#------------------------------------------------------------------------------ #$Date: 2023-09-14 04:39:52 +0300 (Thu, 14 Sep 2023) $ #$Revision: 286336 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/22/2312284.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312284 loop_ _publ_author_name 'Yamashita, Keishiro' 'Nakayama, Kazuya' 'Komatsu, Kazuki' 'Ohhara, Takashi' 'Munakata, Koji' 'Hattori, Takanori' 'Sano-Furukawa, Asami' 'Kagi, Hiroyuki' _publ_section_title ; The hydrogen-bond network in sodium chloride tridecahydrate: analogy with ice VI. ; _journal_coeditor_code NE5013SUP1 _journal_issue 5 _journal_name_full 'Acta crystallographica Section B, Structural science, crystal engineering and materials' _journal_paper_doi 10.1107/S2052520623007199 _journal_volume 79 _journal_year 2023 _chemical_formula_moiety 'Na Cl, 13(H2 O)' _chemical_formula_sum 'Cl H26 Na O13' _chemical_formula_weight 292.65 _chemical_name_common 'Sodium chloride tridecahydrate' _chemical_name_systematic 'Sodium chloride tridecahydrate' _space_group_crystal_system monoclinic _space_group_IT_number 12 _space_group_name_Hall '-C 2y' _space_group_name_H-M_alt 'C 1 2/m 1' _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 119.475(13) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.403(4) _cell_length_b 11.882(2) _cell_length_c 10.905(3) _cell_measurement_reflns_used 1289 _cell_measurement_temperature 299 _cell_measurement_theta_max 33.9045 _cell_measurement_theta_min 4.1123 _cell_volume 1286.3(6) _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _diffrn_ambient_temperature 299 _diffrn_detector_area_resol_mean 10 _diffrn_measured_fraction_theta_full 0.270 _diffrn_measured_fraction_theta_max 0.263 _diffrn_measurement_details ; scan: Number of images: 80 Slice: -40.0000 - 40.0000 Image width: 1.0000 Exp time: 600.0000 Rotation axis: phi Omega: 0.0000 Chi: 0.0000 Phi: 0.0000 XTD: 80.0000 2theta: 0.0885 ; _diffrn_measurement_device ; RAXIS conversion ; _diffrn_measurement_method dtprofit.ref _diffrn_radiation_detector RX _diffrn_radiation_monochromator cmf _diffrn_radiation_source 'Sealed Tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71075 _diffrn_reflns_av_R_equivalents 0.0242 _diffrn_reflns_av_unetI/netI 0.0200 _diffrn_reflns_Laue_measured_fraction_full 0.270 _diffrn_reflns_Laue_measured_fraction_max 0.263 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 646 _diffrn_reflns_point_group_measured_fraction_full 0.270 _diffrn_reflns_point_group_measured_fraction_max 0.263 _diffrn_reflns_reduction_process 'Lp corrections applied' _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.277 _diffrn_reflns_theta_min 4.293 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_current 24.0000 _diffrn_source_power 1.2000 _diffrn_source_type 'Rigaku (Mo) X-ray Source' _diffrn_source_voltage 50.0000 _diffrn_standards_interval_time 0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.383 _exptl_absorpt_correction_T_max 0.5688 _exptl_absorpt_correction_T_min 0.4839 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details 'self-made program for diamond anvil cell' _exptl_crystal_colour Colorless _exptl_crystal_density_diffrn 1.511 _exptl_crystal_description platelet _exptl_crystal_F_000 632 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.3 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.121 _refine_diff_density_min -0.154 _refine_diff_density_rms 0.034 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.957 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 35 _refine_ls_number_reflns 360 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.957 _refine_ls_R_factor_all 0.0423 _refine_ls_R_factor_gt 0.0423 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0543P)^2^+3.3523P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0987 _refine_ls_wR_factor_ref 0.0987 _reflns_number_gt 360 _reflns_number_total 360 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ne5013sup1.cif _cod_data_source_block NaCl_13H2O _cod_original_sg_symbol_H-M 'C 2/m' _cod_original_formula_sum 'Na Cl O13 H26' _cod_database_code 2312284 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _exptl_absorpt_special_details 'self-made program for diamond anvil cell' _shelx_res_file ; TITL New structure shelx.res created by SHELXL-2018/3 at 17:20:13 on 20-Jul-2022 CELL 0.71075 11.4026 11.8825 10.9052 90.000000 119.4750 90.000000 ZERR 1 0.0035 0.0022 0.0031 0.000000 0.0126 0.000000 LATT 7 SYMM -X,+Y,-Z SFAC Cl Na O H UNIT 4.000000 4.000000 52.000000 104 L.S. 5 LIST 3 ACTA REM BOND $H REM DFIX 0.85 0.02 O10 H8 REM DFIX 0.85 0.02 O10 H6 REM DFIX 0.85 0.02 O11 H2 REM DFIX 0.85 0.02 O11 H9 REM DFIX 0.85 0.02 O4 H7 REM DFIX 0.85 0.02 O4 H10 WGHT 0.054300 3.352300 FVAR 1.20463 CL 1 0.406512 0.000000 0.308055 10.50000 0.02786 NA1 2 0.000000 0.000000 0.000000 10.25000 0.02617 NA2 2 0.000000 0.000000 0.500000 10.25000 0.02558 O2 3 0.852323 0.139656 0.005557 11.00000 0.03213 O1 3 0.106638 0.000000 0.243400 10.50000 0.03275 O4 3 0.994901 0.149385 0.349666 11.00000 0.03145 O6 3 0.740742 0.246375 0.247676 11.00000 0.03384 O3 3 0.237925 0.000000 0.626147 10.50000 0.03103 O8 3 0.306384 0.000000 0.912105 10.50000 0.03394 O5 3 0.344545 0.162596 0.515865 11.00000 0.03086 O7 3 0.480769 0.157583 0.127154 11.00000 0.03559 HKLF 4 REM New structure REM wR2 = 0.0987, GooF = S = 0.957, Restrained GooF = 0.957 for all data REM R1 = 0.0423 for 360 Fo > 4sig(Fo) and 0.0423 for all 360 data REM 35 parameters refined using 0 restraints END WGHT 0.0562 2.2787 REM Highest difference peak 0.121, deepest hole -0.154, 1-sigma level 0.034 Q1 1 0.3607 0.0727 0.7985 11.00000 0.05 0.12 Q2 1 0.8040 0.2621 0.0808 11.00000 0.05 0.11 Q3 1 0.9247 0.0000 0.2531 10.50000 0.05 0.11 Q4 1 0.0647 0.0000 0.0350 10.50000 0.05 0.11 Q5 1 0.3700 0.0000 0.9664 10.50000 0.05 0.11 Q6 1 0.8798 0.1946 0.2951 11.00000 0.05 0.10 Q7 1 0.7354 0.2721 0.3043 11.00000 0.05 0.10 Q8 1 0.1964 0.0000 0.2862 10.50000 0.05 0.10 Q9 1 0.8806 0.1367 0.4355 11.00000 0.05 0.10 Q10 1 0.3470 0.1486 0.5590 11.00000 0.05 0.10 Q11 1 0.3508 0.1893 0.4511 11.00000 0.05 0.10 Q12 1 0.2572 0.0467 0.5750 11.00000 0.05 0.10 Q13 1 0.7936 0.0973 -0.1543 11.00000 0.05 0.10 Q14 1 0.0424 0.0000 -0.0759 10.50000 0.05 0.10 Q15 1 0.4939 0.0000 1.0461 10.50000 0.05 0.10 Q16 1 0.9630 0.1803 0.0813 11.00000 0.05 0.10 Q17 1 0.0774 0.1436 0.1565 11.00000 0.05 0.09 Q18 1 0.2789 0.0000 0.7890 10.50000 0.05 0.09 Q19 1 0.4208 