#------------------------------------------------------------------------------ #$Date: 2025-03-26 05:11:03 +0200 (Wed, 26 Mar 2025) $ #$Revision: 298597 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/28/2312801.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312801 _cell_angle_alpha 90.000 _cell_angle_beta 104.148 _cell_angle_gamma 90.000 _cell_length_a 10.8040 _cell_length_b 13.3892 _cell_length_c 18.8504 _exptl_crystal_F_000 1184.00 _reflns_d_resolution_high 0.7081 _cod_data_source_file aw50984CN2Tsup11.hkl _cod_data_source_block 4CN2T _shelx_title ' MONO1_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 338.06 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1698.21 1319.90 217.67 o 4 0 0 5244.37 4529.46 522.71 o 6 0 0 228.23 226.63 29.10 o 8 0 0 1353.33 1522.67 150.04 o 10 0 0 46.98 52.98 31.05 o 12 0 0 144.88 53.79 55.04 o 14 0 0 38.85 17.10 46.71 o 1 1 0 6390.81 6037.64 978.66 o 2 1 0 2649.86 2133.53 350.24 o 3 1 0 1001.61 838.61 70.16 o 4 1 0 831.35 694.90 58.80 o 5 1 0 26.39 28.68 12.28 o 6 1 0 1046.34 899.97 58.31 o 7 1 0 17.39 13.13 8.02 o 8 1 0 19.43 6.92 10.45 o 9 1 0 171.97 123.82 24.21 o 10 1 0 12.53 5.09 17.66 o 11 1 0 4.05 15.49 21.25 o 12 1 0 94.96 45.77 25.51 o 13 1 0 63.48 31.07 30.61 o 14 1 0 43.46 13.47 28.61 o 2 2 0 485.47 399.61 51.67 o 3 2 0 1284.25 1000.30 96.49 o 4 2 0 9971.35 9181.28 666.55 o 5 2 0 3818.21 3602.60 240.88 o 6 2 0 260.13 235.66 18.35 o 7 2 0 176.37 174.67 17.81 o 8 2 0 38.88 35.75 12.47 o 9 2 0 3.52 11.25 14.06 o 10 2 0 4.71 4.53 18.08 o 11 2 0 119.10 139.09 36.31 o 12 2 0 18.56 47.63 25.34 o 13 2 0 0.01 11.20 24.92 o 14 2 0 13.01 64.64 32.53 o 2 3 0 55.80 40.85 18.65 o 3 3 0 10925.56 10635.31 863.49 o 4 3 0 1007.01 944.72 80.07 o 5 3 0 1930.88 1845.48 115.02 o 6 3 0 17.93 24.29 7.94 o 7 3 0 135.91 168.82 20.98 o 8 3 0 198.08 229.41 21.98 o 9 3 0 137.83 156.02 24.41 o 10 3 0 32.08 29.32 17.11 o 11 3 0 486.42 610.84 60.05 o 12 3 0 0.59 21.60 20.83 o 13 3 0 0.97 42.01 28.63 o 14 3 0 4.82 19.54 37.14 o 0 4 0 3968.87 3642.96 594.29 o 1 4 0 345.83 356.14 34.75 o 2 4 0 26.54 13.69 7.58 o 3 4 0 1210.81 1015.99 98.72 o 4 4 0 7469.83 7029.34 571.45 o 5 4 0 1132.54 944.92 71.89 o 6 4 0 245.79 228.85 28.75 o 7 4 0 120.79 106.02 15.62 o 8 4 0 124.30 72.62 23.51 o 9 4 0 38.25 47.54 16.11 o 10 4 0 87.94 97.43 