 9 -8 4 10.60 4.10 10 7 -4 62.59 17.30 10 7 -4 61.69 13.10 -10 -7 4 43.50 13.00 9 7 -4 130.59 15.00 9 7 -4 110.39 17.70 9 7 -4 118.79 13.90 -9 -7 4 114.49 20.90 8 7 -4 172.28 20.00 8 7 -4 140.69 14.30 8 7 -4 153.98 15.90 -8 -7 4 156.18 20.30 7 7 -4 78.69 12.30 7 7 -4 88.39 16.00 7 7 -4 88.99 10.30 -7 -7 4 120.69 18.80 6 7 -4 13.90 7.10 6 7 -4 14.60 6.50 6 7 -4 7.50 4.80 -6 -7 4 5.90 5.60 5 7 -4 35.90 8.50 5 7 -4 43.60 5.70 5 7 -4 36.10 8.00 -5 -7 4 61.89 11.60 4 7 -4 274.87 19.30 4 7 -4 244.78 18.50 -4 -7 4 283.87 21.00 3 7 -4 84.49 9.70 3 7 -4 67.79 11.10 -3 -7 4 75.99 9.20 -3 -7 4 94.09 11.00 2 7 -4 211.88 16.30 2 7 -4 192.38 14.20 -2 -7 4 228.28 17.00 -2 -7 4 197.18 14.50 1 7 -4 399.46 20.20 1 7 -4 371.36 22.10 -1 -7 4 388.36 22.30 -1 -7 4 414.96 20.50 0 7 -4 5.20 3.00 0 -7 4 1.20 1.50 0 -7 4 -2.70 1.70 0 -7 4 2.70 2.40 -1 7 -4 198.58 14.80 1 -7 4 189.98 15.30 1 -7 4 182.48 8.70 1 -7 4 197.48 12.40 1 -7 4 197.18 12.20 -2 7 -4 2132.89 64.39 2 -7 4 2077.49 67.39 2 -7 4 2135.89 59.39 2 -7 4 2149.78 57.19 2 -7 4 2078.29 58.49 -3 7 -4 34.40 6.80 3 -7 4 27.10 5.20 3 -7 4 31.80 7.50 3 -7 4 39.80 6.70 3 -7 4 34.30 5.80 -4 7 -4 260.97 15.80 4 -7 4 236.18 19.30 4 -7 4 214.28 13.30 4 -7 4 238.08 16.10 -5 7 -4 828.62 30.70 5 -7 4 849.91 31.30 5 -7 4 834.32 41.50 5 -7 4 831.72 36.40 -6 7 -4 291.77 14.70 -6 7 -4 257.47 23.20 6 -7 4 275.97 16.70 6 -7 4 261.87 20.20 -7 7 -4 15.90 8.30 7 -7 4 8.80 6.20 7 -7 4 19.10 5.50 -8 7 -4 99.79 17.50 8 -7 4 118.09 18.50 8 -7 4 100.29 11.20 -9 7 -4 45.80 13.60 9 -7 4 22.20 6.20 9 -7 4 11.00 8.30 10 6 -4 55.89 13.80 10 6 -4 61.49 13.10 -10 -6 4 76.19 15.90 9 6 -4 136.29 15.80 9 6 -4 146.29 14.80 9 6 -4 154.78 19.80 -9 -6 4 79.59 16.40 8 6 -4 -0.20 4.60 8 6 -4 -0.30 5.60 8 6 -4 -10.50 3.80 -8 -6 4 8.00 6.40 7 6 -4 10.20 4.40 7 6 -4 14.20 4.80 -7 -6 4 4.40 5.10 6 6 -4 15.00 7.70 6 6 -4 3.70 4.60 6 6 -4 14.30 4.10 -6 -6 4 19.20 7.80 5 6 -4 964.50 41.40 5 6 -4 959.40 38.70 5 6 -4 922.11 31.30 -5 -6 4 928.11 42.20 4 6 -4 306.97 19.40 4 6 -4 292.37 19.50 4 6 -4 308.27 13.00 -4 -6 4 332.87 21.50 3 6 -4 44.90 8.50 3 6 -4 16.10 3.90 -3 -6 4 27.90 6.60 2 6 -4 636.94 27.00 2 6 -4 618.34 27.80 -2 -6 4 601.54 26.50 -2 -6 4 591.14 27.90 1 6 -4 52.69 7.80 -1 -6 4 64.89 8.20 0 6 -4 215.78 14.50 0 -6 4 203.98 12.80 0 -6 4 202.48 12.40 0 -6 4 207.38 14.60 1 -6 4 325.57 12.70 1 -6 4 317.27 15.60 1 -6 4 315.67 18.70 1 -6 4 308.67 15.80 -2 6 -4 2200.18 63.59 2 -6 4 2136.49 67.09 2 -6 4 2251.57 60.79 2 -6 4 2217.68 59.29 2 -6 4 2147.39 60.49 -3 6 -4 0.00 2.10 3 -6 4 -1.10 2.70 3 -6 4 0.60 2.10 3 -6 4 0.50 1.80 -4 6 -4 2052.39 58.09 4 -6 4 2059.19 62.99 4 -6 4 2019.10 58.59 4 -6 4 2013.60 68.09 -5 6 -4 9.50 3.50 5 -6 4 11.40 3.70 5 -6 4 4.20 4.10 -6 6 -4 386.56 27.90 6 -6 4 396.36 21.50 6 -6 4 404.36 25.70 -7 6 -4 21.10 8.10 7 -6 4 21.40 5.60 7 -6 4 23.10 6.80 -8 6 -4 230.48 24.10 8 -6 4 190.88 20.80 8 -6 4 199.78 17.10 -9 6 -4 -2.80 6.70 9 -6 4 -0.60 3.20 -10 6 -4 19.70 10.90 10 -6 4 13.50 8.60 10 -6 4 20.40 7.30 10 5 -4 4.10 6.50 10 5 -4 11.30 8.10 -10 -5 4 -5.30 6.60 9 5 -4 53.19 10.30 9 5 -4 58.49 12.70 9 5 -4 72.29 11.20 -9 -5 4 68.19 14.10 8 5 -4 50.19 10.50 8 5 -4 53.69 9.80 8 5 -4 62.29 12.20 -8 -5 4 50.59 12.70 7 5 -4 144.09 13.10 7 5 -4 113.79 14.70 7 5 -4 134.69 12.70 -7 -5 4 137.19 16.30 6 5 -4 591.94 25.90 6 5 -4 605.54 28.10 6 5 -4 594.44 32.20 -6 -5 4 591.24 32.70 5 5 -4 230.38 16.30 5 5 -4 254.97 14.00 5 5 -4 240.88 18.30 -5 -5 4 235.38 18.50 4 5 -4 3.50 2.80 4 5 -4 4.80 2.20 4 5 -4 2.50 2.50 -4 -5 4 6.90 3.70 3 5 -4 171.48 12.90 3 5 -4 172.38 13.20 3 5 -4 181.08 7.90 -3 -5 4 179.18 13.80 2 5 -4 2350.06 64.69 2 5 -4 1999.70 71.39 -2 -5 4 2123.89 67.89 -2 -5 4 2335.07 64.19 1 5 -4 283.47 15.30 -1 -5 4 271.37 16.00 -1 -5 4 280.87 15.10 0 5 -4 5.50 1.50 0 5 -4 4.90 2.60 0 -5 4 5.40 2.70 0 -5 4 7.10 1.60 0 -5 4 2.10 1.90 0 -5 4 5.30 2.60 -1 5 -4 305.77 16.20 1 -5 4 315.47 15.40 1 -5 4 307.57 15.30 1 -5 4 307.27 17.30 1 -5 4 285.37 12.50 -2 5 -4 35.90 5.80 2 -5 4 43.20 5.20 2 -5 4 42.30 8.00 2 -5 4 46.30 5.70 -3 5 -4 155.78 10.60 3 -5 4 140.19 12.80 3 -5 4 163.68 11.80 3 -5 4 157.28 11.00 -4 5 -4 874.01 29.50 4 -5 4 916.81 36.20 4 -5 4 904.71 38.60 4 -5 4 886.31 32.70 -5 5 -4 11.20 5.10 -5 5 -4 14.30 3.00 5 -5 4 8.40 4.20 5 -5 4 13.20 4.20 -6 5 -4 288.47 27.80 6 -5 4 282.17 21.30 6 -5 4 295.07 21.00 -7 5 -4 5.10 5.10 7 -5 4 3.70 3.40 7 -5 4 0.00 3.90 -8 5 -4 402.26 32.10 8 -5 4 395.86 25.30 8 -5 4 390.06 29.40 -9 5 -4 -0.20 7.70 9 -5 4 5.60 6.10 9 -5 4 10.70 7.00 -10 5 -4 269.97 28.90 10 -5 4 281.97 23.60 10 -5 4 267.17 27.70 11 4 -4 -1.10 5.70 11 4 -4 1.70 6.60 -11 -4 4 10.00 7.60 10 4 -4 9.60 6.70 10 4 -4 16.40 7.20 -10 -4 4 -1.20 7.40 9 4 -4 16.60 6.00 9 4 -4 21.10 9.30 9 4 -4 16.00 8.00 -9 -4 4 14.70 8.70 8 4 -4 109.69 12.90 8 4 -4 100.89 16.40 8 4 -4 97.69 11.00 -8 -4 4 77.09 14.50 7 4 -4 9.00 4.10 7 4 -4 4.70 4.60 7 4 -4 10.60 4.30 -7 -4 4 17.50 7.00 6 4 -4 14.60 4.40 6 4 -4 25.50 6.30 6 4 -4 33.10 8.40 -6 -4 4 19.60 7.10 5 4 -4 296.97 17.60 5 4 -4 299.87 16.00 -5 -4 4 303.97 20.20 4 4 -4 88.89 7.10 4 4 -4 78.59 9.40 4 4 -4 81.69 8.80 -4 -4 4 82.39 9.40 3 4 -4 50.69 4.40 3 4 -4 57.89 7.20 -3 -4 4 58.69 7.40 2 4 -4 169.88 11.80 2 4 -4 170.08 11.60 -2 -4 4 189.88 12.20 -2 -4 4 169.28 7.00 -2 -4 4 161.98 11.30 -2 -4 4 164.68 6.80 1 4 -4 1771.32 52.39 1 4 -4 1792.32 51.69 -1 -4 4 1809.62 43.00 -1 -4 4 1829.22 52.59 -1 -4 4 1809.72 43.00 -1 -4 4 1754.52 51.99 -1 -4 4 1794.92 53.29 0 4 -4 1685.03 49.90 0 -4 4 1759.22 50.69 0 -4 4 1718.13 49.30 0 -4 4 1732.43 43.50 -1 4 -4 117.99 9.00 1 -4 4 136.99 9.50 1 -4 4 127.89 8.00 1 -4 4 114.49 9.70 -2 4 -4 3007.60 77.19 2 -4 4 2972.40 81.99 2 -4 4 2979.80 77.69 2 -4 4 2990.60 78.59 -3 4 -4 18.50 3.80 3 -4 4 15.60 4.00 3 -4 4 14.10 4.50 3 -4 4 20.80 5.30 -4 4 -4 10.20 2.80 4 -4 4 11.20 4.60 4 -4 4 4.10 3.00 -5 4 -4 912.41 28.70 -5 4 -4 901.21 40.70 5 -4 4 946.61 39.40 5 -4 4 915.11 35.90 -6 4 -4 138.79 15.80 6 -4 4 133.19 12.90 6 -4 4 105.49 13.60 -7 4 -4 69.19 13.80 7 -4 4 94.89 12.00 7 -4 4 73.89 13.40 -8 4 -4 152.88 19.80 8 -4 4 179.48 20.20 8 -4 4 152.38 16.10 -9 4 -4 457.05 47.20 9 -4 4 445.96 34.80 9 -4 4 393.66 29.50 -10 4 -4 1.10 6.20 10 -4 4 4.40 6.70 10 -4 4 -1.20 4.30 11 3 -4 37.80 13.70 -11 -3 4 60.89 15.40 10 3 -4 27.10 9.30 10 3 -4 29.50 9.50 -10 -3 4 51.29 12.60 9 3 -4 117.09 15.70 9 3 -4 102.49 15.90 -9 -3 4 85.49 15.70 8 3 -4 1.60 3.70 8 3 -4 4.30 4.00 8 3 -4 6.20 4.20 -8 -3 4 -4.30 3.10 7 3 -4 48.40 9.10 7 3 -4 48.60 10.90 7 3 -4 43.00 8.90 -7 -3 4 48.70 11.30 6 3 -4 41.00 7.30 6 3 -4 42.70 8.70 6 3 -4 32.40 6.60 -6 -3 4 47.60 9.70 5 3 -4 40.00 7.20 5 3 -4 31.90 5.80 5 3 -4 35.10 7.50 -5 -3 4 49.60 9.00 4 3 -4 827.92 30.60 4 3 -4 845.82 28.30 -4 -3 4 852.51 33.00 3 3 -4 1.30 1.80 3 3 -4 5.20 1.90 3 3 -4 2.80 1.60 -3 -3 4 7.40 3.10 2 3 -4 803.52 28.70 2 3 -4 805.92 29.20 -2 -3 4 841.72 28.60 -2 -3 4 798.22 23.40 1 3 -4 5291.47 132.19 -1 -3 4 5499.55 131.59 -1 -3 4 5613.34 132.69 -1 -3 4 5494.95 125.59 -1 -3 4 5483.85 132.69 0 3 -4 31.00 5.20 0 -3 4 26.00 3.30 0 -3 4 18.90 3.60 0 -3 4 19.50 3.80 -1 3 -4 1022.90 32.30 1 -3 4 1024.40 31.60 1 -3 4 1068.09 34.20 1 -3 4 1035.60 33.60 -2 3 -4 1045.50 32.40 2 -3 4 1073.49 36.70 2 -3 4 1064.09 35.10 2 -3 4 1104.99 35.60 -3 3 -4 3187.98 79.89 3 -3 4 3268.37 89.19 3 -3 4 3237.08 86.89 3 -3 4 3219.68 86.09 -4 3 -4 115.59 11.70 -4 3 -4 113.19 7.00 4 -3 4 108.59 10.90 4 -3 4 101.59 9.90 -5 3 -4 123.89 13.30 5 -3 4 108.69 11.40 5 -3 4 132.39 13.40 -6 