0.1194 0.1617 11.00000 0.05 0.09 Q20 1 0.4897 0.0603 0.3726 11.00000 0.05 0.09 ; _shelx_res_checksum 95894 _shelx_hkl_file ; 0 0 2 266.25 4.53 3 1.613 1.788 32.842 38.635 0.721 0.696 0.501 0 0 3 6594.89 95.46 3 1.554 1.783 29.318 38.431 0.729 0.696 0.508 0 0 4 6748.07 97.92 3 1.504 1.785 25.753 38.500 0.737 0.696 0.513 0 -2 7 15.26 1.09 3 1.358 1.614 3.782 30.056 0.759 0.721 0.547 0 -2 9 3.95 1.05 3 1.377 1.762 10.159 37.533 0.756 0.699 0.529 -1 1 7 104.66 3.07 3 1.383 1.763 11.454 37.591 0.755 0.699 0.528 -1 -1 7 137.20 3.41 3 1.356 1.577 2.297 27.646 0.759 0.726 0.551 1 1 -5 6938.40 101.49 3 1.686 1.628 36.528 30.919 0.710 0.719 0.510 1 -1 -4 6035.38 87.83 3 1.682 1.544 36.342 25.225 0.711 0.731 0.519 1 1 -4 6288.44 91.36 3 1.503 1.509 25.675 22.168 0.737 0.736 0.543 -1 1 4 5934.01 86.34 3 1.413 1.624 16.406 30.668 0.751 0.719 0.540 -1 -1 4 5985.15 86.65 3 1.362 1.440 5.679 14.006 0.758 0.747 0.566 1 -1 -3 1517.71 22.65 3 1.563 1.492 29.895 20.519 0.728 0.739 0.538 -1 1 3 1445.89 21.61 3 1.409 1.567 15.975 26.905 0.751 0.728 0.547 1 1 -3 1529.54 22.45 3 1.373 1.422 9.298 10.838 0.757 0.749 0.567 -1 -1 3 1488.11 21.86 3 1.399 1.435 14.395 13.267 0.753 0.747 0.563 -1 3 6 2409.52 36.70 3 1.445 1.822 20.287 45.133 0.746 0.691 0.515 -1 -3 6 2535.77 37.11 3 1.748 1.824 39.174 40.030 0.701 0.690 0.484 1 -3 -2 1152.45 17.62 3 1.712 1.542 37.693 25.079 0.706 0.731 0.516 -1 3 2 1276.11 19.41 3 1.494 1.762 24.880 37.555 0.738 0.699 0.516 1 -3 -1 1512.67 22.59 3 1.659 1.549 35.221 25.598 0.714 0.730 0.521 -1 3 1 1671.40 24.85 3 1.471 1.670 22.867 33.227 0.742 0.712 0.529 1 -3 0 64.66 1.48 3 1.625 1.571 33.494 27.209 0.719 0.727 0.523 -1 3 0 59.98 1.42 3 1.417 1.551 16.982 25.710 0.750 0.730 0.548 1 -3 1 16.65 0.62 3 1.629 1.629 33.740 30.969 0.718 0.718 0.516 -1 3 -1 15.63 0.55 3 1.355 1.434 1.259 13.124 0.759 0.747 0.568 -1 5 -1 36.68 1.32 3 1.422 1.638 17.628 31.479 0.749 0.717 0.537 -1 7 -2 1361.86 20.61 3 1.387 1.679 12.255 33.675 0.755 0.711 0.537 -1 7 -3 6902.75 99.86 3 1.358 1.583 3.569 28.047 0.759 0.725 0.551 -2 0 10 321.48 6.73 3 1.368 1.730 7.881 36.141 0.758 0.704 0.533 -2 0 9 2587.52 23.98 3 1.362 1.660 5.648 32.683 0.759 0.714 0.542 -2 0 8 1279.38 13.23 3 1.358 1.599 3.990 29.119 0.759 0.723 0.549 2 0 -7 184.59 4.22 3 1.706 1.572 37.435 27.316 0.707 0.727 0.514 -2 0 7 180.69 4.16 3 1.357 1.545 3.066 25.294 0.759 0.731 0.555 2 0 -611373.61 92.84 3 1.567 1.503 30.156 21.630 0.728 0.737 0.536 -2 0 610628.29 154.06 3 1.357 1.496 3.115 20.998 0.759 0.738 0.560 -2 2 8 52.35 2.79 3 1.363 1.755 6.124 37.249 0.758 0.700 0.531 -2 -2 8 62.57 1.92 3 1.469 1.601 22.712 29.211 0.742 0.723 0.536 2 2 -7 860.09 13.71 3 1.618 1.629 33.148 30.977 0.720 0.718 0.517 -2 2 7 742.54 12.86 3 1.368 1.700 7.797 34.716 0.758 0.708 0.537 -2 -2 7 705.03 11.28 3 1.481 1.561 23.798 26.510 0.740 0.728 0.539 2 -2 -6 1882.68 28.92 3 1.696 1.489 36.963 20.235 0.709 0.739 0.524 2 2 -6 1975.17 29.36 3 1.458 1.519 21.688 23.100 0.744 0.735 0.546 -2 2 6 1923.50 29.46 3 1.372 1.646 8.908 31.930 0.757 0.716 0.542 -2 -2 6 1934.59 28.77 3 1.518 1.549 26.784 25.564 0.735 0.730 0.537 2 -2 1 9.16 0.47 3 1.503 1.675 25.678 33.501 0.737 0.712 0.525 2 4 -7 174.75 3.44 3 1.557 1.711 29.481 35.283 0.729 0.707 0.515 -2 4 7 167.45 4.81 3 1.392 1.844 13.287 43.102 0.754 0.688 0.518 -2 4 6 8970.29 131.90 3 1.401 1.853 14.699 41.087 0.752 0.686 0.517 2 4 -6 9498.36 137.24 3 1.375 1.549 9.711 25.584 0.756 0.730 0.552 -2 6 4 439.21 8.63 3 1.428 1.835 18.390 43.940 0.748 0.689 0.516 -2 6 3 767.61 13.21 3 1.425 1.859 18.019 41.270 0.749 0.686 0.513 -2 6 2 683.76 11.62 3 1.414 1.772 16.616 37.962 0.750 0.698 0.524 -2 6 1 180.38 4.08 3 1.395 1.681 13.721 33.784 0.753 0.711 0.536 -2 6 0 9912.56 143.77 3 1.370 1.591 8.549 28.587 0.757 0.724 0.548 -2 6 -1 1074.14 16.48 3 1.355 1.521 0.477 23.266 0.760 0.734 0.558 -2 8 -1 27.93 1.76 3 1.360 1.662 4.930 32.787 0.759 0.714 0.541 -2 8 -2 18.82 1.16 3 1.361 1.607 5.384 29.599 0.759 0.722 0.547 -2 8 -3 3.11 0.75 3 1.489 1.717 24.468 35.548 0.739 0.706 0.522 -2 10 -2 426.73 5.90 3 1.356 1.749 2.153 36.977 0.759 0.701 0.532 -2 10 -3 113.35 2.99 3 1.405 1.760 15.328 37.482 0.752 0.700 0.526 -3 1 11 68.64 3.67 3 1.375 1.764 9.810 37.646 0.756 0.699 0.529 -3 -1 11 117.58 3.82 3 1.460 1.727 21.864 36.020 0.744 0.704 0.524 -3 1 10 401.59 7.98 3 1.367 1.690 7.749 34.228 0.758 0.710 0.538 -3 -1 10 425.11 8.00 3 1.444 1.646 20.175 31.908 0.746 0.716 0.534 3 1 -9 718.44 9.00 3 1.707 1.636 37.479 31.372 0.707 0.717 0.507 -3 1 9 741.90 9.55 3 1.363 1.625 6.190 30.726 0.758 0.719 0.545 -3 -1 9 733.94 8.91 3 1.435 1.581 19.245 27.884 0.747 0.726 0.542 3 -1 -8 33.62 2.29 3 1.648 1.507 34.704 22.007 0.716 0.736 0.527 3 1 -8 32.44 1.90 3 1.557 1.551 29.538 25.746 0.729 0.730 0.532 -3 1 8 32.57 2.03 3 1.361 1.568 5.218 27.023 0.759 0.727 0.552 -3 -1 8 39.11 2.29 3 1.435 1.529 19.211 23.991 0.747 0.733 0.548 3 -1 -7 3983.51 60.10 3 1.541 1.463 28.432 17.274 0.731 0.743 0.543 3 1 -7 4004.13 59.33 3 1.449 1.492 20.748 20.553 0.745 0.739 0.550 -3 1 7 3737.70 55.58 3 1.360 1.517 4.975 22.969 0.759 0.735 0.558 -3 -1 7 3921.57 58.07 3 1.445 1.491 20.293 20.489 0.746 0.739 0.551 3 -1 -6 275.34 5.58 3 1.458 1.432 21.629 12.686 0.744 0.748 0.556 3 1 -6 268.77 5.24 3 1.379 1.464 10.801 17.455 0.756 0.743 0.561 -3 1 6 269.21 5.39 3 1.362 1.472 5.682 18.361 0.758 0.742 0.563 -3 -1 6 268.24 5.31 3 1.470 1.470 22.809 18.172 0.742 0.742 0.551 3 -1 -5 5483.39 80.20 3 1.397 1.416 14.095 9.469 0.753 0.750 0.565 3 1 -5 5570.61 81.18 3 1.355 1.483 0.624 19.594 0.760 0.740 0.562 -3 1 5 5268.45 77.07 3 1.367 1.433 7.654 12.939 0.758 0.748 0.566 -3 -1 5 5537.89 80.74 3 1.523 1.475 27.179 18.663 0.734 0.741 0.544 3 -3 -7 9500.67 138.96 3 1.658 1.444 35.167 14.690 0.714 0.746 0.533 3 3 -7 9653.11 140.09 3 1.383 1.541 11.627 24.994 0.755 0.731 0.552 -3 3 7 9020.67 131.90 3 1.358 1.648 3.863 32.017 0.759 0.716 0.543 3 -3 -5 400.16 7.64 3 1.501 1.406 25.506 6.612 0.737 0.752 0.554 -3 3 5 387.06 7.29 3 1.357 1.540 3.428 24.851 0.759 0.732 0.555 3 3 -5 415.16 7.04 3 1.429 1.713 18.572 35.337 0.748 0.706 0.528 3 -3 -3 33.44 1.60 3 1.401 1.398 14.700 2.511 0.752 0.753 0.567 -3 3 3 34.70 1.58 3 1.356 1.444 1.820 14.598 0.759 0.746 0.567 3 -3 -2 232.00 4.39 3 1.370 1.410 8.602 7.692 0.757 0.751 0.569 -3 3 2 227.68 4.34 3 1.367 1.412 7.552 8.483 0.758 0.751 0.569 3 -3 0 1909.18 28.28 3 1.362 1.489 5.689 20.233 0.758 0.739 0.561 -3 3 0 1982.37 29.37 3 1.569 