#------------------------------------------------------------------------------ #$Date: 2022-08-27 05:37:18 +0300 (Sat, 27 Aug 2022) $ #$Revision: 277423 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/41/2244151.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244151 loop_ _publ_author_name 'Naghiyev, Farid N.' 'Khrustalev, Victor N.' 'Venskovsky, Nikolai U.' 'Akkurt, Mehmet' 'Khalilov, Ali N.' 'Bhattarai, Ajaya' 'Mamedov, \.Ibrahim G.' _publ_section_title ; Crystal structure and Hirshfeld surface analysis of ethyl 2'-amino-5-bromo-3'-cyano-6'-methyl-2-oxospiro[indoline-3,4'-pyran]-5'-carboxylate ; _journal_coeditor_code YK2174 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first ; ; _journal_paper_doi 10.1107/S2056989022008271 _journal_volume 78 _journal_year 2022 _chemical_formula_iupac 'C17 H14 Br N3 O4' _chemical_formula_moiety 'C17 H14 Br N3 O4' _chemical_formula_sum 'C17 H14 Br N3 O4' _chemical_formula_weight 404.22 _chemical_name_systematic 'Ethyl 2'-amino-5-bromo-3'-cyano-6'-methyl-2-oxospiro[indoline-3,4'-pyran]-5'-carboxylate' _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 9.3880(9) _cell_length_b 12.2260(12) _cell_length_c 28.693(3) _cell_measurement_reflns_used 1000 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 25.0 _cell_measurement_theta_min 1.5 _cell_volume 3293.3(6) _computing_cell_refinement ; iMosflm (Battye et al., 2011) ; _computing_data_collection ; Marccd (Doyle, 2011) ; _computing_data_reduction ; iMosflm (Battye et al., 2011) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; PLATON (Spek, 2020) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.992 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Rayonix SX-165 CCD' _diffrn_measurement_method '/f scan' _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.74500 _diffrn_reflns_av_R_equivalents 0.0577 _diffrn_reflns_av_unetI/netI 0.0293 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 39 _diffrn_reflns_limit_l_min -39 _diffrn_reflns_number 29648 _diffrn_reflns_theta_full 26.551 _diffrn_reflns_theta_max 31.013 _diffrn_reflns_theta_min 1.488 _exptl_absorpt_coefficient_mu 2.841 _exptl_absorpt_correction_T_max 0.716 _exptl_absorpt_correction_T_min 0.626 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (Scala; Evans, 2006) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.631 _exptl_crystal_description prism _exptl_crystal_F_000 1632 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.794 _refine_diff_density_min -0.662 _refine_ls_extinction_coef 0.0033(5) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL-2018/3 (Sheldrick, 2015b) ; _refine_ls_goodness_of_fit_ref 1.131 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 248 _refine_ls_number_reflns 4526 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.131 _refine_ls_R_factor_all 0.0480 _refine_ls_R_factor_gt 0.0448 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0170P)^2^+5.6891P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0893 _refine_ls_wR_factor_ref 0.0908 _reflns_number_gt 4225 _reflns_number_total 4526 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yk2174sup1.cif _cod_data_source_block I _cod_database_code 2244151 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.675 _shelx_estimated_absorpt_t_max 0.764 _shelx_hkl_file ; 0 0 1 -0.15 0.02 0 0 -2 167.00 6.75 0 0 2 160.30 6.48 0 0 -3 0.01 0.19 0 0 3 0.01 0.20 0 0 -4 79.40 3.27 0 0 4 79.29 3.26 0 0 -5 0.09 0.32 0 0 5 0.07 0.36 0 0 -7 -0.02 0.44 0 0 7 0.57 0.47 0 0 -8 60.97 2.62 0 0 8 58.96 2.55 0 0 -9 0.29 0.48 0 0 9 1.11 0.56 0 0 -11 0.21 0.54 0 0 11 0.37 0.62 0 0 12 902.40 36.49 0 0 -13 0.67 0.58 0 0 13 -0.05 0.68 0 0 -14 23.28 1.26 0 0 14 26.41 1.44 0 0 -15 -0.32 0.69 0 0 15 0.67 0.78 0 0 -16 964.10 39.00 0 0 16 1049.00 42.46 0 0 -17 0.26 0.78 0 0 17 0.09 0.82 0 0 18 1683.00 67.98 0 0 -19 0.37 0.77 0 0 19 0.70 0.91 0 0 -20 49.16 2.32 0 0 20 52.06 2.57 0 0 -21 0.31 0.79 0 0 21 0.40 1.04 0 0 -22 172.60 7.19 0 0 22 172.20 7.28 0 0 -23 -0.02 0.91 0 0 23 -1.29 1.00 0 0 -24 83.67 3.65 0 0 24 85.40 3.87 0 0 -25 -0.27 0.76 0 0 25 -0.40 1.10 0 0 -26 517.60 21.05 0 0 26 508.80 20.77 0 0 -27 0.45 0.83 0 0 27 0.16 1.06 0 0 -28 2.90 0.87 0 0 28 5.08 1.18 0 0 -29 1.09 0.80 0 0 29 0.67 1.22 0 0 -30 137.70 5.85 0 0 30 116.80 5.10 0 0 -31 -0.73 0.79 0 0 31 1.03 1.14 0 0 -32 6.09 0.92 0 0 32 5.71 1.22 0 0 -33 0.67 0.75 0 0 33 2.18 1.10 0 0 -34 18.20 1.19 0 0 34 18.79 1.54 0 0 -35 0.86 0.86 0 0 35 0.47 1.23 0 0 -36 1.42 0.81 0 0 36 3.09 1.14 0 0 -37 0.46 0.83 0 0 37 0.53 1.11 0 0 -38 24.29 1.35 0 0 38 24.77 1.65 0 0 -39 1.43 0.80 0 0 39 1.09 1.04 0 -1 39 0.74 1.07 0 1 -39 1.38 0.78 0 -1 38 0.42 1.04 0 1 -38 0.48 0.76 0 -1 37 -0.62 1.05 0 1 -37 0.93 0.82 0 -1 36 -1.57 1.10 0 1 -36 1.67 0.78 0 -1 35 -1.05 1.15 0 1 -35 0.00 0.84 0 -1 34 1.19 1.15 0 1 -34 -0.14 0.88 0 -1 33 0.78 1.12 0 1 -33 1.76 0.79 0 -1 32 -1.41 1.10 0 1 -32 0.26 0.80 0 -1 31 0.25 1.09 0 1 -31 1.03 0.83 0 -1 30 1.21 1.13 0 1 -30 2.26 0.82 0 -1 29 0.49 1.19 0 1 -29 1.51 0.82 0 -1 28 1.21 1.16 0 1 -28 1.47 0.86 0 -1 27 3.00 1.17 0 1 -27 2.53 0.84 0 -1 26 3.08 1.07 0 1 -26 0.88 0.82 0 -1 25 1.05 1.08 0 1 -25 0.96 0.85 0 -1 24 2.32 1.09 0 1 -24 0.52 0.82 0 -1 23 -0.70 1.04 0 1 -23 1.79 0.95 0 -1 22 1.25 1.04 0 1 -22 1.47 0.91 0 -1 21 2.33 1.05 0 1 -21 1.24 0.83 0 -1 20 0.41 1.03 0 1 -20 0.46 0.81 0 -1 19 2.20 1.00 0 1 -19 1.80 0.81 0 -1 18 0.74 0.94 0 1 -18 1.64 0.79 0 -1 17 2.63 0.95 0 1 -17 4.10 0.79 0 -1 16 2.74 0.92 0 1 -16 7.23 0.82 0 -1 15 1.07 0.84 0 1 -15 1.64 0.68 0 -1 14 -0.61 0.77 0 1 -14 0.65 0.56 0 -1 13 -1.07 0.73 0 1 -13 0.12 0.59 0 -1 12 -0.31 0.72 0 1 -12 2.40 0.65 0 -1 11 1.13 0.63 0 1 -11 2.00 0.60 0 -1 10 0.99 0.56 0 1 -10 0.69 0.52 0 -1 9 3.09 0.58 0 1 -9 3.57 0.54 0 -1 8 0.81 0.47 0 1 -8 0.12 0.48 0 -1 7 2.05 0.48 0 1 -7 1.34 0.44 0 -1 6 1.11 0.42 0 1 -6 1.71 0.39 0 -1 5 1.86 0.39 0 1 -5 0.49 0.34 0 -1 4 0.32 0.30 0 1 -4 0.84 0.30 0 -1 3 3.46 0.32 0 1 -3 4.74 0.34 0 -1 2 0.71 0.18 0 1 -2 0.48 0.18 0 -1 1 0.67 0.15 0 1 -1 0.89 0.14 0 -1 0 0.54 0.11 0 -1 -1 0.87 0.12 0 1 1 0.63 0.12 0 -1 -2 0.51 0.16 0 1 2 0.35 0.13 0 -1 -3 3.33 0.27 0 1 3 3.65 0.27 0 -1 -4 0.73 0.29 0 1 4 0.82 0.28 0 -1 -5 1.54 0.36 0 1 5 1.70 0.35 0 -1 -6 1.38 0.39 0 1 6 1.07 0.38 0 -1 -7 2.12 0.44 0 1 7 2.45 0.46 0 -1 -8 0.25 0.44 0 1 8 0.24 0.46 0 -1 -9 3.62 0.53 0 1 9 2.56 0.50 0 -1 -10 0.29 0.51 0 1 10 0.49 0.53 0 -1 -11 1.54 0.55 0 1 11 2.02 0.60 0 -1 -12 0.43 0.58 0 1 12 0.47 0.61 0 -1 -13 0.16 0.65 0 1 13 0.33 0.62 0 -1 -14 0.02 0.66 0 1 14 0.70 0.74 0 -1 -15 0.32 0.68 0 1 15 0.20 0.75 0 -1 -16 1.29 0.77 0 1 16 0.98 0.80 0 -1 -17 2.93 0.80 0 1 17 1.34 0.88 0 -1 -18 3.57 0.77 0 1 18 12.41 1.11 0 -1 -19 2.29 0.75 0 1 19 1.34 0.95 0 -1 -20 1.92 0.82 0 1 20 1.15 0.93 0 -1 -21 1.88 0.87 0 1 21 1.51 1.02 0 -1 -22 0.69 0.89 0 1 22 0.30 1.04 0 -1 -23 0.13 0.92 0 1 23 -0.67 0.99 0 -1 -24 1.87 0.90 0 1 24 0.90 1.08 0 -1 -25 0.29 0.81 0 1 25 -0.20 1.05 0 -1 -26 1.66 0.87 0 1 26 -0.11 1.10 0 -1 -27 2.84 0.87 0 1 27 2.96 1.08 0 -1 -28 -0.38 0.85 0 1 28 0.45 1.10 0 -1 -29 2.58 0.90 0 1 29 0.94 1.17 0 -1 -30 -0.27 0.88 0 1 30 0.01 1.24 0 -1 -31 2.23 0.87 0 1 31 0.11 1.11 0 -1 -32 1.01 0.86 0 1 32 0.52 1.11 0 -1 -33 0.47 0.81 0 1 33 -0.31 1.20 0 -1 -34 -0.16 0.76 0 1 34 2.13 1.23 0 -1 -35 1.02 0.84 0 1 35 0.49 1.16 0 -1 -36 0.60 0.78 0 1 36 -0.19 1.11 0 -1 -37 0.27 0.78 0 1 37 1.19 1.09 0 -1 -38 -0.24 0.82 0 1 38 0.56 1.12 0 -1 -39 0.87 0.80 0 1 39 2.04 1.02 0 -2 39 45.53 2.23 0 2 -39 46.00 2.11 0 -2 38 1.82 1.09 0 2 -38 2.90 0.89 0 -2 37 210.90 8.80 0 2 -37 200.90 8.27 0 -2 36 54.53 2.73 0 2 -36 42.53 2.10 0 -2 35 182.00 7.66 0 2 -35 187.10 7.80 0 -2 34 0.28 1.11 0 2 -34 1.13 0.80 0 -2 33 209.80 8.79 0 2 -33 220.50 9.09 0 -2 32 27.30 1.75 0 2 -32 27.23 1.49 0 -2 31 154.60 6.61 0 2 -31 145.70 6.12 0 -2 30 0.62 1.15 0 2 -30 0.55 0.81 0 -2 29 260.40 10.83 0 2 -29 258.30 10.66 0 -2 28 15.55 1.44 0 2 -28 16.92 1.20 0 -2 27 696.70 28.35 0 2 -27 795.50 32.26 0 -2 26 0.42 1.11 0 2 -26 1.05 0.86 0 -2 25 632.40 25.74 0 2 -25 660.10 26.80 0 -2 24 108.90 4.77 0 2 -24 110.30 4.72 0 -2 23 271.40 11.24 0 2 -23 262.10 10.79 0 -2 22 2.77 1.05 0 2 -22 3.24 0.84 0 -2 21 601.90 24.51 0 2 -21 685.90 27.84 0 -2 20 142.50 6.08 0 2 -20 137.00 5.77 0 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29.60 0 -2 -16 116.70 4.95 0 2 16 115.30 4.92 0 -2 -17 16.88 1.23 0 2 17 20.05 1.31 0 -2 -18 108.00 4.64 0 2 18 108.00 4.67 0 -2 -19 1630.00 65.83 0 2 19 1444.00 58.36 0 -2 -20 145.80 6.15 0 2 20 146.30 6.22 0 -2 -21 660.00 26.81 0 2 21 642.40 26.12 0 -2 -22 3.00 0.90 0 2 22 3.76 1.05 0 -2 -23 287.70 11.83 0 2 23 288.10 11.91 0 -2 -24 114.30 4.90 0 2 24 97.49 4.33 0 -2 -25 649.80 26.37 0 2 25 702.30 28.56 0 -2 -26 -0.21 0.77 0 2 26 -1.52 1.05 0 -2 -27 707.80 28.68 0 2 27 668.60 27.20 0 -2 -28 16.00 1.15 0 2 28 15.63 1.41 0 -2 -29 286.70 11.77 0 2 29 273.80 11.36 0 -2 -30 0.93 0.81 0 2 30 2.08 1.15 0 -2 -31 164.00 6.87 0 2 31 143.00 6.14 0 -2 -32 31.26 1.70 0 2 32 32.48 1.95 0 -2 -33 228.10 9.42 0 2 33 251.80 10.48 0 -2 -34 0.97 0.87 0 2 34 1.07 1.20 0 -2 -35 203.90 8.46 0 2 35 196.00 8.24 0 -2 -36 39.87 1.96 0 2 36 44.36 2.33 0 -2 -37 189.40 7.85 0 2 37 187.50 7.85 0 -2 -38 3.63 0.76 0 2 38 1.70 1.09 0 -2 -39 49.14 2.24 0 2 39 47.61 2.38 0 3 -39 -0.20 0.76 0 -3 38 -0.71 0.98 0 3 -38 -1.17 0.72 0 -3 37 1.22 1.05 0 3 -37 1.98 0.77 0 -3 36 0.71 1.08 0 3 -36 0.28 0.89 0 -3 35 2.33 1.13 0 3 -35 0.24 0.78 0 -3 34 -1.00 1.06 0 3 -34 -0.37 0.82 0 -3 33 0.37 1.14 0 3 -33 2.51 0.97 0 -3 32 2.00 1.15 0 3 -32 1.04 0.86 0 -3 31 0.53 1.13 0 3 -31 1.30 0.84 0 -3 30 0.08 1.08 0 3 -30 -0.42 0.92 0 -3 29 1.94 1.16 0 3 -29 -0.36 0.81 0 -3 28 -0.76 1.11 0 3 -28 0.93 0.89 0 -3 27 0.23 1.10 0 3 -27 2.44 0.84 0 -3 26 0.97 1.01 0 3 -26 2.04 0.91 0 -3 25 3.18 1.06 0 3 -25 2.66 0.89 0 -3 24 -0.15 1.04 0 3 -24 2.09 0.80 0 -3 23 0.73 1.14 0 3 -23 1.94 0.93 0 -3 22 1.82 1.13 0 3 -22 0.59 0.95 0 -3 21 12.57 1.32 0 3 -21 2.65 0.91 0 -3 20 45.54 2.31 0 3 -20 26.94 1.59 0 -3 19 4.10 0.97 0 3 -19 1.80 0.84 0 -3 18 3.19 1.01 0 3 -18 0.14 0.81 0 -3 17 2.62 0.93 0 3 -17 8.84 0.95 0 -3 16 0.25 0.87 0 3 -16 2.01 0.77 0 -3 15 6.52 0.98 0 3 -15 5.47 0.83 0 -3 14 5.46 0.87 0 3 -14 5.09 0.81 0 -3 13 0.53 0.73 0 3 -13 2.62 0.68 0 -3 12 1.04 0.73 0 3 -12 1.13 0.61 0 -3 11 1.22 0.64 0 3 -11 1.52 0.62 0 -3 10 2.37 0.67 0 3 -10 2.54 0.65 0 -3 9 -0.78 0.54 0 3 -9 -0.13 0.56 0 -3 8 3.19 0.58 0 3 -8 3.23 0.58 0 -3 7 0.98 0.50 0 3 -7 0.80 0.49 0 -3 6 3.06 0.52 0 3 -6 3.11 0.50 0 -3 5 4.97 0.52 0 3 -5 5.71 0.51 0 -3 4 3.36 0.46 0 3 -4 3.97 0.46 0 -3 3 7.95 0.56 0 3 -3 7.97 0.55 0 -3 2 3.92 0.41 0 3 -2 3.90 0.39 0 -3 1 2.90 0.38 0 3 -1 2.33 