17.92 o 11 4 0 97.49 92.84 29.94 o 12 4 0 3.08 34.75 46.57 o 13 4 0 17.86 76.56 59.88 o 14 4 0 14.91 27.69 45.60 o 1 5 0 1776.04 1562.51 149.53 o 2 5 0 3.64 -6.86 6.86 o 3 5 0 693.99 699.22 70.29 o 4 5 0 255.75 228.79 24.11 o 5 5 0 513.86 538.89 46.67 o 6 5 0 2.82 2.21 9.20 o 7 5 0 315.30 366.70 34.10 o 8 5 0 0.78 11.21 12.39 o 9 5 0 0.05 0.95 13.30 o 10 5 0 371.19 394.49 40.63 o 11 5 0 255.81 233.24 48.70 o 12 5 0 9.69 7.10 47.90 o 13 5 0 10.90 -43.47 52.34 o 14 5 0 5.09 112.53 53.93 o 0 6 0 3489.60 3587.84 415.43 o 1 6 0 2577.41 2650.32 194.84 o 2 6 0 107.83 132.29 18.84 o 3 6 0 510.09 684.12 71.71 o 4 6 0 7.56 -2.00 10.01 o 5 6 0 288.93 268.43 29.42 o 6 6 0 254.81 316.52 30.76 o 7 6 0 194.58 195.09 22.68 o 8 6 0 298.48 337.50 33.67 o 9 6 0 760.01 804.00 75.45 o 10 6 0 43.16 62.82 22.11 o 11 6 0 111.99 112.17 29.14 o 12 6 0 19.83 18.63 46.13 o 13 6 0 98.26 139.33 67.45 o 14 6 0 12.77 -65.65 65.65 o 1 7 0 2865.85 2997.07 220.17 o 2 7 0 106.82 107.31 13.48 o 3 7 0 0.18 0.59 8.14 o 4 7 0 63.13 58.48 14.99 o 5 7 0 94.89 117.46 22.47 o 6 7 0 1052.89 1091.70 84.68 o 7 7 0 310.67 313.94 31.46 o 8 7 0 380.25 388.63 37.49 o 9 7 0 19.86 19.00 18.73 o 10 7 0 672.48 671.69 68.03 o 11 7 0 18.87 16.31 33.83 o 12 7 0 0.82 14.01 32.30 o 13 7 0 3.60 -23.06 57.66 o 0 8 0 658.42 779.98 82.96 o 1 8 0 8.18 15.77 8.43 o 2 8 0 613.56 671.70 53.43 o 3 8 0 81.91 68.99 11.75 o 4 8 0 353.52 331.14 40.55 o 5 8 0 2375.40 2338.33 225.20 o 6 8 0 422.33 377.23 38.97 o 7 8 0 915.04 897.18 72.10 o 8 8 0 45.73 18.68 17.63 o 9 8 0 64.05 75.00 22.33 o 10 8 0 30.04 82.09 25.91 o 11 8 0 41.07 31.05 24.61 o 12 8 0 4.86 4.65 27.79 o 13 8 0 32.29 18.63 60.33 o 1 9 0 256.50 278.72 27.84 o 2 9 0 41.26 30.92 14.66 o 3 9 0 1337.17 1243.37 106.33 o 4 9 0 1763.31 1632.77 159.98 o 5 9 0 3576.56 3518.48 334.88 o 6 9 0 510.16 507.45 49.91 o 7 9 0 70.68 77.73 20.49 o 8 9 0 3.95 24.51 17.61 o 9 9 0 1.37 6.13 18.39 o 10 9 0 115.15 91.25 26.10 o 11 9 0 3.21 48.24 26.98 o 12 9 0 17.03 52.30 30.73 o 0 10 0 3764.69 4102.87 388.45 o 1 10 0 311.35 362.22 34.39 o 2 10 0 586.44 652.92 54.62 o 3 10 0 2557.87 2474.92 205.98 o 4 10 0 136.54 129.65 25.16 o 5 10 0 848.98 893.41 96.41 o 6 10 0 34.27 40.22 24.94 o 7 10 0 154.09 97.65 24.01 o 8 10 0 7.48 23.23 18.76 o 9 10 0 62.70 12.24 21.09 o 10 10 0 85.15 73.35 25.52 o 11 