#------------------------------------------------------------------------------ #$Date: 2023-11-07 04:58:10 +0200 (Tue, 07 Nov 2023) $ #$Revision: 287456 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/23/2312334.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312334 _cell_angle_alpha 90.000 _cell_angle_beta 99.554 _cell_angle_gamma 90.000 _cell_length_a 8.3209 _cell_length_b 27.3213 _cell_length_c 15.7839 _exptl_crystal_F_000 1936.00 _reflns_d_resolution_high 0.7500 _cod_data_source_file dg30462bsup3.hkl _cod_data_source_block 2b _shelx_title ' 007c-22024' _shelx_refln_list_code 4 _shelx_f_calc_maximum 394.75 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 75512.36 83423.75 1999.55 o 4 0 0 4040.86 3666.94 152.09 o 6 0 0 1177.30 1605.67 146.58 o 8 0 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741.02 95.13 o 4 4 0 11.62 -152.10 152.10 o 5 4 0 38.25 245.62 140.31 o 6 4 0 3691.00 4223.21 161.35 o 7 4 0 213.86 94.30 167.40 o 8 4 0 11496.23 11392.42 278.51 o 9 4 0 640.69 637.15 266.20 o 10 4 0 9728.53 11551.32 1055.05 o 1 5 0 15241.36 13635.28 449.69 o 2 5 0 17840.90 16999.99 1051.19 o 3 5 0 3289.96 2650.91 162.05 o 4 5 0 770.54 583.90 118.94 o 5 5 0 713.85 792.13 147.58 o 6 5 0 7138.97 7407.34 208.60 o 7 5 0 4631.57 3872.87 196.68 o 8 5 0 1434.44 1381.30 229.67 o 9 5 0 2.61 246.58 260.82 o 10 5 0 1224.00 2105.85 728.57 o 0 6 0 12383.18 12480.40 451.31 o 1 6 0 1407.24 751.43 160.40 o 2 6 0 675.46 981.24 234.78 o 3 6 0 1908.44 2001.70 136.73 o 4 6 0 1738.73 1867.96 131.14 o 5 6 0 97.74 117.65 134.50 o 6 6 0 3781.67 4360.42 285.45 o 7 6 0 1710.49 1766.74 188.21 o 8 6 0 15.79 -40.12 173.87 o 9 6 0 11981.60 11413.81 278.36 o 10 6 0 3122.01 4136.89 422.05 o 1 7 0 7828.43 8310.64 175.53 o 2 7 0 7227.45 5854.41 463.90 o 3 7 0 17593.66 16859.98 436.74 o 4 7 0 13638.01 14451.46 269.23 o 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