#------------------------------------------------------------------------------ #$Date: 2021-07-24 08:13:33 +0300 (Sat, 24 Jul 2021) $ #$Revision: 267733 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/38/2243879.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243879 loop_ _publ_author_name 'Bouzian, Younos' 'Chkirate, Karim' 'Mague, Joel T.' 'Al-Ostoot, Fares Hezam' 'Hammou Ahabchane, Noureddine' 'Essassi, El Mokhtar' _publ_section_title ; Crystal structure, Hirshfeld surface analysis and density functional theory study of benzyl 2-oxo-1-(prop-2-yn-1-yl)-1,2-dihydroquinoline-4-carboxylate ; _journal_coeditor_code TX2040 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 824 _journal_page_last 828 _journal_paper_doi 10.1107/S2056989021007416 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac 'C20 H15 N O3' _chemical_formula_moiety 'C20 H15 N O3' _chemical_formula_sum 'C20 H15 N O3' _chemical_formula_weight 317.33 _chemical_name_systematic ; Benzyl 2-oxo-1-(prop-2-yn-1-yl)-1,2-dihydroquinoline-4-carboxylate ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 96.1550(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.2284(3) _cell_length_b 13.7693(4) _cell_length_c 13.9230(4) _cell_measurement_reflns_used 9939 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 33.2503 _cell_measurement_theta_min 2.4897 _cell_volume 1568.37(9) _computing_cell_refinement ; SAINT (Bruker, 2020) ; _computing_data_collection ; APEX3 (Bruker, 2020) ; _computing_data_reduction ; SAINT (Bruker, 2020) ; _computing_molecular_graphics ; DIAMOND (Brandenburg & Putz, 2012) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2018/1 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 150(2) _diffrn_detector_area_resol_mean 7.3910 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measurement_device 'Bruker D8 QUEST PHOTON 3 diffractometer' _diffrn_measurement_device_type 'Bruker D8 QUEST PHOTON 3 diffractometer' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0246 _diffrn_reflns_av_unetI/netI 0.0130 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 80207 _diffrn_reflns_theta_full 33.000 _diffrn_reflns_theta_max 33.354 _diffrn_reflns_theta_min 2.943 _diffrn_source 'fine-focus sealed tube' _diffrn_source_current 30.0 _diffrn_source_power 1.50 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.091 _exptl_absorpt_correction_T_max 0.97 _exptl_absorpt_correction_T_min 0.93 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.344 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 664 _exptl_crystal_size_max 0.437 _exptl_crystal_size_mid 0.348 _exptl_crystal_size_min 0.320 _refine_diff_density_max 0.460 _refine_diff_density_min -0.211 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 217 _refine_ls_number_reflns 6020 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0517 _refine_ls_R_factor_gt 0.0460 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0739P)^2^+0.3685P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1282 _refine_ls_wR_factor_ref 0.1331 _reflns_number_gt 5304 _reflns_number_total 6020 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file tx2040sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2243879 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.961 _shelx_estimated_absorpt_t_max 0.971 _shelx_hkl_file ; -1 0 0 16.80 0.90 1 0 0 23.00 0.90 1 0 0 15.80 0.90 1 0 0 22.80 0.90 1 0 0 20.90 0.80 1 0 0 23.00 0.80 -1 0 0 20.10 0.80 1 0 0 15.70 0.70 1 0 0 18.40 0.90 -1 0 0 20.20 0.90 -3 0 0 2.10 0.60 -3 0 0 1.30 0.30 -3 0 0 1.00 0.50 -3 0 0 0.40 0.60 -3 0 0 1.00 0.70 3 0 0 1.50 0.60 3 0 0 1.00 0.50 -3 0 0 0.90 0.50 3 0 0 1.00 0.70 3 0 0 0.00 0.60 3 0 0 3.10 0.70 3 0 0 0.40 0.70 -3 0 0 1.60 0.80 -3 0 0 0.30 0.70 -3 0 0 1.70 0.60 -4 0 0 1.50 0.80 -4 0 0 0.00 0.30 -4 0 0 -0.30 0.80 -4 0 0 -0.80 0.60 -4 0 0 0.70 0.50 -4 0 0 -0.50 0.80 -4 0 0 -1.20 0.70 -4 0 0 0.60 0.60 4 0 0 1.40 0.60 4 0 0 -0.60 0.80 4 0 0 0.60 0.60 -4 0 0 0.10 0.90 4 0 0 1.50 0.70 -4 0 0 1.20 0.60 4 0 0 1.00 0.70 4 0 0 1.40 0.70 -4 0 0 0.50 0.80 4 0 0 -0.80 0.80 5 0 0 1.30 0.70 -5 0 0 1.10 0.40 5 0 0 0.20 1.10 -5 0 0 0.70 0.70 -5 0 0 0.50 1.00 -5 0 0 0.40 0.40 -5 0 0 0.80 0.90 5 0 0 1.60 0.90 5 0 0 0.70 1.10 -5 0 0 -0.10 0.70 -5 0 0 0.50 0.80 -5 0 0 1.10 1.10 -5 0 0 0.40 1.20 5 0 0 1.90 1.00 5 0 0 0.40 0.80 -5 0 0 2.10 1.30 -5 0 0 -0.10 0.80 5 0 0 0.40 1.10 -5 0 0 -0.30 0.90 -6 0 0 109.49 5.10 6 0 0 105.29 4.60 -6 0 0 105.59 4.30 -6 0 0 114.99 5.20 6 0 0 112.79 5.60 -6 0 0 110.49 6.40 -6 0 0 114.39 4.20 6 0 0 102.99 5.10 6 0 0 100.49 5.40 6 0 0 114.29 4.70 -6 0 0 114.29 4.60 -7 0 0 -1.00 1.30 -7 0 0 3.00 1.90 7 0 0 0.00 1.70 -7 0 0 -0.30 1.20 -7 0 0 3.50 1.60 7 0 0 -2.90 1.20 7 0 0 0.20 1.30 7 0 0 -1.70 1.50 -7 0 0 0.80 1.70 -7 0 0 0.80 1.10 8 0 0 272.57 9.60 8 0 0 278.87 11.00 -8 0 0 293.47 10.80 8 0 0 289.37 11.20 -8 0 0 295.17 10.80 -8 0 0 279.07 11.10 8 0 0 286.27 9.60 -8 0 0 280.57 8.90 9 0 0 -0.30 2.00 -9 0 0 0.20 2.00 -9 0 0 -2.30 1.70 -9 0 0 -0.10 1.90 9 0 0 0.30 1.50 9 0 0 2.20 2.10 -10 0 0 15.80 3.60 10 0 0 27.00 4.70 10 0 0 21.10 3.30 -10 0 0 22.60 4.50 10 0 0 20.00 4.30 -10 0 0 20.50 4.00 -11 0 0 3.20 3.00 11 0 0 0.50 1.80 -11 0 0 -0.10 2.50 11 0 0 1.60 2.80 -11 0 0 1.70 2.30 -12 0 0 23.00 5.30 12 0 0 23.40 4.20 -12 0 0 32.40 5.00 12 0 0 20.10 5.00 -12 0 0 28.40 5.80 0 -1 0 0.00 0.10 0 -1 0 0.00 0.10 0 -1 0 0.10 0.10 0 -1 0 0.10 0.10 0 -1 0 0.00 0.10 0 -1 0 0.00 0.10 0 -1 0 -0.10 0.10 0 -1 0 0.10 0.10 0 -1 0 0.00 0.10 0 -1 0 -0.10 0.10 0 1 0 0.00 0.10 0 1 0 0.10 0.10 0 1 0 0.10 0.10 0 1 0 0.00 0.10 0 1 0 0.00 0.10 0 1 0 0.00 0.10 0 1 0 0.00 0.10 0 1 0 -0.10 0.10 0 1 0 -0.10 0.10 0 1 0 0.10 0.10 -2 -1 0 4.10 0.80 -2 -1 0 3.00 0.90 -2 -1 0 4.00 0.50 2 -1 0 3.00 0.90 -2 -1 0 2.70 0.70 2 -1 0 3.70 0.80 -2 -1 0 3.80 0.60 2 -1 0 3.70 0.70 2 -1 0 3.30 0.30 -2 -1 0 3.00 0.50 -2 -1 0 5.60 0.60 -2 -1 0 2.70 0.60 2 -1 0 3.60 0.60 2 -1 0 2.20 0.70 2 -1 0 2.00 0.60 -2 -1 0 2.00 0.70 2 1 0 3.80 0.70 -2 1 0 2.40 0.60 -2 1 0 2.90 0.70 -2 1 0 4.90 1.00 2 1 0 3.20 0.80 -2 1 0 2.70 0.70 -2 1 0 2.10 0.50 2 1 0 6.20 1.00 -2 1 0 2.20 0.60 2 1 0 4.60 0.60 2 1 0 3.60 0.60 -2 1 0 2.90 0.70 2 1 0 3.50 0.60 -2 1 0 2.90 0.70 3 -1 0 1236.58 28.70 -3 -1 0 1275.07 29.30 -3 -1 0 1243.98 28.20 -3 -1 0 1249.38 28.80 -3 -1 0 1251.57 28.70 -3 -1 0 1258.27 28.10 -3 -1 0 1245.28 28.70 -3 -1 0 1217.78 29.20 -3 -1 0 1239.78 28.10 3 -1 0 1223.08 29.20 3 -1 0 1228.78 29.20 -3 -1 0 1238.88 28.00 3 -1 0 1254.07 28.60 -3 -1 0 1245.18 29.20 3 -1 0 1215.68 29.00 -3 1 0 1219.08 29.10 3 1 0 1262.37 28.00 -3 1 0 1186.28 30.10 -3 1 0 1257.87 29.10 3 1 0 1274.17 28.80 3 1 0 1231.28 29.20 3 1 0 1234.08 28.30 -3 1 0 1208.58 28.20 3 1 0 1245.18 28.30 -3 1 0 1257.57 29.20 -3 1 0 1240.48 28.50 -3 1 0 1187.58 28.50 -3 1 0 1235.38 29.10 3 1 0 1201.68 29.10 -3 1 0 1243.38 28.60 3 1 0 1236.88 28.70 4 -1 0 795.92 19.10 -4 -1 0 820.62 19.80 4 -1 0 808.22 19.20 -4 -1 0 805.52 19.00 -4 -1 0 807.72 20.20 -4 -1 0 797.52 19.50 -4 -1 0 797.32 18.50 -4 -1 0 790.72 19.60 -4 -1 0 796.22 20.20 4 -1 0 681.33 19.20 -4 -1 0 815.92 18.80 -4 -1 0 794.52 18.80 -4 -1 0 804.12 20.10 -4 -1 0 803.82 20.20 4 -1 0 801.92 20.20 4 -1 0 797.22 19.50 4 -1 0 801.42 19.90 4 -1 0 815.42 20.30 -4 1 0 785.22 20.00 -4 1 0 788.62 20.80 -4 1 0 791.82 19.20 -4 1 0 785.32 19.00 4 1 0 770.72 20.00 4 1 0 806.62 19.10 -4 1 0 819.02 20.20 4 1 0 798.92 20.20 -4 1 0 798.42 19.30 -4 1 0 799.92 19.20 4 1 0 785.62 19.60 4 1 0 809.82 18.50 4 1 0 801.62 19.10 4 1 0 817.12 19.60 -4 1 0 818.22 20.10 -4 1 0 802.22 20.10 5 -1 0 710.33 17.20 -5 -1 0 690.73 18.40 -5 -1 0 591.84 17.60 5 -1 0 684.73 18.50 -5 -1 0 695.23 16.80 5 -1 0 679.83 18.10 -5 -1 0 703.43 16.80 5 -1 0 705.43 17.60 5 -1 0 681.73 17.20 -5 -1 0 684.33 16.70 -5 -1 0 704.43 18.50 -5 -1 0 703.03 18.50 5 -1 0 689.73 18.50 -5 -1 0 685.33 16.20 -5 -1 0 687.13 17.50 -5 -1 0 704.13 17.90 5 -1 0 690.73 17.60 -5 -1 0 685.53 18.50 -5 1 0 728.83 18.30 -5 1 0 699.93 18.50 -5 1 0 662.53 17.00 -5 1 0 698.23 17.20 5 1 0 691.63 17.80 -5 1 0 696.93 18.30 5 1 0 704.83 18.10 -5 1 0 686.73 18.40 -5 1 0 696.63 18.60 -5 1 0 703.23 17.40 5 1 0 693.73 17.70 -5 1 0 685.33 17.20 5 1 0 682.93 18.40 5 1 0 708.43 17.30 -5 1 0 694.53 18.40 5 1 0 703.93 18.60 6 -1 0 107.29 4.80 -6 -1 0 115.79 5.50 -6 -1 0 114.19 5.20 -6 -1 0 104.69 3.90 -6 -1 0 113.19 6.50 6 -1 0 107.39 6.20 6 -1 0 110.39 5.50 -6 -1 0 113.29 4.20 -6 -1 0 111.29 3.40 -6 -1 0 112.79 5.30 6 -1 0 106.29 4.40 6 -1 0 118.99 4.90 6 -1 0 109.69 4.40 -6 1 0 121.29 6.60 -6 1 0 107.89 5.20 6 1 0 117.29 5.70 -6 1 0 108.89 4.40 6 1 0 106.09 6.20 6 1 0 111.49 4.80 -6 1 0 106.79 5.30 6 1 0 112.59 5.20 -6 1 0 108.89 4.40 -6 1 0 106.59 4.50 -7 -1 0 133.49 5.00 7 -1 0 132.69 5.30 -7 -1 0 114.29 5.70 7 -1 0 126.19 6.50 -7 -1 0 130.19 6.10 -7 -1 0 127.39 5.50 7 -1 0 120.89 6.40 -7 -1 0 116.89 4.50 -7 -1 0 122.79 4.80 7 -1 0 130.89 5.80 -7 -1 0 137.49 6.70 7 1 0 135.79 6.80 -7 1 0 139.59 6.90 -7 1 0 144.39 5.60 7 1 0 128.19 5.50 -7 1 0 125.49 6.20 -7 1 0 130.79 5.30 7 1 0 126.29 5.40 7 1 0 133.49 6.70 7 1 0 132.29 5.70 -7 1 0 133.09 6.40 8 -1 0 5.80 2.20 8 -1 0 3.80 2.00 -8 -1 0 3.80 2.10 8 -1 0 5.20 2.30 -8 -1 0 5.50 2.30 8 -1 0 6.50 2.00 -8 -1 0 4.70 1.40 -8 -1 0 6.40 2.40 8 1 0 4.30 2.20 8 1 0 5.80 1.90 -8 1 0 4.90 2.40 -8 1 0 6.20 1.80 -8 1 0 3.40 2.20 8 1 0 4.10 2.50 -8 1 0 3.40 2.30 -9 -1 0 10.20 2.90 9 -1 0 9.70 3.10 9 -1 0 9.70 3.00 -9 -1 0 5.30 2.70 -9 -1 0 7.90 2.70 9 -1 0 6.10 2.10 -9 1 0 7.80 2.80 -9 1 0 4.40 2.30 9 1 0 8.10 2.40 -9 1 0 11.50 2.90 9 1 0 9.30 3.10 9 1 0 8.80 2.20 10 -1 0 13.60 3.50 -10 -1 0 7.30 3.00 10 -1 0 7.40 3.50 -10 -1 0 8.20 2.90 10 -1 0 10.10 2.60 -10 -1 0 9.10 2.90 -10 1 0 9.80 3.20 -10 1 0 14.00 3.60 10 1 0 11.60 3.40 10 1 0 9.70 2.20 -11 -1 0 25.50 4.50 -11 -1 0 7.20 3.40 11 -1 0 12.80 3.80 -11 -1 0 15.10 3.70 11 -1 0 12.20 2.60 11 -1 0 10.40 3.90 -11 1 0 11.10 3.70 11 1 0 15.50 4.10 -11 1 0 19.10 4.40 11 1 0 15.30 3.00 -11 1 0 14.90 4.00 12 -1 0 8.00 3.00 -12 -1 0 11.90 3.60 -12 -1 0 7.50 3.20 12 -1 0 8.80 3.30 12 1 0 11.00 3.70 -12 1 0 14.30 4.10 -12 1 0 9.00 4.00 -12 1 0 8.40 3.70 12 1 0 10.00 3.30 0 -2 0 216.08 5.10 0 -2 0 180.38 4.70 0 -2 0 176.08 5.00 0 -2 0 206.98 5.10 0 -2 0 187.08 4.80 0 -2 0 204.38 5.20 0 -2 0 212.78 5.10 0 -2 0 205.88 5.10 0 -2 0 183.98 4.70 0 2 0 208.78 5.10 0 2 0 217.88 4.80 0 2 0 201.58 5.10 0 2 0 210.68 5.20 0 2 0 193.78 5.00 0 2 0 205.18 5.10 0 2 0 212.78 5.10 0 2 0 198.68 5.10 1 -2 0 566.04 13.00 -1 -2 0 540.85 12.30 -1 -2 0 565.84 13.00 -1 -2 0 556.14 12.60 1 -2 0 556.74 12.80 1 -2 0 553.64 12.40 1 -2 0 563.04 13.00 -1 -2 0 514.95 12.90 1 -2 0 549.95 13.00 -1 -2 0 550.04 12.30 -1 -2 0 548.85 12.60 1 -2 0 549.15 12.80 -1 -2 0 549.54 13.00 -1 -2 0 547.25 12.70 1 -2 0 551.64 12.80 -1 -2 0 545.35 12.50 1 -2 0 538.55 13.00 -1 -2 0 552.74 12.90 1 -2 0 530.45 13.00 1 -2 0 542.35 12.60 -1 -2 0 544.25 12.30 -1 2 0 546.75 12.60 -1 2 0 533.15 12.90 1 2 0 546.85 12.70 -1 2 0 534.15 12.90 -1 2 0 546.65 13.00 1 2 0 542.65 12.50 1 2 0 522.05 13.00 -1 2 0 537.75 12.70 -1 2 0 540.45 12.80 1 2 0 539.55 12.70 -1 