1.517 30.250 22.985 0.727 0.735 0.534 3 -3 210543.01 152.27 3 1.471 1.734 22.868 36.332 0.742 0.703 0.522 3 -3 3 517.28 8.21 3 1.588 1.824 31.420 44.924 0.724 0.691 0.500 3 -5 -6 397.29 8.59 3 1.718 1.421 37.949 10.516 0.706 0.749 0.529 -3 5 6 483.18 9.66 3 1.372 1.762 9.149 37.568 0.757 0.699 0.529 3 5 -6 478.71 8.07 3 1.426 1.807 18.144 39.349 0.749 0.693 0.519 3 -5 -4 8151.29 120.01 3 1.590 1.414 31.530 8.895 0.724 0.750 0.543 -3 5 4 7475.34 109.44 3 1.369 1.635 8.154 31.320 0.757 0.718 0.543 3 -5 -3 124.99 3.44 3 1.542 1.418 28.508 9.986 0.731 0.750 0.548 -3 5 3 122.64 3.50 3 1.363 1.573 6.115 27.350 0.758 0.727 0.551 3 -5 -2 1269.66 20.00 3 1.503 1.429 25.676 12.086 0.737 0.748 0.551 -3 5 2 1272.68 19.79 3 1.356 1.514 2.514 22.711 0.759 0.735 0.558 3 -5 -1 7638.47 111.13 3 1.473 1.445 23.133 14.837 0.741 0.746 0.553 -3 5 1 7643.95 111.20 3 1.357 1.469 3.345 17.967 0.759 0.742 0.563 3 -5 0 4224.94 61.81 3 1.452 1.469 21.050 18.044 0.745 0.742 0.553 -3 5 0 4240.31 62.05 3 1.388 1.457 12.490 16.506 0.754 0.744 0.561 3 -5 1 4400.70 64.15 3 1.440 1.503 19.754 21.693 0.747 0.737 0.550 -3 5 -1 4783.30 69.68 3 1.516 1.542 26.651 25.078 0.735 0.731 0.537 3 -5 2 7238.68 104.82 3 1.442 1.555 19.959 26.044 0.746 0.729 0.544 3 -5 3 377.15 5.92 3 1.481 1.656 23.841 32.470 0.740 0.715 0.529 3 7 -8 52.50 1.47 3 1.399 1.800 14.453 39.096 0.753 0.694 0.522 -3 7 8 42.75 3.02 3 1.374 1.787 9.651 48.864 0.757 0.696 0.526 -3 7 7 1632.75 18.72 3 1.379 1.805 10.724 46.839 0.756 0.693 0.524 3 7 -7 1864.25 16.56 3 1.382 1.841 11.282 40.633 0.755 0.688 0.520 -3 7 5 3038.03 29.01 3 1.383 1.855 11.467 42.218 0.755 0.686 0.518 -3 7 4 1453.97 23.61 3 1.380 1.810 10.905 39.465 0.756 0.693 0.523 3 -7 -3 11.29 1.53 3 1.747 1.461 39.123 17.017 0.701 0.743 0.521 -3 7 3 22.12 1.85 3 1.374 1.733 9.476 36.300 0.757 0.703 0.532 -3 7 1 54.66 2.29 3 1.357 1.592 2.738 28.661 0.759 0.724 0.550 -3 7 -112534.61 101.95 3 1.394 1.536 13.636 24.569 0.753 0.732 0.552 -3 7 -2 856.77 13.37 3 1.555 1.665 29.352 32.987 0.729 0.713 0.520 -3 9 1 7497.45 63.81 3 1.360 1.744 4.769 36.790 0.759 0.702 0.533 -3 9 -2 938.34 9.71 3 1.437 1.672 19.476 33.319 0.747 0.712 0.532 -3 11 -1 101.66 3.61 3 1.363 1.784 6.169 38.444 0.758 0.696 0.528 -3 11 -2 2140.72 30.99 3 1.407 1.787 15.606 38.588 0.752 0.696 0.523 -3 11 -3 50.21 2.09 3 1.585 1.819 31.254 45.339 0.725 0.691 0.501 -4 0 11 10.80 1.98 3 1.439 1.660 19.628 32.694 0.747 0.714 0.533 -4 0 9 444.37 6.85 3 1.424 1.535 17.956 24.496 0.749 0.732 0.548 4 0 -8 7676.67 113.94 3 1.458 1.484 21.640 19.728 0.744 0.740 0.550 -4 0 8 7289.32 107.49 3 1.427 1.489 18.249 20.294 0.749 0.739 0.553 4 0 -7 3085.63 46.14 3 1.396 1.466 13.911 17.649 0.753 0.743 0.559 -4 0 7 2979.17 44.80 3 1.437 1.455 19.502 16.186 0.747 0.744 0.556 4 0 -6 1498.13 23.14 3 1.361 1.473 5.533 18.542 0.759 0.741 0.562 -4 0 6 1316.04 20.56 3 1.461 1.433 21.944 12.889 0.743 0.748 0.556 4 0 -3 1034.84 16.21 3 1.482 1.794 23.877 38.866 0.740 0.695 0.514 -4 0 3 1164.11 18.08 3 1.748 1.534 39.179 24.358 0.701 0.732 0.514 -4 2 11 169.40 5.40 3 1.376 1.725 10.140 35.930 0.756 0.705 0.533 -4 -2 11 148.08 4.24 3 1.636 1.741 34.082 36.656 0.717 0.702 0.504 4 -2 -9 577.40 9.07 3 1.635 1.480 34.050 19.236 0.717 0.741 0.531 4 2 -9 594.42 7.87 3 1.479 1.581 23.593 27.946 0.741 0.725 0.537 -4 2 9 505.54 7.79 3 1.367 1.596 7.647 28.898 0.758 0.723 0.548 -4 -2 9 550.18 7.39 3 1.628 1.614 33.663 30.079 0.719 0.721 0.518 4 -2 -8 262.02 5.23 3 1.543 1.449 28.561 15.331 0.731 0.745 0.545 4 2 -8 290.45 5.13 3 1.397 1.539 14.067 24.842 0.753 0.732 0.551 -4 2 8 247.97 5.01 3 1.366 1.542 7.246 25.053 0.758 0.731 0.554 -4 -2 8 247.97 4.56 3 1.653 1.584 34.954 28.097 0.715 0.725 0.518 4 -2 -7 1909.81 29.62 3 1.470 1.428 22.830 11.971 0.742 0.748 0.555 4 2 -7 1925.38 29.29 3 1.358 1.542 3.735 25.067 0.759 0.731 0.555 -4 2 7 1786.82 27.78 3 1.367 1.495 7.560 20.816 0.758 0.738 0.559 -4 -2 7 1802.99 27.61 3 1.707 1.577 37.439 27.619 0.707 0.726 0.514 4 -2 -6 6562.18 96.26 3 1.415 1.419 16.783 10.108 0.750 0.750 0.562 4 2 -6 6577.33 96.05 3 1.367 1.606 7.452 29.544 0.758 0.722 0.547 -4 2 6 6375.32 93.48 3 1.371 1.453 8.775 16.008 0.757 0.745 0.564 4 -2 -5 2426.22 36.56 3 1.377 1.424 10.343 11.096 0.756 0.749 0.566 -4 2 5 2479.89 37.30 3 1.381 1.420 11.139 10.389 0.756 0.750 0.566 4 -2 -1 697.92 11.28 3 1.444 1.709 20.268 35.157 0.746 0.707 0.527 -4 2 1 716.19 11.59 3 1.756 1.566 39.501 26.860 0.700 0.728 0.509 4 4 -10 110.10 3.46 3 1.570 1.779 30.328 38.249 0.727 0.697 0.507 -4 4 10 89.96 4.02 3 1.356 1.792 2.453 38.774 0.759 0.695 0.528 4 -4 -8 2996.29 29.04 3 1.653 1.426 34.959 11.480 0.715 0.749 0.535 4 4 -8 3012.08 26.57 3 1.362 1.628 5.826 30.911 0.758 0.719 0.545 -4 4 8 2793.20 27.40 3 1.355 1.664 0.513 32.909 0.760 0.713 0.542 4 -4 -7 298.04 6.91 3 1.576 1.410 30.693 7.765 0.726 0.751 0.545 -4 4 7 286.73 6.56 3 1.355 1.607 0.338 29.649 0.760 0.722 0.548 4 4 -7 308.63 5.92 3 1.367 1.693 7.489 34.403 0.758 0.709 0.537 4 -4 -4 3889.11 57.72 3 1.421 1.402 17.480 5.007 0.749 0.752 0.564 -4 4 4 3870.04 57.39 3 1.359 1.464 4.594 17.367 0.759 0.743 0.564 4 -4 -210494.30 152.31 3 1.369 1.435 8.169 13.299 0.757 0.747 0.566 -4 4 210122.97 146.92 3 1.399 1.418 14.443 9.913 0.753 0.750 0.564 4 -4 0 1175.89 18.06 3 1.355 1.512 1.504 22.490 0.759 0.736 0.559 -4 4 0 1128.08 17.44 3 1.643 1.552 34.445 25.793 0.716 0.730 0.523 4 -4 1 1183.24 18.08 3 1.363 1.572 6.276 27.279 0.758 0.727 0.551 4 -4 3 430.31 7.16 3 1.401 1.740 14.743 36.599 0.752 0.702 0.529 4 -4 4 9492.54 15.33 3 1.422 1.841 17.717 40.642 0.749 0.688 0.516 4 -4 5 1428.94 12.75 3 1.434 1.836 19.160 43.837 0.747 0.689 0.515 4 6 -9 411.85 6.97 3 1.395 1.769 13.762 37.849 0.753 0.698 0.526 -4 6 9 387.94 8.89 3 1.356 1.849 2.501 42.712 0.759 0.687 0.522 -4 6 8 1138.08 14.18 3 1.357 1.830 3.394 40.227 0.759 0.690 0.524 4 6 -8 1205.29 12.17 3 1.357 1.774 2.757 38.033 0.759 0.698 0.530 4 -6 -5 908.46 15.75 3 1.593 1.402 31.738 4.677 0.724 0.752 0.544 -4 6 5 838.12 14.91 3 1.357 1.639 2.863 31.509 0.759 0.717 0.544 4 -6 -418225.93 150.98 3 1.548 1.409 28.943 7.348 0.730 0.751 0.549 -4 6 417432.55 142.73 3 1.355 1.582 1.151 27.980 0.759 0.725 0.551 4 -6 -3 635.91 11.24 3 1.512 1.421 26.357 10.512 0.736 0.749 0.551 -4 6 3 617.28 10.87 3 1.356 1.531 1.702 24.163 0.759 0.733 0.557 4 -6 -2 1603.85 24.92 3 1.484 1.439 24.055 13.878 0.740 0.747 0.552 -4 6 2 1557.02 24.30 3 1.363 1.491 6.032 20.477 0.758 0.739 0.560 4 -6 -1 336.49 