#------------------------------------------------------------------------------ #$Date: 2016-04-06 13:46:40 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181860 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/00/3500013.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500013 _cell_angle_alpha 90.000 _cell_angle_beta 121.326 _cell_angle_gamma 90.000 _cell_length_a 13.5424 _cell_length_b 17.9856 _cell_length_c 15.0719 _exptl_crystal_F_000 1384.00 _reflns_d_resolution_high 0.7111 _cod_data_source_file rufen3.hkl _cod_data_source_block rufen3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Ru(bpy)2Cl(DMSO)](PF6).H2O' _shelx_refln_list_code 4 _shelx_f_calc_maximum 390.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 121346.80 45534.93 255.30 o 2 0 0 2762.63 522.60 34.91 o 3 0 0 15154.16 25434.87 349.13 o 4 0 0 17622.43 13839.54 293.48 o 5 0 0 37214.45 38882.73 482.23 o 6 0 0 12446.15 10430.12 274.94 o 7 0 0 2121.79 2130.75 114.56 o 8 0 0 1799.06 1769.63 88.37 o 9 0 0 1038.85 1010.28 66.55 o 10 0 0 2368.28 2442.79 124.38 o 11 0 0 554.09 528.05 72.01 o 12 0 0 642.31 749.53 77.46 o 13 0 0 59.18 305.48 72.01 o 14 0 0 40.89 -22.91 80.74 o 15 0 0 243.95 356.76 91.65 o 2 1 0 33269.71 30592.96 355.67 o 3 1 0 52231.79 53267.91 348.32 o 4 1 0 23802.92 21994.55 253.81 o 5 1 0 13180.12 13819.92 215.62 o 6 1 0 616.34 820.89 43.10 o 7 1 0 1335.55 1482.19 71.46 o 8 1 0 711.32 542.15 43.10 o 9 1 0 29.66 -41.66 41.66 o 10 1 0 78.77 134.81 45.90 o 11 1 0 192.77 219.97 90.01 o 12 1 0 85.57 58.10 48.21 o 13 1 0 126.04 89.09 53.61 o 14 1 0 15.65 43.61 78.55 o 15 1 0 39.89 136.82 72.01 o 0 2 0 33049.00 6845.04 137.47 o 1 2 0 20371.76 2623.29 219.84 o 2 2 0 48.62 4655.37 174.56 o 3 2 0 41712.81 58805.78 525.87 o 4 2 0 14082.38 10250.10 259.66 o 5 2 0 611.33 810.63 50.19 o 6 2 0 114.90 224.75 48.00 o 7 2 0 456.05 331.67 52.37 o 8 2 0 2758.77 2970.84 148.38 o 9 2 0 87.27 -5.46 60.01 o 10 2 0 16.20 106.92 64.37 o 11 2 0 112.93 180.02 68.73 o 12 2 0 39.42 48.00 68.73 o 13 2 0 39.62 102.56 72.01 o 14 2 0 14.74 6.55 80.74 o 1 3 0 640.57 1318.05 106.92 o 2 3 0 1028.07 413.50 36.00 o 3 3 0 5883.63 7740.76 229.11 o 4 3 0 5524.38 5003.40 198.56 o 5 3 0 2397.67 2398.05 125.47 o 6 3 0 1932.50 2077.30 93.83 o 7 3 0 1948.14 1697.62 82.92 o 8 3 0 1240.43 1317.95 66.55 o 9 3 0 908.75 1047.38 70.92 o 10 3 0 392.88 392.77 70.92 o 11 3 0 11.74 -72.01 72.01 o 12 3 0 10.94 -26.18 73.10 o 13 3 0 48.72 