0.36 0 -3 0 3.64 0.35 0 -3 0 3.70 0.37 0 -3 -1 1.93 0.31 0 3 1 1.62 0.28 0 -3 -2 3.89 0.35 0 3 2 3.62 0.35 0 -3 -3 8.24 0.51 0 3 3 7.73 0.47 0 -3 -4 3.15 0.38 0 3 4 3.66 0.38 0 -3 -5 4.36 0.43 0 3 5 4.65 0.43 0 -3 -6 2.78 0.43 0 3 6 2.25 0.40 0 -3 -7 1.81 0.42 0 3 7 1.63 0.42 0 -3 -8 3.47 0.55 0 3 8 4.07 0.51 0 -3 -9 0.84 0.50 0 3 9 0.43 0.49 0 -3 -10 2.47 0.51 0 3 10 2.34 0.58 0 -3 -11 0.90 0.54 0 3 11 0.37 0.61 0 -3 -12 1.70 0.65 0 3 12 1.91 0.60 0 -3 -13 1.50 0.73 0 3 13 1.19 0.63 0 -3 -14 2.54 0.77 0 3 14 3.16 0.71 0 -3 -15 6.24 0.84 0 3 15 4.39 0.83 0 -3 -16 1.70 0.76 0 3 16 2.88 0.82 0 -3 -17 5.03 0.84 0 3 17 6.36 0.94 0 -3 -18 0.62 0.82 0 3 18 0.64 0.86 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11 25 42.63 2.23 2 -11 -25 42.13 2.17 -2 11 24 6.34 1.25 2 -11 -24 2.39 1.06 -2 11 23 39.43 2.03 2 -11 -23 35.34 1.93 -2 11 22 3.78 1.04 2 -11 -22 4.60 1.03 -2 11 21 137.60 5.84 2 -11 -21 124.60 5.31 -2 11 20 0.86 1.04 2 -11 -20 0.14 0.92 -2 11 19 123.10 5.26 2 -11 -19 115.40 4.98 -2 11 18 11.00 1.16 2 -11 -18 11.82 1.19 -2 11 17 60.99 2.82 2 -11 -17 63.54 2.90 -2 11 16 3.91 1.00 2 -11 -16 4.22 1.04 -2 11 15 74.44 3.31 2 -11 -15 76.55 3.43 -2 11 14 4.53 0.93 2 -11 -14 3.54 0.96 -2 11 13 39.24 2.01 2 -11 -13 40.08 2.04 -2 11 12 65.16 2.98 2 -11 -12 64.78 2.94 -2 11 11 213.20 8.83 2 -11 -11 221.50 9.13 -2 11 10 23.04 1.40 2 -11 -10 25.70 1.48 -2 11 9 14.03 1.17 2 -11 -9 13.40 1.11 -2 11 8 15.85 1.16 2 -11 -8 14.15 1.23 2 -11 -7 2.77 1.02 2 -11 -6 48.77 2.33 2 -11 -6 49.03 2.39 2 -11 -5 1.39 0.88 2 -11 -5 2.46 0.94 2 -11 -4 6.45 0.93 2 -11 -4 8.12 1.00 2 -11 -3 4.35 0.92 2 -11 -3 4.11 0.93 2 -11 -2 98.92 4.28 2 -11 -2 92.52 4.01 2 -11 -1 102.70 4.42 2 -11 -1 100.60 4.35 2 -11 0 252.10 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1.27 2 4 -33 14.21 1.13 -2 -4 32 6.74 1.28 2 4 -32 5.09 0.84 -2 -4 31 7.70 1.19 2 4 -31 6.87 0.85 -2 -4 30 -0.13 1.22 2 4 -30 1.45 0.86 -2 -4 29 79.77 3.72 2 4 -29 79.20 3.52 -2 -4 28 7.00 1.25 2 4 -28 6.93 0.96 -2 -4 27 1.05 1.24 2 4 -27 1.22 0.90 -2 -4 26 7.28 1.22 2 4 -26 8.28 1.00 -2 -4 25 15.18 1.36 2 4 -25 13.68 1.13 -2 -4 24 50.59 2.58 2 4 -24 51.39 2.46 -2 -4 23 191.10 8.07 2 4 -23 192.50 8.01 -2 -4 22 18.37 1.50 2 4 -22 17.20 1.25 -2 -4 21 116.40 5.09 2 4 -21 129.60 5.51 -2 -4 20 21.14 1.54 2 4 -20 19.32 1.34 -2 -4 19 3.34 1.12 2 4 -19 2.13 0.86 -2 -4 18 38.66 2.09 2 4 -18 38.52 1.97 -2 -4 17 7.58 1.08 2 4 -17 9.90 1.01 -2 -4 16 13.13 1.17 2 4 -16 15.54 1.13 -2 -4 15 97.16 4.26 2 4 -15 117.50 4.99 -2 -4 14 38.12 1.97 2 4 -14 37.23 1.83 -2 -4 13 1.99 0.86 2 4 -13 1.27 0.71 -2 -4 12 24.54 1.42 2 4 -12 25.61 1.39 -2 -4 11 82.42 3.58 2 4 -11 96.80 4.12 -2 -4 10 28.58 1.47 2 4 -10 35.10 1.69 -2 -4 9 2.83 0.64 2 4 -9 3.93 0.63 -2 -4 8 24.47 1.29 2 4 -8 23.55 1.20 -2 -4 7 72.40 3.12 2 4 -7 73.27 3.11 -2 -4 6 17.12 0.96 2 4 -6 16.59 0.91 -2 -4 5 241.40 9.84 2 4 -5 250.80 10.21 -2 -4 4 137.00 5.63 2 4 -4 137.70 5.64 -2 -4 3 142.40 5.83 2 4 -3 138.80 5.68 -2 -4 2 60.73 2.54 2 4 -2 64.08 2.66 -2 -4 1 59.78 2.48 2 4 -1 68.82 2.84 -2 -4 0 83.88 3.44 2 4 0 80.64 3.31 -2 -4 -5 268.50 11.15 2 4 5 266.20 11.02 -2 -4 -6 16.61 0.75 2 4 6 17.52 0.78 -2 -4 -7 69.99 2.89 2 4 7 74.21 3.06 -2 -4 -8 23.91 1.08 2 4 8 23.94 1.09 -2 -4 -9 3.99 0.45 2 4 9 4.18 0.48 -2 -4 -10 28.67 1.31 2 4 10 32.47 1.50 -2 -4 -11 92.84 3.86 2 4 11 85.46 3.59 -2 -4 -12 25.58 1.22 2 4 12 25.17 1.28 -2 -4 -13 2.28 0.58 2 4 13 1.84 0.64 -2 -4 -14 38.17 1.79 2 4 14 39.96 1.88 -2 -4 -15 102.20 4.33 2 4 15 98.27 4.20 -2 -4 -16 10.71 0.89 2 4 16 10.73 0.97 -2 -4 -17 8.22 0.87 2 4 17 9.74 0.98 -2 -4 -18 40.33 1.98 2 4 18 37.17 1.92 -2 -4 -19 0.44 0.77 2 4 19 1.55 0.94 -2 -4 -20 19.72 1.17 2 4 20 20.59 1.42 -2 -4 -21 111.10 4.70 2 4 21 109.30 4.73 -2 -4 -22 17.02 1.11 2 4 22 17.73 1.37 -2 -4 -23 193.80 8.01 2 4 23 199.50 8.35 -2 -4 -24 48.73 2.31 2 4 24 48.46 2.46 -2 -4 -25 14.89 1.13 2 4 25 14.48 1.37 -2 -4 -26 8.06 0.98 2 4 26 7.74 1.19 -2 -4 -27 0.85 0.86 2 4 27 1.13 1.24 -2 -4 -28 5.49 0.95 2 4 28 7.36 1.24 -2 -4 -29 76.09 3.31 2 4 29 75.96 3.51 -2 -4 -30 1.91 0.83 2 4 30 -0.78 1.25 -2 -4 -31 4.55 0.99 2 4 31 8.59 1.33 -2 -4 -32 5.71 0.97 2 4 32 4.95 1.18 -2 -4 -33 13.12 1.12 2 4 33 10.33 1.34 -2 -4 -34 7.91 1.00 2 4 34 8.17 1.30 -2 -4 -35 7.39 1.08 2 4 35 7.53 1.29 -2 -4 -36 1.01 0.91 2 4 36 2.04 1.07 -2 -4 -37 13.00 1.07 2 4 37 13.89 1.36 -2 -4 -38 1.13 0.81 -2 -5 37 18.27 1.34 2 5 -37 17.88 1.10 -2 -5 36 5.32 1.09 2 5 -36 5.45 0.86 -2 -5 35 12.28 1.29 2 5 -35 29.87 1.59 -2 -5 34 0.50 1.05 2 5 -34 1.28 0.80 -2 -5 33 12.60 1.36 2 5 -33 13.22 1.04 -2 -5 32 45.07 2.36 2 5 -32 44.72 2.17 -2 -5 31 32.15 1.94 2 5 -31 29.46 1.63 -2 -5 30 10.81 1.32 2 5 -30 13.04 1.14 -2 -5 29 3.71 1.14 2 5 -29 3.10 0.94 -2 -5 28 1.25 1.16 2 5 -28 1.11 0.85 -2 -5 27 93.38 4.18 2 5 -27 100.40 4.35 -2 -5 26 39.94 2.26 2 5 -26 35.68 1.86 -2 -5 25 20.80 1.61 2 5 -25 21.24 1.37 -2 -5 24 5.18 1.13 2 5 -24 5.13 0.93 -2 -5 23 45.11 2.37 2 5 -23 42.81 2.12 -2 -5 22 182.60 7.75 2 5 -22 162.80 6.84 -2 -5 21 212.20 8.91 2 5 -21 203.70 8.46 -2 -5 20 41.96 2.25 2 5 -20 42.36 2.14 -2 -5 19 0.84 1.05 2 5 -19 1.43 0.93 -2 -5 18 259.20 10.77 2 5 -18 212.30 8.80 -2 -5 17 3.12 0.99 2 5 -17 3.09 0.84 -2 -5 16 433.50 17.70 2 5 -16 451.10 18.37 -2 -5 15 34.73 1.89 2 5 -15 34.87 1.77 -2 -5 14 688.50 27.97 2 5 -14 750.20 30.39 -2 -5 13 5.94 0.98 2 5 -13 5.84 0.81 -2 -5 12 243.90 10.05 2 5 -12 244.10 10.03 -2 -5 11 32.87 1.71 2 5 -11 35.19 1.75 -2 -5 10 1204.00 48.66 2 5 -10 1112.00 44.91 -2 -5 9 109.40 4.65 2 5 -9 110.70 4.64 -2 -5 7 10.10 0.85 2 5 -7 11.52 0.80 -2 -5 6 814.50 32.93 2 5 -6 894.70 36.14 -2 -5 5 38.27 1.76 2 5 -5 38.16 1.70 -2 -5 3 121.30 5.00 2 5 -3 129.10 5.30 -2 -5 1 6.18 0.44 2 5 -1 7.65 0.47 -2 -5 -7 10.41 0.53 2 5 7 12.29 0.61 -2 -5 -9 95.49 3.94 2 5 9 104.60 4.31 -2 -5 -10 1146.00 46.31 -2 -5 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0.81 0.80 2 6 21 1.75 0.99 -2 -6 -22 0.54 0.72 2 6 22 2.03 1.05 -2 -6 -23 2.68 0.82 2 6 23 -0.62 1.06 -2 -6 -24 19.67 1.23 2 6 24 24.23 1.65 -2 -6 -25 1.93 0.82 2 6 25 1.82 1.14 -2 -6 -26 15.98 1.16 2 6 26 14.15 1.42 -2 -6 -27 1.56 0.81 2 6 27 1.27 1.18 -2 -6 -28 3.65 0.91 2 6 28 2.99 1.24 -2 -6 -29 5.64 0.98 2 6 29 6.80 1.21 -2 -6 -30 1.37 0.92 2 6 30 1.97 1.23 -2 -6 -31 1.84 0.94 2 6 31 8.25 1.37 -2 -6 -32 2.70 0.94 2 6 32 4.64 1.20 -2 -6 -33 1.85 0.94 2 6 33 2.05 1.29 -2 -6 -34 0.73 0.84 2 6 34 0.92 1.23 -2 -6 -35 0.22 0.83 2 6 35 2.60 1.30 -2 -6 -36 5.76 0.99 2 6 36 8.11 1.18 -2 -7 35 98.10 4.24 2 7 -35 99.69 4.24 -2 -7 34 0.61 1.13 2 7 -34 1.06 0.76 -2 -7 33 143.30 6.12 2 7 -33 139.60 5.87 -2 -7 32 24.54 1.72 2 7 -32 27.43 1.51 -2 -7 31 137.70 5.92 2 7 -31 138.80 5.84 -2 -7 30 12.27 1.25 2 7 -30 10.53 1.03 -2 -7 29 157.50 6.69 2 7 -29 145.90 6.14 -2 -7 28 12.84 1.34 2 7 -28 13.43 1.10 -2 -7 27 371.30 15.23 2 7 -27 385.90 15.76 -2 -7 26 16.82 1.49 2 7 -26 18.96 1.37 -2 -7 25 232.00 9.67 2 7 -25 238.70 9.88 -2 -7 24 18.59 1.53 2 7 -24 20.74 1.35 -2 -7 23 227.50 9.52 2 7 -23 244.00 10.07 -2 -7 22 53.04 2.63 2 7 -22 53.16 2.51 -2 -7 21 228.10 9.50 2 7 -21 231.50 9.57 -2 -7 20 17.96 1.44 2 7 -20 17.44 1.26 -2 -7 19 121.50 5.24 2 7 -19 143.70 6.07 -2 -7 18 41.25 2.15 2 7 -18 51.23 2.46 -2 -7 17 501.60 20.48 2 7 -17 492.40 20.06 -2 -7 16 1.75 1.01 2 7 -16 2.95 0.88 -2 -7 15 557.30 22.70 2 7 -15 536.50 21.81 -2 -7 14 0.92 1.02 2 7 -14 2.09 0.86 -2 -7 13 28.40 1.64 2 7 -13 21.93 1.35 -2 -7 12 16.39 1.30 2 7 -12 18.03 1.19 -2 -7 11 209.10 8.68 2 7 -11 197.00 8.14 -2 -7 10 35.97 1.82 2 7 -10 40.12 1.92 -2 -7 9 132.20 5.56 2 7 -9 127.90 5.35 -2 -7 8 10.82 0.99 2 7 -8 10.99 0.90 -2 -7 7 84.33 3.65 2 7 -7 85.83 3.63 -2 -7 6 37.17 1.76 2 7 -6 40.91 1.86 -2 -7 5 348.40 14.16 2 7 -5 383.60 15.57 -2 -7 4 4.53 0.60 2 7 -4 4.02 0.55 -2 -7 3 6.01 0.59 2 7 -3 6.92 0.59 -2 -7 2 18.59 0.96 -2 -7 1 0.59 0.45 -2 -7 1 0.14 0.42 -2 -7 0 206.30 8.40 -2 -7 0 185.20 7.57 -2 -7 -1 -0.12 0.38 -2 -7 -1 -0.05 0.32 -2 -7 -2 14.81 0.70 -2 -7 -2 13.78 0.67 -2 -7 -8 10.65 0.61 2 7 8 10.49 0.56 -2 -7 -9 121.10 4.99 2 7 9 123.80 5.07 -2 -7 -10 34.78 1.53 2 7 10 37.30 1.63 -2 -7 -11 191.70 7.82 2 7 11 206.40 8.42 -2 -7 -12 15.21 0.86 2 7 12 16.22 0.94 -2 -7 -13 22.04 1.14 2 7 13 23.75 1.22 -2 -7 -14 1.52 0.61 2 7 14 1.86 0.69 -2 -7 -15 513.50 20.83 2 7 15 565.70 22.93 -2 -7 -16 1.31 0.72 2 7 16 0.49 0.73 -2 -7 -17 466.50 18.97 2 7 17 510.40 20.72 -2 -7 -18 36.67 1.75 2 7 18 40.29 1.98 -2 -7 -19 122.50 5.12 2 7 19 135.20 5.67 -2 -7 -20 17.00 1.10 2 7 20 18.02 1.26 -2 -7 -21 237.50 9.76 2 7 21 237.60 9.80 -2 -7 -22 52.46 2.42 2 7 22 56.25 2.64 -2 -7 -23 208.40 8.64 2 7 23 225.70 9.34 -2 -7 -24 18.29 1.22 2 7 24 18.25 1.37 -2 -7 -25 229.20 9.44 2 7 25 238.70 9.88 -2 -7 -26 19.34 1.31 2 7 26 18.00 1.37 -2 -7 -27 370.10 15.13 2 7 27 389.30 15.94 -2 -7 -28 14.56 1.19 2 7 28 11.41 1.29 -2 -7 -29 143.70 6.06 2 7 29 141.70 6.04 -2 -7 -30 13.53 1.17 2 7 30 11.18 1.30 -2 -7 -31 137.80 5.82 2 7 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662.80 26.90 4 -10 0 662.30 26.87 4 -10 3 54.88 2.61 4 -10 3 50.18 2.38 4 -10 4 212.90 8.85 4 -10 4 187.00 7.76 4 -10 5 0.23 0.94 4 -10 5 1.36 0.96 4 -10 6 175.50 7.34 4 -10 6 179.50 7.48 4 -10 7 50.57 2.44 4 -10 7 47.48 2.29 4 -10 8 118.50 5.12 4 -10 8 103.20 4.40 4 -10 9 14.90 1.39 4 -10 9 14.78 1.16 4 -10 10 231.10 9.54 4 -10 10 217.70 9.07 4 -10 11 31.63 1.78 4 -10 11 31.75 1.78 4 -10 12 59.97 2.86 4 -10 12 60.82 2.83 4 -10 13 0.98 1.13 4 -10 13 0.70 0.90 4 -10 14 20.73 1.52 4 -10 14 23.57 1.56 4 -10 15 10.01 1.23 4 -10 15 8.70 1.12 4 -10 16 158.80 6.68 4 -10 16 149.80 6.34 4 -10 17 43.84 2.24 4 -10 17 39.76 2.03 4 -10 18 93.27 4.11 4 -10 18 92.02 4.02 4 -10 19 89.50 3.99 4 -10 19 103.80 4.46 4 -10 20 38.46 2.10 4 -10 20 41.46 2.05 4 -10 21 14.69 1.34 4 -10 21 12.03 1.14 4 -10 22 26.39 1.72 4 -10 22 27.86 1.62 4 -10 23 1.73 1.08 4 -10 24 1.84 1.08 4 -10 25 0.17 1.08 4 -10 26 0.12 1.01 4 -10 27 30.36 1.80 -4 10 -28 1.59 0.69 4 -10 28 0.06 0.99 -4 10 -29 62.28 2.76 4 -10 29 69.07 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24 24.56 1.66 -4 9 -25 0.29 0.91 4 -9 25 1.74 1.11 -4 9 -26 14.18 1.11 4 -9 26 13.22 1.38 -4 9 -27 0.76 0.85 4 -9 27 4.07 1.09 -4 9 -28 3.98 0.92 4 -9 28 3.61 1.11 -4 9 -29 4.46 0.86 4 -9 29 5.04 1.04 -4 9 -30 7.61 0.95 4 -9 30 6.49 1.05 -4 9 -31 2.71 0.87 4 -9 31 2.27 1.00 -4 8 32 -0.41 0.98 4 -8 -32 1.00 0.77 -4 8 31 43.67 2.19 4 -8 -31 41.57 2.01 -4 8 30 5.42 1.15 4 -8 -30 4.97 0.91 -4 8 29 154.40 6.52 4 -8 -29 151.40 6.33 -4 8 28 2.00 1.08 4 -8 -28 -0.94 0.96 -4 8 27 144.60 6.14 4 -8 -27 123.30 5.25 -4 8 26 27.49 1.65 4 -8 -26 29.37 1.66 -4 8 25 60.88 2.86 4 -8 -25 62.81 2.84 -4 8 24 57.74 2.75 4 -8 -24 60.37 