#------------------------------------------------------------------------------
#$Date: 2016-04-06 22:07:23 +0300 (Wed, 06 Apr 2016) $
#$Revision: 181918 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/30/04/2300480.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2300480
_cell_angle_alpha                90.000
_cell_angle_beta                 100.138
_cell_angle_gamma                90.000
_cell_length_a                   5.3460
_cell_length_b                   13.8593
_cell_length_c                   14.1995
_exptl_crystal_F_000             832.00
_reflns_d_resolution_high        0.7676
_cod_data_source_file            kk5175Pb2sup11.hkl
_cod_data_source_block           Pb2
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  P21/n'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            355.17
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 56229.42 47931.05 1265.17 o
4 0 0 10381.86 10737.64 608.35 o
6 0 0 80.33 44.46 50.98 o
1 1 0 370.65 449.38 32.62 o
2 1 0 6202.86 6191.26 159.27 o
3 1 0 12221.35 12255.41 291.77 o
4 1 0 16835.14 17380.24 415.51 o
5 1 0 8813.39 8680.21 272.44 o
6 1 0 11225.29 11005.14 592.02 o
1 2 0 44591.28 39394.59 1160.98 o
2 2 0 17625.70 17047.67 329.94 o
3 2 0 9989.11 10106.06 265.45 o
4 2 0 6566.44 6925.14 376.05 o
5 2 0 609.48 638.82 77.66 o
6 2 0 39.91 25.82 48.60 o
1 3 0 12094.61 11641.11 250.68 o
2 3 0 105.82 164.36 17.89 o
3 3 0 36657.58 37246.53 1052.58 o
4 3 0 251.10 293.81 36.01 o
5 3 0 30726.51 30600.35 795.44 o
6 3 0 92.33 118.40 48.35 o
0 4 0 507.52 619.81 67.54 o
1 4 0 21701.84 20443.11 576.12 o
2 4 0 9883.82 10266.21 192.11 o
3 4 0 14223.42 14825.45 363.36 o
4 4 0 3239.37 3307.49 132.17 o
5 4 0 35.72 44.63 20.96 o
6 4 0 662.32 738.61 94.22 o
1 5 0 6602.83 7014.52 231.25 o
2 5 0 7238.56 7262.53 156.20 o
3 5 0 3342.41 3583.07 116.58 o
4 5 0 14695.17 14442.88 312.22 o
5 5 0 5663.03 5865.90 245.84 o
6 5 0 12462.37 11540.56 621.58 o
0 6 0 74845.88 79323.74 3793.45 o
1 6 0 410.42 486.05 47.26 o
2 6 0 61933.55 58217.71 1551.23 o
3 6 0 30.40 87.04 16.24 o
4 6 0 3964.82 3933.44 210.39 o
5 6 0 95.00 198.65 43.31 o
6 6 0 580.32 507.70 102.05 o
1 7 0 2590.90 2859.21 124.56 o
2 7 0 5751.03 5523.75 218.97 o
3 7 0 12003.57 11420.00 368.68 o
4 7 0 15664.71 15608.20 575.84 o
5 7 0 8581.04 8484.82 474.44 o
6 7 0 11890.39 13426.59 809.32 o
0 8 0 8185.44 8935.21 304.95 o
1 8 0 35795.75 39146.04 1590.08 o
2 8 0 9194.42 8760.36 290.77 o
3 8 0 13465.41 13003.75 482.21 o
4 8 0 479.53 487.91 50.58 o
5 8 0 747.35 709.24 154.34 o
6 8 0 8.73 95.53 65.42 o
