#------------------------------------------------------------------------------ #$Date: 2016-06-01 12:27:03 +0300 (Wed, 01 Jun 2016) $ #$Revision: 183218 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/00/3500036.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500036 _cell_angle_alpha 90.000 _cell_angle_beta 112.990 _cell_angle_gamma 90.000 _cell_length_a 9.74600 _cell_length_b 17.2150 _cell_length_c 11.3600 _exptl_crystal_F_000 772.00 _reflns_d_resolution_high 0.7709 _cod_data_source_file e81_pl.fcf _cod_data_source_block e81 _shelx_title ' e81 P21/n R = 0.03 ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.96 _shelx_f_squared_multiplier 0.010 loop_ _symmetry_equiv_pos_as_xyz x,y,z 1/2-x,1/2+y,1/2-z -x,-y,-z 1/2+x,1/2-y,1/2+z loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status _refln_sint/lambda 2 0 0 1577355.25 1577355.25 12559.28 o 104.96568 4 0 0 11524.33 11524.33 1073.51 o 104.96568 6 0 0 4508.99 4508.99 671.49 o 104.96568 8 0 0 73733.79 73733.79 2715.40 o 104.96568 10 0 0 63722.34 63722.34 2524.33 o 104.96568 1 1 0 1693261.13 1693261.13 13012.54 o 104.96568 2 1 0 45059.07 45059.07 2122.71 o 104.96568 3 1 0 361.39 361.39 190.10 o 104.96568 4 1 0 29501.25 29501.25 1717.59 o 104.96568 5 1 0 30.22 30.22 54.97 o 104.96568 6 1 0 557572.25 557572.25 7467.08 o 104.96568 7 1 0 34026.66 34026.66 1844.63 o 104.96568 8 1 0 52999.21 52999.21 2302.16 o 104.96568 9 1 0 63475.71 63475.71 2519.44 o 104.96568 10 1 0 27.00 27.00 51.96 o 104.96568 11 1 0 7756.88 7756.88 880.73 o 104.96568 0 2 0 119333.05 119333.05 3454.46 o 104.96568 1 2 0 860454.50 860454.50 9276.07 o 104.96568 2 2 0 11121.82 11121.82 1054.60 o 104.96568 3 2 0 17236.39 17236.39 1312.87 o 104.96568 4 2 0 887.96 887.96 297.99 o 104.96568 5 2 0 229771.09 229771.09 4793.44 o 104.96568 6 2 0 5272.88 5272.88 726.15 o 104.96568 7 2 0 173922.14 173922.14 4170.40 o 104.96568 8 2 0 18914.76 18914.76 1375.31 o 104.96568 9 2 0 7239.99 7239.99 850.88 o 104.96568 10 2 0 5868.82 5868.82 766.08 o 104.96568 11 2 0 64.67 64.67 80.42 o 104.96568 1 3 0 36793.81 36793.81 1918.17 o 104.96568 2 3 0 36904.09 36904.09 1921.04 o 104.96568 3 3 0 227242.53 227242.53 4767.00 o 104.96568 4 3 0 15689.81 15689.81 1252.59 o 104.96568 5 3 0 5906.85 5906.85 768.56 o 104.96568 6 3 0 1105.85 1105.85 332.54 o 104.96568 7 3 0 112057.55 112057.55 3347.50 o 104.96568 8 3 0 25411.62 25411.62 1594.10 o 104.96568 9 3 0 22595.28 22595.28 1503.17 o 104.96568 10 3 0 2778.56 2778.56 527.12 o 104.96568 11 3 0 44540.94 44540.94 2110.47 o 104.96568 0 4 0 252744.70 252744.70 5027.37 o 104.96568 1 4 0 187386.09 187386.09 4328.81 o 104.96568 2 4 0 1872275.00 1872275.00 13683.11 o 104.96568 3 4 0 234392.72 234392.72 4841.41 o 104.96568 4 4 0 297875.47 297875.47 5457.80 o 