3 -4 13.80 5.70 6 -3 4 14.20 4.60 6 -3 4 3.00 3.80 -7 3 -4 361.96 27.50 7 -3 4 385.76 24.90 7 -3 4 355.66 26.50 -8 3 -4 330.97 28.10 8 -3 4 348.87 25.20 8 -3 4 345.27 28.00 -9 3 -4 -1.90 6.50 9 -3 4 31.40 8.40 9 -3 4 8.00 7.00 -10 3 -4 18.20 8.80 10 -3 4 2.80 8.20 10 -3 4 9.30 5.90 11 2 -4 140.09 26.70 11 2 -4 81.89 19.00 -11 -2 4 109.79 20.40 10 2 -4 2.30 4.60 10 2 -4 12.90 6.00 -10 -2 4 6.80 7.50 9 2 -4 39.40 9.80 9 2 -4 40.10 10.50 9 2 -4 50.39 6.90 -9 -2 4 42.30 11.20 8 2 -4 10.90 5.30 8 2 -4 14.80 5.70 8 2 -4 19.60 5.20 -8 -2 4 8.00 10.80 7 2 -4 23.80 6.80 7 2 -4 40.60 6.80 7 2 -4 38.80 9.30 -7 -2 4 32.20 8.70 6 2 -4 1.60 2.80 6 2 -4 11.50 4.30 6 2 -4 7.20 3.40 -6 -2 4 1.70 3.90 5 2 -4 201.48 14.60 5 2 -4 183.18 12.20 5 2 -4 180.88 12.40 -5 -2 4 197.38 14.70 4 2 -4 2.00 1.80 4 2 -4 0.50 1.40 4 2 -4 1.60 2.00 -4 -2 4 2.80 2.60 2 2 -4 332.47 16.10 2 2 -4 356.16 16.10 -2 -2 4 337.47 13.30 -2 -2 4 344.67 14.80 1 2 -4 4108.59 102.79 -1 -2 4 4175.98 103.29 -1 -2 4 4186.28 98.89 -1 -2 4 4294.77 100.69 -1 -2 4 4171.78 103.29 0 2 -4 2.90 1.80 0 -2 4 -0.10 0.90 0 -2 4 1.10 1.50 0 -2 4 5.30 1.90 -1 2 -4 427.26 17.00 1 -2 4 412.36 17.50 1 -2 4 416.36 18.10 1 -2 4 433.06 17.60 -2 2 -4 17.40 3.40 2 -2 4 31.10 5.60 2 -2 4 18.50 4.40 2 -2 4 19.70 4.30 -3 2 -4 1004.30 36.10 -3 2 -4 938.91 28.10 3 -2 4 990.10 34.90 3 -2 4 840.22 40.90 -4 2 -4 131.59 12.40 4 -2 4 146.99 12.50 4 -2 4 144.49 12.80 -5 2 -4 842.52 37.70 5 -2 4 873.31 38.10 5 -2 4 819.72 35.60 -6 2 -4 173.98 17.20 6 -2 4 145.89 14.50 6 -2 4 136.99 15.30 -7 2 -4 230.68 21.20 7 -2 4 224.08 18.90 7 -2 4 222.98 20.80 -8 2 -4 127.29 20.30 8 -2 4 89.79 15.30 8 -2 4 72.69 14.70 -9 2 -4 17.50 8.10 9 -2 4 11.40 7.50 9 -2 4 3.30 4.70 -10 2 -4 24.30 9.50 10 -2 4 5.20 6.80 10 -2 4 15.80 7.90 11 1 -4 181.88 24.20 11 1 -4 140.99 21.60 -11 -1 4 135.99 24.70 10 1 -4 201.28 20.40 10 1 -4 160.38 18.00 -10 -1 4 230.78 23.30 9 1 -4 27.70 5.20 9 1 -4 20.20 7.20 9 1 -4 15.40 6.90 -9 -1 4 18.50 8.10 8 1 -4 191.48 12.20 8 1 -4 197.78 17.40 8 1 -4 206.48 17.60 -8 -1 4 184.38 18.10 7 1 -4 342.77 17.30 7 1 -4 375.26 22.70 7 1 -4 370.96 22.50 -7 -1 4 359.16 23.60 6 1 -4 528.85 21.90 6 1 -4 471.25 24.80 6 1 -4 525.95 25.30 -6 -1 4 535.75 26.60 5 1 -4 657.43 25.20 5 1 -4 678.23 27.40 5 1 -4 651.93 27.90 -5 -1 4 650.73 27.80 4 1 -4 144.39 10.80 4 1 -4 136.89 9.70 4 1 -4 139.29 10.10 -4 -1 4 141.99 10.60 3 1 -4 247.88 13.20 3 1 -4 250.27 12.30 3 1 -4 236.58 13.20 -3 -1 4 230.78 12.10 2 1 -4 51.69 5.50 -2 -1 4 45.80 4.70 -2 -1 4 51.59 4.60 -1 -1 4 9999.00 212.18 -1 -1 4 7895.01 214.28 -1 -1 4 9900.71 214.78 0 1 -4 550.54 20.30 0 -1 4 553.74 18.30 0 -1 4 543.65 19.90 0 -1 4 558.34 21.10 -1 1 -4 362.76 15.10 1 -1 4 372.26 17.00 1 -1 4 331.37 15.70 1 -1 4 360.66 15.10 -2 1 -4 16.30 3.80 -2 1 -4 16.80 3.40 2 -1 4 12.90 3.50 2 -1 4 20.70 4.80 -3 1 -4 213.78 10.10 -3 1 -4 221.68 14.20 3 -1 4 206.28 14.20 3 -1 4 209.58 14.30 -4 1 -4 463.95 24.40 4 -1 4 465.45 24.70 4 -1 4 471.95 24.20 -5 1 -4 483.55 27.20 5 -1 4 469.15 25.90 5 -1 4 479.85 27.00 -6 1 -4 80.49 13.40 6 -1 4 104.19 12.90 6 -1 4 86.39 11.60 -7 1 -4 30.40 8.60 7 -1 4 24.30 6.60 7 -1 4 16.10 6.90 -8 1 -4 67.09 15.00 8 -1 4 57.29 12.80 8 -1 4 62.49 11.70 -9 1 -4 7.70 9.90 9 -1 4 19.10 8.00 -10 1 -4 26.00 10.90 10 -1 4 25.80 8.30 10 -1 4 9.60 9.20 12 0 -4 52.29 13.90 12 0 -4 55.09 13.70 -12 0 4 60.09 16.60 11 0 -4 16.30 10.50 11 0 -4 21.00 9.70 -11 0 4 22.70 9.50 10 0 -4 381.36 27.00 10 0 -4 310.67 26.20 -10 0 4 337.97 28.90 9 0 -4 2.70 3.20 9 0 -4 1.10 4.30 -9 0 4 5.00 5.80 8 0 -4 15.80 5.30 8 0 -4 7.90 3.10 8 0 -4 23.00 6.20 -8 0 4 21.40 6.60 7 0 -4 863.51 36.60 7 0 -4 928.01 38.70 7 0 -4 872.11 30.40 -7 0 4 896.71 39.00 6 0 -4 333.67 19.90 6 0 -4 348.07 16.60 6 0 -4 301.67 18.50 -6 0 4 353.76 20.60 5 0 -4 844.42 29.40 5 0 -4 766.42 45.40 5 0 -4 951.80 44.90 -5 0 4 835.42 31.60 4 0 -4 272.37 14.80 4 0 -4 280.77 14.20 4 0 -4 261.97 14.70 -4 0 4 296.27 14.60 3 0 -4 4.20 2.30 3 0 -4 2.40 1.50 3 0 -4 2.30 1.80 -3 0 4 1.30 1.60 2 0 -4 1227.08 36.90 2 0 -4 1188.68 31.60 -2 0 4 1198.28 36.10 -2 0 4 1215.38 31.70 -2 0 4 1272.27 36.70 1 0 -4 1001.60 30.90 1 0 -4 984.80 25.30 1 0 -4 955.00 30.90 -1 0 4 999.50 25.40 -1 0 4 1009.60 31.20 -1 0 4 990.50 30.60 0 0 -4 787.62 26.00 0 0 4 772.42 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64.09 13.40 -7 -7 5 33.30 9.70 6 7 -5 186.88 12.20 6 7 -5 216.98 18.00 6 7 -5 176.48 32.40 -6 -7 5 185.28 19.10 5 7 -5 152.28 14.80 5 7 -5 149.59 15.40 5 7 -5 141.79 8.80 -5 -7 5 140.79 15.80 4 7 -5 492.45 27.40 4 7 -5 516.35 28.00 -4 -7 5 529.35 29.50 3 7 -5 62.09 10.50 3 7 -5 64.09 10.50 -3 -7 5 43.90 9.00 2 7 -5 159.98 13.00 2 7 -5 187.38 15.40 -2 -7 5 145.79 12.90 -2 -7 5 163.78 14.50 1 7 -5 305.27 19.90 -1 -7 5 332.57 20.90 -1 -7 5 322.07 19.30 0 7 -5 227.18 16.80 0 -7 5 265.67 15.90 0 -7 5 220.78 14.60 0 -7 5 249.08 17.70 -1 7 -5 168.08 13.80 1 -7 5 186.28 15.40 1 -7 5 155.38 11.80 1 -7 5 167.98 8.90 1 -7 5 165.68 12.40 -2 7 -5 255.57 17.00 2 -7 5 310.87 14.80 2 -7 5 237.68 18.30 2 -7 5 275.17 15.70 2 -7 5 267.17 15.90 -3 7 -5 817.22 32.60 3 -7 5 697.73 42.30 3 -7 5 827.42 37.60 3 -7 5 752.82 29.90 3 -7 5 831.22 31.30 -4 7 -5 456.45 22.60 4 -7 5 476.45 22.80 4 -7 5 476.15 24.70 4 -7 5 469.15 28.60 -5 7 -5 253.17 19.90 5 -7 5 287.07 17.60 5 -7 5 266.07 19.50 5 -7 5 253.37 21.80 -6 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101.89 9.30 0 -6 5 89.19 5.30 -1 6 -5 30.60 6.40 1 -6 5 20.60 4.80 1 -6 5 20.40 4.30 1 -6 5 33.10 4.80 1 -6 5 23.40 6.20 -2 6 -5 4.30 3.40 2 -6 5 8.20 3.00 2 -6 5 13.70 3.70 2 -6 5 10.60 4.10 2 -6 5 11.30 3.60 -3 6 -5 514.85 24.00 3 -6 5 539.85 24.20 3 -6 5 535.05 24.60 3 -6 5 534.55 28.40 -4 6 -5 1741.43 52.59 4 -6 5 1684.23 62.09 4 -6 5 1786.62 58.09 4 -6 5 1804.72 55.59 -5 6 -5 1.80 2.90 5 -6 5 -4.50 2.60 5 -6 5 2.70 3.00 -6 6 -5 110.39 17.80 -6 6 -5 109.99 7.80 6 -6 5 110.89 11.40 6 -6 5 117.39 15.50 -7 6 -5 320.47 27.30 7 -6 5 328.57 22.00 7 -6 5 279.57 23.60 -8 6 -5 208.38 23.70 8 -6 5 212.78 22.20 8 -6 5 202.78 18.00 -9 6 -5 4.30 7.50 9 -6 5 -4.30 3.50 9 -6 5 0.10 5.80 10 5 -5 35.90 10.90 10 5 -5 30.00 8.60 -10 -5 5 26.20 9.90 9 5 -5 4.80 4.90 9 5 -5 10.30 4.70 9 5 -5 2.90 4.30 -9 -5 5 5.70 5.50 8 5 -5 208.08 20.10 8 5 -5 186.58 15.50 8 5 -5 187.38 16.60 -8 -5 5 186.68 20.10 7 5 -5 151.08 13.70 7 5 -5 142.29 12.90 7 5 -5 110.09 14.70 -7 -5 5 138.79 16.00 6 5 -5 738.33 36.40 6 5 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10 -7 7.50 5.60 -4 -10 7 3.20 4.40 3 10 -7 127.09 16.30 -3 -10 7 156.48 17.50 -3 -10 7 154.78 17.20 2 10 -7 102.29 16.10 -2 -10 7 94.59 15.40 -2 -10 7 104.69 16.60 1 10 -7 68.59 12.70 -1 -10 7 74.59 12.70 -1 -10 7 57.09 10.30 -1 -10 7 67.39 12.70 0 10 -7 51.89 10.80 0 -10 7 87.69 11.10 0 -10 7 73.99 13.60 0 -10 7 71.89 12.10 -1 10 -7 360.16 25.20 1 -10 7 320.67 20.50 1 -10 7 345.77 21.80 1 -10 7 287.77 24.40 -2 10 -7 15.60 6.60 2 -10 7 21.10 6.00 2 -10 7 28.20 7.00 2 -10 7 29.90 5.20 2 -10 7 27.80 8.10 -3 10 -7 -0.20 3.80 3 -10 7 -6.90 3.40 3 -10 7 -0.70 2.60 3 -10 7 2.20 3.50 3 -10 7 -4.20 3.60 -4 10 -7 172.28 21.20 4 -10 7 161.08 14.20 4 -10 7 166.18 20.40 4 -10 7 149.88 14.10 4 -10 7 145.59 13.80 -5 10 -7 42.30 9.50 5 -10 7 34.20 7.50 5 -10 7 32.20 7.40 5 -10 7 20.90 9.00 5 -10 7 28.80 9.80 6 -10 7 -10.80 4.70 6 -10 7 -5.60 2.80 6 -10 7 11.10 6.00 -7 10 -7 1.80 7.50 7 -10 7 9.70 4.30 7 -10 7 7.00 7.00 -9 -9 7 57.39 15.90 8 9 -7 36.60 11.10 -8 -9 7 67.79 15.20 7 9 -7 17.60 8.90 7 9 