2 0 549.05 12.90 1 2 0 543.95 12.90 -1 2 0 554.04 13.00 1 2 0 539.15 12.90 1 2 0 554.74 13.10 -1 2 0 546.75 12.40 -1 2 0 543.75 12.80 -2 -2 0 709.03 16.80 2 -2 0 678.33 16.70 2 -2 0 699.83 16.60 -2 -2 0 694.53 16.10 -2 -2 0 698.23 16.10 2 -2 0 691.93 16.70 -2 -2 0 710.03 16.00 -2 -2 0 688.53 16.30 -2 -2 0 689.43 16.60 2 -2 0 688.23 15.90 -2 -2 0 693.73 15.80 2 -2 0 708.43 16.60 -2 -2 0 704.63 16.00 2 -2 0 677.43 15.80 2 -2 0 681.93 16.60 2 -2 0 682.43 16.60 -2 -2 0 675.23 16.70 2 2 0 689.63 16.70 -2 2 0 688.63 16.50 -2 2 0 692.73 15.80 -2 2 0 668.03 16.70 -2 2 0 691.03 16.70 2 2 0 703.23 16.10 -2 2 0 698.83 16.60 2 2 0 689.83 16.10 2 2 0 697.43 16.60 2 2 0 704.73 16.10 -2 2 0 660.93 16.60 -2 2 0 729.03 16.80 -2 2 0 674.83 16.60 -2 2 0 777.32 15.90 2 2 0 692.83 16.80 2 2 0 693.93 15.80 -3 -2 0 376.86 9.20 -3 -2 0 389.66 9.80 3 -2 0 375.86 10.10 3 -2 0 385.56 10.00 3 -2 0 384.56 8.80 3 -2 0 381.36 10.10 3 -2 0 366.56 10.40 -3 -2 0 388.16 10.00 -3 -2 0 381.06 9.30 3 -2 0 385.26 10.30 -3 -2 0 381.76 9.20 -3 -2 0 383.86 9.30 -3 -2 0 387.66 9.90 3 -2 0 381.36 9.40 -3 -2 0 389.76 10.20 -3 -2 0 389.66 10.40 3 -2 0 368.16 10.20 -3 -2 0 381.26 10.50 -3 -2 0 376.66 10.30 3 -2 0 378.66 10.40 -3 2 0 380.66 10.10 -3 2 0 392.46 10.10 3 2 0 381.36 9.60 3 2 0 381.26 9.80 -3 2 0 380.66 9.40 -3 2 0 385.46 10.40 -3 2 0 383.06 10.00 3 2 0 387.16 10.20 -3 2 0 377.96 10.30 -3 2 0 391.66 10.40 3 2 0 399.46 9.60 -3 2 0 391.36 10.40 3 2 0 387.66 10.50 -3 2 0 381.96 10.40 -3 2 0 387.56 8.80 -4 -2 0 1801.92 40.30 4 -2 0 1756.42 41.20 -4 -2 0 1782.82 41.90 -4 -2 0 1824.92 41.40 -4 -2 0 1839.82 42.10 -4 -2 0 1784.12 40.40 -4 -2 0 1754.32 41.40 -4 -2 0 1811.12 40.30 4 -2 0 1785.92 42.00 -4 -2 0 1763.82 40.30 4 -2 0 1689.43 41.70 -4 -2 0 1815.52 41.30 -4 -2 0 1756.02 40.50 4 -2 0 1804.42 42.10 4 -2 0 1819.52 41.50 4 -2 0 1808.02 40.60 4 2 0 1805.62 40.90 4 2 0 1794.12 40.80 4 2 0 1816.82 41.60 -4 2 0 1750.42 41.20 4 2 0 1793.92 42.20 4 2 0 1771.62 41.20 -4 2 0 1745.13 40.50 4 2 0 1787.12 40.60 -4 2 0 1795.82 42.00 -4 2 0 1761.32 41.80 -4 2 0 1782.52 41.90 -4 2 0 1791.22 41.20 4 2 0 1798.32 42.00 -4 2 0 1802.92 42.00 -4 2 0 1753.92 41.80 -4 2 0 1792.52 41.30 -5 -2 0 1323.47 30.20 5 -2 0 1298.67 31.20 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35.70 2.60 3 -5 0 37.70 2.40 3 5 0 38.60 2.50 -3 5 0 37.20 2.50 3 5 0 36.70 2.30 -3 5 0 37.40 2.50 -3 5 0 36.40 2.40 3 5 0 37.40 2.60 3 5 0 39.50 2.80 -3 5 0 35.70 2.00 -3 5 0 33.00 2.50 3 5 0 38.80 2.10 -3 5 0 38.10 2.60 3 5 0 35.40 2.10 -3 5 0 32.10 2.40 -3 5 0 36.50 2.60 -3 5 0 32.70 2.50 4 -5 0 1274.57 31.70 4 -5 0 1306.97 29.60 -4 -5 0 1269.67 29.40 4 -5 0 1263.37 31.00 -4 -5 0 1268.57 29.60 4 -5 0 1272.27 32.00 -4 -5 0 1235.98 31.30 -4 -5 0 1243.98 31.10 -4 -5 0 1247.78 30.50 -4 -5 0 1259.77 29.60 -4 -5 0 1252.47 31.10 -4 -5 0 1287.77 31.30 4 -5 0 1294.87 31.30 4 -5 0 1286.37 31.40 -4 -5 0 1261.47 29.50 -4 5 0 1273.87 31.20 -4 5 0 1235.58 31.10 -4 5 0 1317.47 31.10 -4 5 0 1292.07 31.10 -4 5 0 1308.67 29.40 4 5 0 1278.67 30.60 4 5 0 1269.67 31.50 4 5 0 1291.17 31.40 -4 5 0 1281.07 31.00 4 5 0 1266.17 30.00 -4 5 0 1311.47 31.40 -4 5 0 1301.17 31.20 -4 5 0 1286.27 30.90 -5 -5 0 12.30 2.10 5 -5 0 10.60 1.10 5 -5 0 10.50 2.10 -5 -5 0 9.80 2.10 -5 -5 0 14.20 1.80 -5 -5 0 11.60 1.60 -5 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-1.90 1.70 8 -5 0 28.30 4.00 -8 -5 0 23.60 3.70 8 -5 0 17.50 3.40 8 -5 0 22.40 3.50 -8 -5 0 32.40 4.00 -8 -5 0 30.30 3.20 -8 -5 0 22.50 2.90 8 5 0 25.60 3.60 8 5 0 23.50 3.80 -8 5 0 32.40 3.90 8 5 0 24.40 2.70 -8 5 0 29.80 3.90 -8 5 0 23.10 3.30 -8 5 0 19.80 3.40 9 -5 0 75.49 5.60 -9 -5 0 79.79 5.00 9 -5 0 70.29 5.90 9 -5 0 77.99 6.10 -9 -5 0 72.49 5.80 -9 -5 0 76.49 4.90 -9 -5 0 76.19 6.00 -9 5 0 69.19 5.80 -9 5 0 77.19 6.00 9 5 0 72.69 5.50 -9 5 0 68.19 5.00 9 5 0 70.19 6.10 9 5 0 76.09 4.40 -9 5 0 74.99 6.00 10 -5 0 22.60 3.80 10 -5 0 27.80 4.60 -10 -5 0 27.60 3.80 -10 -5 0 27.10 3.50 10 -5 0 23.20 4.40 -10 -5 0 24.80 4.50 -10 -5 0 21.70 4.40 -10 5 0 31.30 4.60 10 5 0 23.50 4.30 10 5 0 30.30 3.20 10 5 0 22.50 3.90 -10 5 0 27.00 4.60 -10 5 0 27.70 4.70 11 -5 0 2.30 2.70 -11 -5 0 0.50 2.80 -11 -5 0 8.50 3.50 11 -5 0 5.10 2.80 11 -5 0 5.30 2.90 -11 5 0 2.40 3.00 11 5 0 11.50 3.50 -11 5 0 2.90 2.90 -11 5 0 13.30 4.00 11 5 0 6.70 2.50 -12 -5 0 8.90 3.70 -12 -5 0 9.90 3.80 12 -5 0 12.00 3.20 12 -5 0 4.60 3.60 12 -5 0 4.60 3.30 12 5 0 10.30 4.10 -12 5 0 16.30 4.30 -12 5 0 8.30 3.40 12 5 0 11.30 2.50 -12 5 0 10.10 3.80 0 -6 0 254.17 6.50 0 -6 0 261.67 7.70 0 -6 0 263.57 7.70 0 -6 0 244.88 7.50 0 -6 0 254.27 7.60 0 -6 0 254.07 7.60 0 -6 0 258.87 7.50 0 -6 0 261.77 7.70 0 6 0 250.87 7.80 0 6 0 271.87 7.60 0 6 0 254.67 7.50 0 6 0 262.17 6.50 0 6 0 258.47 7.60 0 6 0 257.47 7.60 0 6 0 251.27 6.40 0 6 0 270.67 7.20 0 6 0 258.57 7.70 0 6 0 258.97 7.70 1 -6 0 725.23 17.80 -1 -6 0 719.83 17.00 -1 -6 0 713.83 17.60 -1 -6 0 718.53 17.40 -1 -6 0 713.33 17.90 -1 -6 0 707.63 18.00 1 -6 0 711.63 18.10 1 -6 0 728.13 17.30 -1 -6 0 714.73 17.90 1 -6 0 675.03 17.80 1 -6 0 725.63 18.00 1 -6 0 706.83 17.00 -1 -6 0 720.73 18.00 1 -6 0 711.23 17.10 -1 -6 0 729.63 17.60 1 -6 0 709.43 17.90 1 -6 0 718.73 18.00 -1 6 0 707.23 17.80 1 6 0 707.43 17.70 -1 6 0 717.83 17.10 1 6 0 708.23 17.40 -1 6 0 696.13 17.90 1 6 0 692.83 18.00 1 6 0 700.63 17.90 1 6 0 709.03 16.90 -1 6 0 721.43 17.90 1 6 0 714.93 17.80 1 6 0 705.03 17.70 -1 6 0 695.03 17.80 -1 6 0 727.53 17.00 -1 6 0 679.43 17.50 -1 6 0 750.92 18.90 -1 6 0 731.73 18.10 2 -6 0 1946.01 46.20 2 -6 0 2004.40 46.20 2 -6 0 2013.70 45.70 -2 -6 0 1974.50 46.80 -2 -6 0 2079.39 46.20 -2 -6 0 1998.20 46.10 2 -6 0 2019.80 46.90 -2 -6 0 2023.50 46.10 2 -6 0 2024.60 47.00 -2 -6 0 2105.49 47.10 2 -6 0 2030.60 47.00 -2 -6 0 2026.40 47.00 -2 -6 0 2029.90 45.90 2 -6 0 2071.79 47.20 2 -6 0 2009.30 46.90 2 -6 0 2034.20 46.30 2 -6 0 2010.40 45.70 -2 -6 0 1989.70 46.80 -2 6 0 1958.00 47.00 -2 6 0 2024.80 46.10 -2 6 0 1966.00 46.30 2 6 0 2065.69 46.40 -2 6 0 2022.70 46.30 2 6 0 2026.90 45.90 2 6 0 2006.10 46.80 -2 6 0 1987.60 46.70 -2 6 0 2024.40 46.40 -2 6 0 2018.80 47.00 2 6 0 1990.20 46.90 -2 6 0 2046.10 47.10 2 6 0 1976.30 47.00 2 6 0 2047.70 46.10 -2 6 0 2017.20 46.80 -3 -6 0 263.27 7.20 -3 -6 0 268.67 6.50 3 -6 0 282.87 8.70 -3 -6 0 269.57 6.60 3 -6 0 247.58 8.40 -3 -6 0 263.87 7.70 3 -6 0 266.07 7.60 3 -6 0 260.77 8.00 -3 -6 0 262.17 6.50 -3 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2.20 6 6 0 22.40 3.10 -7 -6 0 19.00 3.20 7 -6 0 22.30 3.40 7 -6 0 17.80 3.10 -7 -6 0 16.80 2.10 -7 -6 0 15.30 3.00 -7 -6 0 18.70 2.40 7 -6 0 15.50 2.90 7 6 0 19.50 3.10 -7 6 0 17.70 3.20 7 6 0 20.80 2.50 -7 6 0 17.80 2.90 -7 6 0 12.90 2.80 7 6 0 19.40 3.30 7 6 0 18.90 2.40 8 -6 0 -1.70 1.80 -8 -6 0 -0.20 1.70 -8 -6 0 1.30 1.30 -8 -6 0 0.50 1.30 8 -6 0 1.80 1.90 -8 -6 0 -3.80 1.40 8 -6 0 -0.20 1.60 -8 6 0 -0.80 1.60 -8 6 0 -1.90 1.70 8 6 0 2.60 1.90 -8 6 0 1.80 1.80 8 6 0 -1.70 1.80 -8 6 0 -1.30 1.70 8 6 0 -1.00 1.30 9 -6 0 250.47 15.50 9 -6 0 198.08 9.70 -9 -6 0 181.68 7.80 9 -6 0 178.38 8.80 -9 -6 0 190.98 8.00 -9 -6 0 202.98 9.60 -9 6 0 180.08 9.30 -9 6 0 193.78 9.50 -9 6 0 188.38 8.60 9 6 0 203.08 9.20 10 -6 0 33.60 4.40 10 -6 0 26.40 4.70 -10 -6 0 38.50 5.20 10 -6 0 27.90 4.80 -10 -6 0 34.80 5.00 10 6 0 39.60 5.40 -10 6 0 39.70 4.80 -10 6 0 36.90 4.90 10 6 0 36.90 3.60 -10 6 0 36.80 4.90 -10 6 0 36.70 4.90 -11 -6 0 27.70 4.70 -11 -6 0 30.70 4.90 11 -6 0 28.50 4.60 11 -6 0 26.50 5.10 11 -6 0 26.00 5.00 -11 6 0 27.00 4.80 11 6 0 26.20 3.50 -11 6 0 31.80 5.10 -11 6 0 18.00 4.10 11 6 0 29.20 5.10 -12 -6 0 7.20 3.70 -12 -6 0 10.10 3.90 12 -6 0 7.80 3.10 12 -6 0 9.70 3.80 -12 6 0 -0.40 3.20 -12 6 0 8.90 3.70 12 6 0 2.80 3.40 12 6 0 5.00 2.20 -12 6 0 3.50 3.10 0 -7 0 1.90 0.80 0 -7 0 1.90 0.90 0 -7 0 -0.30 0.70 0 -7 0 1.40 0.90 0 -7 0 1.10 1.00 0 -7 0 0.40 0.80 0 -7 0 1.60 0.50 0 -7 0 0.40 0.70 0 7 0 1.20 0.90 0 7 0 3.10 1.00 0 7 0 0.70 0.80 0 7 0 2.30 0.60 0 7 0 1.30 0.80 0 7 0 0.50 0.80 0 7 0 1.20 0.50 0 7 0 0.20 0.80 0 7 0 2.00 0.90 0 7 0 0.50 0.50 -1 -7 0 266.57 8.40 1 -7 0 284.47 8.60 -1 -7 0 275.87 8.20 -1 -7 0 275.87 8.60 1 -7 0 281.57 8.60 1 -7 0 284.97 8.00 -1 -7 0 282.87 8.30 -1 -7 0 287.77 8.50 1 -7 0 271.47 8.50 1 -7 0 266.67 9.50 1 -7 0 271.87 8.40 -1 -7 0 277.57 8.60 1 -7 0 274.67 8.50 1 -7 0 275.37 7.60 1 -7 0 269.97 7.60 -1 -7 0 287.07 7.60 -1 -7 0 281.57 8.10 1 7 0 273.37 7.50 -1 7 0 275.77 8.70 -1 7 0 284.57 8.70 1 7 0 289.67 8.50 1 7 0 298.87 8.20 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107.39 7.30 -8 11 0 88.49 6.70 8 11 0 97.49 7.10 -8 11 0 91.89 7.00 9 -11 0 102.19 7.70 9 -11 0 101.49 7.80 -9 -11 0 130.39 7.80 -9 -11 0 110.89 7.90 9 -11 0 108.09 7.80 -9 11 0 121.69 8.00 9 11 0 119.09 6.10 -9 11 0 136.29 8.40 -9 11 0 113.29 7.60 9 11 0 108.29 7.90 -9 11 0 119.39 8.20 -10 -11 0 13.00 3.90 10 -11 0 9.30 3.90 10 -11 0 11.90 3.70 -10 -11 0 12.20 3.50 10 -11 0 15.10 4.20 -10 11 0 11.20 3.90 10 11 0 13.10 4.10 10 11 0 14.10 2.90 -10 11 0 16.90 4.20 -10 11 0 17.30 3.80 0 -12 0 1.90 2.00 0 -12 0 3.30 1.20 0 -12 0 -1.60 1.40 0 -12 0 0.00 1.70 0 12 0 2.30 1.80 0 12 0 1.00 1.60 -1 -12 0 114.29 4.60 1 -12 0 114.89 6.30 -1 -12 0 106.39 5.80 -1 -12 0 117.69 6.20 1 -12 0 120.09 6.20 1 -12 0 109.89 4.60 1 -12 0 107.59 6.00 1 -12 0 123.69 6.30 -1 12 0 110.19 4.30 -1 12 0 116.29 6.00 1 12 0 111.39 6.00 -1 12 0 111.19 6.10 1 12 0 116.29 6.30 -1 12 0 118.19 6.20 -1 12 0 109.49 4.20 1 12 0 105.69 5.90 1 12 0 106.69 5.80 2 -12 0 49.00 3.50 -2 -12 0 54.69 3.20 2 -12 0 53.19 4.40 -2 -12 0 56.29 4.40 2 -12 0 54.39 4.50 2 -12 0 48.50 4.40 -2 -12 0 54.09 4.30 2 -12 0 53.79 3.30 2 12 0 46.70 3.50 -2 12 0 51.69 4.00 -2 12 0 45.20 4.30 2 12 0 54.49 4.20 2 12 0 48.40 4.20 2 12 0 47.40 4.40 -2 12 0 52.29 3.10 -2 12 0 54.59 4.30 -2 12 0 56.69 3.30 3 -12 0 184.68 8.40 3 -12 0 180.18 8.30 3 -12 0 184.78 6.80 3 -12 0 177.78 6.90 -3 -12 0 190.78 8.50 -3 -12 0 183.18 8.20 3 -12 0 190.48 8.50 -3 -12 0 186.48 6.80 3 12 0 192.28 7.20 -3 12 0 193.78 8.50 -3 12 0 189.98 8.50 3 12 0 196.28 8.00 -3 12 0 191.58 7.10 3 12 0 198.18 8.50 -3 12 0 199.58 7.30 3 12 0 200.48 8.60 -3 12 0 196.28 8.00 4 -12 0 64.19 5.10 4 -12 0 54.29 4.70 -4 -12 0 52.09 3.70 4 -12 0 55.29 4.90 -4 -12 0 54.29 4.80 -4 -12 0 49.80 4.50 4 -12 0 51.39 3.60 4 12 0 51.39 4.00 -4 12 0 46.30 3.70 4 12 0 47.30 3.40 -4 12 0 48.90 3.80 -4 12 0 51.99 4.60 -4 12 0 52.29 4.70 4 12 0 60.19 4.80 -4 12 0 51.19 4.00 4 12 0 57.59 4.70 -5 -12 0 66.19 5.40 -5 -12 0 57.19 4.90 5 -12 0 60.79 4.40 5 -12 0 64.39 5.30 5 -12 0 56.59 5.10 -5 -12 0 61.19 4.20 5 -12 0 59.89 5.20 -5 12 0 66.99 5.40 5 12 0 60.89 4.40 -5 12 0 53.99 4.00 -5 12 0 67.89 4.80 5 12 0 63.19 5.20 5 12 0 55.89 4.70 -5 12 0 63.79 4.60 6 -12 0 113.79 7.50 -6 -12 0 129.39 6.50 6 -12 0 118.99 7.30 -6 -12 0 113.89 7.20 6 -12 0 118.89 7.30 -6 -12 0 131.39 7.70 -6 12 0 123.19 6.80 -6 12 0 126.79 7.50 -6 12 0 128.89 7.00 6 12 0 129.39 7.70 6 12 0 116.99 6.90 6 12 0 124.59 6.20 -7 -12 0 21.20 4.20 -7 -12 0 25.00 4.60 7 -12 0 14.70 3.80 7 -12 0 18.10 4.00 7 -12 0 29.20 4.60 -7 -12 0 17.50 3.50 7 12 0 21.70 3.90 7 12 