6.51 3 1.463 1.464 22.153 17.384 0.743 0.743 0.552 -4 6 1 349.02 6.61 3 1.387 1.473 12.353 18.429 0.755 0.742 0.560 4 -6 0 134.36 3.42 3 1.450 1.497 20.836 21.056 0.745 0.738 0.550 -4 6 0 137.14 3.38 3 1.455 1.498 21.381 21.163 0.744 0.738 0.549 4 -6 1 1367.07 20.84 3 1.446 1.542 20.425 25.010 0.746 0.731 0.545 -4 6 -1 1441.29 22.04 3 1.637 1.627 34.130 30.832 0.717 0.719 0.516 4 -6 2 1757.49 26.34 3 1.457 1.606 21.550 29.579 0.744 0.722 0.537 4 8 -9 131.32 2.89 3 1.378 1.842 10.446 43.329 0.756 0.688 0.520 -4 8 9 112.30 4.94 3 1.359 1.787 4.297 48.807 0.759 0.696 0.528 -4 8 8 1140.65 19.49 3 1.361 1.807 5.195 46.621 0.759 0.693 0.526 4 8 -8 1151.23 16.92 3 1.379 1.815 10.732 45.813 0.756 0.692 0.523 -4 8 6 158.76 4.87 3 1.362 1.860 5.677 41.837 0.758 0.686 0.520 4 -8 -3 221.76 4.89 3 1.703 1.460 37.295 16.861 0.708 0.744 0.526 -4 8 3 241.93 5.15 3 1.356 1.667 1.574 33.057 0.759 0.713 0.541 4 -8 -2 349.74 6.19 3 1.687 1.493 36.540 20.705 0.710 0.738 0.524 -4 8 2 341.59 6.21 3 1.356 1.610 1.869 29.831 0.759 0.721 0.548 4 -8 -1 1922.93 18.77 3 1.685 1.541 36.464 24.947 0.710 0.731 0.520 -4 8 1 2016.81 19.57 3 1.365 1.569 6.826 27.069 0.758 0.727 0.551 4 -8 0 374.87 5.73 3 1.705 1.610 37.353 29.789 0.707 0.721 0.510 -4 8 0 417.85 6.14 3 1.396 1.556 13.929 26.149 0.753 0.729 0.549 -4 8 -1 8.17 1.58 3 1.484 1.607 24.099 29.610 0.740 0.722 0.534 -4 8 -2 92.72 2.51 3 1.745 1.831 39.038 40.287 0.702 0.690 0.484 -4 10 2 5353.17 47.43 3 1.355 1.760 0.495 37.471 0.760 0.700 0.531 -4 10 0 436.53 6.58 3 1.378 1.671 10.528 33.290 0.756 0.712 0.538 -4 10 -1 87.34 3.11 3 1.432 1.687 18.931 34.089 0.748 0.710 0.531 -4 10 -2 3121.28 43.89 3 1.586 1.824 31.314 39.996 0.725 0.691 0.501 -4 12 -2 72.11 3.59 3 1.534 1.835 27.972 43.895 0.732 0.689 0.505 -5 1 12 48.08 3.55 3 1.444 1.689 20.243 34.176 0.746 0.710 0.529 -5 -1 12 48.03 3.24 3 1.585 1.707 31.262 35.094 0.725 0.707 0.513 -5 -1 11 8.55 2.39 3 1.568 1.630 30.240 31.036 0.727 0.718 0.522 5 -1 -9 11.54 2.12 3 1.475 1.485 23.306 19.817 0.741 0.740 0.548 5 1 -9 29.90 2.07 3 1.415 1.542 16.697 25.057 0.750 0.731 0.549 -5 1 9 13.05 2.45 3 1.426 1.505 18.098 21.851 0.749 0.737 0.552 -5 -1 9 11.22 1.69 3 1.571 1.527 30.376 23.841 0.727 0.733 0.533 5 -1 -8 349.58 7.89 3 1.416 1.471 16.914 18.268 0.750 0.742 0.556 5 1 -8 382.92 7.56 3 1.370 1.540 8.559 24.851 0.757 0.732 0.554 -5 1 8 350.09 10.03 3 1.431 1.464 18.704 17.382 0.748 0.743 0.556 -5 -1 8 370.62 7.44 3 1.593 1.499 31.713 21.224 0.724 0.738 0.534 5 -1 -7 906.21 15.26 3 1.377 1.474 10.225 18.655 0.756 0.741 0.561 -5 1 7 943.15 15.72 3 1.444 1.432 20.168 12.748 0.746 0.748 0.558 -5 -1 7 948.66 15.71 3 1.635 1.487 34.051 20.029 0.717 0.739 0.531 -5 1 6 3053.42 45.89 3 1.468 1.413 22.659 8.512 0.742 0.751 0.557 -5 -1 6 3087.59 46.28 3 1.708 1.496 37.524 20.996 0.707 0.738 0.522 5 -1 -5 13.95 1.52 3 1.359 1.549 4.169 25.623 0.759 0.730 0.554 5 1 -5 16.42 1.42 3 1.427 1.792 18.291 38.789 0.748 0.695 0.520 -5 1 5 17.06 1.49 3 1.512 1.409 26.373 7.425 0.736 0.751 0.553 -5 3 12 63.70 4.14 3 1.389 1.768 12.713 37.793 0.754 0.698 0.527 5 3 -11 2033.67 29.91 3 1.549 1.730 28.969 36.134 0.730 0.704 0.514 -5 3 11 2344.30 36.06 3 1.382 1.693 11.256 34.408 0.755 0.709 0.536 5 -3 -10 3057.41 46.03 3 1.645 1.470 34.524 18.177 0.716 0.742 0.531 5 3 -10 3121.96 15.33 3 1.438 1.653 19.615 32.306 0.747 0.715 0.534 -5 3 10 2993.85 44.60 3 1.377 1.628 10.239 30.923 0.756 0.719 0.543 5 -3 -9 1591.52 18.18 3 1.559 1.446 29.625 14.990 0.729 0.746 0.543 5 3 -9 1629.84 16.46 3 1.375 1.626 9.869 30.804 0.756 0.719 0.544 -5 3 9 1497.92 16.64 3 1.375 1.572 9.728 27.262 0.756 0.727 0.550 5 -3 -7 4405.34 65.92 3 1.438 1.425 19.535 11.448 0.747 0.749 0.559 -5 3 7 4119.87 61.79 3 1.378 1.478 10.570 19.027 0.756 0.741 0.560 5 3 -7 4467.00 66.01 3 1.380 1.753 10.815 37.162 0.756 0.701 0.529 5 -3 -4 3100.85 46.37 3 1.357 1.474 3.286 18.655 0.759 0.741 0.563 -5 3 4 3088.25 46.19 3 1.431 1.400 18.771 3.890 0.748 0.753 0.563 5 -3 -3 2798.28 41.88 3 1.356 1.521 2.460 23.267 0.759 0.734 0.558 -5 3 3 2778.99 41.63 3 1.486 1.408 24.242 7.151 0.740 0.751 0.556 5 -3 -2 532.04 9.25 3 1.369 1.588 8.296 28.404 0.757 0.724 0.549 -5 3 2 552.65 9.55 3 1.590 1.452 31.528 15.784 0.724 0.745 0.539 5 -3 0 2035.02 30.83 3 1.440 1.810 19.798 39.472 0.747 0.693 0.517 5 5 -11 19.82 2.11 3 1.525 1.862 27.340 41.692 0.734 0.685 0.503 -5 5 11 50.46 3.92 3 1.363 1.829 6.246 40.181 0.758 0.690 0.523 5 -5 -9 160.70 5.09 3 1.668 1.421 35.675 10.468 0.713 0.749 0.534 -5 5 9 167.68 4.99 3 1.359 1.691 4.379 34.304 0.759 0.709 0.538 5 -5 -8 320.25 7.38 3 1.594 1.409 31.787 7.467 0.724 0.751 0.544 5 5 -8 287.64 5.02 3 1.373 1.845 9.179 40.792 0.757 0.688 0.520 5 -5 -5 120.85 3.89 3 1.445 1.410 20.289 7.731 0.746 0.751 0.560 -5 5 5 115.73 3.78 3 1.366 1.488 7.404 20.164 0.758 0.739 0.560 5 -5 -3 2205.43 33.69 3 1.390 1.442 12.849 14.331 0.754 0.746 0.563 -5 5 3 1924.12 29.60 3 1.400 1.435 14.600 13.147 0.753 0.747 0.562 5 -5 -1 1292.50 20.29 3 1.362 1.503 5.902 21.629 0.758 0.737 0.559 -5 5 1 1328.32 20.75 3 1.540 1.479 28.407 19.142 0.731 0.741 0.542 5 -5 0 820.31 13.41 3 1.357 1.545 2.807 25.288 0.759 0.731 0.555 -5 5 0 877.52 14.31 3 1.737 1.597 38.733 28.991 0.703 0.723 0.508 5 -5 1 623.72 10.37 3 1.355 1.595 0.259 28.855 0.760 0.723 0.549 5 -5 2 14.36 1.41 3 1.356 1.652 1.895 32.243 0.759 0.715 0.543 5 -5 4 87.62 1.90 3 1.356 1.776 2.365 38.145 0.759 0.697 0.529 -5 7 11 18.37 3.27 3 1.357 1.812 3.237 46.051 0.759 0.692 0.526 5 7 -10 621.71 10.05 3 1.385 1.847 11.886 42.848 0.755 0.687 0.519 -5 7 10 593.15 12.52 3 1.356 1.839 2.073 43.574 0.759 0.688 0.523 -5 7 9 9.11 2.73 3 1.355 1.852 1.272 41.026 0.759 0.687 0.522 5 7 -9 7.64 1.59 3 1.357 1.838 3.253 43.659 0.759 0.689 0.523 5 -7 -6 1167.14 14.68 3 1.612 1.401 32.807 4.210 0.721 0.752 0.542 -5 7 6 1126.48 13.89 3 1.356 1.658 1.720 32.568 0.759 0.714 0.542 5 -7 -5 24.87 2.56 3 1.568 1.409 30.226 7.550 0.727 0.751 0.546 -5 7 5 18.43 2.16 3 1.357 1.603 3.130 29.398 0.759 0.722 0.548 5 -7 -3 4902.02 73.28 3 1.505 1.442 25.775 14.362 0.737 0.746 0.550 -5 7 3 4881.83 72.55 3 1.371 1.518 8.799 23.076 0.757 0.735 0.556 5 -7 -2 180.41 4.86 3 1.484 1.468 24.050 17.839 0.740 0.742 0.549 -5 7 2 185.01 4.69 3 1.394 1.497 13.562 21.031 0.754 0.738 0.556 5 -7 -1 1555.20 15.51 3 1.470 1.501 22.809 21.407 0.742 0.737 0.547 -5 7 1 1732.17 17.18 3 1.443 1.502 20.083 21.567 0.746 0.737 0.550 5 -7 0 1283.63 13.15 3 1.464 1.543 22.247 25.143 