#------------------------------------------------------------------------------ #$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $ #$Revision: 176432 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/30/04/2300459.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2300459 loop_ _publ_author_name 'Nogueira, I. C.' 'Cavalcante, L. S.' 'Pereira, P. F. S.' 'de Jesus, M. M.' 'Rivas Mercury, J. M.' 'Batista, N. C.' 'Li, M. Siu' 'Longo, E.' _publ_section_title ; Rietveld refinement, morphology and optical properties of (Ba~1{-~x}Sr~x~)MoO~4~ crystals ; _journal_coeditor_code aj5215 _journal_issue 5 _journal_name_full 'Journal of Applied Crystallography' _journal_page_first 1434 _journal_page_last 1446 _journal_paper_doi 10.1107/S0021889813020335 _journal_volume 46 _journal_year 2013 _chemical_compound_source Scheelite _chemical_formula_analytical BaMoO4 _chemical_formula_moiety 'Ba O4 Mo' _chemical_formula_structural 'Ba Mo O4' _chemical_formula_sum 'Ba Mo O4' _chemical_formula_weight 297.27 _chemical_melting_point 1761 _chemical_name_common 'Barium molybdate' _chemical_name_systematic xx _space_group_IT_number 88 _symmetry_cell_setting tetragonal _symmetry_space_group_name_Hall '-I 4ad' _symmetry_space_group_name_H-M 'I 41/a :2' _audit_creation_date 2012-10-01T00:02 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_update_record ' 2012-10-01T00:02 Initial CIF as created by GSAS2CIF' _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 90.0 _cell_formula_units_Z 4 _cell_length_a 5.584828(21) _cell_length_b 5.584828 _cell_length_c 12.82922(9) _cell_measurement_temperature 298 _cell_volume 400.147(3) _computing_data_collection Jade _computing_data_reduction Jade _computing_structure_refinement GSAS _computing_structure_solution xx _diffrn_ambient_temperature 298 _diffrn_detector scintillation _diffrn_detector_type scintillation _diffrn_measurement_device_type 'Rigaku AFC-7R' _diffrn_radiation_monochromator Jade _diffrn_radiation_polarisn_ratio 0.5 _diffrn_radiation_probe x-ray _diffrn_source Cu _diffrn_source_target Cu _diffrn_source_type Copper _exptl_absorpt_correction_T_max 0.97325 _exptl_absorpt_correction_T_min 0.47522 _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 3 Surface roughness abs. correction (Suortti) Terms = 0.30798E-02 0.13241 Correction is refined. ; _exptl_crystal_density_diffrn 4.934 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 276 _pd_calc_method 'Rietveld Refinement' _pd_char_colour white _pd_char_particle_morphology irregular _pd_instr_location ' ?' _pd_meas_2theta_range_inc 0.02 _pd_meas_2theta_range_max 110.0 _pd_meas_2theta_range_min 10.0 _pd_meas_number_of_points 5001 _pd_meas_scan_method disp _pd_phase_name 'from C:/Ref_BSMO_4s_cop/BMO_cop_4s/BaMoO4.cif' _pd_prep_cool_rate 1 _pd_prep_pressure 100 _pd_prep_temperature 298 _pd_proc_2theta_range_inc 0.02 _pd_proc_2theta_range_max 110.0 _pd_proc_2theta_range_min 10.0 _pd_proc_info_data_reduction Jade _pd_proc_info_datetime 2012-10-01T00:02:28 _pd_proc_info_excluded_regions ' ?' _pd_proc_ls_background_function ; GSAS Background function number 1 with 9 terms. Shifted Chebyshev function of 1st kind 1: 82.4781 2: -29.2710 3: 40.6631 4: -23.7703 5: 20.0941 6: -9.13217 7: 5.39574 8: -3.56143 9: -0.331675 ; _pd_proc_ls_peak_cutoff 0.00030 _pd_proc_ls_profile_function ; CW Profile function number 4 with 17 terms Pseudovoigt profile coefficients as parameterized in P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994). J. Appl. Cryst.,27,892-900. Microstrain broadening by P.W. Stephens, (1999). J. Appl. Cryst.,32,281-289. Peak tails are ignored where the intensity is below 0.0003 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_number_of_points 5001 _pd_spec_mounting ' ?' _refine_ls_goodness_of_fit_all 1.66 _refine_ls_goodness_of_fit_ref 1.40 _refine_ls_matrix_type full _refine_ls_number_parameters 21 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0656 _refine_ls_R_factor_gt 0.0555 _refine_ls_R_Fsqd_factor 0.04185 _refine_ls_shift/su_max 0.05 _refine_ls_shift/su_mean 0.02 _refine_ls_wR_factor_gt 0.0920 _reflns_d_resolution_high 0.944 _reflns_d_resolution_low 5.121 _reflns_limit_h_max 5 _reflns_limit_h_min 0 _reflns_limit_k_max 6 _reflns_limit_k_min 0 _reflns_limit_l_max 13 _reflns_limit_l_min 0 _reflns_number_total 251 _cod_data_source_file aj5215sup1.cif _cod_data_source_block BMO_DIP_CP_publ _cod_depositor_comments ; The following automatic conversions were performed: '_geom_bond_publ_flag' value 'N' changed to 'n' according to /usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/IUCr/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (15 times). '_geom_angle_publ_flag' value 'N' changed to 'n' according to /usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/IUCr/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (55 times). Automatic conversion script Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius ; _cod_original_cell_volume 400.147(4) _cod_original_sg_symbol_Hall -I4ad _cod_original_sg_symbol_H-M 'I 41/a' _cod_database_code 2300459 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -y+3/4,+x+1/4,+z+1/4 3 -x+1/2,-y,+z+1/2 4 +y+3/4,-x+3/4,+z+3/4 -1 -x,-y,-z -2 +y+1/4,-x+3/4,-z+3/4 -3 +x+1/2,+y,-z+1/2 -4 -y+1/4,+x+1/4,-z+1/4 101 +x+1/2,+y+1/2,+z+1/2 102 -y+1/4,+x+3/4,+z+3/4 103 -x,-y+1/2,+z 104 +y+1/4,-x+1/4,+z+1/4 -101 -x+1/2,-y+1/2,-z+1/2 -102 +y+3/4,-x+1/4,-z+1/4 -103 +x,+y+1/2,-z -104 -y+3/4,+x+3/4,-z+3/4 loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Ba Ba1 0.0 0.25 0.625 1.0 Uiso 0.0125 4 Mo Mo1 0.0 0.25 0.125 1.0 Uiso 0.0125 4 O O1 0.22831 0.13536 0.04996 1.0 Uiso 0.0125 16 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Ba 4.0 0.000 0.000 20.1807 3.21367 19.1136 0.28331 10.9054 20.0558 0.77363 51.7460 3.02902 International_Tables_Vol_C Mo 4.0 0.000 0.000 17.8871 1.03649 11.1750 8.48061 6.57891 0.05888 0.0000 0.0000 0.34494 International_Tables_Vol_C O 16.0 0.000 0.000 3.76936 15.0797 2.53342 6.30430 1.91579 40.3445 1.55094 0.31291 0.22789 International_Tables_Vol_C loop_ _diffrn_radiation_wavelength _diffrn_radiation_wavelength_wt _diffrn_radiation_type _diffrn_radiation_wavelength_id 1.540500 1.000 CuK\a 1 1.544300 0.500 CuK\a 2 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Ba1 Ba1 Ba1 82.0884(5) 2_455 2_555 n Ba1 Ba1 Ba1 124.66820(30) 2_455 4_444 n Ba1 Ba1 Ba1 124.66820(30) 2_455 4_454 n Ba1 Ba1 O1 127.90280(10) 2_455 3_555 n Ba1 Ba1 O1 40.61550(20) 2_455 4_455 n Ba1 Ba1 O1 104.18660(30) 2_455 -2_555 n Ba1 Ba1 O1 104.4896(4) 2_455 -3_445 n Ba1 Ba1 O1 84.46860(30) 2_455 101_455 n Ba1 Ba1 O1 40.2694 2_455 -104_445 n Ba1 Ba1 Ba1 124.66820(30) 2_555 4_444 n Ba1 Ba1 Ba1 124.66820(30) 2_555 4_454 n Ba1 Ba1 O1 84.46860(30) 2_555 3_555 n Ba1 Ba1 O1 62.80110(30) 2_555 4_455 n Ba1 Ba1 O1 40.2694 2_555 -2_555 n Ba1 Ba1 O1 165.01030(10) 2_555 -3_445 n Ba1 Ba1 O1 127.90280(10) 2_555 101_455 n Ba1 Ba1 O1 40.61550(20) 2_555 102_334 n Ba1 Ba1 O1 104.4896(4) 2_555 -101_444 n Ba1 Ba1 O1 104.18660(30) 2_555 -104_445 n Ba1 Ba1 Ba1 82.0884(5) 4_444 4_454 n Ba1 Ba1 O1 165.01030(10) 4_444 4_455 n Ba1 Ba1 O1 127.90280(10) 4_444 -2_555 n Ba1 Ba1 O1 104.18660(30) 4_444 101_455 n Ba1 Ba1 O1 84.46860(30) 4_444 -104_445 n Ba1 Ba1 O1 104.18660(30) 4_454 3_555 n Ba1 Ba1 O1 104.4896(4) 4_454 4_455 n Ba1 Ba1 O1 84.46860(30) 4_454 -2_555 n Ba1 Ba1 O1 40.2694 4_454 101_455 n Ba1 Ba1 O1 127.90280(10) 4_454 -104_445 n O1 Ba1 O1 145.05110(10) 3_555 4_455 n O1 Ba1 O1 96.77090(10) 3_555 -2_555 n O1 Ba1 O1 139.83611(30) 3_555 101_455 n O1 Ba1 O1 74.5749(4) 3_555 102_334 n O1 Ba1 O1 66.71730(10) 3_555 -101_444 n O1 Ba1 O1 96.77090(10) 3_555 -104_445 n O1 Ba1 O1 66.71730(10) 4_455 -2_555 n O1 Ba1 O1 130.54640(30) 4_455 -3_445 n O1 Ba1 O1 74.5749(4) 4_455 101_455 n O1 Ba1 O1 130.54640(30) 4_455 -101_444 n O1 Ba1 O1 80.88490(20) 4_455 -104_445 n O1 Ba1 O1 145.05110(10) -2_555 -3_445 n O1 Ba1 O1 96.77090(10) -2_555 101_455 n O1 Ba1 O1 80.88490(20) -2_555 102_334 n O1 Ba1 O1 74.5749(4) -2_555 -101_444 n O1 Ba1 O1 139.83611(30) -2_555 -104_445 n O1 Ba1 O1 96.77090(10) 101_455 -104_445 n O1 Mo1 O1 108.23030(20) 1_555 -4_555 n O1 Mo1 O1 111.9826(4) 1_555 103_343 n O1 Mo1 O1 108.23030(20) 1_555 -102_444 n O1 Mo1 O1 108.23030(20) -4_555 103_343 n O1 Mo1 O1 111.9826(4) -4_555 -102_444 n O1 Mo1 O1 108.23030(20) 103_343 -102_444 n Ba1 O1 Ba1 99.11510(20) 2_554 3_554 n Ba1 O1 Mo1 140.28040(10) 2_554 1_555 n Ba1 O1 Mo1 119.62910(30) 3_554 1_555 n loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ba1 O1 2.803740(10) 3_555 n Ba1 O1 2.783950(10) 4_455 n Ba1 O1 2.803740(10) -2_555 n Ba1 O1 2.783950(10) -3_455 n Ba1 O1 2.803740(10) 101_455 n Ba1 O1 2.783950(10) 102_545 n Ba1 O1 2.783950(10) -101_444 n Ba1 O1 2.803740(10) -104_334 n Mo1 O1 1.721210(10) 1_555 n Mo1 O1 1.721210(10) -4_555 n Mo1 O1 1.721210(10) 103_555 n Mo1 O1 1.721210(10) -102_344 n O1 Ba1 2.783950(10) 2_554 n O1 Ba1 2.803740(10) 3_554 n O1 Mo1 1.721210(10) 1_555 n loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 234.0 0.00427 214.03426 214.04784 236.0 0.00424 213.51360 213.52696 215.0 0.00465 212.99432 213.00754 210.0 0.00476 212.47644 212.48941 215.0 0.00465 211.95995 211.97276 235.0 0.00426 211.44487 211.45749 238.0 0.00420 210.93118 210.94362 222.0 0.00450 210.41885 210.43108 233.0 0.00429 209.90793 209.91998 255.0 0.00392 209.39838 209.41023 224.0 0.00446 208.89023 208.90192 247.0 0.00405 208.38342 208.39491 204.0 0.00490 207.87799 207.88931 193.0 0.00518 207.37396 207.38509 234.0 0.00427 206.87128 206.88225 223.0 0.00448 206.36995 206.38072 233.0 0.00429 205.87003 205.88062 216.0 0.00463 205.37140 205.38181 182.0 0.00549 204.87419 204.88440 220.0 0.00455 204.37828 204.38835 219.0 0.00457 203.88377 203.89366 222.0 0.00450 203.39055 203.40025 197.0 0.00508 202.89871 202.90823 219.0 0.00457 202.40820 202.41757 206.0 0.00485 201.91905 201.92824 242.0 0.00413 201.43118 201.44022 223.0 0.00448 200.94470 200.95354 243.0 0.00412 200.45953 200.46820 218.0 0.00459 199.97569 199.98418 204.0 0.00490 199.49318 199.50151 189.0 0.00529 199.01198 199.02014 188.0 0.00532 198.53210 198.54007 213.0 0.00469 198.05354 198.06136 198.0 0.00505 197.57629 197.58397 226.0 0.00442 197.10033 197.10783 186.0 0.00538 196.62567 196.63304 233.0 0.00429 196.15236 196.15955 211.0 0.00474 195.68034 195.68739 242.0 0.00413 195.20959 195.21648 225.0 0.00444 194.74016 194.74689 202.0 0.00495 194.27203 194.27858 216.0 0.00463 193.80519 193.81157 207.0 0.00483 193.33960 193.34581 209.0 0.00478 192.87532 192.88141 207.0 0.00483 192.41234 192.41824 203.0 0.00493 191.95064 191.95642 211.0 0.00474 191.49017 191.49579 210.0 0.00476 191.03098 191.03648 201.0 0.00498 190.57309 190.57841 210.0 0.00476 190.11647 190.12166 195.0 0.00513 189.66109 189.66612 188.0 0.00532 189.20699 189.21187 218.0 0.00459 188.75414 188.75888 188.0 0.00532 188.30255 188.30716 192.0 0.00521 187.85223 187.85667 205.0 0.00488 187.40311 187.40741 211.0 0.00474 186.95529 186.95946 212.0 0.00472 186.50870 186.51274 214.0 0.00467 186.06337 186.06726 176.0 0.00568 185.61926 185.62300 175.0 0.00571 185.17641 185.18001 186.0 0.00538 184.73477 184.73824 212.0 0.00472 184.29437 184.29770 175.0 0.00571 183.85521 183.85840 191.0 0.00524 183.41725 183.42030 177.0 0.00565 182.98055 182.98347 192.0 0.00521 182.54504 182.54784 186.0 0.00538 182.11079 182.11345 172.0 0.00581 181.67773 181.68024 210.0 0.00476 181.24588 181.24828 187.0 0.00535 180.81525 180.81750 187.0 0.00535 180.38579 180.38797 196.0 0.00510 179.95761 179.95961 174.0 0.00575 179.53055 179.53241 188.0 0.00532 179.10475 179.10651 190.0 0.00526 178.68015 178.68175 180.0 0.00556 178.25670 178.25819 192.0 0.00521 177.83447 177.83585 176.0 0.00568 177.41342 177.41469 172.0 0.00581 176.99356 176.99471 191.0 0.00524 176.57494 176.57593 171.0 0.00585 176.15746 176.15833 171.0 0.00585 175.74112 175.74187 170.0 0.00588 175.32599 175.32663 188.0 0.00532 174.91202 174.91255 187.0 0.00535 174.49924 174.49966 170.0 0.00588 174.08763 174.08791 187.0 0.00535 173.67719 173.67734 171.0 0.00585 173.26790 173.26796 150.0 