104.96568 5 4 0 267781.03 267781.03 5174.76 o 104.96568 6 4 0 50940.52 50940.52 2257.00 o 104.96568 7 4 0 68876.44 68876.44 2624.43 o 104.96568 8 4 0 63599.90 63599.90 2521.90 o 104.96568 9 4 0 17665.13 17665.13 1329.10 o 104.96568 10 4 0 28483.97 28483.97 1687.72 o 104.96568 11 4 0 5500.51 5500.51 741.65 o 104.96568 1 5 0 43128.92 43128.92 2076.75 o 104.96568 2 5 0 97760.67 97760.67 3126.67 o 104.96568 3 5 0 156890.59 156890.59 3960.94 o 104.96568 4 5 0 605612.50 605612.50 7782.11 o 104.96568 5 5 0 14732.24 14732.24 1213.76 o 104.96568 6 5 0 187156.53 187156.53 4326.16 o 104.96568 7 5 0 10960.12 10960.12 1046.91 o 104.96568 8 5 0 26371.10 26371.10 1623.92 o 104.96568 9 5 0 1242.71 1242.71 352.52 o 104.96568 10 5 0 17141.17 17141.17 1309.24 o 104.96568 11 5 0 3.10 3.10 17.61 o 104.96568 0 6 0 144013.56 144013.56 3794.91 o 104.96568 1 6 0 20843.75 20843.75 1443.74 o 104.96568 2 6 0 174297.41 174297.41 4174.89 o 104.96568 3 6 0 626876.69 626876.69 7917.55 o 104.96568 4 6 0 14664.55 14664.55 1210.97 o 104.96568 5 6 0 67562.93 67562.93 2599.29 o 104.96568 6 6 0 7947.29 7947.29 891.48 o 104.96568 7 6 0 2648.28 2648.28 514.61 o 104.96568 8 6 0 28363.12 28363.12 1684.14 o 104.96568 9 6 0 31233.24 31233.24 1767.29 o 104.96568 10 6 0 33359.82 33359.82 1826.47 o 104.96568 11 6 0 1017.24 1017.24 318.94 o 104.96568 1 7 0 253311.23 253311.23 5033.00 o 104.96568 2 7 0 46318.16 46318.16 2152.17 o 104.96568 3 7 0 288786.44 288786.44 5373.89 o 104.96568 4 7 0 89121.99 89121.99 2985.33 o 104.96568 5 7 0 5051.06 5051.06 710.71 o 104.96568 6 7 0 22825.76 22825.76 1510.82 o 104.96568 7 7 0 20220.92 20220.92 1422.00 o 104.96568 8 7 0 2328.29 2328.29 482.52 o 104.96568 9 7 0 60237.33 60237.33 2454.33 o 104.96568 10 7 0 2319.36 2319.36 481.60 o 104.96568 11 7 0 26870.52 26870.52 1639.22 o 104.96568 0 8 0 55259.73 55259.73 2350.74 o 104.96568 1 8 0 84921.81 84921.81 2914.13 o 104.96568 2 8 0 183432.00 183432.00 4282.90 o 104.96568 3 8 0 422491.31 422491.31 6499.93 o 104.96568 4 8 0 15153.49 15153.49 1231.00 o 104.96568 5 8 0 231413.31 231413.31 4810.54 o 104.96568 6 8 0 15495.00 15495.00 1244.79 o 104.96568 7 8 0 86251.48 86251.48 2936.86 o 104.96568 8 8 0 5294.37 5294.37 727.62 o 104.96568 9 8 0 23486.67 23486.67 1532.54 o 104.96568 10 8 0 8964.66 8964.66 946.82 o 104.96568 1 9 0 261851.38 261851.38 5117.14 o 104.96568 2 9 0 101523.22 101523.22 3186.27 o 104.96568 3 9 0 129660.24 129660.24 3600.84 o 104.96568 4 9 0 107328.84 107328.84 3276.11 o 104.96568 5 9 0 726.00 726.00 269.44 o 104.96568 6 9 0 40275.94 40275.94 2006.89 o 104.96568 7 9 0 294.73 294.73 171.68 o 104.96568 8 9 0 36768.66 36768.66 1917.52 o 104.96568 9 9 0 13854.72 13854.72 1177.06 o 104.96568 10 9 0 925.78 925.78 304.27 o 104.96568 0 10 0 381388.06 381388.06 