#------------------------------------------------------------------------------ #$Date: 2020-11-22 01:30:52 +0200 (Sun, 22 Nov 2020) $ #$Revision: 259219 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/00/38/4003828.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4003828 loop_ _publ_author_name 'Zuluaga, Andr\'es Reyes' 'Brock, Aidan J.' 'Pfrunder, Michael C.' 'Phonsri, Wasinee' 'Murray, Keith S.' 'Harding, Phimphaka' 'Micallef, Aaron S.' 'Mullen, Kathleen M.' 'Clegg, Jack K.' 'Harding, David J.' 'McMurtrie, John C.' _publ_section_title ; Three-Way Switchable Single-Crystal-to-Single-Crystal Solvatomorphic Spin Crossover in a Molecular Cocrystal ; _journal_name_full 'Chemistry of Materials' _journal_paper_doi 10.1021/acs.chemmater.0c03396 _journal_year 2020 _chemical_formula_moiety 'C6 F3 I3, C34 H26 Fe N4 O4, C N S' _chemical_formula_sum 'C41 H26 F3 Fe I3 N5 O4 S' _chemical_formula_weight 1178.28 _chemical_name_systematic 'bis(4-methoxy-2-(((quinolin-8-yl)imino)methyl)phenolato)-iron(iii) thiocyanate (2,4,5-tetrafluoro-1,3,5-triiodobenzene)' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2020-04-03 _audit_creation_method ; Olex2 1.3 (compiled 2020.02.04 svn.rd84adfe8 for OlexSys, GUI svn.r6032) ; _cell_angle_alpha 82.654(2) _cell_angle_beta 77.122(2) _cell_angle_gamma 89.231(2) _cell_formula_units_Z 2 _cell_length_a 11.8320(2) _cell_length_b 12.3306(4) _cell_length_c 13.9763(4) _cell_measurement_reflns_used 24889 _cell_measurement_temperature 149.8(3) _cell_measurement_theta_max 32.6040 _cell_measurement_theta_min 2.3890 _cell_volume 1971.24(9) _computing_cell_refinement 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 149.8(3) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 5.8140 _diffrn_detector_type 'Pilatus 300K' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -17.00 34.00 0.50 1.00 -- 7.84 93.00-131.00 102 2 \w -13.00 38.00 0.50 1.00 -- 7.84 -93.00 117.00 102 3 \w -43.00 -16.00 0.50 1.00 -- -9.41 93.00-131.00 54 4 \w -42.00 -16.00 0.50 1.00 -- 7.84 -57.00 -30.00 52 5 \w 0.00 37.00 0.50 1.00 -- 7.84 -99.00 -90.00 74 6 \w -59.00 22.00 0.50 1.00 -- 7.84 -57.00 60.00 162 7 \w -18.00 75.00 0.50 1.00 -- 7.84 77.00 0.00 186 8 \w 5.00 36.00 0.50 1.00 -- 7.84 -99.00 0.00 62 9 \w -7.00 79.00 0.50 1.00 -- 7.84 57.00 60.00 172 10 \w 3.00 40.00 0.50 1.00 -- 7.84 -99.00-180.00 74 11 \w -61.00 -36.00 0.50 1.00 -- 7.84 153.00-168.43 50 12 \w -26.00 68.00 0.50 1.00 -- -9.41 37.00 150.00 188 13 \w -30.00 49.00 0.50 1.00 -- -9.41 77.00 150.00 158 14 \w 6.00 31.00 0.50 1.00 -- -9.41 93.00-131.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 300K' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0272779000 _diffrn_orient_matrix_UB_12 -0.0258394000 _diffrn_orient_matrix_UB_13 -0.0414965000 _diffrn_orient_matrix_UB_21 -0.0202098000 _diffrn_orient_matrix_UB_22 -0.0516395000 _diffrn_orient_matrix_UB_23 0.0263485000 _diffrn_orient_matrix_UB_31 -0.0512830000 _diffrn_orient_matrix_UB_32 0.0055209000 _diffrn_orient_matrix_UB_33 -0.0184175000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0882 _diffrn_reflns_av_unetI/netI 0.0557 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 48483 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.281 _diffrn_reflns_theta_min 2.050 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 2.849 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.12466 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.61a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'dark brown' _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 1.985 _exptl_crystal_description block _exptl_crystal_F_000 1134 _exptl_crystal_preparation 'Combined equal ratios of starting materials' _exptl_crystal_recrystallization_method 'Slow evaporation of the solvent' _exptl_crystal_size_max 2 _exptl_crystal_size_mid 1 _exptl_crystal_size_min 1 _refine_diff_density_max 1.642 _refine_diff_density_min -1.329 _refine_diff_density_rms 0.160 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.100 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 525 _refine_ls_number_reflns 9794 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.100 _refine_ls_R_factor_all 0.0586 _refine_ls_R_factor_gt 0.0448 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0597P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1140 _refine_ls_wR_factor_ref 0.1226 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7648 _reflns_number_total 9794 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cm0c03396_si_006.cif _cod_data_source_block sjcm19ar19a_16_150_00 _cod_database_code 4003828 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C40 H40 N5 O2 Fe S I3 F3' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.163 _shelx_estimated_absorpt_t_min 0.070 _reflns_odcompleteness_completeness 84.09 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 33.35 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C25(H25), C19(H19), C23(H23), C8(H8), C6(H6), C27(H27), C20(H20), C2(H2), C28(H28), C12(H12), C33(H33), C16(H16), C32(H32), C10(H10), C3(H3), C15(H15), C11(H11), C29(H29), C14(H14), C31(H31) 2.b Idealised Me refined as rotating group: C5(H5A,H5B,H5C), C22(H22A,H22B,H22C) ; _shelx_res_file ; TITL sjcm19ar19a_16_150_00_a.res in P-1 sjcm19ar19a_16_150_00.res created by SHELXL-2018/3 at 10:49:28 on 03-Apr-2020 REM Old TITL Sjcm19ar19a_16_150_00 in P-1 REM SHELXT solution in P-1: R1 0.104, Rweak 0.005, Alpha 0.046 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C41 N6 O5 F S Fe I3 CELL 0.71073 11.832 12.3306 13.9763 82.654 77.122 89.231 ZERR 2 0.0002 0.0004 0.0004 0.002 0.002 0.002 LATT 1 SFAC C H F Fe I N O S UNIT 82 52 6 2 6 10 8 2 L.S. 15 PLAN 5 SIZE 1 1 2 TEMP -123 CONF HTAB BOND list 4 MORE -1 BOND $H fmap 2 acta SHEL 50 0.75 REM REM REM WGHT 0.059700 FVAR 0.17776 I3 5 -0.083174 0.236044 0.386216 11.00000 0.02345 0.03474 = 0.03197 -0.00742 -0.00701 0.00417 I1 5 0.284214 0.055042 0.606065 11.00000 0.03059 0.02950 = 0.04938 -0.00247 -0.01488 0.00504 I2 5 -0.008834 0.429322 0.743938 11.00000 0.04742 0.03731 = 0.04253 -0.01649 -0.00669 0.00257 FE1 4 0.514729 0.364520 0.789542 11.00000 0.01763 0.01902 = 0.01681 -0.00412 -0.00360 0.00237 S1 8 -0.202250 0.289566 0.197076 11.00000 0.04733 0.04736 = 0.03093 -0.01117 -0.01222 0.01855 F3 3 0.118802 0.087244 0.451345 11.00000 0.03823 0.03232 = 0.03493 -0.00992 -0.01001 0.01068 F2 3 -0.105723 0.384179 0.558422 11.00000 0.03525 0.04042 = 0.04335 -0.01224 -0.01510 0.01572 O1 7 0.629401 0.472489 0.734898 11.00000 0.02255 0.02439 = 0.01854 -0.00525 -0.00388 0.00148 O3 7 0.591951 0.310464 0.888923 11.00000 0.02136 0.02610 = 0.01853 -0.00619 -0.00521 0.00432 F1 3 0.187509 0.253063 0.717580 11.00000 0.04934 0.03581 = 0.04051 -0.00584 -0.02537 0.00206 O4 7 0.969603 0.039634 0.875423 11.00000 0.02591 0.03505 = 0.03693 -0.00929 -0.01600 0.01068 O2 7 0.694211 0.875887 0.846526 11.00000 0.03077 0.02616 = 0.03814 -0.00913 0.00096 -0.00842 N3 6 0.596511 0.272058 0.695132 11.00000 0.01733 0.01757 = 0.01779 -0.00165 -0.00227 0.00230 N4 6 0.432303 0.410682 0.682163 11.00000 0.01952 0.02472 = 0.01889 -0.00167 -0.00548 0.00000 N1 6 0.422863 0.454372 0.880572 11.00000 0.01801 0.01896 = 0.01775 0.00098 -0.00090 0.00259 N2 6 0.385663 0.257734 0.847783 11.00000 0.02124 0.01995 = 0.01728 -0.00474 -0.00782 0.00142 C25 1 0.687098 0.214962 0.704796 11.00000 0.01892 0.02552 = 0.01829 -0.00746 -0.00239 0.00435 AFIX 43 H25 2 0.725085 0.179735 0.650055 11.00000 -1.20000 AFIX 0 C34 1 0.465184 0.353593 0.602871 11.00000 0.02078 0.01881 = 0.01632 -0.00250 -0.00139 -0.00262 C19 1 0.737764 0.224293 0.958820 11.00000 0.02550 0.02464 = 0.01787 -0.00541 -0.00707 0.00249 AFIX 43 H19 2 0.707425 0.255109 1.018034 11.00000 -1.20000 AFIX 0 C23 1 0.830428 0.130754 0.788500 11.00000 0.02026 0.02289 = 0.02280 -0.00366 -0.00194 0.00358 AFIX 43 H23 2 0.862186 0.098870 0.730139 11.00000 -1.20000 AFIX 0 C26 1 0.553672 0.276337 0.607896 11.00000 0.02069 0.02743 = 0.01410 -0.00333 -0.00364 0.00242 C8 1 0.456889 0.547910 0.900255 11.00000 0.02286 0.01965 = 0.01797 -0.00300 -0.00320 0.00081 AFIX 43 H8 2 0.408254 0.580536 0.952211 11.00000 -1.20000 AFIX 0 C17 1 0.297329 0.300647 0.912269 11.00000 0.02184 0.02251 = 0.01733 -0.00398 -0.00623 0.00240 C18 1 0.684675 0.248774 0.877566 11.00000 0.02075 0.01879 = 0.02006 -0.00317 -0.00635 -0.00037 C24 1 0.734287 0.200766 0.790825 11.00000 0.02010 0.02221 = 0.01951 -0.00526 -0.00450 0.00335 C7 1 0.561606 0.604383 0.849409 11.00000 0.01868 0.02298 = 0.02281 -0.00297 -0.00587 0.00025 C9 1 0.312372 0.409050 0.929974 11.00000 0.01806 0.02082 = 0.01975 -0.00320 -0.00361 -0.00103 C6 1 0.578847 0.707578 0.877536 11.00000 0.02177 0.02243 = 0.02319 -0.00102 -0.00466 0.00067 AFIX 43 H6 2 0.524908 0.732836 0.930902 11.00000 -1.20000 AFIX 0 C13 1 0.194334 0.240546 0.959078 11.00000 0.02220 0.02648 = 0.02064 -0.00241 -0.00652 -0.00284 C21 1 0.878246 0.108444 0.869628 11.00000 0.01804 0.02429 = 0.02933 -0.00729 -0.00774 0.00102 C4 1 0.673314 0.772106 0.828240 11.00000 0.02406 0.02278 = 0.02661 -0.00722 -0.00784 -0.00184 C38 1 0.039412 0.320030 0.641250 11.00000 0.03229 0.02364 = 0.03030 -0.00655 -0.00250 -0.00205 C27 1 0.588212 0.213272 0.531758 11.00000 0.02660 0.02697 = 0.02378 -0.00591 -0.00659 0.00366 AFIX 43 H27 2 0.645345 0.158979 0.535488 11.00000 -1.20000 AFIX 0 C20 1 0.831291 0.157693 0.954601 11.00000 0.02576 0.03097 = 0.02203 -0.00775 -0.01118 -0.00266 AFIX 43 H20 2 0.865350 0.144378 1.010374 11.00000 -1.20000 AFIX 0 C2 1 0.741575 0.630055 0.726374 11.00000 0.02061 0.03228 = 0.02036 -0.00503 -0.00258 0.00033 AFIX 43 H2 2 0.799312 0.604151 0.675948 11.00000 -1.20000 AFIX 0 C1 1 0.642082 0.563506 0.771721 11.00000 0.01949 0.02596 = 0.01802 -0.00306 -0.00799 0.00023 C28 1 0.538524 0.229915 0.449260 11.00000 0.03709 0.02925 = 0.02067 -0.00540 -0.00793 0.00261 AFIX 43 H28 2 0.562875 0.186556 0.397086 11.00000 -1.20000 AFIX 0 N5 6 -0.376685 0.126678 0.229928 11.00000 0.06031 0.04954 = 0.03986 -0.01882 -0.01420 0.01719 C12 1 0.104780 0.293505 1.020356 11.00000 0.01993 0.02859 = 0.03183 -0.00731 0.00059 -0.00488 AFIX 43 H12 2 0.034304 0.255546 1.051878 11.00000 -1.20000 AFIX 0 C33 1 0.353050 0.486898 0.678941 11.00000 0.02339 0.02294 = 0.02503 -0.00229 -0.00576 0.00291 AFIX 43 H33 2 0.330186 0.527048 0.733583 11.00000 -1.20000 AFIX 0 C36 1 0.157293 0.168763 0.584361 11.00000 0.02405 0.02897 = 0.02946 -0.00164 -0.00810 0.00161 C41 1 0.093180 0.164195 0.512425 11.00000 0.03025 0.02313 = 0.02664 -0.00331 -0.00603 0.00399 C16 1 0.375760 0.155204 0.832256 11.00000 0.02750 0.02407 = 0.02159 -0.00591 -0.00615 0.00458 AFIX 43 H16 2 0.437183 0.125062 0.787827 11.00000 -1.20000 AFIX 0 C32 1 0.301174 0.510658 0.596883 11.00000 0.02606 0.02720 = 0.02942 0.00220 -0.00791 0.00543 AFIX 43 H32 2 0.244583 0.566072 0.597150 11.00000 -1.20000 AFIX 0 C30 1 0.416525 0.371217 0.518483 11.00000 0.02130 0.02913 = 0.02103 -0.00107 -0.00333 -0.00117 C10 1 0.223439 0.459163 0.989592 11.00000 0.02295 0.02388 = 0.02925 -0.00865 -0.00154 0.00060 AFIX 43 H10 2 0.231727 0.532813 1.000557 11.00000 -1.20000 AFIX 0 C3 1 0.755787 0.730313 0.753808 11.00000 0.01963 0.03123 = 0.02727 -0.00084 -0.00440 -0.00699 AFIX 43 H3 2 0.823095 0.772900 0.721795 11.00000 -1.20000 AFIX 0 C39 1 -0.020029 0.312944 0.567403 11.00000 0.02588 0.02795 = 0.03648 -0.00333 -0.00543 0.00417 C15 1 0.279187 0.089254 0.878164 11.00000 0.03183 0.02106 = 0.03066 -0.00417 -0.01140 -0.00630 AFIX 43 H15 2 0.276599 0.015471 0.865721 11.00000 -1.20000 AFIX 0 C11 1 0.120395 0.399681 1.033873 11.00000 0.02573 0.03397 = 0.03067 -0.01195 0.00095 0.00114 AFIX 43 H11 2 0.059393 