0.00667 172.85976 172.85970 178.0 0.00562 172.45280 172.45262 140.0 0.00714 172.04697 172.04671 155.0 0.00645 171.64233 171.64194 184.0 0.00543 171.23883 171.23833 168.0 0.00595 170.83643 170.83582 168.0 0.00595 170.43523 170.43452 179.0 0.00559 170.03514 170.03435 153.0 0.00654 169.63626 169.63530 168.0 0.00595 169.23845 169.23743 164.0 0.00610 168.84180 168.84067 149.0 0.00671 168.44626 168.44504 188.0 0.00532 168.05186 168.05051 183.0 0.00546 167.65862 167.65715 155.0 0.00645 167.26646 167.26488 147.0 0.00680 166.87546 166.87379 158.0 0.00633 166.48557 166.48376 164.0 0.00610 166.09680 166.09491 157.0 0.00637 165.70909 165.70714 175.0 0.00571 165.32256 165.32048 177.0 0.00565 164.93712 164.93494 153.0 0.00654 164.55280 164.55052 154.0 0.00649 164.16956 164.16722 174.0 0.00575 163.78743 163.78497 155.0 0.00645 163.40642 163.40387 150.0 0.00667 163.02650 163.02385 167.0 0.00599 162.64767 162.64491 147.0 0.00680 162.26993 162.26709 184.0 0.00543 161.89328 161.89034 157.0 0.00637 161.51772 161.51469 144.0 0.00694 161.14325 161.14014 157.0 0.00637 160.76988 160.76668 145.0 0.00690 160.39752 160.39424 147.0 0.00680 160.02631 160.02295 148.0 0.00676 159.65614 159.65268 164.0 0.00610 159.28708 159.28352 153.0 0.00654 158.91907 158.91542 157.0 0.00637 158.55209 158.54839 147.0 0.00680 158.18626 158.18245 173.0 0.00578 157.82143 157.81752 158.0 0.00633 157.45769 157.45370 145.0 0.00690 157.09497 157.09091 158.0 0.00633 156.73334 156.72920 180.0 0.00556 156.37274 156.36855 142.0 0.00704 156.01321 156.00894 150.0 0.00667 155.65474 155.65036 135.0 0.00741 155.29729 155.29285 134.0 0.00746 154.94090 154.93637 142.0 0.00704 154.58554 154.58096 135.0 0.00741 154.23125 154.22655 140.0 0.00714 153.87796 153.87321 124.0 0.00806 153.52571 153.52090 160.0 0.00625 153.17453 153.16963 175.0 0.00571 152.82434 152.81935 132.0 0.00758 152.47519 152.47014 144.0 0.00694 152.12706 152.12192 136.0 0.00735 151.77997 151.77478 155.0 0.00645 151.43388 151.42863 146.0 0.00685 151.08882 151.08351 150.0 0.00667 150.74480 150.73938 139.0 0.00719 150.40175 150.39630 135.0 0.00741 150.05972 150.05420 144.0 0.00694 149.71867 149.71307 129.0 0.00775 149.37868 149.37303 152.0 0.00658 149.03970 149.03395 144.0 0.00694 148.70169 148.69589 150.0 0.00667 148.36469 148.35880 131.0 0.00763 148.02869 148.02275 166.0 0.00602 147.69368 147.68767 151.0 0.00662 147.35965 147.35362 138.0 0.00725 147.02664 147.02052 143.0 0.00699 146.69458 146.68840 153.0 0.00654 146.36353 146.35728 138.0 0.00725 146.03346 146.02715 151.0 0.00662 145.70439 145.69803 167.0 0.00599 145.37627 145.36986 136.0 0.00735 145.04912 145.04266 138.0 0.00725 144.72296 144.71645 135.0 0.00741 144.39778 144.39122 134.0 0.00746 144.07356 144.06694 121.0 0.00826 143.75032 143.74362 153.0 0.00654 143.42802 143.42130 132.0 0.00758 143.10672 143.09993 149.0 0.00671 142.78636 142.77951 145.0 0.00690 142.46693 142.46007 146.0 0.00685 142.14850 142.14156 147.0 0.00680 141.83101 141.82399 155.0 0.00645 141.51447 141.50740 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77.58266 85.16488 79.0 0.01266 77.61745 84.91965 76.0 0.01316 77.65218 84.69710 85.0 0.01176 77.68687 84.49422 107.0 0.00935 77.72150 84.30864 91.0 0.01099 77.75608 84.26688 75.0 0.01333 77.79062 84.11220 71.0 0.01408 77.82507 83.97038 85.0 0.01176 77.85949 83.84056 86.0 0.01163 77.89384 83.72182 86.0 0.01163 77.92815 83.61343 93.0 0.01075 77.96239 83.51476 82.0 0.01220 77.99659 83.42534 87.0 0.01149 78.03072 83.34461 90.0 0.01111 78.06479 83.27221 83.0 0.01205 78.09879 83.20776 77.0 0.01299 78.13274 83.15003 75.0 0.01333 78.16662 83.10082 78.0 0.01282 78.20044 83.05891 72.0 0.01389 78.23421 83.02426 82.0 0.01220 78.26790 82.99682 91.0 0.01099 78.30154 82.97668 71.0 0.01408 78.33511 82.96388 90.0 0.01111 78.36861 82.95870 82.0 0.01220 78.40203 82.90656 99.0 0.01010 78.43540 82.98309 71.0 0.01408 78.46870 83.00449 60.0 0.01667 78.50192 83.03571 86.0 0.01163 78.53510 83.07784 75.0 0.01333 78.56818 83.13263 94.0 0.01064 78.60122 83.20250 87.0 0.01149 