2.77 -4 8 23 148.30 6.28 4 -8 -23 154.90 6.48 -4 8 22 33.17 1.85 4 -8 -22 28.77 1.63 -4 8 21 110.30 4.77 4 -8 -21 100.20 4.37 -4 8 20 48.74 2.42 4 -8 -20 49.68 2.46 -4 8 19 199.30 8.30 4 -8 -19 183.50 7.72 -4 8 18 271.10 11.17 4 -8 -18 291.70 12.03 -4 8 17 95.43 4.18 4 -8 -17 95.44 4.19 -4 8 16 212.90 8.83 4 -8 -16 246.10 10.20 -4 8 15 4.65 0.99 4 -8 -15 1.87 0.94 -4 8 14 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24 136.60 5.86 -4 -4 -25 42.43 2.09 4 4 25 44.15 2.34 -4 -4 -26 19.23 1.35 4 4 26 18.92 1.55 -4 -4 -27 90.58 3.97 4 4 27 87.78 3.95 -4 -4 -28 4.46 0.93 4 4 28 3.51 1.25 -4 -4 -29 42.07 2.10 4 4 29 40.93 2.27 -4 -4 -30 16.32 1.20 4 4 30 14.54 1.49 -4 -4 -31 6.59 1.07 4 4 31 7.37 1.37 -4 -4 -32 -0.32 0.97 4 4 32 -1.12 1.26 -4 -4 -33 78.93 3.49 4 4 33 79.41 3.63 -4 -4 -34 0.28 0.96 4 4 34 1.76 1.17 -4 -4 -35 37.02 1.86 4 4 35 34.74 2.02 -4 -4 -36 3.90 0.96 4 4 36 3.58 1.09 -4 -5 35 1.89 0.98 4 5 -35 1.37 0.75 -4 -5 34 1.50 1.03 4 5 -34 1.54 0.76 -4 -5 33 6.09 1.23 4 5 -33 8.06 0.93 -4 -5 32 2.21 1.17 4 5 -32 3.15 0.88 -4 -5 31 1.64 1.12 4 5 -31 0.91 0.83 -4 -5 30 0.10 1.12 4 5 -30 0.62 0.87 -4 -5 29 -1.44 1.24 4 5 -29 0.60 0.92 -4 -5 28 2.10 1.13 4 5 -28 -0.24 0.85 -4 -5 27 2.02 1.11 4 5 -27 2.88 0.90 -4 -5 26 4.36 1.13 4 5 -26 5.80 0.94 -4 -5 25 21.64 1.56 4 5 -25 24.00 1.50 -4 -5 24 4.76 1.16 4 5 -24 5.01 0.93 -4 -5 23 4.21 1.20 4 5 -23 1.00 0.87 -4 -5 22 0.03 1.12 4 5 -22 2.37 0.88 -4 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346.50 14.09 -5 -6 2 48.26 2.07 5 6 -2 44.38 1.94 -5 -6 1 109.20 4.50 5 6 -1 104.50 4.32 -5 -6 0 6.42 0.47 5 6 0 10.44 0.58 5 6 12 122.90 5.07 5 6 12 122.80 5.08 5 6 13 838.50 34.07 5 6 13 795.60 32.33 5 6 14 1.63 0.53 5 6 14 2.64 0.65 5 6 15 90.27 3.82 5 6 15 93.95 3.93 5 6 16 3.54 0.80 5 6 16 3.97 0.61 5 6 17 8.82 0.97 -5 -6 -18 75.64 3.25 5 6 18 80.24 3.50 -5 -6 -19 22.74 1.26 5 6 19 19.66 1.28 -5 -6 -20 127.20 5.32 5 6 20 119.70 5.10 -5 -6 -21 20.12 1.21 5 6 21 22.10 1.46 -5 -6 -22 101.90 4.38 5 6 22 91.16 4.01 -5 -6 -23 60.63 2.76 5 6 23 59.02 2.80 -5 -6 -24 89.58 3.89 5 6 24 84.30 3.76 -5 -6 -25 24.48 1.48 5 6 25 26.16 1.65 -5 -6 -26 87.29 3.82 5 6 26 83.74 3.78 -5 -6 -27 2.62 0.99 5 6 27 1.34 1.16 -5 -6 -28 80.13 3.55 5 6 28 81.96 3.75 -5 -6 -29 1.49 1.00 5 6 29 -0.95 1.22 -5 -6 -30 13.84 1.25 5 6 30 15.05 1.50 -5 -6 -31 39.05 2.03 5 6 31 34.40 2.00 -5 -6 -32 48.45 2.35 5 6 32 49.20 2.54 -5 -6 -33 0.20 0.97 5 6 33 -0.27 1.27 -5 -7 32 1.80 1.20 5 7 -32 4.39 0.85 -5 -7 31 0.98 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19 97.08 4.18 6 -11 19 102.70 4.44 6 -11 20 -0.70 0.94 6 -11 20 1.15 0.86 6 -11 21 28.34 1.69 6 -11 21 25.18 1.45 6 -11 22 1.49 1.12 6 -11 22 -0.10 0.88 6 -11 23 41.51 2.07 6 -11 23 41.95 1.99 -6 10 26 0.34 0.91 6 -10 -26 -1.09 0.88 -6 10 25 2.50 1.00 6 -10 -25 2.89 0.85 -6 10 24 11.37 1.18 6 -10 -24 14.01 1.13 -6 10 23 2.08 0.99 6 -10 -23 1.59 0.90 -6 10 22 4.41 1.10 6 -10 -22 2.59 0.86 -6 10 21 1.60 1.01 6 -10 -21 1.59 0.88 -6 10 20 17.30 1.33 6 -10 -20 19.84 1.34 -6 10 19 9.25 1.16 6 -10 -19 10.88 1.14 -6 10 18 10.21 1.20 6 -10 -18 12.57 1.18 -6 10 17 0.05 0.98 6 -10 -17 2.36 0.95 -6 10 16 15.25 1.28 6 -10 -16 13.85 1.20 -6 10 15 84.90 3.79 6 -10 -15 85.66 3.78 -6 10 14 58.27 2.77 6 -10 -14 59.42 2.79 -6 10 13 2.64 1.00 6 -10 -13 0.29 0.97 -6 10 12 3.53 0.99 6 -10 -12 3.25 0.98 -6 10 11 1.96 0.98 6 -10 -11 1.47 0.94 -6 10 10 1.75 0.98 6 -10 -10 0.51 0.84 -6 10 9 2.46 0.97 6 -10 -9 0.56 0.91 -6 10 8 18.07 1.34 6 -10 -8 19.42 1.34 -6 10 7 17.71 1.35 6 -10 -7 16.61 1.24 -6 10 6 1.47 1.11 6 -10 -6 0.88 0.99 -6 10 5 49.12 2.40 6 -10 -5 49.64 2.40 6 -10 -4 55.63 2.67 6 -10 -3 12.44 1.24 6 -10 -3 12.18 1.29 6 -10 -2 17.53 1.48 6 -10 -2 17.47 1.33 6 -10 -1 67.97 3.18 6 -10 -1 61.44 2.88 6 -10 0 2.25 1.04 6 -10 0 2.99 1.06 6 -10 1 73.01 3.33 6 -10 1 68.58 3.15 6 -10 2 18.38 1.38 6 -10 2 17.23 1.37 6 -10 4 48.46 2.38 6 -10 4 55.94 2.68 6 -10 5 42.89 2.21 6 -10 5 49.02 2.42 6 -10 6 -0.12 1.01 6 -10 6 1.05 0.92 6 -10 7 16.75 1.31 6 -10 7 17.47 1.23 6 -10 8 18.02 1.34 6 -10 8 15.92 1.21 6 -10 9 2.72 0.96 6 -10 9 3.06 0.89 6 -10 10 0.45 0.94 6 -10 10 0.72 1.14 6 -10 11 0.90 0.89 6 -10 11 1.14 1.00 6 -10 12 3.16 1.04 6 -10 12 3.89 0.94 6 -10 13 0.19 0.86 6 -10 13 1.33 1.05 6 -10 15 86.30 3.86 6 -10 15 86.52 3.78 6 -10 16 14.23 1.37 6 -10 16 14.77 1.16 6 -10 17 1.10 1.04 6 -10 17 0.87 0.90 6 -10 18 12.25 1.11 6 -10 18 8.93 1.16 6 -10 19 8.44 1.15 6 -10 19 9.22 1.09 6 -10 20 18.56 1.40 6 -10 20 18.06 1.25 6 -10 21 1.59 1.10 6 -10 21 2.84 0.88 6 -10 23 2.10 1.08 6 -10 23 4.03 0.88 6 -10 24 11.23 1.17 6 -10 24 13.50 1.04 6 -10 25 3.11 0.96 6 -10 25 3.90 0.89 6 -10 26 -0.32 0.96 6 -10 26 1.39 0.72 -6 9 28 0.69 1.03 6 -9 -28 1.09 0.84 -6 9 27 8.84 1.09 6 -9 -27 9.16 0.98 -6 9 26 5.83 1.05 6 -9 -26 4.29 0.90 -6 9 25 -0.58 1.07 6 -9 -25 1.36 0.94 -6 9 24 53.28 2.59 6 -9 -24 50.81 2.40 -6 9 23 21.88 1.49 6 -9 -23 18.66 1.31 -6 9 22 13.80 1.24 6 -9 -22 12.26 1.15 -6 9 21 53.92 2.61 6 -9 -21 58.46 2.76 -6 9 20 109.40 4.73 6 -9 -20 120.80 5.16 -6 9 19 4.08 1.13 6 -9 -19 4.83 1.01 -6 9 18 63.91 3.01 6 -9 -18 69.63 3.15 -6 9 17 9.24 1.21 6 -9 -17 10.95 1.09 -6 9 16 177.00 7.40 6 -9 -16 167.80 7.02 -6 9 15 0.29 1.00 6 -9 -15 2.60 0.91 -6 9 14 96.76 4.24 6 -9 -14 88.88 3.90 -6 9 13 13.75 1.22 6 -9 -13 16.67 1.28 -6 9 12 6.69 1.06 6 -9 -12 5.50 1.11 -6 9 11 42.76 2.18 6 -9 -11 50.21 2.44 -6 9 10 249.20 10.30 6 -9 -10 278.60 11.49 -6 9 9 24.41 1.56 6 -9 -9 28.05 1.66 -6 9 8 317.20 13.04 6 -9 -8 312.50 12.84 -6 9 7 0.38 0.97 6 -9 -7 2.90 1.02 -6 9 6 208.40 8.69 6 -9 -6 207.40 8.64 -6 9 5 0.26 1.00 6 -9 -5 -0.51 1.00 -6 9 4 264.80 10.94 6 -9 -4 251.10 10.40 6 -9 -3 10.54 1.26 6 -9 -2 370.20 15.15 6 -9 -1 35.38 1.94 6 -9 -1 32.32 1.80 6 -9 0 285.40 11.75 6 -9 0 314.50 12.90 6 -9 1 27.70 1.67 6 -9 1 29.42 1.70 6 -9 2 439.60 17.95 6 -9 2 452.90 18.44 6 -9 3 11.53 1.24 6 -9 3 13.08 1.15 6 -9 4 332.40 13.67 6 -9 4 319.40 13.08 6 -9 5 -0.34 1.06 6 -9 5 -0.63 0.86 6 -9 6 218.60 9.10 6 -9 6 190.40 7.89 6 -9 7 0.68 1.03 6 -9 7 0.22 0.94 6 -9 8 303.30 12.48 6 -9 8 308.20 12.65 6 -9 9 23.91 1.58 6 -9 9 23.56 1.49 6 -9 10 271.20 11.20 6 -9 10 258.60 10.66 6 -9 11 48.53 2.43 6 -9 11 44.45 2.23 6 -9 12 7.94 1.19 6 -9 12 7.68 1.06 6 -9 13 15.99 1.38 6 -9 13 14.49 1.17 6 -9 14 84.93 3.81 6 -9 14 77.50 3.42 6 -9 15 1.90 1.10 6 -9 15 1.42 0.85 6 -9 17 7.29 1.20 6 -9 17 8.51 1.02 6 -9 18 62.12 2.91 6 -9 18 57.85 2.72 6 -9 19 1.62 1.03 6 -9 19 0.49 0.92 6 -9 20 108.50 4.72 6 -9 20 105.50 4.52 6 -9 21 52.16 2.51 6 -9 21 50.82 2.38 6 -9 22 10.37 1.32 6 -9 22 12.51 1.14 6 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3.74 0.97 6 -8 -8 3.06 1.02 -6 8 7 5.76 1.05 6 -8 -7 7.56 1.05 -6 8 6 24.84 1.53 6 -8 -6 26.38 1.53 -6 8 5 17.75 1.31 6 -8 -5 18.46 1.34 -6 8 4 26.97 1.61 6 -8 -4 29.63 1.64 -6 8 3 64.75 2.98 6 -8 -3 69.61 3.11 -6 8 2 0.81 0.94 6 -8 -2 1.74 0.91 6 -8 -1 10.68 1.13 6 -8 0 27.19 1.70 6 -8 0 22.97 1.43 6 -8 1 11.10 1.22 6 -8 1 9.05 1.08 6 -8 2 2.38 1.07 6 -8 2 1.69 0.91 6 -8 3 63.32 2.95 6 -8 3 64.35 2.96 6 -8 4 30.51 1.78 6 -8 4 26.27 1.55 6 -8 5 15.94 1.33 6 -8 5 16.74 1.30 6 -8 6 20.97 1.45 6 -8 6 24.40 1.54 6 -8 7 7.97 1.18 6 -8 7 5.80 1.04 6 -8 8 3.37 1.13 6 -8 8 3.56 1.05 6 -8 9 0.31 0.95 6 -8 9 0.02 0.91 6 -8 10 17.19 1.28 6 -8 10 16.13 1.29 6 -8 11 0.56 0.98 6 -8 11 0.33 0.80 6 -8 12 13.98 1.30 6 -8 12 13.33 1.12 6 -8 13 2.00 1.04 6 -8 13 0.89 0.84 6 -8 14 5.40 1.11 6 -8 14 3.47 0.90 6 -8 15 -0.30 1.04 6 -8 15 1.12 0.91 6 -8 16 15.50 1.37 6 -8 16 12.71 1.20 6 -8 17 33.76 1.92 6 -8 17 39.02 2.04 6 -8 18 8.34 1.17 6 -8 18 7.41 1.06 6 -8 19 6.91 1.09 6 -8 19 4.88 0.96 6 -8 20 5.71 1.15 6 -8 20 3.92 0.90 6 -8 21 4.62 1.04 6 -8 21 2.89 0.88 6 -8 23 19.18 1.43 6 -8 23 15.24 1.25 6 -8 24 2.41 1.19 6 -8 24 3.35 0.83 6 -8 25 0.78 1.02 6 -8 25 2.47 0.95 6 -8 26 13.69 1.05 6 -8 26 13.57 1.27 6 -8 27 10.81 1.11 6 -8 27 12.49 1.12 6 -8 28 -0.91 0.79 6 -8 28 0.05 0.98 6 -8 29 9.03 1.01 6 -8 29 8.56 1.02 6 -7 -31 24.06 1.41 -6 7 30 13.14 1.21 6 -7 -30 15.69 1.09 -6 7 29 177.20 7.39 6 -7 -29 158.90 6.61 -6 7 28 6.73 1.14 6 -7 -28 6.20 0.93 -6 7 27 129.90 5.54 6 -7 -27 141.50 5.95 -6 7 26 3.17 1.08 6 -7 -26 4.92 0.94 -6 7 25 157.10 6.64 6 -7 -25 147.90 6.21 -6 7 24 56.66 2.75 6 -7 -24 54.62 2.56 -6 7 23 157.80 6.67 6 -7 -23 151.20 6.35 -6 7 22 0.13 1.08 6 -7 -22 0.75 0.91 -6 7 21 84.45 3.78 6 -7 -21 95.01 4.18 -6 7 20 10.11 1.20 6 -7 -20 15.96 1.28 -6 7 19 146.90 6.22 6 -7 -19 152.30 6.41 -6 7 18 7.07 1.14 6 -7 -18 8.08 1.06 -6 7 17 291.90 12.01 6 -7 -17 337.10 13.82 -6 7 16 16.74 1.32 6 -7 -16 15.04 1.23 -6 7 15 33.21 1.86 6 -7 -15 31.70 1.71 -6 7 14 2.69 1.02 6 -7 -14 2.95 0.98 -6 7 13 99.81 4.36 6 -7 -13 100.30 4.36 -6 7 12 22.13 1.48 6 -7 -12 25.50 1.54 -6 7 11 138.40 5.88 6 -7 -11 132.00 5.59 -6 7 10 -0.23 0.98 6 -7 -10 2.16 0.86 -6 7 9 125.00 5.34 6 -7 -9 139.60 5.90 -6 7 8 -0.51 0.85 6 -7 -8 0.56 0.84 -6 7 7 78.42 3.49 6 -7 -7 72.24 3.27 -6 7 6 0.59 0.91 6 -7 -6 1.45 0.92 -6 7 5 18.07 1.30 6 -7 -5 15.88 1.37 -6 7 4 4.11 0.94 6 -7 -4 5.28 1.04 -6 7 3 73.73 3.30 6 -7 -3 66.41 3.07 -6 7 2 5.86 1.07 6 -7 -2 2.78 0.97 -6 7 1 4.93 0.98 6 -7 -1 6.23 1.05 6 -7 0 2.54 1.03 6 -7 1 5.21 0.99 6 -7 1 4.77 0.98 6 -7 2 6.27 1.09 6 -7 2 5.05 0.97 6 -7 3 70.69 3.20 6 -7 3 72.62 3.28 6 -7 4 4.62 1.01 6 -7 4 4.01 0.91 6 -7 5 19.33 1.38 6 -7 5 18.13 1.23 6 -7 6 1.53 0.97 6 -7 6 1.93 0.85 6 -7 8 1.57 0.95 6 -7 8 -0.69 0.85 6 -7 9 126.00 5.39 6 -7 9 132.30 5.61 6 -7 10 1.23 0.94 6 -7 10 1.05 0.84 6 -7 11 147.60 6.24 6 -7 11 133.10 5.65 6 -7 12 23.41 1.51 6 -7 12 22.26 1.40 6 -7 14 2.15 1.00 6 -7 14 3.55 0.96 6 -7 15 29.87 1.77 6 -7 15 29.01 1.68 6 -7 16 12.74 1.33 6 -7 16 15.38 1.23 6 -7 17 307.80 12.65 6 -7 17 303.90 12.47 6 -7 18 6.94 1.26 6 -7 18 7.16 1.01 6 -7 19 135.10 5.76 6 -7 19 135.80 5.72 6 -7 20 9.50 1.25 6 -7 20 10.58 1.07 6 -7 21 89.77 3.98 6 -7 21 85.49 3.77 6 -7 22 2.98 1.09 6 -7 22 3.60 1.02 6 -7 23 160.10 6.76 6 -7 23 151.20 6.36 6 -7 24 58.54 2.80 6 -7 24 54.16 2.52 6 -7 26 2.33 1.12 6 -7 26 1.65 0.80 6 -7 27 141.40 5.98 6 -7 27 156.30 6.56 6 -7 28 7.05 1.14 6 -7 29 164.90 6.89 6 -7 30 13.96 1.17 -6 6 32 0.99 0.99 6 -6 -32 -0.02 0.77 -6 6 31 9.93 1.13 6 -6 -31 13.13 1.14 -6 6 30 19.67 1.50 6 -6 -30 25.11 1.42 -6 6 29 5.94 1.19 6 -6 -29 5.30 0.84 -6 6 28 4.11 1.11 6 -6 -28 4.39 0.88 -6 6 27 29.38 1.74 6 -6 -27 32.91 1.77 -6 6 26 3.00 1.12 6 -6 -26 2.00 0.96 -6 6 25 14.55 1.36 6 -6 -25 14.55 1.15 -6 6 24 38.66 2.04 6 -6 -24 38.82 1.99 -6 6 23 4.11 1.18 6 -6 -23 3.91 0.96 -6 6 22 21.50 1.49 6 -6 -22 20.14 1.36 -6 6 21 -0.22 1.01 6 -6 -21 2.12 0.93 -6 6 20 6.66 1.17 6 -6 -20 6.99 1.01 -6 6 19 1.37 1.03 6 -6 -19 