0.743 0.731 0.543 -5 7 0 1362.89 13.92 3 1.547 1.559 28.875 26.365 0.730 0.729 0.532 5 -7 1 1763.26 16.55 3 1.469 1.601 22.683 29.210 0.742 0.723 0.536 5 -7 2 389.98 5.14 3 1.492 1.685 24.723 34.003 0.739 0.710 0.525 -5 9 9 519.52 19.37 3 1.355 1.802 0.286 47.131 0.760 0.694 0.527 -5 9 6 1721.48 27.64 3 1.355 1.817 0.272 39.747 0.760 0.692 0.525 5 -9 -4 597.25 9.16 3 1.712 1.450 37.675 15.512 0.706 0.745 0.526 -5 9 4 648.93 10.07 3 1.357 1.690 3.037 34.258 0.759 0.710 0.539 5 -9 -3 7.38 2.09 3 1.691 1.480 36.735 19.269 0.709 0.741 0.525 5 -9 -2 49.98 2.83 3 1.682 1.520 36.318 23.249 0.711 0.734 0.522 -5 9 2 51.07 3.19 3 1.375 1.602 9.867 29.289 0.756 0.722 0.546 5 -9 -1 290.81 5.53 3 1.688 1.576 36.592 27.571 0.710 0.726 0.516 -5 9 1 293.13 5.43 3 1.405 1.586 15.360 28.267 0.752 0.725 0.545 -5 11 3 37.78 3.39 3 1.360 1.793 4.994 38.802 0.759 0.695 0.527 -5 11 2 16.10 2.31 3 1.370 1.743 8.519 36.718 0.757 0.702 0.532 -5 11 1 36.03 2.58 3 1.393 1.714 13.347 35.400 0.754 0.706 0.532 -5 11 0 329.90 7.15 3 1.441 1.721 19.909 35.719 0.746 0.705 0.526 -5 11 -1 84.45 3.31 3 1.548 1.800 28.943 39.080 0.730 0.694 0.507 6 0 -12 281.73 11.10 3 1.606 1.622 32.470 30.531 0.722 0.719 0.519 -6 0 12 296.17 11.41 3 1.550 1.631 29.078 31.098 0.730 0.718 0.524 6 0 -11 396.05 8.66 3 1.508 1.575 26.022 27.528 0.736 0.726 0.535 -6 0 11 406.74 8.55 3 1.541 1.567 28.431 26.971 0.731 0.727 0.532 6 0 -9 201.08 4.80 3 1.389 1.544 12.659 25.201 0.754 0.731 0.551 -6 0 9 196.62 5.07 3 1.550 1.478 29.072 19.112 0.730 0.741 0.541 6 0 -8 5654.40 49.61 3 1.362 1.561 5.684 26.531 0.758 0.728 0.552 -6 0 8 5239.78 45.82 3 1.573 1.452 30.511 15.861 0.727 0.745 0.541 6 0 -7 19.92 1.90 3 1.355 1.606 1.514 29.571 0.759 0.722 0.548 -6 0 7 19.05 2.33 3 1.612 1.440 32.823 14.009 0.721 0.747 0.538 6 0 -612710.78 104.77 3 1.371 1.686 8.863 34.042 0.757 0.710 0.538 -6 0 612249.26 101.22 3 1.677 1.444 36.110 14.690 0.711 0.746 0.531 6 2 -13 141.92 6.51 3 1.697 1.812 37.035 39.545 0.709 0.692 0.490 -6 2 13 146.35 6.83 3 1.457 1.728 21.550 36.042 0.744 0.704 0.524 6 -2 -12 436.33 15.99 3 1.678 1.553 36.144 25.902 0.711 0.730 0.519 6 2 -12 450.28 16.18 3 1.554 1.714 29.320 35.388 0.729 0.706 0.515 -6 2 12 438.28 16.18 3 1.444 1.650 20.191 32.162 0.746 0.715 0.534 6 -2 -11 699.04 13.48 3 1.577 1.516 30.795 22.856 0.726 0.735 0.534 6 2 -11 763.27 13.43 3 1.456 1.655 21.487 32.399 0.744 0.715 0.532 -6 2 11 737.24 13.41 3 1.436 1.585 19.308 28.203 0.747 0.725 0.542 6 -2 -9 690.21 10.33 3 1.441 1.480 19.882 19.293 0.746 0.740 0.553 6 2 -9 712.99 9.32 3 1.361 1.642 5.234 31.720 0.759 0.716 0.544 -6 2 9 744.85 10.61 3 1.434 1.484 19.163 19.756 0.747 0.740 0.553 6 -2 -7 193.31 5.21 3 1.370 1.497 8.513 21.029 0.757 0.738 0.559 6 2 -7 172.17 4.97 3 1.384 1.804 11.810 39.231 0.755 0.693 0.524 -6 2 7 178.15 4.89 3 1.459 1.419 21.727 10.087 0.744 0.750 0.558 6 -2 -3 34.23 1.88 3 1.406 1.768 15.475 37.805 0.752 0.698 0.525 -6 2 3 36.29 2.04 3 1.741 1.468 38.898 17.842 0.702 0.742 0.521 6 -4 -11 201.19 6.57 3 1.668 1.472 35.691 18.381 0.713 0.742 0.529 6 4 -11 210.83 5.14 3 1.420 1.760 17.401 37.463 0.750 0.700 0.524 -6 4 11 188.67 6.28 3 1.390 1.668 12.953 33.097 0.754 0.713 0.538 6 -4 -10 155.12 5.41 3 1.585 1.452 31.244 15.793 0.725 0.745 0.540 6 4 -10 157.20 4.62 3 1.367 1.744 7.679 36.771 0.758 0.702 0.532 -6 4 10 149.34 5.13 3 1.387 1.607 12.356 29.594 0.755 0.722 0.545 6 -4 -9 950.84 13.01 3 1.518 1.440 26.798 13.982 0.735 0.747 0.549 6 4 -9 979.94 11.72 3 1.356 1.792 2.151 38.761 0.759 0.695 0.528 -6 4 9 918.82 12.12 3 1.387 1.553 12.257 25.916 0.755 0.730 0.551 6 -4 -4 255.01 5.80 3 1.359 1.507 4.353 21.981 0.759 0.737 0.559 -6 4 4 258.35 5.82 3 1.469 1.408 22.682 7.033 0.742 0.751 0.558 6 -4 -3 1969.43 30.44 3 1.355 1.551 0.285 25.755 0.760 0.730 0.554 -6 4 3 1944.14 30.08 3 1.534 1.422 27.976 10.742 0.732 0.749 0.549 6 -4 -2 5926.91 87.22 3 1.359 1.609 4.450 29.756 0.759 0.721 0.547 -6 4 2 6233.83 91.58 3 1.649 1.470 34.758 18.120 0.715 0.742 0.531 6 -4 -1 2536.50 38.31 3 1.370 1.682 8.590 33.858 0.757 0.711 0.538 6 -4 011152.85 162.16 3 1.388 1.771 12.426 37.936 0.755 0.698 0.527 6 -4 2 1514.63 14.87 3 1.430 1.818 18.612 45.510 0.748 0.691 0.517 6 -4 3 1611.81 15.55 3 1.448 1.788 20.638 48.746 0.745 0.696 0.518 6 6 -11 208.82 7.98 3 1.397 1.849 14.135 42.700 0.753 0.687 0.517 -6 6 11 205.21 9.04 3 1.371 1.798 8.789 39.001 0.757 0.694 0.526 6 -6 -10 94.08 5.37 3 1.696 1.425 36.987 11.371 0.709 0.749 0.531 6 6 -10 98.75 3.28 3 1.356 1.849 2.391 42.710 0.759 0.687 0.522 -6 6 10 108.14 5.41 3 1.369 1.728 8.065 36.051 0.757 0.704 0.533 -6 6 9 539.48 11.01 3 1.368 1.666 7.778 32.997 0.758 0.713 0.540 6 -6 -5 14.15 2.75 3 1.441 1.434 19.914 13.034 0.746 0.747 0.558 -6 6 5 13.64 2.01 3 1.388 1.483 12.528 19.584 0.754 0.740 0.558 6 -6 -4 3997.32 60.05 3 1.416 1.453 16.842 15.926 0.750 0.745 0.559 -6 6 4 3719.59 56.00 3 1.408 1.459 15.793 16.716 0.751 0.744 0.559 6 -6 -3 1373.53 22.22 3 1.396 1.478 13.962 19.011 0.753 0.741 0.558 -6 6 3 1250.55 20.34 3 1.444 1.450 20.236 15.575 0.746 0.745 0.556 6 -6 -2 3106.63 46.92 3 1.382 1.509 11.334 22.184 0.755 0.736 0.556 6 -6 -1 44.34 2.50 3 1.372 1.546 9.047 25.374 0.757 0.731 0.553 -6 6 1 46.73 2.30 3 1.627 1.524 33.636 23.565 0.719 0.734 0.527 6 -6 0 2923.14 26.47 3 1.366 1.590 7.214 28.535 0.758 0.724 0.549 6 -6 1 394.57 5.87 3 1.362 1.641 6.011 31.632 0.758 0.717 0.544 6 -6 2 1780.07 16.68 3 1.362 1.699 5.701 34.668 0.758 0.708 0.537 6 8 -11 417.03 14.38 3 1.387 1.793 12.374 48.116 0.755 0.695 0.524 -6 8 11 545.44 20.05 3 1.363 1.824 6.328 44.891 0.758 0.691 0.524 6 8 -10 135.68 5.60 3 1.356 1.789 1.946 48.641 0.759 0.696 0.528 -6 8 10 133.83 6.84 3 1.361 1.854 5.562 42.323 0.759 0.686 0.521 6 -8 -5 887.42 12.48 3 1.562 1.432 29.827 12.608 0.728 0.748 0.545 -6 8 5 798.92 11.45 3 1.371 1.588 8.891 28.401 0.757 0.724 0.548 6 -8 -4 221.12 5.82 3 1.533 1.451 27.912 15.738 0.733 0.745 0.546 -6 8 4 214.09 5.20 3 1.383 1.551 11.630 25.758 0.755 0.730 0.551 6 -8 -3 13.54 2.23 3 1.512 1.477 26.328 18.988 0.736 0.741 0.545 -6 8 3 13.86 2.09 3 1.405 1.527 15.402 23.828 0.752 0.733 0.551 6 -8 -2 4175.69 37.53 3 1.497 1.510 25.166 22.349 0.738 0.736 0.543 -6 8 2 4252.50 38.48 3 1.446 1.523 20.447 23.481 0.746 0.734 0.547 6 -8 -1 1268.46 14.10 3 1.490 1.553 24.557 25.864 0.739 0.730 0.539 -6 8 1 1368.72 14.85 3 1.522 1.552 27.064 25.814 0.734 0.730 0.536 6 -8 0 334.69 5.69 3 1.491 1.607 24.699 29.624 0.739 0.722 0.533 -6 