78.63415 83.29166 80.0 0.01250 78.66702 83.40691 61.0 0.01639 78.69984 83.55989 82.0 0.01220 78.73255 83.76876 82.0 0.01220 78.76521 84.16276 100.0 0.01000 78.79779 84.59670 85.0 0.01176 78.83030 85.23279 71.0 0.01408 78.86272 85.93854 80.0 0.01250 78.89507 87.26429 97.0 0.01031 78.92735 89.09811 82.0 0.01220 78.95953 91.50862 85.0 0.01176 78.99164 94.60449 97.0 0.01031 79.02367 98.33459 91.0 0.01099 79.05562 102.57017 84.0 0.01190 79.08748 107.05308 103.0 0.00971 79.11928 111.38028 123.0 0.00813 79.15097 115.00883 116.0 0.00862 79.18259 117.32862 125.0 0.00800 79.21411 117.85728 103.0 0.00971 79.24555 116.48669 107.0 0.00935 79.27692 113.55082 111.0 0.00901 79.30819 109.63763 96.0 0.01042 79.33938 105.34886 99.0 0.01010 79.37046 101.17426 72.0 0.01389 79.40147 97.51316 89.0 0.01124 79.43238 94.38124 63.0 0.01587 79.46320 92.16437 78.0 0.01282 79.49393 90.78320 91.0 0.01099 79.52454 90.21343 79.0 0.01266 79.55511 90.39409 68.0 0.01471 79.58554 91.23811 85.0 0.01176 79.61591 92.63247 88.0 0.01136 79.64615 94.42874 87.0 0.01149 79.67632 96.44283 94.0 0.01064 79.70638 98.42895 93.0 0.01075 79.73631 100.08945 96.0 0.01042 79.76619 101.10732 63.0 0.01587 79.79594 101.24232 87.0 0.01149 79.82561 100.44807 81.0 0.01235 79.85516 98.89548 80.0 0.01250 79.88461 96.87383 85.0 0.01176 79.91396 94.67274 99.0 0.01010 79.94322 92.52237 85.0 0.01176 79.97235 90.58041 72.0 0.01389 80.00138 88.93693 107.0 0.00935 80.03030 87.62420 63.0 0.01587 80.05911 86.63055 80.0 0.01250 80.08782 85.91580 83.0 0.01205 80.11642 85.42635 87.0 0.01149 80.14491 85.10747 63.0 0.01587 80.17329 84.90948 77.0 0.01299 80.20155 84.79693 80.0 0.01250 80.22970 84.74082 71.0 0.01408 80.25774 84.72248 69.0 0.01449 80.28566 84.73000 90.0 0.01111 80.31347 84.75618 97.0 0.01031 80.34116 84.79695 77.0 0.01299 80.36873 84.84991 88.0 0.01136 80.39618 84.91386 70.0 0.01429 80.42351 84.98830 72.0 0.01389 80.45071 85.07322 64.0 0.01563 80.47780 85.16914 80.0 0.01250 80.50478 85.27715 81.0 0.01235 80.53162 85.39951 92.0 0.01087 80.55834 85.59253 73.0 0.01370 80.58494 85.75938 84.0 0.01190 80.61140 85.96360 86.0 0.01163 80.63774 86.22408 72.0 0.01389 80.66396 86.56902 81.0 0.01235 80.69005 87.03783 95.0 0.01053 80.71600 87.68049 70.0 0.01429 80.74184 88.55414 78.0 0.01282 80.76752 89.71451 86.0 0.01163 80.79309 91.20245 90.0 0.01111 80.81852 93.02796 104.0 0.00962 80.84382 95.15279 98.0 0.01020 80.86897 97.47704 93.0 0.01075 80.89400 99.82993 77.0 0.01299 80.91888 101.97299 90.0 0.01111 80.94364 103.59970 85.0 0.01176 80.96825 104.43274 91.0 0.01099 80.99271 104.32521 95.0 0.01053 81.01706 103.35091 81.0 0.01235 81.04124 101.76114 89.0 0.01124 81.06528 99.86308 86.0 0.01163 81.08919 97.95638 79.0 0.01266 81.11295 96.19524 88.0 0.01136 81.13654 94.74434 75.0 0.01333 81.16003 93.68162 86.0 0.01163 81.18333 93.03725 91.0 0.01099 81.20650 92.80834 83.0 0.01205 81.22952 92.97264 107.0 0.00935 81.25240 93.49757 84.0 0.01190 81.27512 94.34282 93.0 0.01075 81.29767 95.45718 107.0 0.00935 81.32008 96.77265 95.0 0.01053 81.34233 98.19785 107.0 0.00935 81.36445 99.61320 99.0 0.01010 81.38638 100.87309 106.0 0.00943 81.40817 101.82917 101.0 0.00990 81.42979 102.37148 103.0 0.00971 81.45126 102.49796 111.0 0.00901 81.47256 102.30878 104.0 0.00962 81.49370 101.95582 89.0 0.01124 81.51469 101.58768 86.0 0.01163 81.53551 101.32365 108.0 0.00926 81.55618 101.01465 107.0 0.00935 81.57665 101.18165 129.0 0.00775 81.59698 101.61312 108.0 0.00926 81.61713 102.31390 111.0 0.00901 81.63710 103.27810 99.0 0.01010 81.65693 104.49790 129.0 0.00775 81.67657 105.97083 116.0 0.00862 81.69604 107.70576 116.0 0.00862 81.71533 109.72888 130.0 0.00769 81.73445 112.09167 119.0 0.00840 81.75341 114.88516 136.0 0.00735 81.77218 118.26534 113.0 0.00885 81.79077 122.49564 129.0 0.00775 81.80917 128.01204 143.0 0.00699 81.82742 135.51315 149.0 0.00671 81.84547 146.06827 173.0 0.00578 81.86335 161.22083 236.0 0.00424 81.88103 183.04796 235.0 0.00426 81.89854 213.99687 249.0 0.00402 81.91588 257.14456 278.0 0.00360 81.93300 