#------------------------------------------------------------------------------ #$Date: 2021-07-21 08:24:53 +0300 (Wed, 21 Jul 2021) $ #$Revision: 267669 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/38/2243877.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243877 _cell_angle_alpha 103.273 _cell_angle_beta 103.662 _cell_angle_gamma 98.785 _cell_length_a 8.5737 _cell_length_b 10.7967 _cell_length_c 13.0183 _exptl_crystal_F_000 582.70 _reflns_d_resolution_high 0.6375 _cod_data_source_file hb7977IIsup3.hkl _cod_data_source_block II _shelx_title ' ew1-37f_cs_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 252.12 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1222.20 1223.84 44.19 o 2 0 0 3231.57 3096.06 37.99 o 3 0 0 6773.99 6439.57 67.60 o 4 0 0 9515.75 9720.12 101.35 o 5 0 0 23.94 30.28 3.27 o 6 0 0 1956.72 1972.88 26.53 o 7 0 0 689.83 705.44 17.18 o 8 0 0 28.19 31.99 5.62 o 9 0 0 1095.37 1047.88 19.07 o 10 0 0 1693.91 1719.04 60.82 o 11 0 0 321.95 302.68 17.69 o -12 1 0 74.16 84.22 39.83 o -11 1 0 805.53 769.54 29.08 o -10 1 0 235.08 200.60 10.07 o -9 1 0 794.85 797.92 15.36 o -8 1 0 1201.26 1207.44 24.09 o -7 1 0 1787.00 1779.91 26.84 o -6 1 0 103.79 120.53 6.21 o -5 1 0 6014.26 6111.05 97.57 o -4 1 0 7470.88 7539.64 121.57 o -3 1 0 985.90 1005.91 18.73 o -2 1 0 4216.54 4362.32 61.02 o -1 1 0 31177.15 27490.09 490.36 o 0 1 0 584.79 683.29 15.28 o 1 1 0 11546.10 11766.49 117.01 o 2 1 0 7990.14 7899.74 87.63 o 3 1 0 105.61 87.18 3.75 o 4 1 0 45.50 49.34 3.28 o 5 1 0 6263.88 6255.93 65.61 o 6 1 0 1369.46 1412.83 17.49 o 7 1 0 13.30 13.26 2.63 o 8 1 0 1253.73 1238.48 20.89 o 9 1 0 1941.80 1932.03 35.28 o 10 1 0 350.41 335.10 16.56 o 11 1 0 321.67 324.68 22.77 o -12 2 0 824.62 791.93 46.57 o -11 2 0 82.41 90.10 13.37 o -10 2 0 504.00 377.97 41.80 o -9 2 0 2537.99 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635.15 12.26 o -3 -7 2 2364.83 2404.05 26.00 o -2 -7 2 357.52 378.97 7.72 o -1 -7 2 118.54 134.14 4.84 o 0 -7 2 7122.35 6892.13 70.85 o 1 -7 2 3030.18 3026.79 30.13 o 2 -7 2 1155.70 1333.14 18.78 o 3 -7 2 7394.32 7376.62 80.20 o 4 -7 2 6291.62 5943.29 61.80 o 5 -7 2 228.52 265.98 10.64 o 6 -7 2 1916.75 1967.74 34.30 o 7 -7 2 2897.94 2910.16 43.74 o 8 -7 2 414.49 420.49 16.77 o 9 -7 2 530.53 505.21 17.64 o 10 -7 2 747.54 751.69 27.60 o 11 -7 2 325.31 372.88 23.92 o 12 -7 2 105.24 103.90 26.21 o -11 -6 2 521.50 522.72 45.32 o -10 -6 2 293.42 306.92 17.15 o -9 -6 2 121.46 128.29 10.89 o -8 -6 2 895.38 912.36 22.01 o -7 -6 2 1908.64 1971.13 32.14 o -6 -6 2 8.42 7.73 4.23 o -5 -6 2 56.67 64.77 5.57 o -4 -6 2 3909.48 3908.03 43.67 o -3 -6 2 316.64 362.04 7.66 o -2 -6 2 540.05 514.06 9.16 o -1 -6 2 8354.29 8156.67 81.58 o 0 -6 2 4659.74 4745.75 47.20 o 1 -6 2 1742.29 1853.85 23.62 o 2 -6 2 23524.33 23777.74 256.00 o 3 -6 2 9229.91 9185.34 96.41 o 4 -6 2 603.57 558.64 13.30 o 5 -6 2 2771.25 2775.39 43.05 o 6 -6 2 2194.69 2208.38 28.62 o 7 -6 2 729.46 727.03 15.42 o 8 -6 2 320.58 333.84 10.69 o 9 -6 2 705.40 