53.46 77.46 o 14 3 0 96.11 112.37 80.74 o 0 4 0 40816.64 39212.22 399.31 o 1 4 0 27600.40 41230.27 1148.84 o 2 4 0 36.55 1239.39 56.73 o 3 4 0 67.28 525.87 40.37 o 4 4 0 2449.27 3758.55 182.20 o 5 4 0 18293.18 15642.99 320.76 o 6 4 0 27648.25 26685.17 408.04 o 7 4 0 6594.27 6553.73 229.11 o 8 4 0 180.10 86.19 61.10 o 9 4 0 3044.36 2752.63 135.29 o 10 4 0 3187.60 3234.86 141.83 o 11 4 0 2425.21 2213.67 115.65 o 12 4 0 1018.98 1112.84 86.19 o 13 4 0 107.08 180.02 77.46 o 14 4 0 30.99 139.65 81.83 o 1 5 0 22992.30 24082.19 248.00 o 2 5 0 25423.19 26332.77 377.49 o 3 5 0 7836.15 7075.24 223.66 o 4 5 0 6371.05 8358.28 238.93 o 5 5 0 13.10 -25.09 44.73 o 6 5 0 750.67 1064.83 58.91 o 7 5 0 5578.44 5304.52 200.75 o 8 5 0 3236.23 3305.78 162.56 o 9 5 0 1443.17 1554.70 78.55 o 10 5 0 1110.96 1083.38 80.74 o 11 5 0 18.01 -16.37 75.28 o 12 5 0 257.99 212.75 78.55 o 13 5 0 394.70 285.85 86.19 o 14 5 0 245.97 327.30 89.46 o 0 6 0 11858.84 13395.50 280.39 o 1 6 0 2494.60 2874.61 121.10 o 2 6 0 9792.73 9514.75 260.75 o 3 6 0 183.19 -39.28 39.28 o 4 6 0 27.58 85.10 42.55 o 5 6 0 1780.24 1655.07 75.28 o 6 6 0 977.97 882.63 57.82 o 7 6 0 1877.34 1891.82 89.46 o 8 6 0 135.98 164.74 57.82 o 9 6 0 26.71 -31.64 61.10 o 10 6 0 104.59 36.00 66.55 o 11 6 0 192.69 161.47 73.10 o 12 6 0 15.41 -76.37 76.37 o 13 6 0 39.73 75.28 76.37 o 14 6 0 0.78 27.28 82.92 o 1 7 0 693.71 579.50 28.15 o 2 7 0 3336.14 3566.53 165.83 o 3 7 0 10096.84 12438.68 285.85 o 4 7 0 6864.08 5692.92 218.20 o 5 7 0 18.13 -10.91 46.91 o 6 7 0 258.76 220.39 53.46 o 7 7 0 343.23 357.85 58.91 o 8 7 0 160.08 69.83 60.01 o 9 7 0 758.59 824.81 69.83 o 10 7 0 92.73 45.82 65.46 o 11 7 0 10.75 151.65 69.83 o 12 7 0 2.38 -73.10 73.10 o 13 7 0 73.98 57.82 79.64 o 14 7 0 81.70 6.55 88.37 o 0 8 0 13518.71 18226.52 333.85 o 1 8 0 29136.51 28601.82 292.39 o 2 8 0 11935.06 13358.40 296.76 o 3 8 0 3034.41 2221.31 136.38 o 4 8 0 4689.59 5151.78 210.57 o 5 8 0 730.26 761.53 54.55 o 6 8 0 7339.22 7614.20 222.57 o 7 8 0 4170.18 4320.42 180.02 o 8 8 0 102.73 50.19 60.01 o 9 8 0 2.07 -19.64 63.28 o 10 8 0 268.94 161.47 70.92 o 11 8 0 906.02 828.08 79.64 o 12 8 0 338.70 304.39 79.64 o 13 8 0 23.23 -10.91 79.64 o 14 8 0 0.74 -12.00 86.19 o 1 9 0 9371.03 9715.79 182.83 o 2 9 0 23835.24 28375.15 416.77 o 3 9 0 11332.21 10580.68 261.84 o 4 9 0 18826.88 18586.55 332.76 o 5 9 0 713.55 723.34 56.73 o 6 9 0 723.79 702.61 63.28 o 7 9 0 1102.56 952.46 67.64 o 8 9 0 