0.434587 1.074686 11.00000 -1.20000 AFIX 0 C29 1 0.455716 0.307095 0.441833 11.00000 0.02980 0.03478 = 0.02183 0.00052 -0.01032 -0.00161 AFIX 43 H29 2 0.424470 0.317406 0.384383 11.00000 -1.20000 AFIX 0 C37 1 0.127692 0.247139 0.647187 11.00000 0.03161 0.02385 = 0.02972 0.00447 -0.01167 0.00105 C35 1 -0.304489 0.193990 0.216517 11.00000 0.05716 0.04046 = 0.02296 -0.01593 -0.01829 0.03264 C40 1 0.005104 0.236079 0.500980 11.00000 0.02661 0.03112 = 0.02937 -0.00119 -0.00678 -0.00070 C14 1 0.188790 0.130283 0.940646 11.00000 0.02830 0.02664 = 0.02921 -0.00163 -0.00623 -0.00813 AFIX 43 H14 2 0.122585 0.085749 0.971682 11.00000 -1.20000 AFIX 0 C31 1 0.332019 0.454433 0.517529 11.00000 0.03019 0.03084 = 0.02504 0.00154 -0.01081 0.00430 AFIX 43 H31 2 0.297587 0.470518 0.462193 11.00000 -1.20000 AFIX 0 C5 1 0.600232 0.927790 0.905144 11.00000 0.03650 0.02033 = 0.03664 -0.00708 -0.00677 -0.00510 AFIX 137 H5A 2 0.532817 0.928283 0.875144 11.00000 -1.50000 H5B 2 0.622713 1.003143 0.908626 11.00000 -1.50000 H5C 2 0.580464 0.887678 0.972020 11.00000 -1.50000 AFIX 0 C22 1 0.997633 -0.031288 0.801435 11.00000 0.03041 0.03513 = 0.03197 -0.00397 -0.00762 0.01182 AFIX 137 H22A 2 1.025212 0.012051 0.736686 11.00000 -1.50000 H22B 2 0.928487 -0.073707 0.800594 11.00000 -1.50000 H22C 2 1.058552 -0.081175 0.815942 11.00000 -1.50000 AFIX 0 HKLF 4 REM sjcm19ar19a_16_150_00_a.res in P-1 REM wR2 = 0.1226, GooF = S = 1.100, Restrained GooF = 1.100 for all data REM R1 = 0.0448 for 7648 Fo > 4sig(Fo) and 0.0586 for all 9794 data REM 525 parameters refined using 0 restraints END WGHT 0.0597 0.0000 REM Instructions for potential hydrogen bonds EQIV $1 x+1, y, z+1 HTAB C19 S1_$1 EQIV $2 -x+1, -y+1, -z+2 HTAB C6 O3_$2 EQIV $3 x+1, y, z HTAB C2 I2_$3 EQIV $4 -x, -y+1, -z+1 HTAB C33 S1_$4 HTAB C33 N1 HTAB C16 N3 HTAB C32 I3_$4 EQIV $5 -x+1, -y+1, -z+1 HTAB C3 I3_$5 EQIV $6 -x, -y, -z+1 HTAB C15 N5_$6 HTAB C22 I1_$3 REM Highest difference peak 1.642, deepest hole -1.329, 1-sigma level 0.160 Q1 1 0.3129 0.0654 0.5428 11.00000 0.05 1.64 Q2 1 -0.0632 0.3391 0.3408 11.00000 0.05 1.29 Q3 1 -0.1179 0.2191 0.4531 11.00000 0.05 1.01 Q4 1 0.3007 0.1546 0.5643 11.00000 0.05 0.99 Q5 1 0.0230 0.4464 0.6812 11.00000 0.05 0.94 ; _shelx_res_checksum 44783 _shelx_hkl_file ; 0 0 2 268.45 13.13 0 0 -2 245.25 13.04 0 0 -3 36.83 3.16 0 0 3 31.19 2.95 0 0 -4 58.16 4.12 0 0 4 67.86 4.96 0 0 -4 57.97 4.80 0 0 4 51.15 4.45 0 0 -5 624.08 32.39 0 0 5 751.26 33.95 0 0 -5 670.29 33.78 0 0 5 640.51 33.52 0 0 -6 669.90 33.73 0 0 6 742.77 35.34 0 0 6 671.01 35.24 0 0 -6 662.85 35.09 0 0 6 667.49 35.08 0 0 7 0.78 1.01 0 0 7 1.11 1.29 0 0 -7 0.54 1.21 0 0 -7 1.40 0.90 0 0 7 1.33 1.45 0 0 -8 483.56 22.72 0 0 -8 448.48 22.47 0 0 -8 410.99 23.40 0 0 -8 403.80 25.39 0 0 8 446.25 25.29 0 0 -8 447.65 25.36 0 0 8 430.12 24.98 0 0 8 397.93 25.02 0 0 -9 162.67 9.28 0 0 -9 154.56 12.58 0 0 -9 179.51 12.67 0 0 9 179.09 12.62 0 0 9 168.53 12.73 0 0 10 110.11 9.27 0 0 10 109.82 10.34 0 0 -10 106.13 10.45 0 0 10 114.06 10.15 0 0 -10 120.29 10.27 0 0 -11 12.71 1.97 0 0 11 7.48 2.74 0 0 -11 13.09 1.91 0 0 11 17.39 3.54 0 0 11 11.31 3.78 0 0 -11 13.18 2.87 0 0 -11 18.11 4.43 0 0 11 15.81 3.89 0 0 -11 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107.26 0 -4 -3 2311.61 107.85 0 -4 -3 2300.47 108.29 0 4 4 678.04 34.25 0 -4 -4 674.30 34.80 0 -4 -4 724.15 35.35 0 4 4 659.21 32.65 0 -4 -5 349.79 20.16 0 -4 -5 361.52 20.00 0 4 5 358.74 19.57 0 4 5 349.90 19.77 0 4 5 331.67 17.05 0 -4 -6 192.32 12.83 0 4 6 165.07 12.00 0 4 6 177.74 11.94 0 4 7 92.89 8.28 0 -4 -7 101.32 8.76 0 4 7 80.57 7.97 0 4 7 97.51 8.18 0 -4 -8 253.65 17.22 0 4 8 245.63 17.04 0 4 8 240.61 16.98 0 4 8 270.50 16.95 0 4 9 564.95 30.51 0 -4 -9 516.47 30.28 0 4 9 474.99 29.91 0 4 9 496.89 29.45 0 4 10 83.81 8.85 0 4 10 82.07 8.83 0 -4 -10 80.05 9.02 0 4 11 249.33 17.99 0 -4 -11 221.35 17.66 0 4 11 242.54 17.87 0 4 12 205.01 17.03 0 -4 -12 220.55 17.78 0 4 12 228.17 17.48 0 4 13 1.79 2.53 0 4 13 5.08 3.15 0 -4 -13 5.07 3.18 0 4 14 8.51 4.02 0 4 14 8.53 3.82 0 4 15 1.46 3.51 0 4 15 2.59 2.97 0 4 15 0.72 2.90 0 4 15 0.66 2.90 0 4 15 2.19 2.94 0 4 16 11.80 4.99 0 4 16 17.25 5.43 0 4 16 18.99 5.78 0 4 16 10.44 4.92 0 4 16 16.44 5.15 0 4 17 37.92 8.56 0 4 17 54.21 9.77 0 4 18 15.76 5.35 0 4 18 6.21 4.46 0 4 18 20.92 6.66 0 4 19 -0.84 2.77 0 -4 -19 0.41 2.06 0 4 19 -1.03 4.22 0 4 19 4.45 4.13 0 -5 18 5.35 4.24 0 -5 18 2.11 3.25 0 -5 17 9.04 3.25 0 -5 17 12.42 5.15 0 -5 17 9.84 4.26 0 5 -16 0.51 2.14 0 -5 16 0.37 1.94 0 5 -16 -1.96 4.25 0 -5 16 0.76 2.87 0 -5 16 0.61 2.64 0 5 -15 -1.90 3.73 0 -5 15 2.24 2.73 0 5 -15 1.77 3.00 0 -5 15 3.38 2.28 0 5 -15 0.89 3.18 0 -5 15 2.81 3.19 0 5 -14 6.35 3.27 0 -5 14 6.19 2.41 0 5 -14 5.59 2.93 0 -5 14 4.09 2.97 0 5 -14 3.14 1.51 0 5 -14 4.07 3.99 0 -5 14 5.18 3.66 0 5 -13 8.61 3.29 0 -5 13 12.81 2.91 0 5 -13 9.24 3.40 0 -5 13 6.04 3.15 0 5 -13 9.82 2.17 0 5 -13 11.05 4.06 0 5 -13 8.17 4.35 0 -5 13 7.13 3.64 0 -5 12 0.84 1.85 0 5 -12 0.96 1.13 0 -5 12 0.50 1.54 0 5 -12 -0.41 2.35 0 5 -12 -1.36 3.11 0 5 -12 -0.86 3.23 0 5 -11 19.62 2.90 0 -5 11 17.01 2.96 0 5 -11 12.73 4.44 0 5 -11 17.58 4.66 0 5 -10 4.84 1.73 0 -5 10 3.95 1.61 0 5 -10 3.18 2.80 0 -5 10 3.45 2.59 0 -5 9 172.21 11.89 0 5 -9 142.20 13.52 0 -5 9 151.13 9.66 0 5 -9 162.30 10.25 0 -5 9 168.09 12.72 0 5 -9 162.55 14.21 0 5 -8 69.09 9.72 0 -5 8 60.01 6.17 0 5 -8 78.99 7.91 0 -5 8 74.75 5.20 0 5 -8 55.94 8.53 0 -5 8 60.86 6.11 0 5 -8 89.36 9.72 0 -5 8 72.94 7.41 0 -5 7 16.98 3.19 0 5 -7 17.63 3.66 0 -5 7 17.48 2.91 0 5 -6 110.71 7.31 0 -5 6 101.80 7.87 0 -5 6 102.64 7.57 0 5 -6 90.51 8.32 0 5 -5 0.18 0.81 0 -5 5 0.67 1.08 0 5 -5 0.55 1.22 0 -5 5 0.17 0.78 0 5 -4 3.12 1.27 0 -5 4 0.87 1.16 0 -5 4 3.10 1.16 0 5 -4 4.09 1.55 0 5 -4 3.37 0.89 0 -5 3 99.77 7.93 0 5 -3 98.68 7.13 0 -5 3 83.38 7.13 0 5 -3 103.92 7.61 0 -5 3 104.48 6.65 0 5 -3 101.70 5.84 0 -5 2 7.61 1.96 0 -5 2 7.75 1.82 0 -5 2 7.92 1.45 0 5 -2 8.25 1.72 0 5 -2 6.86 1.07 0 -5 1 180.06 10.23 0 -5 1 183.31 11.41 0 -5 1 161.18 10.88 0 5 -1 171.75 10.21 0 5 0 38.88 4.14 0 -5 0 42.17 4.56 0 -5 0 38.50 4.03 0 5 0 36.54 3.37 0 5 1 1.44 0.70 0 -5 -1 2.20 0.81 0 -5 -1 2.56 1.29 0 5 1 1.51 0.95 0 -5 -1 2.04 1.18 0 5 2 132.81 6.84 0 -5 -2 131.64 9.29 0 -5 -2 124.73 8.98 0 5 2 146.79 9.06 0 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3.37 0 5 16 0.73 2.60 0 5 16 0.73 2.46 0 5 17 0.88 3.49 0 5 17 0.78 2.93 0 5 17 -0.78 2.60 0 5 17 -0.88 3.39 0 -5 -18 5.08 2.92 0 5 18 3.81 4.14 0 5 18 6.43 5.13 0 -5 -19 0.46 1.80 0 -6 18 4.52 4.13 0 -6 18 1.35 3.32 0 -6 17 17.74 6.22 0 -6 17 17.05 5.07 0 -6 16 9.21 2.94 0 -6 16 11.74 5.09 0 -6 16 19.94 5.30 0 6 -15 3.05 3.52 0 -6 15 11.33 3.00 0 6 -15 14.96 6.34 0 -6 15 16.76 5.27 0 -6 15 12.93 4.30 0 6 -14 52.19 7.90 0 -6 14 61.06 5.99 0 6 -14 52.85 7.59 0 6 -14 69.36 11.15 0 -6 14 70.48 9.69 0 -6 14 61.98 8.02 0 6 -13 0.99 2.81 0 -6 13 8.52 3.46 0 6 -13 3.31 2.76 0 -6 13 7.30 2.27 0 6 -13 3.14 3.45 0 -6 13 4.29 3.21 0 6 -12 12.73 4.16 0 -6 12 17.10 3.98 0 6 -12 18.77 4.60 0 -6 12 14.35 2.67 0 6 -12 17.83 2.99 0 6 -12 12.25 4.79 0 -6 12 20.51 5.03 0 -6 11 53.10 6.24 0 6 -11 38.69 4.37 0 -6 11 43.69 4.21 0 6 -11 36.06 7.46 0 6 -11 32.15 6.30 0 6 -10 5.29 3.61 0 -6 10 11.27 2.08 0 6 -10 11.25 2.43 0 -6 9 281.74 14.65 0 6 -9 298.41 20.96 0 6 -9 285.87 16.04 0 -6 9 262.22 18.29 0 6 -9 307.04 21.49 0 -6 8 95.06 7.91 0 6 -8 125.35 12.84 0 -6 8 96.80 6.10 0 6 -8 96.18 7.45 0 -6 8 89.33 7.99 0 6 -8 97.45 11.37 0 -6 8 91.20 8.79 0 -6 7 34.99 2.73 0 6 -7 34.39 7.34 0 -6 7 35.19 4.10 0 6 -7 40.73 5.56 0 6 -7 14.20 5.94 0 6 -7 15.46 4.85 0 -6 6 4.47 1.64 0 6 -6 3.88 2.11 0 6 -6 2.37 2.95 0 6 -6 2.35 1.26 0 -6 5 17.93 3.17 0 6 -5 15.98 2.60 0 6 -5 21.74 8.81 0 6 -5 12.75 3.02 0 -6 5 16.31 2.44 0 -6 4 307.44 18.81 0 6 -4 313.82 17.63 0 -6 4 336.17 18.57 0 6 -4 287.85 15.41 0 -6 4 311.35 16.80 0 6 -4 321.54 18.79 0 -6 3 213.94 11.80 0 6 -3 203.09 12.89 0 -6 3 197.65 12.75 0 -6 3 208.36 13.36 0 6 -3 196.71 10.61 0 -6 2 46.07 5.07 0 -6 2 49.19 4.99 0 6 -2 42.73 3.34 0 6 -2 48.58 4.71 0 -6 2 48.20 4.25 0 -6 1 30.27 3.96 0 -6 1 24.96 3.59 0 6 -1 30.73 3.29 0 6 0 1117.50 58.29 0 -6 0 1275.56 56.01 0 -6 0 1160.25 58.13 0 -6 0 1291.26 59.36 0 6 0 1061.68 56.50 0 6 1 117.57 8.83 0 6 1 106.83 7.74 0 -6 -1 112.34 8.89 0 -6 -1 104.32 8.86 0 6 2 17.57 4.58 0 6 2 14.38 3.87 0 6 2 16.36 2.70 0 -6 -2 16.75 3.02 0 -6 -2 18.35 3.12 0 6 3 12.94 3.06 0 6 3 13.27 3.19 0 6 3 13.15 1.43 0 -6 -3 8.24 2.40 0 6 3 11.99 2.32 0 -6 -3 12.88 2.77 0 6 4 108.45 7.78 0 6 4 101.83 7.54 0 6 4 87.28 6.14 0 -6 -4 92.45 8.35 0 6 4 97.82 7.74 0 -6 -4 104.41 8.92 0 6 5 17.20 2.38 0 6 5 17.83 2.94 0 -6 -5 15.81 3.29 0 -6 -5 15.63 3.54 0 -6 -5 19.23 3.38 0 6 5 15.05 2.26 0 6 6 458.43 26.25 0 -6 -6 476.15 26.90 0 6 6 484.99 25.91 0 -6 -6 493.99 27.75 0 6 6 492.39 26.50 0 6 6 426.32 23.24 0 -6 -7 0.83 1.68 0 6 7 0.35 1.42 0 6 7 1.05 1.48 0 6 7 0.60 1.22 0 -6 -7 0.73 1.33 0 -6 -8 407.45 25.49 0 6 8 418.23 24.68 0 6 8 399.51 24.48 0 6 8 374.98 23.39 0 -6 -9 20.81 4.64 0 6 9 21.66 4.31 0 6 9 26.49 4.34 0 6 9 16.87 4.06 0 6 10 88.21 9.37 0 -6 -10 86.89 9.80 0 6 10 85.39 8.85 0 6 10 89.71 9.64 0 6 10 78.43 6.02 0 6 11 31.49 3.37 0 6 11 37.56 6.01 0 -6 -11 37.71 6.79 0 6 11 43.54 6.69 0 6 12 10.99 3.70 0 -6 -12 8.43 3.85 0 6 12 13.99 4.32 0 6 13 86.48 10.28 0 6 13 78.85 10.02 0 6 14 85.77 10.54 0 6 14 57.48 9.16 0 6 15 2.10 2.80 0 6 16 14.20 5.20 0 6 17 4.93 4.13 0 6 17 -0.80 4.28 0 6 17 2.63 3.98 0 -6 -18 -2.06 3.24 0 6 18 -0.87 3.26 0 6 18 0.95 3.37 0 6 18 -0.89 3.34 0 -6 -19 5.76 3.01 0 -7 18 7.37 4.48 0 -7 17 14.81 4.68 0 -7 17 18.08 6.21 0 -7 16 1.14 2.35 0 -7 16 2.42 3.00 0 -7 15 1.06 2.56 0 -7 15 0.62 1.36 0 -7 15 2.26 2.81 0 7 -15 -2.88 4.01 0 -7 14 0.96 1.56 0 -7 14 2.43 2.59 0 -7 14 2.77 3.37 0 7 -14 -2.76 3.93 0 -7 13 93.74 9.42 0 7 -13 78.66 9.84 0 -7 13 91.61 6.60 0 7 -13 82.50 11.94 0 -7 13 84.30 10.71 0 -7 12 148.43 11.50 0 7 -12 120.89 11.86 0 -7 12 123.40 7.88 0 -7 12 138.47 12.89 0 7 -12 122.83 12.30 0 -7 11 -0.52 2.90 0 7 -11 2.74 3.06 0 -7 11 1.81 2.06 0 -7 11 0.81 1.02 0 7 -11 2.35 3.14 0 -7 10 23.20 4.09 0 7 -10 18.85 4.73 0 -7 10 26.24 2.63 0 7 -10 29.68 5.98 0 7 -9 2.61 1.75 0 -7 9 1.70 1.74 0 7 -9 1.51 2.29 0 -7 9 2.12 0.86 0 7 -9 -0.61 3.74 0 7 -9 6.33 3.76 0 7 -8 59.52 9.64 0 7 -8 74.92 9.78 0 7 -8 58.82 5.81 0 -7 8 48.64 6.00 0 7 -7 215.32 18.80 0 7 -7 230.60 19.70 0 7 -7 169.01 17.31 0 -7 6 51.10 4.95 0 7 -6 52.19 6.47 0 7 -6 36.89 8.11 0 7 -6 34.62 8.43 0 -7 5 111.46 9.72 0 -7 5 80.61 8.12 0 7 -5 115.31 9.91 0 -7 5 115.67 7.88 0 7 -5 95.98 13.72 0 -7 4 460.84 25.07 0 -7 4 375.23 23.62 0 7 -4 453.63 24.98 0 -7 4 454.16 22.60 0 -7 3 295.80 18.41 0 -7 3 304.94 18.21 0 -7 3 323.92 16.82 0 7 -3 303.51 18.12 0 7 -2 9.15 1.46 0 7 -2 10.57 2.27 0 -7 2 16.82 3.02 0 -7 2 10.58 2.10 0 -7 2 10.68 2.66 0 -7 1 78.21 7.15 0 -7 1 65.03 6.47 0 7 -1 60.91 5.44 0 -7 0 16.71 3.03 0 7 0 15.33 3.02 0 -7 0 12.40 1.78 0 7 0 11.29 2.00 0 -7 0 17.47 3.25 0 7 0 5.11 1.02 0 7 0 25.47 7.80 0 7 1 506.25 38.56 0 7 1 447.31 37.11 0 7 1 680.38 33.07 0 -7 -1 754.40 35.49 0 7 1 719.67 34.91 0 -7 -1 669.99 32.28 0 -7 -1 660.99 35.09 0 -7 -1 609.46 34.51 0 7 2 608.81 37.65 0 7 2 582.94 37.01 0 7 2 679.97 33.53 0 7 2 722.40 35.03 0 -7 -2 634.88 35.40 0 -7 -2 660.00 35.49 0 7 3 156.14 11.78 0 7 3 143.20 11.44 0 7 3 163.63 11.20 0 -7 -3 130.58 11.13 0 -7 -3 144.32 11.46 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-8 4 2.08 1.67 0 -8 4 1.53 1.82 0 -8 4 1.96 1.19 0 8 -4 6.76 4.86 0 8 -4 1.46 0.87 0 8 -4 2.80 4.88 0 8 -3 148.96 11.12 0 -8 3 117.58 10.34 0 -8 3 153.40 11.59 0 -8 3 154.87 9.81 0 8 -3 90.79 13.55 0 8 -3 110.52 15.62 0 8 -2 171.80 11.93 