0.49 0.92 -6 6 18 6.27 1.11 6 -6 -18 7.19 1.07 -6 6 17 2.42 1.08 6 -6 -17 3.58 0.97 -6 6 16 4.59 1.07 6 -6 -16 4.19 1.03 -6 6 15 4.06 1.05 6 -6 -15 4.10 0.95 -6 6 14 7.74 1.15 6 -6 -14 9.82 1.10 -6 6 13 49.93 2.43 6 -6 -13 56.17 2.69 -6 6 12 31.35 1.75 6 -6 -12 29.82 1.71 -6 6 11 1.33 0.99 6 -6 -11 0.72 1.04 -6 6 10 121.90 5.20 6 -6 -10 126.90 5.45 -6 6 9 8.19 1.05 6 -6 -9 7.48 1.04 -6 6 8 245.60 10.15 6 -6 -8 259.00 10.70 -6 6 7 6.17 1.01 6 -6 -7 5.87 0.95 -6 6 6 1.70 0.92 6 -6 -6 0.58 0.87 -6 6 5 9.76 1.05 6 -6 -5 10.05 1.15 -6 6 4 7.55 1.02 6 -6 -4 9.45 1.05 -6 6 3 3.50 0.90 6 -6 -3 5.44 0.95 -6 6 2 17.74 1.28 6 -6 -2 15.66 1.21 -6 6 1 2.01 0.87 6 -6 -1 2.30 0.89 -6 6 0 17.40 1.25 6 -6 0 16.14 1.19 6 -6 1 6.55 0.93 6 -6 2 14.75 1.16 6 -6 2 16.11 1.32 6 -6 3 10.08 1.01 6 -6 3 10.41 1.11 6 -6 4 7.80 0.96 6 -6 4 9.26 1.05 6 -6 5 12.11 1.17 6 -6 5 12.96 1.12 6 -6 6 0.31 0.99 6 -6 6 1.64 0.91 6 -6 7 5.92 1.05 6 -6 7 5.58 0.98 6 -6 8 249.00 10.29 6 -6 8 244.30 10.10 6 -6 9 8.71 1.23 6 -6 9 8.22 1.04 6 -6 10 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25.01 -6 -5 5 3.57 0.76 6 5 -5 1.38 0.72 -6 -5 4 329.00 13.41 6 5 -4 308.80 12.61 -6 -5 3 5.80 0.79 6 5 -3 5.74 0.77 -6 -5 2 844.90 34.18 6 5 -2 850.40 34.42 -6 -5 1 55.62 2.42 6 5 -1 55.62 2.46 -6 -5 0 675.60 27.34 6 5 0 622.90 25.24 6 5 1 50.28 2.21 6 5 2 832.20 33.71 6 5 2 782.80 31.69 6 5 3 4.73 0.52 6 5 3 5.12 0.61 6 5 4 314.90 12.81 6 5 4 327.50 13.34 6 5 5 1.62 0.49 6 5 5 1.95 0.51 6 5 6 603.50 24.49 6 5 6 631.30 25.63 6 5 7 1.75 0.50 6 5 7 1.40 0.49 6 5 8 671.90 27.25 6 5 8 643.00 26.08 6 5 9 22.74 1.16 6 5 9 23.72 1.17 6 5 10 322.90 13.14 6 5 10 300.80 12.25 6 5 11 21.64 1.11 6 5 11 20.21 1.11 6 5 12 291.70 11.88 6 5 12 273.40 11.17 6 5 13 26.08 1.31 6 5 13 22.75 1.26 6 5 14 310.20 12.64 6 5 14 285.90 11.69 6 5 15 37.06 1.83 6 5 15 41.97 1.93 6 5 16 325.70 13.28 6 5 16 309.10 12.66 6 5 17 19.42 1.32 6 5 17 20.77 1.23 6 5 18 27.46 1.60 6 5 18 30.08 1.59 6 5 19 111.60 4.78 6 5 19 109.80 4.65 6 5 20 64.93 2.99 6 5 20 73.20 3.22 6 5 21 2.94 1.06 6 5 22 3.35 1.15 -6 -5 -23 20.52 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8 -4 23.59 1.18 -6 -8 3 61.35 2.59 6 8 -3 58.81 2.50 6 8 22 6.60 0.77 6 8 22 6.64 0.70 6 8 23 2.03 0.80 6 8 23 1.88 0.76 6 8 24 -0.33 0.96 6 8 24 1.35 0.73 6 8 25 1.79 0.97 6 8 25 1.71 0.83 6 8 26 13.07 1.26 6 8 26 11.00 1.03 6 8 27 11.51 1.24 6 8 27 9.39 1.13 6 8 28 0.66 1.08 6 8 28 3.04 1.08 6 8 29 7.42 1.21 6 8 29 6.33 1.16 -6 -9 28 -1.34 1.15 6 9 -28 -1.51 1.17 -6 -9 27 6.36 1.33 6 9 -27 10.47 1.09 -6 -9 26 4.15 1.16 6 9 -26 4.27 0.98 -6 -9 25 -2.53 1.14 6 9 -25 -0.74 0.93 -6 -9 24 50.00 2.56 6 9 -24 56.23 2.66 -6 -9 23 15.16 1.54 6 9 -23 17.36 1.35 -6 -9 22 11.07 1.48 6 9 -22 11.35 1.20 -6 -9 21 53.99 2.74 6 9 -21 53.55 2.55 -6 -9 20 106.30 4.69 6 9 -20 102.20 4.43 -6 -9 19 4.86 1.32 6 9 -19 4.72 0.99 -6 -9 18 83.63 3.77 6 9 -18 95.39 4.15 -6 -9 17 10.29 1.33 6 9 -17 12.24 1.13 -6 -9 16 166.30 7.02 6 9 -16 163.20 6.83 -6 -9 15 1.57 1.11 6 9 -15 3.23 0.99 -6 -9 14 75.94 3.45 6 9 -14 83.77 3.69 -6 -9 13 13.26 1.28 6 9 -13 14.32 1.18 -6 -9 12 7.85 1.08 6 9 -12 5.72 1.00 -6 -9 11 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1.04 7 -12 13 -0.19 0.91 7 -12 13 2.77 0.90 7 -12 14 0.61 0.91 7 -12 14 2.68 0.96 7 -12 15 17.35 1.18 7 -12 15 14.85 1.18 7 -12 16 3.09 0.85 7 -12 16 2.09 0.99 7 -12 17 2.77 0.87 7 -12 17 4.51 0.95 -7 11 21 2.81 1.01 7 -11 -21 4.58 0.92 -7 11 20 10.45 1.10 7 -11 -20 10.33 0.95 -7 11 19 21.38 1.41 7 -11 -19 18.19 1.26 -7 11 18 29.12 1.66 7 -11 -18 27.63 1.55 -7 11 17 47.50 2.38 7 -11 -17 43.97 2.15 -7 11 16 39.66 2.06 7 -11 -16 37.32 1.90 -7 11 15 12.46 1.22 7 -11 -15 15.02 1.15 -7 11 14 -0.95 1.00 7 -11 -14 1.18 0.90 -7 11 13 45.38 2.26 7 -11 -13 40.41 2.05 -7 11 12 16.79 1.30 7 -11 -12 17.66 1.30 -7 11 11 87.00 3.86 7 -11 -11 83.58 3.68 -7 11 10 40.08 2.09 7 -11 -10 36.82 1.90 -7 11 9 31.21 1.78 7 -11 -9 30.77 1.66 -7 11 8 8.96 1.25 7 -11 -8 5.82 1.02 7 -11 -7 33.40 1.74 7 -11 -6 1.59 0.97 7 -11 -5 40.59 2.11 7 -11 -5 36.44 1.92 7 -11 -4 20.43 1.51 7 -11 -4 20.99 1.43 7 -11 -3 89.36 3.94 7 -11 -3 102.90 4.49 7 -11 -2 3.56 1.16 7 -11 -2 2.88 1.04 7 -11 -1 120.70 5.20 7 -11 -1 125.70 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13 62.85 2.91 7 -8 -13 66.94 3.05 -7 8 12 5.37 1.06 7 -8 -12 3.17 0.89 -7 8 11 63.51 2.96 7 -8 -11 58.36 2.69 -7 8 10 0.07 0.91 7 -8 -10 0.40 0.86 -7 8 9 18.49 1.38 7 -8 -9 18.21 1.28 -7 8 8 2.89 1.01 7 -8 -8 5.64 1.02 -7 8 7 2.75 1.03 7 -8 -7 2.17 0.99 -7 8 6 153.90 6.50 7 -8 -6 154.40 6.52 -7 8 5 161.70 6.81 7 -8 -5 174.20 7.31 -7 8 4 16.08 1.30 7 -8 -4 17.11 1.36 -7 8 3 6.91 1.09 7 -8 -3 7.21 1.10 7 -8 -2 2.37 1.00 7 -8 -1 119.30 5.11 7 -8 0 -0.20 0.97 7 -8 0 0.59 0.93 7 -8 1 118.30 5.07 7 -8 1 113.10 4.88 7 -8 2 0.23 0.97 7 -8 2 1.53 0.94 7 -8 3 9.12 1.14 7 -8 3 11.36 1.10 7 -8 4 13.78 1.27 7 -8 4 16.60 1.24 7 -8 5 158.10 6.67 7 -8 5 152.00 6.37 7 -8 6 149.40 6.27 7 -8 6 155.70 6.58 7 -8 7 1.12 1.01 7 -8 7 3.16 0.92 7 -8 8 5.53 1.09 7 -8 8 4.49 0.95 7 -8 9 16.93 1.32 7 -8 9 19.24 1.34 7 -8 10 2.56 1.02 7 -8 10 0.09 0.96 7 -8 11 59.26 2.79 7 -8 11 59.31 2.80 7 -8 12 1.66 1.05 7 -8 12 2.87 1.05 7 -8 13 66.49 3.07 7 -8 13 69.98 3.19 7 -8 14 39.33 2.11 7 -8 14 36.51 1.90 7 -8 15 0.79 1.02 7 -8 15 0.59 0.85 7 -8 16 18.48 1.44 7 -8 16 17.83 1.19 7 -8 17 4.65 1.03 7 -8 17 2.18 0.89 7 -8 18 38.54 2.06 7 -8 18 39.94 2.05 7 -8 19 4.96 1.07 7 -8 19 4.48 0.95 7 -8 20 8.19 1.13 7 -8 20 7.83 1.02 7 -8 21 1.55 0.97 7 -8 21 -0.60 0.87 7 -8 22 24.14 1.59 7 -8 22 22.67 1.43 7 -8 24 67.82 3.11 7 -8 24 67.48 3.06 7 -8 25 6.36 1.07 7 -8 25 4.46 0.84 7 -8 26 4.10 0.96 7 -8 26 4.20 0.94 7 -8 27 0.05 0.95 7 -8 27 -0.17 0.75 7 -7 -29 0.00 0.79 -7 7 28 24.37 1.51 7 -7 -28 21.24 1.32 -7 7 27 0.54 1.01 7 -7 -27 2.08 0.91 -7 7 26 0.78 1.12 7 -7 -26 1.09 0.94 -7 7 25 8.57 1.15 7 -7 -25 9.57 1.05 -7 7 24 3.69 1.07 7 -7 -24 3.19 0.81 -7 7 23 13.67 1.30 7 -7 -23 14.56 1.15 -7 7 22 2.14 1.12 7 -7 -22 4.59 0.97 -7 7 21 39.98 2.16 7 -7 -21 40.35 2.08 -7 7 20 0.74 1.04 7 -7 -20 1.83 0.98 -7 7 19 45.35 2.28 7 -7 -19 42.50 2.17 -7 7 18 0.93 1.01 7 -7 -18 -0.34 0.91 -7 7 17 30.13 1.71 7 -7 -17 27.71 1.62 -7 7 16 2.19 1.05 7 -7 -16 0.27 0.93 -7 7 15 171.40 7.18 7 -7 -15 169.10 7.11 -7 7 14 10.47 1.18 7 -7 -14 10.94 1.18 -7 7 13 248.10 10.27 7 -7 -13 220.10 9.15 -7 7 12 2.51 1.08 7 -7 -12 4.26 1.06 -7 7 11 111.50 4.83 7 -7 -11 134.00 5.74 -7 7 10 7.06 1.03 7 -7 -10 6.44 1.06 -7 7 9 191.60 7.99 7 -7 -9 194.40 8.12 -7 7 8 42.17 2.17 7 -7 -8 43.60 2.19 -7 7 7 155.80 6.57 7 -7 -7 160.10 6.73 -7 7 6 6.66 1.08 7 -7 -6 8.68 1.10 -7 7 5 167.00 7.02 7 -7 -5 159.50 6.72 -7 7 4 7.38 1.09 7 -7 -4 10.78 1.14 -7 7 3 409.30 16.71 7 -7 -3 413.20 16.86 -7 7 2 67.52 3.10 7 -7 -2 69.20 3.14 -7 7 1 183.60 7.66 7 -7 -1 173.40 7.25 7 -7 0 12.91 1.15 7 -7 1 163.20 6.86 7 -7 1 175.40 7.32 7 -7 2 153.60 6.48 7 -7 2 171.00 7.15 7 -7 3 484.10 19.73 7 -7 3 430.10 17.54 7 -7 5 163.90 6.89 7 -7 5 153.70 6.47 7 -7 6 6.50 1.15 7 -7 6 8.03 1.15 7 -7 7 155.00 6.55 7 -7 7 153.90 6.49 7 -7 8 39.78 2.15 7 -7 8 41.42 2.12 7 -7 9 174.60 7.31 7 -7 9 175.20 7.33 7 -7 10 4.12 1.03 7 -7 10 7.15 1.04 7 -7 12 1.44 1.01 7 -7 12 1.65 0.93 7 -7 13 231.60 9.60 7 -7 13 205.30 8.50 7 -7 14 9.22 1.02 7 -7 14 9.74 1.21 7 -7 15 171.50 7.21 7 -7 15 165.70 6.94 7 -7 16 0.04 1.08 7 -7 16 0.78 0.95 7 -7 17 32.88 1.91 7 -7 17 31.42 1.76 7 -7 18 -0.29 1.07 7 -7 18 0.14 0.95 7 -7 19 44.45 2.26 7 -7 19 42.62 2.11 7 -7 20 2.70 1.03 7 -7 20 0.79 0.88 7 -7 21 37.80 1.99 7 -7 21 38.71 1.99 7 -7 22 7.54 1.13 7 -7 22 8.34 1.05 7 -7 23 13.19 1.28 7 -7 23 13.47 1.11 7 -7 24 4.33 1.12 7 -7 24 2.60 0.91 7 -7 25 8.02 1.18 7 -7 25 6.19 0.95 7 -7 26 -0.13 1.07 7 -7 26 0.35 0.83 7 -7 27 3.55 1.02 7 -7 27 1.38 0.84 7 -7 28 24.18 1.45 7 -7 28 24.20 1.40 7 -7 29 -2.64 0.99 -7 6 30 6.51 1.02 7 -6 -30 5.07 0.87 -7 6 29 18.48 1.32 7 -6 -29 16.94 1.15 -7 6 28 10.19 1.12 7 -6 -28 12.99 1.02 -7 6 27 11.03 1.22 7 -6 -27 11.33 1.05 -7 6 26 4.90 1.06 7 -6 -26 6.61 1.04 -7 6 25 5.39 1.10 7 -6 -25 6.50 1.05 -7 6 24 31.55 1.89 7 -6 -24 35.46 1.83 -7 6 23 17.34 1.40 7 -6 -23 15.17 1.18 -7 6 22 1.51 1.03 7 -6 -22 3.77 0.90 -7 6 21 9.41 1.26 7 -6 -21 6.58 0.98 -7 6 20 39.98 2.14 7 -6 -20 48.29 2.34 -7 6 19 20.57 1.49 7 -6 -19 25.28 1.54 -7 6 18 1.74 1.07 7 -6 -18 4.30 1.00 -7 6 17 22.18 1.50 7 -6 -17 21.93 1.46 -7 6 16 0.07 1.00 7 -6 -16 1.70 0.95 -7 6 15 67.56 3.13 7 -6 -15 64.81 2.99 -7 6 14 226.80 9.40 7 -6 -14 237.50 9.84 -7 6 13 173.30 7.27 7 -6 -13 161.30 6.79 -7 6 12 13.32 1.26 7 -6 -12 16.17 1.26 -7 6 11 51.99 2.54 7 -6 -11 48.95 2.33 -7 6 10 40.14 2.13 7 -6 -10 37.95 1.95 -7 6 9 1.96 1.02 7 -6 -9 2.16 0.91 -7 6 8 35.42 1.91 7 -6 -8 38.19 1.98 -7 6 7 121.50 5.20 7 -6 -7 114.80 4.92 -7 6 6 0.01 0.95 7 -6 -6 0.65 0.95 -7 6 5 250.10 10.31 7 -6 -5 238.50 9.85 -7 6 4 4.12 0.96 7 -6 -4 2.11 0.99 -7 6 3 196.40 8.17 7 -6 -3 199.30 8.30 -7 6 2 1.34 0.90 7 -6 -2 1.63 1.01 -7 6 1 39.00 2.06 7 -6 -1 36.08 1.96 -7 6 0 1.30 0.72 7 -6 0 2.88 0.97 7 -6 1 39.00 2.05 7 -6 2 13.42 1.22 7 -6 2 16.74 1.31 7 -6 3 199.40 8.30 7 -6 3 201.20 8.38 7 -6 5 239.20 9.89 7 -6 5 228.60 9.44 7 -6 6 1.76 0.99 7 -6 6 1.08 0.92 7 -6 7 110.10 4.76 7 -6 7 109.70 4.70 7 -6 8 35.31 1.84 7 -6 8 36.42 1.94 7 -6 9 2.93 1.03 7 -6 9 2.43 0.98 7 -6 10 40.66 2.09 7 -6 10 43.17 2.17 7 -6 11 46.33 2.32 7 -6 11 45.17 2.23 7 -6 12 13.75 1.30 7 -6 12 16.66 1.28 7 -6 13 146.00 6.21 7 -6 13 140.20 5.93 7 -6 14 232.60 9.65 7 -6 14 230.40 9.55 7 -6 15 65.46 3.05 7 -6 15 67.94 3.12 7 -6 16 0.43 1.02 7 -6 16 1.96 0.92 7 -6 17 24.24 1.59 7 -6 17 21.69 1.36 7 -6 18 2.71 1.08 7 -6 18 2.27 0.92 7 -6 19 24.49 1.58 7 -6 19 20.85 1.38 7 -6 20 41.46 2.14 7 -6 20 40.79 2.09 7 -6 21 6.92 1.10 7 -6 21 6.28 1.06 7 -6 22 1.08 0.99 7 -6 22 2.08 0.94 7 -6 23 16.41 1.45 7 -6 23 14.01 1.11 7 -6 24 33.50 1.82 7 -6 24 34.88 1.99 7 -6 25 6.42 1.08 7 -6 25 7.76 0.97 7 -6 26 3.49 1.09 7 -6 26 3.72 0.95 7 -6 27 9.41 1.14 7 -6 27 8.45 1.02 7 -6 28 8.53 1.24 7 -6 28 9.37 1.02 7 -6 29 16.18 1.14 7 -6 29 20.14 1.38 7 -6 30 4.31 0.97 7 -6 30 3.78 1.09 -7 5 31 -0.74 0.98 7 -5 -31 1.77 0.76 -7 5 30 71.69 3.22 7 -5 -30 65.89 2.96 -7 5 29 11.73 1.18 7 -5 -29 9.80 1.03 -7 5 28 126.20 5.38 7 -5 -28 127.90 5.38 -7 5 27 17.98 1.45 7 -5 -27 17.91 1.19 -7 5 26 69.98 3.26 7 -5 -26 79.23 3.52 -7 5 25 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12.46 1.26 7 6 -12 15.23 1.28 -7 -6 11 49.27 2.40 7 6 -11 42.78 2.16 -7 -6 10 39.80 2.07 7 6 -10 37.65 1.92 -7 -6 9 3.11 0.90 7 6 -9 0.93 0.93 -7 -6 8 34.81 1.80 7 6 -8 33.62 1.77 -7 -6 7 110.10 4.67 7 6 -7 103.30 4.43 -7 -6 6 2.38 0.80 7 6 -6 1.33 0.88 -7 -6 5 250.40 10.27 