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267.47 18.40 4 -8 7 265.27 18.30 4 -8 7 278.47 19.00 4 -8 7 255.77 18.70 4 -8 7 292.27 24.20 -5 8 -7 7.10 5.20 5 -8 7 19.20 7.90 5 -8 7 12.90 5.30 -6 8 -7 5.50 4.90 6 -8 7 8.20 5.60 6 -8 7 7.40 4.80 -7 8 -7 -2.80 6.00 7 -8 7 0.20 3.90 7 -8 7 1.20 5.50 -8 8 -7 72.09 17.20 8 -8 7 83.49 16.00 8 -8 7 86.39 14.00 10 7 -7 -18.50 7.50 10 7 -7 12.30 8.20 -10 -7 7 0.80 7.10 9 7 -7 14.40 7.90 9 7 -7 5.30 7.60 9 7 -7 20.10 7.00 -9 -7 7 7.40 5.80 8 7 -7 2.20 5.30 8 7 -7 21.10 7.30 8 7 -7 12.20 9.20 -8 -7 7 17.80 8.30 7 7 -7 177.18 17.60 7 7 -7 170.78 18.40 7 7 -7 155.88 12.00 -7 -7 7 151.28 18.60 6 7 -7 29.10 9.80 6 7 -7 27.00 8.40 -6 -7 7 13.30 6.20 5 7 -7 8.70 5.00 5 7 -7 24.70 6.90 -5 -7 7 6.00 5.90 4 7 -7 -0.70 2.40 4 7 -7 -4.20 2.70 -4 -7 7 4.60 3.70 3 7 -7 7.80 3.40 3 7 -7 3.60 4.20 -3 -7 7 5.80 3.50 -3 -7 7 17.40 5.90 2 7 -7 19.50 6.00 -2 -7 7 7.30 5.00 -2 -7 7 22.60 7.00 -2 -7 7 18.00 6.00 1 7 -7 172.58 15.70 -1 -7 7 172.58 15.20 -1 -7 7 146.89 25.30 -1 -7 7 165.38 15.10 0 7 -7 130.99 13.10 0 -7 7 124.29 12.40 0 -7 7 116.29 12.90 0 -7 7 112.19 7.40 -1 7 -7 106.99 12.00 1 -7 7 114.69 13.00 1 -7 7 118.59 11.80 1 -7 7 113.39 9.10 1 -7 7 117.49 11.40 -2 7 -7 -6.70 2.30 2 -7 7 -3.90 2.80 2 -7 7 2.40 3.10 2 -7 7 0.80 2.30 -3 7 -7 331.37 20.80 3 -7 7 352.06 20.60 3 -7 7 342.67 24.60 3 -7 7 299.17 28.90 -4 7 -7 141.39 13.00 4 -7 7 147.99 16.80 4 -7 7 149.39 14.00 4 -7 7 122.19 13.20 -5 7 -7 3.20 3.90 5 -7 7 -6.30 2.70 -6 7 -7 13.40 8.70 6 -7 7 1.10 4.00 6 -7 7 3.20 5.10 -7 7 -7 64.09 20.20 7 -7 7 64.99 13.90 7 -7 7 65.99 17.90 -8 7 -7 0.10 7.60 8 -7 7 -1.00 7.50 8 -7 7 -2.60 3.60 10 6 -7 81.49 15.40 10 6 -7 114.59 14.80 10 6 -7 77.99 14.60 -10 -6 7 98.99 18.40 9 6 -7 25.60 9.40 9 6 -7 31.70 10.80 -9 -6 7 49.40 13.50 8 6 -7 42.00 8.40 8 6 -7 59.29 13.80 8 6 -7 55.19 11.40 -8 -6 7 35.40 11.10 7 6 -7 89.79 17.00 7 6 -7 124.59 15.50 7 6 -7 110.89 10.80 -7 -6 7 90.79 15.30 6 6 -7 444.66 28.80 6 6 -7 448.86 27.40 5 6 -7 6.30 4.00 5 6 -7 -0.70 2.80 -5 -6 7 3.50 2.80 -5 -6 7 3.50 3.60 4 6 -7 45.20 9.90 4 6 -7 32.20 8.00 -4 -6 7 39.40 4.70 -4 -6 7 26.20 7.40 3 6 -7 -1.50 2.20 -3 -6 7 4.60 3.10 -3 -6 7 0.50 3.10 -3 -6 7 4.00 2.00 2 6 -7 11.30 4.60 -2 -6 7 3.00 2.90 -2 -6 7 10.20 4.70 -2 -6 7 4.10 3.20 1 6 -7 52.59 9.30 -1 -6 7 48.00 8.60 -1 -6 7 53.49 5.00 -1 -6 7 44.80 8.40 -1 -6 7 47.20 8.30 0 6 -7 123.99 12.80 0 -6 7 96.49 10.80 0 -6 7 109.79 8.00 0 -6 7 72.09 9.40 0 -6 7 102.79 11.40 -1 6 -7 233.28 16.90 1 -6 7 220.98 16.30 1 -6 7 223.98 13.20 1 -6 7 225.38 17.30 -2 6 -7 185.08 14.70 2 -6 7 157.28 15.30 2 -6 7 179.08 13.40 2 -6 7 164.38 14.30 -3 6 -7 36.60 7.40 3 -6 7 51.79 9.30 3 -6 7 52.49 9.30 3 -6 7 25.90 8.00 -4 6 -7 82.99 9.20 4 -6 7 69.49 12.80 4 -6 7 75.09 12.50 4 -6 7 80.59 10.60 -5 6 -7 17.80 6.20 5 -6 7 11.40 6.70 5 -6 7 29.20 8.30 -6 6 -7 38.70 11.60 6 -6 7 33.60 10.00 6 -6 7 51.99 9.90 -7 6 -7 -0.60 5.50 7 -6 7 4.90 6.30 7 -6 7 6.30 5.40 -8 6 -7 66.89 15.70 8 -6 7 33.10 11.80 8 -6 7 38.00 10.50 10 5 -7 48.20 9.90 10 5 -7 60.79 11.90 10 5 -7 31.90 10.40 -10 -5 7 60.69 15.80 9 5 -7 84.89 15.40 9 5 -7 133.79 15.70 9 5 -7 83.59 13.70 -9 -5 7 95.69 17.00 8 5 -7 194.38 16.20 8 5 -7 214.08 18.30 8 5 -7 183.78 19.80 -8 -5 7 221.28 21.60 7 5 -7 79.39 14.50 7 5 -7 82.19 13.30 7 5 -7 82.99 11.10 -7 -5 7 78.49 14.50 6 5 -7 101.79 9.50 6 5 -7 97.69 12.60 6 5 -7 102.59 12.90 -6 -5 7 100.69 12.90 5 5 -7 52.79 9.60 5 5 -7 48.00 8.80 -5 -5 7 73.59 12.00 -5 -5 7 54.19 6.60 4 5 -7 144.79 13.90 4 5 -7 142.99 14.20 -4 -5 7 150.78 9.80 -4 -5 7 146.59 13.80 3 5 -7 814.02 35.80 -3 -5 7 793.02 25.90 -3 -5 7 815.32 34.10 2 5 -7 -3.60 2.10 -2 -5 7 -2.50 1.70 -2 -5 7 0.50 1.60 1 5 -7 753.32 32.90 -1 -5 7 747.23 25.00 -1 -5 7 721.93 32.20 -1 -5 7 732.93 31.10 0 5 -7 556.04 26.90 0 -5 7 526.05 25.80 0 -5 7 570.34 22.00 0 -5 7 519.95 26.30 0 -5 7 516.35 25.70 -1 5 -7 2.30 3.10 1 -5 7 -1.60 2.50 1 -5 7 -2.00 1.80 1 -5 7 3.40 2.90 -2 5 -7 99.09 10.80 2 -5 7 107.29 10.80 2 -5 7 120.39 12.40 2 -5 7 106.89 11.40 -3 5 -7 284.87 17.60 3 -5 7 329.17 21.00 3 -5 7 289.47 20.80 3 -5 7 278.57 18.70 -4 5 -7 20.70 8.60 4 -5 7 7.10 4.50 4 -5 7 23.90 6.90 -5 5 -7 597.94 35.20 -5 5 -7 537.25 23.00 5 -5 7 553.34 31.10 5 -5 7 601.94 33.50 -6 5 -7 26.40 9.00 6 -5 7 28.50 8.30 6 -5 7 16.60 7.60 -7 5 -7 -4.20 5.50 7 -5 7 16.80 8.70 7 -5 7 8.60 5.80 -8 5 -7 0.40 7.90 8 -5 7 13.90 8.60 8 -5 7 -0.10 4.40 11 4 -7 26.30 8.90 11 4 -7 15.40 7.70 -11 -4 7 1.50 7.60 10 4 -7 4.60 5.30 10 4 -7 1.10 4.50 10 4 -7 11.00 5.70 -10 -4 7 6.40 6.90 9 4 -7 37.60 9.40 9 4 -7 32.60 8.10 9 4 -7 60.89 11.00 -9 -4 7 58.99 13.00 8 4 -7 43.30 8.70 8 4 -7 40.50 9.30 8 4 -7 51.29 11.60 -8 -4 7 39.40 10.10 7 4 -7 34.60 9.40 7 4 -7 48.70 9.20 7 4 -7 51.89 10.60 -7 -4 7 37.90 9.80 6 4 -7 316.57 22.30 6 4 -7 283.27 17.10 6 4 -7 302.47 21.10 -6 -4 7 294.47 21.10 5 4 -7 5.80 4.40 5 4 -7 1.90 3.50 -5 -4 7 14.00 5.30 4 4 -7 -0.90 2.10 4 4 -7 2.40 3.30 -4 -4 7 -1.70 2.50 -4 -4 7 1.80 2.40 3 4 -7 51.09 9.40 -3 -4 7 56.69 6.20 -3 -4 7 61.59 10.20 -3 -4 7 48.00 7.80 2 4 -7 2.00 2.70 -2 -4 7 6.70 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213.68 19.60 6 7 -8 209.58 20.80 -6 -7 8 213.28 19.80 -6 -7 8 185.38 12.30 5 7 -8 428.06 29.00 5 7 -8 493.85 30.50 -5 -7 8 488.05 30.50 -5 -7 8 455.95 17.30 4 7 -8 12.30 7.20 -4 -7 8 8.10 5.00 -4 -7 8 16.30 6.50 3 7 -8 58.59 11.50 -3 -7 8 52.29 11.30 -3 -7 8 54.29 10.20 2 7 -8 136.39 14.50 -2 -7 8 162.48 15.20 -2 -7 8 136.79 14.00 1 7 -8 58.79 11.00 -1 -7 8 43.10 9.10 -1 -7 8 62.09 5.50 -1 -7 8 57.89 10.00 -1 -7 8 47.10 8.90 0 7 -8 170.38 16.20 0 -7 8 176.88 14.70 0 -7 8 142.29 14.00 0 -7 8 161.38 10.00 0 -7 8 149.19 14.90 -1 7 -8 26.70 7.20 1 -7 8 40.50 9.30 1 -7 8 42.40 9.40 1 -7 8 16.70 7.80 1 -7 8 24.50 5.80 -2 7 -8 32.90 8.40 2 -7 8 27.30 7.90 2 -7 8 32.20 7.80 2 -7 8 31.20 7.50 2 -7 8 25.70 5.90 -3 7 -8 18.10 7.40 3 -7 8 18.40 6.60 3 -7 8 24.00 6.20 3 -7 8 27.10 6.70 -4 7 -8 2.50 3.90 4 -7 8 0.10 4.60 4 -7 8 11.80 5.10 4 -7 8 4.70 3.10 -5 7 -8 0.00 4.30 -5 7 -8 -4.50 3.40 5 -7 8 0.00 3.50 5 -7 8 0.00 4.70 -6 7 -8 21.80 9.00 6 -7 8 22.20 7.90 6 -7 8 24.10 7.60 -7 7 -8 -8.30 5.70 7 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-9 402.36 31.30 -4 9 9 367.06 30.00 3 -9 -9 200.88 22.10 -3 9 9 220.38 23.00 2 -9 -9 6.10 6.60 -2 9 9 -5.90 4.80 1 -9 -9 208.68 24.10 -1 9 9 270.57 25.00 0 -9 -9 235.28 38.40 0 9 9 298.17 26.50 -1 -9 -9 7.90 6.60 1 9 9 28.10 9.10 -2 -9 -9 75.89 16.40 2 9 9 88.59 17.40 7 -10 -9 -6.00 5.80 -7 10 9 4.60 6.30 6 -10 -9 56.89 13.60 -6 10 9 32.60 10.80 5 -10 -9 25.10 10.60 -5 10 9 31.30 12.40 4 -10 -9 415.76 33.30 -4 10 9 386.56 33.90 3 -10 -9 49.90 13.10 -3 10 9 52.39 13.50 2 -10 -9 21.90 10.30 -2 10 9 47.80 14.30 1 -10 -9 27.50 9.10 -1 10 9 31.60 11.60 0 -10 -9 764.42 46.80 0 10 9 771.92 45.20 -6 11 9 107.49 18.30 5 -11 -9 1.60 6.40 -5 11 9 7.40 6.80 4 -11 -9 47.10 12.80 -4 11 9 32.70 12.70 3 -11 -9 17.70 9.70 -3 11 9 22.20 10.60 2 -11 -9 44.20 12.50 -2 11 9 53.29 12.20 3 13 -10 5.30 8.80 -3 -13 10 5.10 7.70 -3 -13 10 3.60 5.70 2 13 -10 22.60 10.70 -2 -13 10 23.40 10.20 -2 -13 10 49.80 12.60 1 13 -10 -8.20 5.80 -1 -13 10 2.30 6.90 -1 -13 10 -3.40 4.90 0 13 -10 89.79 18.90 0 -13 10 77.89 14.90 0 -13 10 78.59 16.30 -1 13 -10 -13.70 6.40 1 -13 10 21.40 9.90 1 -13 10 8.60 6.10 5 12 -10 20.10 9.90 -5 -12 10 41.90 13.60 -5 -12 10 24.30 10.20 4 12 -10 -1.10 8.20 -4 -12 10 2.70 7.00 -4 -12 10 7.40 7.50 3 12 -10 22.90 10.50 -3 -12 10 39.80 11.90 -3 -12 10 46.90 14.40 2 12 -10 43.80 11.30 -2 -12 10 28.90 9.50 -2 -12 10 26.20 10.30 1 12 -10 7.10 7.50 -1 -12 10 21.40 8.00 -1 -12 10 14.80 9.50 0 12 -10 15.30 8.20 0 -12 10 -2.00 4.60 0 -12 10 12.10 6.70 -1 12 -10 -9.80 12.50 1 -12 10 3.90 7.30 1 -12 10 8.70 7.00 2 -12 10 53.59 12.10 2 -12 10 41.90 13.20 3 -12 10 7.80 5.50 3 -12 10 23.40 10.40 6 11 -10 2.30 5.00 -6 -11 10 -3.80 7.10 -6 -11 10 21.60 8.70 5 11 -10 216.38 23.80 -5 -11 10 202.88 23.50 -5 -11 10 245.28 25.00 4 11 -10 66.39 15.50 -4 -11 10 99.29 16.60 3 11 -10 255.57 28.20 -3 -11 10 276.37 25.10 -3 -11 10 226.58 23.20 2 11 -10 2.60 7.40 -2 -11 10 9.20 7.30 -2 -11 10 2.60 4.90 1 11 -10 259.77 25.20 -1 -11 10 213.48 23.30 -1 -11 10 272.47 23.60 0 11 -10 28.40 10.10 0 -11 10 25.60 8.30 0 -11 10 9.20 7.30 -1 11 -10 91.09 16.40 1 -11 10 97.79 16.60 1 -11 10 76.89 15.80 -2 11 -10 1.70 6.70 2 -11 10 2.00 3.70 2 -11 10 7.60 7.20 -3 11 -10 -0.60 6.40 3 -11 10 6.00 5.30 3 -11 10 -2.60 6.40 -4 11 -10 -4.10 6.70 4 -11 10 17.50 9.90 4 -11 10 8.40 5.80 7 10 -10 13.10 10.50 -7 -10 10 19.90 9.30 -7 -10 10 11.70 8.00 6 10 -10 105.09 19.30 -6 -10 10 66.09 16.00 -6 -10 10 72.29 15.50 5 10 -10 28.50 10.70 -5 -10 10 35.10 11.40 -5 -10 10 22.90 9.60 4 10 -10 176.88 20.50 -4 -10 10 195.48 22.40 -4 -10 10 203.08 21.10 3 10 -10 9.50 7.50 -3 -10 10 1.30 4.40 -3 -10 10 1.80 4.80 2 10 -10 7.30 6.10 -2 -10 10 3.70 4.90 -2 -10 10 3.80 5.00 1 10 -10 8.00 7.80 -1 -10 10 2.90 5.20 -1 -10 10 -0.90 4.10 0 10 -10 486.05 33.50 0 -10 10 511.75 32.30 0 -10 10 525.85 34.50 -1 10 -10 186.28 20.40 1 -10 10 184.58 18.40 1 -10 10 150.78 18.50 -2 10 -10 22.90 9.90 2 -10 10 17.60 6.20 2 -10 10 31.00 9.70 -3 10 -10 238.58 22.20 3 -10 10 242.18 40.20 3 -10 10 262.07 22.40 3 -10 10 241.68 18.80 -4 10 -10 130.19 16.40 4 -10 10 153.38 19.80 4 -10 10 150.28 15.90 4 -10 10 165.78 17.10 5 -10 10 39.70 9.40 5 -10 10 19.90 9.90 8 9 -10 23.30 10.70 -8 -9 10 17.80 9.80 -8 -9 10 39.60 11.90 -7 -9 10 4.40 6.00 6 9 -10 52.79 13.00 -6 -9 10 48.50 12.20 5 9 -10 13.10 7.40 -5 -9 10 16.00 7.50 -5 -9 10 1.00 5.10 4 9 -10 19.90 8.10 -4 -9 10 4.30 5.50 -4 -9 10 14.10 6.90 3 9 -10 -9.40 3.70 -3 -9 10 6.00 5.40 -3 -9 10 -1.30 4.60 2 9 -10 37.60 9.10 -2 -9 10 69.29 13.40 -2 -9 10 60.39 11.40 1 9 -10 264.17 23.70 -1 -9 10 270.07 22.80 -1 -9 10 262.47 22.90 0 9 -10 -7.30 3.50 0 -9 10 0.80 3.20 0 -9 10 3.70 4.70 -1 9 -10 19.60 8.20 1 -9 10 13.60 6.70 1 -9 10 12.70 7.00 1 -9 10 15.30 6.00 -2 9 -10 78.49 14.80 2 -9 10 86.89 10.90 2 -9 10 86.69 15.10 2 -9 10 91.19 14.40 -3 9 -10 255.57 22.30 3 -9 10 270.77 19.60 3 -9 10 265.37 25.00 3 -9 10 301.97 24.20 -4 9 -10 93.79 14.30 4 -9 10 85.59 13.90 4 -9 10 110.69 15.20 -5 9 -10 12.90 8.10 5 -9 10 4.00 5.00 5 -9 10 10.80 8.50 9 8 -10 21.10 11.50 9 8 -10 4.70 8.80 -9 -8 10 13.60 9.60 8 8 -10 3.60 7.60 8 8 -10 0.10 7.50 -8 -8 10 7.30 6.80 -8 -8 10 29.60 9.50 7 8 -10 88.59 16.00 -7 -8 10 132.89 21.30 -7 -8 10 101.69 17.00 6 8 -10 11.80 7.90 -6 -8 10 3.80 5.70 -6 -8 10 20.30 8.80 5 8 -10 151.58 18.80 -5 -8 10 166.18 18.10 -5 -8 10 176.38 20.30 4 8 -10 15.70 7.40 -4 -8 10 15.60 6.80 -4 -8 10 12.30 7.00 3 8 -10 8.10 7.00 -3 -8 10 28.60 8.80 -3 -8 10 23.20 8.00 -2 -8 10 8.00 5.60 -2 -8 10 10.50 5.50 1 8 -10 25.10 8.80 -1 -8 10 20.70 6.80 -1 -8 10 16.40 4.30 -1 -8 10 6.90 5.90 0 8 -10 34.50 9.80 0 -8 10 15.30 5.70 0 -8 10 36.90 6.80 0 -8 10 41.30 9.90 -1 8 -10 5.80 5.80 1 -8 10 5.80 4.60 1 -8 10 -3.00 4.80 1 -8 10 14.30 4.70 -2 8 -10 8.60 6.40 2 -8 10 18.90 7.10 2 -8 10 14.90 5.60 2 -8 10 12.70 5.80 -3 8 -10 61.59 11.90 3 -8 10 57.59 13.40 3 -8 10 81.39 14.40 3 -8 10 61.09 11.60 -4 8 -10 6.60 6.80 4 -8 10 4.50 4.30 4 -8 10 13.10 7.60 -5 8 -10 25.60 9.90 5 -8 10 24.70 8.20 5 -8 10 55.39 12.70 -6 8 -10 32.40 14.20 6 -8 10 32.20 11.40 6 -8 10 34.90 9.00 9 7 -10 12.40 8.10 9 7 -10 11.90 8.30 -9 -7 10 21.80 9.00 8 7 -10 89.59 17.60 8 7 -10 67.99 15.30 -8 -7 10 77.69 15.90 -8 -7 10 56.59 18.70 7 7 -10 5.20 7.20 -7 -7 10 10.10 7.10 -7 -7 10 4.20 6.40 -7 -7 10 12.50 8.90 6 7 -10 77.49 15.30 -6 -7 10 74.39 9.40 -6 -7 10 95.19 15.60 -6 -7 10 93.49 17.40 5 7 -10 14.30 7.60 -5 -7 10 0.20 6.20 -5 -7 10 21.90 7.00 -5 -7 10 22.00 5.20 4 7 -10 21.80 7.60 -4 -7 10 31.20 5.10 -4 -7 10 25.10 7.90 -4 -7 10 45.20 10.30 3 7 -10 9.00 5.30 -3 -7 10 6.60 5.60 -3 -7 10 8.20 3.30 -3 -7 10 14.30 6.80 2 7 -10 33.60 8.60 -2 -7 10 20.70 6.70 -2 -7 10 22.60 7.00 -2 -7 10 19.60 4.60 1 7 -10 16.80 6.70 -1 -7 10 17.60 6.10 -1 -7 10 15.50 6.00 0 7 -10 217.58 19.90 0 -7 10 216.38 20.00 0 -7 10 199.28 14.20 -1 7 -10 9.40 5.50 1 -7 10 3.70 4.60 1 -7 10 2.20 3.90 1 -7 10 -0.20 3.90 -2 7 -10 29.60 13.60 2 -7 10 26.40 8.20 2 -7 10 10.10 6.20 2 -7 10 16.90 7.40 -3 7 -10 25.50 8.50 3 -7 10 22.80 8.30 3 -7 10 13.80 6.80 -4 7 -10 10.00 5.70 4 -7 10 13.70 7.30 4 -7 10 9.90 6.90 -5 7 -10 62.09 14.20 5 -7 10 49.40 11.30 5 -7 10 76.69 14.50 -6 7 -10 29.80 11.30 6 -7 10 8.50 5.90 6 -7 10 15.90 8.90 10 6 -10 49.30 14.10 10 6 -10 76.99 15.50 -10 -6 10 44.20 13.40 9 6 -10 131.79 21.20 9 6 -10 141.19 20.80 -9 -6 10 156.38 18.70 -9 -6 10 94.09 17.70 8 6 -10 141.09 21.20 8 6 -10 130.59 20.00 -8 -6 10 101.29 19.70 -8 -6 10 113.99 13.90 -8 -6 10 115.39 17.70 7 6 -10 128.59 16.60 -7 -6 10 135.99 13.30 -7 -6 10 119.89 20.20 -7 -6 10 135.19 16.70 6 6 -10 143.19 17.40 -6 -6 10 147.09 16.00 -6 -6 10 139.59 12.30 -6 -6 10 142.19 17.70 5 6 -10 48.60 11.00 -5 -6 10 64.29 10.00 -5 -6 10 59.99 10.80 -5 -6 10 39.00 9.20 4 6 -10 191.58 19.20 -4 -6 10 174.48 16.20 -4 -6 10 180.08 12.50 -4 -6 10 193.28 18.90 3 6 -10 29.40 8.60 -3 -6 10 40.30 8.90 -3 -6 10 41.80 7.10 -3 -6 10 53.59 10.90 2 6 -10 29.10 8.30 -2 -6 10 23.50 8.40 -2 -6 10 31.80 7.40 -2 -6 10 32.90 6.20 1 6 -10 249.88 30.70 -1 -6 10 262.47 21.30 -1 -6 10 263.67 19.70 -1 -6 10 242.28 15.50 0 6 -10 34.60 8.20 0 -6 10 50.19 8.70 0 -6 10 41.20 10.70 0 -6 10 55.39 10.50 -1 6 -10 6.50 5.10 1 -6 10 4.40 7.10 1 -6 10 6.60 4.70 1 -6 10 -3.10 3.10 -2 6 -10 -6.20 3.20 2 -6 10 -3.60 3.10 2 -6 10 4.70 4.30 2 -6 10 -1.80 3.20 -3 6 -10 295.37 21.40 3 -6 10 298.47 24.50 3 -6 10 310.77 22.60 -4 6 -10 57.69 10.30 -4 6 -10 47.90 11.30 4 -6 10 76.99 14.20 4 -6 10 64.69 13.20 -5 6 -10 38.40 11.30 5 -6 10 50.39 12.60 5 -6 10 25.40 8.70 -6 6 -10 18.60 9.10 6 -6 10 23.00 9.90 6 -6 10 39.60 11.00 10 5 -10 8.30 7.10 10 5 -10 2.30 5.60 -10 -5 10 12.50 7.50 -10 -5 10 -2.60 6.50 9 5 -10 1.60 5.80 9 5 -10 17.40 8.40 -9 -5 10 17.90 8.20 -9 -5 10 16.40 7.10 8 5 -10 32.70 9.60 -8 -5 10 38.90 10.40 -8 -5 10 20.70 7.00 -8 -5 10 22.60 9.30 7 5 -10 41.60 10.70 -7 -5 10 60.49 11.70 -7 -5 10 90.19 16.60 -7 -5 10 49.80 9.50 6 5 -10 79.49 14.70 -6 -5 10 67.49 11.60 -6 -5 10 55.49 11.20 -6 -5 10 87.89 10.90 5 5 -10 18.20 7.10 -5 -5 10 30.00 7.80 -5 -5 10 11.90 4.80 -5 -5 10 15.70 5.80 4 5 -10 66.09 12.60 -4 -5 10 52.19 10.30 -4 -5 10 71.59 8.90 -4 -5 10 68.49 10.30 3 5 -10 3.20 3.80 -3 -5 10 5.00 3.30 -3 -5 10 0.40 2.80 -3 -5 10 2.40 5.40 2 5 -10 215.48 18.80 -2 -5 10 175.68 13.90 -2 -5 10 195.08 15.70 -2 -5 10 210.88 19.00 1 5 -10 144.79 15.90 -1 -5 10 171.48 13.50 -1 -5 10 166.28 17.10 -1 -5 10 156.68 14.10 0 5 -10 7.10 5.10 0 -5 10 -2.30 2.90 0 -5 10 8.40 4.10 0 -5 10 5.70 4.20 -1 5 -10 62.09 11.20 1 -5 10 50.49 10.30 1 -5 10 44.10 9.40 1 -5 10 39.60 8.70 -2 5 -10 101.09 12.70 2 -5 10 99.39 14.70 2 -5 10 136.89 16.00 2 -5 10 84.89 11.30 -3 5 -10 0.30 4.00 -3 5 -10 6.30 4.70 3 -5 10 8.80 6.00 3 -5 10 9.10 4.50 -4 5 -10 451.35 30.80 -4 5 -10 466.55 25.60 4 -5 10 494.15 32.00 4 -5 10 