6175.66 o 104.96568 1 10 0 1555.35 1555.35 394.38 o 104.96568 2 10 0 205305.55 205305.55 4531.07 o 104.96568 3 10 0 7187.52 7187.52 847.79 o 104.96568 4 10 0 67060.13 67060.13 2589.60 o 104.96568 5 10 0 53.07 53.07 72.85 o 104.96568 6 10 0 4133.57 4133.57 642.93 o 104.96568 7 10 0 1711.46 1711.46 413.70 o 104.96568 8 10 0 18196.53 18196.53 1348.95 o 104.96568 9 10 0 20.41 20.41 45.18 o 104.96568 10 10 0 22856.04 22856.04 1511.82 o 104.96568 1 11 0 59400.27 59400.27 2437.22 o 104.96568 2 11 0 95745.11 95745.11 3094.27 o 104.96568 3 11 0 83747.18 83747.18 2893.91 o 104.96568 4 11 0 112525.43 112525.43 3354.48 o 104.96568 5 11 0 2511.88 2511.88 501.19 o 104.96568 6 11 0 39954.16 39954.16 1998.85 o 104.96568 7 11 0 5647.67 5647.67 751.51 o 104.96568 8 11 0 19269.88 19269.88 1388.16 o 104.96568 9 11 0 12596.86 12596.86 1122.36 o 104.96568 10 11 0 7.13 7.13 26.70 o 104.96568 0 12 0 226.26 226.26 150.42 o 104.96568 1 12 0 40542.53 40542.53 2013.52 o 104.96568 2 12 0 12379.72 12379.72 1112.64 o 104.96568 3 12 0 29372.88 29372.88 1713.85 o 104.96568 4 12 0 3967.95 3967.95 629.92 o 104.96568 5 12 0 136022.72 136022.72 3688.13 o 104.96568 6 12 0 141.50 141.50 118.95 o 104.96568 7 12 0 50164.84 50164.84 2239.75 o 104.96568 8 12 0 2348.18 2348.18 484.58 o 104.96568 9 12 0 4469.89 4469.89 668.57 o 104.96568 1 13 0 184327.66 184327.66 4293.34 o 104.96568 2 13 0 15260.53 15260.53 1235.34 o 104.96568 3 13 0 49875.45 49875.45 2233.28 o 104.96568 4 13 0 92.65 92.65 96.25 o 104.96568 5 13 0 3168.23 3168.23 562.87 o 104.96568 6 13 0 7218.83 7218.83 849.64 o 104.96568 7 13 0 28867.03 28867.03 1699.03 o 104.96568 8 13 0 1758.84 1758.84 419.38 o 104.96568 9 13 0 28842.64 28842.64 1698.31 o 104.96568 0 14 0 334274.50 334274.50 5781.65 o 104.96568 1 14 0 6704.16 6704.16 818.79 o 104.96568 2 14 0 61762.10 61762.10 2485.20 o 104.96568 3 14 0 69994.57 69994.57 2645.65 o 104.96568 4 14 0 24514.23 24514.23 1565.70 o 104.96568 5 14 0 52220.55 52220.55 2285.18 o 104.96568 6 14 0 1998.52 1998.52 447.05 o 104.96568 7 14 0 2175.94 2175.94 466.47 o 104.96568 8 14 0 22637.89 22637.89 1504.59 o 104.96568 9 14 0 4555.41 4555.41 674.94 o 104.96568 1 15 0 59988.75 59988.75 2449.26 o 104.96568 2 15 0 139472.03 139472.03 3734.60 o 104.96568 3 15 0 1305.00 1305.00 361.25 o 104.96568 4 15 0 110556.66 110556.66 3325.01 o 104.96568 5 15 0 1953.42 1953.42 441.97 o 104.96568 6 15 0 64373.50 64373.50 2537.19 o 104.96568 7 15 0 475.89 475.89 218.15 o 104.96568 8 15 0 11552.75 11552.75 1074.84 o 104.96568 0 16 0 535.71 535.71 231.46 o 104.96568 1 16 0 16021.43 16021.43 1265.76 o 104.96568 2 16 0 24368.47 24368.47 1561.04 o 104.96568 3 16 0 34184.51 34184.51 1848.91 o 104.96568 4 16 0 38418.79 38418.79 1960.07 o 104.96568 5 16 0 3266.84 3266.84 571.56 