1919.99 2078.39 86.19 o 9 9 0 1224.57 1371.41 79.64 o 10 9 0 180.43 -4.36 72.01 o 11 9 0 79.59 93.83 72.01 o 12 9 0 71.14 101.46 77.46 o 13 9 0 230.95 403.68 88.37 o 0 10 0 921.28 573.87 42.55 o 1 10 0 3905.35 5024.22 137.31 o 2 10 0 1530.58 1458.69 57.82 o 4 10 0 468.57 423.31 57.82 o 5 10 0 149.05 222.57 53.46 o 6 10 0 313.89 314.21 58.91 o 7 10 0 52.07 159.29 57.82 o 8 10 0 140.02 185.47 64.37 o 9 10 0 24.54 36.00 67.64 o 10 10 0 150.61 212.75 69.83 o 11 10 0 35.34 40.37 73.10 o 12 10 0 53.93 30.55 78.55 o 13 10 0 50.63 19.64 90.55 o 1 11 0 478.32 523.91 34.32 o 2 11 0 207.95 269.48 46.91 o 3 11 0 4529.27 4218.96 184.38 o 4 11 0 219.63 137.47 55.64 o 5 11 0 335.28 280.39 60.01 o 6 11 0 468.37 574.97 61.10 o 7 11 0 781.69 854.27 70.92 o 8 11 0 952.51 925.18 77.46 o 9 11 0 637.83 625.15 79.64 o 10 11 0 68.84 75.28 73.10 o 11 11 0 0.31 -48.00 74.19 o 12 11 0 63.78 313.12 77.46 o 13 11 0 26.88 12.00 88.37 o 0 12 0 594.43 302.21 45.82 o 1 12 0 1876.26 2379.86 88.13 o 2 12 0 855.96 614.24 55.64 o 3 12 0 1095.79 744.07 61.10 o 4 12 0 3166.34 3402.88 160.38 o 5 12 0 3108.71 3059.21 150.56 o 6 12 0 1937.42 1982.38 102.56 o 7 12 0 186.21 197.47 65.46 o 8 12 0 73.46 122.19 70.92 o 9 12 0 396.85 432.04 79.64 o 10 12 0 645.81 497.50 79.64 o 11 12 0 404.99 667.70 79.64 o 12 12 0 161.03 152.74 87.28 o 1 13 0 1572.91 1700.59 59.27 o 2 13 0 5133.23 5569.64 189.84 o 3 13 0 6697.70 6705.39 195.29 o 4 13 0 1016.98 984.10 66.55 o 5 13 0 0.07 -46.91 61.10 o 6 13 0 715.11 713.52 67.64 o 7 13 0 1780.64 1754.35 93.83 o 8 13 0 2554.46 2561.71 112.37 o 9 13 0 1814.62 1978.01 96.01 o 10 13 0 362.18 372.04 81.83 o 11 13 0 6.96 -60.01 77.46 o 12 13 0 222.96 187.65 90.55 o 0 14 0 177.98 220.39 52.37 o 1 14 0 66.26 -3.89 37.41 o 2 14 0 557.01 616.42 66.55 o 3 14 0 737.82 631.70 69.83 o 4 14 0 405.41 284.76 64.37 o 5 14 0 58.81 21.82 62.19 o 6 14 0 283.55 307.67 65.46 o 7 14 0 81.02 222.57 66.55 o 8 14 0 26.64 -73.10 75.28 o 9 14 0 3.03 76.37 76.37 o 10 14 0 44.52 -77.46 77.46 o 11 14 0 115.22 218.20 79.64 o 12 14 0 33.05 34.91 86.19 o 1 15 0 70.45 41.40 38.55 o 2 15 0 913.22 859.72 68.73 o 3 15 0 1061.85 1367.04 74.19 o 4 15 0 403.39 500.78 64.37 o 5 15 0 161.21 145.11 63.28 o 6 15 0 41.27 1.09 63.28 o 7 15 0 53.76 57.82 67.64 o 8 15 0 261.34 282.57 74.19 o 9 15 0 244.74 266.21 77.46 o 10 15 0 87.82 16.37 77.46 o 11 15 0 0.00 -19.64 82.92 o 0 16 0 1423.56 1611.43 84.01 o 1 16 0 696.43 790.21 45.90 o 2 16 