8 0 350.98 5.93 3 1.668 1.640 35.653 31.592 0.713 0.717 0.511 6 -8 1 200.27 4.70 3 1.507 1.682 25.923 33.837 0.737 0.711 0.523 -6 10 7 35.49 3.47 3 1.359 1.850 4.545 40.962 0.759 0.687 0.521 -6 10 6 2098.06 32.65 3 1.361 1.784 5.551 38.453 0.759 0.696 0.528 6 -10 -5 7.30 2.34 3 1.738 1.452 38.792 15.824 0.703 0.745 0.523 -6 10 5 13.88 2.61 3 1.366 1.726 7.194 35.957 0.758 0.704 0.534 6 -10 -4 1146.18 19.85 3 1.714 1.480 37.771 19.330 0.706 0.740 0.523 -6 10 4 1332.71 21.64 3 1.374 1.677 9.590 33.606 0.757 0.711 0.538 6 -10 -3 158.88 5.70 3 1.701 1.518 37.183 23.024 0.708 0.735 0.520 -6 10 3 174.56 5.58 3 1.390 1.641 12.904 31.668 0.754 0.717 0.540 6 -10 -2 192.01 5.76 3 1.700 1.568 37.146 26.973 0.708 0.727 0.515 -6 10 2 207.45 5.59 3 1.420 1.624 17.351 30.642 0.750 0.719 0.539 6 -10 -1 395.77 8.14 3 1.716 1.635 37.833 31.306 0.706 0.718 0.507 -6 10 1 465.56 9.16 3 1.474 1.635 23.225 31.312 0.741 0.718 0.532 -6 12 3 1037.68 35.42 3 1.386 1.792 12.212 38.793 0.755 0.695 0.525 -6 12 2 1088.71 36.98 3 1.412 1.765 16.268 37.673 0.751 0.699 0.525 -6 12 0 36.91 3.36 3 1.546 1.821 28.759 39.894 0.731 0.691 0.505 7 -1 -12 1396.17 12.83 3 1.535 1.585 28.030 28.182 0.732 0.725 0.531 7 1 -12 1381.72 13.59 3 1.480 1.663 23.731 32.873 0.740 0.713 0.528 -7 1 12 1317.02 44.51 3 1.538 1.584 28.246 28.093 0.732 0.725 0.531 -7 -1 12 1355.01 45.33 3 1.723 1.621 38.162 30.476 0.705 0.720 0.507 7 -1 -11 68.40 3.75 3 1.464 1.561 22.242 26.514 0.743 0.728 0.541 7 1 -11 69.67 4.09 3 1.416 1.640 16.856 31.577 0.750 0.717 0.538 -7 1 11 71.42 4.14 3 1.533 1.528 27.917 23.880 0.733 0.733 0.537 -7 -1 11 68.64 3.76 3 1.721 1.565 38.060 26.816 0.705 0.728 0.513 7 -1 -10 387.65 8.50 3 1.412 1.554 16.393 25.966 0.751 0.729 0.548 7 1 -10 403.93 8.68 3 1.375 1.643 9.893 31.732 0.756 0.716 0.542 -7 1 10 407.88 9.21 3 1.537 1.483 28.156 19.619 0.732 0.740 0.542 -7 -1 10 419.86 8.74 3 1.734 1.525 38.601 23.635 0.703 0.734 0.516 7 -1 -9 2269.44 23.27 3 1.378 1.563 10.471 26.678 0.756 0.728 0.550 7 1 -9 2266.35 22.95 3 1.357 1.674 2.847 33.421 0.759 0.712 0.541 -7 1 9 2266.61 23.37 3 1.550 1.449 29.023 15.371 0.730 0.745 0.544 7 -1 -8 84.64 3.46 3 1.359 1.592 4.473 28.641 0.759 0.724 0.549 7 1 -8 87.24 3.30 3 1.359 1.739 4.301 36.530 0.759 0.703 0.533 -7 1 8 89.51 3.49 3 1.574 1.425 30.588 11.432 0.726 0.749 0.544 7 -3 -13 19.68 3.45 3 1.707 1.559 37.479 26.343 0.707 0.729 0.515 7 3 -13 22.82 3.52 3 1.535 1.832 27.992 40.303 0.732 0.689 0.505 -7 3 13 30.50 4.21 3 1.460 1.693 21.910 34.393 0.743 0.709 0.527 7 -3 -12 158.92 7.65 3 1.608 1.526 32.596 23.713 0.721 0.734 0.529 7 3 -12 163.30 7.05 3 1.441 1.767 19.863 37.758 0.746 0.699 0.521 -7 3 12 155.48 7.42 3 1.451 1.623 20.925 30.573 0.745 0.719 0.536 7 -3 -11 1034.84 19.09 3 1.531 1.504 27.726 21.761 0.733 0.737 0.540 7 3 -11 1068.99 17.69 3 1.384 1.747 11.719 36.894 0.755 0.701 0.530 -7 3 11 1000.92 17.63 3 1.446 1.563 20.391 26.648 0.746 0.728 0.543 7 -3 -10 39.82 3.75 3 1.470 1.493 22.853 20.684 0.742 0.739 0.548 7 3 -10 38.91 2.68 3 1.358 1.770 3.537 37.892 0.759 0.698 0.530 -7 3 10 40.12 3.25 3 1.445 1.513 20.356 22.554 0.746 0.736 0.549 7 -3 -9 54.74 3.93 3 1.424 1.493 17.964 20.647 0.749 0.739 0.553 7 3 -9 34.48 2.42 3 1.360 1.842 4.676 40.693 0.759 0.688 0.522 -7 3 9 49.00 3.80 3 1.450 1.471 20.875 18.224 0.745 0.742 0.553 7 -3 -4 31.04 2.27 3 1.364 1.682 6.565 33.862 0.758 0.711 0.539 -7 3 4 27.11 2.12 3 1.650 1.420 34.812 10.233 0.715 0.750 0.536 7 -3 -3 2583.50 39.52 3 1.382 1.772 11.256 37.984 0.755 0.698 0.527 7 -5 -12 416.10 15.79 3 1.704 1.482 37.327 19.511 0.708 0.740 0.524 7 5 -12 468.87 16.50 3 1.415 1.848 16.702 42.812 0.750 0.687 0.516 -7 5 12 446.81 16.65 3 1.408 1.714 15.768 35.416 0.751 0.706 0.531 7 -5 -11 81.13 5.29 3 1.620 1.464 33.230 17.377 0.720 0.743 0.535 7 5 -11 81.56 4.18 3 1.365 1.853 7.063 42.382 0.758 0.686 0.520 -7 5 11 74.69 5.40 3 1.403 1.648 15.100 32.049 0.752 0.716 0.538 7 -5 -10 154.79 5.84 3 1.552 1.453 29.187 15.972 0.730 0.745 0.543 7 5 -10 147.14 4.64 3 1.356 1.831 2.416 44.287 0.759 0.690 0.524 -7 5 10 150.63 5.92 3 1.402 1.591 14.866 28.579 0.752 0.724 0.545 7 -5 -5 1530.41 16.91 3 1.375 1.508 9.808 22.156 0.756 0.736 0.557 -7 5 5 1525.89 16.68 3 1.468 1.422 22.647 10.851 0.742 0.749 0.556 7 -5 -4 188.37 4.52 3 1.363 1.543 6.207 25.122 0.758 0.731 0.554 -7 5 4 190.76 4.64 3 1.517 1.422 26.692 10.837 0.735 0.749 0.551 7 -5 -1 556.27 7.79 3 1.357 1.702 3.344 34.814 0.759 0.708 0.537 7 -5 1 531.15 7.64 3 1.368 1.852 7.801 41.025 0.758 0.687 0.520 7 -5 2 51.58 2.46 3 1.372 1.836 9.112 43.818 0.757 0.689 0.521 7 -7 -11 92.53 5.57 3 1.737 1.437 38.721 13.490 0.703 0.747 0.525 7 7 -11 150.60 6.41 3 1.357 1.795 3.246 47.907 0.759 0.695 0.527 -7 7 11 143.59 7.17 3 1.383 1.775 11.636 38.071 0.755 0.698 0.527 7 -7 -6 2999.83 29.31 3 1.474 1.449 23.171 15.429 0.741 0.745 0.552 -7 7 6 2936.60 29.10 3 1.402 1.516 14.954 22.851 0.752 0.735 0.553 7 -7 -5 151.30 4.57 3 1.447 1.468 20.502 17.868 0.746 0.742 0.553 -7 7 5 148.43 4.48 3 1.421 1.489 17.549 20.223 0.749 0.739 0.554 7 -7 -3 5976.26 52.23 3 1.409 1.522 15.871 23.372 0.751 0.734 0.552 -7 7 3 5942.52 51.96 3 1.503 1.477 25.630 18.996 0.737 0.741 0.546 7 -7 -2 629.61 9.17 3 1.397 1.558 14.031 26.270 0.753 0.729 0.549 -7 7 2 721.46 9.76 3 1.588 1.508 31.456 22.105 0.724 0.736 0.533 7 -7 -1 162.82 4.16 3 1.389 1.601 12.627 29.208 0.754 0.723 0.545 -7 7 1 162.97 4.92 3 1.737 1.582 38.745 28.005 0.703 0.725 0.510 7 -7 0 1689.26 17.25 3 1.384 1.651 11.795 32.177 0.755 0.715 0.540 7 -7 1 851.26 13.73 3 1.384 1.710 11.725 35.201 0.755 0.707 0.534 7 -7 2 5.77 1.50 3 1.389 1.782 12.745 38.386 0.754 0.696 0.525 7 -9 -7 37.35 3.77 3 1.637 1.431 34.124 12.503 0.717 0.748 0.536 -7 9 7 33.42 3.45 3 1.379 1.675 10.684 33.467 0.756 0.712 0.538 7 -9 -5 920.94 16.06 3 1.570 1.466 30.310 17.686 0.727 0.743 0.540 -7 9 5 868.54 15.49 3 1.400 1.590 14.518 28.521 0.753 0.724 0.545 7 -9 -4 11.13 3.44 3 1.547 1.493 28.837 20.625 0.731 0.739 0.540 -7 9 4 8.98 2.29 3 1.422 1.564 17.609 26.718 0.749 0.728 0.545 7 -9 -3 48.39 3.14 3 1.531 1.526 27.742 23.730 0.733 0.734 0.538 -7 9 3 44.67 3.02 3 1.458 1.554 21.682 25.991 0.744 0.729 0.543 7 -9 -2 65.22 4.10 3 1.522 1.568 27.119 27.008 0.734 0.727 0.534 -7 9 2 77.14 3.89 3 1.520 1.569 26.936 27.048 0.735 0.727 0.534 7 -9 -1 564.89 10.53 3 1.522 1.622 27.108 30.514 0.734 0.720 0.528 -7 9 1 597.99 10.81 3 1.627 1.622 33.628 30.539 0.719 0.719 0.517 7 -9 0 998.65 16.31 3 