1 9 0 2197.56 2353.91 117.75 o
2 9 0 636.10 611.90 53.72 o
3 9 0 25586.01 25563.06 1148.73 o
4 9 0 478.70 431.63 72.94 o
5 9 0 33088.36 33078.86 1362.91 o
0 10 0 20889.29 21232.87 651.88 o
1 10 0 21885.39 21611.30 508.10 o
2 10 0 8234.90 8909.30 365.88 o
3 10 0 11265.06 11085.55 506.56 o
4 10 0 2924.78 2849.97 285.36 o
5 10 0 1427.30 1431.82 385.57 o
1 11 0 1751.00 1649.91 105.32 o
2 11 0 6974.28 7203.27 212.74 o
3 11 0 4246.70 4010.56 232.31 o
4 11 0 9429.06 10191.59 553.27 o
5 11 0 2889.22 3140.12 873.67 o
0 12 0 39864.18 40200.04 964.35 o
1 12 0 1318.80 1345.08 95.10 o
2 12 0 26206.99 26693.58 974.60 o
3 12 0 509.62 577.05 81.22 o
4 12 0 7196.57 7159.62 558.87 o
5 12 0 36.34 100.71 83.92 o
1 13 0 2842.52 2708.31 146.43 o
2 13 0 6000.20 6041.54 293.47 o
3 13 0 7119.21 7181.07 390.16 o
4 13 0 9300.68 9310.18 872.45 o
0 14 0 8775.70 8753.20 460.92 o
1 14 0 15847.32 15331.97 455.01 o
2 14 0 3009.07 2834.93 228.88 o
3 14 0 3403.62 3434.44 260.72 o
4 14 0 757.99 720.72 153.10 o
1 15 0 1651.48 1762.74 136.04 o
2 15 0 10.98 66.56 45.49 o
3 15 0 13423.77 13066.41 750.83 o
0 16 0 11215.21 10576.00 530.09 o
1 16 0 10762.95 9634.76 442.62 o
2 16 0 7910.67 7323.21 388.33 o
3 16 0 3891.01 3440.29 358.87 o
1 17 0 1143.44 1300.53 152.42 o
2 17 0 2786.56 2457.95 219.22 o
0 18 0 15571.72 13688.46 1027.63 o
-5 0 1 14783.46 13893.47 677.12 o
-3 0 1 34519.99 33328.31 1123.69 o
-1 0 1 15480.80 17312.33 2973.44 o
1 0 1 7344.39 7969.32 525.87 o
3 0 1 5981.10 6139.57 472.68 o
5 0 1 16309.50 16539.86 960.73 o
-6 1 1 341.98 279.34 86.60 o
-5 1 1 1449.92 1569.48 119.80 o
-4 1 1 18.48 68.76 19.07 o
-3 1 1 13388.28 13356.38 381.11 o
-2 1 1 1875.99 1941.39 72.08 o
-1 1 1 47217.41 39997.00 1725.87 o
1 1 1 43007.64 41969.56 1097.72 o
2 1 1 19079.67 18166.18 695.48 o
3 1 1 26785.03 25953.48 520.86 o
4 1 1 3344.89 3417.19 171.85 o
5 1 1 6275.21 6450.25 309.58 o
6 1 1 487.07 438.62 171.30 o
-6 2 1 14977.26 14206.08 526.60 o
-5 2 1 4126.98 3861.52 214.10 o
-4 2 1 43922.48 41515.86 1875.06 o
-3 2 1 4562.05 4475.53 124.36 o
-2 2 1 40623.06 38139.40 821.40 o
-1 2 1 4700.22 4698.53 207.41 o
0 2 1 9411.74 9323.23 413.48 o
1 2 1 111.33 191.35 27.49 o
2 2 1 5721.29 5715.08 132.81 o
3 2 1 6271.11 6507.64 226.03 o
4 2 1 23672.25 24261.44 647.11 o
5 2 1 10776.79 9803.81 458.08 o
6 2 1 19365.11 19474.02 747.29 o
-6 3 1 831.20 813.39 112.43 o
-5 3 1 506.42 569.64 70.54 o
-4 3 1 4810.48 5008.44 174.16 o
-3 3 1 219.90 287.93 25.34 o
-2 3 1 30199.23 28934.36 662.24 o
-1 3 1 2343.23 2307.80 71.50 o
0 3 1 50632.07 49113.66 899.28 o