10 0 5.91 18.73 25.43 o 12 10 0 8.07 -17.41 32.14 o 1 11 0 120.34 136.57 18.26 o 2 11 0 193.50 239.30 33.95 o 3 11 0 2.14 37.94 14.40 o 4 11 0 1314.23 1401.90 138.74 o 5 11 0 103.75 123.02 35.15 o 6 11 0 103.32 64.84 26.79 o 7 11 0 66.20 36.05 23.51 o 8 11 0 158.07 96.76 23.64 o 9 11 0 7.04 25.82 21.04 o 10 11 0 28.64 27.58 24.43 o 11 11 0 0.04 -18.99 29.07 o 12 11 0 8.84 70.16 49.23 o 0 12 0 55.31 63.60 27.26 o 1 12 0 64.32 49.50 13.90 o 2 12 0 2.67 29.38 16.03 o 3 12 0 0.52 23.50 13.96 o 4 12 0 70.32 34.68 25.27 o 5 12 0 538.09 563.77 85.26 o 6 12 0 213.96 203.48 44.47 o 7 12 0 15.31 10.61 25.40 o 8 12 0 127.98 173.33 34.28 o 9 12 0 28.70 26.42 24.59 o 10 12 0 12.72 19.22 27.34 o 11 12 0 71.76 80.96 33.78 o 1 13 0 39.74 41.43 14.55 o 2 13 0 24.42 25.65 20.23 o 3 13 0 16.60 -1.69 18.94 o 4 13 0 50.65 49.96 28.50 o 5 13 0 330.57 379.68 65.76 o 6 13 0 2.20 6.63 36.81 o 7 13 0 59.92 29.09 31.35 o 8 13 0 29.10 26.14 24.48 o 9 13 0 28.63 45.61 25.94 o 10 13 0 7.07 49.00 43.44 o 0 14 0 4.57 18.07 25.22 o 1 14 0 0.57 1.47 14.72 o 2 14 0 55.34 116.91 31.21 o 3 14 0 17.15 11.93 45.69 o 4 14 0 6.16 -5.71 31.49 o 5 14 0 74.65 60.55 31.84 o 6 14 0 13.08 33.89 30.90 o 7 14 0 0.43 24.37 31.63 o 8 14 0 63.18 37.78 39.84 o 9 14 0 7.63 7.79 27.27 o 1 15 0 23.58 47.51 33.76 o 2 15 0 2.73 19.23 22.21 o 3 15 0 0.53 -3.86 21.20 o 4 15 0 1.20 47.46 31.06 o 5 15 0 101.55 168.86 42.36 o 6 15 0 203.49 251.26 52.20 o 7 15 0 5.29 -6.49 33.09 o 8 15 0 66.89 173.99 63.00 o 1 16 0 37.47 61.30 64.32 o 2 16 0 4.50 23.56 23.84 o 3 16 0 117.06 229.78 43.09 o 4 16 0 0.09 3.18 22.47 o 5 16 0 0.51 -15.03 39.47 o 6 16 0 98.19 111.74 39.05 o 7 16 0 8.31 54.36 34.95 o 2 17 0 0.23 0.00 41.69 o 3 17 0 14.38 29.50 28.25 o 4 17 0 0.02 3.24 24.97 o 5 17 0 73.55 119.64 39.82 o 6 17 0 18.58 5.13 28.51 o 2 18 0 45.68 150.83 61.22 o 3 18 0 86.72 73.66 51.47 o 4 18 0 1.03 73.38 34.35 o -13 0 1 30.99 -6.02 36.50 o -11 0 1 2.79 70.63 31.94 o -9 0 1 4500.31 4226.33 491.58 o -7 0 1 1889.77 1991.31 164.09 o -5 0 1 1169.58 1169.87 139.30 o -3 0 1 1751.41 1487.69 173.62 o 1 0 1 1111.43 846.66 140.66 o 3 0 1 6136.25 4730.43 544.60 o 5 0 1 924.35 843.39 71.37 o 7 0 1 2199.68 2152.80 177.06 o 9 0 1 26.21 21.50 26.26 o 11 0 1 32.54 46.41 54.12 o 13 0 1 37.71 97.14 44.53 o -14 1 1 12.85 -12.26 30.48 o -13 1 1 219.59 