7 6 -5 216.20 8.92 -7 -6 4 1.85 0.76 7 6 -4 2.33 0.76 -7 -6 3 190.10 7.82 7 6 -3 172.80 7.13 -7 -6 2 3.22 0.68 7 6 -2 1.29 0.77 -7 -6 1 33.68 1.58 7 6 -1 31.54 1.54 7 6 0 -0.37 0.64 7 6 1 32.81 1.53 7 6 1 36.62 1.65 7 6 2 1.10 0.54 7 6 2 1.88 0.51 7 6 3 175.00 7.18 7 6 3 171.60 7.06 7 6 4 3.04 0.49 7 6 4 2.76 0.51 7 6 11 38.36 1.71 7 6 11 42.26 1.84 7 6 12 14.26 0.83 7 6 12 11.84 0.80 7 6 13 136.90 5.65 7 6 13 135.30 5.61 7 6 14 215.00 8.81 7 6 14 204.00 8.39 7 6 15 54.04 2.43 7 6 15 56.59 2.46 7 6 16 1.33 0.67 7 6 16 0.20 0.81 7 6 17 20.10 1.17 7 6 17 18.99 1.26 7 6 18 0.74 0.93 7 6 18 1.67 0.77 7 6 19 19.45 1.19 7 6 19 18.20 1.31 7 6 20 38.14 1.86 7 6 20 33.40 1.89 7 6 21 5.96 1.17 7 6 21 5.27 0.87 7 6 22 0.65 1.16 7 6 22 3.50 0.86 7 6 23 15.10 1.18 7 6 23 11.75 1.42 7 6 24 33.45 1.80 7 6 24 30.52 1.93 7 6 25 6.62 1.29 7 6 25 5.98 1.07 7 6 26 2.46 1.32 7 6 26 5.31 1.07 7 6 27 10.93 1.20 7 6 27 10.24 1.47 7 6 28 6.94 1.40 7 6 28 10.21 1.22 7 6 29 13.37 1.52 7 6 29 14.93 1.40 7 6 30 3.74 1.42 7 6 30 4.39 1.44 -7 -7 29 1.57 1.10 7 7 -29 1.69 0.98 -7 -7 28 26.31 1.66 7 7 -28 24.49 1.52 -7 -7 27 3.08 1.14 7 7 -27 4.14 1.00 -7 -7 26 0.95 1.26 7 7 -26 1.70 1.09 -7 -7 25 7.59 1.31 7 7 -25 6.75 1.13 -7 -7 24 1.71 1.27 7 7 -24 3.57 0.94 -7 -7 23 12.52 1.38 7 7 -23 12.57 1.14 -7 -7 22 2.73 1.24 7 7 -22 4.98 1.03 -7 -7 21 42.36 2.28 7 7 -21 38.57 2.02 -7 -7 20 0.85 1.25 7 7 -20 2.14 0.94 -7 -7 19 38.80 2.07 7 7 -19 40.26 2.11 -7 -7 18 0.22 1.14 7 7 -18 0.73 0.99 -7 -7 17 28.09 1.80 7 7 -17 28.04 1.65 -7 -7 16 1.62 1.11 7 7 -16 -0.52 1.04 -7 -7 15 182.70 7.64 7 7 -15 174.60 7.31 -7 -7 14 10.96 1.27 7 7 -14 9.03 1.13 -7 -7 13 228.50 9.46 7 7 -13 224.10 9.27 -7 -7 12 3.93 1.03 7 7 -12 1.40 0.95 -7 -7 11 122.00 5.18 7 7 -11 118.50 5.07 -7 -7 10 7.38 1.08 7 7 -10 3.11 0.95 -7 -7 9 190.20 7.89 7 7 -9 164.20 6.87 -7 -7 8 42.53 2.08 7 7 -8 42.27 2.05 -7 -7 7 154.80 6.45 7 7 -7 146.70 6.12 -7 -7 6 7.17 0.90 7 7 -6 6.57 0.89 -7 -7 5 143.30 5.94 7 7 -5 145.30 6.06 -7 -7 4 8.71 0.85 7 7 -4 6.96 0.83 -7 -7 3 414.90 16.88 7 7 -3 380.50 15.49 -7 -7 2 62.75 2.69 7 7 -2 56.29 2.46 7 7 -1 150.10 6.19 7 7 19 33.26 1.54 7 7 19 36.91 1.77 7 7 20 1.09 0.65 7 7 20 0.78 0.79 7 7 21 34.37 1.79 7 7 21 35.43 1.72 7 7 22 2.49 0.84 7 7 22 3.51 1.03 7 7 23 9.64 1.23 7 7 23 12.88 1.05 7 7 24 1.92 1.10 7 7 24 2.44 0.87 7 7 25 5.20 1.18 7 7 25 7.11 1.03 7 7 26 -0.43 1.00 7 7 26 2.39 1.09 7 7 27 3.93 1.27 7 7 27 2.66 1.22 7 7 28 23.84 1.58 7 7 28 26.31 1.77 -7 -8 27 -0.55 1.03 7 8 -27 3.42 1.06 -7 -8 26 2.72 1.13 7 8 -26 5.06 0.97 -7 -8 25 3.83 1.15 7 8 -25 3.81 1.06 -7 -8 24 44.89 2.39 7 8 -24 54.47 2.66 -7 -8 23 0.45 1.22 7 8 -23 0.41 1.12 -7 -8 22 19.72 1.52 7 8 -22 18.47 1.41 -7 -8 21 -1.41 1.22 7 8 -21 -1.82 1.09 -7 -8 20 8.55 1.19 7 8 -20 8.81 1.14 -7 -8 19 22.98 1.61 7 8 -19 10.40 1.23 -7 -8 18 42.63 2.27 7 8 -18 45.26 2.25 -7 -8 17 23.66 1.64 7 8 -17 20.05 1.44 -7 -8 16 16.50 1.42 7 8 -16 18.47 1.40 -7 -8 15 0.25 1.10 7 8 -15 1.05 1.01 -7 -8 14 34.97 1.93 7 8 -14 39.95 2.10 -7 -8 13 69.48 3.18 7 8 -13 65.80 3.03 -7 -8 12 2.88 1.04 7 8 -12 2.20 0.99 -7 -8 11 56.66 2.67 7 8 -11 55.14 2.59 -7 -8 10 2.51 1.02 7 8 -10 -0.15 0.89 -7 -8 9 15.36 1.15 7 8 -9 15.00 1.18 -7 -8 8 5.80 0.89 7 8 -8 5.50 0.87 -7 -8 7 1.92 0.74 7 8 -7 1.88 0.81 -7 -8 6 143.20 5.93 7 8 -6 144.00 5.98 -7 -8 5 150.10 6.20 7 8 -5 141.80 5.89 -7 -8 4 12.27 0.80 7 8 -4 11.76 0.82 -7 -8 3 5.22 0.56 7 8 -3 4.79 0.58 7 8 26 2.00 0.87 7 8 26 1.48 0.95 7 8 27 1.67 1.03 7 8 27 0.77 0.91 -7 -9 25 6.23 1.20 -7 -9 24 43.27 2.28 7 9 -24 39.03 2.07 -7 -9 23 25.96 1.73 7 9 -23 29.94 1.69 -7 -9 22 55.65 2.73 7 9 -22 52.49 2.51 -7 -9 21 14.92 1.52 7 9 -21 12.86 1.21 -7 -9 20 30.31 1.93 7 9 -20 25.85 1.60 -7 -9 19 8.06 1.31 7 9 -19 5.17 1.03 -7 -9 18 43.80 2.35 7 9 -18 42.99 2.19 -7 -9 17 8.86 1.29 7 9 -17 6.68 1.10 -7 -9 16 71.85 3.29 7 9 -16 69.28 3.15 -7 -9 15 14.68 1.43 7 9 -15 11.84 1.13 -7 -9 14 35.29 1.93 7 9 -14 37.75 1.95 -7 -9 13 11.06 1.16 7 9 -13 12.86 1.16 -7 -9 12 89.25 3.91 7 9 -12 90.40 3.95 -7 -9 11 8.83 1.13 7 9 -11 5.18 0.96 -7 -9 10 28.51 1.58 7 9 -10 27.73 1.51 -7 -9 9 61.51 2.72 7 9 -9 62.60 2.83 -7 -9 8 3.08 0.73 7 9 -8 2.90 0.88 -7 -9 7 40.33 1.87 7 9 -7 36.03 1.76 -7 -9 6 7.39 0.78 7 9 -6 6.84 0.81 -7 -9 5 16.89 0.90 7 9 -5 15.17 0.91 -7 -10 23 5.47 1.09 -7 -10 22 27.37 1.75 -7 -10 21 4.67 1.21 7 10 -21 13.28 1.49 -7 -10 20 16.12 1.51 7 10 -20 20.06 1.59 -7 -10 19 36.48 2.11 7 10 -19 39.87 2.13 -7 -10 18 9.46 1.34 7 10 -18 8.82 1.19 -7 -10 17 26.94 1.76 7 10 -17 30.58 1.80 -7 -10 16 9.17 1.34 7 10 -16 11.10 1.19 -7 -10 15 0.06 1.18 7 10 -15 -0.52 1.04 -7 -10 14 17.00 1.39 7 10 -14 17.49 1.28 -7 -10 13 16.21 1.34 7 10 -13 14.89 1.24 -7 -10 12 17.95 1.38 7 10 -12 14.54 1.22 -7 -10 11 1.72 1.04 7 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14.08 1.26 8 -12 0 0.44 0.95 8 -12 0 1.15 0.94 8 -12 1 12.68 1.14 8 -12 1 14.86 1.28 8 -12 2 19.21 1.32 8 -12 2 18.73 1.26 8 -12 3 3.83 1.07 8 -12 3 2.43 0.97 8 -12 4 1.73 0.98 8 -12 4 0.53 0.90 8 -12 5 0.18 0.96 8 -12 5 0.17 0.94 8 -12 6 2.12 0.94 8 -12 6 1.94 0.92 8 -12 7 0.70 0.95 8 -12 7 1.84 0.89 8 -12 8 22.04 1.38 8 -12 8 20.91 1.36 8 -12 9 52.80 2.47 8 -12 9 57.00 2.56 8 -12 10 45.44 2.22 8 -12 10 45.63 2.12 8 -12 11 18.28 1.23 8 -12 11 15.83 1.13 8 -12 12 0.95 0.89 8 -12 12 3.18 0.91 8 -12 13 11.20 1.05 8 -12 13 13.46 1.02 -8 11 17 -0.84 0.99 8 -11 -17 0.38 0.88 -8 11 16 1.27 0.94 8 -11 -16 2.34 0.83 -8 11 15 12.07 1.14 8 -11 -15 13.14 1.06 -8 11 14 12.64 1.17 8 -11 -14 16.13 1.19 -8 11 13 0.37 0.92 8 -11 -13 0.21 0.85 -8 11 12 15.87 1.25 8 -11 -12 14.82 1.16 -8 11 11 9.90 1.11 8 -11 -11 11.89 1.11 -8 11 10 1.80 0.96 8 -11 -10 2.36 0.92 -8 11 9 0.61 1.04 8 -11 -9 0.53 0.88 -8 11 8 0.97 0.80 8 -11 -8 0.37 0.90 8 -11 -7 0.74 0.92 8 -11 -6 2.03 0.97 8 -11 -6 2.13 0.97 8 -11 -5 1.66 0.96 8 -11 -5 0.95 1.00 8 -11 -4 7.89 1.07 8 -11 -4 9.30 1.24 8 -11 -3 3.22 1.05 8 -11 -3 2.79 0.95 8 -11 -2 41.84 2.13 8 -11 -2 49.70 2.41 8 -11 0 4.32 0.98 8 -11 0 2.62 1.07 8 -11 1 15.75 1.30 8 -11 1 14.78 1.18 8 -11 2 42.27 2.16 8 -11 2 41.10 2.05 8 -11 3 4.32 1.07 8 -11 3 5.71 0.99 8 -11 4 8.70 1.13 8 -11 4 10.70 1.14 8 -11 5 -0.35 1.09 8 -11 5 1.61 0.94 8 -11 6 0.12 0.99 8 -11 6 0.61 1.04 8 -11 7 -0.04 1.08 8 -11 7 -1.35 0.95 8 -11 8 1.11 0.93 8 -11 8 0.23 0.88 8 -11 9 -0.13 0.97 8 -11 9 1.69 0.85 8 -11 10 4.56 0.91 8 -11 10 1.69 1.06 8 -11 11 10.71 1.12 8 -11 11 12.35 1.01 8 -11 12 18.54 1.35 8 -11 12 14.14 1.18 8 -11 13 0.11 0.96 8 -11 13 1.48 0.87 8 -11 14 16.64 1.25 8 -11 14 15.40 1.19 8 -11 15 12.17 1.09 8 -11 15 12.96 1.09 8 -11 16 0.97 0.89 8 -11 16 2.25 0.85 8 -11 17 0.66 0.96 8 -11 17 0.45 0.74 -8 10 20 22.28 1.40 8 -10 -20 22.88 1.36 -8 10 19 12.52 1.09 8 -10 -19 16.39 1.16 -8 10 18 5.79 1.05 8 -10 -18 6.71 0.90 -8 10 17 8.50 1.15 8 -10 -17 5.93 0.95 -8 10 16 25.15 1.58 8 -10 -16 20.90 1.32 -8 10 15 8.76 1.13 8 -10 -15 9.88 1.05 -8 10 14 25.56 1.56 8 -10 -14 27.88 1.62 -8 10 13 4.19 1.11 8 -10 -13 4.34 0.99 -8 10 12 68.72 3.12 8 -10 -12 69.41 3.19 -8 10 11 41.71 2.11 8 -10 -11 35.71 1.88 -8 10 10 60.85 2.82 8 -10 -10 57.36 2.69 -8 10 9 0.14 1.14 8 -10 -9 2.09 0.94 -8 10 8 109.70 4.75 8 -10 -8 119.90 5.14 -8 10 7 30.77 1.78 8 -10 -7 29.36 1.69 -8 10 6 122.60 5.25 8 -10 -6 101.50 4.40 8 -10 -5 12.23 1.20 8 -10 -4 54.54 2.59 8 -10 -4 51.98 2.51 8 -10 -2 149.40 6.29 8 -10 -2 155.80 6.56 8 -10 -1 3.20 1.05 8 -10 -1 3.90 1.09 8 -10 0 104.10 4.47 8 -10 0 110.40 4.78 8 -10 1 3.47 0.95 8 -10 1 3.95 1.03 8 -10 2 169.20 7.11 8 -10 2 158.00 6.62 8 -10 3 2.73 0.97 8 -10 3 1.70 1.03 8 -10 4 71.31 3.23 8 -10 4 71.46 3.27 8 -10 5 9.99 1.15 8 -10 5 9.83 1.21 8 -10 6 108.90 4.71 8 -10 6 106.20 4.61 8 -10 7 28.63 1.72 8 -10 7 26.07 1.59 8 -10 8 114.10 4.92 8 -10 8 110.80 4.78 8 -10 9 2.21 1.00 8 -10 9 1.80 0.94 8 -10 10 57.61 2.63 8 -10 10 64.55 2.99 8 -10 11 35.74 1.85 8 -10 11 39.78 2.05 8 -10 12 69.12 3.15 8 -10 12 63.70 2.90 8 -10 13 4.83 0.99 8 -10 13 5.42 1.06 8 -10 14 30.43 1.69 8 -10 14 27.31 1.60 8 -10 16 22.87 1.39 8 -10 16 19.20 1.36 8 -10 17 8.58 1.08 8 -10 17 6.13 0.96 8 -10 18 6.53 0.98 8 -10 18 7.81 0.93 8 -10 19 12.13 1.09 8 -10 19 14.38 1.12 8 -10 20 20.62 1.21 8 -10 20 24.15 1.45 -8 9 22 15.96 1.24 8 -9 -22 16.95 1.24 -8 9 21 12.66 1.20 8 -9 -21 11.23 1.10 -8 9 20 0.96 1.13 8 -9 -20 0.80 0.90 -8 9 19 6.34 1.12 8 -9 -19 7.11 1.00 -8 9 18 7.41 1.15 8 -9 -18 6.16 0.91 -8 9 17 9.96 1.12 8 -9 -17 9.55 1.08 -8 9 16 2.35 0.97 8 -9 -16 4.24 0.91 -8 9 15 21.20 1.40 8 -9 -15 24.39 1.44 -8 9 14 14.57 1.27 8 -9 -14 15.85 1.22 -8 9 13 0.06 0.99 8 -9 -13 0.77 0.92 -8 9 12 2.04 1.02 8 -9 -12 0.94 0.93 -8 9 11 0.41 1.00 8 -9 -11 0.05 0.88 -8 9 10 1.99 0.98 8 -9 -10 1.18 0.85 -8 9 9 2.41 0.97 8 -9 -9 2.63 0.89 -8 9 8 17.65 1.35 8 -9 -8 18.65 1.33 -8 9 7 2.72 0.99 8 -9 -7 0.58 0.89 -8 9 6 0.30 0.99 8 -9 -6 1.68 0.91 -8 9 5 1.06 0.99 8 -9 -5 5.23 0.98 8 -9 -4 28.29 1.59 8 -9 -3 4.29 0.92 8 -9 -2 15.03 1.38 8 -9 -2 16.77 1.26 8 -9 -1 4.33 1.06 8 -9 -1 4.89 0.92 8 -9 0 -0.23 1.03 8 -9 0 0.47 0.86 8 -9 1 4.49 1.10 8 -9 1 4.31 0.90 8 -9 2 12.94 1.21 8 -9 2 13.08 1.14 8 -9 3 5.38 1.09 8 -9 3 2.73 0.94 8 -9 4 32.51 1.87 8 -9 4 30.39 1.71 8 -9 5 1.44 1.05 8 -9 5 2.76 0.97 8 -9 6 -0.01 1.09 8 -9 6 -0.78 1.00 8 -9 7 1.12 0.99 8 -9 7 0.26 1.01 8 -9 8 19.72 1.44 8 -9 8 16.81 1.28 8 -9 9 1.40 1.00 8 -9 9 3.40 0.91 8 -9 10 0.66 0.93 8 -9 10 0.34 0.93 8 -9 11 0.91 1.05 8 -9 11 1.80 0.93 8 -9 12 0.55 1.02 8 -9 12 -0.10 0.93 8 -9 13 1.48 1.02 8 -9 13 -0.15 0.93 8 -9 14 15.91 1.31 8 -9 14 14.09 1.18 8 -9 15 22.94 1.47 8 -9 15 22.68 1.41 8 -9 16 3.83 1.05 8 -9 16 2.45 0.97 8 -9 17 11.85 1.23 8 -9 17 9.06 1.09 8 -9 18 5.01 1.06 8 -9 18 6.01 0.94 8 -9 19 5.35 1.16 8 -9 19 7.66 0.97 8 -9 20 0.20 0.91 8 -9 20 -0.27 0.90 8 -9 21 10.16 1.11 8 -9 21 9.95 0.99 8 -9 22 16.03 1.16 8 -9 22 13.95 1.12 -8 8 24 2.49 0.94 8 -8 -24 3.36 0.80 -8 8 23 31.66 1.73 8 -8 -23 36.81 1.82 -8 8 22 44.66 2.21 8 -8 -22 45.63 2.16 -8 8 21 89.64 3.94 8 -8 -21 109.50 4.71 -8 8 20 15.68 1.38 8 -8 -20 15.17 1.21 -8 8 19 52.77 2.54 8 -8 -19 47.14 2.30 -8 8 18 2.07 1.10 8 -8 -18 3.40 0.95 -8 8 17 14.80 1.35 8 -8 -17 18.92 1.30 -8 8 16 26.16 1.63 8 -8 -16 27.23 1.57 -8 8 15 110.40 4.78 8 -8 -15 116.10 4.96 -8 8 14 56.87 2.70 8 -8 -14 53.72 2.53 -8 8 13 6.62 1.08 8 -8 -13 7.94 1.02 -8 8 12 43.04 2.20 8 -8 -12 40.76 2.02 -8 8 11 55.27 2.62 8 -8 -11 57.58 2.68 -8 8 10 131.00 5.58 8 -8 -10 124.80 5.29 -8 8 9 30.08 1.74 8 -8 -9 26.84 1.50 -8 8 8 66.93 3.07 8 -8 -8 64.07 2.90 -8 8 7 0.61 1.00 8 -8 -7 3.36 0.93 -8 8 6 64.09 3.02 8 -8 -6 64.19 2.91 -8 8 5 69.97 3.21 8 -8 -5 73.11 3.28 -8 8 4 138.20 5.87 8 -8 -4 138.10 5.83 -8 8 3 32.31 1.79 8 -8 -3 