1 3 1 2915.19 2911.89 159.08 o
2 3 1 37566.91 36498.81 495.36 o
3 3 1 1087.75 1222.13 75.80 o
4 3 1 10637.41 11237.21 358.36 o
5 3 1 9.75 53.38 23.27 o
6 3 1 1335.54 1384.77 147.74 o
-6 4 1 16459.26 15887.27 555.10 o
-5 4 1 7488.19 7727.69 298.48 o
-4 4 1 43285.08 42259.30 754.11 o
-3 4 1 5650.92 5436.22 234.02 o
-2 4 1 33389.95 31406.87 752.98 o
-1 4 1 5989.81 5903.72 146.30 o
0 4 1 4806.56 4960.99 174.96 o
1 4 1 3395.96 3378.86 166.22 o
2 4 1 1671.32 1619.25 58.42 o
3 4 1 3609.12 3767.86 133.32 o
4 4 1 22845.89 22189.78 597.75 o
5 4 1 4704.00 4663.81 221.51 o
6 4 1 23284.51 20873.26 918.27 o
-6 5 1 163.28 234.53 49.21 o
-5 5 1 494.10 539.13 70.64 o
-4 5 1 107.47 83.51 20.03 o
-3 5 1 7344.24 7501.93 205.49 o
-2 5 1 7784.04 7977.28 158.92 o
-1 5 1 70727.62 65975.63 1563.88 o
0 5 1 21901.61 20034.46 555.72 o
1 5 1 89222.59 87585.39 5296.75 o
2 5 1 13138.10 12847.01 319.04 o
3 5 1 32247.08 32217.18 560.55 o
4 5 1 4436.30 4330.44 171.31 o
5 5 1 2358.73 2323.94 148.47 o
6 5 1 621.21 616.36 125.31 o
-6 6 1 54.36 45.78 61.05 o
-5 6 1 19203.39 19010.15 508.00 o
-4 6 1 107.26 101.99 18.69 o
-3 6 1 22826.24 23981.61 606.29 o
-2 6 1 725.33 852.13 45.66 o
-1 6 1 26093.03 28051.97 1057.14 o
0 6 1 595.77 593.90 48.15 o
1 6 1 44.21 107.79 21.26 o
2 6 1 1.87 23.66 24.53 o
3 6 1 7353.66 7307.33 196.60 o
4 6 1 409.73 294.54 40.54 o
5 6 1 8514.69 8431.82 304.41 o
6 6 1 67.93 66.35 50.47 o
-6 7 1 911.41 1110.26 306.46 o
-5 7 1 212.99 193.51 49.89 o
-4 7 1 466.13 542.81 49.98 o
-3 7 1 9295.27 10298.47 224.97 o
-2 7 1 3910.51 3999.21 121.18 o
-1 7 1 47597.75 43768.60 1302.12 o
0 7 1 6636.08 6593.51 167.04 o
1 7 1 38013.63 38628.96 1910.38 o
2 7 1 7710.01 8104.26 344.86 o
3 7 1 38508.81 39202.99 643.75 o
4 7 1 1211.01 1314.34 81.15 o
5 7 1 3604.05 3736.18 374.75 o
6 7 1 91.57 287.98 170.10 o
-6 8 1 15946.06 16200.85 1442.68 o
-5 8 1 5598.87 5987.06 482.86 o
-4 8 1 20634.09 21564.42 535.31 o
-3 8 1 5742.59 6248.94 233.81 o
-2 8 1 23263.93 23395.71 402.92 o
-1 8 1 6516.66 6898.85 307.25 o
0 8 1 4588.78 5021.21 164.58 o
1 8 1 1086.86 1102.33 68.87 o
2 8 1 11660.97 12256.84 301.80 o
3 8 1 5096.05 4936.75 230.04 o
4 8 1 12021.11 12574.99 420.59 o
5 8 1 2349.44 2682.42 325.13 o
6 8 1 14542.34 15631.76 916.15 o
-5 9 1 1036.45 1271.20 223.50 o
-4 9 1 850.11 924.68 147.24 o
-3 9 1 35.17 63.75 17.90 o
-2 9 1 10856.27 11249.55 417.52 o
-1 9 1 372.96 466.27 59.65 o
0 9 1 23171.53 24471.98 730.77 o
1 9 1 206.45 243.15 32.88 o
2 9 1 30923.21 31291.87 1543.69 o
3 9 1 863.37 906.52 96.25 o
4 9 1 8931.55 8188.35 632.28 o