230.25 40.32 o -12 1 1 3.60 18.23 24.27 o -11 1 1 20.96 13.93 22.67 o -10 1 1 150.64 171.72 28.49 o -9 1 1 932.36 965.21 88.24 o -8 1 1 253.24 249.19 22.72 o -7 1 1 482.54 505.24 31.10 o -6 1 1 2.24 -0.46 8.67 o -5 1 1 519.85 500.13 37.39 o -4 1 1 3028.30 2603.40 212.89 o -3 1 1 2018.92 1807.60 148.57 o 1 1 1 1376.49 1026.24 169.03 o 2 1 1 401.68 336.45 42.45 o 3 1 1 1154.58 896.60 74.46 o 4 1 1 15.94 0.75 7.02 o 5 1 1 769.46 767.35 54.52 o 6 1 1 1573.03 1491.24 87.50 o 7 1 1 52.26 48.62 9.55 o 8 1 1 163.01 134.20 18.38 o 9 1 1 24.07 61.82 19.75 o 10 1 1 123.35 124.53 25.40 o 11 1 1 5.49 8.75 21.42 o 12 1 1 62.32 22.20 24.57 o 13 1 1 25.42 62.35 26.12 o 14 1 1 47.98 100.88 33.89 o -14 2 1 6.71 30.67 27.95 o -13 2 1 1.00 2.00 23.66 o -12 2 1 2.25 -21.35 22.02 o -11 2 1 34.32 29.02 21.50 o -10 2 1 1.34 8.74 19.85 o -9 2 1 427.64 409.21 35.93 o -8 2 1 12.60 24.74 11.97 o -7 2 1 46.29 47.27 11.24 o -6 2 1 956.15 902.33 58.93 o -5 2 1 11631.40 11442.90 758.56 o -4 2 1 74.63 70.39 10.78 o -3 2 1 1082.74 899.17 86.81 o -2 2 1 3094.70 2769.63 453.90 o 2 2 1 5264.44 4418.56 507.47 o 3 2 1 1202.32 929.86 90.18 o 4 2 1 123.72 122.35 12.49 o 5 2 1 81.99 61.86 10.70 o 6 2 1 253.38 267.87 20.42 o 7 2 1 484.56 456.58 33.64 o 8 2 1 722.15 719.38 51.36 o 9 2 1 731.88 718.07 55.14 o 10 2 1 176.50 164.69 30.25 o 11 2 1 99.74 99.28 23.86 o 12 2 1 0.77 13.96 21.71 o 13 2 1 7.68 -8.52 27.26 o 14 2 1 5.06 30.25 32.02 o -14 3 1 25.79 114.96 51.53 o -13 3 1 30.91 29.95 27.63 o -12 3 1 168.72 188.49 29.05 o -11 3 1 16.47 32.09 18.52 o -10 3 1 136.01 112.98 23.14 o -9 3 1 0.24 1.74 12.94 o -8 3 1 747.32 716.88 50.41 o -7 3 1 399.39 374.62 29.49 o -6 3 1 3.81 7.28 8.17 o -5 3 1 1148.60 1092.00 69.30 o -4 3 1 798.02 673.81 58.14 o -3 3 1 2184.00 1884.74 154.99 o -2 3 1 9224.62 8834.14 1014.36 o 1 3 1 2763.87 2420.94 396.49 o 2 3 1 1438.49 1187.75 140.29 o 3 3 1 4811.39 4553.71 370.51 o 4 3 1 519.85 509.55 41.19 o 5 3 1 298.28 263.04 20.82 o 6 3 1 538.88 531.78 36.59 o 7 3 1 5.15 5.59 9.51 o 8 3 1 373.62 413.51 30.32 o 9 3 1 585.30 653.98 55.03 o 10 3 1 76.56 43.96 25.24 o 11 3 1 9.31 55.20 20.17 o 12 3 1 74.83 126.88 29.79 o 13 3 1 39.63 51.90 36.98 o 14 3 1 0.01 -29.85 45.72 o -14 4 1 2.82 47.50 44.30 o -13 4 1 0.07 13.29 37.91 o -12 4 1 10.29 35.57 68.56 o -11 4 1 212.83 215.44 44.48 