34.45 1.86 8 -8 -2 46.39 2.28 8 -8 -1 27.67 1.69 8 -8 -1 25.38 1.56 8 -8 0 158.30 6.67 8 -8 0 152.60 6.44 8 -8 2 48.98 2.42 8 -8 2 55.34 2.65 8 -8 3 31.75 1.81 8 -8 3 30.15 1.76 8 -8 4 134.70 5.75 8 -8 4 140.70 5.98 8 -8 6 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135.10 5.72 8 4 17 151.10 6.31 8 4 18 73.26 3.36 8 4 18 76.29 3.39 8 4 19 4.01 1.17 8 4 19 2.09 0.97 8 4 20 12.95 1.36 8 4 20 14.95 1.24 8 4 21 30.45 1.91 8 4 21 31.72 1.77 8 4 22 39.89 2.23 8 4 22 38.10 1.98 8 4 23 74.50 3.49 8 4 23 70.06 3.17 8 4 24 28.52 1.95 8 4 24 26.86 1.66 8 4 25 28.15 1.92 8 4 25 27.02 1.65 8 4 26 -0.93 1.28 8 4 26 -0.68 1.08 8 4 27 14.65 1.55 8 4 27 19.81 1.51 8 4 29 8.71 1.39 -8 -5 28 -1.65 1.18 8 5 -28 -0.57 0.91 -8 -5 27 0.99 1.20 8 5 -27 0.84 0.89 -8 -5 26 9.56 1.32 8 5 -26 9.93 1.09 -8 -5 25 0.07 1.28 8 5 -25 0.21 0.89 -8 -5 24 2.51 1.19 8 5 -24 2.04 0.96 -8 -5 23 0.86 1.11 8 5 -23 0.71 0.96 -8 -5 22 3.89 1.19 8 5 -22 1.15 0.95 -8 -5 21 -0.93 1.21 8 5 -21 1.33 0.95 -8 -5 20 4.40 1.14 8 5 -20 3.31 1.05 -8 -5 19 22.22 1.53 8 5 -19 19.48 1.42 -8 -5 18 41.32 2.18 8 5 -18 43.36 2.26 -8 -5 17 53.11 2.61 8 5 -17 49.53 2.50 -8 -5 16 28.76 1.71 8 5 -16 16.07 1.41 -8 -5 15 30.10 1.81 8 5 -15 7.99 1.20 -8 -5 14 23.24 1.56 8 5 -14 25.48 1.64 -8 -5 13 9.47 1.15 8 5 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0.62 0.80 8 5 17 7.43 1.13 8 5 17 8.86 1.00 8 5 18 38.12 2.01 8 5 18 39.89 1.96 8 5 19 18.34 1.46 8 5 19 18.15 1.30 8 5 20 5.58 1.25 8 5 20 3.89 0.98 8 5 21 -0.24 1.20 8 5 21 -0.58 0.99 8 5 22 3.62 1.28 8 5 22 3.04 0.99 8 5 23 -1.07 0.95 8 5 23 0.85 1.19 8 5 24 1.85 1.27 8 5 24 0.56 0.98 8 5 25 2.48 1.31 8 5 25 0.02 1.03 8 5 26 8.39 1.52 8 5 26 7.83 1.17 8 5 27 1.39 1.40 8 5 27 -0.56 1.16 -8 -6 27 114.10 4.93 8 6 -27 99.74 4.28 -8 -6 26 0.90 1.22 8 6 -26 1.55 1.01 -8 -6 25 69.75 3.26 8 6 -25 73.14 3.28 -8 -6 24 4.97 1.24 8 6 -24 3.52 1.06 -8 -6 23 42.35 2.26 8 6 -23 42.54 2.19 -8 -6 22 13.77 1.34 8 6 -22 16.67 1.35 -8 -6 21 22.19 1.61 8 6 -21 25.24 1.56 -8 -6 20 3.52 1.20 8 6 -20 3.85 1.01 -8 -6 19 7.72 1.25 8 6 -19 8.56 1.05 -8 -6 18 58.41 2.84 8 6 -18 62.09 2.88 -8 -6 17 165.80 6.99 8 6 -17 187.20 7.82 -8 -6 16 5.62 1.23 8 6 -16 5.07 1.04 -8 -6 15 103.50 4.54 8 6 -15 107.10 4.68 -8 -6 14 42.35 2.16 8 6 -14 42.80 2.22 -8 -6 13 62.78 2.88 8 6 -13 60.26 2.86 -8 -6 12 58.29 2.73 8 6 -12 54.47 2.62 -8 -6 11 5.86 1.00 8 6 -11 6.67 1.08 -8 -6 10 42.44 2.12 8 6 -10 39.42 2.06 -8 -6 9 5.59 1.01 8 6 -9 7.05 1.12 -8 -6 8 282.30 11.58 8 6 -8 276.10 11.36 -8 -6 7 75.56 3.35 8 6 -7 72.10 3.24 -8 -6 6 56.30 2.63 8 6 -6 52.62 2.50 -8 -6 5 6.93 0.95 8 6 -5 5.71 0.95 -8 -6 4 124.20 5.20 8 6 -4 120.30 5.11 -8 -6 3 6.11 0.86 8 6 -3 7.51 0.93 -8 -6 2 138.50 5.77 8 6 -2 121.80 5.14 -8 -6 1 0.87 0.76 8 6 -1 0.12 0.77 8 6 0 11.00 0.89 8 6 0 11.33 0.94 8 6 1 -0.77 0.76 8 6 1 0.69 0.69 8 6 2 127.20 5.27 8 6 2 127.10 5.30 8 6 3 6.26 0.73 8 6 3 4.06 0.74 8 6 4 118.10 4.91 8 6 4 114.00 4.76 8 6 5 6.92 0.67 8 6 5 6.48 0.71 8 6 6 55.74 2.43 8 6 6 51.25 2.23 8 6 7 70.03 2.98 8 6 7 65.56 2.79 8 6 8 264.60 10.84 8 6 8 280.30 11.50 8 6 9 9.26 0.74 8 6 9 9.28 0.75 8 6 10 37.59 1.73 8 6 10 38.74 1.74 8 6 12 50.36 2.25 8 6 12 51.20 2.24 8 6 13 59.72 2.59 8 6 13 56.50 2.51 8 6 14 37.77 1.82 8 6 14 38.66 1.79 8 6 15 98.03 4.18 8 6 15 97.87 4.11 8 6 16 4.63 0.75 8 6 16 4.71 0.92 8 6 17 159.80 6.61 8 6 17 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13.50 1.22 10 2 2 5.41 1.14 10 2 2 3.34 1.04 10 2 4 22.70 1.48 10 2 4 20.11 1.50 10 2 5 16.51 1.29 10 2 5 17.48 1.45 10 2 6 25.53 1.52 10 2 6 27.26 1.72 10 2 7 17.97 1.39 10 2 7 18.42 1.40 10 2 8 3.44 1.03 10 2 8 3.19 1.09 10 2 9 8.73 1.12 10 2 9 9.72 1.18 10 2 10 8.69 1.23 10 2 10 9.52 1.20 10 2 11 10.88 1.25 10 2 11 11.52 1.19 10 2 12 2.62 1.06 10 2 12 1.57 1.01 10 2 13 18.94 1.44 10 2 13 15.65 1.35 10 2 14 0.58 1.17 10 2 14 0.07 0.95 10 2 15 9.80 1.23 10 2 15 10.76 1.21 10 2 16 1.61 1.15 10 2 16 2.44 1.10 10 2 17 2.46 1.10 10 2 17 0.90 1.12 10 2 18 4.54 1.27 10 2 18 3.23 1.13 10 2 19 2.73 1.29 10 2 19 1.52 1.05 10 2 21 10.73 1.43 10 2 21 11.02 1.39 10 2 22 11.86 1.48 10 2 22 15.71 1.58 10 2 23 0.48 1.28 10 2 24 1.97 1.29 -10 -3 24 12.92 1.37 10 3 -24 14.06 1.14 -10 -3 23 49.01 2.39 10 3 -23 46.68 2.27 -10 -3 22 2.26 1.10 10 3 -22 2.13 1.09 -10 -3 21 50.80 2.54 10 3 -21 52.31 2.51 -10 -3 20 7.21 1.30 10 3 -20 7.81 1.09 -10 -3 19 139.20 5.91 10 3 -19 133.90 5.69 -10 -3 18 22.28 1.52 10 3 -18 25.24 1.60 -10 -3 17 41.83 2.20 10 3 -17 40.77 2.14 -10 -3 16 4.62 1.21 10 3 -16 5.36 1.05 -10 -3 15 19.79 1.51 10 3 -15 19.23 1.42 -10 -3 14 29.47 1.76 10 3 -14 29.91 1.84 -10 -3 13 43.69 2.27 10 3 -13 45.77 2.32 -10 -3 12 20.65 1.47 10 3 -12 23.13 1.54 -10 -3 11 98.21 4.30 10 3 -11 92.08 4.08 -10 -3 10 57.69 2.76 10 3 -10 56.28 2.72 -10 -3 9 39.86 2.13 10 3 -9 38.37 2.13 -10 -3 8 97.12 4.27 10 3 -8 96.78 4.30 -10 -3 7 19.89 1.38 10 3 -7 18.63 1.37 -10 -3 6 46.36 2.31 10 3 -6 43.59 2.27 -10 -3 5 11.87 1.21 10 3 -5 9.82 1.28 -10 -3 4 19.11 1.35 10 3 -4 16.70 1.42 -10 -3 3 1.38 1.03 10 3 -3 1.81 0.94 -10 -3 2 19.28 1.41 10 3 -2 20.58 1.49 -10 -3 1 15.54 1.25 10 3 -1 20.79 1.51 10 3 0 41.39 2.15 10 3 1 17.07 1.45 10 3 1 17.03 1.39 10 3 2 22.42 1.42 10 3 2 24.16 1.55 10 3 3 1.30 1.00 10 3 3 3.68 1.01 10 3 4 17.85 1.33 10 3 4 16.25 1.30 10 3 5 11.95 1.17 10 3 5 10.57 1.17 10 3 6 46.62 2.28 10 3 6 46.15 2.31 10 3 7 20.82 1.42 10 3 7 21.73 1.47 10 3 8 89.65 3.93 10 3 8 100.10 4.38 10 3 9 40.01 2.10 10 3 9 41.42 2.16 10 3 10 54.39 2.60 10 3 10 60.03 2.80 10 3 11 85.04 3.77 10 3 11 92.74 4.06 10 3 12 20.71 1.51 10 3 12 20.13 1.46 10 3 13 43.22 2.20 10 3 13 43.40 2.19 10 3 14 30.05 1.76 10 3 14 29.35 1.81 10 3 15 21.48 1.59 10 3 15 20.82 1.47 10 3 16 4.90 1.18 10 3 16 5.26 1.16 10 3 17 38.34 2.15 10 3 17 40.24 2.11 10 3 18 24.60 1.71 10 3 18 21.29 1.48 10 3 19 129.30 5.57 10 3 19 124.50 5.31 10 3 20 6.37 1.19 10 3 20 7.93 1.36 10 3 21 51.49 2.60 10 3 21 48.15 2.42 10 3 22 2.10 1.36 10 3 22 6.49 1.27 10 3 23 42.21 2.35 10 3 24 9.00 1.61 -10 -4 23 0.46 1.15 10 4 -23 0.68 1.04 -10 -4 22 4.70 1.07 10 4 -22 5.24 0.97 -10 -4 21 14.71 1.31 10 4 -21 16.03 1.28 -10 -4 20 -1.27 1.18 10 4 -20 0.39 1.08 -10 -4 19 16.52 1.49 10 4 -19 16.28 1.41 -10 -4 18 1.30 1.23 10 4 -18 -0.46 1.17 -10 -4 17 13.92 1.33 10 4 -17 16.24 1.38 -10 -4 16 24.17 1.57 10 4 -16 18.33 1.49 -10 -4 15 10.31 1.31 10 4 -15 10.42 1.28 -10 -4 14 35.37 1.95 10 4 -14 24.15 1.57 -10 -4 13 -0.08 1.05 10 4 -13 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10 4 15 6.62 1.20 10 4 16 1.04 1.24 10 4 16 2.04 1.08 10 4 17 17.52 1.34 10 4 17 16.91 1.52 10 4 18 1.16 1.36 10 4 18 -0.41 1.13 10 4 19 15.86 1.61 10 4 19 16.16 1.38 10 4 20 -0.36 1.12 10 4 20 -0.22 1.38 10 4 21 15.21 1.57 10 4 21 16.70 1.40 10 4 22 3.35 1.41 10 4 22 5.34 1.18 10 4 23 2.77 1.47 10 4 23 -1.83 1.16 -10 -5 22 9.79 1.22 10 5 -22 1.18 1.02 -10 -5 21 11.28 1.34 10 5 -21 13.32 1.28 -10 -5 20 9.81 1.31 10 5 -20 11.13 1.22 -10 -5 19 7.28 1.28 10 5 -19 6.65 1.05 -10 -5 18 24.03 1.63 10 5 -18 21.68 1.48 -10 -5 17 15.22 1.41 10 5 -17 16.31 1.38 -10 -5 16 79.88 3.60 10 5 -16 80.36 3.65 -10 -5 15 6.07 1.22 10 5 -15 4.19 1.25 -10 -5 14 63.52 2.99 10 5 -14 70.48 3.29 -10 -5 13 18.42 1.44 10 5 -13 20.13 1.56 -10 -5 12 70.21 3.18 10 5 -12 77.35 3.53 -10 -5 11 -1.17 1.06 10 5 -11 1.00 1.14 -10 -5 10 132.90 5.64 10 5 -10 128.30 5.51 -10 -5 9 3.72 1.17 10 5 -9 1.79 1.21 -10 -5 8 126.50 5.38 10 5 -8 122.60 5.28 -10 -5 7 12.56 1.27 10 5 -7 13.37 1.39 -10 -5 6 179.60 7.50 10 5 -6 171.80 7.21 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2.37 0.94 10 6 8 3.14 0.92 10 6 8 3.93 0.90 10 6 9 0.35 0.87 10 6 9 -0.62 0.82 10 6 10 2.53 0.94 10 6 10 2.32 0.92 10 6 11 0.56 0.99 10 6 11 1.23 0.85 10 6 12 5.39 1.00 10 6 12 5.87 0.95 10 6 13 6.67 1.08 10 6 13 6.04 0.89 10 6 14 0.63 1.02 10 6 14 1.49 0.89 10 6 15 2.38 0.94 10 6 15 1.70 1.02 10 6 16 18.43 1.29 10 6 16 15.02 1.28 10 6 17 -1.72 1.01 10 6 17 1.10 1.00 10 6 18 6.97 1.17 10 6 18 6.33 1.02 10 6 19 0.48 1.00 10 6 19 0.01 1.09 10 6 20 10.50 1.29 10 6 20 8.88 1.17 -10 -7 19 46.16 2.36 -10 -7 18 15.53 1.44 -10 -7 17 92.76 4.05 -10 -7 16 1.16 1.12 10 7 -16 3.92 1.40 -10 -7 15 50.88 2.46 10 7 -15 51.64 2.67 -10 -7 14 16.83 1.37 10 7 -14 16.38 1.48 -10 -7 13 28.86 1.75 10 7 -13 29.53 1.84 -10 -7 12 1.69 1.13 10 7 -12 1.68 1.18 -10 -7 11 14.82 1.39 10 7 -11 13.25 1.35 -10 -7 10 1.68 1.15 10 7 -10 1.10 1.16 -10 -7 9 8.35 1.14 10 7 -9 6.59 1.20 -10 -7 8 1.94 0.96 10 7 -8 1.20 1.18 -10 -7 7 16.35 1.26 10 7 -7 16.97 1.41 -10 -7 6 0.16 0.96 10 7 -6 0.93 1.17 -10 -7 5 68.31 3.03 10 7 -5 71.96 3.29 10 7 -4 1.24 1.07 10 7 -3 0.18 1.02 10 7 -3 1.56 0.91 10 7 -2 6.64 0.94 10 7 -2 6.21 1.09 10 7 -1 5.35 0.90 10 7 -1 6.83 1.03 10 7 0 2.98 0.90 10 7 0 3.46 0.91 10 7 1 3.92 0.88 10 7 1 5.08 0.84 10 7 2 7.37 0.83 10 7 2 5.94 0.82 -10 -8 16 3.67 1.17 -10 -8 15 -0.32 1.13 10 8 -15 -3.99 1.20 -10 -8 14 3.37 1.11 10 8 -14 3.69 1.20 -10 -8 13 4.10 1.12 10 8 -13 5.20 1.19 -10 -8 12 0.82 1.05 10 8 -12 -0.12 1.11 -10 -8 11 11.83 1.24 10 8 -11 11.44 1.33 -10 -8 10 3.56 1.05 10 8 -10 1.92 1.17 -10 -8 9 -0.73 0.99 10 8 -9 -0.54 1.11 -10 -8 8 3.51 1.03 10 8 -8 3.37 1.10 -10 -8 7 0.81 0.99 10 8 -7 1.84 1.07 -10 -8 6 0.11 0.85 10 8 -6 0.80 1.05 10 8 -5 1.53 1.05 10 8 -5 -0.02 0.91 10 8 -4 5.33 0.94 10 8 -4 4.19 0.94 10 8 -3 0.01 0.85 10 8 -3 -0.09 0.76 -10 -9 13 6.43 1.22 10 9 -13 7.78 1.32 -10 -9 12 3.70 1.10 10 9 -12 3.68 1.21 -10 -9 11 1.71 1.05 10 9 -11 3.01 1.26 -10 -9 10 97.85 4.22 10 9 -10 95.25 4.18 -10 -9 9 1.12 0.99 10 9 -9 1.28 1.10 -10 -9 8 46.83 2.18 10 9 -8 49.26 2.35 10 9 -7 2.57 1.04 10 9 -6 11.68 1.01 10 9 -6 10.96 0.91 10 10 -9 -3.98 1.00 -11 8 9 5.20 1.18 11 -8 -9 6.16 0.99 -11 8 8 4.18 1.11 11 -8 -8 4.71 0.96 -11 8 7 37.59 1.88 11 -8 -7 33.07 1.74 11 -8 -6 5.36 0.97 11 -8 -5 4.61 0.95 11 -8 -5 5.49 0.98 11 -8 -4 1.43 1.01 11 -8 -4 1.62 0.94 11 -8 -3 0.56 0.88 11 -8 -3 -0.22 0.91 11 -8 -2 14.88 1.20 11 -8 -2 15.50 1.22 11 -8 -1 13.88 1.15 11 -8 -1 12.87 1.14 11 -8 0 2.29 0.95 11 -8 0 1.84 0.93 11 -8 1 14.90 1.17 11 -8 1 15.08 1.22 11 -8 2 15.81 1.23 11 -8 2 16.94 1.24 11 -8 3 3.96 0.97 11 -8 3 1.24 0.88 11 -8 4 2.69 0.96 11 -8 4 1.54 0.98 11 -8 5 3.56 0.92 11 -8 5 4.86 0.92 11 -8 6 3.80 1.01 11 -8 6 4.82 0.92 11 -8 7 29.83 1.61 11 -8 7 29.22 1.63 11 -8 8 2.97 0.85 11 -8 8 2.96 0.93 11 -8 9 6.33 0.97 11 -8 9 5.29 0.99 -11 7 13 137.50 5.82 11 -7 -13 120.60 5.10 -11 7 12 8.30 1.06 11 -7 -12 8.40 0.96 -11 7 11 74.66 3.28 11 -7 -11 80.43 3.53 -11 7 10 17.12 1.21 11 -7 -10 16.63 1.31 -11 7 9 15.82 1.27 11 -7 -9 19.11 1.31 -11 7 8 0.52 0.93 11 -7 -8 0.94 0.88 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1.38 -11 -6 