Crystallography Open Database

Information card for entry 4001683

Preview

Coordinates	4001683.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Ge O8 Si3
Calculated formula	Ge1.0155 O8 Si2.9845
Title of publication	Intergrown New Zeolite Beta Polymorphs with Interconnected 12-Ring Channels Solved by Combining Electron Crystallography and Single-Crystal X-ray Diffraction
Authors of publication	Yu, Zheng-Bao; Han, Yu; Zhao, Lan; Huang, Shiliang; Zheng, Qi-Yu; Lin, Shuangzheng; Córdova, Armando; Zou, Xiaodong; Sun, Junliang
Journal of publication	Chemistry of Materials
Year of publication	2012
Journal volume	24
Journal issue	19
Pages of publication	3701
a	12.59 ± 0.002 Å
b	12.852 ± 0.002 Å
c	13.984 ± 0.004 Å
α	90°
β	107.63 ± 0.02°
γ	90°
Cell volume	2156.4 ± 0.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	3
Space group number	10
Hermann-Mauguin space group symbol	P 1 2/m 1
Hall space group symbol	-P 2y
Residual factor for all reflections	0.1595
Residual factor for significantly intense reflections	0.1139
Weighted residual factors for significantly intense reflections	0.2917
Weighted residual factors for all reflections included in the refinement	0.3195
Goodness-of-fit parameter for all reflections included in the refinement	0.974
Diffraction radiation wavelength	0.6889 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178377 (current)	2016-03-21	cif/4/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/00.	4001683.cif
107967	2014-03-25	cif/4 Changing the entity to the proper non-English character for many entries in subdir 4	4001683.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4001683.cif
71985	2013-01-21	cif/ Adding structures of 4001683 via cif-deposit CGI script.	4001683.cif