5 9 1 30.47 121.31 91.67 o
-5 10 1 5333.15 5109.02 469.82 o
-4 10 1 20304.75 21267.21 952.66 o
-3 10 1 3361.33 3628.19 171.81 o
-2 10 1 14512.57 16401.54 688.45 o
-1 10 1 730.81 843.03 97.31 o
0 10 1 865.06 933.54 66.82 o
1 10 1 380.46 474.82 56.89 o
2 10 1 1969.54 2130.02 182.98 o
3 10 1 383.91 402.80 62.84 o
4 10 1 18617.25 17995.49 763.39 o
5 10 1 4046.93 4149.15 432.27 o
-5 11 1 265.12 359.37 214.61 o
-4 11 1 300.18 330.36 89.71 o
-3 11 1 6807.74 8069.40 365.03 o
-2 11 1 1679.65 2080.82 169.67 o
-1 11 1 26721.05 25879.73 784.90 o
0 11 1 13268.64 13686.29 308.12 o
1 11 1 46867.60 48415.55 1637.28 o
2 11 1 3383.80 3791.07 163.61 o
3 11 1 17753.24 18088.20 662.42 o
4 11 1 1509.71 1994.67 212.72 o
5 11 1 2849.69 3021.78 377.31 o
-5 12 1 12421.63 13647.40 2427.41 o
-4 12 1 682.11 697.90 243.71 o
-3 12 1 20080.26 21546.80 661.24 o
-2 12 1 187.66 258.33 55.14 o
-1 12 1 3035.67 3178.76 163.85 o
0 12 1 356.63 416.70 46.15 o
1 12 1 4.70 19.76 12.02 o
2 12 1 168.90 172.73 32.46 o
3 12 1 5328.09 5121.93 257.60 o
4 12 1 194.02 224.45 76.47 o
5 12 1 12664.62 13416.25 2789.80 o
-4 13 1 105.38 104.90 65.72 o
-3 13 1 3410.98 3718.19 277.12 o
-2 13 1 3893.61 4046.11 206.06 o
-1 13 1 18522.67 18090.48 573.81 o
0 13 1 7538.59 7629.31 227.53 o
1 13 1 36227.26 35736.61 850.31 o
2 13 1 2600.34 2543.72 192.04 o
3 13 1 12987.79 13065.29 599.09 o
4 13 1 1911.06 2050.32 224.40 o
-4 14 1 19587.20 19548.61 1060.99 o
-3 14 1 4981.56 5456.20 808.24 o
-2 14 1 15271.07 15314.59 587.96 o
-1 14 1 868.53 1078.16 107.01 o
0 14 1 1162.51 1213.58 114.84 o
1 14 1 18.83 89.63 27.36 o
2 14 1 1225.95 1207.45 130.11 o
3 14 1 799.08 682.19 100.10 o
4 14 1 9037.41 9408.71 669.28 o
-3 15 1 141.71 80.47 44.87 o
-2 15 1 8168.50 7806.80 398.12 o
-1 15 1 367.31 491.99 73.76 o
0 15 1 19772.48 18926.74 533.03 o
1 15 1 937.82 877.73 123.34 o
2 15 1 19622.16 17547.13 647.87 o
3 15 1 1.12 68.65 53.46 o
-3 16 1 2945.04 2974.44 333.25 o
-2 16 1 9442.61 8473.21 421.20 o
-1 16 1 478.38 564.50 100.81 o
0 16 1 1950.79 2086.83 152.70 o
1 16 1 118.28 138.12 55.47 o
2 16 1 2033.94 1998.68 200.38 o
3 16 1 745.83 707.36 156.92 o
-2 17 1 4847.10 4383.29 296.97 o
-1 17 1 13499.44 12274.82 511.35 o
0 17 1 5289.05 4498.93 287.23 o
1 17 1 18443.94 16321.87 617.72 o
2 17 1 3924.87 3427.49 261.27 o
0 18 1 63.44 52.58 90.58 o
-6 0 2 10706.00 10212.48 796.65 o
-4 0 2 5.34 25.10 36.89 o
-2 0 2 11786.80 11583.90 379.84 o
2 0 2 126148.02 103173.44 2703.69 o
4 0 2 27807.02 25783.86 900.60 o
6 0 2 5249.53 5376.69 575.29 o
-6 1 2 11292.12 10723.43 578.70 o