0 25.40 3.10 -7 12 0 26.00 3.80 -7 12 0 18.60 3.90 7 12 0 15.80 3.70 -7 12 0 20.50 4.10 -8 -12 0 7.00 3.00 -8 -12 0 9.20 3.20 8 -12 0 7.90 3.20 8 -12 0 6.70 3.20 8 -12 0 8.70 3.40 -8 12 0 3.40 3.00 8 12 0 7.20 2.40 -8 12 0 6.50 2.90 8 12 0 4.50 2.80 -8 12 0 7.70 3.30 9 -12 0 -3.50 3.10 9 -12 0 11.70 3.60 -9 -12 0 6.90 3.40 9 -12 0 5.40 3.40 -9 -12 0 8.00 3.30 -9 12 0 11.30 3.50 -9 12 0 12.70 3.70 9 12 0 9.10 3.60 -9 12 0 8.70 3.30 9 12 0 9.90 2.20 10 -12 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5.70 -3 -13 0 134.19 7.00 -3 13 0 136.99 7.30 3 13 0 130.09 6.60 -3 13 0 144.29 7.40 -3 13 0 136.09 5.80 -3 13 0 139.19 6.80 3 13 0 148.79 7.60 -3 13 0 140.19 6.80 3 13 0 130.19 7.10 -4 -13 0 17.20 2.90 4 -13 0 23.00 4.00 -4 -13 0 16.70 3.30 4 -13 0 23.50 2.80 4 -13 0 25.50 3.90 4 -13 0 21.20 3.70 -4 -13 0 17.00 3.10 4 13 0 22.90 3.20 4 13 0 22.40 3.80 -4 13 0 17.50 3.00 -4 13 0 22.30 4.80 -4 13 0 19.30 3.50 4 13 0 15.70 3.30 -4 13 0 20.30 3.00 -4 13 0 17.50 2.90 -5 -13 0 77.59 6.20 -5 -13 0 81.79 4.90 5 -13 0 84.59 6.20 5 -13 0 73.29 5.80 -5 -13 0 72.89 5.80 5 -13 0 71.19 5.80 5 13 0 80.09 6.00 -5 13 0 82.99 6.20 5 13 0 84.29 5.20 5 13 0 79.89 5.90 -5 13 0 87.69 5.00 -5 13 0 86.19 5.50 -6 -13 0 160.48 9.40 6 -13 0 167.58 8.70 -6 -13 0 166.78 7.60 6 -13 0 155.18 8.80 6 -13 0 141.39 8.90 6 13 0 154.48 7.60 -6 13 0 163.28 8.00 -6 13 0 155.08 7.70 6 13 0 160.58 8.30 -6 13 0 126.79 9.80 6 13 0 147.89 8.70 -7 -13 0 372.86 13.40 -7 -13 0 389.76 15.30 7 -13 0 392.26 16.50 7 -13 0 385.36 15.10 7 -13 0 357.56 14.80 -7 -13 0 383.16 15.00 7 13 0 369.36 12.90 7 13 0 385.66 14.40 -7 13 0 373.46 14.10 -7 13 0 369.86 14.80 -7 13 0 397.06 14.50 7 13 0 409.06 15.40 -8 -13 0 34.20 5.20 8 -13 0 33.10 4.90 8 -13 0 49.90 5.90 8 -13 0 25.60 4.90 -8 -13 0 37.10 5.40 8 13 0 24.30 5.20 -8 13 0 40.00 5.10 -8 13 0 34.20 5.00 8 13 0 43.20 4.20 -8 13 0 36.90 5.40 -9 -13 0 89.49 7.40 9 -13 0 73.49 7.20 9 -13 0 73.59 7.00 -9 -13 0 79.49 7.20 9 13 0 69.79 6.90 9 13 0 74.49 5.10 -9 13 0 76.19 6.90 -9 13 0 64.49 6.40 -9 13 0 75.69 6.90 0 -14 0 2140.99 53.89 0 -14 0 2260.07 54.19 0 -14 0 2099.19 51.69 0 14 0 2180.18 53.29 0 14 0 2196.38 53.99 0 14 0 2243.58 54.29 -1 -14 0 174.88 8.60 -1 -14 0 181.98 6.90 1 -14 0 169.98 8.60 1 -14 0 188.88 8.10 -1 -14 0 196.98 8.80 1 -14 0 199.68 9.00 1 14 0 187.48 8.20 -1 14 0 190.18 8.90 1 14 0 191.58 8.70 1 14 0 202.58 9.10 -1 14 0 194.38 8.90 -1 14 0 190.28 8.60 2 -14 0 29.70 4.30 -2 -14 0 36.60 4.30 -2 -14 0 33.90 3.20 -2 -14 0 35.60 4.30 2 -14 0 37.80 4.40 2 -14 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66.99 6.60 -7 14 0 77.79 6.10 7 14 0 73.99 6.40 -7 14 0 79.59 6.80 -7 14 0 83.89 6.50 7 14 0 74.79 7.00 7 14 0 74.09 5.20 8 -14 0 8.90 3.60 -8 -14 0 16.20 4.00 -8 -14 0 6.70 3.50 8 -14 0 14.90 4.60 -8 14 0 6.20 3.60 8 14 0 7.90 2.40 -8 14 0 9.90 3.20 -8 14 0 10.80 3.40 8 14 0 6.80 4.30 -9 -14 0 26.20 5.30 -9 -14 0 38.00 6.50 9 -14 0 26.50 6.10 9 14 0 26.60 3.70 9 14 0 23.00 5.90 -9 14 0 19.60 4.50 -9 14 0 21.10 4.80 -9 14 0 20.60 5.20 0 -15 0 12.20 3.30 0 -15 0 8.50 2.70 0 15 0 6.90 2.30 0 15 0 8.90 2.40 1 -15 0 117.99 7.30 -1 -15 0 118.19 7.20 -1 -15 0 119.19 7.10 1 -15 0 129.59 7.40 -1 15 0 120.99 7.20 -1 15 0 108.39 6.90 1 15 0 122.19 7.30 1 15 0 115.69 6.40 -1 15 0 115.89 6.80 1 15 0 123.89 7.10 2 -15 0 2.10 2.20 -2 -15 0 3.00 2.40 2 -15 0 0.60 2.50 -2 -15 0 1.20 2.20 2 -15 0 2.20 2.00 2 15 0 -0.10 2.10 -2 15 0 3.60 2.40 -2 15 0 -1.30 1.90 2 15 0 0.60 1.80 -2 15 0 0.10 1.80 2 15 0 3.70 2.20 2 15 0 0.80 2.10 3 -15 0 4.00 2.40 -3 -15 0 3.70 2.70 3 -15 0 4.80 2.50 -3 -15 0 8.40 2.90 3 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12 -2 35.90 5.10 -8 12 2 35.80 4.80 7 -12 -2 92.99 6.80 7 -12 -2 74.09 6.20 -7 -12 2 92.99 6.90 7 -12 -2 93.99 6.50 -7 -12 2 78.89 5.40 -7 -12 2 67.89 7.70 -7 12 2 78.49 6.00 7 12 -2 76.39 6.10 7 12 -2 86.19 6.80 -7 12 2 82.79 6.20 -7 12 2 95.49 6.70 7 12 -2 82.39 4.90 -6 -12 2 28.30 3.30 6 -12 -2 25.20 3.60 6 -12 -2 26.30 4.10 6 -12 -2 32.70 4.50 6 -12 -2 29.10 4.40 -6 -12 2 25.00 4.20 -6 -12 2 27.70 3.90 6 12 -2 25.40 4.20 -6 12 2 28.70 3.80 6 12 -2 22.90 4.00 -6 12 2 31.70 3.90 6 12 -2 25.40 3.10 -6 12 2 33.20 4.50 5 -12 -2 67.19 5.20 -5 -12 2 61.59 5.20 -5 -12 2 45.60 4.50 -5 -12 2 61.89 3.90 5 -12 -2 55.29 4.40 5 -12 -2 60.79 5.30 5 -12 -2 58.49 4.80 -5 12 2 58.29 5.00 5 12 -2 57.09 5.10 -5 12 2 58.49 4.20 5 12 -2 62.89 5.30 -5 12 2 58.49 4.40 5 12 -2 59.99 4.10 -5 12 2 55.39 4.30 -4 -12 2 278.67 11.30 4 -12 -2 269.07 11.10 4 -12 -2 296.77 10.90 4 -12 -2 291.17 10.20 4 -12 -2 292.47 11.40 -4 -12 2 285.77 9.00 -4 -12 2 292.57 10.90 -4 12 2 298.47 11.40 4 12 -2 286.77 9.80 4 12 -2 290.17 11.20 -4 12 2 291.47 10.00 4 12 -2 286.17 11.30 -4 12 2 299.37 10.50 4 12 -2 278.57 9.90 -4 12 2 283.17 12.10 -4 12 2 302.07 10.30 3 -12 -2 68.69 4.90 3 -12 -2 64.49 4.10 3 -12 -2 62.69 3.50 3 -12 -2 65.89 5.10 -3 -12 2 67.29 4.70 -3 -12 2 65.79 3.30 3 -12 -2 75.19 5.30 -3 -12 2 60.09 4.90 3 12 -2 66.69 4.40 3 12 -2 61.69 4.80 3 12 -2 62.09 4.70 -3 12 2 68.69 5.00 -3 12 2 62.59 3.90 -3 12 2 64.89 3.90 3 12 -2 67.59 5.00 -3 12 2 73.19 5.10 -3 12 2 63.99 4.60 2 -12 -2 32.80 3.50 -2 -12 2 31.90 3.60 -2 -12 2 31.00 3.30 2 -12 -2 27.10 2.90 -2 -12 2 28.90 2.00 2 -12 -2 25.50 3.60 2 -12 -2 28.60 3.70 -2 12 2 33.20 3.40 2 12 -2 30.00 3.70 -2 12 2 30.30 2.50 -2 12 2 25.30 3.20 2 12 -2 29.70 3.10 -2 12 2 28.90 2.40 -2 12 2 33.40 3.60 2 12 -2 28.50 3.20 1 -12 -2 155.78 7.20 -1 -12 2 150.68 7.30 -1 -12 2 145.69 4.70 1 -12 -2 154.98 6.20 -1 -12 2 148.29 6.80 1 -12 -2 148.89 7.00 1 -12 -2 148.89 7.40 -1 12 2 156.78 7.00 -1 12 2 153.18 7.20 1 12 -2 163.18 6.90 -1 12 2 150.78 5.10 1 12 -2 150.68 6.90 -1 12 2 156.18 7.30 -1 12 2 143.29 6.10 1 12 -2 152.58 7.40 -1 12 2 143.89 5.00 0 -12 -2 206.48 8.60 0 -12 2 218.98 6.30 0 -12 2 234.08 9.30 0 -12 2 215.38 9.20 0 -12 -2 227.78 8.80 0 -12 -2 227.78 7.90 0 -12 2 222.28 8.70 0 -12 -2 227.78 9.20 0 12 -2 216.98 8.70 0 12 -2 218.18 9.00 0 12 2 220.38 8.30 0 12 -2 216.28 6.50 0 12 2 222.18 9.00 0 12 -2 239.38 7.30 0 12 2 222.98 8.50 0 12 -2 233.88 9.10 0 12 2 226.78 9.20 -1 -12 -2 2004.50 46.90 1 -12 2 1935.91 48.50 -1 -12 -2 1911.01 49.10 1 -12 2 2010.40 49.00 -1 -12 -2 2028.70 48.40 -1 -12 -2 2012.10 48.70 1 -12 2 1975.90 45.10 1 -12 2 2011.90 48.30 -1 12 -2 1989.40 48.50 -1 12 -2 1932.01 45.80 1 12 2 1993.80 49.00 -1 12 -2 2005.80 48.50 1 12 2 1996.00 47.40 -1 12 -2 1995.50 45.80 1 12 2 1966.20 48.00 1 12 2 1928.81 48.50 -2 -12 -2 9.20 2.00 2 -12 2 5.30 2.10 2 -12 2 5.80 2.30 -2 -12 -2 5.10 2.20 2 -12 2 3.50 2.40 -2 -12 -2 6.70 1.70 -2 -12 -2 5.30 2.10 2 -12 2 6.90 1.40 2 -12 2 12.30 2.40 -2 12 -2 11.10 2.60 2 12 2 5.70 2.20 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5.30 2.40 5 13 3 5.20 2.60 -5 13 -3 6.30 2.00 5 13 3 6.00 2.70 -5 13 -3 9.80 3.00 -5 13 -3 6.50 2.50 -6 -13 -3 25.50 4.10 6 -13 3 26.90 4.80 -6 -13 -3 27.00 3.90 6 -13 3 26.90 4.30 -6 -13 -3 20.80 4.30 6 13 3 33.00 4.00 -6 13 -3 16.70 3.70 6 13 3 26.30 4.00 -6 13 -3 27.80 4.10 6 13 3 23.10 4.60 -6 13 -3 12.60 3.50 -7 -13 -3 510.95 18.60 -7 -13 -3 484.25 18.10 7 -13 3 525.85 18.20 7 -13 3 510.65 18.60 -7 13 -3 501.65 17.60 7 13 3 516.05 18.70 -7 13 -3 511.35 18.20 7 13 3 515.45 17.00 -7 13 -3 537.55 17.80 8 -13 3 0.60 2.90 -8 -13 -3 4.70 3.00 8 -13 3 7.70 4.00 -8 -13 -3 -0.10 2.80 -8 13 -3 1.50 2.50 8 13 3 0.00 3.30 8 13 3 2.20 2.30 -8 13 -3 5.80 3.30 -8 13 -3 0.60 2.80 -9 -13 -3 54.39 5.60 9 -13 3 42.40 6.00 9 -13 3 30.60 5.20 -9 13 -3 42.30 5.50 -9 13 -3 28.80 5.80 -9 13 -3 52.79 6.10 -9 -14 3 -1.80 3.10 9 -14 -3 1.40 3.40 9 -14 -3 5.80 3.90 -9 -14 3 1.00 3.20 -9 14 3 2.60 2.90 -9 14 3 1.30 3.50 8 -14 -3 97.89 7.80 8 -14 -3 76.89 7.00 -8 -14 3 78.39 7.10 -8 -14 3 81.39 6.80 -8 14 3 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36.70 5.50 -7 15 -3 36.90 5.10 7 15 3 44.90 5.70 7 15 3 49.60 5.10 7 15 3 37.90 5.70 -7 15 -3 37.70 5.40 -8 -15 -3 2.50 3.10 8 -15 3 5.80 3.90 8 -15 3 1.60 3.10 -8 15 -3 -0.80 2.80 -8 15 -3 3.50 3.30 8 15 3 3.40 2.80 -8 15 -3 1.60 3.00 8 15 3 1.80 3.30 -8 -16 3 15.80 4.40 8 -16 -3 13.30 4.00 -8 16 3 7.40 4.10 8 16 -3 17.10 5.20 -8 16 3 12.20 4.40 8 16 -3 10.40 2.60 -7 -16 3 16.90 4.70 7 -16 -3 10.00 3.70 -7 -16 3 18.70 3.90 7 16 -3 17.10 3.50 -7 16 3 15.90 4.00 7 16 -3 9.70 4.50 6 -16 -3 334.97 14.70 -6 -16 3 336.37 13.80 -6 -16 3 332.07 14.70 -6 16 3 342.17 14.70 6 16 -3 340.97 14.40 6 16 -3 339.17 12.20 -5 -16 3 7.00 2.90 -5 -16 3 10.80 3.50 5 -16 -3 18.70 4.50 5 16 -3 8.90 3.60 -5 16 3 9.50 3.00 -5 16 3 12.70 3.30 5 16 -3 9.00 2.40 4 -16 -3 9.80 3.30 -4 -16 3 10.40 3.30 -4 -16 3 11.80 3.30 4 -16 -3 6.60 3.30 -4 16 3 7.80 2.60 -4 16 3 6.90 2.90 4 16 -3 7.60 2.90 4 16 -3 10.30 2.70 3 -16 -3 -0.90 2.50 -3 -16 3 2.20 2.50 -3 -16 3 4.00 2.40 3 -16 -3 2.10 2.50 -3 16 3 3.50 2.20 3 16 -3 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4 3.40 1.30 -6 4 4 5.70 2.00 -6 4 4 3.30 1.10 6 4 -4 4.40 0.80 6 4 -4 5.20 1.90 5 -4 -4 107.49 5.30 -5 -4 4 100.09 4.80 5 -4 -4 97.89 5.10 -5 -4 4 89.49 4.50 -5 -4 4 97.29 4.50 -5 -4 4 92.79 4.60 5 -4 -4 92.59 4.40 5 -4 -4 100.89 4.40 5 -4 -4 89.49 4.70 -5 -4 4 96.19 4.20 5 -4 -4 98.39 4.40 -5 -4 4 103.39 4.70 -5 -4 4 99.69 4.30 5 -4 -4 95.79 4.00 -5 -4 4 93.29 4.90 -5 4 4 96.49 4.90 -5 4 4 99.89 5.00 5 4 -4 101.49 4.60 5 4 -4 100.99 4.70 -5 4 4 95.79 4.30 -5 4 4 96.29 3.90 -5 4 4 98.39 4.20 -4 -4 4 48.00 2.80 4 -4 -4 44.50 3.10 4 -4 -4 42.80 2.90 -4 -4 4 42.10 2.50 4 -4 -4 42.10 2.40 -4 -4 4 45.70 2.70 -4 -4 4 46.00 2.70 -4 -4 4 44.10 2.90 -4 -4 4 45.20 2.60 4 -4 -4 44.40 3.20 4 -4 -4 45.30 2.80 -4 -4 4 42.80 2.90 4 -4 -4 42.50 2.50 -4 4 4 42.10 3.00 -4 4 4 38.20 2.50 4 4 -4 44.40 3.00 -4 4 4 40.70 2.90 -4 4 4 39.90 2.40 4 4 -4 41.70 2.80 -4 4 4 39.90 2.90 -4 4 4 43.80 3.00 -4 4 4 44.30 3.00 -4 4 4 39.50 2.50 -4 4 4 45.00 2.60 4 4 -4 41.90 2.90 4 4 -4 42.90 2.70 3 -4 -4 135.99 5.20 3 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107.19 5.90 6 6 4 109.69 6.30 6 6 4 108.29 5.00 -6 6 -4 118.49 5.70 6 6 4 114.09 6.30 -6 6 -4 122.39 6.00 -6 6 -4 122.79 6.30 -7 -6 -4 53.89 4.90 7 -6 4 51.19 4.60 -7 -6 -4 64.89 5.00 7 -6 4 47.50 4.50 -7 -6 -4 56.79 3.70 7 -6 4 54.29 3.80 7 -6 4 57.99 5.10 -7 -6 -4 56.89 3.70 -7 6 -4 61.39 4.80 7 6 4 54.49 4.20 -7 6 -4 57.09 4.30 7 6 4 56.49 4.90 -7 6 -4 59.39 4.60 7 6 4 52.99 4.90 -7 6 -4 64.89 5.20 -8 -6 -4 147.99 6.60 8 -6 4 159.58 8.60 -8 -6 -4 163.08 8.40 -8 -6 -4 159.68 8.50 8 -6 4 150.98 8.10 -8 -6 -4 154.78 6.80 8 -6 4 150.68 8.10 8 6 4 165.78 8.40 8 6 4 156.48 7.40 -8 6 -4 148.49 8.10 -8 6 -4 179.28 8.30 8 6 4 152.48 8.50 -8 6 -4 167.88 7.60 -8 6 -4 149.69 8.20 -9 -6 -4 4.30 2.70 9 -6 4 4.40 2.70 9 -6 4 4.00 3.00 9 -6 4 4.00 2.50 -9 -6 -4 3.90 2.30 -9 6 -4 2.00 2.40 9 6 4 3.60 2.10 9 6 4 2.50 2.50 -9 6 -4 2.90 2.40 9 6 4 7.20 4.20 -9 6 -4 -0.70 2.20 -10 -6 -4 187.68 10.30 10 -6 4 191.28 10.50 10 -6 4 165.88 9.50 -10 -6 -4 183.18 10.20 10 -6 4 173.78 9.90 10 6 4 187.68 10.50 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-8 7 4 14.80 3.20 8 7 -4 17.90 3.50 8 7 -4 18.30 1.70 -7 -7 4 4.50 2.10 7 -7 -4 