315.06345 430.0 0.002326 81.94994 389.66635 487.0 0.002053 81.96671 481.32626 591.0 0.001692 81.98328 588.10529 771.0 0.001297 81.99966 705.09717 920.0 0.001087 82.01585 823.92078 1026.0 0.000975 82.03184 932.49200 1147.0 0.000872 82.04765 1015.70691 1151.0 0.000869 82.06324 1058.51208 1123.0 0.000890 82.07865 1051.85071 1068.0 0.000936 82.09387 997.66266 951.0 0.001052 82.10887 907.78577 762.0 0.001312 82.12370 798.00958 630.0 0.001587 82.13830 682.92419 525.0 0.001905 82.15271 573.84222 504.0 0.001984 82.16692 478.59491 384.0 0.002604 82.18092 401.92950 352.0 0.002841 82.19471 346.08670 296.0 0.003378 82.20831 311.46576 287.0 0.003484 82.22169 297.27866 343.0 0.002915 82.23487 302.04672 334.0 0.002994 82.24783 323.84171 334.0 0.002994 82.26058 360.26288 461.0 0.002169 82.27312 408.23267 471.0 0.002123 82.28545 463.71063 528.0 0.001894 82.29757 521.42419 630.0 0.001587 82.30946 574.75378 681.0 0.001468 82.32114 616.22595 692.0 0.001445 82.33260 639.36389 655.0 0.001527 82.34384 641.72650 653.0 0.001531 82.35486 626.77521 668.0 0.001497 82.36566 602.46106 602.0 0.001661 82.37623 577.90717 559.0 0.001789 82.38658 560.77802 572.0 0.001748 82.39671 555.99524 565.0 0.001770 82.40662 565.23480 648.0 0.001543 82.41628 586.76996 660.0 0.001515 82.42571 615.55060 649.0 0.001541 82.43494 643.60815 687.0 0.001456 82.44392 661.26477 777.0 0.001287 82.45265 659.86737 657.0 0.001522 82.46117 635.44037 596.0 0.001678 82.46944 590.38318 625.0 0.001600 82.47749 531.51685 483.0 0.002070 82.48528 466.71771 389.0 0.002571 82.49285 402.78314 316.0 0.003165 82.50016 344.75851 267.0 0.00375 82.50725 295.93314 258.0 0.00388 82.51408 258.05389 237.0 0.00422 82.52068 231.65532 222.0 0.00450 82.52702 216.45744 215.0 0.00465 82.53313 211.75284 218.0 0.00459 82.53897 216.67505 231.0 0.00433 82.54459 230.27876 289.0 0.003460 82.54995 251.45274 294.0 0.003401 82.55503 278.75662 321.0 0.003115 82.55987 310.26001 394.0 0.002538 82.56447 343.42191 410.0 . . . loop_ _refln_index_h _refln_index_k _refln_index_l _pd_refln_wavelength_id _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing 0 1 1 1 o 348.936 416.656 0.00 5.12067 0 1 1 2 o 338.921 416.656 0.00 5.12067 0 1 3 1 o 190.101 81.819 0.00 3.39534 0 1 3 2 o 143.151 81.819 0.00 3.39534 1 1 2 1 o 106911.27 106836.75 180.00 3.36288 1 1 2 2 o 107635.86 106836.75 180.00 3.36288 0 0 4 1 o 81493.04 79120.07 180.00 3.20731 0 0 4 2 o 81232.16 79120.07 180.00 3.20731 0 2 0 1 o 71310.76 68726.81 180.00 2.79241 0 2 0 2 o 72322.76 68726.81 180.00 2.79241 0 2 2 1 o 1566.095 1834.361 180.00 2.56033 0 2 2 2 o 1490.773 1834.361 180.00 2.56033 1 1 4 1 o 3128.551 3453.896 180.00 2.48964 1 1 4 2 o 3010.394 3453.896 180.00 2.48964 1 2 1 1 o -5.983 6.499 0.00 2.45158 2 1 1 1 o 6794.885 7165.447 0.00 2.45158 2 1 1 2 o 6573.337 7165.447 0.00 2.45158 1 2 1 2 o -13.446 6.499 0.00 2.45158 0 1 5 1 o 3936.757 4419.010 180.00 2.33155 0 1 5 2 o 3839.344 4419.010 180.00 2.33155 2 1 3 1 o 650.914 683.364 0.00 2.15672 1 2 3 1 o 7069.553 7369.613 180.00 2.15672 2 1 3 2 o 602.550 683.364 0.00 2.15672 1 2 3 2 o 6622.351 7369.613 180.00 2.15672 0 2 4 1 o 83244.19 82032.20 0.00 2.10605 0 2 4 2 o 81842.65 82032.20 0.00 2.10605 2 2 0 1 o 68822.84 66879.88 180.00 1.97453 2 2 0 2 o 66681.14 66879.88 180.00 1.97453 2 2 2 1 o 275.735 238.847 180.00 1.88715 2 2 2 2 o 256.916 238.847 180.00 1.88715 1 1 6 1 o 67011.26 64917.54 0.00 1.88028 1 1 6 2 o 65295.01 64917.54 0.00 1.88028 0 3 1 1 o 2079.919 2241.521 180.00 1.84231 0 3 1 2 o 2321.394 2241.521 180.00 1.84231 1 2 5 1 o 167.203 6.564 0.00 1.78971 2 1 5 1 o 255.792 86.102 180.00 1.78971 2 1 5 2 o 250.537 86.102 180.00 1.78971 1 2 5 2 o 162.229 6.564 0.00 1.78971 0 1 7 1 o 2716.837 2450.963 180.00 1.74138 0 1 7 2 o 2731.009 2450.963 180.00 1.74138 0 3 3 1 o 1217.905 1130.565 180.00 1.70689 1 3 2 1 o 70718.05 71656.04 0.00 1.70272 3 1 2 1 o 45507.70 46111.38 180.00 1.70272 0 3 3 2 o 1114.392 1130.565 180.00 1.70689 1 3 2 2 o 70020.88 71656.04 0.00 1.70272 3 1 2 2 o 45059.08 46111.38 180.00 1.70272 