o -10 4 1 0.31 22.19 14.73 o -9 4 1 32.19 23.45 13.83 o -8 4 1 58.79 71.15 13.95 o -7 4 1 49.55 42.38 12.34 o -6 4 1 19.72 30.94 10.68 o -5 4 1 2315.83 2124.93 157.14 o -4 4 1 8059.60 8078.94 585.52 o -3 4 1 502.07 567.55 58.73 o -2 4 1 510.85 580.54 51.87 o -1 4 1 1805.56 1531.62 124.48 o 0 4 1 64.45 56.84 23.09 o 1 4 1 856.41 647.76 79.25 o 2 4 1 5498.80 5321.46 610.10 o 3 4 1 1262.39 1215.04 101.32 o 4 4 1 170.26 189.89 18.54 o 5 4 1 86.18 65.71 11.17 o 6 4 1 0.02 14.20 13.39 o 7 4 1 339.29 336.78 30.36 o 8 4 1 5.21 7.30 11.35 o 9 4 1 186.33 203.26 22.21 o 10 4 1 113.62 81.36 21.68 o 11 4 1 1.72 51.50 36.66 o 12 4 1 57.84 70.39 40.77 o 13 4 1 14.55 90.31 56.33 o 14 4 1 5.39 64.20 56.77 o -14 5 1 13.49 25.90 101.13 o -13 5 1 129.49 206.82 73.67 o -12 5 1 69.56 156.18 60.34 o -11 5 1 3.07 -21.07 28.68 o -10 5 1 1469.81 1728.79 135.44 o -9 5 1 18.33 54.04 18.53 o -8 5 1 561.85 587.29 51.23 o -7 5 1 539.19 562.75 48.77 o -6 5 1 1249.83 1140.56 86.90 o -5 5 1 581.94 551.29 51.35 o -4 5 1 730.72 714.10 61.92 o -3 5 1 0.19 -7.75 7.75 o -2 5 1 3392.87 3363.08 274.92 o -1 5 1 7.07 4.91 8.07 o 0 5 1 752.73 709.59 60.66 o 1 5 1 348.33 473.80 59.35 o 2 5 1 776.92 655.10 54.63 o 3 5 1 2578.44 2579.55 245.44 o 4 5 1 0.13 2.28 7.62 o 5 5 1 119.88 96.54 14.94 o 6 5 1 286.07 280.84 26.86 o 7 5 1 2.04 12.37 12.96 o 8 5 1 4.12 20.28 14.21 o 9 5 1 0.60 16.13 15.43 o 10 5 1 0.90 12.71 22.66 o 11 5 1 10.27 47.31 37.62 o 12 5 1 38.27 -23.07 47.02 o 13 5 1 9.07 63.87 58.55 o 14 5 1 12.32 94.30 94.03 o -14 6 1 10.76 97.58 76.29 o -13 6 1 10.69 61.21 59.44 o -12 6 1 39.76 -5.32 49.69 o -11 6 1 14.60 40.55 24.02 o -10 6 1 136.80 138.25 24.28 o -9 6 1 462.10 395.06 37.79 o -8 6 1 130.54 134.93 20.50 o -7 6 1 30.20 43.41 12.90 o -6 6 1 259.84 278.46 26.09 o -5 6 1 233.00 232.03 26.56 o -4 6 1 439.17 459.85 50.70 o -3 6 1 7.57 0.06 8.61 o -2 6 1 5169.85 5372.50 437.97 o -1 6 1 2522.96 2731.08 200.11 o 0 6 1 7385.06 8461.45 688.06 o 1 6 1 749.47 807.28 61.72 o 2 6 1 1734.89 1571.49 130.58 o 3 6 1 5.09 32.47 12.25 o 4 6 1 10.13 21.55 10.99 o 5 6 1 15.55 25.28 11.52 o 6 6 1 100.11 100.16 15.23 o 7 6 1 45.28 62.13 14.28 o 8 6 1 412.56 396.92 37.92 o 9 6 1 158.70 150.04 27.68 o 10 6 1 6.19 11.23 20.66 o 11 6 1 5.58 -22.48 22.48 o 12 6 1 202.11 345.42 95.01 o 13 6 1 45.76 165.03 71.87 o -13 