1.534 1.692 27.921 34.368 0.732 0.709 0.520 7 -11 -4 79.13 4.72 3 1.736 1.527 38.675 23.805 0.703 0.733 0.516 -7 11 4 125.30 6.63 3 1.409 1.689 15.970 34.191 0.751 0.710 0.533 7 -11 -3 27.40 2.87 3 1.731 1.574 38.463 27.411 0.704 0.727 0.511 -7 11 3 37.38 3.34 3 1.439 1.669 19.683 33.190 0.747 0.713 0.532 7 -11 -2 24.61 3.04 3 1.740 1.636 38.837 31.336 0.702 0.717 0.504 -7 11 2 31.07 2.86 3 1.489 1.674 24.498 33.408 0.739 0.712 0.526 8 0 -11 753.66 14.23 3 1.397 1.651 14.075 32.225 0.753 0.715 0.539 -8 0 11 749.27 13.73 3 1.690 1.509 36.704 22.218 0.710 0.736 0.522 8 0 -10 1060.00 17.89 3 1.368 1.670 7.990 33.201 0.757 0.713 0.540 8 0 -9 322.27 7.85 3 1.356 1.711 1.906 35.274 0.759 0.707 0.537 -8 0 9 313.60 6.54 3 1.738 1.451 38.777 15.712 0.703 0.745 0.523 8 0 -8 4497.62 41.32 3 1.359 1.780 4.183 38.301 0.759 0.697 0.529 8 -2 -13 15.47 3.46 3 1.570 1.601 30.325 29.247 0.727 0.723 0.525 8 2 -13 19.28 2.92 3 1.467 1.781 22.515 38.328 0.742 0.697 0.517 -8 2 13 17.57 3.95 3 1.548 1.613 28.895 29.983 0.730 0.721 0.526 8 -2 -12 168.76 8.39 3 1.497 1.578 25.120 27.719 0.738 0.726 0.536 8 2 -12 170.25 7.48 3 1.406 1.757 15.452 37.342 0.752 0.700 0.526 -8 2 12 159.07 7.26 3 1.540 1.552 28.355 25.816 0.732 0.730 0.534 8 -2 -11 97.32 5.18 3 1.441 1.569 19.932 27.076 0.746 0.727 0.543 8 2 -11 100.12 4.14 3 1.370 1.766 8.407 37.730 0.757 0.699 0.529 -8 2 11 97.76 4.41 3 1.539 1.502 28.303 21.543 0.732 0.737 0.539 8 -2 -10 1251.65 20.97 3 1.401 1.573 14.747 27.396 0.752 0.727 0.547 8 2 -10 1131.10 18.69 3 1.355 1.810 1.391 39.480 0.759 0.693 0.526 -8 2 10 1243.04 20.48 3 1.546 1.462 28.781 17.123 0.731 0.743 0.543 8 -2 -5 14.12 1.98 3 1.379 1.849 10.760 40.920 0.756 0.687 0.519 8 -4 -13 19.38 3.98 3 1.649 1.543 34.719 25.094 0.716 0.731 0.523 8 4 -13 28.41 2.92 3 1.437 1.844 19.442 43.168 0.747 0.688 0.514 -8 4 13 19.05 4.46 3 1.471 1.668 22.907 33.125 0.742 0.713 0.529 8 -4 -11 134.17 5.94 3 1.506 1.511 25.848 22.394 0.737 0.736 0.542 8 4 -11 137.57 4.60 3 1.357 1.840 3.130 43.462 0.759 0.688 0.523 -8 4 11 126.29 5.60 3 1.462 1.548 22.024 25.525 0.743 0.730 0.543 8 -4 -5 829.17 11.06 3 1.355 1.648 0.539 32.061 0.760 0.716 0.544 -8 4 5 859.90 11.53 3 1.613 1.408 32.868 7.071 0.721 0.751 0.542 8 -4 -4 7979.02 28.01 3 1.357 1.711 3.350 35.284 0.759 0.707 0.536 -8 4 4 8011.14 69.15 3 1.705 1.431 37.388 12.436 0.707 0.748 0.529 8 -4 -2 694.23 9.55 3 1.377 1.857 10.367 42.042 0.756 0.686 0.519 8 -4 -1 50.59 2.59 3 1.393 1.819 13.382 45.387 0.754 0.691 0.521 8 -4 0 98.17 3.70 3 1.409 1.789 15.964 48.594 0.751 0.695 0.522 8 -6 -12 572.47 17.88 3 1.664 1.482 35.487 19.486 0.713 0.740 0.528 8 6 -12 584.65 17.02 3 1.367 1.797 7.718 47.664 0.758 0.694 0.526 -8 6 12 544.18 17.21 3 1.424 1.698 17.943 34.624 0.749 0.708 0.531 8 -6 -6 809.43 11.57 3 1.400 1.520 14.532 23.164 0.753 0.735 0.553 -8 6 6 794.70 11.42 3 1.478 1.447 23.499 15.050 0.741 0.746 0.552 8 -6 -5 307.24 6.31 3 1.383 1.549 11.479 25.598 0.755 0.730 0.551 -8 6 5 323.10 6.71 3 1.517 1.438 26.703 13.712 0.735 0.747 0.549 8 -6 -2 190.22 5.05 3 1.358 1.681 3.721 33.779 0.759 0.711 0.540 8 -6 -1 63.64 3.24 3 1.356 1.739 1.823 36.555 0.759 0.703 0.534 8 -6 0 706.75 12.15 3 1.355 1.804 0.444 39.263 0.760 0.693 0.527 8 -6 1 484.07 9.02 3 1.355 1.860 0.523 41.866 0.760 0.686 0.521 8 -6 2 1796.34 26.70 3 1.355 1.830 0.523 44.341 0.760 0.690 0.524 8 -8 -6 30.06 4.29 3 1.483 1.487 23.992 20.066 0.740 0.739 0.547 -8 8 6 26.40 2.94 3 1.439 1.525 19.662 23.651 0.747 0.734 0.548 8 -8 -5 62.49 4.31 3 1.460 1.511 21.833 22.414 0.744 0.736 0.547 -8 8 5 63.57 3.58 3 1.467 1.506 22.514 21.936 0.742 0.737 0.547 -8 8 4 2281.29 34.57 3 1.510 1.501 26.217 21.492 0.736 0.737 0.543 8 -8 -3 124.55 4.44 3 1.428 1.577 18.381 27.610 0.748 0.726 0.543 -8 8 3 132.27 4.94 3 1.579 1.517 30.901 22.941 0.726 0.735 0.533 8 -8 -2 436.12 8.86 3 1.419 1.619 17.225 30.370 0.750 0.720 0.540 -8 8 2 439.07 8.97 3 1.690 1.563 36.722 26.630 0.710 0.728 0.517 8 -8 -1 21.99 2.28 3 1.414 1.670 16.579 33.224 0.751 0.712 0.535 8 -8 0 797.85 13.47 3 1.414 1.731 16.594 36.201 0.750 0.704 0.528 8 -10 -7 50.06 4.71 3 1.646 1.466 34.571 17.644 0.716 0.743 0.532 -8 10 7 51.24 4.39 3 1.407 1.676 15.568 33.511 0.752 0.712 0.535 8 -10 -5 112.91 6.05 3 1.589 1.514 31.513 22.628 0.724 0.735 0.533 -8 10 5 119.62 6.44 3 1.443 1.608 20.063 29.679 0.746 0.722 0.538 8 -10 -4 1284.34 43.67 3 1.572 1.547 30.473 25.463 0.727 0.730 0.531 -8 10 4 1244.09 42.05 3 1.477 1.594 23.450 28.786 0.741 0.724 0.536 8 -10 -3 110.79 5.98 3 1.562 1.590 29.850 28.501 0.728 0.724 0.527 -8 10 3 113.77 6.18 3 1.531 1.600 27.774 29.153 0.733 0.723 0.530 8 -10 -1 217.88 8.68 3 1.570 1.713 30.322 35.350 0.727 0.706 0.514 -8 12 4 426.73 13.60 3 1.464 1.724 22.254 35.885 0.743 0.705 0.523 -8 12 2 446.06 13.79 3 1.589 1.754 31.478 37.197 0.724 0.700 0.507 9 -1 -13 157.19 7.30 3 1.476 1.675 23.395 33.500 0.741 0.712 0.527 9 1 -13 150.11 7.50 3 1.433 1.775 19.020 38.078 0.748 0.697 0.521 -9 1 13 150.60 6.60 3 1.679 1.568 36.178 26.989 0.711 0.727 0.517 9 -1 -12 880.23 30.51 3 1.425 1.668 17.973 33.094 0.749 0.713 0.534 9 1 -12 915.39 31.58 3 1.390 1.774 12.801 38.057 0.754 0.698 0.526 -9 1 12 794.95 27.80 3 1.676 1.515 36.037 22.769 0.712 0.735 0.523 9 1 -11 8.46 2.47 3 1.364 1.800 6.639 39.102 0.758 0.694 0.526 9 -1 -9 9.19 2.87 3 1.356 1.752 1.981 37.115 0.759 0.701 0.532 9 -3 -13 384.84 13.52 3 1.536 1.601 28.069 29.215 0.732 0.723 0.529 9 3 -13 396.70 13.04 3 1.403 1.847 15.088 42.864 0.752 0.687 0.517 -9 3 13 366.90 12.41 3 1.556 1.586 29.427 28.288 0.729 0.725 0.528 9 -3 -12 551.59 20.55 3 1.476 1.590 23.368 28.493 0.741 0.724 0.537 9 3 -12 460.26 17.00 3 1.368 1.842 8.002 43.265 0.757 0.688 0.521 -9 3 12 537.46 19.76 3 1.552 1.531 29.162 24.167 0.730 0.733 0.535 9 -3 -11 31.38 3.55 3 1.431 1.590 18.724 28.543 0.748 0.724 0.542 -9 3 11 35.73 3.46 3 1.555 1.486 29.357 19.914 0.729 0.740 0.539 -9 5 9 9.05 2.77 3 1.503 1.463 25.618 17.249 0.737 0.743 0.548 9 -5 -5 356.58 7.12 3 1.357 1.689 3.199 34.203 0.759 0.710 0.539 -9 5 5 403.06 8.04 3 1.673 1.424 35.907 11.078 0.712 0.749 0.533 9 -5 -4 118.91 4.31 3 1.355 1.748 0.211 36.958 0.760 0.701 0.533 9 -5 -2 2852.41 27.95 3 1.360 1.850 5.154 42.607 0.759 0.687 0.521 9 -5 -1 402.03 8.70 3 1.366 1.819 7.250 45.368 0.758 0.691 0.524 9 -5 0 201.29 5.87 3 1.371 1.794 8.891 48.009 0.757 0.695 0.526 9 -5 1 216.80 5.65 3 1.376 1.775 9.985 50.480 0.756 0.698 0.528 -9 7 11 12.57 3.32 3 1.446 1.630 20.396 30.987 