0 -8 2 172.92 12.60 0 -8 2 210.47 13.67 0 8 -2 146.28 16.90 0 8 -2 121.64 16.07 0 8 -1 23.84 6.60 0 8 -1 13.13 2.52 0 8 -1 16.58 6.13 0 -8 1 15.30 3.50 0 -8 1 15.94 3.45 0 8 0 11.31 4.92 0 8 0 11.94 4.63 0 -8 0 5.54 2.09 0 8 0 10.28 2.10 0 -8 0 4.67 1.40 0 8 0 9.30 2.72 0 -8 0 13.22 3.21 0 -8 0 11.13 2.61 0 8 1 52.67 7.96 0 8 1 47.07 7.39 0 8 1 52.71 4.90 0 -8 -1 62.29 6.42 0 8 1 54.63 5.95 0 -8 -1 39.73 4.05 0 -8 -1 49.99 6.05 0 -8 -1 56.17 6.18 0 8 2 173.00 14.16 0 -8 -2 173.41 12.62 0 8 2 172.19 14.19 0 8 2 170.02 11.02 0 8 2 167.31 12.11 0 -8 -2 147.05 12.47 0 -8 -2 163.03 12.66 0 8 3 89.72 8.41 0 -8 -3 83.78 8.02 0 8 3 90.93 8.53 0 8 3 82.16 7.54 0 -8 -3 63.49 7.80 0 -8 -3 76.00 8.18 0 8 4 17.88 3.26 0 -8 -4 21.05 3.83 0 8 4 19.61 3.43 0 8 4 18.72 3.45 0 -8 -4 14.91 3.80 0 -8 -4 16.54 3.93 0 8 5 8.99 2.24 0 -8 -5 15.17 3.24 0 -8 -5 8.48 3.22 0 -8 -5 3.64 2.32 0 8 5 12.04 2.86 0 8 6 178.61 11.53 0 -8 -6 163.60 12.85 0 8 6 151.02 11.51 0 -8 -6 170.70 13.47 0 8 7 252.18 16.71 0 -8 -7 245.43 18.39 0 -8 -7 251.20 17.59 0 8 7 241.97 15.86 0 8 7 206.21 15.88 0 8 7 211.68 13.52 0 -8 -8 1.71 2.28 0 8 8 -0.43 1.47 0 -8 -8 0.49 1.85 0 8 8 0.72 1.60 0 8 8 -0.87 1.83 0 8 8 -0.19 0.93 0 -8 -9 0.61 2.67 0 8 9 0.47 1.82 0 8 9 2.34 1.41 0 8 9 0.48 2.02 0 8 9 0.15 0.94 0 8 10 32.70 5.66 0 -8 -10 28.12 6.30 0 8 10 19.22 4.92 0 8 10 19.24 4.16 0 8 11 40.64 6.64 0 8 11 32.86 5.69 0 8 11 31.90 6.27 0 8 12 196.47 15.15 0 8 12 204.34 16.43 0 8 13 80.40 9.74 0 8 13 87.91 10.71 0 -8 -14 18.94 7.07 0 8 14 115.90 12.27 0 8 15 39.42 7.85 0 -8 -15 1.90 4.68 0 8 16 -2.94 4.78 0 -8 -16 1.05 4.56 0 8 16 -0.81 3.65 0 -8 -16 -0.58 2.30 0 8 17 13.77 5.77 0 -8 -17 7.19 3.66 0 -8 -17 -1.15 6.11 0 8 17 9.42 5.25 0 8 17 9.52 4.54 0 -8 -18 16.13 4.89 0 8 18 16.18 6.10 0 -8 -19 1.27 2.20 0 -9 17 3.50 3.16 0 -9 16 4.89 3.12 0 -9 16 0.86 2.96 0 -9 15 33.25 5.93 0 9 -15 24.16 7.54 0 -9 15 23.32 6.68 0 9 -15 19.40 6.27 0 -9 14 5.59 3.13 0 9 -14 1.02 3.59 0 -9 14 0.75 2.94 0 9 -14 0.68 3.41 0 9 -13 3.20 4.25 0 -9 13 8.98 4.17 0 9 -13 7.23 4.54 0 9 -12 0.64 3.31 0 -9 12 -1.92 3.77 0 -9 12 3.13 2.36 0 -9 11 -0.59 3.00 0 9 -11 1.08 3.62 0 9 -11 -0.70 2.70 0 -9 11 1.80 2.04 0 -9 10 126.22 9.60 0 9 -10 94.67 11.53 0 9 -10 110.28 11.92 0 -9 10 80.04 9.18 0 9 -10 70.38 13.07 0 -9 10 97.32 10.71 0 -9 9 14.18 3.94 0 -9 9 17.59 3.65 0 9 -9 7.66 3.94 0 9 -9 13.71 4.87 0 9 -9 19.36 7.39 0 9 -8 74.96 9.63 0 -9 8 69.51 6.63 0 -9 8 47.67 6.91 0 9 -8 70.10 10.23 0 9 -8 88.44 10.61 0 9 -7 140.50 13.85 0 -9 7 118.21 9.04 0 9 -7 112.68 11.93 0 -9 7 103.46 10.18 0 -9 7 114.82 11.42 0 9 -7 108.40 13.09 0 9 -6 4.41 2.78 0 -9 6 0.41 2.05 0 9 -6 0.72 3.32 0 9 -6 1.54 3.99 0 -9 6 1.45 2.51 0 9 -5 25.42 2.15 0 9 -5 27.60 7.27 0 9 -5 32.63 8.00 0 -9 5 30.44 5.39 0 -9 4 69.68 7.81 0 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33.51 6.02 0 -9 -6 3.42 2.26 0 9 6 1.33 1.55 0 9 6 0.26 1.07 0 -9 -6 3.33 2.82 0 9 6 3.95 2.06 0 -9 -6 2.59 1.91 0 -9 -6 1.13 2.03 0 9 7 161.50 13.42 0 9 7 143.69 10.99 0 -9 -7 177.89 14.09 0 -9 -7 192.97 16.10 0 9 7 174.63 10.79 0 9 7 181.08 13.41 0 -9 -7 186.17 15.42 0 9 7 164.22 11.49 0 9 8 4.46 1.70 0 -9 -8 3.86 3.04 0 9 8 4.60 2.58 0 -9 -8 2.99 2.79 0 9 8 5.83 2.55 0 -9 -8 8.38 3.39 0 9 8 6.04 2.76 0 -9 -8 5.08 2.38 0 9 9 19.57 3.08 0 9 9 27.44 5.45 0 -9 -9 29.42 6.35 0 9 9 19.83 4.74 0 9 9 34.24 5.23 0 -9 -9 22.74 5.43 0 -9 -10 6.38 4.05 0 9 10 1.63 2.20 0 9 10 -0.56 2.22 0 9 10 -0.47 1.19 0 9 10 -0.44 2.03 0 -9 -11 42.94 7.92 0 9 11 82.68 9.49 0 9 11 90.87 8.88 0 9 12 2.08 2.80 0 9 12 4.44 3.61 0 -9 -12 4.34 4.50 0 -9 -13 28.83 7.26 0 9 13 32.02 3.52 0 9 14 15.40 5.51 0 -9 -14 4.41 4.75 0 -9 -14 18.20 4.94 0 -9 -15 13.59 6.76 0 9 15 25.94 6.79 0 -9 -15 27.52 5.89 0 -9 -16 2.53 2.95 0 -9 -16 1.06 4.20 0 9 16 0.84 2.78 0 9 16 1.46 2.73 0 -9 -17 3.26 3.43 0 -9 -17 1.17 5.24 0 9 17 3.93 3.65 0 -9 -18 0.67 2.75 0 -9 -19 0.70 2.53 0 -10 16 5.29 3.70 0 -10 16 4.95 3.28 0 10 -15 -2.37 4.85 0 -10 15 0.83 3.06 0 -10 15 5.13 3.02 0 10 -14 20.30 6.18 0 10 -14 12.31 6.50 0 10 -14 11.83 5.71 0 -10 14 19.47 5.91 0 -10 14 22.37 4.85 0 10 -13 7.92 4.60 0 -10 13 7.95 3.08 0 10 -13 1.25 4.41 0 -10 13 6.54 3.73 0 -10 12 8.15 3.91 0 -10 12 9.41 3.22 0 10 -12 2.55 4.79 0 10 -12 9.71 5.02 0 -10 11 46.49 7.63 0 10 -11 31.83 9.86 0 10 -10 35.79 7.59 0 -10 10 29.36 6.31 0 -10 10 21.58 5.07 0 -10 10 30.24 4.80 0 10 -10 37.99 7.29 0 10 -9 15.85 5.54 0 -10 9 15.63 4.39 0 -10 9 23.40 4.09 0 10 -9 18.23 5.73 0 10 -9 6.26 5.55 0 -10 8 28.13 5.60 0 10 -8 44.88 7.85 0 10 -8 43.07 7.85 0 -10 8 52.47 5.82 0 -10 7 3.03 1.89 0 10 -7 5.41 4.05 0 10 -7 1.34 2.77 0 -10 7 2.89 2.38 0 10 -6 158.78 14.81 0 -10 6 170.00 11.48 0 10 -6 207.93 17.16 0 10 -6 173.66 16.32 0 -10 5 280.39 19.95 0 10 -5 307.22 23.39 0 10 -5 290.03 22.98 0 10 -5 243.26 19.88 0 10 -4 3.86 1.17 0 10 -4 0.72 3.34 0 -10 4 6.86 3.09 0 10 -4 -0.77 4.21 0 10 -3 19.47 2.74 0 10 -3 38.37 7.67 0 -10 3 13.56 3.80 0 -10 3 26.26 5.06 0 10 -3 37.87 8.04 0 -10 2 41.62 6.01 0 -10 2 59.54 7.47 0 10 -2 38.75 3.77 0 10 -2 40.02 7.74 0 10 -2 44.17 8.68 0 10 -1 83.38 10.71 0 10 -1 93.48 7.98 0 -10 1 104.46 9.76 0 -10 1 101.72 7.15 0 10 -1 83.45 5.35 0 -10 1 115.79 10.46 0 10 -1 123.47 12.90 0 10 0 258.42 20.18 0 10 0 261.81 20.14 0 10 0 244.34 15.22 0 -10 0 257.35 17.81 0 -10 0 234.70 14.29 0 -10 0 262.58 18.08 0 -10 0 247.73 17.26 0 10 1 52.23 7.81 0 10 1 48.21 7.55 0 10 1 49.90 5.27 0 -10 -1 42.63 6.21 0 10 1 52.57 6.76 0 -10 -1 56.03 7.32 0 -10 -1 52.46 6.83 0 10 2 126.63 11.19 0 10 2 128.21 11.22 0 10 2 94.41 7.97 0 -10 -2 91.20 9.46 0 10 2 93.16 9.20 0 -10 -2 94.93 10.23 0 -10 -2 89.08 9.67 0 10 3 271.46 17.33 0 -10 -3 249.44 17.37 0 10 3 279.49 17.71 0 10 3 213.54 15.97 0 10 3 227.19 14.90 0 -10 -3 194.67 17.26 0 -10 -3 206.31 16.89 0 10 4 243.08 16.43 0 -10 -4 247.34 17.58 0 10 4 245.09 15.65 0 10 4 257.74 17.12 0 -10 -4 224.60 18.85 0 -10 -4 208.94 17.70 0 -10 -5 3.68 2.36 0 10 5 0.34 1.35 0 -10 -5 -0.65 2.47 0 10 5 1.24 1.67 0 -10 -5 0.59 2.12 0 10 6 2.72 1.82 0 -10 -6 6.16 2.72 0 10 6 2.52 1.83 0 10 6 3.32 1.12 0 -10 -6 3.33 2.79 0 10 6 2.60 2.08 0 -10 -6 3.82 2.78 0 10 7 3.06 1.85 0 -10 -7 0.98 1.66 0 10 7 1.78 1.54 0 10 7 -0.14 1.01 0 -10 -7 -2.09 2.32 0 -10 -7 0.66 2.36 0 10 7 1.25 1.85 0 -10 -7 3.39 3.19 0 -10 -8 169.77 13.50 0 10 8 149.96 10.39 0 10 8 174.34 12.90 0 -10 -8 144.90 11.60 0 -10 -8 159.38 15.33 0 -10 -9 268.66 19.08 0 10 9 235.57 14.87 0 10 9 310.48 18.70 0 -10 -9 301.57 18.95 0 10 9 260.32 18.66 0 10 10 17.40 3.01 0 10 10 19.68 4.45 0 -10 -10 25.63 5.38 0 10 10 21.14 5.29 0 -10 -11 53.27 7.90 0 10 11 66.45 8.13 0 -10 -11 46.42 8.04 0 10 11 40.30 4.03 0 10 11 68.98 9.06 0 10 12 77.69 10.01 0 10 12 74.62 8.98 0 -10 -12 102.98 10.72 0 10 13 -0.19 1.04 0 10 13 -1.43 3.26 0 -10 -13 -0.79 3.32 0 -10 -14 -1.27 2.78 0 10 14 -1.54 3.49 0 -10 -14 -1.76 4.29 0 10 15 16.33 5.73 0 -10 -15 3.86 5.01 0 -10 -15 13.90 4.49 0 10 15 10.87 4.92 0 10 16 0.87 3.91 0 -10 -16 -1.06 5.58 0 -10 -16 4.80 3.30 0 10 16 5.12 3.64 0 10 17 34.63 7.56 0 -10 -17 34.09 7.04 0 -10 -18 11.76 4.52 0 -10 -19 16.84 5.36 0 -11 15 -0.86 3.14 0 -11 15 -1.07 3.05 0 11 -14 2.86 5.26 0 -11 14 5.69 3.99 0 -11 14 1.50 2.53 0 11 -13 -0.78 4.77 0 -11 13 2.33 2.58 0 11 -13 -1.46 5.42 0 -11 13 3.06 3.54 0 -11 12 4.35 3.71 0 11 -12 -3.01 4.70 0 11 -12 1.48 4.89 0 -11 12 -0.43 2.16 0 11 -11 -1.48 5.54 0 -11 11 -0.68 2.57 0 -11 11 0.58 2.62 0 -11 11 -1.63 2.28 0 -11 10 -0.58 3.24 0 -11 10 -0.65 3.07 0 -11 10 0.77 2.04 0 11 -10 -3.49 4.49 0 11 -10 1.47 4.52 0 11 -9 107.73 13.16 0 -11 9 118.68 9.60 0 -11 9 66.77 9.45 0 11 -9 106.35 12.40 0 11 -9 45.73 12.65 0 11 -8 3.90 3.60 0 -11 8 2.75 2.69 0 -11 8 3.12 2.24 0 11 -8 -0.69 3.71 0 11 -8 2.73 5.47 0 -11 7 4.01 2.17 0 -11 7 1.60 2.45 0 11 -7 6.90 4.13 0 11 -7 7.49 3.72 0 -11 6 12.21 3.33 0 -11 6 11.41 3.84 0 11 -6 16.19 5.07 0 11 -6 22.16 6.28 0 -11 5 4.60 2.85 0 11 -5 9.06 4.72 0 11 -5 6.38 3.49 0 11 -4 70.02 5.01 0 11 -4 94.18 11.50 0 11 -4 77.47 9.32 0 11 -3 127.28 11.57 0 -11 3 97.49 10.86 0 -11 3 135.79 12.72 0 11 -3 119.94 8.21 0 11 -3 157.92 14.81 0 11 -3 169.26 15.74 0 11 -2 33.21 6.53 0 11 -2 16.45 2.64 0 -11 2 13.25 3.99 0 -11 2 10.99 2.63 0 -11 2 27.66 5.52 0 11 -2 20.35 5.83 0 11 -1 273.34 19.99 0 11 -1 275.41 19.80 0 11 -1 220.77 12.45 0 -11 1 235.92 16.29 0 -11 1 248.54 17.38 0 -11 1 239.97 17.11 0 11 0 105.29 10.97 0 -11 0 76.13 8.70 0 11 0 96.90 10.62 0 -11 0 88.36 9.38 0 -11 0 75.31 8.38 0 11 1 -0.53 2.46 0 -11 -1 3.41 2.50 0 11 1 -0.28 1.50 0 11 1 -0.47 1.91 0 -11 -1 0.50 2.26 0 11 1 -0.56 2.90 0 11 2 23.67 3.86 0 11 2 23.62 4.75 0 11 2 27.67 5.45 0 -11 -2 18.18 4.65 0 -11 -2 21.73 4.89 0 11 3 9.16 3.13 0 11 3 8.42 2.48 0 -11 -3 4.51 2.75 0 -11 -3 10.09 3.99 0 11 3 10.43 3.36 0 -11 -4 170.30 14.34 0 11 4 157.62 13.25 0 11 4 173.80 12.48 0 -11 -4 147.29 15.40 0 -11 -4 178.75 15.51 0 -11 -5 119.97 11.82 0 11 5 129.41 10.65 0 11 5 114.64 10.90 0 11 5 129.41 10.38 0 -11 -5 102.27 12.92 0 -11 -5 111.36 12.49 0 11 6 10.37 3.05 0 11 6 13.35 3.36 0 -11 -6 12.68 3.98 0 11 6 18.81 4.65 0 -11 -6 12.66 5.10 0 -11 -6 11.26 4.45 0 -11 -7 7.60 3.55 0 11 7 6.23 2.44 0 11 7 9.71 3.70 0 11 7 4.87 2.17 0 -11 -8 141.93 12.61 0 11 8 133.13 9.86 0 11 8 85.88 6.52 0 -11 -8 86.10 8.60 0 11 8 150.65 12.22 0 11 8 104.20 10.95 0 -11 -9 40.28 6.69 0 11 9 33.42 4.72 0 11 9 23.37 3.37 0 -11 -9 29.21 5.57 0 11 9 37.89 6.13 0 11 9 31.84 6.19 0 11 10 3.60 1.84 0 11 10 -0.27 1.37 0 -11 -10 5.69 3.47 0 11 10 2.03 2.32 0 -11 -10 1.79 2.74 0 11 11 12.58 3.15 0 -11 -11 17.49 5.24 0 11 11 17.32 3.00 0 -11 -12 8.34 3.64 0 -11 -12 6.34 2.12 0 -11 -12 12.42 5.01 0 11 12 4.18 3.43 0 -11 -13 25.53 7.05 0 11 13 76.95 10.66 0 11 14 61.56 5.39 0 11 14 115.87 13.34 0 -11 -14 123.83 12.82 0 11 14 143.53 13.26 0 -11 -14 54.18 10.49 0 11 15 0.85 3.70 0 11 15 4.17 3.78 0 -11 -15 -0.94 4.05 0 -11 -15 2.16 2.84 0 11 16 8.92 4.33 0 -11 -16 3.07 5.38 0 -11 -16 3.74 3.59 0 -11 -17 -1.11 4.93 0 -11 -17 0.77 2.84 0 -12 14 3.15 2.78 0 -12 14 4.24 3.71 0 12 -14 1.64 4.88 0 -12 13 0.49 2.64 0 12 -13 1.68 5.47 0 -12 13 -1.62 3.43 0 12 -12 1.70 5.57 0 -12 12 4.63 3.81 0 -12 12 5.58 3.26 0 12 -11 -1.69 6.30 0 -12 11 -1.47 3.16 0 -12 11 0.66 2.92 0 -12 11 1.31 2.11 0 -12 10 15.56 5.01 0 -12 10 4.51 3.42 0 12 -10 6.81 4.38 0 12 -10 3.32 5.89 0 -12 10 12.80 3.74 0 12 -9 3.20 4.97 0 -12 9 16.95 5.07 0 -12 9 17.73 4.03 0 -12 8 1.82 2.76 0 -12 8 0.38 2.07 0 12 -8 -2.16 4.17 0 12 -8 6.10 6.67 0 -12 7 11.84 3.42 0 -12 7 4.73 3.10 0 12 -7 8.54 4.35 0 12 -7 12.34 4.86 0 -12 6 2.30 2.91 0 12 -6 -2.12 4.21 0 12 -6 0.77 2.50 0 -12 5 5.69 3.10 0 12 -5 18.27 5.61 0 12 -5 16.59 5.09 0 12 -4 -0.69 3.41 0 12 -4 2.03 0.97 0 12 -4 4.77 3.23 0 -12 3 83.22 7.23 0 12 -3 72.51 8.78 0 12 -3 65.22 5.63 0 -12 2 2.71 1.81 0 -12 2 0.56 2.24 0 12 -2 0.86 1.93 0 12 -2 0.18 1.09 0 12 -2 -0.65 3.34 0 -12 1 41.25 4.89 0 -12 1 44.18 7.22 0 12 -1 43.53 5.82 0 12 -1 48.34 4.48 0 12 0 11.75 4.51 0 -12 0 9.41 3.61 0 12 0 3.69 3.62 0 -12 0 1.08 1.58 0 -12 0 5.61 3.06 0 -12 0 5.30 3.46 0 12 1 3.84 3.15 0 -12 -1 5.03 3.04 0 12 1 6.32 3.88 0 -12 -1 8.20 3.45 0 -12 -1 4.99 2.88 0 12 2 -1.01 2.24 0 -12 -2 1.67 2.46 0 -12 -2 -0.64 2.11 0 12 2 -1.53 2.25 0 12 3 -1.41 2.32 0 -12 -3 -0.56 2.03 0 12 3 1.47 2.34 0 -12 -3 -1.41 3.64 0 -12 -3 -0.62 2.21 0 -12 -4 5.10 2.98 0 12 4 -0.92 2.37 0 12 4 3.40 2.63 0 12 4 3.67 2.24 0 -12 -4 -0.79 3.27 0 -12 -4 9.32 4.00 0 -12 -5 8.03 3.53 0 12 5 8.64 3.18 0 12 5 15.46 3.69 0 12 5 7.89 3.36 0 -12 -5 10.43 4.88 0 12 5 7.45 2.87 0 12 6 -1.24 2.07 0 -12 -6 0.59 1.98 0 12 6 1.52 2.14 0 12 6 1.57 1.94 0 12 7 2.42 2.08 0 -12 -7 1.20 2.65 0 12 7 5.28 3.01 0 12 7 3.74 2.43 0 -12 -8 22.10 5.68 0 12 8 