7 1 15.80 105.57 70.08 o -12 7 1 5.54 13.72 32.32 o -11 7 1 0.02 15.38 23.33 o -10 7 1 2.21 25.03 21.22 o -9 7 1 25.38 20.73 16.34 o -8 7 1 0.06 24.98 14.73 o -7 7 1 6.26 -1.45 12.12 o -6 7 1 41.26 46.32 31.12 o -5 7 1 62.96 70.35 14.26 o -4 7 1 54.34 63.96 14.73 o -3 7 1 279.96 272.19 29.45 o -2 7 1 49.36 36.60 8.81 o -1 7 1 1788.14 1743.09 129.35 o 0 7 1 61.43 98.03 15.67 o 1 7 1 1560.05 1684.68 124.75 o 2 7 1 368.79 431.24 37.40 o 3 7 1 148.34 138.10 17.82 o 4 7 1 5.67 11.81 9.91 o 5 7 1 139.98 140.55 18.52 o 6 7 1 348.48 338.04 31.95 o 7 7 1 226.75 261.19 32.60 o 8 7 1 82.53 59.68 19.56 o 9 7 1 311.67 269.40 35.79 o 10 7 1 12.68 -0.52 19.91 o 11 7 1 15.72 13.37 25.20 o 12 7 1 203.52 154.20 53.44 o 13 7 1 17.84 -56.78 56.78 o -13 8 1 2.20 -50.56 54.11 o -12 8 1 15.30 17.71 30.10 o -11 8 1 5.04 24.15 25.36 o -10 8 1 70.02 54.99 32.41 o -9 8 1 99.05 95.51 23.90 o -8 8 1 59.64 111.50 20.09 o -7 8 1 2.13 17.32 13.70 o -6 8 1 94.10 95.52 17.76 o -5 8 1 602.16 627.66 79.49 o -4 8 1 184.32 202.82 29.66 o -3 8 1 139.27 148.97 17.35 o -2 8 1 553.99 648.55 51.96 o -1 8 1 154.61 184.59 20.21 o 0 8 1 23.35 23.98 10.85 o 1 8 1 4603.18 4849.32 354.41 o 2 8 1 762.64 776.26 62.03 o 3 8 1 118.88 131.12 20.13 o 4 8 1 31.59 55.69 16.93 o 5 8 1 187.95 187.27 23.16 o 6 8 1 460.90 525.87 51.29 o 7 8 1 645.98 762.87 71.72 o 8 8 1 293.78 323.68 37.74 o 9 8 1 200.71 167.05 28.09 o 10 8 1 29.28 38.64 21.93 o 11 8 1 36.68 77.90 28.12 o 12 8 1 40.04 52.12 32.73 o 13 8 1 0.35 15.97 51.45 o -13 9 1 1.21 49.68 56.77 o -12 9 1 39.93 82.18 33.30 o -11 9 1 16.25 28.10 25.49 o -10 9 1 11.05 17.69 22.27 o -9 9 1 47.53 55.32 21.66 o -8 9 1 12.73 -3.26 15.75 o -7 9 1 203.50 175.89 25.64 o -6 9 1 1938.82 1802.66 152.73 o -5 9 1 89.87 80.14 20.24 o -4 9 1 57.64 73.29 18.90 o -3 9 1 206.24 201.05 26.05 o -2 9 1 69.72 28.61 11.52 o -1 9 1 248.55 256.61 26.09 o 0 9 1 372.56 451.19 35.78 o 1 9 1 776.59 901.00 71.38 o 2 9 1 590.38 789.36 72.60 o 3 9 1 176.29 227.87 31.03 o 4 9 1 325.17 381.46 47.32 o 5 9 1 5887.19 6226.05 588.25 o 6 9 1 39.28 140.11 153.06 o 7 9 1 10.66 19.10 19.33 o 8 9 1 5.64 25.29 18.04 o 9 9 1 32.28 63.79 22.06 o 10 9 1 29.99 34.49 23.82 o 11 9 1 0.02 33.15 25.79 o 12 9 1 35.05 43.04 29.43 o -12 10 1 19.89 62.10 33.77 o -11 10 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