466.65 30.80 -5 5 -10 16.40 8.20 5 -5 10 2.30 5.60 5 -5 10 -1.20 5.80 -6 5 -10 -11.50 6.00 6 -5 10 3.50 5.70 6 -5 10 -2.90 6.90 10 4 -10 5.20 5.70 10 4 -10 14.60 8.10 -10 -4 10 -4.40 5.50 9 4 -10 61.39 12.60 -9 -4 10 50.99 11.50 -9 -4 10 44.80 12.50 8 4 -10 4.50 6.00 -8 -4 10 0.80 4.60 -8 -4 10 -5.00 6.40 -8 -4 10 2.80 4.00 7 4 -10 350.56 26.30 -7 -4 10 343.17 23.30 -7 -4 10 297.67 21.20 6 4 -10 5.70 5.00 -6 -4 10 4.90 3.80 -6 -4 10 7.90 10.00 -6 -4 10 2.00 3.70 5 4 -10 26.60 9.60 -5 -4 10 29.70 7.00 -5 -4 10 10.80 5.10 -5 -4 10 30.00 7.60 4 4 -10 32.10 9.70 -4 -4 10 33.20 7.80 -4 -4 10 26.80 6.10 -4 -4 10 21.10 7.50 3 4 -10 0.50 3.70 -3 -4 10 2.10 4.40 -3 -4 10 1.90 2.60 -3 -4 10 1.30 2.90 2 4 -10 176.58 16.70 -2 -4 10 163.28 13.80 -2 -4 10 157.68 13.30 -2 -4 10 216.68 23.50 1 4 -10 116.09 13.90 -1 -4 10 137.29 15.00 -1 -4 10 125.99 11.90 -1 -4 10 120.09 11.80 0 4 -10 2.70 3.90 0 -4 10 2.00 3.70 0 -4 10 -1.70 3.30 0 -4 10 -1.60 3.20 -1 4 -10 126.19 13.90 1 -4 10 118.79 14.90 1 -4 10 101.69 12.40 1 -4 10 140.69 13.70 -2 4 -10 1.90 3.90 2 -4 10 1.30 3.10 2 -4 10 3.20 3.70 -3 4 -10 80.59 12.00 -3 4 -10 70.19 13.00 3 -4 10 44.90 9.80 3 -4 10 104.19 16.70 -4 4 -10 28.40 7.00 -4 4 -10 24.30 8.70 4 -4 10 36.30 10.40 4 -4 10 19.90 7.40 -5 4 -10 47.00 11.80 5 -4 10 31.20 9.60 5 -4 10 34.70 11.30 -6 4 -10 -3.40 7.60 6 -4 10 3.30 6.90 6 -4 10 7.90 5.60 -11 -3 10 19.20 9.70 10 3 -10 93.89 16.20 -10 -3 10 91.59 15.60 9 3 -10 481.15 31.60 -9 -3 10 451.55 30.50 -9 -3 10 502.45 31.50 8 3 -10 11.90 6.30 -8 -3 10 13.80 6.60 -8 -3 10 19.90 7.70 7 3 -10 11.50 6.00 -7 -3 10 4.40 5.50 -7 -3 10 3.90 5.90 -7 -3 10 8.30 4.90 6 3 -10 11.50 6.60 -6 -3 10 25.60 6.80 -6 -3 10 30.50 6.90 -6 -3 10 21.00 7.10 5 3 -10 633.34 36.70 -5 -3 10 638.54 28.90 -5 -3 10 668.93 31.00 -5 -3 10 624.84 34.70 4 3 -10 296.17 22.90 -4 -3 10 283.17 22.10 -4 -3 10 279.47 18.70 -4 -3 10 261.47 16.90 3 3 -10 90.39 14.30 -3 -3 10 97.39 12.70 -3 -3 10 78.09 10.00 -3 -3 10 89.29 9.70 2 3 -10 186.08 17.40 -2 -3 10 146.19 15.80 -2 -3 10 167.38 14.40 -2 -3 10 165.78 12.70 1 3 -10 294.47 21.90 -1 -3 10 311.27 22.70 -1 -3 10 302.87 19.70 -1 -3 10 313.87 18.00 0 3 -10 298.77 21.30 0 -3 10 286.17 18.00 0 -3 10 279.07 21.80 0 -3 10 268.07 19.40 -1 3 -10 -2.00 3.10 1 -3 10 1.80 3.70 1 -3 10 0.20 3.60 -2 3 -10 3.30 4.10 -2 3 -10 9.70 4.30 2 -3 10 -1.60 6.90 2 -3 10 -8.40 3.10 -3 3 -10 27.60 7.30 -3 3 -10 21.80 6.50 3 -3 10 15.20 6.70 3 -3 10 18.70 7.20 -4 3 -10 188.08 18.10 -4 3 -10 207.58 16.30 4 -3 10 207.38 20.80 4 -3 10 207.78 21.50 -5 3 -10 90.89 15.90 5 -3 10 77.19 15.40 5 -3 10 67.69 12.90 -6 3 -10 -9.00 4.50 6 -3 10 -2.70 5.90 6 -3 10 -13.40 6.10 11 2 -10 -11.00 6.50 -11 -2 10 -6.10 8.30 10 2 -10 55.29 11.10 -10 -2 10 37.00 9.80 9 2 -10 332.87 25.60 -9 -2 10 296.77 23.20 8 2 -10 4.60 4.50 -8 -2 10 -2.60 4.50 -8 -2 10 -4.70 3.40 7 2 -10 2.30 5.40 -7 -2 10 1.20 3.90 -7 -2 10 6.70 4.50 -7 -2 10 10.60 6.20 6 2 -10 82.69 22.80 -6 -2 10 86.49 9.50 -6 -2 10 59.19 10.50 -6 -2 10 61.29 11.00 5 2 -10 229.78 19.80 -5 -2 10 213.78 18.50 -5 -2 10 206.68 17.10 -5 -2 10 229.78 14.70 4 2 -10 498.25 30.30 -4 -2 10 505.65 22.40 -4 -2 10 569.64 28.30 -4 -2 10 535.85 30.70 3 2 -10 700.73 35.70 -3 -2 10 749.92 36.30 -3 -2 10 706.13 26.60 -3 -2 10 681.83 32.40 2 2 -10 9.10 4.80 -2 -2 10 1.40 2.70 -2 -2 10 3.00 3.20 -2 -2 10 3.50 4.00 1 2 -10 245.88 19.80 -1 -2 10 259.07 18.70 -1 -2 10 221.78 14.20 -1 -2 10 244.98 20.20 0 2 -10 670.63 33.50 0 -2 10 677.93 35.20 0 -2 10 627.14 32.10 -1 2 -10 16.20 5.70 -1 2 -10 21.60 6.80 1 -2 10 24.30 7.20 1 -2 10 28.50 7.90 -2 2 -10 36.50 8.30 -2 2 -10 46.20 8.60 2 -2 10 32.20 8.70 2 -2 10 40.70 10.50 -3 2 -10 -0.20 3.60 -3 2 -10 10.20 4.70 3 -2 10 6.60 5.30 3 -2 10 0.30 3.60 -4 2 -10 8.80 6.30 -4 2 -10 15.90 5.80 4 -2 10 16.10 7.80 4 -2 10 11.20 7.10 -5 2 -10 46.80 11.90 5 -2 10 44.00 11.20 5 -2 10 30.00 11.20 -6 2 -10 0.70 6.80 6 -2 10 2.60 4.70 6 -2 10 16.00 7.90 11 1 -10 -8.40 6.80 11 1 -10 13.80 6.80 -11 -1 10 -4.30 7.00 10 1 -10 155.58 17.70 -10 -1 10 176.98 19.00 9 1 -10 -5.80 4.70 -9 -1 10 11.10 6.50 8 1 -10 34.70 8.80 -8 -1 10 51.59 9.70 -8 -1 10 31.90 8.30 7 1 -10 132.19 16.10 -7 -1 10 131.29 12.70 -7 -1 10 120.09 19.50 -7 -1 10 142.39 16.90 6 1 -10 398.56 36.00 -6 -1 10 446.86 22.40 -6 -1 10 455.85 27.90 -6 -1 10 505.25 28.50 5 1 -10 472.45 29.60 -5 -1 10 496.75 29.10 -5 -1 10 487.55 27.90 -5 -1 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402.46 22.80 -3 -4 12 381.86 28.80 2 4 -12 288.47 23.80 -2 -4 12 243.08 19.40 -2 -4 12 247.68 17.60 -2 -4 12 229.38 21.90 1 4 -12 -2.10 3.80 -1 -4 12 9.10 4.90 -1 -4 12 -3.30 3.20 -1 -4 12 -2.80 4.00 0 4 -12 1.10 4.50 0 -4 12 -1.70 3.70 0 -4 12 8.90 4.80 0 -4 12 10.70 4.60 -1 4 -12 49.70 11.40 1 -4 12 56.69 13.40 1 -4 12 39.50 10.50 -2 4 -12 71.79 12.20 -2 4 -12 69.49 12.10 2 -4 12 66.29 14.90 2 -4 12 63.29 12.80 -3 4 -12 2.80 6.70 -3 4 -12 7.40 5.60 3 -4 12 10.60 7.80 3 -4 12 13.50 7.70 -4 4 -12 53.59 11.80 -4 4 -12 29.10 9.10 4 -4 12 28.00 10.80 4 -4 12 37.30 13.80 10 3 -12 11.30 8.40 -10 -3 12 21.00 8.40 -10 -3 12 2.40 6.50 9 3 -12 10.20 6.30 -9 -3 12 18.20 8.70 -9 -3 12 11.80 7.70 8 3 -12 4.40 5.20 -8 -3 12 17.50 8.00 -8 -3 12 17.50 6.80 7 3 -12 159.48 18.80 -7 -3 12 184.68 18.00 -7 -3 12 135.29 14.10 6 3 -12 12.00 6.40 -6 -3 12 -3.40 5.80 -6 -3 12 10.20 5.20 -6 -3 12 3.90 10.00 5 3 -12 3.10 3.60 -5 -3 12 3.10 4.30 -5 -3 12 5.00 4.80 -5 -3 12 6.00 4.10 4 3 -12 43.70 10.10 -4 -3 12 46.60 10.50 -4 -3 12 60.09 8.70 -4 -3 12 52.19 9.50 3 3 -12 20.40 8.20 -3 -3 12 14.10 6.60 -3 -3 12 19.20 5.00 -3 -3 12 14.20 6.20 2 3 -12 189.88 19.50 -2 -3 12 217.48 15.20 -2 -3 12 189.28 20.10 -2 -3 12 204.38 17.70 1 3 -12 5.20 5.90 -1 -3 12 6.10 5.30 -1 -3 12 7.20 8.80 -1 -3 12 11.90 5.00 0 3 -12 10.00 6.60 0 -3 12 10.80 6.00 0 -3 12 11.50 5.90 -1 3 -12 6.20 5.40 -1 3 -12 3.90 4.30 1 -3 12 5.10 5.00 -2 3 -12 11.00 6.60 -2 3 -12 8.80 6.10 2 -3 12 13.40 6.90 2 -3 12 6.50 5.60 -3 3 -12 14.00 7.60 -3 3 -12 -1.50 4.70 3 -3 12 6.10 6.00 3 -3 12 10.70 7.10 -4 3 -12 5.70 6.20 -4 3 -12 11.70 8.10 4 -3 12 2.80 6.10 4 -3 12 -1.60 4.60 10 2 -12 14.90 8.10 -10 -2 12 10.40 7.60 -10 -2 12 17.40 8.30 9 2 -12 7.90 6.90 -9 -2 12 11.60 7.40 -9 -2 12 8.60 7.40 8 2 -12 19.30 6.80 -8 -2 12 21.90 6.40 -8 -2 12 28.90 8.20 7 2 -12 9.60 5.10 -7 -2 12 5.70 5.00 -7 -2 12 0.90 4.60 6 2 -12 15.70 7.80 -6 -2 12 12.10 5.80 -6 -2 12 2.00 5.10 -6 -2 12 20.20 5.70 5 2 -12 6.80 5.20 -5 -2 12 8.00 5.50 -5 -2 12 9.40 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25.20 9 -3 -13 43.80 12.00 -9 3 13 34.70 11.50 8 -3 -13 183.28 21.70 -8 3 13 119.79 21.10 -7 3 13 11.80 12.00 6 -3 -13 55.69 13.60 -6 3 13 47.00 12.70 5 -3 -13 35.70 10.50 -5 3 13 38.00 10.80 4 -3 -13 97.79 17.50 -4 3 13 113.09 18.00 3 -3 -13 8.20 5.70 -3 3 13 9.60 7.30 2 -3 -13 -4.10 5.30 -2 3 13 -0.40 6.10 1 -3 -13 74.09 16.10 -1 3 13 42.60 13.00 0 -3 -13 49.20 12.10 0 3 13 59.69 13.90 -1 -3 -13 -4.30 6.70 1 3 13 5.50 7.20 -2 -3 -13 55.19 13.10 2 3 13 43.70 12.80 8 -4 -13 2.10 5.90 -8 4 13 18.60 9.30 7 -4 -13 -1.40 4.50 -7 4 13 12.40 8.90 6 -4 -13 -2.80 5.00 -6 4 13 0.30 7.10 5 -4 -13 349.17 45.00 -5 4 13 297.37 34.10 4 -4 -13 63.59 14.90 -4 4 13 72.79 15.20 3 -4 -13 -6.50 3.40 -3 4 13 -0.10 8.60 2 -4 -13 -0.30 7.60 -2 4 13 6.60 8.90 -1 4 13 2.70 7.90 0 -4 -13 369.16 29.70 0 4 13 342.17 30.50 -1 -4 -13 -4.10 6.60 1 4 13 4.90 9.30 8 -5 -13 -1.20 5.90 -8 5 13 14.00 8.00 7 -5 -13 35.50 12.60 -7 5 13 46.00 14.00 6 -5 -13 879.81 50.89 -6 5 13 939.11 53.59 5 -5 -13 20.80 8.80 -5 5 13 24.50 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8.40 -4 -8 14 -2.40 5.70 3 8 -14 168.28 21.60 -3 -8 14 132.39 20.40 -3 -8 14 131.69 16.50 2 8 -14 11.10 8.50 -2 -8 14 25.20 8.60 -2 -8 14 7.60 8.80 1 8 -14 297.27 28.60 -1 -8 14 337.37 36.80 -1 -8 14 311.07 25.80 0 8 -14 0.50 9.10 0 -8 14 25.00 9.40 0 -8 14 7.20 8.10 -1 8 -14 308.07 27.90 1 -8 14 287.67 26.60 1 -8 14 342.37 29.50 1 -8 14 320.27 27.20 6 7 -14 0.00 7.10 -6 -7 14 -7.10 8.50 -6 -7 14 2.10 6.70 5 7 -14 26.30 11.20 -5 -7 14 56.89 12.00 -5 -7 14 67.79 16.10 4 7 -14 -2.40 6.50 -4 -7 14 -1.70 5.60 -4 -7 14 4.30 8.80 3 7 -14 98.49 19.10 -3 -7 14 81.39 16.20 -3 -7 14 49.80 12.90 -3 -7 14 72.79 14.20 2 7 -14 7.90 7.00 -2 -7 14 -12.60 4.80 -2 -7 14 -0.80 6.00 -2 -7 14 5.30 7.70 1 7 -14 14.40 9.10 -1 -7 14 -2.20 6.30 -1 -7 14 -2.70 6.50 -1 -7 14 6.30 6.80 0 7 -14 9.10 7.90 0 -7 14 9.90 7.80 0 -7 14 20.00 7.20 0 -7 14 -0.60 5.60 -1 7 -14 24.80 9.80 1 -7 14 10.40 8.00 1 -7 14 -3.20 7.90 1 -7 14 24.30 11.00 7 6 -14 75.99 16.30 -7 -6 14 60.39 12.90 6 6 -14 86.29 18.40 -6 -6 14 65.09 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10.70 3 5 -14 33.20 9.80 -3 -5 14 28.80 8.00 -3 -5 14 26.40 8.10 -3 -5 14 22.50 10.00 2 5 -14 -2.40 6.80 -2 -5 14 -0.20 5.80 -2 -5 14 -2.80 5.80 -2 -5 14 14.10 7.20 1 5 -14 104.39 18.50 -1 -5 14 129.79 16.30 -1 -5 14 120.49 20.20 -1 -5 14 110.49 14.30 0 5 -14 12.90 5.50 0 -5 14 9.20 7.40 -1 5 -14 15.40 8.10 -1 5 -14 20.40 8.40 1 -5 14 17.30 8.50 1 -5 14 4.50 7.70 -2 5 -14 45.10 12.60 -2 5 -14 25.60 10.50 2 -5 14 30.00 14.70 2 -5 14 12.10 8.90 8 4 -14 125.29 21.10 -8 -4 14 119.59 18.20 7 4 -14 24.30 12.50 -7 -4 14 15.90 8.10 -7 -4 14 -1.80 7.20 6 4 -14 106.89 19.40 -6 -4 14 102.79 13.30 -6 -4 14 115.09 17.30 5 4 -14 66.89 15.90 -5 -4 14 65.39 12.30 -5 -4 14 58.39 15.30 -5 -4 14 79.99 11.90 4 4 -14 659.33 42.10 -4 -4 14 636.04 41.10 -4 -4 14 617.74 29.70 -4 -4 14 639.34 35.20 3 4 -14 297.27 28.30 -3 -4 14 326.37 28.30 -3 -4 14 288.67 19.30 -3 -4 14 304.57 23.60 2 4 -14 37.90 11.30 -2 -4 14 42.50 9.70 -2 -4 14 26.80 10.40 -2 -4 14 37.80 8.10 1 4 -14 9.90 6.30 -1 -4 14 17.00 7.10 -1 -4 14 7.90 7.00 0 4 -14 41.50 12.00 0 4 -14 40.40 15.30 0 -4 14 51.79 12.00 0 -4 14 69.49 13.70 -1 4 -14 33.00 11.00 -1 4 -14 45.50 10.50 1 -4 14 35.80 11.90 1 -4 14 46.00 11.90 -2 4 -14 233.18 22.10 -2 4 -14 255.07 22.30 2 -4 14 213.78 30.00 2 -4 14 230.28 23.30 8 3 -14 3.00 7.90 -8 -3 14 11.40 9.60 7 3 -14 59.99 14.00 -7 -3 14 52.29 12.90 -6 -3 14 22.70 8.80 5 3 -14 49.20 13.30 -5 -3 14 24.20 12.50 -5 -3 14 30.80 11.10 4 3 -14 12.90 6.70 -4 -3 14 16.10 6.70 -4 -3 14 6.40 7.20 3 3 -14 0.20 6.20 -3 -3 14 5.70 5.00 -3 -3 14 -9.80 5.90 2 3 -14 7.70 5.70 -2 -3 14 11.60 8.10 -2 -3 14 0.30 6.20 1 3 -14 78.09 15.50 1 3 -14 109.49 13.50 -1 -3 14 134.39 20.10 -1 -3 14 101.89 17.40 0 3 -14 -5.50 4.30 0 3 -14 4.50 5.60 0 -3 14 -2.90 6.10 0 -3 14 5.10 7.00 -1 3 -14 5.00 5.30 -1 3 -14 5.20 8.90 1 -3 14 -2.30 5.80 1 -3 14 19.00 8.20 -2 3 -14 104.69 15.40 -2 3 -14 67.99 13.50 2 -3 14 92.69 17.50 2 -3 14 89.29 17.40 8 2 -14 2.70 6.40 -8 -2 14 1.00 7.20 7 2 -14 223.88 25.00 -7 -2 14 187.48 20.70 6 2 -14 5.80 8.70 -6 -2 14 20.90 8.60 5 2 -14 16.40 8.50 -5 -2 14 23.90 9.40 4 2 -14 15.60 8.30 -4 -2 14 6.50 8.40 -4 -2 14 4.80 5.50 3 2 -14 12.90 6.80 -3 -2 14 -0.50 5.70 -3 -2 14 15.80 7.40 2 2 -14 0.50 4.50 -2 -2 14 13.00 7.00 -2 -2 14 11.30 7.70 1 2 -14 -9.20 4.10 -1 -2 14 3.90 7.20 -1 -2 14 11.40 6.50 0 2 -14 135.89 16.90 0 -2 14 147.69 22.00 0 -2 14 126.69 21.40 -1 2 -14 12.20 7.40 1 -2 14 6.50 8.00 1 -2 14 0.50 6.50 -2 2 -14 -2.40 5.20 2 -2 14 -4.90 6.10 2 -2 14 -3.10 7.60 9 1 -14 2.00 7.10 -9 -1 14 8.10 7.00 -8 -1 14 13.20 7.10 7 1 -14 114.29 19.50 -7 -1 14 98.79 17.60 6 1 -14 101.29 22.90 -6 -1 14 90.89 15.40 5 1 -14 19.50 10.30 -5 -1 14 28.70 10.90 4 1 -14 45.20 12.10 -4 -1 14 42.60 10.00 3 1 -14 166.58 20.40 -3 -1 14 161.98 19.20 -3 -1 14 172.58 31.70 2 1 -14 11.60 6.60 -2 -1 14 23.00 8.80 -2 -1 14 -7.90 6.40 1 1 -14 66.99 14.40 -1 -1 14 61.99 13.90 -1 -1 14 35.50 10.30 0 1 -14 20.50 8.60 0 -1 14 13.50 7.70 0 -1 14 23.30 9.10 -1 1 -14 12.30 6.50 1 -1 14 -5.90 7.00 1 -1 14 8.90 7.90 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206.18 25.00 3 -5 -14 31.90 11.50 -3 5 14 37.40 12.80 2 -5 -14 44.10 11.80 -2 5 14 41.10 13.30 5 7 -15 -0.20 6.60 -5 -7 15 -4.80 7.90 -5 -7 15 16.80 10.30 4 7 -15 77.99 17.50 -4 -7 15 69.49 13.20 -4 -7 15 66.09 16.90 3 7 -15 13.20 8.90 -3 -7 15 3.80 6.40 -3 -7 15 14.80 10.10 -2 -7 15 25.80 10.50 -2 -7 15 25.40 8.60 1 7 -15 62.39 14.80 -1 -7 15 67.19 13.50 -1 -7 15 53.89 13.40 -1 -7 15 61.69 15.40 6 6 -15 -9.80 6.20 -6 -6 15 9.10 8.80 5 6 -15 36.10 12.30 -5 -6 15 15.00 9.80 -5 -6 15 29.00 11.90 4 6 -15 3.10 6.30 -4 -6 15 11.20 9.00 -4 -6 15 9.10 5.90 3 6 -15 10.40 8.40 -3 -6 15 20.20 7.30 -3 -6 15 -3.90 7.00 -3 -6 15 7.80 7.90 2 6 -15 41.20 11.40 -2 -6 15 47.50 12.60 -2 -6 15 55.89 11.70 -2 -6 15 61.39 12.40 1 6 -15 39.40 13.40 -1 -6 15 32.30 9.60 -1 -6 15 19.20 11.10 -1 -6 15 54.49 12.10 0 6 -15 5.10 7.90 0 -6 15 -0.40 10.30 0 -6 15 25.40 10.40 6 5 -15 -0.20 5.10 -6 -5 15 -2.80 7.80 5 5 -15 34.30 11.20 -5 -5 15 40.80 10.30 -5 -5 15 44.30 15.60 4 5 -15 15.10 7.00 -4 -5 15 5.00 7.00 -4 -5 15 2.20 6.90 3 5 -15 2.00 7.10 -3 -5 15 -1.90 6.30 2 5 -15 46.60 12.60 -2 -5 15 60.09 13.00 -2 -5 15 28.10 10.80 -2 -5 15 52.29 15.30 1 5 -15 6.70 6.50 -1 -5 15 9.80 7.80 -1 -5 15 14.40 9.10 0 5 -15 117.99 19.30 0 5 -15 108.69 16.20 0 -5 15 117.39 18.60 0 -5 15 82.19 18.70 7 4 -15 -2.10 5.90 -7 -4 15 26.20 10.90 6 4 -15 91.69 19.40 -6 -4 15 87.69 15.60 5 4 -15 11.60 6.90 -5 -4 15 9.30 8.10 4 4 -15 96.89 18.20 -4 -4 15 63.49 12.80 -4 -4 15 82.79 17.40 3 4 -15 6.60 7.60 -3 -4 15 20.70 8.10 -3 -4 15 15.80 9.10 2 4 -15 -1.90 5.70 -2 -4 15 -17.80 7.60 -2 -4 15 -12.00 6.50 1 4 -15 0.80 6.50 -1 -4 15 -4.10 6.00 -1 -4 15 -0.90 8.50 0 4 -15 5.60 7.30 0 -4 15 -0.20 7.80 7 3 -15 18.80 9.40 -7 -3 15 8.50 8.70 6 3 -15 9.10 8.10 -6 -3 15 21.00 9.20 5 3 -15 2.40 5.40 -5 -3 15 1.90 6.80 4 3 -15 4.20 5.90 -4 -3 15 0.40 7.30 3 3 -15 37.90 12.30 -3 -3 15 24.80 9.50 -3 -3 15 5.80 15.30 2 3 -15 -3.30 5.40 -2 -3 15 4.40 6.00 -2 -3 15 17.90 9.90 1 3 -15 165.68 21.40 -1 -3 15 121.59 20.00 -1 -3 15 92.69 17.40 0 3 -15 12.90 9.30 0 -3 15 8.60 10.00 0 -3 15 17.20 10.20 7 2 -15 37.00 10.70 -7 -2 15 12.40 8.00 6 2 -15 -13.10 6.30 -6 -2 15 8.60 8.10 5 2 -15 36.70 12.90 -5 -2 15 14.50 8.30 4 2 -15 190.88 22.40 -4 -2 15 213.18 21.90 3 2 -15 35.00 10.90 -3 -2 15 10.80 8.20 2 2 -15 6.20 8.20 -2 -2 15 -1.60 6.80 1 2 -15 20.40 9.00 -1 -2 15 -0.80 14.00 -1 -2 15 15.60 10.80 0 2 -15 22.80 9.10 0 -2 15 11.70 9.10 0 -2 15 12.60 8.50 7 1 -15 22.40 9.10 -7 -1 15 11.90 9.10 6 1 -15 1.80 9.10 -6 -1 15 38.80 13.60 5 1 -15 8.50 7.60 -5 -1 15 4.70 7.50 4 1 -15 6.60 6.50 -4 -1 15 6.90 7.30 3 1 -15 22.50 9.30 -3 -1 15 28.10 11.00 2 1 -15 0.00 6.20 1 1 -15 216.58 23.20 -1 -1 15 166.68 21.30 0 1 -15 16.00 8.30 0 -1 15 -5.70 6.40 7 0 -15 48.30 14.10 -7 0 15 39.10 11.10 6 0 -15 36.30 13.20 -6 0 15 12.00 8.10 5 0 -15 13.70 8.50 -5 0 15 -10.20 7.30 4 0 -15 27.70 9.00 -4 0 15 39.90 15.30 3 0 -15 -9.20 5.90 -3 0 15 7.50 7.10 2 0 -15 -4.90 5.70 -2 0 15 2.30 5.40 1 0 -15 2.10 6.90 -1 0 15 31.40 12.30 0 0 -15 1.20 7.50 0 0 15 4.70 6.70 7 -1 -15 26.00 10.50 -7 1 15 15.60 9.70 6 -1 -15 20.70 10.40 -6 1 15 43.50 12.40 5 -1 -15 83.39 17.60 -5 1 15 136.19 22.00 4 -1 -15 26.00 10.80 -4 1 15 45.60 12.40 3 -1 -15 9.60 9.00 -3 1 15 6.50 8.70 2 -1 -15 48.10 12.90 -2 1 15 47.70 12.90 1 -1 -15 37.10 11.20 -1 1 15 32.30 10.70 6 -2 -15 39.40 13.50 -6 2 15 7.40 9.40 5 -2 -15 61.29 16.00 -5 2 15 42.10 13.00 4 -2 -15 -3.30 6.30 -4 2 15 8.80 6.70 3 -2 -15 27.70 9.40 -3 2 15 10.10 7.80 2 -2 -15 10.20 6.10 -2 2 15 8.40 8.30 5 -3 -15 66.79 16.70 -5 3 15 49.00 14.80 4 -3 -15 31.00 14.10 -4 3 15 55.79 15.40 3 -3 -15 66.29 16.50 -3 3 15 60.89 16.70 4 4 -16 26.60 10.80 -4 -4 16 16.40 9.10 3 4 -16 2.90 8.50 -3 -4 16 13.20 9.80 5 3 -16 401.36 34.80 4 3 -16 110.59 21.30 3 3 -16 11.90 8.40 -3 -3 16 38.10 11.00 5 2 -16 2.50 7.20 -5 -2 16 8.00 8.70 4 2 -16 57.29 14.00 -4 -2 16 80.09 16.70 3 2 -16 6.50 7.90 -3 -2 16 -6.80 6.80 5 1 -16 8.10 7.30 -5 -1 16 22.40 10.30 4 1 -16 0.10 6.80 -4 -1 16 -3.00 6.30 3 1 -16 -3.20 6.90 -3 -1 16 -13.60 7.