0.746 0.718 0.536 9 -7 -6 48.31 4.42 3 1.411 1.564 16.153 26.752 0.751 0.728 0.547 -9 7 6 44.05 3.36 3 1.528 1.464 27.526 17.378 0.733 0.743 0.545 9 -7 -5 109.98 4.52 3 1.395 1.597 13.695 29.014 0.753 0.723 0.545 -9 7 5 115.88 5.09 3 1.579 1.462 30.862 17.163 0.726 0.743 0.539 9 -7 -3 29.32 2.81 3 1.374 1.683 9.584 33.908 0.757 0.711 0.538 9 -7 -2 2034.52 30.99 3 1.368 1.736 8.047 36.434 0.757 0.703 0.532 9 -7 -1 1106.24 18.30 3 1.365 1.797 6.955 38.967 0.758 0.694 0.526 9 -7 0 214.48 5.59 3 1.364 1.864 6.416 41.489 0.758 0.685 0.519 9 -9 -9 21.37 5.44 3 1.597 1.480 31.956 19.306 0.723 0.740 0.535 -9 9 9 19.54 3.61 3 1.434 1.644 19.069 31.809 0.747 0.716 0.535 9 -9 -5 907.02 31.71 3 1.481 1.565 23.761 26.814 0.740 0.728 0.539 -9 9 5 900.76 30.93 3 1.527 1.535 27.474 24.499 0.733 0.732 0.537 9 -9 -4 92.86 4.45 3 1.465 1.601 22.387 29.265 0.743 0.722 0.537 -9 9 4 97.98 4.57 3 1.587 1.541 31.351 25.006 0.725 0.731 0.530 9 -9 -2 191.10 8.17 3 1.450 1.697 20.847 34.590 0.745 0.709 0.528 9 -9 -1 44.17 3.66 3 1.450 1.761 20.888 37.490 0.745 0.699 0.521 9 -11 -6 77.50 5.55 3 1.641 1.540 34.329 24.920 0.717 0.731 0.524 -9 11 6 75.20 5.07 3 1.469 1.660 22.711 32.715 0.742 0.714 0.530 9 -11 -5 311.27 10.86 3 1.622 1.575 33.333 27.493 0.719 0.726 0.523 -9 11 5 322.44 11.11 3 1.502 1.643 25.586 31.749 0.737 0.716 0.528 9 -11 -4 53.11 4.21 3 1.610 1.618 32.715 30.296 0.721 0.720 0.519 -9 11 4 60.91 4.43 3 1.553 1.642 29.238 31.729 0.730 0.716 0.523 9 -11 -2 625.80 18.60 3 1.615 1.742 32.978 36.688 0.720 0.702 0.506 -9 11 2 732.14 24.57 3 1.755 1.726 39.441 35.977 0.700 0.704 0.493 10 0 -13 116.53 6.89 3 1.416 1.792 16.901 38.772 0.750 0.695 0.521 10 0 -12 77.31 5.21 3 1.382 1.806 11.387 39.319 0.755 0.693 0.524 -10 2 11 53.17 5.36 3 1.694 1.452 36.868 15.870 0.709 0.745 0.528 10 -6 -9 31.54 4.84 3 1.424 1.589 17.944 28.466 0.749 0.724 0.542 10 -6 -6 19.90 3.57 3 1.371 1.689 8.861 34.182 0.757 0.710 0.537 -10 6 6 21.00 2.91 3 1.666 1.434 35.556 13.004 0.713 0.747 0.533 10 -6 -5 325.02 8.10 3 1.363 1.738 6.225 36.508 0.758 0.703 0.533 -10 6 5 337.13 8.36 3 1.749 1.448 39.232 15.222 0.701 0.745 0.523 10 -6 -4 99.27 4.97 3 1.358 1.796 3.843 38.930 0.759 0.695 0.527 10 -6 -3 80.71 4.56 3 1.356 1.862 1.775 41.395 0.759 0.685 0.520 10 -6 -2 1772.93 27.70 3 1.355 1.836 0.114 43.853 0.760 0.689 0.523 10 -6 -1 32.12 2.74 3 1.355 1.810 1.309 46.263 0.759 0.693 0.526 10 -6 0 972.76 32.95 3 1.356 1.789 2.101 48.592 0.759 0.695 0.528 10 -8 -6 43.22 3.88 3 1.427 1.619 18.289 30.344 0.748 0.720 0.539 -10 8 6 40.24 3.90 3 1.592 1.490 31.677 20.364 0.724 0.739 0.535 10 -8 -4 68.74 4.65 3 1.401 1.700 14.725 34.752 0.752 0.708 0.533 -10 8 4 80.46 4.91 3 1.753 1.521 39.373 23.286 0.701 0.734 0.514 10 -8 -3 105.60 5.56 3 1.393 1.752 13.438 37.099 0.754 0.701 0.528 10 -8 -1 12.67 3.06 3 1.386 1.858 12.203 41.984 0.755 0.686 0.518 10 -8 0 313.15 11.69 3 1.388 1.828 12.481 44.538 0.754 0.690 0.521 -10 10 7 467.38 15.25 3 1.515 1.593 26.599 28.742 0.735 0.724 0.532 10 -10 -6 28.17 3.85 3 1.527 1.596 27.449 28.923 0.733 0.723 0.530 -10 10 6 29.11 3.97 3 1.552 1.578 29.201 27.738 0.730 0.726 0.530 10 -10 -5 449.40 14.30 3 1.510 1.633 26.205 31.180 0.736 0.718 0.528 -10 10 5 462.39 14.87 3 1.606 1.578 32.479 27.715 0.722 0.726 0.524 10 -10 -4 1690.63 48.75 3 1.499 1.677 25.310 33.612 0.738 0.711 0.525 -10 10 4 1797.62 17.33 3 1.686 1.597 36.526 28.981 0.710 0.723 0.514 10 -10 -3 36.63 4.33 3 1.493 1.732 24.839 36.218 0.739 0.704 0.520 -11 5 10 37.62 5.25 3 1.634 1.448 33.993 15.182 0.718 0.745 0.535 11 -7 -5 138.01 6.86 3 1.374 1.798 9.559 39.026 0.757 0.694 0.525 11 -7 -3 246.43 10.07 3 1.363 1.840 6.315 43.476 0.758 0.688 0.522 11 -7 -2 101.12 5.47 3 1.361 1.815 5.250 45.732 0.759 0.692 0.525 11 -7 -1 9.34 2.38 3 1.359 1.794 4.648 47.980 0.759 0.695 0.527 11 -9 -6 21.09 3.67 3 1.450 1.685 20.865 34.003 0.745 0.710 0.529 -11 9 6 44.54 5.71 3 1.674 1.527 35.967 23.828 0.712 0.733 0.522 11 -9 -5 259.80 9.81 3 1.437 1.729 19.424 36.083 0.747 0.704 0.526 -11 9 5 242.27 9.19 3 1.758 1.542 39.562 25.060 0.700 0.731 0.512 11 -9 -4 266.50 9.59 3 1.427 1.780 18.311 38.287 0.748 0.697 0.522 12 -6 -4 22.81 3.10 3 1.356 1.793 1.720 48.123 0.759 0.695 0.528 12 -6 -3 30.41 3.29 3 1.355 1.776 0.287 50.323 0.760 0.697 0.530 ; _shelx_hkl_checksum 39925 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl Cl 0.40651(15) 0.000000 0.30805(14) 0.0279(5) Uiso 1 2 d S . P . . Na1 Na 0.000000 0.000000 0.000000 0.0262(7) Uiso 1 4 d S . P . . Na2 Na 0.000000 0.000000 0.500000 0.0256(7) Uiso 1 4 d S . P . . O2 O 0.8523(3) 0.1397(2) 0.0056(3) 0.0321(7) Uiso 1 1 d . . . . . O1 O 0.1066(5) 0.000000 0.2434(5) 0.0328(9) Uiso 1 2 d S . P . . O4 O 0.9949(3) 0.1494(2) 0.3497(3) 0.0314(7) Uiso 1 1 d . . . . . O6 O 0.7407(3) 0.2464(2) 0.2477(3) 0.0338(8) Uiso 1 1 d . . . . . O3 O 0.2379(5) 0.000000 0.6261(5) 0.0310(9) Uiso 1 2 d S . P . . O8 O 0.3064(5) 0.000000 0.9121(5) 0.0339(9) Uiso 1 2 d S . P . . O5 O 0.3445(3) 0.1626(2) 0.5159(3) 0.0309(7) Uiso 1 1 d . . . . . O7 O 0.4808(3) 0.1576(2) 0.1272(3) 0.0356(8) Uiso 1 1 d . . . . . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Na1 O1 180.00(12) . 5 ? O1 Na1 O2 87.13(10) . 6_455 ? O1 Na1 O2 92.87(10) 5 6_455 ? O1 Na1 O2 92.87(10) . 2_655 ? O1 Na1 O2 87.13(10) 5 2_655 ? O2 Na1 O2 180.00(16) 6_455 2_655 ? O1 Na1 O2 87.13(10) . 1_455 ? O1 Na1 O2 92.87(10) 5 1_455 ? O2 Na1 O2 88.13(13) 6_455 1_455 ? O2 Na1 O2 91.87(13) 2_655 1_455 ? O1 Na1 O2 92.87(10) . 5_655 ? O1 Na1 O2 87.13(10) 5 5_655 ? O2 Na1 O2 91.87(13) 6_455 5_655 ? O2 Na1 O2 88.13(13) 2_655 5_655 ? O2 Na1 O2 180.00(12) 1_455 5_655 ? O3 Na2 O3 180.0 5_556 . ? O3 Na2 O4 88.13(10) 5_556 6_455 ? O3 Na2 O4 91.87(10) . 6_455 ? O3 Na2 O4 91.87(10) 5_556 2_656 ? O3 Na2 O4 88.13(10) . 2_656 ? O4 Na2 O4 180.0 6_455 2_656 ? O3 Na2 O4 88.13(10) 5_556 1_455 ? O3 Na2 O4 91.87(10) . 1_455 ? O4 Na2 O4 95.53(13) 6_455 1_455 ? O4 Na2 O4 84.47(13) 2_656 1_455 ? O3 Na2 O4 91.87(10) 5_556 5_656 ? O3 Na2 O4 88.13(10) . 5_656 ? O4 Na2 O4 84.47(13) 6_455 5_656 ? O4 Na2 O4 95.53(13) 2_656 5_656 ? O4 Na2 O4 180.0 1_455 5_656 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Na1 O1 2.313(4) . ? Na1 O1 2.313(4) 5 ? Na1 O2 2.386(3) 6_455 ? Na1 O2 2.386(3) 2_655 ? Na1 O2 2.386(3) 1_455 ? Na1 O2 2.386(3) 5_655 ? Na2 O3 2.362(5) 5_556 ? Na2 O3 2.362(5) . ? Na2 O4 2.398(3) 6_455 ? Na2 O4 2.398(3) 2_656 ? Na2 O4 2.398(3) 1_455 ? Na2 O4 2.398(3) 5_656 ? _cod_database_fobs_code 2312284