11 6.37 1.16 11 6 -11 9.14 1.46 -11 -6 10 0.99 1.08 11 6 -10 0.85 1.29 -11 -6 9 39.00 2.10 11 6 -9 40.97 2.24 -11 -6 8 5.57 1.12 11 6 -8 7.76 1.31 -11 -6 7 57.35 2.68 11 6 -7 57.78 2.82 -11 -6 6 4.90 1.04 11 6 -6 6.18 1.24 -11 -6 5 7.05 0.99 11 6 -5 6.35 1.28 11 6 -4 5.80 1.23 11 6 -3 10.93 1.36 11 6 -3 8.07 1.25 11 6 -2 14.79 1.38 11 6 -2 15.42 1.34 11 6 -1 23.45 1.64 11 6 -1 21.11 1.38 11 6 0 -0.16 1.04 11 6 0 0.92 1.20 11 6 1 20.68 1.48 11 6 1 19.12 1.53 11 6 2 13.36 1.33 11 6 2 13.99 1.28 11 6 3 9.73 1.19 11 6 3 8.19 1.16 11 6 5 5.41 1.02 11 6 5 4.61 1.06 11 6 6 5.32 1.01 11 6 6 6.03 1.11 11 6 7 58.59 2.72 11 6 7 59.54 2.72 11 6 8 5.72 1.07 11 6 8 5.32 1.06 11 6 9 34.87 1.82 11 6 9 36.46 1.97 11 6 10 3.18 1.10 11 6 10 1.44 1.02 11 6 11 4.31 1.08 11 6 11 3.89 0.98 11 6 12 0.90 0.94 11 6 12 3.08 0.98 11 6 13 13.33 1.20 11 6 13 13.38 1.15 11 6 14 2.39 0.91 11 6 14 2.02 1.02 11 6 15 1.73 1.11 11 6 15 2.06 0.98 -11 -7 13 117.10 5.04 -11 -7 12 9.69 1.24 -11 -7 11 61.27 2.83 11 7 -11 56.32 2.89 -11 -7 10 15.46 1.37 11 7 -10 16.44 1.50 -11 -7 9 14.04 1.32 11 7 -9 13.14 1.34 -11 -7 8 2.05 1.12 11 7 -8 3.18 1.24 -11 -7 7 24.85 1.58 11 7 -7 24.92 1.69 11 7 -6 1.65 1.24 11 7 -5 112.90 4.82 11 7 -5 108.80 4.75 11 7 -4 23.04 1.50 11 7 -4 28.34 1.86 11 7 -3 68.48 3.06 11 7 -3 65.28 3.05 11 7 0 4.45 1.12 11 7 0 0.91 1.02 11 7 2 4.05 0.86 11 7 2 1.90 0.97 11 7 4 22.22 1.22 -11 -8 9 6.13 1.24 11 8 -9 2.06 1.24 -11 -8 8 3.95 1.09 11 8 -8 2.02 1.19 11 8 -7 27.27 1.69 11 8 -6 2.86 1.04 11 8 -6 2.68 1.14 11 8 -5 4.68 1.19 11 8 -5 1.04 1.03 11 8 -4 0.91 0.99 11 8 -4 -0.15 0.91 11 8 -3 0.95 0.85 11 8 -3 0.34 0.91 12 -6 -5 0.49 0.90 12 -6 -4 6.12 0.97 12 -6 -4 6.30 0.95 12 -6 -3 4.41 1.03 12 -6 -3 1.55 0.93 12 -6 -2 31.56 1.69 12 -6 -2 30.04 1.65 12 -6 -1 1.67 0.87 12 -6 -1 4.97 0.98 12 -6 0 17.06 1.26 12 -6 0 16.44 1.21 12 -6 4 4.21 0.99 12 -6 4 5.98 0.99 12 -6 5 -0.69 1.09 -12 5 9 26.72 1.54 12 -5 -9 27.02 1.52 -12 5 8 4.48 1.09 12 -5 -8 4.59 0.88 -12 5 7 23.67 1.48 12 -5 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1.14 12 1 5 0.96 1.06 12 1 6 0.45 1.17 12 1 6 0.19 1.19 12 1 7 0.13 1.12 12 1 7 2.13 1.19 12 1 8 15.29 1.34 12 1 8 12.71 1.42 12 1 9 2.89 1.30 12 1 9 0.85 1.23 12 1 11 0.12 1.04 12 1 12 5.41 1.22 12 1 13 -0.68 1.08 12 1 14 5.16 1.11 -12 -2 14 10.27 1.15 12 2 -14 -1.69 1.05 -12 -2 13 10.92 1.12 12 2 -13 7.72 1.15 -12 -2 12 7.06 1.17 12 2 -12 10.23 1.14 -12 -2 11 40.23 2.07 12 2 -11 39.27 2.11 -12 -2 10 4.57 1.21 12 2 -10 4.91 1.16 -12 -2 9 22.36 1.50 12 2 -9 21.84 1.54 -12 -2 8 7.66 1.21 12 2 -8 7.25 1.24 -12 -2 7 5.37 1.13 12 2 -7 3.72 1.15 -12 -2 6 1.30 1.12 12 2 -6 -0.46 1.11 -12 -2 5 7.65 1.21 12 2 -5 8.34 1.30 -12 -2 4 24.82 1.56 12 2 -4 21.20 1.54 12 2 -3 0.14 1.16 12 2 -2 21.73 1.64 12 2 -2 23.64 1.62 12 2 -1 9.01 1.35 12 2 -1 6.74 1.22 12 2 1 7.01 1.23 12 2 1 7.54 1.16 12 2 2 26.33 1.71 12 2 2 27.82 1.81 12 2 3 -0.13 1.16 12 2 3 2.38 1.10 12 2 4 22.93 1.60 12 2 4 26.25 1.85 12 2 5 8.76 1.30 12 2 5 8.92 1.37 12 2 6 1.24 1.14 12 2 6 1.49 1.12 12 2 7 6.45 1.39 12 2 7 4.05 1.23 12 2 8 6.60 1.31 12 2 8 10.04 1.36 12 2 11 35.54 2.00 12 2 12 8.06 1.32 12 2 13 11.31 1.32 -12 -3 13 1.81 1.01 -12 -3 12 -1.18 1.04 -12 -3 11 15.64 1.25 -12 -3 10 3.98 1.13 -12 -3 9 4.97 1.15 12 3 -9 2.04 1.14 -12 -3 8 -0.11 0.99 12 3 -8 2.17 1.31 -12 -3 7 -0.86 1.06 12 3 -7 5.21 1.34 -12 -3 6 0.55 1.05 12 3 -6 4.04 1.26 -12 -3 5 16.88 1.36 12 3 -5 20.34 1.66 12 3 -4 7.73 1.35 12 3 -3 1.66 1.25 12 3 -3 1.37 1.12 12 3 -2 3.26 1.40 12 3 -2 3.76 1.34 12 3 -1 2.45 1.29 12 3 -1 1.59 1.04 12 3 0 61.87 2.92 12 3 0 66.74 3.20 12 3 1 1.75 1.07 12 3 1 2.84 1.22 12 3 2 1.55 1.14 12 3 2 1.25 1.23 12 3 3 1.36 1.10 12 3 3 2.29 1.20 12 3 4 4.87 1.22 12 3 4 7.09 1.24 12 3 5 18.34 1.56 12 3 5 18.38 1.45 12 3 6 -0.52 1.14 12 3 6 -0.78 1.31 12 3 7 0.18 1.28 12 3 7 -1.23 1.35 12 3 8 0.75 1.20 12 3 8 3.59 1.21 12 3 9 8.77 1.31 12 3 9 5.20 1.23 12 3 10 5.75 1.32 12 3 10 4.30 1.32 12 3 11 14.87 1.42 12 3 12 -1.44 1.20 -12 -4 11 27.08 1.64 -12 -4 10 8.88 1.13 -12 -4 9 1.78 1.04 -12 -4 8 80.63 3.59 -12 -4 7 4.54 1.13 -12 -4 6 80.37 3.57 12 4 -6 55.72 2.90 12 4 -5 4.11 1.52 12 4 -4 67.35 3.26 12 4 -3 1.00 1.30 12 4 -3 1.80 1.17 12 4 -2 50.40 2.59 12 4 -2 48.69 2.46 12 4 -1 30.72 1.89 12 4 -1 33.17 1.91 12 4 0 35.36 2.04 12 4 0 35.96 1.94 12 4 1 32.08 1.88 12 4 1 30.56 1.89 12 4 2 46.50 2.41 12 4 2 50.15 2.49 12 4 3 1.24 1.15 12 4 3 -0.53 1.30 12 4 4 56.19 2.70 12 4 4 54.96 2.72 12 4 5 1.03 1.21 12 4 5 3.16 1.16 12 4 6 86.47 3.87 12 4 6 83.02 3.77 12 4 7 2.04 1.24 12 4 7 2.39 1.26 12 4 8 79.35 3.60 12 4 8 83.99 3.81 12 4 9 2.00 1.34 12 4 9 1.55 1.24 12 4 10 13.72 1.48 12 4 10 14.95 1.48 12 4 11 31.33 1.95 12 4 11 28.76 1.87 -12 -5 9 25.20 1.63 -12 -5 8 4.07 1.17 -12 -5 7 20.78 1.60 -12 -5 6 3.74 1.08 12 5 -5 10.54 1.58 12 5 -4 2.81 1.30 12 5 -4 7.41 1.42 12 5 -3 8.37 1.30 12 5 -3 11.29 1.50 12 5 -1 2.25 1.22 12 5 -1 1.77 1.43 12 5 0 5.36 1.20 12 5 0 8.63 1.33 12 5 1 1.55 1.17 12 5 1 2.25 1.15 12 5 2 14.52 1.39 12 5 2 13.14 1.41 12 5 3 6.53 1.25 12 5 3 6.84 1.30 12 5 4 0.66 1.27 12 5 4 0.62 1.17 12 5 5 20.74 1.61 12 5 5 21.66 1.60 12 5 6 3.36 1.27 12 5 6 1.87 1.11 12 5 7 22.32 1.55 12 5 7 22.55 1.66 12 5 8 4.20 1.26 12 5 8 2.04 1.34 12 5 9 18.91 1.67 12 6 -4 4.82 1.26 12 6 -4 4.06 1.36 12 6 -3 -0.71 1.24 12 6 -3 1.43 1.26 12 6 -2 24.19 1.67 12 6 -2 26.73 1.78 12 6 -1 0.97 1.14 12 6 -1 3.55 1.27 12 6 0 14.46 1.36 12 6 0 11.26 1.39 12 6 1 2.25 1.18 12 6 1 -0.08 1.28 12 6 2 25.32 1.66 12 6 2 22.97 1.65 12 6 3 0.83 1.07 12 6 3 -0.99 1.27 12 6 4 4.85 1.25 12 6 4 5.14 1.30 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 71967 _shelx_res_file ; TITL T-376 in Pbca shelx.res created by SHELXL-2018/3 at 12:12:18 on 21-Jul-2022 CELL 0.74500 9.3880 12.2260 28.6930 90.000 90.000 90.000 ZERR 8.00 0.0009 0.0012 0.0028 0.000 0.000 0.000 LATT 1 SYMM 1/2 - X, - Y, 1/2 + Z SYMM - X, 1/2 + Y, 1/2 - Z SYMM 1/2 + X, 1/2 - Y, - Z SFAC C H N O BR DISP C 0.0026 0.0018 12.639 DISP H 0 0 0.6258 DISP N 0.0069 0.0036 21.8413 DISP O 0.0121 0.0067 36.524 DISP Br -0.5532 2.6290 11258.3748 UNIT 136 112 24 32 8 MERG 2 EXYZ C5 C5' EADP C5 C5' EXYZ C7 C7' EADP C7 C7' FMAP 2 PLAN 5 SIZE 0.100 0.120 0.150 ACTA BOND $H CONF L.S. 13 TEMP -173.00 WGHT 0.017000 5.689100 EXTI 0.003281 FVAR 0.22905 0.96759 PART 1 BR1 5 0.628873 0.856942 0.508009 21.00000 0.02753 0.03873 = 0.02357 -0.00799 -0.00248 -0.00819 PART 2 BR1' 5 0.840434 0.511658 0.417622 -21.00000 0.02069 0.02783 = 0.02528 0.00844 0.00143 0.00839 PART 0 O1 4 0.187137 0.817850 0.302576 11.00000 0.01604 0.02400 = 0.02726 0.00328 -0.00008 -0.00046 O2 4 0.460321 0.572739 0.275367 11.00000 0.02130 0.02139 = 0.02277 -0.00407 0.00258 -0.00180 O3 4 0.123026 0.544438 0.392976 11.00000 0.02335 0.02987 = 0.02858 0.00221 0.00533 -0.00639 O4 4 0.358981 0.517163 0.387710 11.00000 0.02406 0.02060 = 0.02952 0.00568 0.00504 -0.00076 N1 3 0.623357 0.579360 0.335125 11.00000 0.02053 0.02080 = 0.02486 -0.00076 0.00155 0.00539 H1 2 0.678479 0.524102 0.326829 11.00000 -1.20000 C2 1 0.502757 0.608428 0.312774 11.00000 0.01739 0.01639 = 0.02229 0.00166 0.00393 -0.00094 C3 1 0.427215 0.699356 0.341936 11.00000 0.01428 0.01535 = 0.01991 0.00044 0.00137 0.00010 C3A 1 0.523019 0.703998 0.384704 11.00000 0.01668 0.01776 = 0.02030 0.00197 0.00051 -0.00202 C4 1 0.517928 0.771955 0.423215 11.00000 0.01953 0.02221 = 0.02198 -0.00066 0.00104 -0.00292 AFIX 43 H4 2 0.442127 0.822416 0.427551 11.00000 -1.20000 AFIX 0 PART 1 C5 1 0.628510 0.763357 0.455375 21.00000 0.02310 0.03117 = 0.02003 -0.00131 -0.00063 -0.00652 PART 2 C5' 1 0.628510 0.763357 0.455375 -21.00000 0.02310 0.03117 = 0.02003 -0.00131 -0.00063 -0.00652 AFIX 43 H5' 2 0.627663 0.809277 0.482082 -21.00000 -1.20000 AFIX 0 PART 0 C6 1 0.740089 0.689780 0.449674 11.00000 0.02214 0.03308 = 0.02468 0.00527 -0.00413 -0.00374 AFIX 43 H6 2 0.812267 0.684771 0.472782 11.00000 -1.20000 AFIX 0 PART 1 C7 1 0.746671 0.623495 0.410362 21.00000 0.01900 0.02857 = 0.02870 0.00543 -0.00102 0.00269 AFIX 43 H7 2 0.822784 0.573406 0.405830 21.00000 -1.20000 AFIX 0 PART 2 C7' 1 0.746671 0.623495 0.410362 -21.00000 0.01900 0.02857 = 0.02870 0.00543 -0.00102 0.00269 PART 0 C7A 1 0.637694 0.633447 0.378050 11.00000 0.01962 0.02029 = 0.02319 0.00280 0.00103 -0.00051 C8 1 0.320478 0.860776 0.298948 11.00000 0.01818 0.02040 = 0.01888 -0.00175 0.00103 -0.00072 N8 3 0.318740 0.958302 0.278405 11.00000 0.01908 0.02207 = 0.02569 0.00490 -0.00051 0.00197 H8A 2 0.395895 0.987450 0.266187 11.00000 -1.20000 H8B 2 0.239799 0.987533 0.269473 11.00000 -1.20000 C9 1 0.436125 0.807607 0.316519 11.00000 0.01558 0.01640 = 0.02095 -0.00061 0.00029 -0.00176 C10 1 0.271402 0.669721 0.349575 11.00000 0.01743 0.01724 = 0.02077 -0.00108 0.00310 -0.00267 C11 1 0.165356 0.725288 0.329159 11.00000 0.01679 0.02173 = 0.02188 -0.00264 0.00236 -0.00253 C12 1 0.567960 0.863113 0.315679 11.00000 0.02329 0.01686 = 0.02163 0.00183 -0.00191 -0.00072 N12 3 0.674842 0.908308 0.316162 11.00000 0.02601 0.02942 = 0.03386 0.00695 -0.00493 -0.00950 C13 1 0.238742 0.572115 0.378505 11.00000 0.02255 0.01913 = 0.02002 -0.00363 0.00244 -0.00320 C14 1 0.352526 0.429714 0.421799 11.00000 0.03306 0.02015 = 0.02841 0.00542 0.00387 -0.00243 AFIX 23 H14A 2 0.319199 0.361186 0.407002 11.00000 -1.20000 H14B 2 0.285916 0.449044 0.447248 11.00000 -1.20000 AFIX 0 C15 1 0.500992 0.415336 0.440641 11.00000 0.04139 0.03888 = 0.04825 0.02065 -0.00352 -0.00176 AFIX 137 H15A 2 0.501376 0.356587 0.463876 11.00000 -1.50000 H15B 2 0.532513 0.483667 0.455218 11.00000 -1.50000 H15C 2 0.565745 0.396395 0.415096 11.00000 -1.50000 AFIX 0 C16 1 0.008847 0.702972 0.329659 11.00000 0.01602 0.03270 = 0.03502 0.00386 0.00236 -0.00293 AFIX 137 H16A 2 -0.007451 0.624599 0.334448 11.00000 -1.50000 H16B 2 -0.032855 0.725376 0.299839 11.00000 -1.50000 H16C 2 -0.035784 0.744306 0.355019 11.00000 -1.50000 AFIX 0 HKLF 4 REM T-376 in Pbca REM wR2 = 0.0908, GooF = S = 1.131, Restrained GooF = 1.131 for all data REM R1 = 0.0448 for 4225 Fo > 4sig(Fo) and 0.0480 for all 4526 data REM 248 parameters refined using 0 restraints END WGHT 0.0170 5.6887 REM Highest difference peak 0.794, deepest hole -0.662, 1-sigma level 0.079 Q1 1 0.7075 0.8197 0.5096 11.00000 0.05 0.79 Q2 1 0.5760 0.9012 0.4995 11.00000 0.05 0.70 Q3 1 0.6218 0.8439 0.5276 11.00000 0.05 0.63 Q4 1 0.6323 0.8375 0.4902 11.00000 0.05 0.44 Q5 1 0.6257 0.8629 0.4565 11.00000 0.05 0.42 ; _shelx_res_checksum 16450 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br Br1 0.62887(3) 0.85694(2) 0.50801(2) 0.02994(10) Uani d 0.9676(11) A 1 Br Br1' 0.8404(7) 0.5117(6) 0.4176(2) 0.025(2) Uani d 0.0324(11) A 