26.62 4.78 0 12 8 24.87 5.53 0 12 8 19.26 4.93 0 -12 -9 -1.27 2.13 0 12 9 -2.61 1.97 0 12 9 1.20 1.12 0 12 9 -1.13 2.59 0 12 9 -1.86 3.17 0 12 10 49.64 4.98 0 12 10 81.05 7.49 0 -12 -10 98.50 11.10 0 -12 -10 45.18 7.09 0 12 11 5.87 2.23 0 -12 -11 7.63 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139.41 9.73 -5 9 -6 112.34 16.20 -5 9 -6 158.60 14.59 5 -9 7 3.44 1.65 -5 9 -7 7.97 2.81 -5 9 -7 0.82 1.48 -5 9 -7 9.09 5.62 5 -9 7 4.69 3.30 5 -9 8 4.91 2.01 -5 9 -8 11.60 5.92 -5 9 -8 4.56 2.20 -5 9 -8 10.79 3.46 5 -9 9 -0.26 1.33 -5 9 -9 -1.13 2.29 -5 9 -9 -1.19 4.00 -5 9 -9 -1.73 2.68 5 -9 10 12.97 2.98 -5 9 -10 15.07 3.87 -5 9 -10 13.40 6.77 -5 9 -10 22.81 5.44 5 -9 11 3.21 3.53 5 -9 11 5.10 1.76 -5 9 -11 6.33 3.14 -5 9 -11 7.46 5.68 -5 9 -11 12.37 4.64 5 -9 12 52.75 9.85 -5 9 -12 27.67 7.00 -5 9 -12 42.52 7.03 5 -9 13 8.41 4.56 5 -9 13 12.24 2.25 -5 9 -13 8.54 3.84 -5 9 -13 3.83 4.62 5 -9 14 0.90 1.18 -5 9 -14 4.26 5.08 -5 9 -14 0.68 3.03 -5 9 -15 2.81 4.64 -5 9 -15 6.79 3.73 -5 9 -16 5.11 5.62 -5 8 17 -1.29 3.03 -5 8 16 48.63 7.80 -5 8 15 0.55 2.37 -5 8 14 4.42 3.85 -5 8 14 -1.01 3.59 -5 8 14 1.52 2.28 -5 8 13 19.92 6.25 -5 8 13 22.28 6.78 -5 8 13 13.77 3.84 -5 8 12 0.78 3.28 -5 8 12 0.41 1.88 -5 8 12 0.85 3.22 -5 8 11 65.82 9.73 -5 8 11 62.66 6.72 -5 8 11 56.17 9.35 -5 8 10 113.64 8.85 -5 8 10 127.59 12.80 5 -8 -10 52.89 9.84 5 -8 -10 46.51 8.22 -5 8 9 5.75 2.21 5 -8 -9 1.97 2.23 -5 8 9 6.98 3.44 5 -8 -9 1.53 2.59 5 -8 -9 0.54 2.27 5 -8 -8 75.68 9.60 5 -8 -8 77.41 8.38 -5 8 8 79.51 9.68 -5 8 8 71.17 6.85 5 -8 -8 63.93 9.46 5 -8 -8 80.84 8.54 -5 8 7 0.34 1.32 5 -8 -7 -0.60 1.99 5 -8 -7 1.98 2.14 -5 8 7 1.60 2.16 5 -8 -7 1.57 1.97 -5 8 7 0.28 1.08 5 -8 -7 -0.65 2.29 5 -8 -6 7.48 4.18 -5 8 6 4.89 2.51 -5 8 6 5.76 2.77 5 -8 -6 10.35 3.11 -5 8 6 6.50 1.87 -5 8 6 6.20 2.11 5 -8 -6 3.72 3.04 5 -8 -5 17.58 4.00 -5 8 5 8.60 3.16 -5 8 5 10.89 2.51 -5 8 5 11.01 2.61 5 -8 -5 11.29 3.05 5 -8 -5 11.20 4.11 -5 8 4 5.58 2.54 5 -8 -4 6.03 2.54 -5 8 4 4.95 2.46 -5 8 4 4.27 1.88 -5 8 4 9.81 2.99 5 -8 -4 6.34 2.35 5 -8 -4 7.77 3.30 -5 8 3 61.93 7.59 5 -8 -3 87.74 8.59 -5 8 3 62.76 6.82 -5 8 3 79.10 7.13 -5 8 3 57.64 6.25 5 -8 -3 83.73 8.36 5 -8 -3 62.72 6.49 5 -8 -3 60.54 8.05 5 -8 -2 396.83 22.73 -5 8 2 307.58 19.54 -5 8 2 297.90 19.02 -5 8 2 344.60 20.15 5 -8 -2 291.34 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3.41 -5 8 -8 12.30 5.87 -5 8 -8 5.35 2.30 -5 8 -8 9.71 3.90 5 -8 8 6.67 1.97 -5 8 -9 14.69 3.42 -5 8 -9 8.43 4.86 -5 8 -9 1.38 2.71 -5 8 -9 16.27 5.08 5 -8 9 9.17 2.29 5 -8 10 4.10 1.69 -5 8 -10 3.80 3.31 -5 8 -10 2.95 2.39 -5 8 -10 1.08 3.90 5 -8 11 3.00 2.70 -5 8 -11 -0.96 2.77 -5 8 -11 1.11 4.22 5 -8 11 0.37 0.92 5 -8 12 -1.62 3.55 5 -8 12 2.23 1.31 -5 8 -12 8.63 4.80 -5 8 -12 1.61 2.53 -5 8 -12 4.54 4.77 5 -8 13 26.09 3.11 5 -8 13 26.99 7.74 -5 8 -13 8.95 5.40 -5 8 -13 16.80 4.98 5 -8 14 0.93 3.29 5 -8 14 0.55 1.21 -5 8 -14 -0.67 3.13 -5 8 -14 -0.90 4.21 5 -8 15 19.93 3.10 -5 8 -15 7.88 5.68 -5 8 -15 17.91 5.38 -5 8 -16 2.14 5.13 -5 8 -18 1.85 3.88 -5 7 17 6.69 3.84 -5 7 16 0.62 2.64 -5 7 15 11.76 5.73 -5 7 15 13.50 5.57 -5 7 15 19.55 4.99 -5 7 14 49.33 9.91 -5 7 14 36.18 8.04 -5 7 14 46.55 7.25 -5 7 13 17.20 6.08 -5 7 13 14.17 5.39 -5 7 13 8.98 3.13 -5 7 12 1.66 3.49 -5 7 12 3.36 2.32 -5 7 12 5.15 3.74 5 -7 -11 13.79 4.27 5 -7 -11 16.30 4.57 -5 7 11 24.02 6.27 -5 7 11 28.89 4.76 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29.43 -5 6 4 627.07 32.47 5 -6 -4 580.16 29.70 5 -6 -4 516.89 32.45 5 -6 -3 232.14 14.85 5 -6 -3 229.43 14.65 -5 6 3 237.28 15.01 -5 6 3 241.12 13.14 -5 6 3 207.58 14.87 -5 6 3 223.42 15.75 5 -6 -3 184.33 15.30 5 -6 -2 132.75 10.33 5 -6 -2 152.36 10.64 -5 6 2 120.90 9.82 -5 6 2 165.55 10.96 -5 6 2 134.00 11.40 5 -6 -2 111.19 10.46 -5 6 1 393.71 21.73 -5 6 1 362.25 21.62 -5 6 1 380.34 21.52 5 -6 -1 374.37 22.13 5 -6 -1 381.59 22.50 -5 6 1 368.06 23.23 -5 6 0 2.33 1.86 5 -6 0 5.96 2.03 -5 6 0 4.90 1.80 -5 6 0 3.30 1.73 5 -6 0 4.01 1.81 -5 6 0 2.27 1.29 -5 6 -1 19.95 4.09 5 -6 1 25.10 4.04 -5 6 -1 25.11 4.05 5 -6 1 21.94 3.85 -5 6 -1 22.07 3.11 5 -6 2 321.30 19.40 5 -6 2 288.21 16.88 -5 6 -2 252.46 18.17 5 -6 2 308.25 18.88 -5 6 -2 283.66 16.10 5 -6 2 323.34 19.27 -5 6 -2 276.24 19.11 -5 6 -2 302.76 22.71 -5 6 -3 -0.38 1.54 5 -6 3 0.68 1.38 5 -6 3 2.23 1.77 -5 6 -3 0.92 0.79 -5 6 -3 0.41 1.37 5 -6 3 1.88 1.60 -5 6 -3 2.00 2.84 5 -6 4 408.04 23.77 -5 6 -4 336.46 23.99 5 -6 4 441.77 25.55 5 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40.53 5.39 7 5 10 226.85 17.05 -7 -5 -10 229.95 17.79 7 5 10 268.56 18.86 7 5 10 229.40 15.44 7 5 11 73.65 8.78 -7 -5 -11 66.03 8.89 -7 -5 -11 46.64 6.39 -7 -5 -11 37.57 7.51 7 5 11 76.43 9.67 7 5 11 66.11 6.87 -7 -5 -12 0.79 1.87 -7 -5 -12 3.48 4.16 7 5 12 3.43 2.91 7 5 12 1.98 1.61 7 5 12 1.77 2.49 -7 -5 -13 6.95 2.90 7 5 13 14.03 4.69 -7 -5 -13 9.03 5.27 7 5 13 15.97 5.42 7 5 13 13.73 2.66 7 5 14 0.15 0.76 7 5 14 0.58 0.73 -7 -5 -14 -0.75 2.06 -7 -5 -14 2.48 3.64 7 5 14 -0.84 3.20 7 5 14 1.38 2.32 7 5 14 1.39 3.05 -7 -5 -15 7.91 2.76 -7 -5 -15 14.45 6.07 7 5 15 20.28 6.73 7 5 15 12.63 5.18 7 5 15 16.30 4.96 -7 -5 -16 58.47 7.01 -7 -5 -16 61.60 11.45 7 5 16 101.78 12.59 7 5 16 101.07 11.56 7 5 17 0.63 2.50 -7 -5 -17 1.07 4.25 7 5 17 7.70 5.17 -7 -5 -17 -0.85 1.49 -7 -6 15 6.40 3.55 -7 -6 15 2.92 5.32 -7 -6 14 2.77 2.64 -7 -6 14 2.92 6.20 -7 -6 13 6.79 3.44 -7 -6 13 4.33 5.93 -7 -6 12 0.49 2.12 -7 -6 12 1.31 3.08 -7 -6 12 5.61 5.80 -7 -6 11 9.20 3.43 -7 -6 11 4.25 3.17 -7 -6 11 4.07 5.66 -7 -6 10 60.25 8.32 -7 -6 10 65.68 7.49 -7 -6 9 1.61 2.04 -7 -6 9 4.13 2.94 -7 -6 8 109.94 10.25 -7 -6 8 121.42 10.48 -7 -6 8 117.28 9.29 7 6 -8 112.00 11.87 7 6 -7 50.14 7.96 -7 -6 7 66.23 7.36 -7 -6 7 57.59 7.25 7 6 -7 21.50 4.35 -7 -6 7 14.01 7.31 7 6 -6 3.12 2.92 7 6 -6 1.19 2.46 -7 -6 6 6.09 2.75 -7 -6 6 4.84 2.53 -7 -6 6 -1.13 4.08 -7 -6 5 54.31 11.37 7 6 -5 60.84 8.50 -7 -6 5 73.66 7.60 7 6 -5 81.32 10.90 -7 -6 4 19.88 5.24 7 6 -4 17.20 4.64 7 6 -4 9.40 4.18 -7 -6 4 16.47 3.26 -7 -6 4 16.47 3.52 7 6 -4 10.20 3.90 -7 -6 4 18.81 6.86 7 6 -3 133.20 13.62 -7 -6 3 176.09 16.11 -7 -6 3 229.22 13.60 -7 -6 3 205.95 13.56 7 6 -3 223.05 17.35 7 6 -3 210.92 16.06 -7 -6 3 88.42 15.01 7 6 -2 379.59 24.03 -7 -6 2 407.57 21.94 7 6 -2 392.19 25.14 7 6 -2 345.96 23.42 -7 -6 2 347.03 25.27 -7 -6 2 387.14 22.58 7 6 -1 4.97 2.57 7 6 -1 5.51 2.70 -7 -6 1 8.40 3.63 7 6 -1 6.88 2.92 -7 -6 1 5.70 2.20 -7 -6 1 8.51 2.76 -7 -6 1 14.85 5.85 7 6 0 52.53 6.60 7 6 0 56.33 7.12 -7 -6 0 57.57 5.92 7 6 0 42.17 6.36 -7 -6 0 52.14 7.71 7 6 0 54.41 6.37 -7 -6 0 58.96 6.73 -7 -6 0 49.96 3.63 -7 -6 -1 1.70 3.66 7 6 1 12.77 3.32 7 6 1 10.53 3.16 7 6 1 7.08 2.68 -7 -6 -1 8.39 3.55 -7 -6 -1 14.97 3.02 -7 -6 -1 9.15 3.03 7 6 1 11.56 3.10 -7 -6 -1 12.34 2.03 -7 -6 -2 134.34 16.31 7 6 2 198.72 13.99 7 6 2 197.95 14.01 7 6 2 185.06 14.18 -7 -6 -2 189.19 15.85 -7 -6 -2 203.81 13.55 7 6 2 183.03 13.30 -7 -6 -2 198.77 14.59 7 6 2 180.57 11.17 7 6 3 253.79 17.03 7 6 3 253.62 16.82 7 6 3 250.02 17.50 -7 -6 -3 226.75 18.58 -7 -6 -3 274.68 17.18 7 6 3 303.17 18.11 -7 -6 -3 285.39 18.74 -7 -6 -3 207.00 20.45 7 6 4 73.72 7.26 7 6 4 72.89 7.47 -7 -6 -4 87.27 9.50 7 6 4 77.95 8.08 -7 -6 -4 71.06 8.45 7 6 4 80.16 7.72 7 6 4 109.91 10.33 -7 -6 -4 97.48 12.09 -7 -6 -5 104.25 10.89 7 6 5 124.21 10.34 7 6 5 131.95 10.17 7 6 5 139.76 9.93 -7 -6 -5 144.69 12.07 7 6 5 138.34 10.57 7 6 5 80.33 10.24 -7 -6 -5 75.54 11.23 -7 -6 -6 96.04 8.95 7 6 6 99.54 8.52 7 6 6 100.01 8.21 7 6 6 100.26 8.88 -7 -6 -6 79.36 9.20 -7 -6 -6 92.09 9.92 7 6 6 93.97 8.85 7 6 6 57.77 8.89 -7 -6 -6 80.60 10.68 -7 -6 -7 305.07 19.56 7 6 7 305.56 18.97 7 6 7 298.28 17.85 7 6 7 300.37 18.59 -7 -6 -7 284.16 19.98 7 6 7 266.39 16.60 -7 -6 -7 324.25 21.29 7 6 7 328.25 19.93 -7 -6 -7 256.26 20.96 7 6 8 86.48 7.75 -7 -6 -8 88.76 9.29 7 6 8 92.66 9.26 -7 -6 -8 86.50 9.17 7 6 8 74.57 8.18 7 6 8 112.73 7.88 -7 -6 -9 11.98 3.89 7 6 9 15.69 3.11 7 6 9 24.59 4.06 7 6 9 37.83 6.04 7 6 9 25.59 4.91 -7 -6 -9 24.41 5.24 7 6 10 15.11 4.11 -7 -6 -10 13.18 4.30 -7 -6 -10 6.86 3.18 7 6 10 12.94 2.89 7 6 10 15.13 4.19 7 6 10 13.65 3.11 7 6 11 12.15 4.03 7 6 11 8.50 2.53 7 6 11 15.58 4.37 7 6 11 16.31 3.57 -7 -6 -11 14.49 4.57 -7 -6 -11 12.30 3.67 7 6 12 251.09 19.70 -7 -6 -12 218.17 17.25 -7 -6 -12 206.36 19.52 7 6 12 305.96 21.83 7 6 12 267.65 16.31 -7 -6 -13 98.65 10.13 7 6 13 124.67 13.02 7 6 13 111.10 12.45 -7 -6 -13 98.96 12.43 7 6 13 108.41 12.95 7 6 13 104.16 8.10 7 6 14 57.54 8.94 7 6 14 53.94 8.77 -7 -6 -14 27.77 7.49 7 6 14 65.14 10.03 -7 -6 -14 29.86 5.57 7 6 15 31.83 2.79 7 6 15 30.77 2.78 -7 -6 -15 37.96 6.05 -7 -6 -15 23.03 7.50 7 6 15 68.10 10.86 7 6 15 59.65 9.67 7 6 15 61.11 9.24 -7 -6 -16 0.42 1.67 -7 -6 -16 0.96 4.03 7 6 16 1.96 3.49 7 6 16 -0.81 2.29 7 6 16 -0.68 2.26 -7 -6 -17 0.80 1.91 7 6 17 0.65 2.31 -7 -6 -17 -2.08 5.38 7 6 17 3.21 4.02 7 6 17 1.74 3.46 -7 -7 14 3.27 5.29 -7 -7 14 -0.51 2.58 -7 -7 13 1.60 5.22 -7 -7 13 7.80 3.36 -7 -7 12 -1.55 5.45 -7 -7 12 0.46 2.29 -7 -7 12 -1.29 2.78 -7 -7 11 -1.50 4.95 -7 -7 11 3.04 2.30 -7 -7 11 4.13 3.06 -7 -7 10 10.04 7.23 -7 -7 10 7.15 3.28 -7 -7 10 10.67 3.37 -7 -7 9 3.05 2.66 -7 -7 9 1.94 2.02 7 7 -8 9.74 4.21 7 7 -8 3.83 2.53 -7 -7 8 5.52 2.65 -7 -7 8 8.98 3.41 -7 -7 7 6.48 5.70 7 7 -7 0.67 2.77 -7 -7 7 1.56 2.81 7 7 -7 4.36 3.23 -7 -7 7 0.35 1.84 -7 -7 7 -0.44 2.18 7 7 -6 27.05 6.26 -7 -7 6 32.34 4.74 -7 -7 6 34.89 5.43 -7 -7 6 38.36 6.35 -7 -7 5 0.71 2.71 7 7 -5 0.58 2.28 -7 -7 5 1.54 1.91 7 7 -5 0.64 2.52 -7 -7 5 6.05 5.99 -7 -7 4 7.76 3.83 7 7 -4 1.64 2.39 -7 -7 4 5.49 2.66 -7 -7 4 1.17 4.74 7 7 -3 1.05 2.29 7 7 -3 1.35 2.40 -7 -7 3 1.05 1.62 7 7 -2 81.68 9.44 7 7 -2 87.25 10.34 -7 -7 2 92.14 8.33 7 7 -2 85.23 9.50 -7 -7 2 82.55 10.64 -7 -7 2 84.54 8.80 -7 -7 2 47.55 10.76 -7 -7 1 9.26 5.60 7 7 -1 3.82 2.69 7 7 -1 2.74 2.49 7 7 -1 5.24 2.83 -7 -7 1 9.19 4.30 -7 -7 1 6.93 2.47 -7 -7 1 5.92 2.62 -7 -7 1 1.82 0.67 7 7 0 94.58 9.23 -7 -7 0 81.26 7.68 7 7 0 71.93 8.70 7 7 0 87.93 9.10 -7 -7 0 67.39 9.65 7 7 0 94.53 9.00 -7 -7 0 98.32 9.22 -7 -7 0 72.89 5.35 -7 -7 -1 2.82 4.04 7 7 1 13.48 3.54 7 7 1 16.44 4.00 7 7 1 9.20 3.18 -7 -7 -1 9.78 4.12 -7 -7 -1 13.28 3.07 7 7 1 14.16 3.45 -7 -7 -1 15.05 4.00 -7 -7 -1 11.82 2.19 -7 -7 -2 15.38 2.71 7 7 2 18.56 3.89 7 7 2 15.56 3.66 -7 -7 -2 4.11 2.98 7 7 2 16.57 3.81 -7 -7 -2 22.20 3.87 -7 -7 -2 13.36 3.87 7 7 2 15.92 3.50 -7 -7 -2 -0.90 3.50 -7 -7 -3 9.52 4.87 7 7 3 31.46 4.90 7 7 3 25.23 4.46 -7 -7 -3 24.36 5.48 7 7 3 27.16 4.70 7 7 3 27.02 4.53 -7 -7 -3 22.98 5.05 7 7 3 32.35 3.83 -7 -7 -3 32.50 4.20 7 7 4 -0.36 1.37 7 7 4 0.69 1.44 7 7 4 0.50 2.53 7 7 4 -0.39 1.41 -7 -7 -4 -0.52 2.38 -7 -7 -4 4.96 3.35 7 7 4 0.80 1.76 -7 -7 -4 0.55 2.12 7 7 5 6.35 2.32 7 7 5 9.24 2.77 -7 -7 -5 0.54 1.97 7 7 5 5.56 2.47 7 7 5 4.20 2.20 -7 -7 -5 5.40 3.07 7 7 5 1.63 2.67 -7 -7 -5 4.78 4.22 7 7 6 3.32 1.88 -7 -7 -6 1.59 1.93 7 7 6 5.52 2.34 7 7 6 4.07 3.21 7 7 6 5.18 2.35 -7 -7 -6 3.34 2.73 -7 -7 -6 -1.52 3.08 7 7 7 2.37 2.00 -7 -7 -7 2.10 2.61 7 7 7 1.34 1.70 7 7 7 1.70 2.11 -7 -7 -7 1.73 2.19 -7 -7 -7 9.20 4.35 7 7 8 27.80 4.34 -7 -7 -8 15.18 4.25 7 7 8 11.47 2.88 -7 -7 -8 21.58 5.12 7 7 8 24.77 4.69 7 7 8 2.56 3.32 -7 -7 -8 26.70 5.16 7 7 8 29.30 4.88 -7 -7 -9 96.32 10.68 7 7 9 92.57 9.91 7 7 9 99.98 8.98 7 7 9 105.77 8.05 -7 -7 -9 97.12 11.00 7 7 9 94.83 10.11 -7 -7 -9 97.51 10.52 7 7 10 -0.52 2.09 -7 -7 -10 0.60 1.98 7 7 10 1.73 1.71 7 7 10 -0.54 2.40 -7 -7 -10 0.54 2.07 -7 -7 -11 8.26 3.36 7 7 11 22.04 5.01 -7 -7 -11 21.58 5.42 -7 -7 -11 15.93 4.94 7 7 11 30.92 6.12 7 7 11 21.13 3.79 7 7 12 1.85 2.72 7 7 12 2.99 1.99 7 7 12 1.30 2.88 7 7 12 -0.32 1.69 -7 -7 -12 1.06 2.33 -7 -7 -13 0.53 