0 287.79 51.28 65.46 o 3 16 0 246.89 97.10 67.64 o 4 16 0 204.56 100.37 64.37 o 5 16 0 965.78 1039.74 76.37 o 6 16 0 411.79 477.87 70.92 o 7 16 0 209.64 63.28 72.01 o 8 16 0 124.37 57.82 78.55 o 9 16 0 80.80 -45.82 79.64 o 10 16 0 247.52 414.59 80.74 o 1 17 0 322.32 382.95 45.13 o 2 17 0 2690.20 2713.36 116.74 o 3 17 0 3467.24 3262.14 117.83 o 4 17 0 966.56 968.82 74.19 o 5 17 0 102.62 14.18 66.55 o 6 17 0 80.92 -73.10 73.10 o 7 17 0 613.59 440.77 81.83 o 8 17 0 754.92 763.71 91.65 o 9 17 0 294.84 213.84 85.10 o 10 17 0 55.52 18.55 82.92 o 0 18 0 1204.31 1259.03 73.10 o 1 18 0 915.93 1036.55 51.26 o 2 18 0 301.84 272.75 68.73 o 3 18 0 32.15 -67.64 67.64 o 4 18 0 567.83 504.05 75.28 o 5 18 0 433.28 568.42 77.46 o 6 18 0 134.28 174.56 72.01 o 7 18 0 12.84 -12.00 77.46 o 8 18 0 27.83 -18.55 85.10 o 9 18 0 19.92 30.55 85.10 o 1 19 0 126.59 127.35 47.44 o 2 19 0 67.56 74.19 65.46 o 3 19 0 81.39 -5.46 68.73 o 4 19 0 230.49 171.29 75.28 o 5 19 0 21.48 18.55 72.01 o 6 19 0 59.47 -80.74 80.74 o 7 19 0 129.64 206.20 80.74 o 8 19 0 144.88 137.47 88.37 o 0 20 0 717.01 836.81 74.19 o 1 20 0 297.83 221.99 49.30 o 2 20 0 0.34 48.00 66.55 o 3 20 0 34.07 -3.27 68.73 o 4 20 0 213.13 259.66 73.10 o 5 20 0 347.68 382.95 78.55 o 6 20 0 195.12 314.21 84.01 o 7 20 0 177.96 202.93 88.37 o 1 21 0 166.99 156.52 51.67 o 2 21 0 498.78 519.32 79.64 o 3 21 0 556.02 565.15 77.46 o 4 21 0 290.32 118.92 81.83 o 5 21 0 7.48 -34.91 81.83 o 6 21 0 110.84 177.84 82.92 o 0 22 0 383.11 511.69 80.74 o 1 22 0 223.10 263.42 54.71 o 2 22 0 48.46 -72.01 79.64 o 3 22 0 4.35 -10.91 78.55 o 4 22 0 279.53 306.58 85.10 o 5 22 0 435.75 570.60 90.55 o 1 23 0 27.86 12.13 57.84 o 2 23 0 12.14 -52.37 82.92 o 0 24 0 304.81 330.58 88.37 o 1 24 0 210.36 125.27 62.84 o 1 25 0 70.33 32.92 74.19 o -15 1 1 82.27 46.60 61.30 o -14 1 1 63.19 102.19 55.16 o -13 1 1 12.89 -4.18 50.13 o -12 1 1 234.35 182.47 51.30 o -11 1 1 773.11 897.99 52.84 o -10 1 1 637.42 667.32 87.28 o -9 1 1 935.92 944.83 46.29 o -8 1 1 301.89 337.72 45.82 o -7 1 1 538.19 489.44 35.10 o -6 1 1 18.55 122.73 31.24 o -5 1 1 2231.92 2074.66 65.52 o -4 1 1 3910.27 3388.80 119.55 o -3 1 1 19772.38 18883.93 210.97 o -2 1 1 2709.94 3809.43 104.53 o 0 1 1 21737.55 15369.50 298.57 o 1 1 1 30157.13 40850.58 174.96 o 2 1 1 2787.14 1989.74 72.51 o 3 1 1 227.98 234.86 32.73 o 4 1 1 1217.30 891.13 58.91 o 5 1 1 1547.25 2209.45 76.73 o 6 1 1 1884.32 1573.01 105.28 o 7 1 1 446.39 403.55 