681.36 16.35 o 10 -6 2 206.46 185.45 13.04 o 11 -6 2 214.27 212.66 22.79 o -11 -5 2 139.88 165.32 39.13 o -10 -5 2 139.08 136.82 11.70 o -9 -5 2 817.21 836.78 23.55 o -8 -5 2 790.86 787.25 19.33 o -7 -5 2 26.66 25.26 4.86 o -6 -5 2 3202.75 3204.26 42.52 o -5 -5 2 3883.24 3817.91 44.14 o -4 -5 2 140.04 138.27 4.60 o -3 -5 2 261.24 251.12 6.18 o -2 -5 2 15379.48 15479.29 131.61 o -1 -5 2 545.92 521.52 8.02 o 0 -5 2 432.82 473.62 7.82 o 1 -5 2 19292.01 20030.53 266.57 o 2 -5 2 1140.56 1092.37 18.41 o 3 -5 2 1816.29 1965.21 25.21 o 4 -5 2 4496.71 4305.96 66.43 o 5 -5 2 4265.11 4181.93 45.99 o 6 -5 2 63.09 61.33 4.12 o 7 -5 2 1080.56 1091.07 19.14 o 8 -5 2 1844.94 1843.46 30.46 o 9 -5 2 216.03 192.10 9.62 o 10 -5 2 211.19 190.91 19.30 o 11 -5 2 901.09 863.35 39.75 o -11 -4 2 115.86 113.40 28.86 o -10 -4 2 793.89 822.19 23.67 o -9 -4 2 606.23 621.48 19.59 o -8 -4 2 260.19 239.26 9.57 o -7 -4 2 2484.30 2518.01 39.38 o -6 -4 2 2834.15 2784.75 35.36 o -5 -4 2 1194.34 1163.68 19.46 o -4 -4 2 2176.65 2208.21 29.41 o -3 -4 2 4731.83 4628.25 44.34 o -2 -4 2 17.27 18.95 2.07 o -1 -4 2 3695.65 3769.12 37.17 o 0 -4 2 9611.91 9328.59 96.07 o 1 -4 2 32.72 32.15 5.75 o 2 -4 2 44.99 67.43 2.68 o 3 -4 2 4997.16 4680.14 49.06 o 4 -4 2 4486.77 4592.36 103.49 o 5 -4 2 163.89 142.26 5.64 o 6 -4 2 1027.64 1029.69 20.08 o 7 -4 2 1904.23 1839.73 31.58 o 8 -4 2 218.34 214.10 11.52 o 9 -4 2 878.39 826.19 19.97 o 10 -4 2 1231.16 1209.53 60.71 o 11 -4 2 446.28 445.04 22.99 o -12 -3 2 167.36 178.98 34.97 o -11 -3 2 1312.44 1357.28 52.53 o -10 -3 2 647.19 659.81 22.37 o -9 -3 2 353.77 364.15 14.45 o -8 -3 2 1857.31 1809.44 29.76 o -7 -3 2 3376.77 3288.45 47.12 o -6 -3 2 2533.26 2532.36 30.80 o -5 -3 2 5431.99 5327.88 54.07 o -4 -3 2 1921.20 1865.12 22.61 o -3 -3 2 26.95 29.02 1.82 o -2 -3 2 821.09 802.89 10.42 o -1 -3 2 9112.04 8934.99 85.62 o 0 -3 2 1189.28 1135.55 17.69 o 1 -3 2 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10 -2 2 417.70 424.87 21.21 o 11 -2 2 997.51 1060.21 35.00 o -12 -1 2 74.78 31.99 22.09 o -11 -1 2 517.91 495.17 19.62 o -10 -1 2 979.06 996.70 26.99 o -9 -1 2 745.11 770.68 35.51 o -8 -1 2 103.50 108.24 10.39 o -7 -1 2 1241.69 1248.39 27.62 o -6 -1 2 1903.62 1902.87 25.33 o -5 -1 2 98.11 100.91 4.40 o -4 -1 2 2103.82 1969.01 25.02 o -3 -1 2 5310.35 5090.18 50.75 o -2 -1 2 106.39 99.82 3.12 o -1 -1 2 5183.53 5101.57 56.43 o 0 -1 2 21425.86 21759.33 252.45 o 1 -1 2 9853.12 9947.79 89.89 o 2 -1 2 2813.42 2927.25 25.26 o 3 -1 2 21219.34 21085.32 166.76 o 4 -1 2 4076.41 3951.03 35.28 o 5 -1 2 826.85 867.84 12.97 o 6 -1 2 2369.92 2352.63 27.66 o 7 -1 2 1962.79 2048.01 29.52 o 8 -1 2 167.72 173.80 8.52 o 9 -1 2 688.63 705.22 22.88 o 10 -1 2 778.97 852.31 29.64 o 11 -1 2 10.05 14.80 11.77 o -12 0 2 195.60 202.91 20.50 o -11 0 2 521.92 497.76 20.48 o -10 0 2 546.87 543.72 18.10 o -9 0 2 118.58 134.60 11.26 o -8 0 2 1956.90 1969.80 34.47 o -7 0 2 187.27 213.37 8.61 o -6 0 2 30.90 31.08 3.16 o 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