2.11 7 7 13 2.16 3.54 7 7 13 0.67 2.40 -7 -7 -14 8.83 3.73 7 7 14 15.03 5.42 -7 -7 -14 9.88 5.13 7 7 14 14.40 5.02 7 7 14 8.24 4.19 -7 -7 -15 13.25 3.93 -7 -7 -15 19.42 6.42 7 7 15 15.62 5.72 7 7 15 10.82 4.71 7 7 15 7.12 4.04 -7 -7 -16 3.51 2.52 -7 -7 -16 8.57 5.23 7 7 16 11.38 5.34 7 7 16 13.31 4.92 7 7 16 11.99 4.51 -7 -7 -17 9.83 3.63 -7 -7 -17 13.31 7.05 7 7 17 31.04 8.52 7 7 17 26.34 6.22 7 7 17 27.53 7.41 7 7 18 0.64 2.39 -7 -7 -18 0.47 2.50 -7 -8 13 8.82 7.81 -7 -8 13 6.49 3.07 -7 -8 12 -1.71 5.17 -7 -8 12 0.44 1.97 -7 -8 11 14.34 3.78 -7 -8 11 21.20 5.32 -7 -8 10 6.34 7.20 -7 -8 10 18.44 4.17 -7 -8 10 19.09 4.91 7 8 -9 1.19 2.31 -7 -8 9 -0.51 2.31 -7 -8 9 0.77 1.87 -7 -8 8 -1.49 5.65 7 8 -8 -1.63 3.06 -7 -8 8 8.11 2.87 -7 -8 8 10.48 3.58 -7 -8 7 0.36 1.69 -7 -8 7 2.25 2.43 7 8 -7 0.69 2.57 -7 -8 7 7.24 6.87 7 8 -6 101.45 12.13 -7 -8 6 98.57 12.45 -7 -8 5 180.34 12.87 -7 -8 5 129.11 14.88 7 8 -5 149.26 14.58 -7 -8 4 -0.77 2.95 7 8 -4 -0.64 3.08 -7 -8 4 3.97 5.07 -7 -8 4 -0.39 1.93 7 8 -3 9.33 3.71 -7 -8 3 9.08 4.44 -7 -8 3 7.19 2.80 7 8 -3 7.14 3.43 -7 -8 3 -1.27 4.32 7 8 -2 36.66 7.48 -7 -8 2 54.67 6.36 -7 -8 2 54.70 8.96 7 8 -2 50.98 7.41 -7 -8 2 53.72 7.31 -7 -8 2 48.85 11.07 -7 -8 1 14.86 2.15 7 8 -1 21.50 5.19 7 8 -1 21.58 4.71 -7 -8 1 20.13 5.73 -7 -8 1 24.30 4.24 -7 -8 1 20.58 4.70 -7 -8 1 8.15 6.20 -7 -8 0 168.05 19.56 7 8 0 159.62 13.26 -7 -8 0 170.91 12.63 7 8 0 161.14 14.03 -7 -8 0 157.50 15.42 7 8 0 143.94 13.11 -7 -8 0 120.10 10.71 7 8 0 178.76 14.05 -7 -8 0 200.18 14.76 -7 -8 0 159.23 9.86 -7 -8 -1 28.31 8.33 7 8 1 52.20 6.67 7 8 1 54.11 7.13 -7 -8 -1 50.00 8.01 7 8 1 49.88 6.80 -7 -8 -1 35.03 4.61 -7 -8 -1 45.90 5.86 7 8 1 44.70 6.28 -7 -8 -1 65.21 8.11 -7 -8 -1 45.99 4.74 -7 -8 -2 2.64 1.71 7 8 2 2.67 2.24 7 8 2 3.70 2.26 -7 -8 -2 3.21 3.19 7 8 2 0.46 2.09 -7 -8 -2 7.41 2.65 -7 -8 -2 -0.38 1.29 -7 -8 -2 2.72 2.99 7 8 2 2.90 2.31 -7 -8 -2 3.99 4.05 7 8 3 139.50 11.52 7 8 3 150.96 11.90 -7 -8 -3 130.00 13.38 7 8 3 149.13 12.29 7 8 3 147.87 11.97 7 8 3 109.05 11.50 -7 -8 -3 155.06 13.75 -7 -8 -3 142.63 10.65 -7 -8 -4 86.12 12.34 7 8 4 53.22 6.76 7 8 4 53.27 6.72 7 8 4 63.83 7.65 -7 -8 -4 71.73 9.30 7 8 4 67.64 7.84 7 8 4 100.63 10.09 -7 -8 -4 72.33 9.23 7 8 4 67.49 6.46 -7 -8 -4 58.68 6.72 -7 -8 -5 28.17 4.98 7 8 5 38.51 4.99 7 8 5 41.56 5.60 7 8 5 39.39 5.36 7 8 5 30.76 6.44 7 8 5 48.78 6.52 -7 -8 -5 34.61 6.55 7 8 5 43.86 6.14 7 8 6 94.97 8.58 -7 -8 -6 83.73 10.30 7 8 6 86.17 9.02 7 8 6 70.70 9.82 7 8 6 88.65 9.06 -7 -8 -6 85.67 10.03 7 8 7 -0.37 1.87 7 8 7 -1.91 3.11 7 8 7 0.91 2.03 -7 -8 -7 -0.65 2.58 -7 -8 -7 1.18 2.14 7 8 7 -0.45 1.95 7 8 8 0.75 1.77 7 8 8 0.66 3.10 -7 -8 -8 -0.67 2.52 7 8 8 1.44 2.46 -7 -8 -8 1.19 2.53 -7 -8 -9 1.21 2.18 7 8 9 -0.42 1.55 7 8 9 1.54 2.20 7 8 9 3.83 2.60 -7 -8 -9 2.06 2.85 7 8 9 -0.51 1.85 -7 -8 -9 0.68 2.28 7 8 10 10.70 2.69 7 8 10 5.79 3.18 7 8 10 18.21 4.69 -7 -8 -10 11.62 4.07 7 8 11 61.34 8.69 7 8 11 57.69 5.84 -7 -8 -11 50.80 7.88 -7 -8 -12 22.07 5.49 7 8 12 27.29 6.13 7 8 12 22.54 3.74 7 8 12 28.65 6.29 -7 -8 -12 18.85 4.81 7 8 12 25.34 4.12 -7 -8 -13 -0.61 2.44 7 8 13 1.37 2.45 7 8 13 2.70 1.90 7 8 13 0.71 2.99 7 8 13 1.15 1.34 7 8 14 4.43 3.37 7 8 14 1.80 1.99 -7 -8 -14 -0.60 2.85 7 8 14 0.78 3.26 7 8 14 0.19 1.19 7 8 15 21.22 5.73 7 8 15 29.71 7.34 7 8 15 26.97 6.72 7 8 16 -0.72 2.70 -7 -8 -16 -0.58 2.62 7 8 16 0.92 3.28 7 8 16 -1.71 3.71 -7 -8 -17 19.97 5.41 7 8 17 41.45 8.03 -7 -8 -18 1.70 2.19 7 8 18 2.01 2.73 -7 -9 11 1.81 5.92 -7 -9 10 -1.75 5.35 -7 -9 10 3.32 3.25 7 9 -9 13.25 4.66 -7 -9 9 26.08 5.55 -7 -9 8 6.61 6.91 7 9 -8 6.75 4.51 -7 -9 8 7.90 3.38 -7 -9 7 1.88 2.53 -7 -9 7 -1.62 5.78 -7 -9 6 12.19 3.65 7 9 -6 7.06 3.91 -7 -9 6 1.58 6.02 -7 -9 5 8.28 3.20 7 9 -5 8.32 3.94 -7 -9 5 2.54 3.05 7 9 -4 61.72 9.11 -7 -9 4 63.59 10.21 7 9 -3 261.28 20.74 -7 -9 3 297.95 24.12 7 9 -2 11.96 4.18 -7 -9 2 11.28 5.06 -7 -9 2 11.79 3.44 -7 -9 2 18.63 4.78 -7 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401.63 24.74 -7 -9 -5 387.81 26.90 7 9 6 41.37 5.81 -7 -9 -6 48.11 6.89 -7 -9 -6 40.14 7.35 7 9 6 49.98 7.02 7 9 6 46.68 6.31 7 9 6 50.69 7.14 -7 -9 -6 48.62 8.56 -7 -9 -6 51.37 10.24 -7 -9 -7 -1.33 2.69 7 9 7 1.01 2.10 7 9 7 0.50 2.30 -7 -9 -7 0.74 2.78 -7 -9 -7 0.52 2.25 -7 -9 -8 17.52 5.32 -7 -9 -8 21.51 5.21 -7 -9 -8 12.90 5.57 7 9 9 236.92 17.18 -7 -9 -9 204.93 17.70 -7 -9 -10 31.37 7.32 7 9 10 33.99 3.99 -7 -9 -11 17.30 5.20 7 9 11 23.77 3.78 7 9 11 37.83 6.96 7 9 11 43.19 7.15 7 9 12 3.23 2.96 -7 -9 -12 4.20 3.32 -7 -9 -12 8.46 3.65 7 9 12 7.11 2.22 7 9 12 3.93 3.53 7 9 12 3.60 1.76 7 9 13 137.26 13.50 7 9 13 63.24 6.51 -7 -9 -13 53.74 9.62 7 9 13 125.00 13.04 7 9 13 87.65 7.72 7 9 14 50.22 5.79 7 9 14 75.53 10.58 7 9 14 68.43 10.37 -7 -9 -14 57.53 9.29 7 9 15 0.05 0.46 -7 -9 -15 2.06 2.97 7 9 15 0.64 0.50 7 9 15 1.48 1.77 7 9 15 1.39 2.46 7 9 15 0.84 3.16 7 9 15 1.62 3.38 7 9 16 4.39 3.98 -7 -9 -16 7.42 4.29 7 9 16 15.48 6.24 7 9 16 7.82 4.36 7 9 17 1.46 2.99 -7 -9 -17 1.33 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5 98.21 10.62 -8 6 5 71.13 9.09 8 -6 -5 95.41 8.01 8 -6 -5 84.46 10.01 8 -6 -4 144.93 11.91 -8 6 4 142.60 12.14 -8 6 4 116.13 11.73 -8 6 4 104.87 11.57 8 -6 -4 103.78 13.80 8 -6 -4 141.03 9.60 8 -6 -4 144.05 12.97 -8 6 3 65.46 8.27 8 -6 -3 101.21 9.49 -8 6 3 102.35 9.50 8 -6 -3 64.03 10.85 -8 6 2 36.76 5.71 8 -6 -2 35.81 5.49 8 -6 -2 39.89 7.99 -8 6 2 37.65 5.59 -8 6 2 40.10 6.32 -8 6 1 250.25 15.95 8 -6 -1 250.97 16.77 -8 6 1 198.20 15.07 8 -6 -1 197.87 10.85 -8 6 1 247.87 17.86 -8 6 1 220.02 18.10 8 -6 -1 196.99 18.66 -8 6 0 201.78 13.79 -8 6 0 201.21 12.30 8 -6 0 190.03 14.50 -8 6 0 182.26 13.73 8 -6 0 174.55 10.15 -8 6 0 179.09 15.39 -8 6 0 157.50 15.69 8 -6 0 162.56 16.58 -8 6 -1 59.18 6.25 8 -6 1 48.54 5.65 -8 6 -1 54.06 4.81 -8 6 -1 59.87 6.75 -8 6 -1 47.26 8.24 -8 6 -1 59.67 8.09 8 -6 1 47.57 5.66 8 -6 1 53.96 4.69 8 -6 1 49.19 6.82 8 -6 2 -0.44 1.70 8 -6 2 0.27 1.14 8 -6 2 -0.57 3.08 8 -6 2 0.97 1.05 8 -6 2 -0.67 1.95 -8 6 -2 0.73 2.28 -8 6 -2 0.56 1.78 8 -6 3 10.22 3.15 8 -6 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5.96 8 -6 11 20.08 2.27 -8 6 -11 24.19 6.03 -8 6 -12 1.30 3.19 8 -6 12 1.98 0.79 8 -6 13 91.53 12.69 -8 6 -13 89.82 11.44 -8 6 -14 4.91 4.49 -8 6 -14 9.21 4.64 8 -6 14 4.86 4.74 8 -6 15 -1.04 3.68 -8 6 -15 2.75 4.58 -8 6 -15 -0.79 2.80 -8 6 -16 4.08 5.51 -8 6 -16 0.82 3.37 -8 6 -17 -1.11 5.11 -8 6 -17 1.67 3.41 -8 6 -18 23.54 6.73 -8 5 14 14.66 3.54 8 -5 -14 12.21 5.34 -8 5 13 19.81 6.98 -8 5 13 26.69 7.06 8 -5 -13 17.22 3.68 -8 5 13 23.41 4.09 8 -5 -13 13.37 5.18 -8 5 12 4.56 4.31 -8 5 12 6.46 4.21 -8 5 12 4.48 2.16 8 -5 -12 5.66 3.55 8 -5 -11 5.74 3.59 -8 5 11 5.04 3.83 -8 5 11 0.75 3.44 8 -5 -11 3.05 2.20 -8 5 11 3.46 1.74 8 -5 -11 7.99 3.70 8 -5 -10 2.29 2.40 -8 5 10 0.77 2.94 -8 5 10 2.10 3.67 8 -5 -10 3.20 2.26 -8 5 10 2.38 1.40 8 -5 -10 1.71 2.23 -8 5 9 0.53 0.98 8 -5 -9 -0.51 2.15 -8 5 9 -1.41 3.10 -8 5 9 -1.30 2.87 8 -5 -9 -0.83 1.89 8 -5 -9 -0.91 3.76 -8 5 9 0.14 0.94 8 -5 -9 -0.53 1.87 -8 5 8 195.26 15.52 -8 5 8 171.34 15.12 8 -5 -8 77.95 13.05 8 -5 -8 176.14 12.85 -8 5 8 103.49 9.20 8 -5 -8 161.33 12.79 8 -5 -8 167.81 13.47 -8 5 7 198.17 15.12 -8 5 7 179.73 14.73 8 -5 -7 74.87 12.69 8 -5 -7 167.82 12.70 -8 5 7 91.04 11.64 -8 5 7 109.26 10.10 8 -5 -7 157.02 12.05 8 -5 -7 189.79 13.73 -8 5 6 19.13 4.63 -8 5 6 25.46 5.33 8 -5 -6 24.30 7.20 -8 5 6 23.00 5.67 8 -5 -6 16.95 3.76 -8 5 6 17.89 4.18 8 -5 -6 18.54 4.53 -8 5 5 200.59 15.29 -8 5 5 203.50 15.32 8 -5 -5 222.27 15.36 -8 5 5 143.99 14.41 8 -5 -5 190.54 12.88 -8 5 5 143.84 13.15 8 -5 -5 195.25 14.81 -8 5 4 57.37 7.31 -8 5 4 64.05 7.52 8 -5 -4 60.61 7.38 8 -5 -4 49.66 9.16 -8 5 4 62.19 8.08 8 -5 -4 52.06 5.50 -8 5 4 58.63 7.37 8 -5 -4 54.81 7.26 -8 5 3 35.08 5.17 -8 5 3 33.59 5.28 8 -5 -3 33.24 7.57 8 -5 -3 40.02 5.89 8 -5 -3 29.31 3.73 -8 5 2 61.47 7.29 -8 5 2 56.85 6.86 8 -5 -2 61.51 6.99 8 -5 -2 69.36 7.73 8 -5 -2 52.77 9.38 8 -5 -2 48.42 4.47 -8 5 1 18.17 3.96 -8 5 1 11.39 2.99 8 -5 -1 16.35 3.60 -8 5 1 12.29 3.58 -8 5 1 24.13 5.26 8 -5 -1 13.70 1.89 8 -5 -1 30.15 6.65 8 -5 -1 12.69 3.48 8 -5 0 159.83 12.80 -8 5 0 174.06 12.32 -8 5 0 167.16 11.78 8 -5 0 127.36 7.23 8 -5 0 154.71 15.16 -8 5 0 164.57 13.54 -8 5 0 157.36 13.99 -8 5 -1 178.67 12.69 -8 5 -1 176.43 13.29 8 -5 1 193.12 10.46 -8 5 -1 165.34 14.71 -8 5 -1 142.39 14.75 8 -5 1 189.55 16.85 8 -5 1 167.79 13.89 8 -5 2 169.98 13.72 -8 5 -2 167.77 9.57 -8 5 -2 162.01 11.88 8 -5 2 156.94 14.38 8 -5 2 176.09 10.44 8 -5 2 213.95 13.24 -8 5 -2 168.12 15.75 8 -5 2 178.23 16.22 -8 5 -2 162.01 14.57 8 -5 3 3.45 2.15 -8 5 -3 1.80 1.47 8 -5 3 2.08 1.48 8 -5 3 -0.54 2.39 8 -5 3 0.36 2.06 -8 5 -3 -0.68 2.76 -8 5 -3 2.67 2.18 8 -5 4 321.36 18.83 8 -5 4 327.31 22.75 8 -5 4 314.64 21.34 8 -5 4 330.18 20.97 -8 5 -4 325.50 24.85 -8 5 -4 339.26 23.37 8 -5 5 136.52 12.01 8 -5 5 173.51 13.80 -8 5 -5 157.22 15.50 -8 5 -5 136.85 13.01 8 -5 5 125.31 11.41 8 -5 5 130.58 9.57 -8 5 -6 156.89 16.49 8 -5 6 161.23 13.74 8 -5 6 167.22 14.10 -8 5 -6 188.22 15.64 8 -5 6 183.47 11.46 8 -5 6 177.27 13.86 -8 5 -7 56.34 9.71 8 -5 7 72.35 8.21 8 -5 7 58.06 7.70 -8 5 -7 71.38 9.12 8 -5 7 74.03 6.05 8 -5 7 79.00 8.42 8 -5 8 1.09 1.33 8 -5 8 -1.87 1.89 8 -5 8 1.88 2.29 -8 5 -8 -0.84 3.05 -8 5 -8 -0.58 1.98 8 -5 8 -0.47 2.12 8 -5 8 1.01 1.23 8 -5 9 317.67 19.99 -8 5 -9 321.78 27.80 -8 5 -9 441.18 27.38 8 -5 9 430.25 25.92 8 -5 9 435.01 20.95 8 -5 10 341.41 18.61 -8 5 -10 306.58 23.70 8 -5 10 304.79 24.69 8 -5 11 0.77 3.79 8 -5 11 1.49 2.62 8 -5 11 4.08 1.58 -8 5 -11 5.12 2.94 8 -5 12 4.15 3.34 8 -5 12 3.50 1.59 8 -5 12 -2.24 4.02 8 -5 13 12.48 5.06 -8 5 -13 7.59 4.72 -8 5 -13 6.81 3.97 8 -5 13 9.15 2.17 -8 5 -14 60.83 9.28 -8 5 -14 41.98 8.92 8 -5 14 58.84 10.55 8 -5 14 48.11 4.77 -8 5 -15 63.14 9.79 8 -5 15 77.87 12.26 8 -5 15 60.92 5.35 8 -5 16 1.08 3.31 -8 5 -16 5.94 3.58 -8 5 -16 7.49 5.66 -8 5 -17 15.00 5.10 -8 5 -17 6.97 5.60 -8 5 -18 17.99 5.41 8 -4 -14 0.65 1.59 -8 4 14 0.86 1.98 8 -4 -14 0.89 3.65 -8 4 13 34.83 8.34 -8 4 13 19.90 6.63 8 -4 -13 27.01 4.73 -8 4 13 31.37 5.08 8 -4 -13 22.53 6.48 8 -4 -12 4.38 3.56 -8 4 12 1.79 3.57 -8 4 12 3.87 3.53 8 -4 -12 5.62 2.56 -8 4 12 4.29 2.26 8 -4 -12 3.67 3.00 8 -4 -11 42.96 7.78 -8 4 11 52.74 9.33 -8 4 11 41.85 8.24 8 -4 -11 43.47 6.34 -8 4 11 51.20 5.66 8 -4 -11 38.34 6.80 8 -4 -10 -0.59 2.81 -8 4 10 0.76 3.34 -8 4 10 -0.67 2.83 8 -4 -10 0.87 1.99 -8 4 10 0.44 1.26 8 -4 -10 2.07 2.73 8 -4 -9 58.74 7.91 -8 4 9 68.64 9.73 -8 4 9 66.97 9.11 8 -4 -9 52.62 7.11 -8 4 9 62.10 4.93 8 -4 -9 52.20 7.32 8 -4 -8 19.01 4.51 8 -4 -8 7.19 4.95 -8 4 8 10.77 4.33 -8 4 8 14.56 4.57 8 -4 -8 17.19 4.26 8 -4 -8 16.77 4.11 -8 4 7 15.14 4.46 -8 4 7 23.63 5.18 -8 4 7 10.62 1.21 8 -4 -7 12.32 3.59 8 -4 -7 17.66 3.96 -8 4 6 34.71 6.05 -8 4 6 38.15 6.19 -8 4 6 34.92 4.42 8 -4 -6 32.60 5.15 8 -4 -6 33.60 5.31 -8 4 5 40.38 6.13 -8 4 5 42.85 6.20 8 -4 -5 40.05 6.06 -8 4 5 30.10 5.98 8 -4 -5 38.39 5.18 -8 4 5 34.37 4.88 8 -4 -5 44.35 5.88 -8 4 4 -0.42 1.80 8 -4 -4 0.79 2.65 -8 4 4 1.55 2.09 -8 4 4 0.72 1.67 -8 4 4 -0.88 1.78 8 -4 -4 -0.46 1.85 -8 4 3 72.13 7.89 8 -4 -3 72.78 7.89 -8 4 3 67.21 7.35 8 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7.70 3.91 -8 -4 -6 17.88 4.81 8 4 7 209.93 14.36 -8 -4 -7 225.12 14.91 8 4 7 202.71 13.35 -8 -4 -7 196.14 14.74 8 4 7 106.00 13.76 8 4 7 231.39 15.22 -8 -4 -7 134.86 14.45 8 4 8 20.48 6.42 8 4 8 81.82 8.23 -8 -4 -8 75.57 8.10 8 4 8 41.61 5.70 -8 -4 -8 50.68 6.64 8 4 8 62.30 6.21 8 4 8 89.87 8.84 -8 -4 -8 63.47 8.34 8 4 9 0.67 3.26 8 4 9 4.66 2.39 8 4 9 0.80 1.31 8 4 9 2.96 2.12 -8 -4 -9 0.50 2.17 8 4 9 1.15 1.41 8 4 9 2.58 2.64 8 4 9 3.03 2.19 8 4 10 7.69 3.23 