o 104.96568 6 16 0 98.37 98.37 99.18 o 104.96568 7 16 0 31750.01 31750.01 1781.85 o 104.96568 8 16 0 127.00 127.00 112.69 o 104.96568 1 17 0 27126.73 27126.73 1647.02 o 104.96568 2 17 0 6455.20 6455.20 803.44 o 104.96568 3 17 0 17035.14 17035.14 1305.19 o 104.96568 4 17 0 11228.64 11228.64 1059.65 o 104.96568 5 17 0 155.77 155.77 124.81 o 104.96568 6 17 0 1726.42 1726.42 415.50 o 104.96568 7 17 0 1081.67 1081.67 328.89 o 104.96568 0 18 0 9442.75 9442.75 971.74 o 104.96568 1 18 0 1767.90 1767.90 420.46 o 104.96568 2 18 0 1523.04 1523.04 390.26 o 104.96568 3 18 0 17688.74 17688.74 1329.99 o 104.96568 4 18 0 5025.64 5025.64 708.92 o 104.96568 5 18 0 27111.76 27111.76 1646.57 o 104.96568 6 18 0 586.57 586.57 242.19 o 104.96568 1 19 0 27273.51 27273.51 1651.47 o 104.96568 2 19 0 472.55 472.55 217.38 o 104.96568 3 19 0 662.27 662.27 257.35 o 104.96568 4 19 0 54281.91 54281.91 2329.85 o 104.96568 5 19 0 1680.96 1680.96 410.00 o 104.96568 6 19 0 26031.22 26031.22 1613.42 o 104.96568 0 20 0 54879.21 54879.21 2342.63 o 104.96568 1 20 0 6646.12 6646.12 815.24 o 104.96568 2 20 0 9612.69 9612.69 980.44 o 104.96568 3 20 0 4312.64 4312.64 656.71 o 104.96568 4 20 0 1046.12 1046.12 323.44 o 104.96568 5 20 0 2612.24 2612.24 511.10 o 104.96568 1 21 0 7374.82 7374.82 858.77 o 104.96568 2 21 0 1301.16 1301.16 360.72 o 104.96568 3 21 0 11293.10 11293.10 1062.69 o 104.96568 0 22 0 8597.54 8597.54 927.23 o 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104079.08 3226.13 o 104.96568 -1 1 1 6977.14 6977.14 835.29 o 104.96568 0 1 1 1309139.63 1309139.63 11441.76 o 104.96568 1 1 1 29007.40 29007.40 1703.16 o 104.96568 2 1 1 33089.74 33089.74 1819.06 o 104.96568 3 1 1 50523.37 50523.37 2247.74 o 104.96568 4 1 1 3318.24 3318.24 576.04 o 104.96568 5 1 1 280375.63 280375.63 5295.05 o 104.96568 6 1 1 132.18 132.18 114.97 o 104.96568 7 1 1 411230.66 411230.66 6412.73 o 104.96568 8 1 1 185275.03 185275.03 4304.36 o 104.96568 9 1 1 1982.27 1982.27 445.23 o 104.96568 10 1 1 26640.00 26640.00 1632.18 o 104.96568 11 1 1 265.07 265.07 162.81 o 104.96568 -11 2 1 31808.08 31808.08 1783.48 o 104.96568 -10 2 1 859.16 859.16 293.11 o 104.96568 -9 2 1 610.82 610.82 247.15 o 104.96568 -8 2 1 163791.48 163791.48 4047.12 o 104.96568 -7 2 1 40618.45 40618.45 2015.40 o 104.96568 -6 2 1 436331.78 436331.78 6605.54 o 104.96568 -5 2 1 69777.58 69777.58 2641.54 o 104.96568 -4 2 1 400819.41 400819.41 6331.03 o 104.96568 -3 2 1 124245.10 124245.10 3524.84 o 104.96568 -2 2 1 50082.05 50082.05 2237.90 o 104.96568 -1 2 1 339076.44 339076.44 5823.03 o 104.96568 0 2 1 27654.43 27654.43 1662.96 o 104.96568 1 2 1 539980.19 539980.19 7348.33 o 104.96568 2 2 1 206797.56 206797.56 4547.50 o 104.96568 3 2 1 6957.94 6957.94 834.14 o 104.96568 4 2 1 243369.80 