4.80 2.30 7 -7 -4 4.40 2.40 7 -7 -4 7.70 2.50 -7 -7 4 5.70 1.80 -7 -7 4 7.30 1.80 -7 -7 4 5.20 2.30 7 -7 -4 5.30 2.00 -7 7 4 6.00 2.30 7 7 -4 8.40 2.60 7 7 -4 5.30 1.60 -7 7 4 3.90 2.30 -7 7 4 7.10 1.60 7 7 -4 4.90 2.00 7 7 -4 5.20 1.00 -7 7 4 5.80 2.30 -6 -7 4 16.80 3.00 -6 -7 4 21.10 2.50 -6 -7 4 17.00 2.40 6 -7 -4 17.60 3.10 6 -7 -4 17.60 3.50 6 -7 -4 17.80 2.70 6 -7 -4 17.40 3.30 -6 -7 4 14.50 3.10 -6 7 4 13.50 3.00 -6 7 4 20.10 2.50 6 7 -4 19.40 1.80 -6 7 4 13.30 2.80 6 7 -4 15.70 3.00 6 7 -4 26.30 3.50 6 7 -4 16.80 1.70 -6 7 4 17.00 3.50 5 -7 -4 883.51 23.80 5 -7 -4 884.41 23.70 5 -7 -4 874.91 23.50 5 -7 -4 902.51 22.50 -5 -7 4 833.62 22.00 -5 -7 4 830.72 21.40 -5 -7 4 862.31 22.40 -5 -7 4 875.11 21.70 -5 -7 4 864.91 24.50 -5 -7 4 878.21 22.40 5 -7 -4 825.12 21.90 5 7 -4 894.71 23.50 -5 7 4 844.52 22.20 -5 7 4 855.21 22.80 -5 7 4 876.21 22.20 -5 7 4 879.31 23.40 -5 7 4 889.01 23.90 5 7 -4 886.01 20.80 5 7 -4 899.11 22.40 -5 7 4 900.41 23.50 5 7 -4 868.61 20.70 5 7 -4 897.41 23.60 -4 -7 4 3.40 1.40 -4 -7 4 2.20 1.20 4 -7 -4 1.00 1.30 4 -7 -4 1.90 1.10 -4 -7 4 3.40 1.20 -4 -7 4 3.90 1.00 4 -7 -4 1.90 1.30 4 -7 -4 1.40 1.30 4 -7 -4 2.60 1.40 4 -7 -4 3.60 1.50 -4 -7 4 2.70 1.00 -4 -7 4 3.70 0.90 -4 -7 4 2.60 1.50 -4 7 4 -0.50 1.10 -4 7 4 1.70 1.20 4 7 -4 2.80 0.90 4 7 -4 2.20 1.40 4 7 -4 2.30 1.00 4 7 -4 3.10 1.40 -4 7 4 4.50 1.60 4 7 -4 2.20 0.80 -4 7 4 1.60 1.30 -4 7 4 3.80 1.50 -4 7 4 1.30 1.20 4 7 -4 1.30 1.00 -3 -7 4 32.50 2.80 3 -7 -4 32.80 2.80 3 -7 -4 34.90 2.90 3 -7 -4 38.70 2.80 -3 -7 4 34.50 2.90 -3 -7 4 34.70 1.50 3 -7 -4 34.40 2.70 3 -7 -4 35.40 1.50 3 -7 -4 35.10 3.00 3 -7 -4 29.90 2.70 3 -7 -4 34.20 2.50 -3 -7 4 36.40 2.00 -3 -7 4 32.10 2.80 -3 -7 4 35.90 2.80 -3 -7 4 35.00 2.00 -3 -7 4 38.40 2.10 -3 -7 4 31.80 2.40 -3 -7 4 36.60 2.90 -3 -7 4 33.40 1.90 -3 -7 4 38.40 1.50 3 7 -4 39.80 2.70 -3 7 4 29.60 2.50 -3 7 4 32.80 2.20 3 7 -4 37.80 2.00 -3 7 4 34.00 2.80 3 7 -4 36.50 2.10 -3 7 4 36.30 2.70 3 7 -4 36.20 2.10 -3 7 4 35.50 2.90 3 7 -4 35.10 2.10 -3 7 4 32.70 2.90 -3 7 4 31.10 2.50 3 7 -4 35.70 3.00 -3 7 4 31.80 2.90 2 -7 -4 14.50 2.00 -2 -7 4 16.20 2.10 2 -7 -4 18.10 2.30 -2 -7 4 16.80 1.40 2 -7 -4 16.50 1.40 -2 -7 4 15.60 1.70 -2 -7 4 17.60 1.10 -2 -7 4 14.80 1.40 -2 -7 4 13.60 1.10 2 -7 -4 14.60 1.90 -2 -7 4 13.80 1.30 2 -7 -4 15.60 1.70 -2 -7 4 15.10 1.90 2 -7 -4 16.90 1.90 -2 -7 4 12.50 1.90 -2 -7 4 14.00 2.00 2 -7 -4 13.40 2.10 2 -7 -4 15.50 2.20 -2 -7 4 14.80 1.50 2 7 -4 11.10 1.80 2 7 -4 14.70 1.60 -2 7 4 19.20 1.40 2 7 -4 14.70 1.40 -2 7 4 16.10 1.60 -2 7 4 15.90 2.00 -2 7 4 17.30 1.90 -2 7 4 14.30 2.00 2 7 -4 14.10 1.70 -2 7 4 15.20 1.80 2 7 -4 14.10 2.10 -2 7 4 15.70 1.90 -2 7 4 14.50 1.90 2 7 -4 18.80 2.00 2 7 -4 10.70 1.30 -2 7 4 12.90 2.00 1 -7 -4 1989.40 46.50 -1 -7 4 1983.50 45.40 1 -7 -4 1971.80 45.10 1 -7 -4 1936.11 46.00 1 -7 -4 1991.70 46.50 -1 -7 4 1946.61 44.80 -1 -7 4 1983.80 47.30 1 -7 -4 1962.80 46.40 1 -7 -4 2029.60 45.40 -1 -7 4 1954.80 45.30 -1 -7 4 1990.70 45.50 -1 -7 4 1909.81 47.10 -1 -7 4 1953.60 46.50 -1 -7 4 1943.31 44.80 -1 -7 4 1995.90 46.60 -1 7 4 1979.90 46.40 -1 7 4 1975.40 45.20 -1 7 4 1977.60 46.50 -1 7 4 1976.50 46.10 1 7 -4 1965.20 46.50 -1 7 4 1987.20 46.50 1 7 -4 1983.00 44.90 -1 7 4 1924.51 44.90 1 7 -4 1974.10 44.90 1 7 -4 1869.31 45.50 -1 7 4 1965.20 45.00 -1 7 4 1955.40 45.90 1 7 -4 1903.71 45.20 1 7 -4 1949.10 45.70 -1 7 4 2069.39 47.50 1 7 -4 1942.91 46.20 1 7 -4 2006.10 47.70 0 -7 -4 54.99 2.30 0 -7 4 48.70 2.50 0 -7 -4 52.79 2.80 0 -7 -4 44.50 2.90 0 -7 4 49.00 3.00 0 -7 4 45.00 2.50 0 -7 -4 46.60 3.10 0 -7 4 51.29 3.30 0 -7 4 47.00 2.60 0 -7 4 46.80 3.50 0 -7 -4 48.40 2.70 0 -7 4 52.99 2.90 0 -7 4 47.30 2.90 0 -7 -4 46.10 3.00 0 -7 -4 48.30 2.70 0 -7 4 47.50 3.10 0 -7 -4 50.09 3.20 0 -7 -4 49.90 2.70 0 -7 4 45.90 2.90 0 7 -4 43.10 2.90 0 7 -4 46.70 2.40 0 7 -4 50.19 3.10 0 7 4 52.99 3.20 0 7 4 47.90 2.80 0 7 -4 52.69 3.20 0 7 -4 49.30 2.90 0 7 4 43.10 2.60 0 7 4 45.90 2.10 0 7 -4 52.39 3.60 0 7 4 57.49 3.00 0 7 4 50.39 2.20 0 7 -4 43.80 2.50 0 7 4 50.59 3.20 0 7 4 51.69 3.20 0 7 -4 49.20 2.60 1 -7 4 264.07 7.90 -1 -7 -4 230.08 8.00 1 -7 4 272.27 8.30 -1 -7 -4 269.67 8.30 1 -7 4 277.07 8.50 -1 -7 -4 261.17 8.50 -1 -7 -4 258.57 8.00 -1 -7 -4 266.87 6.80 1 -7 4 263.27 8.40 1 -7 4 267.57 8.40 -1 -7 -4 257.27 7.60 -1 -7 -4 262.37 8.50 -1 -7 -4 272.17 8.60 1 -7 4 245.48 7.70 -1 -7 -4 266.67 8.50 -1 -7 -4 258.97 8.00 1 -7 4 264.37 8.50 1 -7 4 267.37 8.80 1 7 4 219.08 8.00 1 7 4 262.47 7.70 -1 7 -4 255.67 8.40 1 7 4 270.37 8.60 1 7 4 269.97 8.70 1 7 4 257.67 6.70 1 7 4 263.87 8.60 -1 7 -4 259.27 7.80 -1 7 -4 248.68 8.40 1 7 4 267.87 6.80 -1 7 -4 257.37 7.70 -1 7 -4 260.27 8.50 1 7 4 257.67 8.30 1 7 4 261.37 8.10 -1 7 -4 237.18 8.10 -1 7 -4 262.77 8.60 -1 7 -4 266.17 8.60 2 -7 4 366.56 11.00 2 -7 4 364.56 10.50 -2 -7 -4 339.27 10.80 -2 -7 -4 374.66 9.10 -2 -7 -4 370.26 11.20 2 -7 4 356.76 11.50 -2 -7 -4 363.66 10.90 -2 -7 -4 372.36 11.00 2 -7 4 377.06 11.30 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5.90 2.80 -8 8 4 1.00 2.20 -8 8 4 4.30 2.40 8 8 -4 2.70 2.40 8 8 -4 3.80 1.20 8 8 -4 3.80 2.30 -7 -8 4 349.87 10.90 7 -8 -4 372.26 12.40 7 -8 -4 363.86 13.30 7 -8 -4 375.06 13.70 7 -8 -4 350.26 12.70 -7 -8 4 352.76 11.00 -7 -8 4 365.36 12.90 -7 -8 4 358.06 12.20 -7 8 4 375.66 13.40 7 8 -4 384.36 13.20 7 8 -4 355.76 9.80 7 8 -4 349.07 12.20 -7 8 4 365.96 13.20 -7 8 4 383.06 13.20 -6 -8 4 899.51 25.00 6 -8 -4 918.51 25.50 6 -8 -4 918.81 24.30 -6 -8 4 923.61 23.10 6 -8 -4 924.91 25.20 6 -8 -4 898.71 25.70 -6 -8 4 968.30 26.00 -6 -8 4 900.91 23.00 6 8 -4 917.71 22.10 6 8 -4 944.91 25.50 6 8 -4 916.51 22.20 -6 8 4 949.01 25.40 -6 8 4 919.11 23.40 6 8 -4 929.11 23.70 -6 8 4 957.20 25.60 -6 8 4 921.81 25.70 6 8 -4 898.51 24.80 -5 -8 4 90.99 4.50 5 -8 -4 96.79 5.50 -5 -8 4 87.99 4.60 5 -8 -4 97.89 5.60 5 -8 -4 95.19 5.70 -5 -8 4 96.19 4.60 -5 -8 4 90.69 5.10 -5 -8 4 90.79 4.00 5 -8 -4 89.59 4.70 -5 -8 4 90.69 5.60 -5 8 4 89.39 5.30 -5 8 4 83.09 5.50 -5 8 4 92.69 5.10 5 8 -4 95.19 5.60 -5 8 4 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5 739.23 17.60 2 -3 -5 732.43 18.50 2 -3 -5 728.83 18.80 2 -3 -5 738.83 18.40 -2 -3 5 741.33 18.30 -2 -3 5 768.12 16.90 -2 -3 5 735.43 18.20 2 -3 -5 743.13 18.40 2 -3 -5 777.02 18.50 -2 -3 5 753.22 18.30 2 3 -5 749.62 17.40 2 3 -5 748.93 18.40 -2 3 5 752.52 18.50 -2 3 5 768.62 18.80 2 3 -5 747.43 17.90 -2 3 5 743.43 17.50 -2 3 5 741.93 18.30 -2 3 5 747.13 16.80 -2 3 5 707.63 19.00 2 3 -5 753.32 17.50 -2 3 5 773.82 18.90 -2 3 5 737.53 18.20 -2 3 5 747.53 18.70 -2 3 5 751.32 18.30 2 3 -5 742.13 18.30 2 3 -5 741.33 18.70 1 -3 -5 1870.21 43.30 -1 -3 5 1913.01 43.90 -1 -3 5 1878.21 42.20 -1 -3 5 1858.11 43.70 -1 -3 5 1902.51 42.80 1 -3 -5 1891.71 43.80 1 -3 -5 1886.01 43.70 -1 -3 5 1911.71 43.40 -1 -3 5 1853.41 43.80 1 -3 -5 1906.01 43.50 -1 -3 5 1907.71 42.20 1 -3 -5 1878.91 43.40 -1 -3 5 1875.01 43.30 1 -3 -5 1854.61 43.00 1 -3 -5 1908.31 43.90 -1 -3 5 1910.61 42.80 -1 -3 5 1896.51 43.40 -1 -3 5 1877.21 42.60 1 -3 -5 1936.61 43.70 1 3 -5 1860.51 43.40 -1 3 5 1880.61 43.00 -1 3 5 1914.51 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161.48 7.50 -4 2 -9 171.38 6.40 4 2 9 152.78 7.20 -4 2 -9 169.68 7.20 4 2 9 172.38 6.50 -4 2 -9 161.68 7.20 -4 2 -9 157.18 7.30 -5 -2 -9 57.59 4.10 -5 -2 -9 54.19 4.10 -5 -2 -9 60.79 4.00 -5 -2 -9 56.99 4.60 5 -2 9 50.09 3.30 5 -2 9 50.39 4.50 5 -2 9 56.19 4.70 5 -2 9 48.70 4.40 -5 -2 -9 45.20 5.40 -5 2 -9 52.19 4.40 5 2 9 54.49 3.60 -5 2 -9 54.59 4.60 -5 2 -9 47.80 4.10 5 2 9 49.20 4.40 5 2 9 49.90 4.20 -5 2 -9 50.69 4.10 -5 2 -9 57.49 3.60 -6 -2 -9 5.80 2.00 -6 -2 -9 4.60 1.90 -6 -2 -9 6.70 2.30 6 -2 9 4.00 2.30 -6 -2 -9 5.90 2.70 6 -2 9 1.40 1.90 6 -2 9 5.90 2.40 -6 2 -9 3.80 2.00 6 2 9 8.60 2.70 -6 2 -9 6.00 1.70 -6 2 -9 3.00 2.20 6 2 9 3.40 2.10 -6 2 -9 5.40 2.20 6 2 9 10.00 2.70 7 -2 9 1.40 2.00 7 -2 9 0.90 1.90 -7 -2 -9 -2.50 1.70 -7 -2 -9 0.00 1.80 -7 -2 -9 -2.10 1.70 7 -2 9 1.50 2.10 -7 -2 -9 0.70 2.00 -7 2 -9 4.50 2.40 7 2 9 1.20 2.00 7 2 9 1.90 2.10 7 2 9 -1.10 1.90 -7 2 -9 2.20 2.30 -7 2 -9 -2.20 1.80 -8 -2 -9 241.38 10.90 8 -2 9 214.88 10.70 -8 -2 -9 235.08 10.00 -8 -2 -9 223.38 10.00 -8 -2 -9 222.48 10.00 8 -2 9 222.68 11.00 8 -2 9 239.78 10.30 -8 2 -9 223.58 10.40 -8 2 -9 225.58 10.40 8 2 9 215.18 10.60 -8 2 -9 230.98 15.20 8 2 9 218.98 10.90 8 2 9 217.08 11.20 -9 -2 -9 3.70 2.50 -9 -2 -9 -3.30 2.20 -9 -2 -9 4.10 2.50 9 -2 9 1.60 2.90 -9 -2 -9 -1.00 2.70 9 -2 9 2.00 2.90 9 -2 9 2.60 2.80 9 2 9 2.30 2.70 -9 2 -9 2.00 2.60 -9 2 -9 -0.50 2.80 9 2 9 2.20 2.50 9 2 9 -1.80 2.60 -9 2 -9 4.10 3.00 10 -2 9 15.00 3.70 -10 -2 -9 20.50 4.90 -10 -2 -9 10.00 3.80 -10 -2 -9 17.90 4.50 -10 -2 -9 18.00 3.70 10 -2 9 15.70 4.20 -10 2 -9 17.60 4.40 -10 2 -9 21.80 4.50 10 2 9 29.80 4.90 10 2 9 24.40 4.60 -10 2 -9 12.10 3.80 10 2 9 15.20 3.50 -11 -3 9 67.59 6.80 -11 -3 9 72.49 6.40 11 -3 -9 82.29 7.10 -11 -3 9 78.59 6.70 11 -3 -9 72.49 4.80 -11 3 9 66.99 6.80 -11 3 9 76.39 6.50 -11 3 9 57.39 6.90 -10 -3 9 17.30 3.80 -10 -3 9 9.20 3.00 10 -3 -9 13.50 2.90 -10 -3 9 14.80 3.80 -10 -3 9 13.90 4.30 10 -3 -9 10.90 3.40 -10 3 9 10.80 3.50 -10 3 9 10.40 3.30 -10 3 9 12.60 3.40 -9 -3 9 3.50 2.40 -9 -3 9 5.30 2.40 9 -3 -9 0.20 2.20 9 -3 -9 4.50 2.30 9 -3 -9 5.50 1.80 -9 3 9 0.70 2.40 -9 3 9 2.90 2.30 -9 3 9 9.90 3.30 -8 -3 9 8.50 2.70 8 -3 -9 12.10 3.40 -8 -3 9 11.70 2.70 8 -3 -9 8.90 1.90 8 -3 -9 9.80 2.80 -8 -3 9 11.20 2.60 -8 -3 9 11.30 2.60 -8 3 9 11.50 3.10 -8 3 9 5.50 2.60 -8 3 9 6.50 2.20 7 -3 -9 2.20 2.30 -7 -3 9 2.30 1.80 7 -3 -9 5.90 2.30 -7 -3 9 4.20 1.90 7 -3 -9 2.90 1.50 -7 -3 9 0.90 1.90 -7 3 9 7.10 2.50 -7 3 9 6.30 2.00 7 3 -9 6.40 2.60 -7 3 9 6.10 2.30 6 -3 -9 8.40 2.70 6 -3 -9 10.60 2.00 -6 -3 9 15.80 2.40 6 -3 -9 10.60 2.80 -6 -3 9 10.50 2.60 6 -3 -9 10.10 2.40 6 3 -9 8.20 2.20 -6 3 9 11.50 2.50 6 3 -9 10.80 2.60 -6 3 9 4.20 2.20 5 -3 -9 238.38 9.10 -5 -3 9 222.78 8.40 -5 -3 9 222.58 7.60 -5 -3 9 211.98 7.60 5 -3 -9 229.68 8.40 5 -3 -9 222.68 9.20 -5 -3 9 234.08 9.10 5 -3 -9 226.88 7.90 -5 -3 9 222.58 7.70 -5 3 9 220.08 7.90 5 3 -9 229.68 8.50 5 3 -9 225.38 8.60 -5 3 9 229.18 6.70 5 3 -9 238.68 6.40 -5 3 9 226.58 9.10 -5 3 9 216.78 9.20 5 3 -9 232.68 6.30 5 3 -9 230.18 8.70 4 -3 -9 2010.00 47.00 4 -3 -9 1956.40 46.80 -4 -3 9 1876.61 45.80 4 -3 -9 1998.60 46.90 -4 -3 9 1994.90 47.00 -4 -3 9 1872.41 46.20 -4 -3 9 2102.49 48.90 4 -3 -9 2038.40 48.40 4 -3 -9 2007.30 48.00 -4 -3 9 2032.80 48.40 -4 -3 9 1993.20 47.50 4 -3 -9 1986.10 48.10 -4 -3 9 2004.10 46.40 -4 3 9 1956.40 46.70 4 3 -9 1980.40 47.10 4 3 -9 1960.80 49.10 -4 3 9 1983.10 48.30 4 3 -9 2011.00 45.40 4 3 -9 2007.60 47.60 -4 3 9 1999.50 45.70 4 3 -9 1986.70 45.30 -4 3 9 1982.20 48.10 -4 3 9 1939.01 46.00 -3 -3 9 250.27 7.70 -3 -3 9 251.07 8.70 3 -3 -9 242.08 7.90 -3 -3 9 243.18 6.90 -3 -3 9 246.18 6.30 -3 -3 9 242.18 9.60 -3 -3 9 245.78 7.90 3 -3 -9 248.88 9.10 3 -3 -9 254.87 8.40 3 -3 -9 240.88 7.50 3 -3 -9 247.18 8.70 3 -3 -9 235.18 9.00 -3 -3 9 234.38 7.50 -3 3 9 242.18 7.80 3 3 -9 249.38 8.60 -3 3 9 254.17 7.90 -3 3 9 263.27 9.10 -3 3 9 249.38 7.70 3 3 -9 