8 4 10 7.59 2.42 8 4 10 8.61 2.79 -8 -4 -10 5.51 3.19 -8 -4 -10 7.64 2.87 8 4 10 4.54 1.95 8 4 10 2.31 2.58 8 4 10 7.40 3.21 8 4 11 9.55 3.69 -8 -4 -11 18.84 4.96 -8 -4 -11 10.16 3.10 8 4 11 6.64 2.71 8 4 11 14.76 3.32 8 4 11 10.25 4.47 8 4 11 9.66 4.53 8 4 11 6.34 3.18 -8 -4 -12 38.02 5.67 8 4 12 30.65 6.29 8 4 12 42.57 5.69 8 4 12 35.83 5.69 8 4 12 38.87 7.78 8 4 12 43.48 7.85 8 4 12 35.07 5.16 -8 -4 -13 15.35 3.76 8 4 13 21.29 5.61 8 4 13 25.29 4.95 8 4 13 28.32 7.05 -8 -4 -13 7.00 4.82 8 4 13 17.26 3.51 -8 -4 -14 4.25 2.07 8 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13.01 -10 8 -8 68.76 13.29 -10 8 -8 72.14 11.51 10 -8 9 1.05 3.75 -10 8 -9 -1.25 4.48 -10 8 -9 4.46 4.37 10 -8 10 -0.60 1.24 10 -8 10 -0.26 1.19 10 -8 10 -1.38 4.26 -10 8 -10 1.30 4.00 -10 8 -10 -0.91 2.82 10 -8 11 0.82 2.72 -10 8 -11 -0.94 2.90 10 -8 12 -0.89 4.31 -10 8 -13 0.99 4.08 -10 8 -14 2.02 3.97 10 -7 -12 33.35 5.84 10 -7 -11 1.88 2.40 10 -7 -10 33.06 5.91 -10 7 10 40.86 8.63 -10 7 10 42.33 8.80 10 -7 -9 24.09 5.00 -10 7 9 35.22 7.67 -10 7 9 27.01 6.72 -10 7 8 18.17 5.74 10 -7 -8 11.28 3.77 -10 7 8 6.36 4.15 -10 7 8 5.67 2.66 -10 7 8 20.47 5.99 -10 7 7 7.62 3.82 10 -7 -7 7.33 3.17 -10 7 7 4.47 3.88 -10 7 7 5.39 2.82 -10 7 7 3.50 3.32 -10 7 6 6.31 3.67 10 -7 -6 6.41 3.03 -10 7 6 15.34 5.30 -10 7 6 6.08 3.20 -10 7 6 5.83 3.60 -10 7 5 90.08 10.62 -10 7 5 76.02 10.14 -10 7 5 98.62 10.64 -10 7 5 64.13 9.31 10 -7 -5 66.95 10.02 -10 7 4 138.14 12.57 -10 7 4 123.43 11.41 -10 7 4 87.28 10.90 -10 7 4 66.71 10.45 10 -7 -4 107.19 12.44 -10 7 3 52.93 7.57 -10 7 3 55.85 7.14 10 -7 -3 65.52 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43.32 7.83 -10 3 8 27.17 6.36 10 -3 -8 30.46 6.46 10 -3 -8 26.99 4.88 -10 3 7 126.83 12.63 -10 3 7 123.66 12.43 10 -3 -7 56.91 12.74 -10 3 7 58.25 10.15 10 -3 -7 150.87 13.95 10 -3 -7 120.82 10.07 -10 3 6 147.33 13.26 -10 3 6 141.64 12.70 10 -3 -6 54.10 12.22 -10 3 6 65.11 10.49 10 -3 -6 149.86 14.16 10 -3 -6 119.09 9.96 -10 3 5 7.72 3.39 -10 3 5 5.66 3.23 -10 3 5 6.10 3.97 10 -3 -5 8.32 2.35 10 -3 -5 4.02 3.14 10 -3 -5 8.20 2.80 -10 3 4 24.35 6.07 10 -3 -4 30.88 4.51 10 -3 -4 44.04 10.14 -10 3 4 29.17 5.71 10 -3 -4 32.63 4.82 10 -3 -3 13.95 3.99 -10 3 3 10.29 3.46 -10 3 3 6.61 3.55 10 -3 -3 8.41 2.68 10 -3 -3 9.65 5.72 10 -3 -3 8.55 3.88 10 -3 -3 10.07 2.80 -10 3 2 50.27 6.85 10 -3 -2 47.64 7.00 -10 3 2 56.98 8.10 10 -3 -2 46.63 6.03 10 -3 -2 63.12 11.95 10 -3 -2 48.03 7.89 10 -3 -2 39.23 5.63 -10 3 1 300.88 21.65 -10 3 1 353.65 21.53 10 -3 -1 332.58 21.70 -10 3 0 32.63 5.65 10 -3 0 30.90 5.36 -10 3 0 38.65 5.49 10 -3 0 31.05 6.39 10 -3 0 23.95 7.37 -10 3 -1 7.19 3.26 10 -3 1 4.23 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68.86 11.23 10 -3 7 83.49 13.45 10 -3 7 138.31 13.37 10 -3 8 469.96 25.31 10 -3 8 385.55 24.83 10 -3 8 468.57 28.45 10 -3 8 434.05 24.24 -10 3 -8 430.87 28.76 10 -3 8 314.17 28.60 10 -3 8 342.22 31.68 10 -3 8 482.58 30.77 10 -3 9 128.62 10.38 10 -3 9 112.14 9.60 10 -3 9 140.14 12.90 -10 3 -9 133.51 13.38 10 -3 9 145.79 15.13 10 -3 10 12.30 5.01 10 -3 10 2.27 1.38 10 -3 10 0.90 2.99 -10 3 -10 12.08 4.14 10 -3 10 12.61 2.99 10 -3 11 14.25 3.27 10 -3 11 7.89 4.74 10 -3 11 7.93 1.39 10 -3 11 6.58 4.38 10 -3 12 1.93 1.92 10 -3 12 2.80 4.43 10 -3 12 3.16 2.40 10 -3 13 77.49 7.52 10 -3 13 71.57 12.02 10 -3 13 72.06 9.28 10 -3 14 89.23 8.39 10 -3 14 83.84 10.92 10 -3 14 101.36 14.54 10 -3 15 1.92 2.94 10 -3 15 5.60 4.67 10 -2 -13 0.65 2.52 10 -2 -12 16.20 6.07 -10 2 11 0.79 3.42 -10 2 11 2.21 1.41 10 -2 -11 5.80 4.14 -10 2 11 2.55 3.55 10 -2 -10 22.14 6.12 -10 2 10 21.24 6.17 -10 2 10 15.53 2.07 10 -2 -10 22.06 4.29 -10 2 10 30.85 6.86 -10 2 9 6.22 3.92 10 -2 -9 5.31 2.56 -10 2 9 2.90 3.32 -10 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6.55 4.11 -10 -2 9 -1.88 3.07 -10 -2 9 0.35 1.86 -10 -2 9 -2.17 4.09 -10 -2 9 -2.00 3.96 -10 -2 8 5.91 3.44 -10 -2 8 6.91 2.44 -10 -2 8 2.14 3.83 -10 -2 8 9.87 4.15 -10 -2 7 0.75 1.24 -10 -2 7 -1.11 2.82 -10 -2 7 1.13 2.60 -10 -2 6 6.51 2.08 -10 -2 6 8.86 3.83 -10 -2 6 10.94 3.77 -10 -2 5 98.20 10.05 -10 -2 5 97.12 9.90 -10 -2 5 89.84 7.00 -10 -2 4 3.69 2.43 -10 -2 4 1.74 2.01 10 2 -4 6.89 3.84 -10 -2 4 2.61 1.58 -10 -2 4 0.99 3.11 -10 -2 3 84.55 8.56 10 2 -3 77.28 9.98 -10 -2 3 74.75 7.84 10 2 -3 60.24 10.21 -10 -2 3 41.66 7.77 -10 -2 3 66.41 5.74 -10 -2 3 78.61 12.29 -10 -2 2 23.60 7.15 -10 -2 2 36.29 5.39 10 2 -2 30.73 6.11 -10 -2 2 33.30 4.83 10 2 -2 20.38 6.19 -10 -2 2 17.48 5.03 -10 -2 2 30.37 3.63 10 2 -2 19.66 4.17 -10 -2 1 0.91 3.54 10 2 -1 13.23 4.23 -10 -2 1 12.81 3.37 -10 -2 1 18.87 3.51 10 2 -1 6.78 4.27 -10 -2 1 9.64 4.00 -10 -2 1 13.67 2.59 10 2 -1 5.97 2.90 10 2 0 4.26 3.02 10 2 0 6.97 3.49 10 2 0 7.21 5.21 -10 -2 0 10.60 4.95 10 2 0 6.90 3.22 -10 -2 0 7.87 2.36 -10 -2 0 10.03 3.00 10 2 0 12.30 4.75 -10 -2 0 5.70 3.40 -10 -2 0 8.75 2.18 10 2 0 7.22 1.51 10 2 1 3.04 4.77 -10 -2 -1 18.69 6.19 10 2 1 29.69 5.56 -10 -2 -1 36.92 5.05 -10 -2 -1 39.30 4.58 10 2 1 29.75 6.47 -10 -2 -1 18.42 4.57 10 2 1 25.36 3.50 10 2 1 22.71 5.12 10 2 1 30.34 6.35 10 2 1 33.84 3.50 10 2 2 9.01 5.82 -10 -2 -2 27.72 6.76 10 2 2 29.61 5.52 -10 -2 -2 36.83 4.59 10 2 2 32.31 6.60 -10 -2 -2 31.07 5.42 10 2 2 30.45 3.84 10 2 2 36.34 4.13 10 2 2 29.17 6.10 10 2 2 29.00 5.91 10 2 3 69.00 8.90 10 2 3 79.01 8.47 -10 -2 -3 80.00 7.01 10 2 3 73.10 7.50 10 2 3 71.23 9.53 -10 -2 -3 58.31 7.30 10 2 3 72.18 6.04 10 2 3 81.45 6.88 10 2 4 0.58 2.20 -10 -2 -4 -0.76 2.93 10 2 4 6.98 5.34 10 2 4 -0.45 2.18 10 2 4 0.34 1.42 10 2 4 -1.13 2.95 -10 -2 -4 0.31 1.42 10 2 4 0.75 1.49 10 2 4 3.36 2.78 10 2 4 0.33 1.53 10 2 5 8.05 4.16 -10 -2 -5 8.15 4.27 10 2 5 13.31 4.15 10 2 5 11.44 3.37 10 2 5 16.03 3.21 10 2 5 4.96 4.88 10 2 5 3.86 3.15 10 2 5 11.13 2.80 10 2 5 16.78 3.65 10 2 6 -1.00 3.98 10 2 6 4.79 2.25 10 2 6 1.89 1.46 10 2 6 5.33 2.32 10 2 6 5.10 3.31 10 2 6 5.58 3.90 10 2 6 2.91 2.43 10 2 6 6.03 2.75 10 2 7 1.89 1.72 10 2 7 2.96 1.62 10 2 7 2.05 1.94 10 2 7 2.84 3.46 10 2 7 0.87 3.46 10 2 7 3.53 2.67 10 2 8 47.15 5.70 10 2 8 37.98 4.11 10 2 8 33.70 4.91 10 2 8 43.16 7.51 10 2 8 30.06 7.84 10 2 9 1.74 1.19 10 2 9 0.32 1.61 10 2 9 4.47 3.01 10 2 9 5.10 4.62 10 2 9 3.60 2.81 10 2 9 -1.01 4.40 10 2 10 10.16 2.23 10 2 10 10.66 2.77 10 2 10 11.22 3.74 10 2 10 9.52 4.32 10 2 10 12.26 4.36 10 2 10 8.21 5.32 10 2 10 11.52 4.27 10 2 11 9.77 4.37 10 2 11 9.65 2.98 10 2 11 8.15 2.19 10 2 11 3.93 2.90 10 2 11 8.33 4.76 10 2 11 9.94 4.05 10 2 11 4.15 5.03 10 2 11 13.48 4.60 10 2 11 7.35 2.33 10 2 12 8.93 2.45 10 2 12 11.27 5.06 10 2 12 5.53 2.79 10 2 12 -1.04 3.88 10 2 12 7.54 4.19 10 2 13 1.38 1.96 10 2 13 4.43 3.73 10 2 13 0.44 1.94 10 2 13 -1.04 3.65 10 2 13 -0.82 2.74 10 2 14 5.05 2.65 10 2 14 2.70 3.41 10 2 14 5.12 2.43 10 2 14 8.22 6.08 10 2 14 -0.83 3.16 10 2 14 3.53 3.53 10 2 15 1.42 1.51 10 2 15 3.20 1.78 10 2 15 2.00 4.07 10 2 15 0.91 3.25 10 2 15 0.95 3.18 10 2 15 4.05 3.69 10 2 16 2.12 1.92 10 2 16 4.98 5.15 10 2 16 -1.02 3.86 10 2 17 1.09 4.29 10 2 17 -1.02 2.10 10 2 18 1.35 3.12 -10 -3 13 2.44 4.46 -10 -3 12 2.44 4.99 -10 -3 11 3.46 3.35 -10 -3 11 -4.84 4.75 -10 -3 10 52.83 6.75 -10 -3 10 40.75 7.86 -10 -3 9 17.12 3.98 -10 -3 9 11.18 4.40 -10 -3 8 21.17 5.38 -10 -3 8 20.39 4.04 -10 -3 8 8.00 5.46 -10 -3 8 19.51 5.25 -10 -3 7 5.83 2.30 -10 -3 7 5.91 3.42 -10 -3 7 7.31 3.58 -10 -3 6 180.60 14.38 -10 -3 6 161.00 11.40 -10 -3 6 184.60 14.69 -10 -3 5 44.86 6.68 -10 -3 5 47.36 5.23 -10 -3 5 27.70 8.26 -10 -3 5 43.47 6.57 -10 -3 4 11.45 5.81 -10 -3 4 10.66 2.65 -10 -3 4 10.35 3.40 -10 -3 4 16.08 4.00 -10 -3 3 30.46 8.55 -10 -3 3 53.29 6.66 10 3 -3 48.46 8.33 -10 -3 3 56.79 6.72 -10 -3 3 38.15 7.21 -10 -3 3 51.36 5.41 10 3 -3 34.34 5.05 -10 -3 2 11.88 5.39 10 3 -2 12.74 4.24 -10 -3 2 15.39 3.76 -10 -3 2 12.24 3.19 10 3 -2 17.18 4.86 10 3 -2 9.18 4.72 -10 -3 2 3.59 3.18 -10 -3 2 11.68 2.69 10 3 -2 2.91 2.34 10 3 -1 254.86 18.59 -10 -3 1 243.35 16.16 -10 -3 1 246.20 15.32 10 3 -1 252.21 18.67 10 3 -1 162.78 14.61 10 3 -1 226.62 19.43 -10 -3 1 166.25 16.19 -10 -3 1 251.56 14.61 -10 -3 1 144.37 18.44 10 3 0 143.24 13.25 -10 -3 0 146.98 11.68 -10 -3 0 150.69 10.96 -10 -3 0 138.80 12.78 -10 -3 0 103.69 14.46 -10 -3 0 151.60 10.64 10 3 0 103.53 10.94 10 3 0 141.01 14.51 -10 -3 -1 -2.70 4.00 10 3 1 5.89 3.30 10 3 1 4.69 3.48 -10 -3 -1 5.70 2.11 10 3 1 8.02 2.27 -10 -3 -1 0.95 2.20 -10 -3 -1 9.61 2.67 10 3 1 2.44 2.23 10 3 2 16.13 4.59 10 3 2 1.02 4.36 -10 -3 -2 9.56 4.67 10 3 2 25.17 5.16 -10 -3 -2 30.81 4.26 10 3 2 16.36 4.97 10 3 2 22.91 3.49 -10 -3 -2 16.31 4.04 -10 -3 -2 17.14 3.45 10 3 2 24.61 2.98 10 3 3 -0.59 2.37 10 3 3 1.19 1.97 10 3 3 2.02 3.60 -10 -3 -3 -0.84 2.83 10 3 3 2.45 2.46 10 3 3 4.76 3.10 -10 -3 -3 0.85 1.89 -10 -3 -3 2.56 1.64 10 3 3 1.13 1.49 10 3 3 1.86 1.48 10 3 4 264.49 19.61 -10 -3 -4 210.74 20.50 10 3 4 143.70 19.47 10 3 4 300.04 18.85 10 3 4 266.97 16.99 10 3 4 271.22 19.53 -10 -3 -4 258.67 16.58 10 3 4 165.70 16.42 10 3 4 277.25 16.00 10 3 4 265.00 15.97 -10 -3 -5 225.29 19.98 10 3 5 228.72 17.90 10 3 5 241.90 16.67 10 3 5 241.73 15.34 10 3 5 126.22 18.20 10 3 5 157.75 16.01 10 3 5 268.08 15.64 10 3 5 254.82 15.86 10 3 6 2.78 2.21 10 3 6 2.34 3.54 10 3 6 -1.00 4.36 -10 -3 -6 0.75 2.89 10 3 6 4.11 2.19 10 3 6 2.10 1.51 10 3 6 1.36 1.99 10 3 6 3.33 3.46 10 3 6 3.89 2.22 10 3 7 95.59 7.72 10 3 7 79.66 8.44 10 3 7 86.21 12.15 10 3 7 69.15 8.62 10 3 7 48.72 9.25 10 3 7 112.78 9.43 10 3 8 11.00 6.18 10 3 8 56.57 6.45 10 3 8 63.00 5.59 10 3 8 53.70 6.27 10 3 8 31.41 6.00 10 3 8 21.69 6.63 10 3 8 36.54 8.47 10 3 9 28.87 4.76 10 3 9 29.09 3.83 10 3 9 24.82 4.34 10 3 9 20.80 5.16 10 3 9 24.56 7.46 10 3 9 31.19 5.97 10 3 10 8.80 2.44 10 3 10 6.71 3.71 10 3 10 6.09 4.13 10 3 10 11.55 4.15 10 3 10 -1.00 4.36 10 3 10 8.25 2.63 10 3 11 -0.95 2.36 10 3 11 1.63 3.45 10 3 11 -0.30 1.68 10 3 11 1.00 3.94 10 3 11 0.56 2.65 10 3 11 -2.62 2.89 10 3 12 1.98 4.15 10 3 12 18.12 4.64 10 3 12 22.09 5.76 10 3 12 14.31 5.02 10 3 12 19.38 3.68 10 3 12 13.58 4.18 10 3 12 15.55 5.42 10 3 13 3.91 4.74 10 3 13 16.56 4.16 10 3 13 18.89 4.15 10 3 13 12.61 5.51 10 3 13 16.33 5.70 10 3 13 19.47 5.96 10 3 14 70.76 11.27 10 3 14 58.14 6.92 10 3 14 60.18 10.03 10 3 14 73.41 10.80 10 3 15 3.05 1.66 10 3 15 2.76 1.84 10 3 15 5.53 4.34 10 3 15 4.57 4.46 10 3 15 4.41 3.59 10 3 16 29.73 4.64 10 3 16 60.15 11.15 10 3 16 36.54 8.91 10 3 16 51.97 9.66 10 3 17 12.03 6.11 10 3 17 7.36 2.85 -10 -4 13 -1.36 5.47 -10 -4 12 1.34 4.96 -10 -4 11 2.64 5.17 -10 -4 11 0.67 2.49 -10 -4 10 10.47 3.74 -10 -4 10 1.28 4.82 -10 -4 10 12.50 4.45 -10 -4 10 9.81 4.33 -10 -4 9 30.55 5.38 -10 -4 9 24.75 5.96 -10 -4 8 3.97 2.24 -10 -4 8 3.64 5.51 -10 -4 8 1.80 2.29 -10 -4 7 -0.36 1.90 -10 -4 7 1.56 2.19 -10 -4 7 1.11 2.43 -10 -4 6 2.36 1.93 -10 -4 6 9.19 6.01 -10 -4 6 7.87 3.48 -10 -4 6 2.56 2.61 -10 -4 5 50.65 6.86 -10 -4 5 42.07 5.51 -10 -4 5 55.29 7.17 -10 -4 4 189.32 13.41 -10 -4 4 187.83 13.40 -10 -4 4 187.17 11.83 10 4 -4 97.67 8.74 -10 -4 4 99.55 15.34 -10 -4 3 2.11 2.43 -10 -4 3 4.77 2.60 10 4 -3 6.42 2.45 -10 -4 3 7.17 4.04 -10 -4 3 5.69 2.30 -10 -4 3 10.65 5.93 -10 -4 2 22.71 7.45 -10 -4 2 41.53 5.68 10 4 -2 37.60 7.50 -10 -4 2 31.92 4.89 -10 -4 2 19.05 5.47 -10 -4 2 30.82 4.60 10 4 -2 18.99 4.26 10 4 -1 3.05 2.95 -10 -4 1 3.10 1.88 10 4 -1 2.52 2.50 -10 -4 1 4.34 2.32 10 4 -1 2.83 3.20 -10 -4 1 6.17 3.59 -10 -4 1 3.36 2.13 -10 -4 1 8.03 4.98 10 4 0 87.54 10.07 10 4 0 92.10 10.32 -10 -4 0 92.52 8.10 10 4 0 79.42 10.48 -10 -4 0 62.12 8.56 -10 -4 0 89.62 8.26 -10 -4 -1 165.60 18.74 10 4 1 217.86 16.84 -10 -4 -1 224.68 14.25 10 4 1 192.35 16.98 -10 -4 -1 186.15 15.08 10 4 1 179.56 13.17 -10 -4 -1 215.90 14.50 10 4 1 184.48 9.90 -10 -4 -2 