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 21048 _shelx_res_file ; TITL T429 in P-1 CELL 0.71073 8.0218 10.2278 10.6714 98.8503 108.0048 96.3852 ZERR 2.000 0.0002 0.0003 0.0003 0.0007 0.0007 0.0006 LATT 1 SFAC C H N O CL UNIT 34 28 6 8 2 TEMP -173.0 SIZE 0.15 0.20 0.25 OMIT 0 0 1 OMIT 0 1 0 OMIT -1 -3 3 OMIT 3 1 1 OMIT 1 0 0 OMIT -1 1 4 OMIT -1 -6 9 OMIT 4 -11 2 OMIT 1 2 0 L.S. 12 BOND $H ACTA CONF EQIV $1 -x, -y, -z+1 HTAB N1 O4_$1 EQIV $2 -x, -y+1, -z+1 HTAB N2 Cl1_$2 HTAB N2 O4_$2 HTAB C11 O2 WGHT 0.036600 0.418700 FVAR 1.25048 CL1 5 -0.007861 0.622964 0.869423 11.00000 0.01877 0.03980 = 0.03543 -0.01772 0.00875 0.00475 O1 4 0.205644 0.576392 0.666926 11.00000 0.02103 0.01160 = 0.01568 0.00277 0.00602 0.00664 O2 4 0.348268 0.395012 1.016020 11.00000 0.02925 0.02062 = 0.01398 0.00133 0.00642 -0.00038 O3 4 0.242689 0.200823 0.866493 11.00000 0.02441 0.01269 = 0.01497 0.00423 0.00674 0.00437 O4 4 -0.014099 0.181032 0.547813 11.00000 0.01283 0.01213 = 0.01964 0.00145 0.00291 0.00266 N1 3 0.227302 0.071598 0.585255 11.00000 0.01457 0.00919 = 0.01714 0.00060 0.00324 0.00298 H1 2 0.171256 -0.007544 0.547218 11.00000 -1.20000 N2 3 0.201557 0.584926 0.459187 11.00000 0.02638 0.01540 = 0.01965 0.00799 0.00995 0.00993 H2A 2 0.198352 0.548377 0.381862 11.00000 -1.20000 H2B 2 0.157578 0.660117 0.471364 11.00000 -1.20000 C1 1 0.146774 0.180254 0.591905 11.00000 0.01387 0.01030 = 0.01277 0.00201 0.00406 0.00218 C2 1 0.231799 0.511720 0.555105 11.00000 0.01372 0.01236 = 0.01566 0.00326 0.00518 0.00318 C3 1 0.285493 0.389961 0.549200 11.00000 0.01518 0.01136 = 0.01370 0.00303 0.00546 0.00365 C4 1 0.293130 0.307482 0.656699 11.00000 0.01255 0.00907 = 0.01294 0.00212 0.00438 0.00286 C5 1 0.270190 0.392500 0.777591 11.00000 0.01144 0.01235 = 0.01208 0.00088 0.00367 0.00210 C6 1 0.235270 0.517487 0.777294 11.00000 0.01355 0.01305 = 0.01345 0.00100 0.00320 0.00285 C7 1 0.322378 0.332664 0.432953 11.00000 0.02327 0.01738 = 0.01775 0.00794 0.00794 0.01006 N7 3 0.354716 0.285006 0.339682 11.00000 0.04608 0.03172 = 0.02234 0.01125 0.01701 0.02394 C8 1 0.292783 0.334591 0.900962 11.00000 0.01273 0.01437 = 0.01564 0.00294 0.00594 0.00282 C9 1 0.263230 0.129984 0.977577 11.00000 0.03621 0.01965 = 0.01948 0.00975 0.01336 0.00907 AFIX 23 H9A 2 0.175085 0.149147 1.022531 11.00000 -1.20000 H9B 2 0.383963 0.158775 1.044640 11.00000 -1.20000 AFIX 0 C10 1 0.234024 -0.016753 0.918745 11.00000 0.05275 0.01815 = 0.02927 0.01107 0.01627 0.01060 AFIX 137 H10A 2 0.241867 -0.068371 0.989897 11.00000 -1.50000 H10B 2 0.325088 -0.034849 0.877867 11.00000 -1.50000 H10C 2 0.116003 -0.043070 0.849970 11.00000 -1.50000 AFIX 0 C11 1 0.219877 0.613864 0.891020 11.00000 0.01817 0.01752 = 0.01691 -0.00319 0.00286 0.00646 AFIX 23 H11A 2 0.284311 0.703893 0.895973 11.00000 -1.20000 H11B 2 0.275198 0.584801 0.976510 11.00000 -1.20000 AFIX 0 C12 1 0.412769 0.105607 0.647347 11.00000 0.01422 0.01374 = 0.01357 0.00274 0.00454 0.00472 C13 1 0.537354 0.020740 0.665176 11.00000 0.02196 0.01706 = 0.01735 0.00347 0.00711 0.01059 AFIX 43 H13 2 0.503653 -0.073705 0.634869 11.00000 -1.20000 AFIX 0 C14 1 0.715022 0.080608 0.729868 11.00000 0.01937 0.02700 = 0.01706 0.00561 0.00658 0.01308 AFIX 43 H14 2 0.804374 0.025547 0.743121 11.00000 -1.20000 AFIX 0 C15 1 0.764638 0.218936 0.775465 11.00000 0.01297 0.02876 = 0.01570 0.00490 0.00486 0.00653 AFIX 43 H15 2 0.886614 0.256822 0.818937 11.00000 -1.20000 AFIX 0 C16 1 0.635763 0.302417 0.757583 11.00000 0.01453 0.01845 = 0.01284 0.00326 0.00555 0.00298 AFIX 43 H16 2 0.668372 0.396756 0.789255 11.00000 -1.20000 AFIX 0 C17 1 0.459550 0.243899 0.692536 11.00000 0.01357 0.01441 = 0.01105 0.00272 0.00502 0.00410 HKLF 4 REM T429 in P-1 REM R1 = 0.0444 for 4685 Fo > 4sig(Fo) and 0.0612 for all 5899 data REM 236 parameters refined using 0 restraints END WGHT 0.0366 0.4187 REM Highest difference peak 0.435, deepest hole -0.628, 1-sigma level 0.064 Q1 1 0.2727 0.4522 0.5561 11.00000 0.05 0.43 Q2 1 0.0091 0.5613 0.8799 11.00000 0.05 0.43 Q3 1 0.2840 0.3695 0.8357 11.00000 0.05 0.42 Q4 1 0.2202 0.2465 0.6337 11.00000 0.05 0.38 Q5 1 0.2760 0.4632 0.7952 11.00000 0.05 0.37 Q6 1 0.2334 0.0569 0.9423 11.00000 0.05 0.37 Q7 1 0.6297 0.0595 0.6818 11.00000 0.05 0.36 Q8 1 0.5372 0.2734 0.7395 11.00000 0.05 0.36 Q9 1 0.1883 0.1239 0.5771 11.00000 0.05 0.35 Q10 1 0.2742 0.2387 0.3232 11.00000 0.05 0.35 Q11 1 0.4551 0.1773 0.6765 11.00000 0.05 0.34 Q12 1 0.2778 0.3574 0.7051 11.00000 0.05 0.34 Q13 1 0.2357 0.5584 0.8357 11.00000 0.05 0.33 Q14 1 0.3184 0.0889 0.6123 11.00000 0.05 0.31 Q15 1 0.2117 0.4401 0.7468 11.00000 0.05 0.31 Q16 1 0.2817 0.3470 0.5963 11.00000 0.05 0.30 Q17 1 0.3025 0.3707 0.4938 11.00000 0.05 0.30 Q18 1 0.4684 0.0574 0.6813 11.00000 0.05 0.29 Q19 1 0.2312 0.5384 0.5065 11.00000 0.05 0.27 Q20 1 0.3694 0.2742 0.6815 11.00000 0.05 0.26 ; _shelx_res_checksum 28376 _shelxl_version_number .2013 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl Cl1 -0.00786(5) 0.62296(4) 0.86942(4) 0.03426(11) Uani d 1 . . O O1 0.20564(12) 0.57639(8) 0.66693(9) 0.01580(17) Uani d 1 . . O O2 0.34827(14) 0.39501(10) 1.01602(9) 0.0221(2) Uani d 1 . . O O3 0.24269(13) 0.20082(9) 0.86649(9) 0.01705(17) Uani d 1 . . O O4 -0.01410(11) 0.18103(8) 0.54781(9) 0.01560(17) Uani d 1 . . N N1 0.22730(14) 0.07160(10) 0.58525(11) 0.01426(19) Uani d 1 . . H H1 0.171(2) -0.0075(17) 0.5472(17) 0.017 Uiso d 1 . . N N2 0.20156(16) 0.58493(11) 0.45919(12) 0.0189(2) Uani d 1 . . H H2A 0.198(2) 0.5484(18) 0.3819(19) 0.023 Uiso d 1 . . H H2B 0.158(2) 0.6601(18) 0.4714(18) 0.023 Uiso d 1 . . C C1 0.14677(15) 0.18025(11) 0.59191(11) 0.0124(2) Uani d 1 . . C C2 0.23180(15) 0.51172(11) 0.55510(12) 0.0137(2) Uani d 1 . . C C3 0.28549(15) 0.38996(11) 0.54920(12) 0.0131(2) Uani d 1 . . C C4 0.29313(15) 0.30748(11) 0.65670(11) 0.01141(19) Uani d 1 . . C C5 0.27019(15) 0.39250(11) 0.77759(11) 0.01218(19) Uani d 1 . . C C6 0.23527(15) 0.51749(12) 0.77729(12) 0.0138(2) Uani d 1 . . C C7 0.32238(18) 0.33266(13) 0.43295(13) 0.0182(2) Uani d 1 . . N N7 0.3547(2) 0.28501(14) 0.33968(13) 0.0300(3) Uani d 1 . . C C8 0.29278(15) 0.33459(12) 0.90096(12) 0.0139(2) Uani d 1 . . C C9 0.2632(2) 0.12998(14) 0.97758(14) 0.0231(3) Uani d 1 . . H H9A 0.1751 0.1491 1.0225 0.028 Uiso calc 1 . . H H9B 0.3840 0.1588 1.0446 0.028 Uiso calc 1 . . C C10 0.2340(3) -0.01675(15) 0.91875(16) 0.0317(3) Uani d 1 . . H H10A 0.2419 -0.0684 0.9899 0.048 Uiso calc 1 . . H H10B 0.3251 -0.0348 0.8779 0.048 Uiso calc 1 . . H H10C 0.1160 -0.0431 0.8500 0.048 Uiso calc 1 . . C C11 0.21988(17) 0.61386(13) 0.89102(13) 0.0187(2) Uani d 1 . . H H11A 0.2843 