0 2 6 1 o 110.088 111.671 0.00 1.69767 0 2 6 2 o 110.524 111.671 0.00 1.69767 2 2 4 1 o 65106.18 61886.16 0.00 1.68144 2 2 4 2 o 63737.22 61886.16 0.00 1.68144 0 0 8 1 o 35570.30 37009.63 0.00 1.60365 0 0 8 2 o 36017.45 37009.63 0.00 1.60365 1 3 4 1 o -3.486 135.687 0.00 1.54705 3 1 4 1 o 0.000 0.019 0.00 1.54705 3 1 4 2 o 0.000 0.019 0.00 1.54705 1 3 4 2 o -3.486 135.687 0.00 1.54705 2 3 1 1 o -94.691 16.068 0.00 1.53778 3 2 1 1 o 1266.288 2253.240 0.00 1.53778 3 2 1 2 o 890.564 2253.240 0.00 1.53778 2 3 1 2 o -136.856 16.068 0.00 1.53778 0 3 5 1 o -162.137 93.684 0.00 1.50680 0 3 5 2 o -162.137 93.684 0.00 1.50680 1 1 8 1 o -11.024 408.784 180.00 1.48582 1 1 8 2 o -11.024 408.784 180.00 1.48582 2 1 7 1 o -167.705 3.985 0.00 1.47761 1 2 7 1 o 18.754 420.777 0.00 1.47761 1 2 7 2 o -109.545 420.777 0.00 1.47761 2 1 7 2 o -222.497 3.985 0.00 1.47761 2 3 3 1 o 147.438 450.839 180.00 1.45636 3 2 3 1 o -100.677 9.914 180.00 1.45636 3 2 3 2 o -92.153 9.914 180.00 1.45636 2 3 3 2 o 170.824 450.839 180.00 1.45636 2 2 6 1 o 1.815 17.333 0.00 1.45062 2 2 6 2 o -0.481 17.333 0.00 1.45062 0 4 0 1 o 43964.70 46530.68 0.00 1.39621 0 4 0 2 o 44111.97 46530.68 0.00 1.39621 0 2 8 1 o 54394.32 54658.91 180.00 1.39064 0 2 8 2 o 56548.98 54658.91 180.00 1.39064 0 1 9 1 o 507.611 427.270 0.00 1.38119 0 1 9 2 o 629.425 427.270 0.00 1.38119 0 4 2 1 o 1187.897 1166.685 180.00 1.36426 0 4 2 2 o 1132.461 1166.685 180.00 1.36426 1 3 6 1 o 35923.21 36565.67 180.00 1.36166 3 1 6 1 o 63398.12 64532.53 0.00 1.36166 1 3 6 2 o 36163.15 36565.67 180.00 1.36166 3 1 6 2 o 63821.75 64532.53 0.00 1.36166 4 1 1 1 o 952.855 839.843 0.00 1.34703 1 4 1 1 o 211.094 172.793 180.00 1.34703 4 1 1 2 o 1092.401 839.843 0.00 1.34703 1 4 1 2 o 258.387 172.793 180.00 1.34703 3 2 5 1 o 1026.270 863.576 180.00 1.32606 2 3 5 1 o 1826.624 1549.765 0.00 1.32606 2 3 5 2 o 1902.520 1549.765 0.00 1.32606 3 2 5 2 o 1070.870 863.576 180.00 1.32606 0 3 7 1 o 340.314 54.804 0.00 1.30603 0 3 7 2 o 298.161 54.804 0.00 1.30603 1 4 3 1 o 47.470 43.989 0.00 1.29129 4 1 3 1 o 149.218 144.476 0.00 1.29129 1 4 3 2 o 55.627 43.989 0.00 1.29129 4 1 3 2 o 160.330 144.476 0.00 1.29129 3 3 2 1 o 45911.03 44574.84 0.00 1.28949 3 3 2 2 o 49002.13 44574.84 0.00 1.28949 0 4 4 1 o 42707.98 42082.32 180.00 1.28017 0 4 4 2 o 46446.14 42082.32 180.00 1.28017 4 2 0 1 o 44835.30 43936.69 180.00 1.24881 2 4 0 1 o 55508.61 54395.39 0.00 1.24881 2 4 0 2 o 54116.66 54395.39 0.00 1.24881 4 2 0 2 o 43711.69 43936.69 180.00 1.24881 2 2 8 1 o 42225.95 41564.85 180.00 1.24482 1 2 9 1 o 2578.661 2111.113 0.00 1.23802 2 1 9 1 o 85.566 41.616 0.00 1.23802 2 2 8 2 o 43595.32 41564.85 180.00 1.24482 2 1 9 2 o 140.219 41.616 0.00 1.23802 1 2 9 2 o 3160.082 2111.113 0.00 1.23802 4 2 2 1 o 583.666 404.802 0.00 1.22579 2 4 2 1 o 51.307 35.584 0.00 1.22579 2 4 2 2 o 36.758 35.584 0.00 1.22579 4 2 2 2 o 418.154 404.802 0.00 1.22579 1 1 10 1 o 36625.28 38607.62 180.00 1.22015 1 1 10 2 o 38300.13 38607.62 180.00 1.22015 3 3 4 1 o 755.365 796.206 180.00 1.21778 3 3 4 2 o 973.528 796.206 180.00 1.21778 4 1 5 1 o 598.995 703.160 180.00 1.19785 1 4 5 1 o 1345.986 1560.143 0.00 1.19785 1 4 5 2 o 1206.590 1560.143 0.00 1.19785 4 1 5 2 o 531.193 703.160 180.00 1.19785 3 1 8 1 o 0.000 0.003 0.00 1.18723 1 3 8 1 o -0.842 23.638 0.00 1.18723 1 3 8 2 o 12.062 23.638 0.00 1.18723 3 1 8 2 o 0.002 0.003 0.00 1.18723 2 3 7 1 o 1541.710 1714.994 0.00 1.18303 3 2 7 1 o 186.743 220.080 0.00 1.18303 2 3 7 2 o 1781.032 1714.994 0.00 1.18303 3 2 7 2 o 232.784 220.080 0.00 1.18303 0 4 6 1 o 137.359 104.506 0.00 1.16905 0 4 6 2 o 97.147 104.506 0.00 1.16905 0 2 10 1 o 367.378 394.241 0.00 1.16577 2 4 4 1 o 32653.816 32180.744 180.00 1.16371 4 2 4 1 o 35082.31 34574.145 0.00 1.16371 0 2 10 2 o 392.561 394.241 0.00 1.16577 4 2 4 2 o 35728.60 34574.145 0.00 1.16371 2 4 4 2 o 33255.387 32180.744 180.00 1.16371 0 1 11 1 o 286.555 474.738 0.00 1.14166 0 1 11 2 o -52.747 474.738 0.00 1.14166 0 3 9 1 o 194.045 266.305 180.00 1.13178 0 3 9 2 o 295.942 266.305 