54.16 9.69 10 4 2 42.26 6.74 -10 -4 -2 50.52 5.92 -10 -4 -2 39.31 6.03 10 4 2 36.75 5.05 10 4 2 42.10 3.88 -10 -4 -2 44.05 5.94 10 4 2 66.07 8.75 10 4 3 108.41 12.02 10 4 3 148.38 12.66 -10 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190.75 16.16 10 4 10 232.75 14.32 10 4 10 249.88 17.97 10 4 11 50.65 5.68 10 4 11 37.37 6.28 10 4 11 40.87 8.15 10 4 11 36.76 6.55 10 4 11 41.56 7.50 -10 -4 -11 48.10 6.93 10 4 11 40.52 5.48 10 4 12 27.51 4.58 10 4 12 6.92 3.26 10 4 12 23.30 6.11 -10 -4 -12 8.44 3.42 10 4 12 19.98 5.84 10 4 12 23.47 4.98 10 4 13 17.29 5.52 10 4 13 34.31 5.59 10 4 13 31.77 7.75 10 4 13 24.95 6.66 10 4 13 25.61 5.18 10 4 14 23.66 6.57 10 4 14 23.70 4.73 10 4 14 32.30 7.93 10 4 15 19.42 6.42 10 4 15 14.81 5.75 10 4 15 14.83 3.44 10 4 16 7.63 4.94 10 4 16 7.52 4.57 10 4 16 6.54 2.33 10 4 16 9.05 5.36 10 4 17 9.34 4.81 -10 -5 12 2.93 5.68 -10 -5 11 1.42 4.98 -10 -5 11 0.64 2.74 -10 -5 10 1.38 4.87 -10 -5 10 8.38 3.74 -10 -5 9 -0.51 2.29 -10 -5 9 5.37 5.82 -10 -5 9 -0.56 2.46 -10 -5 9 1.28 2.80 -10 -5 8 -0.46 2.43 -10 -5 8 -1.30 4.33 -10 -5 8 -0.59 2.37 -10 -5 7 2.08 2.17 -10 -5 7 1.65 2.20 -10 -5 6 -1.18 2.38 -10 -5 6 -1.23 4.40 -10 -5 6 -1.02 2.51 -10 -5 6 -0.96 2.20 -10 -5 5 0.76 1.70 -10 -5 5 -2.41 4.04 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3 5.21 2.96 -11 -5 3 8.90 3.26 -11 -5 3 7.10 2.91 -11 -5 3 -1.22 3.47 11 5 -3 6.70 2.80 -11 -5 2 33.86 5.63 -11 -5 2 26.15 4.85 -11 -5 2 26.30 4.87 -11 -5 2 9.49 6.30 11 5 -2 16.04 3.92 -11 -5 1 30.69 5.01 -11 -5 1 21.91 7.73 -11 -5 1 25.17 4.70 -11 -5 0 7.08 2.81 -11 -5 0 7.86 5.55 -11 -5 0 5.67 2.69 -11 -5 -1 4.68 2.39 11 5 1 3.48 2.46 -11 -5 -1 -1.09 4.63 -11 -5 -1 5.83 2.93 -11 -5 -2 5.55 2.43 11 5 2 2.19 1.81 -11 -5 -2 2.31 2.53 -11 -5 -2 6.39 4.71 11 5 3 39.13 4.11 11 5 3 38.97 6.63 -11 -5 -3 35.17 5.93 -11 -5 -3 42.21 5.90 11 5 3 41.60 5.59 -11 -5 -3 35.15 5.92 -11 -5 -3 29.04 8.34 11 5 4 33.22 4.20 11 5 4 30.06 5.46 -11 -5 -4 22.69 6.22 11 5 4 31.77 6.64 11 5 4 40.69 5.65 -11 -5 -4 32.35 5.99 -11 -5 -4 14.07 6.17 11 5 5 23.49 4.67 11 5 5 18.42 3.63 -11 -5 -5 18.71 5.45 11 5 5 24.41 4.67 -11 -5 -5 12.64 5.62 11 5 6 14.58 3.71 11 5 6 14.12 3.40 11 5 6 10.54 3.77 -11 -5 -6 6.10 3.70 11 5 6 18.01 4.03 -11 -5 -6 4.68 3.81 11 5 7 17.93 3.88 11 5 7 19.72 4.29 11 5 7 17.59 4.46 11 5 7 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1.57 4.07 15 -2 1 3.39 3.51 15 -2 1 1.46 2.35 -15 2 -1 1.87 2.60 15 -2 1 3.33 4.82 -15 2 -2 0.78 3.65 -15 2 -2 4.76 2.37 15 -2 2 0.89 3.14 15 -2 2 5.96 3.10 15 -2 2 3.26 4.10 -15 2 -3 0.31 1.49 15 -2 3 0.92 3.45 15 -2 3 -0.60 2.79 15 -2 3 -2.13 4.43 15 -2 4 -0.95 3.76 15 -2 4 -0.66 2.84 15 -2 4 1.04 3.46 15 -2 5 13.63 5.61 15 -2 5 6.12 4.98 15 -2 6 58.92 10.82 15 -2 6 40.50 8.67 15 -2 6 40.02 9.37 15 -2 7 -1.97 3.91 15 -2 7 -0.84 1.43 15 -2 7 -0.84 3.33 15 -2 7 1.02 2.55 15 -2 8 10.61 3.15 15 -2 8 12.64 5.60 15 -2 8 12.45 5.38 15 -2 9 -3.93 6.00 15 -2 9 -1.06 2.96 15 -2 10 9.51 5.73 15 -2 10 5.03 2.79 15 -2 11 0.93 3.07 15 -2 11 1.69 2.40 15 -2 11 -2.26 5.25 15 -2 12 -0.63 1.72 15 -2 13 1.39 2.41 15 -2 14 -0.78 3.42 15 -1 -5 18.43 4.83 -15 1 5 15.12 4.80 15 -1 -4 11.82 4.23 -15 1 4 10.66 4.09 15 -1 -3 4.99 3.42 -15 1 3 3.56 2.69 -15 1 2 10.68 5.64 15 -1 -2 19.87 6.07 -15 1 2 23.84 6.11 -15 1 2 25.41 5.06 -15 1 1 4.25 4.27 15 -1 -1 7.30 4.18 -15 1 1 7.24 3.88 -15 1 1 4.80 2.63 -15 1 0 18.75 6.29 15 -1 0 41.92 8.53 15 -1 0 29.59 4.96 -15 1 0 33.12 6.80 -15 1 0 35.22 5.59 -15 1 -1 29.90 7.40 15 -1 1 46.56 8.99 15 -1 1 29.70 5.58 -15 1 -1 50.55 8.12 -15 1 -1 43.37 6.15 15 -1 2 -1.45 3.08 -15 1 -2 -1.55 3.88 -15 1 -2 -1.12 2.38 15 -1 2 1.86 3.87 15 -1 3 2.13 4.02 15 -1 3 0.54 2.35 -15 1 -3 1.76 1.87 15 -1 3 2.88 4.51 15 -1 4 17.73 6.85 15 -1 4 16.35 5.13 15 -1 5 10.20 5.62 15 -1 5 14.71 5.04 15 -1 6 41.96 9.35 15 -1 6 41.86 8.44 15 -1 6 47.12 9.99 15 -1 7 7.86 4.62 15 -1 7 8.51 2.55 15 -1 7 7.23 5.12 15 -1 7 4.16 3.93 15 -1 8 2.90 3.20 15 -1 8 3.03 1.88 15 -1 8 2.63 3.79 15 -1 8 -1.06 4.20 15 -1 9 -1.08 2.70 15 -1 10 0.94 2.86 15 -1 10 2.06 4.25 15 -1 10 1.52 2.42 15 -1 11 -0.92 2.79 15 -1 11 6.67 5.52 15 -1 11 5.59 3.24 15 -1 12 0.89 2.93 15 -1 13 -0.68 2.63 15 -1 14 -0.75 2.89 15 0 -5 1.98 2.56 -15 0 5 7.92 3.70 15 0 -4 7.80 3.50 -15 0 4 3.97 2.92 15 0 -3 55.26 9.50 -15 0 3 72.15 8.86 -15 0 2 62.60 9.27 -15 0 2 42.11 9.24 15 0 -2 54.50 9.56 -15 0 2 44.58 6.90 -15 0 1 4.28 4.42 15 0 -1 2.53 3.65 -15 0 1 7.89 3.88 -15 0 1 3.64 2.61 -15 0 0 -0.86 2.09 -15 0 0 -1.64 3.71 15 0 0 -0.88 3.32 -15 0 0 1.92 2.90 -15 0 -1 3.33 2.55 -15 0 -1 -3.15 4.94 15 0 1 1.84 3.46 15 0 1 1.35 2.10 15 0 2 106.80 14.05 15 0 2 106.11 9.69 -15 0 -2 92.37 9.13 -15 0 -3 85.46 8.82 15 0 3 100.23 14.09 15 0 3 101.19 10.37 15 0 3 88.07 10.32 15 0 4 -0.55 2.83 15 0 4 -0.53 2.05 15 0 5 31.87 8.15 15 0 5 22.86 3.33 15 0 5 38.93 7.21 15 0 6 15.32 3.96 15 0 6 15.77 5.10 15 0 6 10.47 2.83 15 0 6 18.84 6.38 15 0 6 7.32 5.45 15 0 7 47.69 8.64 15 0 7 43.88 5.71 15 0 7 41.78 9.19 15 0 7 45.64 9.82 15 0 8 57.31 9.83 15 0 8 54.84 6.93 15 0 8 52.57 10.12 15 0 8 58.09 11.16 15 0 9 0.46 1.88 15 0 9 1.81 3.38 15 0 9 -1.09 4.09 15 0 10 18.72 6.86 15 0 10 11.87 3.79 15 0 10 17.54 6.24 15 0 10 24.38 7.49 15 0 11 82.11 13.49 15 0 11 74.86 11.68 15 0 11 73.20 9.42 15 0 12 40.24 9.79 15 0 12 39.35 8.41 15 0 12 31.98 6.46 15 0 13 4.24 3.62 15 0 13 2.01 2.73 15 0 14 -2.20 3.10 15 1 -5 11.14 4.29 -15 -1 4 0.57 2.35 15 1 -4 -0.74 2.40 -15 -1 3 3.20 2.58 -15 -1 3 0.94 4.05 15 1 -3 2.33 3.34 -15 -1 2 2.01 2.51 -15 -1 2 0.68 2.83 -15 -1 2 -0.90 4.34 15 1 -2 0.82 2.88 -15 -1 1 27.09 5.42 -15 -1 1 28.36 6.27 -15 -1 1 23.10 6.96 15 1 -1 29.22 7.29 -15 -1 0 40.64 7.23 -15 -1 0 29.24 5.53 -15 -1 0 30.27 7.47 15 1 0 31.43 7.67 -15 -1 -1 11.10 3.76 -15 -1 -1 7.05 4.20 15 1 1 10.59 2.35 -15 -1 -2 9.16 4.81 -15 -1 -2 10.89 3.57 15 1 2 15.44 6.07 15 1 2 2.83 4.32 15 1 2 12.29 3.27 -15 -1 -3 3.87 2.80 15 1 3 3.19 2.63 15 1 4 6.22 3.29 15 1 4 15.05 4.30 15 1 5 28.01 8.01 15 1 5 35.98 6.32 15 1 5 19.63 3.47 15 1 5 30.03 5.83 15 1 6 13.67 6.20 15 1 6 7.50 3.59 15 1 6 8.12 2.87 15 1 6 5.45 2.78 15 1 7 76.00 10.69 15 1 7 84.05 8.44 15 1 7 82.31 12.56 15 1 7 76.84 12.82 15 1 8 3.84 3.59 15 1 8 2.92 2.60 15 1 8 1.87 3.32 15 1 8 2.17 3.33 15 1 9 -1.43 2.21 15 1 9 0.85 2.58 15 1 9 1.10 3.08 15 1 10 -0.52 2.43 15 1 10 -0.90 3.18 15 1 10 -0.92 2.81 15 1 11 12.68 4.28 15 1 11 15.88 5.85 15 1 11 25.09 7.40 15 1 12 32.56 6.51 15 1 12 30.92 7.68 15 1 12 43.51 9.92 15 1 13 18.15 5.70 15 1 13 13.39 4.56 15 1 14 -0.79 2.57 15 1 14 -1.45 2.81 -15 -2 4 -0.59 2.30 -15 -2 3 -0.55 2.48 -15 -2 2 -0.52 2.53 -15 -2 1 9.34 4.02 -15 -2 1 4.50 2.74 -15 -2 0 32.85 5.96 15 2 1 4.28 4.41 -15 -2 -1 1.41 2.64 15 2 2 13.77 2.47 -15 -2 -2 18.17 4.33 15 2 3 -1.47 2.23 -15 -2 -3 0.92 2.09 15 2 4 -1.56 2.87 15 2 4 -1.82 2.04 15 2 5 21.83 7.42 15 2 5 11.82 3.21 15 2 5 26.57 5.24 15 2 6 1.05 4.39 15 2 6 2.21 2.67 15 2 6 -1.87 3.05 15 2 6 -0.53 1.94 15 2 7 18.16 6.90 15 2 7 20.69 5.33 15 2 7 26.75 5.00 15 2 7 18.38 4.40 15 2 8 0.45 3.48 15 2 8 1.41 2.91 15 2 8 1.08 2.71 15 2 9 2.98 2.47 15 2 9 1.56 2.74 15 2 9 4.38 4.11 15 2 10 1.71 3.01 15 2 10 -3.50 3.62 15 2 10 1.09 2.24 15 2 11 4.69 4.03 15 2 11 3.43 3.99 15 2 11 2.96 2.64 15 2 12 16.38 6.49 15 2 12 11.68 4.88 15 2 12 14.01 4.88 15 2 13 4.45 4.12 15 2 13 4.11 3.37 15 2 13 0.81 2.43 15 2 14 1.46 2.54 15 2 14 3.85 3.13 -15 -3 3 7.46 3.51 -15 -3 3 2.79 4.01 -15 -3 2 1.09 2.36 -15 -3 2 -0.89 3.32 -15 -3 1 31.58 5.97 -15 -3 1 13.51 5.86 -15 -3 0 17.34 4.65 -15 -3 0 12.05 5.44 -15 -3 0 11.94 6.50 -15 -3 -1 11.03 3.77 -15 -3 -1 4.58 4.06 -15 -3 -1 1.47 5.20 -15 -3 -2 14.77 5.75 -15 -3 -2 22.29 5.02 15 3 2 10.78 5.72 -15 -3 -3 8.90 3.47 15 3 3 9.20 2.21 15 3 4 35.25 5.25 15 3 4 49.31 5.74 15 3 5 11.65 3.31 15 3 5 12.31 3.70 15 3 6 -1.65 2.56 15 3 6 -1.06 4.42 15 3 6 0.48 1.90 15 3 7 -1.43 3.80 15 3 7 2.14 3.54 15 3 7 0.57 2.34 15 3 8 0.49 2.71 15 3 8 4.31 3.82 15 3 8 8.39 3.76 15 3 9 50.78 7.42 15 3 9 33.73 8.40 15 3 10 67.47 10.37 15 3 10 45.06 9.26 15 3 10 54.33 8.08 15 3 11 6.19 4.11 15 3 11 4.14 3.26 15 3 11 9.76 3.86 15 3 12 -0.97 3.58 15 3 12 0.81 2.82 15 3 12 1.30 3.00 15 3 13 -1.06 3.44 15 3 13 4.87 3.52 15 3 13 1.56 2.89 15 3 14 14.13 5.11 15 3 14 15.02 5.07 15 3 15 2.14 3.13 -15 -4 3 13.93 6.00 -15 -4 2 10.96 3.89 -15 -4 2 4.38 4.50 -15 -4 1 -0.56 2.30 -15 -4 1 3.31 4.25 -15 -4 0 -0.54 2.94 -15 -4 0 1.57 3.92 -15 -4 -1 19.41 9.00 -15 -4 -1 26.53 5.59 -15 -4 -1 14.14 5.33 -15 -4 -2 11.73 7.59 -15 -4 -2 7.89 4.33 -15 -4 -2 13.25 4.18 15 4 2 14.74 5.58 -15 -4 -3 0.52 3.08 -15 -4 -3 4.31 6.49 15 4 4 9.34 3.05 15 4 4 10.26 2.47 15 4 5 14.54 4.18 15 4 5 22.72 4.09 15 4 6 107.69 10.80 15 4 6 116.32 10.82 15 4 7 21.48 4.97 15 4 7 21.13 5.01 15 4 8 26.13 5.59 15 4 8 25.94 7.50 15 4 8 26.38 5.85 15 4 9 29.40 6.54 15 4 9 16.18 4.74 15 4 10 7.49 3.94 15 4 10 5.95 3.47 15 4 11 28.22 7.26 15 4 11 19.25 5.90 15 4 11 24.73 6.06 15 4 12 17.35 6.71 15 4 12 13.22 5.06 15 4 12 24.90 5.98 15 4 13 6.00 4.26 15 4 13 5.72 3.52 15 4 13 6.04 3.94 15 4 14 41.56 7.99 15 4 15 45.22 8.04 -15 -5 2 5.15 4.63 -15 -5 1 0.59 2.53 -15 -5 1 -0.81 3.47 -15 -5 0 -0.57 2.37 -15 -5 0 -0.76 3.41 -15 -5 -1 1.44 3.46 -15 -5 -1 0.57 2.64 -15 -5 -2 -1.51 4.98 -15 -5 -2 1.38 3.22 -15 -5 -2 2.81 2.89 -15 -5 -3 4.43 4.89 -15 -5 -3 5.56 3.34 -15 -5 -4 2.90 5.13 15 5 5 -1.40 2.77 -15 -5 -5 1.42 4.71 15 5 5 0.53 1.54 15 5 6 2.18 1.90 15 5 6 1.00 2.06 15 5 7 0.55 2.80 15 5 8 23.96 5.31 15 5 8 26.74 6.04 15 5 9 5.55 3.58 15 5 9 2.43 2.92 15 5 10 27.95 6.53 15 5 10 17.03 5.26 15 5 11 9.39 4.65 15 5 11 12.66 4.82 15 5 12 -0.87 3.69 15 5 12 3.77 3.35 15 5 12 0.71 2.74 15 5 13 0.95 3.30 15 5 13 -0.74 2.87 15 5 13 1.46 2.53 15 5 14 2.12 3.33 -15 -6 2 15.06 5.86 -15 -6 1 12.52 5.66 -15 -6 0 1.83 3.05 -15 -6 0 2.92 3.62 -15 -6 -1 -1.37 3.50 -15 -6 -1 0.60 2.71 -15 -6 -2 -0.66 3.06 -15 -6 -2 6.54 3.40 15 6 4 1.02 2.44 -15 -6 -5 10.33 6.90 15 6 5 10.41 3.89 -15 -6 -6 1.45 4.42 15 6 6 0.55 2.54 15 6 7 2.93 3.00 15 6 8 9.35 3.51 15 6 8 6.48 4.18 15 6 9 14.91 4.45 15 6 9 11.53 5.00 15 6 10 8.57 3.91 15 6 10 10.85 4.52 15 6 11 45.02 8.23 15 6 11 38.76 7.70 15 6 12 -0.83 3.51 15 6 12 0.74 2.87 15 6 13 2.73 4.30 15 6 13 1.42 2.87 15 6 14 -0.69 2.49 -15 -7 2 5.60 4.16 -15 -7 1 5.23 4.40 -15 -7 -1 3.26 3.52 -15 -7 -1 8.98 4.07 -15 -7 -2 2.50 3.28 -15 -7 -2 1.25 2.59 15 7 4 8.02 3.69 15 7 5 12.65 4.35 15 7 6 1.79 2.66 15 7 7 36.66 7.05 15 7 8 48.38 8.36 15 7 9 2.25 3.46 15 7 9 3.24 2.82 15 7 10 -3.00 3.80 15 7 10 -1.25 2.54 15 7 11 -2.27 3.47 15 7 12 10.31 4.66 15 7 13 56.20 9.99 -15 -8 2 -0.77 3.49 -15 -8 1 0.71 3.24 -15 -8 0 0.65 2.77 -15 -8 -1 4.91 3.45 15 8 4 12.77 4.87 15 8 5 10.79 4.44 15 8 6 1.30 2.77 15 8 7 0.68 3.13 15 8 8 1.44 3.53 15 8 9 24.09 6.49 15 8 10 14.62 5.81 15 8 12 19.05 5.53 -15 -9 0 9.16 4.08 -15 -9 -1 1.72 2.70 15 9 5 1.40 2.84 15 9 6 1.42 2.88 15 9 7 0.74 2.99 15 9 8 -0.77 3.40 15 10 5 24.65 6.39 15 10 6 13.90 5.19 -16 8 -2 4.06 3.60 -16 7 -2 -2.06 3.04 -16 6 -2 0.69 2.95 16 -6 5 20.36 6.69 16 -6 6 1.99 2.99 -16 5 4 11.26 3.94 -16 5 3 10.48 3.56 -16 5 2 9.79 3.35 -16 5 -1 6.31 3.80 -16 5 -2 4.14 3.21 16 -5 4 0.86 3.17 16 -5 5 54.68 9.88 16 -5 6 37.63 9.06 16 -5 7 -1.97 3.64 -16 4 4 0.55 2.21 -16 4 3 16.70 4.40 -16 4 2 11.55 3.69 -16 4 1 8.47 3.11 -16 4 0 1.47 1.69 -16 4 -1 25.09 6.15 -16 4 -1 22.20 4.19 16 -4 1 21.52 5.48 16 -4 2 67.43 9.72 16 -4 3 17.53 5.46 16 -4 4 10.18 4.24 16 -4 5 12.54 5.39 16 -4 6 -2.68 5.05 16 -4 7 47.44 9.89 16 -4 8 50.28 9.94 -16 3 4 1.66 2.53 -16 3 3 3.04 2.33 -16 3 2 4.16 2.55 -16 3 1 13.69 3.81 -16 3 0 -0.40 1.76 -16 3 -1 0.73 1.75 16 -3 1 5.50 3.10 -16 3 -2 0.33 1.84 16 -3 2 6.28 4.31 16 -3 2 0.61 2.79 16 -3 3 