0.7039 0.8960 0.022 Uiso calc 1 . . H H11B 0.2752 0.5848 0.9765 0.022 Uiso calc 1 . . C C12 0.41277(15) 0.10561(12) 0.64735(12) 0.0137(2) Uani d 1 . . C C13 0.53735(17) 0.02074(13) 0.66518(13) 0.0181(2) Uani d 1 . . H H13 0.5037 -0.0737 0.6349 0.022 Uiso calc 1 . . C C14 0.71502(17) 0.08061(14) 0.72987(13) 0.0201(2) Uani d 1 . . H H14 0.8044 0.0255 0.7431 0.024 Uiso calc 1 . . C C15 0.76464(16) 0.21894(14) 0.77546(13) 0.0188(2) Uani d 1 . . H H15 0.8866 0.2568 0.8189 0.023 Uiso calc 1 . . C C16 0.63576(16) 0.30242(12) 0.75758(12) 0.0150(2) Uani d 1 . . H H16 0.6684 0.3968 0.7893 0.018 Uiso calc 1 . . C C17 0.45955(15) 0.24390(12) 0.69254(11) 0.0126(2) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl1 0.01877(16) 0.0398(2) 0.0354(2) 0.00475(13) 0.00875(14) -0.01772(16) O1 0.0210(4) 0.0116(4) 0.0157(4) 0.0066(3) 0.0060(3) 0.0028(3) O2 0.0293(5) 0.0206(4) 0.0140(4) -0.0004(4) 0.0064(4) 0.0013(3) O3 0.0244(4) 0.0127(4) 0.0150(4) 0.0044(3) 0.0067(3) 0.0042(3) O4 0.0128(4) 0.0121(4) 0.0196(4) 0.0027(3) 0.0029(3) 0.0014(3) N1 0.0146(4) 0.0092(4) 0.0171(5) 0.0030(3) 0.0032(4) 0.0006(3) N2 0.0264(6) 0.0154(5) 0.0196(5) 0.0099(4) 0.0099(4) 0.0080(4) C1 0.0139(5) 0.0103(5) 0.0128(5) 0.0022(4) 0.0041(4) 0.0020(4) C2 0.0137(5) 0.0124(5) 0.0157(5) 0.0032(4) 0.0052(4) 0.0033(4) C3 0.0152(5) 0.0114(5) 0.0137(5) 0.0037(4) 0.0055(4) 0.0030(4) C4 0.0125(5) 0.0091(4) 0.0129(5) 0.0029(4) 0.0044(4) 0.0021(4) C5 0.0114(5) 0.0124(5) 0.0121(5) 0.0021(4) 0.0037(4) 0.0009(4) C6 0.0136(5) 0.0130(5) 0.0135(5) 0.0029(4) 0.0032(4) 0.0010(4) C7 0.0233(6) 0.0174(5) 0.0178(6) 0.0101(5) 0.0079(5) 0.0079(4) N7 0.0461(8) 0.0317(6) 0.0223(6) 0.0239(6) 0.0170(6) 0.0113(5) C8 0.0127(5) 0.0144(5) 0.0156(5) 0.0028(4) 0.0059(4) 0.0029(4) C9 0.0362(7) 0.0196(6) 0.0195(6) 0.0091(5) 0.0134(5) 0.0097(5) C10 0.0528(10) 0.0182(6) 0.0293(7) 0.0106(6) 0.0163(7) 0.0111(6) C11 0.0182(5) 0.0175(5) 0.0169(5) 0.0065(4) 0.0029(4) -0.0032(4) C12 0.0142(5) 0.0137(5) 0.0136(5) 0.0047(4) 0.0045(4) 0.0027(4) C13 0.0220(6) 0.0171(5) 0.0173(6) 0.0106(4) 0.0071(5) 0.0035(4) C14 0.0194(6) 0.0270(6) 0.0171(6) 0.0131(5) 0.0066(5) 0.0056(5) C15 0.0130(5) 0.0288(6) 0.0157(5) 0.0065(4) 0.0049(4) 0.0049(5) C16 0.0145(5) 0.0185(5) 0.0128(5) 0.0030(4) 0.0056(4) 0.0033(4) C17 0.0136(5) 0.0144(5) 0.0111(5) 0.0041(4) 0.0050(4) 0.0027(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 O1 C6 . . 119.01(9) ? C8 O3 C9 . . 115.95(10) ? C1 N1 C12 . . 111.77(10) ? C1 N1 H1 . . 123.4(11) ? C12 N1 H1 . . 124.8(11) ? C2 N2 H2A . . 118.0(12) ? C2 N2 H2B . . 119.3(11) ? H2A N2 H2B . . 120.6(16) ? O4 C1 N1 . . 126.32(11) ? O4 C1 C4 . . 125.13(10) ? N1 C1 C4 . . 108.42(9) ? N2 C2 O1 . . 110.94(10) ? N2 C2 C3 . . 127.13(11) ? O1 C2 C3 . . 121.91(10) ? C2 C3 C7 . . 118.87(11) ? C2 C3 C4 . . 122.67(10) ? C7 C3 C4 . . 118.26(10) ? C5 C4 C3 . . 109.52(9) ? C5 C4 C17 . . 112.86(9) ? C3 C4 C17 . . 112.55(9) ? C5 C4 C1 . . 113.49(9) ? C3 C4 C1 . . 107.25(9) ? C17 C4 C1 . . 100.85(9) ? C6 C5 C8 . . 120.03(10) ? C6 C5 C4 . . 121.88(10) ? C8 C5 C4 . . 118.07(9) ? C5 C6 O1 . . 123.81(11) ? C5 C6 C11 . . 127.27(11) ? O1 C6 C11 . . 108.91(10) ? N7 C7 C3 . . 178.80(14) ? O2 C8 O3 . . 123.11(11) ? O2 C8 C5 . . 127.00(11) ? O3 C8 C5 . . 109.89(10) ? O3 C9 C10 . . 106.89(11) ? O3 C9 H9A . . 110.3 ? C10 C9 H9A . . 110.3 ? O3 C9 H9B . . 110.3 ? C10 C9 H9B . . 110.3 ? H9A C9 H9B . . 108.6 ? C9 C10 H10A . . 109.5 ? C9 C10 H10B . . 109.5 ? H10A C10 H10B . . 109.5 ? C9 C10 H10C . . 109.5 ? H10A C10 H10C . . 109.5 ? H10B C10 H10C . . 109.5 ? C6 C11 Cl1 . . 110.59(9) ? C6 C11 H11A . . 109.5 ? Cl1 C11 H11A . . 109.5 ? C6 C11 H11B . . 109.5 ? Cl1 C11 H11B . . 109.5 ? H11A C11 H11B . . 108.1 ? C13 C12 C17 . . 122.36(11) ? C13 C12 N1 . . 128.15(11) ? C17 C12 N1 . . 109.49(10) ? C12 C13 C14 . . 116.79(12) ? C12 C13 H13 . . 121.6 ? C14 C13 H13 . . 121.6 ? C15 C14 C13 . . 121.72(11) ? C15 C14 H14 . . 119.1 ? C13 C14 H14 . . 119.1 ? C14 C15 C16 . . 120.36(12) ? C14 C15 H15 . . 119.8 ? C16 C15 H15 . . 119.8 ? C17 C16 C15 . . 118.24(11) ? C17 C16 H16 . . 120.9 ? C15 C16 H16 . . 120.9 ? C16 C17 C12 . . 120.53(11) ? C16 C17 C4 . . 130.24(11) ? C12 C17 C4 . . 109.23(10) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cl1 C11 . 1.7842(13) ? O1 C2 . 1.3595(15) ? O1 C6 . 1.3725(14) ? O2 C8 . 1.2063(15) ? O3 C8 . 1.3417(14) ? O3 C9 . 1.4586(15) ? O4 C1 . 1.2308(14) ? N1 C1 . 1.3495(14) ? N1 C12 . 1.4064(15) ? N1 H1 . 0.853(17) ? N2 C2 . 1.3379(15) ? N2 H2A . 0.843(19) ? N2 H2B . 0.889(18) ? C1 C4 . 1.5592(16) ? C2 C3 . 1.3610(15) ? C3 C7 . 1.4183(17) ? C3 C4 . 1.5156(16) ? C4 C5 . 1.5138(16) ? C4 C17 . 1.5183(16) ? C5 C6 . 1.3390(16) ? C5 C8 . 1.4944(16) ? C6 C11 . 1.4871(17) ? C7 N7 . 1.1550(18) ? C9 C10 . 1.497(2) ? C9 H9A . 0.9900 ? C9 H9B . 0.9900 ? C10 H10A . 0.9800 ? C10 H10B . 0.9800 ? C10 H10C . 0.9800 ? C11 H11A . 0.9900 ? C11 H11B . 0.9900 ? C12 C13 . 1.3837(16) ? C12 C17 . 1.3907(16) ? C13 C14 . 1.3966(19) ? C13 H13 . 0.9500 ? C14 C15 . 1.393(2) ? C14 H14 . 0.9500 ? C15 C16 . 1.3995(17) ? C15 H15 . 0.9500 ? C16 C17 . 1.3840(16) ? C16 H16 . 0.9500 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 O4 2_556 0.853(17) 1.981(17) 2.8292(14) 173.0(17) yes N2 H2B O4 2_566 0.887(18) 2.095(18) 2.9636(15) 166.0(17) yes C11 H11B O2 . 0.99 2.15 2.9039(17) 131 yes C13 H13 N7 2_656 0.95 2.56 3.333(2) 138 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C12 N1 C1 O4 . . . . -179.07(12) ? C12 N1 C1 C4 . . . . 4.71(13) ? C6 O1 C2 N2 . . . . -178.30(10) ? C6 O1 C2 C3 . . . . 0.39(17) ? N2 C2 C3 C7 . . . . 2.90(19) ? O1 C2 C3 C7 . . . . -175.56(11) ? N2 C2 C3 C4 . . . . -171.94(12) ? O1 C2 C3 C4 . . . . 9.61(18) ? C2 C3 C4 C5 . . . . -11.44(15) ? C7 C3 C4 C5 . . . . 173.69(10) ? C2 C3 C4 C17 . . . . -137.85(12) ? C7 C3 C4 C17 . . . . 47.28(14) ? C2 C3 C4 C1 . . . . 112.13(12) ? C7 C3 C4 C1 . . . . -62.74(13) ? O4 C1 C4 C5 . . . . 58.07(15) ? N1 C1 C4 C5 . . . . -125.66(10) ? O4 C1 C4 C3 . . . . -63.02(15) ? N1 C1 C4 C3 . . . . 113.24(10) ? O4 C1 C4 C17 . . . . 179.05(11) ? N1 C1 C4 C17 . . . . -4.69(12) ? C3 C4 C5 C6 . . . . 4.62(15) ? C17 C4 C5 C6 . . . . 130.85(11) ? C1 C4 C5 C6 . . . . -115.19(12) ? C3 C4 C5 C8 . . . . -173.65(9) ? C17 C4 C5 C8 . . . . -47.42(13) ? C1 C4 C5 C8 . . . . 66.54(13) ? C8 C5 C6 O1 . . . . -177.31(10) ? C4 C5 C6 O1 . . . . 4.46(18) ? C8 C5 C6 C11 . . . . 1.96(18) ? C4 C5 C6 C11 . . . . -176.28(11) ? C2 O1 C6 C5 . . . . -7.59(17) ? C2 O1 C6 C11 . . . . 173.03(10) ? C9 O3 C8 O2 . . . . -1.51(17) ? C9 O3 C8 C5 . . . . 178.03(10) ? C6 C5 C8 O2 . . . . -29.78(18) ? C4 C5 C8 O2 . . . . 148.52(12) ? C6 C5 C8 O3 . . . . 150.69(11) ? C4 C5 C8 O3 . . . . -31.00(14) ? C8 O3 C9 C10 . . . . -169.29(12) ? C5 C6 C11 Cl1 . . . . -103.28(13) ? O1 C6 C11 Cl1 . . . . 76.07(11) ? C1 N1 C12 C13 . . . . 176.98(12) ? C1 N1 C12 C17 . . . . -2.67(14) ? C17 C12 C13 C14 . . . . -0.81(18) ? N1 C12 C13 C14 . . . . 179.59(12) ? C12 C13 C14 C15 . . . . 0.58(19) ? C13 C14 C15 C16 . . . . 0.2(2) ? C14 C15 C16 C17 . . . . -0.69(18) ? C15 C16 C17 C12 . . . . 0.48(17) ? C15 C16 C17 C4 . . . . -178.77(11) ? C13 C12 C17 C16 . . . . 0.29(18) ? N1 C12 C17 C16 . . . . 179.96(10) ? C13 C12 C17 C4 . . . . 179.68(11) ? N1 C12 C17 C4 . . . . -0.65(13) ? C5 C4 C17 C16 . . . . -56.14(16) ? C3 C4 C17 C16 . . . . 68.46(15) ? C1 C4 C17 C16 . . . . -177.56(12) ? C5 C4 C17 C12 . . . . 124.55(10) ? C3 C4 C17 C12 . . . . -110.86(11) ? C1 C4 C17 C12 . . . . 3.13(12) ? _cod_database_fobs_code 2243855