-5 1 2 5404.92 5381.22 364.68 o
-4 1 2 32015.28 28881.29 669.00 o
-3 1 2 25048.82 23873.08 501.83 o
-2 1 2 33526.33 31311.73 515.21 o
-1 1 2 2630.46 2761.86 127.91 o
1 1 2 400.46 606.44 58.26 o
2 1 2 1657.60 1784.84 118.19 o
3 1 2 734.81 803.41 84.63 o
4 1 2 4799.17 4791.27 258.97 o
5 1 2 4553.47 4604.37 290.47 o
6 1 2 7379.01 7434.30 380.92 o
-6 2 2 991.37 933.72 116.89 o
-5 2 2 2761.08 2965.98 256.32 o
-4 2 2 41.74 81.94 25.00 o
-3 2 2 1948.09 1855.00 106.78 o
-2 2 2 6461.80 6286.94 200.86 o
-1 2 2 12901.69 13101.96 310.92 o
0 2 2 13675.70 12817.14 273.95 o
1 2 2 43444.51 41329.02 901.76 o
2 2 2 43649.39 44045.77 629.38 o
3 2 2 16119.54 15625.67 365.63 o
4 2 2 7534.12 7239.86 229.49 o
5 2 2 9054.08 8570.93 377.55 o
6 2 2 328.72 339.75 75.55 o
-6 3 2 265.55 186.74 48.76 o
-5 3 2 38097.69 37115.16 924.67 o
-4 3 2 2321.62 2293.11 102.53 o
-3 3 2 50510.08 49287.72 751.50 o
-2 3 2 11.15 53.95 20.93 o
-1 3 2 58817.98 55731.36 874.20 o
0 3 2 5805.26 5858.63 146.18 o
1 3 2 13712.97 13824.69 350.65 o
2 3 2 368.04 498.56 37.45 o
3 3 2 14345.99 15049.83 316.64 o
4 3 2 933.38 892.45 80.59 o
5 3 2 21378.70 21345.94 656.38 o
6 3 2 25.11 37.80 26.20 o
-6 4 2 2682.50 2734.75 200.41 o
-5 4 2 1601.15 1567.00 135.81 o
-4 4 2 16.09 41.67 18.69 o
-3 4 2 734.76 664.00 45.90 o
-2 4 2 2827.91 2673.09 104.79 o
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0 4 2 40850.63 39676.49 683.62 o
1 4 2 27152.52 26269.64 1026.18 o
2 4 2 12398.25 12421.20 361.53 o
3 4 2 33647.22 33240.51 581.11 o
4 4 2 9631.94 9777.53 284.55 o
5 4 2 5572.20 5711.63 252.57 o
6 4 2 533.43 808.17 126.18 o
-6 5 2 6112.64 6081.23 271.93 o
-5 5 2 6988.27 7248.93 273.63 o
-4 5 2 15433.88 14989.59 404.24 o
-3 5 2 7024.35 6931.77 248.25 o
-2 5 2 29561.25 28404.82 452.71 o
-1 5 2 4266.14 4243.44 116.69 o
0 5 2 2026.32 2124.64 85.58 o
1 5 2 853.82 1003.66 82.13 o
2 5 2 389.81 420.51 44.34 o
3 5 2 2172.84 2280.71 91.14 o
4 5 2 5152.76 5106.98 206.46 o
5 5 2 2045.54 2050.18 141.65 o
6 5 2 8538.23 8532.96 450.62 o
-6 6 2 8333.83 8663.26 419.64 o
-5 6 2 258.17 318.24 56.14 o
-4 6 2 1140.48 1306.73 99.35 o
-3 6 2 74.59 84.71 17.09 o
-2 6 2 16494.36 16094.47 475.68 o
-1 6 2 435.48 439.08 35.74 o
0 6 2 79729.93 77150.94 2361.12 o
1 6 2 740.08 887.32 65.99 o
2 6 2 53831.59 52080.75 4232.83 o
3 6 2 3.67 15.32 31.57 o
4 6 2 32634.10 32379.51 706.47 o
5 6 2 73.63 99.38 57.49 o
6 6 2 3447.13 3374.53 300.28 o
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-5 7 2 9423.21 9096.02 432.65 o
-4 7 2 13238.27 13696.73 322.81 o
-3 7 2 18435.77 18944.72 949.86 o