246.68 8.50 3 3 -9 249.97 7.40 3 3 -9 251.57 8.10 2 -3 -9 454.95 13.50 -2 -3 9 445.56 10.50 2 -3 -9 431.46 12.20 -2 -3 9 439.16 12.10 -2 -3 9 460.75 11.70 2 -3 -9 440.56 12.90 2 -3 -9 448.06 12.90 -2 -3 9 440.86 13.00 -2 -3 9 458.55 12.20 2 -3 -9 472.95 13.40 2 -3 -9 444.06 12.10 -2 -3 9 455.95 13.30 -2 -3 9 457.65 13.70 2 -3 -9 455.15 13.20 -2 3 9 445.66 12.40 2 3 -9 446.66 12.20 2 3 -9 432.56 12.90 2 3 -9 463.65 12.40 2 3 -9 471.55 13.30 -2 3 9 411.56 12.90 -2 3 9 439.36 12.60 -2 3 9 433.36 13.20 2 3 -9 441.96 13.50 -2 3 9 441.86 11.90 -2 3 9 469.35 13.50 -2 3 9 449.95 13.60 -1 -3 9 17.60 2.40 -1 -3 9 14.70 1.80 -1 -3 9 12.20 2.10 1 -3 -9 13.20 2.40 -1 -3 9 12.90 2.20 1 -3 -9 15.00 2.30 -1 -3 9 17.90 2.00 -1 -3 9 15.50 2.30 1 -3 -9 14.00 2.00 1 -3 -9 17.90 2.30 1 -3 -9 15.10 1.70 -1 -3 9 10.60 1.50 -1 -3 9 13.40 1.90 1 -3 -9 11.90 2.00 1 -3 -9 17.20 2.20 1 -3 -9 16.50 2.10 -1 -3 9 12.20 1.80 -1 3 9 11.70 1.90 1 3 -9 16.40 2.00 -1 3 9 13.10 2.20 -1 3 9 15.10 2.30 -1 3 9 10.00 2.00 1 3 -9 15.40 2.20 -1 3 9 11.80 2.00 -1 3 9 11.30 1.50 1 3 -9 10.60 2.00 1 3 -9 16.20 1.80 -1 3 9 12.00 2.00 1 3 -9 12.80 1.70 1 3 -9 15.00 2.30 1 3 -9 12.20 1.80 -1 3 9 9.50 1.90 1 3 -9 15.10 2.20 -1 3 9 15.80 2.10 0 -3 -9 154.58 6.60 0 -3 9 152.28 5.30 0 -3 9 149.99 5.80 0 -3 9 154.58 6.20 0 -3 9 159.68 6.60 0 -3 -9 125.09 5.90 0 -3 -9 152.68 6.00 0 -3 9 156.58 5.80 0 -3 -9 153.88 4.60 0 -3 9 156.48 6.20 0 -3 -9 140.39 5.90 0 -3 -9 151.98 5.20 0 -3 -9 153.78 6.10 0 -3 9 160.08 5.90 0 -3 -9 151.78 6.30 0 -3 9 159.88 6.50 0 -3 -9 160.08 6.40 0 3 -9 157.88 6.20 0 3 9 157.78 6.30 0 3 -9 158.38 5.40 0 3 9 151.48 5.10 0 3 9 155.48 6.00 0 3 -9 147.59 6.20 0 3 -9 156.38 6.30 0 3 -9 143.69 5.90 0 3 9 154.78 6.50 0 3 9 149.29 5.80 0 3 -9 151.18 6.10 0 3 -9 166.38 6.30 0 3 9 165.28 6.30 0 3 -9 148.79 5.40 0 3 9 157.68 6.20 0 3 9 153.08 6.20 0 3 9 169.88 6.10 1 -3 9 63.49 4.20 1 -3 9 66.39 3.90 -1 -3 -9 65.69 4.10 1 -3 9 67.99 3.90 -1 -3 -9 73.69 3.90 -1 -3 -9 62.79 3.90 -1 -3 -9 66.99 3.20 1 -3 9 68.79 3.90 1 -3 9 69.29 3.30 -1 -3 -9 73.39 4.30 1 -3 9 69.89 4.10 -1 -3 -9 71.69 4.20 -1 -3 -9 76.09 3.30 1 -3 9 70.19 3.90 -1 -3 -9 71.29 4.30 -1 -3 -9 64.69 3.80 1 -3 9 66.99 3.80 1 3 9 74.59 3.60 -1 3 -9 64.59 3.90 -1 3 -9 73.49 4.10 1 3 9 69.29 3.80 -1 3 -9 72.09 3.70 1 3 9 75.19 3.20 1 3 9 71.59 4.20 -1 3 -9 70.69 3.40 1 3 9 71.59 4.30 1 3 9 70.79 3.50 -1 3 -9 69.69 4.20 1 3 9 67.69 4.00 1 3 9 74.29 4.20 1 3 9 69.29 3.20 -1 3 -9 75.29 4.20 -1 3 -9 69.69 4.00 -2 -3 -9 12.10 2.10 2 -3 9 8.70 1.90 -2 -3 -9 5.40 1.60 2 -3 9 10.70 2.10 -2 -3 -9 11.10 2.40 2 -3 9 8.00 1.70 2 -3 9 10.10 2.00 2 -3 9 10.90 2.20 -2 -3 -9 11.50 2.30 2 -3 9 11.60 2.00 -2 -3 -9 9.80 1.90 -2 -3 -9 8.90 1.70 2 -3 9 11.60 2.20 -2 -3 -9 11.30 1.80 -2 -3 -9 5.90 1.60 2 3 9 6.00 1.80 2 3 9 8.50 1.90 2 3 9 11.10 2.30 2 3 9 11.20 2.10 -2 3 -9 11.60 2.20 -2 3 -9 10.70 2.10 -2 3 -9 8.70 1.80 -2 3 -9 8.00 1.20 2 3 9 8.20 2.50 -2 3 -9 12.00 2.50 -2 3 -9 10.00 2.10 -2 3 -9 8.90 2.00 2 3 9 8.40 1.50 2 3 9 10.50 1.80 -2 3 -9 7.30 1.90 3 -3 9 4.80 1.70 3 -3 9 5.00 1.50 3 -3 9 6.10 2.20 -3 -3 -9 6.70 1.80 -3 -3 -9 6.40 1.60 3 -3 9 3.30 1.60 -3 -3 -9 6.60 1.90 -3 -3 -9 5.20 1.50 -3 -3 -9 8.80 1.90 -3 -3 -9 7.00 2.10 3 -3 9 6.50 1.70 -3 -3 -9 4.90 1.50 -3 -3 -9 3.50 1.70 3 -3 9 5.10 1.80 3 -3 9 4.80 2.00 -3 3 -9 5.70 1.80 3 3 9 5.40 1.80 -3 3 -9 6.80 1.90 3 3 9 7.80 1.90 3 3 9 5.10 1.80 -3 3 -9 5.20 1.60 3 3 9 3.10 1.80 -3 3 -9 6.10 1.70 -3 3 -9 6.90 2.00 3 3 9 5.70 1.70 -3 3 -9 7.40 1.90 4 -3 9 61.79 3.70 -4 -3 -9 61.99 3.80 4 -3 9 61.39 4.80 -4 -3 -9 63.69 4.50 4 -3 9 66.59 4.70 -4 -3 -9 62.39 4.00 -4 -3 -9 58.19 3.80 -4 -3 -9 60.99 4.00 -4 -3 -9 57.89 4.50 -4 -3 -9 58.19 4.40 4 -3 9 59.89 4.70 -4 3 -9 64.79 3.90 -4 3 -9 64.59 4.40 -4 3 -9 66.29 4.40 4 3 9 58.89 2.90 4 3 9 63.89 4.60 4 3 9 57.99 4.60 4 3 9 64.59 3.90 -4 3 -9 64.19 4.00 -4 3 -9 63.89 4.50 -5 -3 -9 7.40 2.00 5 -3 9 6.40 2.40 5 -3 9 2.60 2.10 -5 -3 -9 7.20 2.00 5 -3 9 7.40 2.50 -5 -3 -9 8.90 2.20 -5 -3 -9 3.20 1.80 -5 3 -9 7.20 2.40 5 3 9 4.70 2.10 -5 3 -9 6.10 2.30 5 3 9 3.00 1.90 5 3 9 8.60 2.20 5 3 9 6.80 1.80 -5 3 -9 11.30 2.10 -5 3 -9 9.10 2.50 -5 3 -9 7.50 2.10 6 -3 9 130.19 7.30 -6 -3 -9 128.29 6.50 -6 -3 -9 123.79 6.40 6 -3 9 136.89 7.20 6 -3 9 125.19 7.50 -6 -3 -9 124.19 6.30 -6 -3 -9 127.89 7.20 -6 3 -9 127.59 6.90 6 3 9 148.39 7.80 6 3 9 123.19 7.10 -6 3 -9 131.49 6.80 -6 3 -9 138.19 7.20 6 3 9 134.09 7.30 -6 3 -9 128.89 5.70 7 -3 9 42.90 4.50 -7 -3 -9 37.70 4.20 -7 -3 -9 44.00 4.20 -7 -3 -9 41.60 4.10 -7 -3 -9 41.70 4.80 7 -3 9 45.40 5.10 7 -3 9 45.10 4.90 7 3 9 43.70 4.70 7 3 9 41.80 4.80 -7 3 -9 43.20 4.60 -7 3 -9 41.10 4.40 7 3 9 44.40 4.90 -7 3 -9 41.10 4.60 -8 -3 -9 11.80 3.20 -8 -3 -9 22.40 3.90 8 -3 9 9.80 3.30 8 -3 9 15.30 3.80 -8 -3 -9 12.30 3.20 8 -3 9 16.60 3.50 -8 -3 -9 13.60 3.50 -8 3 -9 14.80 3.70 8 3 9 11.40 3.20 -8 3 -9 15.10 3.70 8 3 9 20.40 4.20 8 3 9 14.60 3.40 -8 3 -9 18.20 4.00 -9 -3 -9 234.18 11.60 9 -3 9 204.98 11.20 -9 -3 -9 221.88 10.10 -9 -3 -9 205.78 9.90 9 -3 9 234.18 11.40 9 -3 9 212.18 10.60 -9 -3 -9 219.48 10.50 -9 3 -9 222.88 11.00 9 3 9 221.18 11.10 -9 3 -9 235.48 11.00 9 3 9 210.48 11.20 -9 3 -9 216.68 10.60 9 3 9 218.48 10.90 -10 -3 -9 39.30 5.00 10 -3 9 45.70 6.30 -10 -3 -9 42.40 5.80 -10 -3 -9 40.80 6.10 10 -3 9 28.60 5.00 10 3 9 45.00 6.10 -10 3 -9 42.60 5.70 -10 3 -9 38.70 5.90 10 3 9 35.40 5.20 10 3 9 48.90 5.90 -10 3 -9 48.00 5.60 -11 -4 9 40.30 5.60 11 -4 -9 32.20 3.90 -11 -4 9 33.30 5.00 -11 -4 9 43.60 5.50 11 -4 -9 39.90 5.60 -11 4 9 25.80 4.90 -11 4 9 39.60 5.70 -11 4 9 36.70 5.50 10 -4 -9 42.20 3.80 -10 -4 9 40.90 4.90 -10 -4 9 34.40 5.20 10 -4 -9 41.70 5.40 -10 -4 9 38.20 4.90 -10 4 9 39.90 5.70 -10 4 9 42.50 5.40 -10 4 9 40.10 5.40 -9 -4 9 44.00 4.90 9 -4 -9 59.79 5.90 -9 -4 9 49.10 4.90 9 -4 -9 62.19 8.40 9 -4 -9 53.59 4.10 -9 -4 9 45.70 4.70 -9 4 9 55.69 5.50 -9 4 9 54.49 5.50 -9 4 9 38.20 4.90 -8 -4 9 17.00 3.30 8 -4 -9 16.50 2.60 -8 -4 9 11.50 2.70 -8 -4 9 12.40 2.70 8 -4 -9 18.60 3.70 -8 -4 9 12.00 2.80 8 -4 -9 12.60 3.30 -8 4 9 18.00 2.90 -8 4 9 20.30 3.70 -8 4 9 18.30 3.60 -7 -4 9 213.78 9.00 -7 -4 9 224.28 9.10 -7 -4 9 205.58 8.50 7 -4 -9 205.08 9.70 7 -4 -9 216.88 9.20 7 -4 -9 207.68 8.00 -7 -4 9 217.88 8.50 -7 4 9 213.98 9.60 -7 4 9 209.68 8.40 7 4 -9 218.38 9.00 -7 4 9 211.78 9.50 -6 -4 9 298.87 10.10 6 -4 -9 289.67 11.40 -6 -4 9 296.17 10.50 6 -4 -9 286.67 10.70 -6 -4 9 307.57 11.10 6 -4 -9 291.57 9.90 -6 4 9 292.67 11.30 6 4 -9 307.07 10.70 -6 4 9 304.17 10.50 -5 -4 9 683.93 19.20 5 -4 -9 715.13 19.40 5 -4 -9 717.53 20.90 -5 -4 9 708.33 20.50 -5 -4 9 692.13 20.00 -5 -4 9 692.13 19.00 -5 -4 9 721.93 19.30 5 -4 -9 731.83 21.60 5 -4 -9 736.33 20.60 5 4 -9 737.03 17.10 5 4 -9 751.52 17.10 -5 4 9 709.73 17.20 -5 4 9 709.73 20.00 5 4 -9 762.22 20.20 5 4 -9 723.83 19.70 5 4 -9 730.33 20.00 -5 4 9 754.52 21.00 -4 -4 9 2749.23 68.79 4 -4 -9 2952.20 68.99 4 -4 -9 2956.30 69.49 4 -4 -9 2989.30 68.29 4 -4 -9 2980.70 69.19 -4 -4 9 2982.30 69.49 4 -4 -9 2961.20 68.19 -4 -4 9 2875.21 67.69 -4 -4 9 2988.50 67.79 4 -4 -9 3054.99 70.29 -4 -4 9 2911.61 68.89 -4 -4 9 2774.62 66.79 -4 -4 9 2982.40 66.89 -4 4 9 2895.61 67.99 -4 4 9 2936.71 66.39 4 4 -9 2970.00 69.19 -4 4 9 2834.42 67.39 4 4 -9 2962.50 68.49 -4 4 9 2998.90 69.49 4 4 -9 3021.70 67.99 4 4 -9 2985.60 66.29 4 4 -9 2962.30 66.29 -4 4 9 2851.21 70.49 -3 -4 9 606.64 17.90 -3 -4 9 614.34 15.20 3 -4 -9 683.73 21.60 3 -4 -9 611.64 16.70 3 -4 -9 600.84 15.70 3 -4 -9 602.94 16.90 -3 -4 9 626.24 15.20 -3 -4 9 624.34 17.50 -3 -4 9 616.64 16.30 3 -4 -9 619.84 17.30 -3 -4 9 633.04 16.50 -3 -4 9 588.64 16.00 3 -4 -9 634.84 17.90 -3 4 9 600.94 16.50 -3 4 9 610.64 17.80 3 4 -9 620.84 17.70 3 4 -9 628.94 15.80 -3 4 9 601.94 17.40 -3 4 9 632.54 18.70 3 4 -9 615.04 17.10 3 4 -9 615.14 16.30 3 4 -9 636.94 15.80 -3 4 9 630.84 15.80 3 4 -9 625.94 17.10 -2 -4 9 1132.19 28.70 2 -4 -9 1151.88 28.40 -2 -4 9 1093.39 29.00 2 -4 -9 1097.49 27.10 2 -4 -9 1138.79 28.20 2 -4 -9 1143.59 27.40 2 -4 -9 1106.19 28.70 -2 -4 9 1142.69 25.40 -2 -4 9 1112.09 25.40 2 -4 -9 1089.09 28.00 -2 -4 9 1101.29 26.40 -2 -4 9 1090.99 26.70 -2 -4 9 1097.49 29.00 -2 -4 9 1146.39 27.50 2 -4 -9 1114.09 28.20 -2 4 9 1143.09 28.80 -2 4 9 1126.09 27.90 -2 4 9 1122.99 27.20 2 4 -9 1121.49 28.90 -2 4 9 1170.68 28.70 2 4 -9 1133.39 28.10 2 4 -9 1149.69 28.20 2 4 -9 1116.39 27.00 2 4 -9 1083.09 27.30 -2 4 9 1133.59 27.30 1 -4 -9 6.30 1.60 -1 -4 9 7.90 2.00 -1 -4 9 5.90 1.20 1 -4 -9 6.00 1.50 -1 -4 9 9.90 2.10 1 -4 -9 6.20 1.80 1 -4 -9 6.00 1.60 1 -4 -9 5.00 1.60 -1 -4 9 5.30 1.50 -1 -4 9 6.10 1.70 1 -4 -9 7.30 1.60 -1 -4 9 6.60 1.30 1 -4 -9 8.50 1.60 1 4 -9 7.10 1.50 -1 4 9 6.30 1.60 -1 4 9 7.10 1.60 1 4 -9 9.10 1.80 -1 4 9 7.80 1.90 1 4 -9 7.90 1.80 -1 4 9 6.60 1.40 1 4 -9 9.40 2.00 1 4 -9 7.80 1.80 -1 4 9 7.50 2.00 -1 4 9 6.00 1.60 -1 4 9 5.80 1.40 1 4 -9 7.40 1.60 1 4 -9 6.40 1.30 -1 4 9 8.70 1.80 0 -4 9 136.89 4.70 0 -4 9 131.19 5.90 0 -4 9 132.99 5.60 0 -4 9 142.59 6.20 0 -4 -9 138.49 4.40 0 -4 -9 136.39 6.00 0 -4 9 137.09 5.50 0 -4 9 139.59 6.20 0 -4 -9 135.19 5.70 0 -4 -9 135.09 5.10 0 -4 -9 138.29 6.10 0 -4 -9 138.79 6.10 0 -4 -9 138.39 5.60 0 -4 -9 143.99 5.70 0 4 -9 138.69 5.80 0 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5.00 1.80 -4 -5 9 3.10 1.40 4 -5 -9 3.50 2.10 -4 -5 9 -0.30 1.10 4 -5 -9 6.10 1.90 -4 -5 9 4.20 1.60 4 -5 -9 4.50 2.00 -4 -5 9 4.30 2.20 4 5 -9 4.50 1.90 -4 5 9 2.10 1.00 -4 5 9 4.10 1.80 -4 5 9 1.70 1.80 4 5 -9 2.00 1.20 4 5 -9 6.20 1.80 4 5 -9 2.80 1.20 -4 5 9 3.10 2.10 4 5 -9 2.80 1.80 -3 -5 9 13.40 2.70 3 -5 -9 15.70 2.90 3 -5 -9 14.60 2.50 3 -5 -9 15.90 2.70 3 -5 -9 10.70 2.40 3 -5 -9 16.40 2.30 -3 -5 9 13.30 2.20 -3 -5 9 12.80 1.50 -3 -5 9 12.00 1.50 -3 -5 9 10.40 1.70 3 -5 -9 13.10 2.20 -3 5 9 14.40 1.80 3 5 -9 12.70 2.30 3 5 -9 11.90 1.80 3 5 -9 14.90 2.10 3 5 -9 14.90 2.40 3 5 -9 13.60 2.60 -3 5 9 14.50 2.70 -3 5 9 13.40 2.60 -3 5 9 14.70 2.10 -3 5 9 11.00 2.00 3 5 -9 10.70 1.70 2 -5 -9 1377.76 34.40 2 -5 -9 1396.56 34.20 -2 -5 9 1381.76 32.40 -2 -5 9 1416.26 31.50 2 -5 -9 1398.66 34.40 2 -5 -9 1344.37 33.00 -2 -5 9 1399.06 33.80 2 -5 -9 1393.76 33.70 2 -5 -9 1360.56 34.80 -2 -5 9 1381.86 31.50 -2 -5 9 1347.67 32.40 2 -5 -9 1414.96 34.30 -2 5 9 1375.56 33.50 2 5 -9 1394.56 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-10 39.30 4.20 7 -2 10 34.60 4.70 -7 -2 -10 34.90 4.60 -7 -2 -10 40.60 4.30 7 -2 10 34.40 4.60 7 -2 10 28.50 4.10 7 2 10 37.80 4.80 7 2 10 40.10 4.60 -7 2 -10 38.30 4.60 7 2 10 36.10 4.50 -7 2 -10 28.60 4.40 -7 2 -10 37.70 4.50 -8 -2 -10 63.29 5.40 8 -2 10 41.20 5.50 8 -2 10 45.90 5.70 8 -2 10 62.39 5.40 -8 -2 -10 63.69 8.20 -8 -2 -10 56.79 5.70 -8 -2 -10 69.89 5.50 -8 2 -10 70.19 5.90 -8 2 -10 51.29 5.50 8 2 10 62.99 6.00 8 2 10 50.89 5.60 8 2 10 65.29 5.80 -8 2 -10 45.40 5.40 9 -2 10 5.30 2.80 9 -2 10 2.80 2.40 -9 -2 -10 0.40 2.60 -9 -2 -10 7.20 3.70 -9 -2 -10 4.30 3.00 9 -2 10 5.50 3.00 -9 -2 -10 6.10 3.40 9 2 10 4.20 3.20 9 2 10 5.00 2.90 9 2 10 4.70 3.00 -9 2 -10 3.20 2.70 -9 2 -10 6.50 3.00 -9 2 -10 -4.30 2.60 -10 -2 -10 1.30 2.50 -10 2 -10 -1.70 3.80 10 2 10 5.70 3.00 10 2 10 4.70 3.60 -10 2 -10 -4.50 2.60 -10 2 -10 0.00 2.50 -11 -3 10 147.49 8.90 11 -3 -10 123.89 8.60 -11 -3 10 126.09 8.70 11 -3 -10 123.29 6.30 -11 3 10 121.79 8.50 -11 3 10 138.79 9.40 -11 3 10 110.99 8.90 -10 -3 10 124.59 8.20 -10 -3 10 129.29 8.00 10 -3 -10 130.79 8.10 -10 -3 10 125.89 7.70 10 -3 -10 124.19 6.00 -10 3 10 120.99 8.10 -10 3 10 145.79 9.10 -10 3 10 132.89 8.70 9 -3 -10 99.89 5.20 9 -3 -10 101.29 7.50 -9 -3 10 100.19 7.50 -9 -3 10 87.09 6.20 -9 3 10 104.09 7.50 -9 3 10 100.59 7.10 8 -3 -10 100.79 6.00 8 -3 -10 93.99 7.10 -8 -3 10 93.29 5.60 -8 -3 10 101.09 6.40 -8 -3 10 103.09 6.30 -8 -3 10 98.89 5.70 8 -3 -10 102.79 6.40 -8 3 10 107.19 7.90 -8 3 10 97.79 5.80 -8 3 10 105.89 6.80 7 -3 -10 208.68 9.60 7 -3 -10 196.68 7.50 -7 -3 10 190.58 7.70 -7 -3 10 193.98 8.10 -7 -3 10 198.68 8.90 7 -3 -10 197.68 8.50 -7 -3 10 200.58 8.70 -7 3 10 198.58 9.20 7 3 -10 197.08 8.70 -7 3 10 193.78 8.30 -6 -3 10 531.85 15.60 6 -3 -10 505.35 15.70 -6 -3 10 530.45 16.50 6 -3 -10 509.45 16.60 6 -3 -10 521.55 14.90 -6 -3 10 532.25 15.00 6 -3 -10 529.25 17.00 -6 3 10 532.45 16.20 6 3 -10 518.25 16.10 6 3 -10 523.45 16.20 6 3 -10 544.45 16.40 -6 3 10 522.85 16.90 6 3 -10 522.65 12.80 5 -3 -10 291.77 10.80 -5 -3 10 301.87 11.00 5 -3 -10 297.07 11.10 -5 -3 10 308.77 9.40 5 -3 -10 292.67 9.90 -5 -3 10 280.77 11.10 -5 3 10 286.37 8.50 5 3 -10 284.97 10.50 5 3 -10 294.27 10.50 5 3 -10 297.47 10.50 5 3 -10 294.17 8.10 5 3 -10 289.17 8.10 -5 3 10 289.27 11.00 -5 3 10 298.47 10.70 4 -3 -10 860.71 22.20 -4 -3 10 876.61 23.80 -4 -3 10 800.12 21.40 -4 -3 10 800.02 21.10 4 -3 -10 896.01 23.90 4 -3 -10 860.21 22.40 -4 -3 10 859.11 22.30 4 -3 -10 880.61 23.50 -4 -3 10 851.81 23.20 -4 -3 10 874.81 21.60 4 -3 -10 851.31 23.40 4 3 -10 852.31 21.00 -4 3 10 887.41 23.60 4 3 -10 858.21 22.50 -4 3 10 890.51 23.90 -4 3 10 780.02 22.80 -4 3 10 865.41 22.10 -4 3 10 876.91 21.50 4 3 -10 905.01 23.40 4 3 -10 871.51 23.10 4 3 -10 883.01 21.10 -3 -3 10 1.10 1.10 -3 -3 10 0.10 0.80 -3 -3 10 -0.20 1.10 3 -3 -10 -0.30 1.10 -3 -3 10 -0.40 1.00 3 -3 -10 0.50 1.40 3 -3 -10 1.10 1.60 3 -3 -10 1.70 1.20 -3 -3 10 0.40 0.70 -3 -3 10 0.00 1.70 3 -3 -10 -0.30 1.50 3 -3 -10 -0.80 1.00 -3 -3 10 1.70 0.80 -3 -3 10 2.70 1.50 3 -3 -10 3.10 1.30 3 3 -10 0.00 1.00 -3 3 10 0.40 1.20 3 3 -10 -0.70 1.30 3 3 -10 -0.90 0.70 -3 3 10 0.80 1.10 3 3 -10 -1.00 1.30 -3 3 10 0.70 1.10 -3 3 10 2.90 1.40 -3 3 10 0.40 1.50 3 3 -10 0.60 1.00 3 3 -10 -0.70 1.30 2 -3 -10 79.19 4.60 2 -3 -10 82.19 3.70 -2 -3 10 82.39 4.90 -2 -3 10 83.79 3.80 -2 -3 10 79.09 4.80 -2 -3 10 72.29 3.60 2 -3 -10 74.29 4.30 -2 -3 10 81.59 3.50 2 -3 -10 71.19 4.20 2 -3 -10 74.79 4.30 2 3 -10 78.69 4.40 -2 3 10 80.69 4.10 2 3 -10 81.59 4.90 -2 3 10 74.69 4.10 -2 3 10 104.19 8.10 2 3 -10 72.39 3.80 -2 3 10 73.29 3.40 -2 3 10 78.79 4.90 2 3 -10 78.59 3.90 1 -3 -10 43.00 3.50 -1 -3 10 44.50 2.70 -1 -3 10 45.80 3.80 1 -3 -10 42.70 3.10 1 -3 -10 49.40 3.40 1 -3 -10 42.00 3.40 1 -3 -10 46.30 3.50 -1 -3 10 48.40 3.00 1 -3 -10 41.40 2.60 1 -3 -10 43.20 3.30 -1 -3 10 43.50 2.90 -1 3 10 50.29 3.60 1 3 -10 49.70 3.50 1 3 -10 45.10 3.60 -1 3 10 40.60 2.40 -1 3 10 42.50 3.20 -1 3 10 44.00 3.30 -1 3 10 37.10 3.10 -1 3 10 44.30 4.10 1 3 -10 48.00 3.00 1 3 -10 42.40 2.60 0 -3 -10 38.60 2.40 0 -3 -10 35.80 3.00 0 -3 -10 36.20 3.00 0 -3 10 39.20 2.60 0 -3 -10 34.20 3.30 0 -3 10 37.10 2.90 0 -3 10 37.90 3.40 0 -3 -10 33.80 3.20 0 -3 10 39.30 2.90 0 -3 -10 32.20 3.10 0 -3 -10 36.00 3.00 0 3 10 32.20 3.00 0 3 -10 33.40 3.00 0 3 10 36.60 3.10 0 3 10 35.60 2.90 0 3 -10 35.80 2.60 0 3 10 34.50 2.90 0 3 10 39.90 3.20 0 3 -10 33.50 2.60 0 3 10 32.60 2.10 0 3 10 35.60 2.30 0 3 -10 39.20 3.20 0 3 -10 33.30 3.10 0 3 -10 37.50 3.00 1 -3 10 20.90 2.80 1 -3 10 28.70 3.10 -1 -3 -10 28.00 2.80 -1 -3 -10 22.50 2.90 1 -3 10 19.10 2.00 -1 -3 -10 24.60 2.00 1 -3 10 22.50 2.60 -1 -3 -10 28.20 2.70 -1 -3 -10 22.70 2.20 -1 -3 -10 19.70 2.90 -1 -3 -10 24.10 2.80 1 -3 10 26.40 2.70 -1 3 -10 22.50 2.70 -1 3 -10 30.20 2.90 -1 3 -10 25.60 2.60 -1 3 -10 27.10 2.30 -1 3 -10 23.20 2.80 1 3 10 24.00 2.50 1 3 10 25.30 3.00 1 3 10 23.50 2.80 -1 3 -10 28.70 3.10 1 3 10 28.90 3.50 1 3 10 21.00 3.10 1 3 10 21.90 1.90 -1 3 -10 22.20 2.80 -2 -3 -10 7.20 1.90 2 -3 10 2.40 1.60 -2 -3 -10 3.20 1.50 2 -3 10 3.80 2.00 2 -3 10 4.70 1.40 -2 -3 -10 2.50 1.60 2 -3 10 2.20 1.50 -2 -3 -10 6.10 2.10 -2 -3 -10 6.90 1.70 2 -3 10 2.40 1.80 -2 -3 -10 5.80 1.40 2 -3 10 2.20 1.50 -2 -3 -10 5.70 1.70 2 3 10 7.60 2.30 2 3 10 3.00 1.20 -2 3 -10 1.30 1.40 -2 3 -10 0.80 1.70 -2 3 -10 2.90 1.50 2 3 10 1.90 1.60 2 3 10 2.80 1.80 2 3 10 3.00 1.90 -2 3 -10 -0.40 1.40 2 3 10 3.10 1.30 -2 3 -10 3.20 1.40 -2 3 -10 3.70 1.70 3 -3 10 84.29 5.10 -3 -3 -10 98.89 5.00 -3 -3 -10 95.29 5.10 3 -3 10 96.79 5.60 3 -3 10 91.59 5.30 3 -3 10 89.09 5.20 -3 -3 -10 93.19 4.40 -3 -3 -10 88.89 5.50 -3 -3 -10 90.99 5.40 -3 -3 -10 97.19 5.60 3 -3 10 88.69 4.80 3 -3 10 101.69 5.90 -3 3 -10 94.29 4.90 3 3 10 100.79 6.00 3 3 10 97.29 4.10 -3 3 -10 90.59 5.20 3 3 10 95.29 4.90 -3 3 -10 102.49 5.70 -3 3 -10 90.09 5.40 3 3 10 98.49 5.70 -3 3 -10 90.69 4.70 3 3 10 91.19 5.50 -4 -3 -10 150.48 6.20 4 -3 10 133.99 7.00 -4 -3 -10 137.99 7.10 4 -3 10 148.69 7.50 -4 -3 -10 149.19 7.20 4 -3 10 148.09 6.10 -4 -3 -10 141.49 6.60 4 -3 10 146.69 7.30 -4 -3 -10 140.49 6.50 -4 3 -10 146.39 6.40 -4 3 -10 152.48 6.30 -4 3 -10 144.69 7.00 -4 3 -10 142.79 7.20 4 3 10 139.09 7.20 -4 3 -10 148.89 7.10 4 3 10 148.29 7.40 4 3 10 145.59 6.70 4 3 10 139.39 7.20 -5 -3 -10 86.49 5.90 -5 -3 -10 66.19 4.60 5 -3 10 80.49 5.60 5 -3 10 63.89 5.20 -5 -3 -10 85.59 4.80 5 -3 10 82.99 5.70 -5 -3 -10 77.89 5.00 -5 3 -10 77.39 5.40 -5 3 -10 76.19 5.30 5 3 10 70.09 5.40 -5 3 -10 83.89 5.60 5 3 10 75.89 4.60 5 3 10 71.39 5.50 -5 3 -10 76.49 5.00 5 3 10 71.19 5.10 -5 3 -10 69.89 4.40 6 -3 10 71.49 5.50 6 -3 10 79.39 6.00 -6 -3 -10 70.19 5.60 -6 -3 -10 71.59 4.90 6 -3 10 72.29 5.70 -6 -3 -10 78.29 5.20 6 3 10 60.99 5.30 -6 3 -10 71.69 5.50 -6 3 -10 69.09 5.00 6 3 10 80.99 5.90 6 3 10 63.29 5.40 -6 3 -10 74.59 5.50 -7 -3 -10 3.20 2.30 7 -3 10 5.50 3.20 7 -3 10 6.30 2.40 -7 -3 -10 -0.70 2.70 -7 -3 -10 4.50 2.40 -7 -3 -10 4.00 2.10 7 -3 10 2.70 2.20 -7 3 -10 2.90 2.10 7 3 10 7.70 2.90 -7 3 -10 3.80 2.50 7 3 10 3.70 2.50 8 -3 10 58.29 6.10 -8 -3 -10 52.89 5.80 -8 -3 -10 59.69 6.00 8 -3 10 51.89 5.70 8 -3 10 62.09 5.40 -8 -3 -10 62.29 6.10 -8 -3 -10 49.00 4.90 -8 3 -10 54.09 5.50 -8 3 -10 49.40 5.30 8 3 10 57.09 6.00 -8 3 -10 56.29 5.80 8 3 10 52.39 5.50 -9 -3 -10 -1.30 2.80 -9 -3 -10 -3.30 2.40 9 -3 10 -4.50 2.40 -9 -3 -10 1.90 2.40 9 -3 10 1.00 3.70 -9 -3 -10 -0.30 2.60 9 -3 10 -1.10 3.10 9 3 10 3.40 2.80 -9 3 -10 0.50 2.50 9 3 10 -2.60 2.50 -9 3 -10 -2.10 2.40 9 3 10 4.90 3.10 -9 3 -10 -2.80 2.80 -10 -3 -10 11.80 4.00 10 -3 10 12.50 4.30 -10 -3 -10 13.40 4.80 10 3 10 1.90 2.90 10 3 10 6.30 4.10 -10 3 -10 15.00 3.90 -10 3 -10 16.80 4.10 11 -4 -10 8.20 3.50 -11 -4 10 2.70 3.00 -11 -4 10 -0.70 2.70 -11 4 10 5.70 3.30 -11 4 10 6.70 3.80 -10 -4 10 9.60 3.60 10 -4 -10 16.60 4.20 -10 -4 10 2.70 3.00 10 -4 -10 7.60 2.50 -10 -4 10 7.00 3.10 -10 4 10 12.00 3.60 -10 4 10 6.20 3.30 -10 4 10 7.60 3.20 -9 -4 10 1.40 3.20 9 -4 -10 -0.60 1.80 9 -4 -10 0.20 2.40 -9 -4 10 1.20 2.00 9 -4 -10 0.20 1.60 -9 4 10 1.80 2.30 -9 4 10 3.50 2.60 -9 4 10 0.50 2.40 -8 -4 10 5.10 2.40 -8 -4 10 6.10 2.20 -8 -4 10 5.50 2.20 -8 -4 10 5.00 2.30 8 -4 -10 4.00 2.00 8 -4 -10 5.10 2.60 -8 4 10 8.90 2.40 -8 4 10 3.00 2.60 -8 4 10 3.00 2.50 7 -4 -10 20.30 3.20 7 -4 -10 19.30 3.70 7 -4 -10 17.70 2.70 -7 -4 10 16.90 2.80 -7 -4 10 16.10 3.30 -7 -4 10 17.90 3.40 -7 -4 10 16.40 3.10 -7 4 10 15.30 3.20 -7 4 10 18.60 3.80 -7 4 10 16.50 3.10 7 4 -10 15.40 3.10 -6 -4 10 19.80 3.50 6 -4 -10 24.20 3.60 6 -4 -10 26.10 3.40 6 -4 -10 27.70 3.00 -6 -4 10 28.70 3.00 6 -4 -10 28.60 4.00 -6 -4 10 25.10 3.30 -6 4 10 19.60 3.60 -6 4 10 19.60 3.20 6 4 -10 29.20 3.40 6 4 -10 25.10 3.40 6 4 -10 32.20 3.70 5 -4 -10 112.59 6.30 5 -4 -10 122.89 5.90 -5 -4 10 112.49 5.30 5 -4 -10 105.79 6.40 -5 -4 10 113.89 6.00 5 -4 -10 111.99 5.60 -5 -4 10 103.19 6.30 5 4 -10 116.09 6.10 -5 4 10 116.89 6.50 5 4 -10 108.09 3.90 5 4 -10 111.09 4.00 5 4 -10 117.69 6.10 5 4 -10 120.29 6.70 -5 4 10 110.09 6.10 -5 4 10 117.99 4.20 -4 -4 10 777.92 21.70 4 -4 -10 739.93 21.40 4 -4 -10 740.13 21.10 -4 -4 10 720.13 19.50 4 -4 -10 781.22 21.30 -4 -4 10 762.92 19.80 4 -4 -10 771.22 20.20 -4 -4 10 757.42 19.70 -4 -4 10 739.03 18.70 4 -4 -10 742.13 20.30 -4 -4 10 746.73 20.90 -4 4 10 744.13 21.40 -4 4 10 754.92 18.80 4 4 -10 752.72 20.60 4 4 -10 766.92 20.10 4 4 -10 754.82 21.30 4 4 -10 737.73 18.60 -4 4 10 710.43 19.90 4 4 -10 777.62 20.90 4 4 -10 769.72 18.70 -4 4 10 778.92 21.30 3 -4 -10 45.60 3.80 3 -4 -10 41.60 3.10 -3 -4 10 40.40 3.10 3 -4 -10 46.90 3.80 -3 -4 10 36.70 2.90 -3 -4 10 43.50 2.10 -3 -4 10 43.60 1.90 3 -4 -10 37.20 3.40 -3 -4 10 43.40 3.10 -3 -4 10 49.20 4.30 3 -4 -10 41.50 3.90 -3 -4 10 44.10 3.80 -3 -4 10 41.10 2.20 -3 4 10 41.20 3.90 -3 4 10 42.10 2.90 -3 4 10 39.70 3.00 3 4 -10 47.30 2.90 3 4 -10 41.40 2.90 -3 4 10 43.30 3.90 3 4 -10 45.20 3.80 3 4 -10 40.80 3.60 -3 4 10 44.70 3.30 3 4 -10 40.80 3.50 3 4 -10 41.40 3.10 2 -4 -10 137.49 6.20 -2 -4 10 148.69 7.00 2 -4 -10 155.88 5.80 -2 -4 10 146.39 5.40 2 -4 -10 132.39 5.60 2 -4 -10 169.18 7.50 2 -4 -10 157.48 6.90 2 -4 -10 140.49 7.10 -2 -4 10 164.88 5.30 -2 -4 10 156.58 5.90 -2 -4 10 153.18 7.00 2 4 -10 153.98 7.20 2 4 -10 155.58 5.60 2 4 -10 151.88 6.90 2 4 -10 156.08 5.90 -2 4 10 160.78 7.10 -2 4 10 148.69 5.80 -2 4 10 148.09 6.20 2 4 -10 151.28 6.40 -2 4 10 141.79 5.40 -2 4 10 150.58 7.60 1 -4 -10 55.79 3.20 1 -4 -10 60.49 4.10 1 -4 -10 55.39 4.00 -1 -4 10 62.39 3.70 -1 -4 10 57.09 4.20 -1 -4 10 65.79 4.40 -1 -4 10 65.49 3.80 -1 -4 10 53.69 2.90 1 -4 -10 55.99 3.70 1 -4 -10 62.49 3.80 1 -4 -10 53.79 3.80 1 -4 -10 58.19 4.10 -1 4 10 58.79 3.00 1 4 -10 60.69 3.20 -1 4 10 61.29 3.90 -1 4 10 62.49 4.00 1 4 -10 58.29 3.30 1 4 -10 59.59 3.60 1 4 -10 61.59 3.70 -1 4 10 60.79 4.30 1 4 -10 63.59 3.90 -1 4 10 55.49 3.50 1 4 -10 61.79 5.00 0 -4 10 5.10 1.70 0 -4 -10 13.10 2.40 0 -4 10 6.50 1.30 0 -4 -10 6.10 1.40 0 -4 -10 4.90 1.70 0 -4 -10 9.30 1.90 0 -4 10 6.30 2.10 0 -4 -10 9.10 1.70 0 -4 -10 6.00 1.70 0 -4 10 5.20 1.40 0 -4 -10 6.40 2.00 0 -4 -10 5.80 1.60 0 4 -10 8.60 1.60 0 4 10 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10 70.79 5.00 -7 -5 10 64.99 4.80 -7 5 10 60.89 5.30 -7 5 10 71.89 4.90 -7 5 10 72.39 5.60 7 5 -10 69.99 5.00 -6 -5 10 6.00 1.80 -6 -5 10 7.80 2.50 -6 -5 10 6.60 2.00 6 -5 -10 8.70 2.60 -6 -5 10 4.10 2.30 6 -5 -10 6.90 2.00 6 -5 -10 9.50 2.90 6 5 -10 5.80 2.30 -6 5 10 7.60 2.00 6 5 -10 8.00 2.50 -6 5 10 4.90 2.50 5 -5 -10 831.72 23.90 5 -5 -10 814.42 22.40 -5 -5 10 854.11 21.30 5 -5 -10 831.52 23.30 5 -5 -10 842.02 22.80 -5 -5 10 817.92 23.00 -5 -5 10 833.92 22.10 -5 -5 10 836.52 23.70 5 5 -10 823.92 19.80 5 5 -10 837.92 22.70 5 5 -10 824.72 19.90 5 5 -10 828.42 22.00 5 5 -10 846.52 22.80 -5 5 10 845.22 23.20 -5 5 10 800.82 23.60 -4 -5 10 288.37 9.50 -4 -5 10 278.37 