38.18 o 8 1 1 25.41 -24.55 40.12 o 9 1 1 8.23 23.79 43.58 o 10 1 1 87.35 152.51 72.55 o 11 1 1 188.39 198.02 52.46 o 12 1 1 191.49 140.74 53.23 o 13 1 1 68.47 -6.15 56.73 o 14 1 1 20.94 66.62 73.64 o -15 2 1 25.69 -10.91 86.19 o -14 2 1 62.49 -40.37 79.64 o -13 2 1 519.62 495.32 79.64 o -12 2 1 975.17 976.46 82.92 o -11 2 1 1704.47 1807.81 86.19 o -10 2 1 1200.77 1123.75 75.28 o -9 2 1 46.60 105.83 58.91 o -8 2 1 336.26 281.48 53.46 o -7 2 1 8858.73 8338.64 247.66 o -6 2 1 29993.76 27852.56 415.68 o -5 2 1 13921.06 14006.47 305.48 o -4 2 1 3546.30 2358.78 105.83 o -3 2 1 462.08 2395.87 118.92 o -2 2 1 15092.17 26589.16 314.21 o -1 2 1 152152.19 136765.55 1294.49 o 0 2 1 15169.11 27661.24 413.49 o 1 2 1 664.98 46.91 22.91 o 2 2 1 24789.65 28330.42 361.13 o 3 2 1 4901.60 5317.61 212.75 o 4 2 1 34859.94 33736.41 442.95 o 5 2 1 20704.28 20626.75 360.04 o 6 2 1 290.10 325.12 48.00 o 7 2 1 452.26 363.31 54.55 o 8 2 1 1160.15 1227.39 65.46 o 9 2 1 2327.65 2195.13 115.65 o 10 2 1 1139.76 1105.20 79.64 o 11 2 1 1902.49 1970.38 99.28 o 12 2 1 278.76 291.30 79.64 o 13 2 1 87.60 -31.64 79.64 o 14 2 1 209.43 281.48 87.28 o -15 3 1 35.09 70.92 87.28 o -14 3 1 148.39 282.57 77.46 o -13 3 1 318.68 362.22 78.55 o -12 3 1 51.80 45.82 74.19 o -11 3 1 561.21 615.33 78.55 o -10 3 1 486.19 380.76 67.64 o -9 3 1 4964.14 4953.21 182.20 o -8 3 1 4533.06 4374.98 193.11 o -7 3 1 7.61 50.19 49.10 o -6 3 1 1531.88 1785.99 89.46 o -5 3 1 11076.88 12188.83 295.67 o -4 3 1 21424.43 18704.38 329.49 o -3 3 1 15496.91 19027.33 314.21 o -2 3 1 1503.52 2751.54 147.29 o -1 3 1 1.36 -17.72 43.64 o 0 3 1 7946.77 6415.07 284.76 o 1 3 1 4901.70 7588.18 555.33 o 2 3 1 26.61 124.38 38.19 o 3 3 1 1696.23 2907.56 142.92 o 4 3 1 3584.23 3238.14 161.47 o 5 3 1 249.70 384.04 45.82 o 6 3 1 7552.59 7058.88 233.48 o 7 3 1 1785.97 1533.97 79.64 o 8 3 1 226.65 269.48 60.01 o 9 3 1 219.63 377.49 66.55 o 10 3 1 36.38 24.00 69.83 o 11 3 1 374.71 568.42 78.55 o 12 3 1 447.18 464.77 80.74 o 13 3 1 130.06 137.47 79.64 o 14 3 1 84.48 -56.73 90.55 o -15 4 1 3.61 -34.91 88.37 o -14 4 1 18.91 48.00 80.74 o -13 4 1 5.16 3.27 75.28 o -12 4 1 1.81 -15.27 74.19 o -11 4 1 123.15 150.56 73.10 o -10 4 1 0.73 46.91 66.55 o -9 4 1 1995.49 2151.48 104.74 o -8 4 1 461.23 520.41 58.91 o -7 4 1 283.16 402.59 52.37 o -6 4 1 2420.70 2224.58 106.92 o -5 4 1 5840.92 6242.80 225.84 o -4 4 1 3684.51 2107.84 109.10 o -3 4 1 119.50 1129.20 63.28 o -2 4 1 382.05 