-2 7 2 18667.12 17565.62 433.17 o
-1 7 2 16043.90 16562.65 668.76 o
0 7 2 2237.70 2209.38 94.58 o
1 7 2 590.49 686.81 46.05 o
2 7 2 130.28 155.63 39.75 o
3 7 2 715.18 761.80 71.77 o
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5 7 2 4199.61 4301.98 414.14 o
6 7 2 8021.62 8529.83 649.59 o
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-5 8 2 2265.44 2154.22 234.96 o
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2 9 2 3.23 6.33 20.16 o
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4 9 2 4.04 63.11 34.14 o
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-5 10 2 288.80 416.98 112.94 o
-4 10 2 3.35 22.85 32.81 o
-3 10 2 952.41 958.66 82.87 o
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0 10 2 6403.60 6945.93 214.58 o
1 10 2 24776.60 24762.35 1016.52 o
2 10 2 15450.04 16004.52 599.01 o
3 10 2 19832.56 19423.00 663.91 o
4 10 2 4372.51 4120.35 346.10 o
5 10 2 4751.89 4776.42 472.43 o
-5 11 2 5151.89 5849.92 508.75 o
-4 11 2 13673.60 13852.89 1207.77 o
-3 11 2 8839.71 9717.68 358.00 o
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0 11 2 12875.20 13690.96 578.32 o
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2 11 2 2.05 -29.00 29.00 o
3 11 2 188.61 135.30 21.22 o
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5 11 2 1801.60 2197.05 639.17 o
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-1 12 2 717.81 783.38 86.16 o
0 12 2 31457.02 33422.05 1157.76 o
1 12 2 0.95 34.07 23.05 o
2 12 2 32181.43 31367.29 1126.91 o
3 12 2 49.09 57.39 36.12 o
4 12 2 15197.62 15995.51 831.80 o
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0 13 2 5737.73 5665.42 213.67 o
1 13 2 574.62 639.97 66.99 o
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0 1 17 211.17 371.55 145.76 o
1 1 17 5708.89 6271.39 820.73 o
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1 2 17 4157.69 4113.28 510.80 o
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0 3 17 455.84 689.64 195.02 o
1 3 17 6.07 11.46 128.60 o
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0 5 17 61.03 261.08 141.48 o
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0 6 17 508.84 421.70 146.69 o
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0 0 18 341.68 644.83 276.58 o
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-1 1 18 6165.91 6859.94 638.01 o
0 1 18 10466.14 11577.86 850.99 o
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-1 2 18 611.98 712.75 191.51 o
0 2 18 207.79 349.12 150.95 o
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