10.70 4 -5 -10 287.37 10.70 4 -5 -10 282.67 9.90 -4 -5 10 249.88 9.10 -4 -5 10 279.17 8.20 4 -5 -10 286.37 10.50 4 -5 -10 266.97 10.10 4 -5 -10 290.17 9.90 -4 -5 10 289.37 10.50 -4 5 10 284.87 10.70 -4 5 10 283.77 10.40 4 5 -10 278.57 8.20 4 5 -10 278.47 8.20 4 5 -10 282.77 10.00 -4 5 10 275.77 8.10 4 5 -10 263.67 9.00 4 5 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14 7.40 3.30 -7 8 14 9.30 3.30 7 8 -14 12.50 3.30 -7 8 14 5.10 3.00 6 -8 -14 2.10 2.40 -6 -8 14 0.10 2.70 6 -8 -14 3.10 3.00 -6 -8 14 7.60 2.90 6 8 -14 5.60 2.90 6 8 -14 6.30 1.60 -6 8 14 2.60 2.90 6 8 -14 5.90 2.90 -6 8 14 3.10 2.80 5 -8 -14 22.10 4.80 5 -8 -14 28.50 4.40 5 -8 -14 30.90 4.50 -5 -8 14 23.50 4.60 -5 -8 14 22.70 4.50 5 8 -14 34.10 4.40 5 8 -14 25.30 4.60 -5 8 14 27.30 4.60 5 8 -14 28.50 4.50 -5 8 14 30.30 4.80 5 8 -14 26.30 2.80 4 -8 -14 3.70 2.70 4 -8 -14 4.50 2.70 -4 -8 14 -3.00 3.60 -4 -8 14 -0.20 2.00 -4 -8 14 -0.90 2.60 4 8 -14 2.10 2.10 4 8 -14 0.50 1.80 -4 8 14 0.90 2.60 -4 8 14 0.50 2.60 4 8 -14 1.00 1.60 4 8 -14 1.10 2.20 -3 -8 14 32.00 4.10 -3 -8 14 43.30 5.70 -3 -8 14 34.00 5.40 3 -8 -14 28.60 3.90 3 -8 -14 33.30 4.20 3 -8 -14 32.90 5.40 3 -8 -14 35.30 4.30 3 8 -14 31.40 4.00 3 8 -14 38.30 4.10 3 8 -14 31.00 4.90 3 8 -14 40.80 4.30 -3 8 14 36.30 4.60 -2 -8 14 76.69 5.70 2 -8 -14 87.29 6.30 -2 -8 14 84.49 6.70 2 -8 -14 94.09 7.30 -2 -8 14 85.79 6.50 2 -8 -14 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-4 -20 3.70 2.90 3 -4 -20 2.70 2.90 3 -4 -20 4.30 2.80 -3 -4 20 9.10 3.60 3 -4 -20 0.00 3.70 -3 4 20 -0.40 3.20 3 4 -20 -1.60 5.40 3 4 -20 3.30 3.00 2 -4 -20 -0.10 2.60 2 -4 -20 3.10 3.50 2 -4 -20 0.70 2.60 2 -4 -20 4.70 3.10 -2 -4 20 -1.10 3.00 -2 -4 20 -4.50 2.50 -2 4 20 -6.60 2.80 2 4 -20 -2.30 2.90 -2 4 20 1.50 3.20 2 4 -20 -1.10 2.30 2 4 -20 -3.30 2.10 1 -4 -20 91.39 7.50 -1 -4 20 93.69 8.10 1 -4 -20 85.89 7.30 -1 -4 20 71.49 7.50 1 -4 -20 90.99 7.80 1 -4 -20 87.29 7.40 1 4 -20 87.69 7.00 1 4 -20 91.99 7.50 -1 4 20 107.89 8.10 -1 4 20 79.29 6.70 1 4 -20 82.79 7.80 0 -4 20 5.20 3.40 0 -4 -20 6.40 3.80 0 -4 -20 -2.60 2.80 0 -4 -20 7.90 3.40 0 -4 20 9.70 4.00 0 4 20 5.30 3.70 0 4 -20 2.60 2.40 0 4 -20 6.80 4.50 0 4 -20 6.90 3.20 0 4 20 4.30 3.00 1 -4 20 44.20 6.40 -1 -4 -20 27.70 5.40 -1 -4 -20 29.50 5.10 -1 -4 -20 38.10 5.30 1 4 20 37.90 5.40 -1 4 -20 37.20 5.20 -1 4 -20 36.70 5.80 1 4 20 43.60 5.90 -1 4 -20 38.40 5.50 -2 -4 -20 6.10 3.10 -2 -4 -20 -3.10 4.30 2 -4 20 2.20 3.20 2 4 20 1.60 3.60 2 4 20 -2.60 3.20 -2 4 -20 -2.80 2.90 -2 4 -20 2.90 2.80 4 -5 -20 -2.60 3.10 4 -5 -20 4.00 4.30 -4 -5 20 0.50 3.40 -4 -5 20 0.40 3.50 4 -5 -20 0.80 3.10 4 -5 -20 -1.50 3.00 4 5 -20 1.20 2.30 -4 5 20 7.30 3.70 4 5 -20 0.40 2.90 4 5 -20 6.60 3.30 -4 5 20 -2.40 3.40 3 -5 -20 45.80 6.20 3 -5 -20 51.59 6.00 3 -5 -20 51.09 5.70 -3 -5 20 39.90 6.00 -3 -5 20 51.99 7.10 3 5 -20 61.09 6.50 -3 5 20 48.70 6.60 3 5 -20 46.00 5.50 -3 5 20 48.80 6.60 2 -5 -20 1.80 2.70 2 -5 -20 5.10 3.30 2 -5 -20 1.90 2.80 -2 -5 20 8.70 4.00 2 -5 -20 6.70 3.40 -2 5 20 0.20 3.10 2 5 -20 7.60 3.30 -2 5 20 3.40 5.30 2 5 -20 1.40 3.20 -1 -5 20 2.00 3.70 1 -5 -20 7.40 3.70 1 -5 -20 8.50 3.20 1 -5 -20 -0.40 2.60 1 -5 -20 5.60 3.60 -1 -5 20 7.00 3.70 1 5 -20 12.10 3.70 1 5 -20 3.40 2.70 0 -5 20 11.00 4.20 0 -5 -20 14.40 4.30 0 -5 -20 20.60 4.10 0 -5 -20 16.00 4.10 0 5 -20 24.70 4.80 0 5 -20 15.10 4.80 0 5 20 17.00 7.30 0 5 -20 20.70 4.50 0 5 20 22.80 4.50 1 -5 20 37.10 6.30 1 -5 20 37.50 6.10 -1 -5 -20 26.20 5.00 -1 -5 -20 28.00 5.20 -1 5 -20 39.40 5.60 -1 5 -20 35.00 5.00 -1 5 -20 33.50 5.40 1 5 20 41.00 5.70 -2 -5 -20 2.50 3.10 -2 -5 -20 3.30 3.20 2 -5 20 -2.40 3.40 -2 5 -20 0.30 2.80 2 5 20 0.30 5.20 2 5 20 2.60 3.40 -2 5 -20 6.70 3.60 -4 -6 20 5.10 5.20 4 -6 -20 16.20 4.10 4 -6 -20 15.70 3.50 -4 -6 20 12.90 4.60 4 -6 -20 16.30 4.80 4 -6 -20 13.50 4.10 4 6 -20 22.90 5.20 4 6 -20 9.20 3.00 4 6 -20 15.50 4.30 -4 6 20 17.90 4.20 -4 6 20 16.40 4.40 3 -6 -20 2.70 4.00 3 -6 -20 3.30 3.50 -3 -6 20 -2.60 3.20 3 -6 -20 6.90 3.80 3 -6 -20 -1.90 3.10 -3 6 20 1.30 3.30 3 6 -20 2.70 3.30 -3 6 20 4.80 3.50 3 6 -20 2.20 3.10 3 6 -20 2.60 2.30 -2 -6 20 40.50 6.60 2 -6 -20 63.19 6.30 2 -6 -20 46.10 6.20 2 -6 -20 61.39 6.20 2 6 -20 55.89 6.00 -2 6 20 59.99 7.00 2 6 -20 58.99 6.00 2 6 -20 52.19 7.90 -1 -6 20 32.60 8.60 1 -6 -20 38.90 5.40 1 -6 -20 33.80 6.60 1 -6 -20 38.20 5.40 1 6 -20 28.80 5.80 -1 6 20 31.70 6.30 1 6 -20 33.60 5.30 0 -6 20 66.79 7.80 0 -6 -20 83.49 10.10 0 -6 20 85.59 10.00 0 -6 -20 89.29 7.20 0 -6 -20 84.69 7.10 0 6 20 91.59 8.80 0 6 -20 89.89 10.10 0 6 -20 82.09 7.20 0 6 -20 79.39 9.20 0 6 20 83.69 8.00 0 6 -20 85.49 7.30 -1 -6 -20 1.20 3.10 1 -6 20 -1.50 5.00 -1 -6 -20 -0.10 2.70 1 -6 20 1.00 3.50 -1 -6 -20 5.60 3.60 -1 6 -20 1.90 2.70 1 6 20 -2.30 3.30 -1 6 -20 2.50 3.30 1 6 20 5.90 3.20 -1 6 -20 -2.40 2.60 3 -7 -20 22.70 4.60 -3 -7 20 29.10 5.90 3 -7 -20 31.50 5.20 3 -7 -20 21.70 4.50 -3 7 20 27.70 5.50 3 7 -20 23.70 4.30 3 7 -20 27.40 5.50 3 7 -20 28.20 5.00 -2 -7 20 2.10 3.60 -2 -7 20 0.10 3.40 2 -7 -20 -3.10 3.00 2 -7 -20 1.90 3.10 2 -7 -20 -1.60 3.00 2 7 -20 0.20 2.50 -2 7 20 4.80 4.00 2 7 -20 -7.40 2.50 2 7 -20 1.80 3.20 1 -7 -20 56.39 6.80 1 -7 -20 62.59 6.80 -1 -7 20 44.70 6.50 -1 -7 20 51.59 7.20 1 -7 -20 61.99 6.30 1 7 -20 56.99 6.30 1 7 -20 60.89 6.70 1 7 -20 61.49 6.60 -1 7 20 60.59 7.20 1 7 -20 49.00 6.40 0 -7 -20 2.00 3.00 0 -7 20 -3.10 3.70 0 -7 -20 -0.60 2.90 0 -7 20 -1.60 3.80 0 -7 -20 2.00 3.30 0 7 -20 0.40 2.80 0 7 20 5.00 3.50 0 7 -20 1.20 3.00 0 7 -20 4.00 3.20 0 7 -20 0.30 3.10 -4 0 21 1.20 3.40 4 0 -21 -3.70 2.20 -4 0 21 -5.50 3.10 -3 0 21 1.90 3.90 3 0 -21 7.20 3.50 3 0 -21 1.60 2.70 3 0 -21 1.60 3.10 -3 0 21 2.30 3.50 2 0 -21 0.20 2.90 2 0 -21 2.20 2.90 -2 0 21 -2.60 3.60 -2 0 21 -1.00 3.20 -2 0 21 0.30 2.90 -1 0 21 21.20 4.90 -1 0 21 13.60 3.80 1 0 -21 16.90 4.20 1 0 -21 18.30 4.40 1 0 -21 14.80 4.10 -1 0 21 12.30 4.00 0 0 -21 -0.30 2.80 0 0 -21 2.20 3.00 0 0 -21 3.70 3.10 0 0 21 -1.40 3.60 1 0 21 98.59 8.10 -1 0 -21 100.69 7.80 -1 0 -21 91.19 7.80 1 0 21 101.19 8.70 4 -1 -21 5.00 2.90 4 1 -21 -0.70 2.50 -3 -1 21 22.50 5.10 -3 -1 21 14.40 4.40 3 -1 -21 22.00 4.20 3 -1 -21 38.80 5.90 3 -1 -21 18.50 4.20 3 1 -21 20.10 4.10 3 1 -21 27.30 5.30 3 1 -21 31.90 5.10 -3 1 21 19.50 4.90 -3 1 21 20.80 5.00 2 -1 -21 25.70 4.60 -2 -1 21 14.00 4.20 2 -1 -21 17.60 4.20 -2 -1 21 14.20 4.40 2 1 -21 24.70 5.20 -2 1 21 20.30 5.00 2 1 -21 26.80 5.30 -2 1 21 18.80 5.10 2 1 -21 12.20 4.50 -2 1 21 15.20 4.50 -1 -1 21 -3.40 3.00 1 -1 -21 0.10 3.00 -1 -1 21 -2.50 3.30 -1 -1 21 1.70 3.20 1 -1 -21 0.30 3.00 1 -1 -21 -1.50 2.60 1 1 -21 2.90 3.30 1 1 -21 5.20 3.50 -1 1 21 4.80 3.20 -1 1 21 2.80 3.90 -1 1 21 6.20 3.50 1 1 -21 -0.70 2.80 0 -1 21 2.10 3.50 0 -1 -21 6.60 3.40 0 -1 -21 0.80 2.90 0 -1 -21 -3.20 2.80 0 -1 21 2.00 3.70 0 1 -21 0.90 3.00 0 1 -21 3.00 3.30 0 1 -21 -2.40 2.80 0 1 21 -3.40 3.30 1 -1 21 3.20 3.80 -1 -1 -21 -0.30 2.80 -1 -1 -21 5.20 3.20 1 -1 21 -0.10 3.80 1 1 21 2.40 3.90 -1 1 -21 3.00 3.10 -1 1 -21 -1.20 2.60 1 1 21 6.90 3.30 3 -2 -21 71.39 7.00 3 -2 -21 80.49 7.50 3 -2 -21 87.79 7.20 -3 -2 21 86.79 7.90 -3 -2 21 90.19 7.90 -3 -2 21 84.39 7.50 -3 2 21 97.49 8.20 3 2 -21 91.19 7.40 3 2 -21 82.99 7.60 -3 2 21 100.39 8.30 3 2 -21 72.29 6.30 -2 -2 21 -3.90 3.30 2 -2 -21 -0.90 2.80 -2 -2 21 7.30 3.60 2 -2 -21 0.70 3.40 -2 2 21 2.70 3.50 2 2 -21 -0.20 3.10 -2 2 21 0.10 3.60 2 2 -21 -0.30 2.60 2 2 -21 1.30 3.40 -1 -2 21 21.60 5.00 1 -2 -21 28.90 5.50 1 -2 -21 30.80 5.50 1 -2 -21 31.30 5.30 1 2 -21 39.20 5.60 -1 2 21 34.80 5.90 -1 2 21 34.00 5.30 1 2 -21 16.40 4.40 0 -2 -21 42.80 6.00 0 -2 21 44.50 6.20 0 -2 21 37.40 5.90 0 -2 -21 44.40 6.30 0 -2 -21 43.30 5.90 0 2 -21 40.00 6.00 0 2 -21 45.20 5.80 0 2 -21 40.10 6.80 0 2 21 38.80 6.20 1 -2 21 1.10 3.60 1 2 21 8.40 4.30 -1 2 -21 12.60 4.00 -1 2 -21 4.50 3.30 -3 -3 21 40.20 6.40 3 -3 -21 50.69 6.30 3 -3 -21 57.59 6.50 3 -3 -21 46.00 5.80 -3 3 21 46.20 6.80 -3 3 21 44.10 6.60 3 3 -21 50.59 5.40 3 3 -21 51.49 6.10 3 3 -21 45.40 6.10 2 -3 -21 23.00 4.50 2 -3 -21 35.80 5.30 -2 -3 21 19.00 5.10 2 -3 -21 14.40 5.10 2 3 -21 34.20 5.80 2 3 -21 27.40 4.90 2 3 -21 26.90 5.40 -2 3 21 26.10 5.70 -2 3 21 28.30 6.00 1 -3 -21 42.50 6.80 1 -3 -21 36.90 5.80 1 -3 -21 43.30 5.80 -1 -3 21 47.40 6.80 1 -3 -21 54.69 6.40 -1 -3 21 45.60 6.80 -1 3 21 45.90 6.30 -1 3 21 62.69 8.00 1 3 -21 46.50 6.60 1 3 -21 57.99 6.30 1 3 -21 48.80 6.00 0 -3 -21 4.20 3.50 0 -3 21 3.30 4.30 0 -3 -21 -0.60 2.80 0 -3 21 -2.10 3.50 0 -3 -21 -0.70 4.70 0 3 21 5.10 3.50 0 3 -21 -1.50 2.60 0 3 -21 4.40 3.20 2 -4 -21 29.50 5.50 2 -4 -21 21.30 5.40 2 -4 -21 15.60 4.80 2 -4 -21 33.90 6.00 -2 -4 21 18.10 4.30 -2 -4 21 27.40 5.70 -2 4 21 28.80 5.90 2 4 -21 31.30 5.90 2 4 -21 21.90 5.00 2 4 -21 27.20 4.60 -2 4 21 13.50 6.50 -1 -4 21 3.80 3.60 1 -4 -21 3.50 2.90 1 -4 -21 6.40 3.60 -1 -4 21 -2.50 3.20 1 -4 -21 -3.60 3.20 1 -4 -21 5.40 4.30 1 4 -21 1.60 3.00 1 4 -21 7.50 3.80 -1 4 21 4.10 3.40 1 4 -21 -1.40 3.10 0 4 -21 62.99 6.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 67447 _shelx_res_file ; TITL JTM1442_0m_a.res in P2(1)/n JTM1442_0m_a.res created by SHELXL-2018/3 at 15:51:29 on 27-May-2021 REM Old TITL JTM1442_0m in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.148, Rweak 0.004, Alpha 0.023 REM 2.792 for 151 systematic absences, Orientation as input REM Formula found by SHELXT: C19 N2 O3 CELL 0.71073 8.2284 13.7693 13.9230 90.000 96.155 90.000 ZERR 4.000 0.0003 0.0004 0.0004 0.000 0.001 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O UNIT 80 60 4 12 TEMP -123 SIZE 0.32 0.348 0.437 L.S. 5 BOND $H LIST 4 FMAP 2 PLAN 5 CONF ACTA 66 MPLA C7 C13 O2 O3 MPLA N1 > C9 MPLA N1 C10 > C12 MPLA N1 > C9 MPLA C15 > C20 OMIT -1 1 3 OMIT 0 1 1 WGHT 0.073900 0.368500 FVAR 1.05982 O1 4 0.791304 0.569315 0.290787 11.00000 0.02574 0.02981 = 0.04956 -0.01297 0.02027 -0.00885 O2 4 0.153465 0.398525 0.360117 11.00000 0.02225 0.02702 = 0.04744 -0.01084 0.01266 -0.00829 O3 4 0.340269 0.350573 0.264503 11.00000 0.02630 0.02336 = 0.02759 -0.00902 0.00671 -0.00894 N1 3 0.636221 0.636399 0.399867 11.00000 0.01708 0.01500 = 0.02235 -0.00038 0.00259 -0.00257 C1 1 0.490883 0.640535 0.443565 11.00000 0.01756 0.01482 = 0.01708 0.00120 0.00087 -0.00003 C2 1 0.464826 0.717131 0.506937 11.00000 0.02422 0.01772 = 0.02080 -0.00230 0.00148 -0.00059 AFIX 43 H2 2 0.544815 0.766658 0.518906 11.00000 -1.20000 AFIX 0 C3 1 0.322802 0.720500 0.551922 11.00000 0.02698 0.02333 = 0.02405 -0.00506 0.00407 0.00276 AFIX 43 H3 2 0.306866 0.771800 0.595567 11.00000 -1.20000 AFIX 0 C4 1 0.202868 0.649252 0.533749 11.00000 0.02193 0.02772 = 0.02652 -0.00346 0.00695 0.00249 AFIX 43 H4 2 0.106080 0.651845 0.565229 11.00000 -1.20000 AFIX 0 C5 1 0.225380 0.574662 0.469610 11.00000 0.01815 0.02226 = 0.02321 -0.00099 0.00403 0.00000 AFIX 43 H5 2 0.142234 0.527154 0.456509 11.00000 -1.20000 AFIX 0 C6 1 0.369522 0.567976 0.423403 11.00000 0.01596 0.01539 = 0.01737 0.00118 0.00107 0.00049 C7 1 0.401674 0.491621 0.355790 11.00000 0.01646 0.01455 = 0.01863 0.00074 0.00134 -0.00114 C8 1 0.541835 0.492697 0.313408 11.00000 