2861.74 144.01 o -1 4 1 31023.15 53341.99 334.04 o 0 4 1 26015.33 43110.00 301.64 o 1 4 1 46725.72 42043.71 379.67 o 2 4 1 320.83 87.28 38.19 o 3 4 1 77.66 198.56 39.28 o 4 4 1 282.78 396.04 42.55 o 5 4 1 4658.57 4295.33 204.02 o 6 4 1 5239.83 5197.60 211.66 o 7 4 1 686.21 603.33 60.01 o 8 4 1 155.60 120.01 61.10 o 9 4 1 127.91 110.19 65.46 o 10 4 1 311.03 279.30 73.10 o 11 4 1 6.91 0.00 74.19 o 12 4 1 1.03 -49.10 74.19 o 13 4 1 98.83 37.09 80.74 o 14 4 1 15.21 -2.18 88.37 o -15 5 1 53.40 79.64 92.74 o -14 5 1 20.50 2.18 80.74 o -13 5 1 4.66 -77.46 77.46 o -12 5 1 121.32 82.92 75.28 o -11 5 1 121.14 46.91 73.10 o -10 5 1 1930.12 2100.21 112.37 o -9 5 1 717.71 677.52 68.73 o -8 5 1 16.78 7.64 56.73 o -7 5 1 2.15 -53.46 53.46 o -6 5 1 3535.78 3890.56 182.20 o -5 5 1 7158.43 6607.19 226.93 o -4 5 1 851.59 561.87 42.55 o -3 5 1 55.46 -21.82 36.00 o -2 5 1 2236.39 2103.48 90.55 o -1 5 1 7265.73 9974.13 190.38 o 0 5 1 1574.93 262.04 54.01 o 1 5 1 16825.37 27925.39 948.09 o 2 5 1 687.49 7.64 39.28 o 3 5 1 3011.56 3918.93 190.93 o 4 5 1 935.16 1171.75 56.73 o 5 5 1 23.32 158.20 44.73 o 6 5 1 172.53 96.01 53.46 o 7 5 1 2330.31 2252.95 127.65 o 8 5 1 1998.19 1799.09 112.37 o 9 5 1 1.24 14.18 61.10 o 10 5 1 282.48 290.21 73.10 o 11 5 1 151.69 100.37 79.64 o 12 5 1 48.20 -39.28 77.46 o 13 5 1 72.28 123.28 80.74 o 14 5 1 6.36 -32.73 91.65 o -14 6 1 7.51 75.28 80.74 o -13 6 1 491.77 578.24 87.28 o -12 6 1 1378.35 1314.67 87.28 o -11 6 1 1037.36 908.82 79.64 o -10 6 1 532.66 646.97 69.83 o -9 6 1 1.13 -61.10 61.10 o -8 6 1 4860.02 4885.57 189.84 o -7 6 1 14510.94 13991.19 285.85 o -6 6 1 5444.23 5932.95 216.02 o -5 6 1 7715.93 7259.62 235.66 o -4 6 1 1681.86 1507.78 75.28 o -3 6 1 22405.14 26699.35 396.04 o -2 6 1 32784.02 31443.09 418.95 o -1 6 1 8368.68 11696.59 346.94 o 0 6 1 7251.40 5632.22 181.65 o 1 6 1 2940.38 4855.29 177.29 o 2 6 1 6169.56 8066.98 242.21 o 3 6 1 3486.99 3045.03 156.02 o 4 6 1 3423.94 3309.05 168.02 o 5 6 1 7678.44 7146.16 234.57 o 6 6 1 3192.73 2922.83 157.11 o 7 6 1 258.24 317.49 57.82 o 8 6 1 5.56 57.82 60.01 o 9 6 1 219.94 151.65 65.46 o 10 6 1 2022.24 2326.05 114.56 o 11 6 1 797.16 675.34 79.64 o 12 6 1 47.29 214.93 73.10 o 13 6 1 19.87 42.55 82.92 o 14 6 1 127.17 113.47 91.65 o -14 7 1 315.27 418.95 88.37 o -13 7 1 82.98 -57.82 79.64 o -12 7 1 5.09 12.00 73.10 o -11 7 1 607.03 625.15 74.19 o -10 7 1 985.51 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