243369.80 4933.25 o 104.96568 5 2 1 6680.01 6680.01 817.31 o 104.96568 6 2 1 331649.97 331649.97 5758.91 o 104.96568 7 2 1 4942.43 4942.43 703.02 o 104.96568 8 2 1 43166.50 43166.50 2077.66 o 104.96568 9 2 1 9803.31 9803.31 990.12 o 104.96568 10 2 1 3679.15 3679.15 606.56 o 104.96568 11 2 1 611.13 611.13 247.21 o 104.96568 -11 3 1 103.11 103.11 101.54 o 104.96568 -10 3 1 77563.94 77563.94 2785.03 o 104.96568 -9 3 1 2003.05 2003.05 447.55 o 104.96568 -8 3 1 23433.37 23433.37 1530.80 o 104.96568 -7 3 1 1015.09 1015.09 318.61 o 104.96568 -6 3 1 4909.75 4909.75 700.70 o 104.96568 -5 3 1 7352.64 7352.64 857.48 o 104.96568 -4 3 1 1586.65 1586.65 398.33 o 104.96568 -3 3 1 7612.23 7612.23 872.48 o 104.96568 -2 3 1 998843.63 998843.63 9994.22 o 104.96568 -1 3 1 1631733.13 1631733.13 12773.93 o 104.96568 0 3 1 1302625.00 1302625.00 11413.26 o 104.96568 1 3 1 49246.68 49246.68 2219.16 o 104.96568 2 3 1 807343.44 807343.44 8985.23 o 104.96568 3 3 1 264.30 264.30 162.57 o 104.96568 4 3 1 14940.50 14940.50 1222.31 o 104.96568 5 3 1 2133.92 2133.92 461.94 o 104.96568 6 3 1 45379.21 45379.21 2130.24 o 104.96568 7 3 1 222.90 222.90 149.30 o 104.96568 8 3 1 15379.82 15379.82 1240.15 o 104.96568 9 3 1 1819.17 1819.17 426.52 o 104.96568 10 3 1 18818.15 18818.15 1371.79 o 104.96568 11 3 1 1780.48 1780.48 421.96 o 104.96568 -11 4 1 44193.29 44193.29 2102.22 o 104.96568 -10 4 1 5092.28 5092.28 713.60 o 104.96568 -9 4 1 74643.63 74643.63 2732.10 o 104.96568 -8 4 1 27562.77 27562.77 1660.20 o 104.96568 -7 4 1 81001.93 81001.93 2846.08 o 104.96568 -6 4 1 140339.77 140339.77 3746.19 o 104.96568 -5 4 1 133902.75 133902.75 3659.27 o 104.96568 -4 4 1 897442.88 897442.88 9473.35 o 104.96568 -3 4 1 879666.63 879666.63 9379.05 o 104.96568 -2 4 1 201.73 201.73 142.03 o 104.96568 -1 4 1 154932.11 154932.11 3936.14 o 104.96568 0 4 1 441449.50 441449.50 6644.17 o 104.96568 1 4 1 602805.31 602805.31 7764.05 o 104.96568 2 4 1 32340.24 32340.24 1798.34 o 104.96568 3 4 1 84789.38 84789.38 2911.86 o 104.96568 4 4 1 33903.18 33903.18 1841.28 o 104.96568 5 4 1 70399.59 70399.59 2653.29 o 104.96568 6 4 1 195188.69 195188.69 4418.02 o 104.96568 7 4 1 17305.43 17305.43 1315.50 o 104.96568 8 4 1 1582.34 1582.34 397.79 o 104.96568 9 4 1 11418.06 11418.06 1068.55 o 104.96568 10 4 1 2342.20 2342.20 483.96 o 104.96568 11 4 1 21954.64 21954.64 1481.71 o 104.96568 -11 5 1 3399.07 3399.07 583.02 o 104.96568 -10 5 1 211.94 211.94 145.58 o 104.96568 -9 5 1 36476.14 36476.14 1909.87 o 104.96568 -8 5 1 17584.25 17584.25 1326.06 o 104.96568 -7 5 1 49417.25 49417.25 2223.00 o 104.96568 -6 5 1 1342.57 1342.57 366.41 o 104.96568 -5 5 1 308889.75 308889.75 5557.79 o 104.96568 -4 5 1 89305.38 89305.38 2988.40 o 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