data_3000222
loop_
_publ_author_name
'Gines M. Esteban-Parra'
'Eider San Sebasti\'an'
'Javier Cepeda'
'Cristina S\'anchez-Gonz\'alez'
'Lorenzo Rivas'
'Juan Llopis'
'Pilar Aranda'
'Miguel Quir\'os'
'Antonio Rodr\'iguez-Di\'eguez'
_journal_name_full               'To be published in Dalton Trans.'
_diffrn_ambient_temperature      100(2)
_cell_measurement_temperature    100(2)
_chemical_formula_sum            'C24 H48 N22 O16 Zn'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_length_a                   7.1837(5)
_cell_length_b                   11.4156(9)
_cell_length_c                   12.8451(10)
_cell_angle_alpha                80.763(3)
_cell_angle_beta                 82.269(3)
_cell_angle_gamma                77.782(3)
_cell_volume                     1010.63(13)
_diffrn_radiation_wavelength     0.71069
_diffrn_radiation_type           MoK\a
_refine_ls_R_factor_all          0.0462
_refine_ls_R_factor_gt           0.0363
_refine_ls_wR_factor_gt          0.0919
_refine_ls_wR_factor_ref         0.0988
_refine_ls_goodness_of_fit_ref   0.924
_cod_hold_until_date             2019-12-25
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
? ? ? ?