#------------------------------------------------------------------------------ #$Date: 2022-07-27 05:08:08 +0300 (Wed, 27 Jul 2022) $ #$Revision: 276958 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/41/2244135.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244135 _cell_angle_alpha 96.736 _cell_angle_beta 101.490 _cell_angle_gamma 95.216 _cell_length_a 9.9635 _cell_length_b 14.4905 _cell_length_c 20.1131 _exptl_crystal_F_000 1275.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file vm2269Isup2.hkl _cod_data_source_block I _shelx_title ' shi_4382_rola_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 259.55 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 40.42 23.29 3.03 o 2 0 0 8982.46 9258.36 88.04 o 3 0 0 12.44 11.56 3.79 o 4 0 0 1815.22 1782.93 49.71 o 5 0 0 801.31 745.87 38.48 o 6 0 0 107.71 125.53 45.87 o 7 0 0 1126.43 990.29 111.06 o 8 0 0 1139.34 1227.71 98.87 o 9 0 0 0.17 -18.13 20.23 o 10 0 0 3.48 37.38 25.95 o 11 0 0 41.63 45.17 32.46 o -11 1 0 132.44 208.88 36.28 o -10 1 0 23.96 40.28 25.91 o -9 1 0 426.54 458.86 65.40 o -8 1 0 78.61 66.63 14.23 o -7 1 0 85.05 78.71 13.71 o -6 1 0 8611.68 8430.07 152.87 o -5 1 0 178.63 183.55 20.70 o -4 1 0 77.55 93.98 8.08 o -3 1 0 348.52 358.38 14.96 o -2 1 0 10663.61 11924.98 84.62 o -1 1 0 1447.67 1445.31 29.01 o 1 1 0 2.01 10.71 9.06 o 2 1 0 4809.47 5059.70 69.82 o 3 1 0 0.46 6.14 6.15 o 4 1 0 145.76 154.58 11.53 o 5 1 0 26.02 34.83 7.54 o 6 1 0 4787.73 4788.69 114.79 o 7 1 0 1170.55 1137.36 90.96 o 8 1 0 303.67 321.94 43.56 o 9 1 0 22.28 16.80 20.88 o 10 1 0 449.31 462.49 69.79 o 11 1 0 0.42 -10.47 18.96 o -11 2 0 379.42 333.71 67.41 o -10 2 0 26.54 40.05 26.90 o -9 2 0 152.65 235.01 46.16 o -8 2 0 78.85 63.76 27.13 o -7 2 0 185.92 180.57 20.11 o -6 2 0 281.11 244.89 20.53 o -5 2 0 14.41 15.40 5.33 o -4 2 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