180.00 1.13178 3 3 6 1 o 30912.891 30608.500 180.00 1.12096 3 3 6 2 o 31824.107 30608.500 180.00 1.12096 0 5 1 1 o 160.460 199.797 0.00 1.11276 0 5 1 2 o 77.880 199.797 0.00 1.11276 4 3 1 1 o 166.564 205.630 180.00 1.11276 3 4 1 1 o 254.294 303.995 180.00 1.11276 3 4 1 2 o 147.089 303.995 180.00 1.11276 4 3 1 2 o 82.297 205.630 180.00 1.11276 1 4 7 1 o 1061.446 1114.454 180.00 1.08931 4 1 7 1 o 357.884 379.266 180.00 1.08931 4 1 7 2 o 390.781 379.266 180.00 1.08931 1 4 7 2 o 1143.002 1114.454 180.00 1.08931 0 5 3 1 o 1251.948 1345.591 0.00 1.08071 1 5 2 1 o 27296.754 28898.781 180.00 1.07965 5 1 2 1 o 33373.848 35332.47 180.00 1.07965 0 5 3 2 o 1261.687 1345.591 0.00 1.08071 3 4 3 1 o 406.518 442.693 0.00 1.08071 4 3 3 1 o 1253.503 1349.014 180.00 1.08071 1 5 2 2 o 28138.211 28898.781 180.00 1.07965 5 1 2 2 o 34402.586 35332.47 180.00 1.07965 4 2 6 1 o 36.080 38.903 180.00 1.07836 2 4 6 1 o 3.172 3.420 180.00 1.07836 3 4 3 2 o 410.335 442.693 0.00 1.08071 4 3 3 2 o 1263.580 1349.014 180.00 1.08071 2 2 10 1 o 74.566 72.725 0.00 1.07579 4 2 6 2 o 40.226 38.903 180.00 1.07836 2 4 6 2 o 3.536 3.420 180.00 1.07836 2 2 10 2 o 83.360 72.725 0.00 1.07579 0 0 12 1 o 40772.25 39845.09 180.00 1.06910 0 0 12 2 o 42457.60 39845.09 180.00 1.06910 1 2 11 1 o 38.348 0.174 0.00 1.05675 2 1 11 1 o 1134.981 918.664 0.00 1.05675 1 2 11 2 o 10.494 0.174 0.00 1.05675 2 1 11 2 o 977.144 918.664 0.00 1.05675 0 4 8 1 o 31985.465 29828.715 0.00 1.05302 0 4 8 2 o 32749.275 29828.715 0.00 1.05302 2 3 9 1 o 888.808 750.822 180.00 1.04890 3 2 9 1 o 36.640 9.033 0.00 1.04890 2 3 9 2 o 1104.184 750.822 180.00 1.04890 3 2 9 2 o 79.730 9.033 0.00 1.04890 3 1 10 1 o 29638.799 28473.082 180.00 1.03796 1 3 10 1 o 29676.883 28509.645 0.00 1.03796 1 5 4 1 o 55.601 55.874 0.00 1.03650 5 1 4 1 o 90.863 91.309 180.00 1.03650 3 1 10 2 o 30281.396 28473.082 180.00 1.03796 1 3 10 2 o 30320.289 28509.645 0.00 1.03796 5 1 4 2 o 105.107 91.309 180.00 1.03650 1 5 4 2 o 64.317 55.874 0.00 1.03650 5 2 1 1 o 31.101 2.415 0.00 1.03370 2 5 1 1 o 726.277 605.925 0.00 1.03370 1 1 12 1 o 155.174 130.717 0.00 1.03195 5 2 1 2 o 10.373 2.415 0.00 1.03370 2 5 1 2 o 639.310 605.925 0.00 1.03370 1 1 12 2 o 124.633 130.717 0.00 1.03195 0 5 5 1 o -17.772 23.544 180.00 1.02413 3 4 5 1 o 202.734 303.056 0.00 1.02413 4 3 5 1 o -19.742 22.074 0.00 1.02413 0 5 5 2 o -64.757 23.544 180.00 1.02413 4 3 5 2 o -64.038 22.074 0.00 1.02413 3 4 5 2 o 96.463 303.056 0.00 1.02413 3 3 8 1 o -7.401 172.418 180.00 1.01747 3 3 8 2 o -7.401 172.418 180.00 1.01747 5 2 3 1 o -29.446 183.613 180.00 1.00786 2 5 3 1 o -105.931 10.815 0.00 1.00786 5 2 3 2 o 116.457 183.613 180.00 1.00786 2 5 3 2 o -25.983 10.815 0.00 1.00786 0 2 12 1 o 23445.809 23229.115 0.00 0.99843 0 2 12 2 o 25444.953 23229.115 0.00 0.99843 0 3 11 1 o 519.786 411.717 180.00 0.98835 4 4 0 1 o 21032.729 18768.908 0.00 0.98727 0 3 11 2 o 441.607 411.717 180.00 0.98835 2 4 8 1 o 21427.176 20003.656 0.00 0.98529 4 2 8 1 o 25570.482 23873.334 180.00 0.98529 4 4 0 2 o 19728.557 18768.908 0.00 0.98727 4 2 8 2 o 26385.475 23873.334 180.00 0.98529 2 4 8 2 o 22110.781 20003.656 0.00 0.98529 1 4 9 1 o 267.550 215.000 180.00 0.98191 4 1 9 1 o 157.667 118.979 0.00 0.98191 1 4 9 2 o 376.635 215.000 180.00 0.98191 4 1 9 2 o 237.976 118.979 0.00 0.98191 1 5 6 1 o 30561.145 27405.666 0.00 0.97482 5 1 6 1 o 22122.381 19835.682 0.00 0.97482 4 4 2 1 o 10.349 8.713 180.00 0.97578 5 1 6 2 o 22685.660 19835.682 0.00 0.97482 1 5 6 2 o 31338.438 27405.666 0.00 0.97482 0 1 13 1 o 94.508 59.960 180.00 0.97181 4 4 2 2 o 9.440 8.713 180.00 0.97578 0 1 13 2 o 94.078 59.960 180.00 0.97181 5 2 5 1 o 589.847 898.424 180.00 0.96151 2 5 5 1 o 464.528 716.174 180.00 0.96151 5 2 5 2 o 232.735 898.424 180.00 0.96151 2 5 5 2 o 173.301 716.174 180.00 0.96151 0 5 7 1 o -2.511 143.925 180.00 0.95379 0 5 7 2 o 145.505 143.925 180.00 0.95379 3 4 7 1 o 71.232 301.150 180.00 0.95379 4 3 7 1 o -5.210 139.555 0.00 0.95379 3 4 7 2 o 305.765 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