2 O O1 0.18714(16) 0.81785(13) 0.30258(5) 0.0224(3) Uani d 1 . . O O2 0.46032(16) 0.57274(12) 0.27537(5) 0.0218(3) Uani d 1 . . O O3 0.12303(17) 0.54444(14) 0.39298(6) 0.0273(3) Uani d 1 . . O O4 0.35898(17) 0.51716(13) 0.38771(6) 0.0247(3) Uani d 1 . . N N1 0.62336(19) 0.57936(15) 0.33512(6) 0.0221(4) Uani d 1 . . H H1 0.678(3) 0.524(2) 0.3268(10) 0.026 Uiso d 1 . . C C2 0.5028(2) 0.60843(16) 0.31277(7) 0.0187(4) Uani d 1 . . C C3 0.4272(2) 0.69936(16) 0.34194(7) 0.0165(3) Uani d 1 . . C C3A 0.5230(2) 0.70400(16) 0.38470(7) 0.0183(4) Uani d 1 . . C C4 0.5179(2) 0.77196(17) 0.42322(7) 0.0212(4) Uani d 1 . . H H4 0.442127 0.822416 0.427551 0.025 Uiso calc 1 A 1 C C5 0.6285(2) 0.76336(19) 0.45537(7) 0.0248(4) Uani d 0.9676(11) A 1 C C5' 0.6285(2) 0.76336(19) 0.45537(7) 0.0248(4) Uani d 0.0324(11) A 2 H H5' 0.627663 0.809277 0.482082 0.030 Uiso calc 0.0324(11) A 2 C C6 0.7401(2) 0.6898(2) 0.44967(8) 0.0266(4) Uani d 1 . . H H6 0.812267 0.684771 0.472782 0.032 Uiso calc 1 A 1 C C7 0.7467(2) 0.62349(19) 0.41036(8) 0.0254(4) Uani d 0.9676(11) A 1 H H7 0.822784 0.573406 0.405830 0.031 Uiso calc 0.9676(11) A 1 C C7' 0.7467(2) 0.62349(19) 0.41036(8) 0.0254(4) Uani d 0.0324(11) A 2 C C7A 0.6377(2) 0.63345(17) 0.37805(7) 0.0210(4) Uani d 1 . . C C8 0.3205(2) 0.86078(17) 0.29895(7) 0.0192(4) Uani d 1 . . N N8 0.3187(2) 0.95830(15) 0.27841(7) 0.0223(4) Uani d 1 . . H H8A 0.396(3) 0.987(2) 0.2662(10) 0.027 Uiso d 1 . . H H8B 0.240(3) 0.988(2) 0.2695(9) 0.027 Uiso d 1 . . C C9 0.4361(2) 0.80761(16) 0.31652(7) 0.0176(4) Uani d 1 . . C C10 0.2714(2) 0.66972(16) 0.34957(7) 0.0185(4) Uani d 1 . . C C11 0.1654(2) 0.72529(17) 0.32916(7) 0.0201(4) Uani d 1 . . C C12 0.5680(2) 0.86311(16) 0.31568(7) 0.0206(4) Uani d 1 . . N N12 0.6748(2) 0.90831(17) 0.31616(7) 0.0298(4) Uani d 1 . . C C13 0.2387(2) 0.57211(17) 0.37850(7) 0.0206(4) Uani d 1 . . C C14 0.3525(3) 0.42971(18) 0.42180(8) 0.0272(5) Uani d 1 . . H H14A 0.319199 0.361186 0.407002 0.033 Uiso calc 1 . . H H14B 0.285916 0.449044 0.447248 0.033 Uiso calc 1 . . C C15 0.5010(3) 0.4153(2) 0.44064(11) 0.0428(7) Uani d 1 . . H H15A 0.501376 0.356587 0.463876 0.064 Uiso calc 1 . . H H15B 0.532513 0.483667 0.455218 0.064 Uiso calc 1 . . H H15C 0.565745 0.396395 0.415096 0.064 Uiso calc 1 . . C C16 0.0088(2) 0.7030(2) 0.32966(8) 0.0279(5) Uani d 1 . . H H16A -0.007451 0.624599 0.334448 0.042 Uiso calc 1 . . H H16B -0.032855 0.725376 0.299839 0.042 Uiso calc 1 . . H H16C -0.035784 0.744306 0.355019 0.042 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Br1 0.02753(14) 0.03873(16) 0.02357(13) -0.00819(10) -0.00248(9) -0.00799(9) Br1' 0.021(3) 0.028(4) 0.025(3) 0.008(3) 0.001(2) 0.008(2) O1 0.0160(7) 0.0240(7) 0.0273(7) -0.0005(6) -0.0001(6) 0.0033(6) O2 0.0213(7) 0.0214(7) 0.0228(7) -0.0018(6) 0.0026(5) -0.0041(5) O3 0.0234(8) 0.0299(8) 0.0286(8) -0.0064(6) 0.0053(6) 0.0022(6) O4 0.0241(8) 0.0206(7) 0.0295(8) -0.0008(6) 0.0050(6) 0.0057(6) N1 0.0205(8) 0.0208(8) 0.0249(8) 0.0054(7) 0.0016(7) -0.0008(7) C2 0.0174(9) 0.0164(8) 0.0223(9) -0.0009(7) 0.0039(7) 0.0017(7) C3 0.0143(8) 0.0153(8) 0.0199(8) 0.0001(7) 0.0014(7) 0.0004(7) C3A 0.0167(8) 0.0178(8) 0.0203(9) -0.0020(7) 0.0005(7) 0.0020(7) C4 0.0195(9) 0.0222(9) 0.0220(9) -0.0029(8) 0.0010(7) -0.0007(7) C5 0.0231(10) 0.0312(11) 0.0200(9) -0.0065(9) -0.0006(8) -0.0013(8) C5' 0.0231(10) 0.0312(11) 0.0200(9) -0.0065(9) -0.0006(8) -0.0013(8) C6 0.0221(10) 0.0331(11) 0.0247(10) -0.0037(9) -0.0041(8) 0.0053(9) C7 0.0190(9) 0.0286(10) 0.0287(10) 0.0027(8) -0.0010(8) 0.0054(8) C7' 0.0190(9) 0.0286(10) 0.0287(10) 0.0027(8) -0.0010(8) 0.0054(8) C7A 0.0196(9) 0.0203(9) 0.0232(9) -0.0005(8) 0.0010(7) 0.0028(7) C8 0.0182(9) 0.0204(9) 0.0189(9) -0.0007(7) 0.0010(7) -0.0017(7) N8 0.0191(8) 0.0221(8) 0.0257(9) 0.0020(7) -0.0005(7) 0.0049(7) C9 0.0156(8) 0.0164(8) 0.0210(9) -0.0018(7) 0.0003(7) -0.0006(7) C10 0.0174(9) 0.0172(8) 0.0208(8) -0.0027(7) 0.0031(7) -0.0011(7) C11 0.0168(9) 0.0217(9) 0.0219(9) -0.0025(7) 0.0024(7) -0.0026(7) C12 0.0233(10) 0.0169(8) 0.0216(9) -0.0007(8) -0.0019(7) 0.0018(7) N12 0.0260(10) 0.0294(10) 0.0339(10) -0.0095(8) -0.0049(8) 0.0070(8) C13 0.0225(9) 0.0191(9) 0.0200(9) -0.0032(8) 0.0024(7) -0.0036(7) C14 0.0331(12) 0.0201(9) 0.0284(10) -0.0024(9) 0.0039(9) 0.0054(8) C15 0.0414(15) 0.0389(14) 0.0483(16) -0.0018(12) -0.0035(12) 0.0206(12) C16 0.0160(9) 0.0327(11) 0.0350(12) -0.0029(9) 0.0024(8) 0.0039(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0026 0.0018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0069 0.0036 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0121 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.5532 2.6290 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C8 O1 C11 . . 119.65(16) ? C13 O4 C14 . . 117.86(17) ? C2 N1 C7A . . 111.92(17) ? C2 N1 H1 . . 124.4(19) ? C7A N1 H1 . . 122.7(18) ? O2 C2 N1 . . 126.56(19) ? O2 C2 C3 . . 125.12(18) ? N1 C2 C3 . . 108.30(17) ? C9 C3 C3A . . 108.85(16) ? C9 C3 C10 . . 109.30(16) ? C3A C3 C10 . . 117.41(16) ? C9 C3 C2 . . 109.83(15) ? C3A C3 C2 . . 100.96(16) ? C10 C3 C2 . . 110.12(16) ? C4 C3A C7A . . 120.55(19) ? C4 C3A C3 . . 130.23(19) ? C7A C3A C3 . . 108.85(17) ? C3A C4 C5' . . 117.3(2) ? C3A C4 C5 . . 117.3(2) ? C3A C4 H4 . . 121.4 ? C5 C4 H4 . . 121.4 ? C6 C5 C4 . . 122.2(2) ? C6 C5 Br1 . . 118.89(16) ? C4 C5 Br1 . . 118.93(17) ? C6 C5' C4 . . 122.2(2) ? C6 C5' H5' . . 118.9 ? C4 C5' H5' . . 118.9 ? C7 C6 C5 . . 120.4(2) ? C7' C6 C5' . . 120.4(2) ? C7 C6 H6 . . 119.8 ? C5 C6 H6 . . 119.8 ? C7A C7 C6 . . 117.3(2) ? C7A C7 H7 . . 121.3 ? C6 C7 H7 . . 121.3 ? C7A C7' C6 . . 117.3(2) ? C7A C7' Br1' . . 123.7(3) ? C6 C7' Br1' . . 114.0(3) ? C7' C7A C3A . . 122.2(2) ? C7 C7A C3A . . 122.2(2) ? C7' C7A N1 . . 128.0(2) ? C7 C7A N1 . . 128.0(2) ? C3A C7A N1 . . 109.74(18) ? N8 C8 O1 . . 111.60(18) ? N8 C8 C9 . . 127.0(2) ? O1 C8 C9 . . 121.37(18) ? C8 N8 H8A . . 122.0(19) ? C8 N8 H8B . . 121(2) ? H8A N8 H8B . . 115(3) ? C8 C9 C12 . . 117.58(18) ? C8 C9 C3 . . 123.48(18) ? C12 C9 C3 . . 118.49(17) ? C11 C10 C13 . . 119.88(18) ? C11 C10 C3 . . 122.01(18) ? C13 C10 C3 . . 118.02(17) ? C10 C11 O1 . . 123.18(18) ? C10 C11 C16 . . 129.3(2) ? O1 C11 C16 . . 107.50(18) ? N12 C12 C9 . . 178.3(2) ? O3 C13 O4 . . 123.23(19) ? O3 C13 C10 . . 126.9(2) ? O4 C13 C10 . . 109.82(17) ? O4 C14 C15 . . 106.84(19) ? O4 C14 H14A . . 110.4 ? C15 C14 H14A . . 110.4 ? O4 C14 H14B . . 110.4 ? C15 C14 H14B . . 110.4 ? H14A C14 H14B . . 108.6 ? C14 C15 H15A . . 109.5 ? C14 C15 H15B . . 109.5 ? H15A C15 H15B . . 109.5 ? C14 C15 H15C . . 109.5 ? H15A C15 H15C . . 109.5 ? H15B C15 H15C . . 109.5 ? C11 C16 H16A . . 109.5 ? C11 C16 H16B . . 109.5 ? H16A C16 H16B . . 109.5 ? C11 C16 H16C . . 109.5 ? H16A C16 H16C . . 109.5 ? H16B C16 H16C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Br1 C5 . 1.895(2) ? Br1' C7' . 1.639(7) ? O1 C8 . 1.361(2) ? O1 C11 . 1.380(3) ? O2 C2 . 1.225(3) ? O3 C13 . 1.211(3) ? O4 C13 . 1.340(3) ? O4 C14 . 1.450(3) ? N1 C2 . 1.349(3) ? N1 C7A . 1.404(3) ? N1 H1 . 0.88(3) ? C2 C3 . 1.562(3) ? C3 C9 . 1.513(3) ? C3 C3A . 1.523(3) ? C3 C10 . 1.523(3) ? C3A C4 . 1.383(3) ? C3A C7A . 1.393(3) ? C4 C5' . 1.393(3) ? C4 C5 . 1.393(3) ? C4 H4 . 0.9500 ? C5 C6 . 1.390(3) ? C5' C6 . 1.390(3) ? C5' H5' . 0.9500 ? C6 C7' . 1.390(3) ? C6 C7 . 1.390(3) ? C6 H6 . 0.9500 ? C7 C7A . 1.386(3) ? C7 H7 . 0.9500 ? C7' C7A . 1.386(3) ? C8 N8 . 1.330(3) ? C8 C9 . 1.362(3) ? N8 H8A . 0.88(3) ? N8 H8B . 0.86(3) ? C9 C12 . 1.412(3) ? C10 C11 . 1.340(3) ? C10 C13 . 1.486(3) ? C11 C16 . 1.494(3) ? C12 N12 . 1.146(3) ? C14 C15 . 1.505(4) ? C14 H14A . 0.9900 ? C14 H14B . 0.9900 ? C15 H15A . 0.9800 ? C15 H15B . 0.9800 ? C15 H15C . 0.9800 ? C16 H16A . 0.9800 ? C16 H16B . 0.9800 ? C16 H16C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 N12 8_755 0.88(3) 2.00(3) 2.874(3) 170(2) yes N8 H8A O2 3_655 0.88(3) 2.08(3) 2.940(2) 165(3) yes N8 H8B O2 8_665 0.86(3) 2.15(3) 2.971(2) 158(2) yes C16 H16A O3 . 0.98 2.30 2.865(3) 116.00 yes C14 H14A Cg2 8_655 0.99 2.92 3.773(3) 145 yes C15 H15B Cg3 1_555 0.98 2.99 3.729(3) 133 yes C15 H15B Cg4 1_555 0.98 2.99 3.729(3) 133 no loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C7A N1 C2 O2 . . . . -178.0(2) ? C7A N1 C2 C3 . . . . 3.9(2) ? O2 C2 C3 C9 . . . . -68.0(2) ? N1 C2 C3 C9 . . . . 110.08(18) ? O2 C2 C3 C3A . . . . 177.15(19) ? N1 C2 C3 C3A . . . . -4.7(2) ? O2 C2 C3 C10 . . . . 52.4(3) ? N1 C2 C3 C10 . . . . -129.51(18) ? C9 C3 C3A C4 . . . . 61.3(3) ? C10 C3 C3A C4 . . . . -63.5(3) ? C2 C3 C3A C4 . . . . 176.8(2) ? C9 C3 C3A C7A . . . . -111.51(18) ? C10 C3 C3A C7A . . . . 123.70(19) ? C2 C3 C3A C7A . . . . 4.0(2) ? C7A C3A C4 C5' . . . . -2.4(3) ? C3 C3A C4 C5' . . . . -174.5(2) ? C7A C3A C4 C5 . . . . -2.4(3) ? C3 C3A C4 C5 . . . . -174.5(2) ? C3A C4 C5 C6 . . . . -0.2(3) ? C3A C4 C5 Br1 . . . . 178.57(15) ? C3A C4 C5' C6 . . . . -0.2(3) ? C4 C5 C6 C7 . . . . 1.8(3) ? Br1 C5 C6 C7 . . . . -176.99(17) ? C4 C5' C6 C7' . . . . 1.8(3) ? C5 C6 C7 C7A . . . . -0.7(3) ? C5' C6 C7' C7A . . . . -0.7(3) ? C5' C6 C7' Br1' . . . . -156.6(3) ? C6 C7' C7A C3A . . . . -2.0(3) ? Br1' C7' C7A C3A . . . . 151.5(3) ? C6 C7' C7A N1 . . . . 177.2(2) ? Br1' C7' C7A N1 . . . . -29.3(4) ? C6 C7 C7A C3A . . . . -2.0(3) ? C6 C7 C7A N1 . . . . 177.2(2) ? C4 C3A C7A C7' . . . . 3.6(3) ? C3 C3A C7A C7' . . . . 177.22(19) ? C4 C3A C7A C7 . . . . 3.6(3) ? C3 C3A C7A C7 . . . . 177.22(19) ? C4 C3A C7A N1 . . . . -175.73(18) ? C3 C3A C7A N1 . . . . -2.1(2) ? C2 N1 C7A C7' . . . . 179.5(2) ? C2 N1 C7A C7 . . . . 179.5(2) ? C2 N1 C7A C3A . . . . -1.2(2) ? C11 O1 C8 N8 . . . . -170.14(17) ? C11 O1 C8 C9 . . . . 7.7(3) ? N8 C8 C9 C12 . . . . 4.1(3) ? O1 C8 C9 C12 . . . . -173.39(18) ? N8 C8 C9 C3 . . . . 176.28(19) ? O1 C8 C9 C3 . . . . -1.2(3) ? C3A C3 C9 C8 . . . . -136.6(2) ? C10 C3 C9 C8 . . . . -7.1(3) ? C2 C3 C9 C8 . . . . 113.8(2) ? C3A C3 C9 C12 . . . . 35.6(2) ? C10 C3 C9 C12 . . . . 165.02(18) ? C2 C3 C9 C12 . . . . -74.1(2) ? C9 C3 C10 C11 . . . . 10.0(3) ? C3A C3 C10 C11 . . . . 134.6(2) ? C2 C3 C10 C11 . . . . -110.7(2) ? C9 C3 C10 C13 . . . . -173.50(16) ? C3A C3 C10 C13 . . . . -48.9(2) ? C2 C3 C10 C13 . . . . 65.8(2) ? C13 C10 C11 O1 . . . . 178.68(18) ? C3 C10 C11 O1 . . . . -4.9(3) ? C13 C10 C11 C16 . . . . -1.6(3) ? C3 C10 C11 C16 . . . . 174.8(2) ? C8 O1 C11 C10 . . . . -4.6(3) ? C8 O1 C11 C16 . . . . 175.58(18) ? C14 O4 C13 O3 . . . . -8.9(3) ? C14 O4 C13 C10 . . . . 170.02(17) ? C11 C10 C13 O3 . . . . -13.4(3) ? C3 C10 C13 O3 . . . . 170.1(2) ? C11 C10 C13 O4 . . . . 167.81(18) ? C3 C10 C13 O4 . . . . -8.8(2) ? C13 O4 C14 C15 . . . . -156.2(2) ? _cod_database_fobs_code 2244151