0.01964 0.01641 = 0.02600 -0.00320 0.00593 -0.00279 AFIX 43 H8 2 0.560136 0.442273 0.269253 11.00000 -1.20000 AFIX 0 C9 1 0.665838 0.567330 0.332189 11.00000 0.01914 0.01782 = 0.02839 -0.00273 0.00681 -0.00248 C10 1 0.764721 0.710185 0.420908 11.00000 0.01974 0.01918 = 0.02805 -0.00088 0.00132 -0.00509 AFIX 23 H10A 2 0.775440 0.725750 0.490720 11.00000 -1.20000 H10B 2 0.870536 0.683646 0.405222 11.00000 -1.20000 AFIX 0 C11 1 0.727268 0.799349 0.364982 11.00000 0.02369 0.02192 = 0.03324 0.00020 0.00720 -0.00616 C12 1 0.692981 0.870274 0.318801 11.00000 0.03131 0.02912 = 0.04838 0.01060 0.01377 -0.00212 AFIX 163 H12 2 0.665529 0.927061 0.281827 11.00000 -1.20000 AFIX 0 C13 1 0.283173 0.410237 0.328862 11.00000 0.01833 0.01669 = 0.02127 -0.00006 0.00077 -0.00181 C14 1 0.232076 0.272533 0.226352 11.00000 0.02952 0.02486 = 0.02472 -0.00675 0.00080 -0.00925 AFIX 23 H14A 2 0.266692 0.250123 0.164117 11.00000 -1.20000 H14B 2 0.119369 0.298095 0.213628 11.00000 -1.20000 AFIX 0 C15 1 0.232234 0.187820 0.294040 11.00000 0.02296 0.02168 = 0.02501 -0.00819 0.00342 -0.00493 C16 1 0.365959 0.125017 0.306249 11.00000 0.02681 0.03365 = 0.03454 -0.01258 0.00165 0.00201 AFIX 43 H16 2 0.457268 0.135594 0.271197 11.00000 -1.20000 AFIX 0 C17 1 0.365791 0.046785 0.369790 11.00000 0.05218 0.03160 = 0.04260 -0.00852 -0.00673 0.01175 AFIX 43 H17 2 0.457907 0.004905 0.378888 11.00000 -1.20000 AFIX 0 C18 1 0.231968 0.029980 0.419595 11.00000 0.08243 0.02986 = 0.03846 0.00256 0.00660 -0.00127 AFIX 43 H18 2 0.232480 -0.023368 0.462895 11.00000 -1.20000 AFIX 0 C19 1 0.097134 0.090640 0.406595 11.00000 0.06188 0.03333 = 0.04090 -0.00352 0.02139 -0.01119 AFIX 43 H19 2 0.004674 0.078535 0.440243 11.00000 -1.20000 AFIX 0 C20 1 0.097744 0.169395 0.344020 11.00000 0.03086 0.02526 = 0.03547 -0.00843 0.01232 -0.00544 AFIX 43 H20 2 0.005332 0.211073 0.335298 11.00000 -1.20000 AFIX 0 HKLF 4 REM JTM1442_0m_a.res in P2(1)/n REM wR2 = 0.133066, GooF = S = 1.03317, Restrained GooF = 1.03317 for all data REM R1 = 0.046050 for 5304 Fo > 4sig(Fo) and 0.051740 for all 6020 data REM 217 parameters refined using 0 restraints END WGHT 0.0739 0.3684 REM Highest difference peak 0.460, deepest hole -0.211, 1-sigma level 0.049 Q1 1 0.5754 0.6424 0.4279 11.00000 0.05 0.46 Q2 1 0.2960 0.5748 0.4435 11.00000 0.05 0.45 Q3 1 0.4682 0.4976 0.3316 11.00000 0.05 0.44 Q4 1 0.4789 0.6804 0.4753 11.00000 0.05 0.43 Q5 1 0.4315 0.6024 0.4353 11.00000 0.05 0.43 ; _shelx_res_checksum 53278 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.79130(8) 0.56932(5) 0.29079(6) 0.03386(17) Uani d 1 . . O O2 0.15346(8) 0.39853(5) 0.36012(6) 0.03159(16) Uani d 1 . . O O3 0.34027(8) 0.35057(5) 0.26450(5) 0.02547(14) Uani d 1 . . N N1 0.63622(8) 0.63640(5) 0.39987(5) 0.01811(12) Uani d 1 . . C C1 0.49088(9) 0.64053(5) 0.44357(5) 0.01656(13) Uani d 1 . . C C2 0.46483(10) 0.71713(6) 0.50694(6) 0.02098(14) Uani d 1 . . H H2 0.544815 0.766658 0.518906 0.025 Uiso calc 1 . . C C3 0.32280(11) 0.72050(6) 0.55192(6) 0.02469(16) Uani d 1 . . H H3 0.306866 0.771800 0.595567 0.030 Uiso calc 1 . . C C4 0.20287(10) 0.64925(7) 0.53375(6) 0.02508(16) Uani d 1 . . H H4 0.106080 0.651845 0.565229 0.030 Uiso calc 1 . . C C5 0.22538(10) 0.57466(6) 0.46961(6) 0.02108(14) Uani d 1 . . H H5 0.142234 0.527154 0.456509 0.025 Uiso calc 1 . . C C6 0.36952(9) 0.56798(5) 0.42340(5) 0.01629(13) Uani d 1 . . C C7 0.40167(8) 0.49162(5) 0.35579(5) 0.01659(13) Uani d 1 . . C C8 0.54184(9) 0.49270(6) 0.31341(6) 0.02043(14) Uani d 1 . . H H8 0.560136 0.442273 0.269253 0.025 Uiso calc 1 . . C C9 0.66584(10) 0.56733(6) 0.33219(6) 0.02148(15) Uani d 1 . . C C10 0.76472(10) 0.71018(6) 0.42091(6) 0.02241(15) Uani d 1 . . H H10A 0.775440 0.725750 0.490720 0.027 Uiso calc 1 . . H H10B 0.870536 0.683646 0.405222 0.027 Uiso calc 1 . . C C11 0.72727(11) 0.79935(6) 0.36498(7) 0.02598(17) Uani d 1 . . C C12 0.69298(13) 0.87027(8) 0.31880(9) 0.0356(2) Uani d 1 . . H H12 0.665529 0.927061 0.281827 0.043 Uiso calc 1 . . C C13 0.28317(9) 0.41024(5) 0.32886(6) 0.01886(14) Uani d 1 . . C C14 0.23208(11) 0.27253(7) 0.22635(6) 0.02652(17) Uani d 1 . . H H14A 0.266692 0.250123 0.164117 0.032 Uiso calc 1 . . H H14B 0.119369 0.298095 0.213628 0.032 Uiso calc 1 . . C C15 0.23223(10) 0.18782(6) 0.29404(6) 0.02316(15) Uani d 1 . . C C16 0.36596(12) 0.12502(8) 0.30625(7) 0.0318(2) Uani d 1 . . H H16 0.457268 0.135594 0.271197 0.038 Uiso calc 1 . . C C17 0.36579(17) 0.04679(9) 0.36979(9) 0.0430(3) Uani d 1 . . H H17 0.457907 0.004905 0.378888 0.052 Uiso calc 1 . . C C18 0.2320(2) 0.02998(9) 0.41959(9) 0.0502(3) Uani d 1 . . H H18 0.232480 -0.023368 0.462895 0.060 Uiso calc 1 . . C C19 0.09713(18) 0.09064(9) 0.40660(9) 0.0442(3) Uani d 1 . . H H19 0.004674 0.078535 0.440243 0.053 Uiso calc 1 . . C C20 0.09774(12) 0.16940(7) 0.34402(7) 0.02989(19) Uani d 1 . . H H20 0.005332 0.211073 0.335298 0.036 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0257(3) 0.0298(3) 0.0496(4) -0.0088(3) 0.0203(3) -0.0130(3) O2 0.0222(3) 0.0270(3) 0.0474(4) -0.0083(2) 0.0127(3) -0.0108(3) O3 0.0263(3) 0.0234(3) 0.0276(3) -0.0089(2) 0.0067(2) -0.0090(2) N1 0.0171(3) 0.0150(3) 0.0224(3) -0.0026(2) 0.0026(2) -0.0004(2) C1 0.0176(3) 0.0148(3) 0.0171(3) 0.0000(2) 0.0009(2) 0.0012(2) C2 0.0242(3) 0.0177(3) 0.0208(3) -0.0006(3) 0.0015(3) -0.0023(2) C3 0.0270(4) 0.0233(4) 0.0240(3) 0.0028(3) 0.0041(3) -0.0051(3) C4 0.0219(3) 0.0277(4) 0.0265(4) 0.0025(3) 0.0070(3) -0.0035(3) C5 0.0182(3) 0.0223(3) 0.0232(3) 0.0000(2) 0.0040(2) -0.0010(3) C6 0.0160(3) 0.0154(3) 0.0174(3) 0.0005(2) 0.0011(2) 0.0012(2) C7 0.0165(3) 0.0145(3) 0.0186(3) -0.0011(2) 0.0013(2) 0.0007(2) C8 0.0196(3) 0.0164(3) 0.0260(3) -0.0028(2) 0.0059(3) -0.0032(2) C9 0.0191(3) 0.0178(3) 0.0284(4) -0.0025(2) 0.0068(3) -0.0027(3) C10 0.0197(3) 0.0192(3) 0.0281(4) -0.0051(3) 0.0013(3) -0.0009(3) C11 0.0237(3) 0.0219(4) 0.0332(4) -0.0062(3) 0.0072(3) 0.0002(3) C12 0.0313(4) 0.0291(4) 0.0484(6) -0.0021(4) 0.0138(4) 0.0106(4) C13 0.0183(3) 0.0167(3) 0.0213(3) -0.0018(2) 0.0008(2) -0.0001(2) C14 0.0295(4) 0.0249(4) 0.0247(4) -0.0092(3) 0.0008(3) -0.0067(3) C15 0.0230(3) 0.0217(3) 0.0250(3) -0.0049(3) 0.0034(3) -0.0082(3) C16 0.0268(4) 0.0337(5) 0.0345(4) 0.0020(3) 0.0016(3) -0.0126(4) C17 0.0522(7) 0.0316(5) 0.0426(6) 0.0117(5) -0.0067(5) -0.0085(4) C18 0.0824(10) 0.0299(5) 0.0385(6) -0.0013(6) 0.0066(6) 0.0026(4) C19 0.0619(7) 0.0333(5) 0.0409(6) -0.0112(5) 0.0214(5) -0.0035(4) C20 0.0309(4) 0.0253(4) 0.0355(4) -0.0054(3) 0.0123(3) -0.0084(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C13 O3 C14 . . 116.87(7) ? C9 N1 C1 . . 123.16(6) ? C9 N1 C10 . . 115.85(6) ? C1 N1 C10 . . 120.93(6) ? N1 C1 C2 . . 119.87(7) ? N1 C1 C6 . . 120.08(6) ? C2 C1 C6 . . 120.05(7) ? C3 C2 C1 . . 120.12(7) ? C3 C2 H2 . . 119.9 ? C1 C2 H2 . . 119.9 ? C2 C3 C4 . . 120.62(7) ? C2 C3 H3 . . 119.7 ? C4 C3 H3 . . 119.7 ? C5 C4 C3 . . 119.80(8) ? C5 C4 H4 . . 120.1 ? C3 C4 H4 . . 120.1 ? C4 C5 C6 . . 121.24(7) ? C4 C5 H5 . . 119.4 ? C6 C5 H5 . . 119.4 ? C5 C6 C1 . . 118.15(7) ? C5 C6 C7 . . 124.21(7) ? C1 C6 C7 . . 117.65(6) ? C8 C7 C6 . . 119.87(6) ? C8 C7 C13 . . 117.37(7) ? C6 C7 C13 . . 122.76(6) ? C7 C8 C9 . . 123.06(7) ? C7 C8 H8 . . 118.5 ? C9 C8 H8 . . 118.5 ? O1 C9 N1 . . 121.42(7) ? O1 C9 C8 . . 122.54(7) ? N1 C9 C8 . . 116.04(7) ? C11 C10 N1 . . 111.46(7) ? C11 C10 H10A . . 109.3 ? N1 C10 H10A . . 109.3 ? C11 C10 H10B . . 109.3 ? N1 C10 H10B . . 109.3 ? H10A C10 H10B . . 108.0 ? C12 C11 C10 . . 178.18(10) ? C11 C12 H12 . . 180.0 ? O2 C13 O3 . . 123.21(7) ? O2 C13 C7 . . 125.74(7) ? O3 C13 C7 . . 111.05(6) ? O3 C14 C15 . . 112.63(7) ? O3 C14 H14A . . 109.1 ? C15 C14 H14A . . 109.1 ? O3 C14 H14B . . 109.1 ? C15 C14 H14B . . 109.1 ? H14A C14 H14B . . 107.8 ? C20 C15 C16 . . 119.00(9) ? C20 C15 C14 . . 120.58(8) ? C16 C15 C14 . . 120.41(8) ? C17 C16 C15 . . 120.11(10) ? C17 C16 H16 . . 119.9 ? C15 C16 H16 . . 119.9 ? C18 C17 C16 . . 120.18(11) ? C18 C17 H17 . . 119.9 ? C16 C17 H17 . . 119.9 ? C17 C18 C19 . . 120.23(11) ? C17 C18 H18 . . 119.9 ? C19 C18 H18 . . 119.9 ? C18 C19 C20 . . 119.68(11) ? C18 C19 H19 . . 120.2 ? C20 C19 H19 . . 120.2 ? C19 C20 C15 . . 120.76(10) ? C19 C20 H20 . . 119.6 ? C15 C20 H20 . . 119.6 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C9 . 1.2355(10) ? O2 C13 . 1.2058(10) ? O3 C13 . 1.3375(10) ? O3 C14 . 1.4588(10) ? N1 C9 . 1.3788(10) ? N1 C1 . 1.3999(10) ? N1 C10 . 1.4730(10) ? C1 C2 . 1.4062(10) ? C1 C6 . 1.4192(10) ? C2 C3 . 1.3846(11) ? C2 H2 . 0.9500 ? C3 C4 . 1.3953(12) ? C3 H3 . 0.9500 ? C4 C5 . 1.3864(11) ? C4 H4 . 0.9500 ? C5 C6 . 1.4116(10) ? C5 H5 . 0.9500 ? C6 C7 . 1.4543(10) ? C7 C8 . 1.3507(10) ? C7 C13 . 1.5062(10) ? C8 C9 . 1.4520(11) ? C8 H8 . 0.9500 ? C10 C11 . 1.4687(12) ? C10 H10A . 0.9900 ? C10 H10B . 0.9900 ? C11 C12 . 1.1865(14) ? C12 H12 . 0.9500 ? C14 C15 . 1.4995(13) ? C14 H14A . 0.9900 ? C14 H14B . 0.9900 ? C15 C20 . 1.3922(12) ? C15 C16 . 1.3955(13) ? C16 C17 . 1.3940(17) ? C16 H16 . 0.9500 ? C17 C18 . 1.382(2) ? C17 H17 . 0.9500 ? C18 C19 . 1.385(2) ? C18 H18 . 0.9500 ? C19 C20 . 1.3914(16) ? C19 H19 . 0.9500 ? C20 H20 . 0.9500 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C2 H2 Cg3 3_666 0.95 2.94 3.8206(10) 154 y C4 H4 O2 3_566 0.95 2.57 3.4846(11) 162 y C5 H5 O2 . 0.95 2.23 2.8917(11) 126 y C12 H12 O1 2_655 0.95 2.25 3.1463(14) 157 y C14 H14A Cg2 2_545 0.99 2.65 3.4652(9) 140 y C16 H16 O1 2_645 0.95 2.50 3.3443(12) 148 y loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C9 N1 C1 C2 . . . . -175.56(7) ? C10 N1 C1 C2 . . . . 1.37(10) ? C9 N1 C1 C6 . . . . 3.97(11) ? C10 N1 C1 C6 . . . . -179.10(7) ? N1 C1 C2 C3 . . . . -178.65(7) ? C6 C1 C2 C3 . . . . 1.82(11) ? C1 C2 C3 C4 . . . . -1.16(13) ? C2 C3 C4 C5 . . . . -0.41(13) ? C3 C4 C5 C6 . . . . 1.33(13) ? C4 C5 C6 C1 . . . . -0.66(11) ? C4 C5 C6 C7 . . . . 179.70(7) ? N1 C1 C6 C5 . . . . 179.56(7) ? C2 C1 C6 C5 . . . . -0.91(11) ? N1 C1 C6 C7 . . . . -0.77(10) ? C2 C1 C6 C7 . . . . 178.76(7) ? C5 C6 C7 C8 . . . . 178.41(7) ? C1 C6 C7 C8 . . . . -1.23(11) ? C5 C6 C7 C13 . . . . -0.72(11) ? C1 C6 C7 C13 . . . . 179.64(6) ? C6 C7 C8 C9 . . . . 0.28(12) ? C13 C7 C8 C9 . . . . 179.45(7) ? C1 N1 C9 O1 . . . . 175.57(8) ? C10 N1 C9 O1 . . . . -1.50(12) ? C1 N1 C9 C8 . . . . -4.77(11) ? C10 N1 C9 C8 . . . . 178.16(7) ? C7 C8 C9 O1 . . . . -177.70(9) ? C7 C8 C9 N1 . . . . 2.64(12) ? C9 N1 C10 C11 . . . . 96.66(8) ? C1 N1 C10 C11 . . . . -80.48(9) ? C14 O3 C13 O2 . . . . 4.71(12) ? C14 O3 C13 C7 . . . . -175.41(7) ? C8 C7 C13 O2 . . . . 179.78(8) ? C6 C7 C13 O2 . . . . -1.07(12) ? C8 C7 C13 O3 . . . . -0.10(10) ? C6 C7 C13 O3 . . . . 179.05(7) ? C13 O3 C14 C15 . . . . -80.18(10) ? O3 C14 C15 C20 . . . . 107.82(9) ? O3 C14 C15 C16 . . . . -73.57(10) ? C20 C15 C16 C17 . . . . -1.82(13) ? C14 C15 C16 C17 . . . . 179.56(8) ? C15 C16 C17 C18 . . . . 1.23(16) ? C16 C17 C18 C19 . . . . 0.10(18) ? C17 C18 C19 C20 . . . . -0.80(19) ? C18 C19 C20 C15 . . . . 0.19(17) ? C16 C15 C20 C19 . . . . 1.12(14) ? C14 C15 C20 C19 . . . . 179.74(9) ? _cod_database_fobs_code 2243879