4.71 4.22 16 -3 3 7.95 4.18 16 -3 4 10.10 4.21 16 -3 5 1.56 2.73 16 -3 6 23.62 7.08 16 -3 7 21.73 7.32 16 -3 8 1.94 4.32 16 -3 9 -3.11 4.95 -16 2 4 1.13 2.60 -16 2 3 8.87 3.53 16 -2 -3 7.47 3.53 -16 2 2 1.93 2.22 16 -2 -2 0.74 2.23 -16 2 1 12.14 3.55 16 -2 -1 11.95 4.74 -16 2 0 -0.42 1.74 16 -2 0 0.85 2.78 -16 2 -1 0.40 1.71 16 -2 1 2.70 3.70 16 -2 1 0.96 2.21 -16 2 -2 0.74 1.71 16 -2 2 -0.95 4.06 16 -2 2 0.54 2.40 16 -2 3 1.80 2.77 -16 2 -3 3.25 2.13 16 -2 3 0.99 3.46 16 -2 4 4.63 3.66 16 -2 4 4.08 4.21 16 -2 5 -0.73 2.98 16 -2 5 4.20 4.13 16 -2 6 0.79 3.09 16 -2 7 5.16 4.26 16 -2 8 2.80 4.31 16 -2 9 -4.02 5.82 16 -2 10 1.08 4.42 -16 1 4 12.66 4.22 -16 1 3 12.83 4.14 16 -1 -3 8.88 4.07 -16 1 2 -1.00 2.39 16 -1 -2 0.80 2.94 -16 1 1 22.15 4.90 16 -1 -1 29.80 7.21 -16 1 0 45.47 6.66 16 -1 0 51.39 9.64 -16 1 -1 11.18 3.54 16 -1 1 17.06 6.14 -16 1 -2 0.41 1.76 16 -1 2 0.99 3.25 16 -1 3 28.57 5.85 -16 1 -3 23.83 4.46 16 -1 3 31.78 8.26 16 -1 4 38.12 7.18 16 -1 4 58.09 10.95 16 -1 5 10.08 4.26 16 -1 5 7.57 5.23 16 -1 6 2.97 3.31 16 -1 7 1.63 3.18 16 -1 7 -2.24 3.95 16 -1 8 42.70 9.21 16 -1 9 73.56 12.12 16 -1 10 15.70 6.09 16 -1 11 2.26 3.93 16 0 -4 40.85 7.88 -16 0 3 11.03 3.87 16 0 -3 7.96 4.37 -16 0 2 11.45 3.83 16 0 -2 8.47 4.44 -16 0 1 5.44 3.07 16 0 -1 4.48 3.68 -16 0 0 4.76 2.83 16 0 0 3.77 3.88 -16 0 -1 48.27 6.90 -16 0 -1 38.26 8.37 16 0 1 53.37 10.18 -16 0 -2 16.29 5.98 -16 0 -2 10.73 3.77 16 0 2 14.39 5.89 -16 0 -3 0.85 2.04 16 0 3 3.19 4.39 16 0 4 7.08 3.38 16 0 4 10.91 5.78 16 0 5 22.19 5.43 16 0 6 39.24 7.49 16 0 7 -2.29 4.28 16 0 8 20.11 6.11 16 0 9 3.42 2.23 16 0 9 2.74 3.75 16 0 10 37.79 8.92 16 0 11 29.98 5.85 16 0 11 20.46 7.35 16 0 12 -0.60 2.43 16 0 13 42.55 7.61 16 1 -4 13.36 5.18 -16 -1 3 5.16 3.09 -16 -1 2 9.77 3.87 16 1 -2 4.41 3.61 -16 -1 1 0.52 2.33 16 1 -1 4.65 3.98 -16 -1 0 2.02 3.31 16 1 0 0.98 3.63 -16 -1 -1 1.47 2.71 16 1 1 -2.04 3.58 -16 -1 -2 -0.96 2.59 16 1 2 1.06 4.16 -16 -1 -3 0.46 2.16 16 1 3 1.09 4.51 16 1 4 0.92 2.40 16 1 4 3.36 4.18 16 1 5 -2.17 3.28 16 1 6 -0.62 3.17 16 1 6 -1.15 3.52 16 1 7 2.09 2.86 16 1 8 6.13 2.72 16 1 8 8.52 4.39 16 1 9 8.65 3.14 16 1 9 6.80 3.94 16 1 10 1.53 2.34 16 1 10 1.87 3.25 16 1 11 2.24 2.65 16 1 11 -1.01 3.74 16 1 12 -1.10 3.81 16 1 13 1.98 2.53 16 2 -4 0.82 2.63 16 2 -3 0.87 2.99 -16 -2 2 32.45 6.31 -16 -2 1 4.93 3.12 16 2 -1 4.83 4.30 -16 -2 0 0.53 2.46 -16 -2 0 -0.88 3.78 16 2 0 -1.01 3.32 -16 -2 -1 26.38 7.19 -16 -2 -1 35.75 6.43 16 2 1 48.62 10.27 -16 -2 -2 7.51 4.56 -16 -2 -2 15.85 4.44 16 2 2 14.22 6.25 -16 -2 -3 7.00 3.36 16 2 3 8.99 5.24 16 2 6 21.88 5.02 16 2 6 25.89 8.10 16 2 7 23.28 5.80 16 2 8 16.98 4.29 16 2 8 15.62 5.45 16 2 9 0.79 2.75 16 2 10 6.93 3.22 16 2 10 5.23 4.02 16 2 11 6.95 3.56 16 2 11 6.68 4.40 16 2 12 1.25 2.41 16 2 12 8.35 5.11 16 2 13 1.33 2.92 -16 -3 1 4.63 3.51 -16 -3 0 12.37 4.27 -16 -3 0 8.64 5.04 -16 -3 -1 5.00 4.38 -16 -3 -1 -0.55 2.37 -16 -3 -2 17.93 6.16 -16 -3 -2 28.84 5.91 -16 -3 -3 70.52 9.01 16 3 6 -2.35 2.81 16 3 6 -0.47 2.45 16 3 7 27.45 5.23 16 3 7 21.91 5.61 16 3 8 42.12 7.68 16 3 9 1.07 2.46 16 3 9 -0.73 2.55 16 3 10 -1.13 2.78 16 3 10 -0.82 3.01 16 3 11 18.22 4.86 16 3 11 9.93 4.99 16 3 12 51.67 8.25 16 3 12 76.22 11.97 16 3 13 10.28 4.51 -16 -4 0 11.86 4.25 -16 -4 -1 14.59 5.62 -16 -4 -1 16.33 4.74 -16 -4 -2 -0.79 3.25 -16 -4 -2 4.61 2.95 -16 -4 -3 1.70 2.72 16 4 6 -0.89 2.75 16 4 8 3.38 3.25 16 4 9 10.03 3.93 16 4 9 11.43 4.39 16 4 10 3.63 2.77 16 4 10 0.76 2.63 16 4 11 0.64 2.93 16 4 12 5.41 3.40 16 4 12 3.73 3.60 -16 -5 0 27.74 7.27 -16 -5 -1 1.56 3.47 -16 -5 -1 -0.62 2.77 -16 -5 -2 14.45 5.44 -16 -5 -2 17.67 4.95 16 5 7 7.05 3.41 16 5 8 2.39 2.93 16 5 9 -1.37 3.45 16 5 10 3.32 3.63 16 5 10 0.71 2.58 16 5 11 0.68 3.22 16 5 11 0.80 2.74 16 5 12 4.99 3.47 16 5 12 6.18 4.42 -16 -6 0 2.35 4.06 -16 -6 -1 14.23 5.39 16 6 6 11.70 4.24 16 6 7 5.93 3.57 16 6 8 -0.64 2.92 16 6 9 33.75 7.15 16 6 10 23.30 6.57 16 6 11 4.40 3.68 -16 -7 0 8.18 4.54 -16 -7 -1 2.14 3.47 16 7 6 25.30 5.94 16 7 8 -0.68 3.22 16 7 9 -1.46 3.67 16 7 10 7.25 4.39 -16 -8 0 3.53 3.61 -16 -8 -1 5.39 3.91 16 8 6 0.68 2.97 16 8 7 0.70 3.06 16 8 8 0.74 2.82 16 8 9 1.55 3.11 17 -6 3 5.90 4.29 17 -5 3 8.46 5.04 17 -5 4 46.74 9.06 17 -5 5 9.50 4.92 17 -4 4 19.30 5.94 17 -4 5 37.18 8.13 17 -4 6 7.40 4.66 -17 3 3 0.52 2.44 17 -3 4 1.44 3.29 17 -3 6 -1.71 3.46 17 -3 7 0.92 3.38 17 -3 8 0.99 2.71 -17 2 2 44.86 7.01 -17 2 1 3.87 2.76 17 -2 -1 1.66 2.85 -17 2 0 24.87 5.04 17 -2 0 14.19 5.59 -17 2 -1 13.82 3.87 17 -2 1 8.48 5.06 17 -2 2 0.99 3.45 17 -2 3 9.37 5.14 17 -2 5 45.45 8.20 17 -2 7 2.59 3.51 17 -2 8 6.59 4.15 17 -2 9 8.16 4.49 -17 1 2 16.56 4.46 17 -1 -2 13.17 4.83 -17 1 1 3.58 2.65 17 -1 -1 1.76 2.63 -17 1 0 9.34 3.53 17 -1 0 9.37 4.74 -17 1 -1 -0.94 2.38 17 -1 1 0.99 2.97 -17 1 -2 38.55 6.21 17 -1 2 57.20 10.94 17 -1 6 2.94 3.37 17 -1 8 40.82 8.60 17 -1 9 2.90 3.73 17 -1 10 1.05 3.13 -17 0 2 -0.56 2.46 17 0 -2 0.88 2.61 -17 0 1 10.78 4.15 17 0 -1 13.12 5.50 -17 0 0 -1.04 2.38 17 0 0 -0.99 3.43 -17 0 -1 3.53 2.84 17 0 1 6.27 4.80 -17 0 -2 -0.97 2.14 17 0 2 -1.09 3.55 17 0 7 11.22 4.50 17 0 9 3.61 3.82 17 0 10 0.99 3.18 17 1 -2 -0.93 2.75 -17 -1 1 25.51 5.75 17 1 -1 39.38 8.75 -17 -1 0 8.24 3.94 17 1 0 8.32 4.94 -17 -1 -1 1.08 2.29 17 1 1 1.09 3.79 -17 -1 -2 -1.05 2.73 17 1 8 0.76 2.45 17 1 9 0.84 2.71 17 1 10 -0.92 3.72 17 1 11 1.01 3.24 -17 -2 0 17.49 4.80 -17 -2 -1 43.35 7.31 -17 -2 -2 9.51 3.79 17 2 10 39.92 8.36 17 2 11 8.59 4.64 -17 -3 -1 14.48 4.55 -17 -3 -2 0.59 2.81 -17 -4 -2 -1.25 2.54 -18 -1 -1 -0.58 2.64 -18 -2 -2 0.60 2.40 0 0 0 0.00 0.00 TITL Sjcm19ar19a_16_150_00 in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 11.831995 12.330566 13.976333 82.6541 77.1225 89.2315 ZERR 2.00 0.000240 0.000358 0.000384 0.0023 0.0021 0.0021 LATT 1 SFAC C H N O F S Fe I UNIT 80.00 80.00 10.00 4.00 6.00 2.00 2.00 6.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 42858 _olex2_exptl_crystal_mounting_method 'Paratone oil' _olex2_submission_original_sample_id Sjcm19ar19a_16_150_00 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 4.514 _oxdiff_exptl_absorpt_empirical_full_min 0.519 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I3 I -0.08317(2) 0.23604(2) 0.38622(2) 0.02967(9) Uani 1 1 d . . . . . I1 I 0.28421(3) 0.05504(2) 0.60606(2) 0.03582(10) Uani 1 1 d . . . . . I2 I -0.00883(3) 0.42932(3) 0.74394(3) 0.04195(10) Uani 1 1 d . . . . . Fe1 Fe 0.51473(4) 0.36452(4) 0.78954(4) 0.01771(12) Uani 1 1 d . . . . . S1 S -0.20225(11) 0.28957(11) 0.19708(9) 0.0409(3) Uani 1 1 d . . . . . F3 F 0.1188(2) 0.0872(2) 0.45135(19) 0.0345(6) Uani 1 1 d . . . . . F2 F -0.1057(2) 0.3842(2) 0.5584(2) 0.0382(6) Uani 1 1 d . . . . . O1 O 0.6294(2) 0.4725(2) 0.73490(19) 0.0217(6) Uani 1 1 d . . . . . O3 O 0.5920(2) 0.3105(2) 0.88892(19) 0.0216(6) Uani 1 1 d . . . . . F1 F 0.1875(2) 0.2531(2) 0.7176(2) 0.0394(6) Uani 1 1 d . . . . . O4 O 0.9696(2) 0.0396(3) 0.8754(2) 0.0309(7) Uani 1 1 d . . . . . O2 O 0.6942(3) 0.8759(2) 0.8465(2) 0.0325(7) Uani 1 1 d . . . . . N3 N 0.5965(3) 0.2721(3) 0.6951(2) 0.0179(6) Uani 1 1 d . . . . . N4 N 0.4323(3) 0.4107(3) 0.6822(2) 0.0210(7) Uani 1 1 d . . . . . N1 N 0.4229(3) 0.4544(3) 0.8806(2) 0.0190(6) Uani 1 1 d . . . . . N2 N 0.3857(3) 0.2577(3) 0.8478(2) 0.0187(6) Uani 1 1 d . . . . . C25 C 0.6871(3) 0.2150(3) 0.7048(3) 0.0208(8) Uani 1 1 d . . . . . H25 H 0.725085 0.179735 0.650055 0.025 Uiso 1 1 calc R U . . . C34 C 0.4652(3) 0.3536(3) 0.6029(3) 0.0190(7) Uani 1 1 d . . . . . C19 C 0.7378(3) 0.2243(3) 0.9588(3) 0.0221(8) Uani 1 1 d . . . . . H19 H 0.707425 0.255109 1.018034 0.027 Uiso 1 1 calc R U . . . C23 C 0.8304(3) 0.1308(3) 0.7885(3) 0.0224(8) Uani 1 1 d . . . . . H23 H 0.862186 0.098870 0.730139 0.027 Uiso 1 1 calc R U . . . C26 C 0.5537(3) 0.2763(3) 0.6079(3) 0.0207(8) Uani 1 1 d . . . . . C8 C 0.4569(3) 0.5479(3) 0.9003(3) 0.0203(8) Uani 1 1 d . . . . . H8 H 0.408254 0.580536 0.952211 0.024 Uiso 1 1 calc R U . . . C17 C 0.2973(3) 0.3006(3) 0.9123(3) 0.0202(7) Uani 1 1 d . . . . . C18 C 0.6847(3) 0.2488(3) 0.8776(3) 0.0195(7) Uani 1 1 d . . . . . C24 C 0.7343(3) 0.2008(3) 0.7908(3) 0.0204(8) Uani 1 1 d . . . . . C7 C 0.5616(3) 0.6044(3) 0.8494(3) 0.0213(8) Uani 1 1 d . . . . . C9 C 0.3124(3) 0.4091(3) 0.9300(3) 0.0196(7) Uani 1 1 d . . . . . C6 C 0.5788(3) 0.7076(3) 0.8775(3) 0.0227(8) Uani 1 1 d . . . . . H6 H 0.524908 0.732836 0.930902 0.027 Uiso 1 1 calc R U . . . C13 C 0.1943(3) 0.2405(3) 0.9591(3) 0.0229(8) Uani 1 1 d . . . . . C21 C 0.8782(3) 0.1084(3) 0.8696(3) 0.0232(8) Uani 1 1 d . . . . . C4 C 0.6733(3) 0.7721(3) 0.8282(3) 0.0238(8) Uani 1 1 d . . . . . C38 C 0.0394(4) 0.3200(4) 0.6412(3) 0.0292(9) Uani 1 1 d . . . . . C27 C 0.5882(4) 0.2133(3) 0.5318(3) 0.0254(8) Uani 1 1 d . . . . . H27 H 0.645345 0.158979 0.535488 0.031 Uiso 1 1 calc R U . . . C20 C 0.8313(3) 0.1577(4) 0.9546(3) 0.0249(8) Uani 1 1 d . . . . . H20 H 0.865350 0.144378 1.010374 0.030 Uiso 1 1 calc R U . . . C2 C 0.7416(3) 0.6301(4) 0.7264(3) 0.0246(8) Uani 1 1 d . . . . . H2 H 0.799312 0.604151 0.675948 0.029 Uiso 1 1 calc R U . . . C1 C 0.6421(3) 0.5635(3) 0.7717(3) 0.0205(8) Uani 1 1 d . . . . . C28 C 0.5385(4) 0.2299(4) 0.4493(3) 0.0286(9) Uani 1 1 d . . . . . H28 H 0.562875 0.186556 0.397086 0.034 Uiso 1 1 calc R U . . . N5 N -0.3767(4) 0.1267(4) 0.2299(3) 0.0484(11) Uani 1 1 d . . . . . C12 C 0.1048(3) 0.2935(4) 1.0204(3) 0.0274(9) Uani 1 1 d . . . . . H12 H 0.034304 0.255546 1.051878 0.033 Uiso 1 1 calc R U . . . C33 C 0.3531(3) 0.4869(3) 0.6789(3) 0.0238(8) Uani 1 1 d . . . . . H33 H 0.330186 0.527048 0.733583 0.029 Uiso 1 1 calc R U . . . C36 C 0.1573(4) 0.1688(4) 0.5844(3) 0.0274(9) Uani 1 1 d . . . . . C41 C 0.0932(4) 0.1642(3) 0.5124(3) 0.0267(9) Uani 1 1 d . . . . . C16 C 0.3758(3) 0.1552(3) 0.8323(3) 0.0241(8) Uani 1 1 d . . . . . H16 H 0.437183 0.125062 0.787827 0.029 Uiso 1 1 calc R U . . . C32 C 0.3012(4) 0.5107(4) 0.5969(3) 0.0278(9) Uani 1 1 d . . . . . H32 H 0.244583 0.566072 0.597150 0.033 Uiso 1 1 calc R U . . . C30 C 0.4165(3) 0.3712(4) 0.5185(3) 0.0242(8) Uani 1 1 d . . . . . C10 C 0.2234(3) 0.4592(3) 0.9896(3) 0.0256(8) Uani 1 1 d . . . . . H10 H 0.231727 0.532813 1.000557 0.031 Uiso 1 1 calc R U . . . C3 C 0.7558(3) 0.7303(4) 0.7538(3) 0.0264(9) Uani 1 1 d . . . . . H3 H 0.823095 0.772900 0.721795 0.032 Uiso 1 1 calc R U . . . C39 C -0.0200(4) 0.3129(4) 0.5674(3) 0.0305(9) Uani 1 1 d . . . . . C15 C 0.2792(4) 0.0893(3) 0.8782(3) 0.0270(9) Uani 1 1 d . . . . . H15 H 0.276599 0.015471 0.865721 0.032 Uiso 1 1 calc R U . . . C11 C 0.1204(4) 0.3997(4) 1.0339(3) 0.0306(9) Uani 1 1 d . . . . . H11 H 0.059393 0.434587 1.074686 0.037 Uiso 1 1 calc R U . . . C29 C 0.4557(4) 0.3071(4) 0.4418(3) 0.0284(9) Uani 1 1 d . . . . . H29 H 0.424470 0.317406 0.384383 0.034 Uiso 1 1 calc R U . . . C37 C 0.1277(4) 0.2471(4) 0.6472(3) 0.0283(9) Uani 1 1 d . . . . . C35 C -0.3045(5) 0.1940(4) 0.2165(3) 0.0380(12) Uani 1 1 d . . . . . C40 C 0.0051(4) 0.2361(4) 0.5010(3) 0.0292(9) Uani 1 1 d . . . . . C14 C 0.1888(4) 0.1303(4) 0.9406(3) 0.0282(9) Uani 1 1 d . . . . . H14 H 0.122585 0.085749 0.971682 0.034 Uiso 1 1 calc R U . . . C31 C 0.3320(4) 0.4544(4) 0.5175(3) 0.0284(9) Uani 1 1 d . . . . . H31 H 0.297587 0.470518 0.462193 0.034 Uiso 1 1 calc R U . . . C5 C 0.6002(4) 0.9278(3) 0.9051(3) 0.0310(9) Uani 1 1 d . . . . . H5A H 0.532817 0.928283 0.875144 0.047 Uiso 1 1 calc R U . . . H5B H 0.622713 1.003143 0.908626 0.047 Uiso 1 1 calc R U . . . H5C H 0.580464 0.887678 0.972020 0.047 Uiso 1 1 calc R U . . . C22 C 0.9976(4) -0.0313(4) 0.8014(3) 0.0325(10) Uani 1 1 d . . . . . H22A H 1.025212 0.012051 0.736686 0.049 Uiso 1 1 calc R U . . . H22B H 0.928487 -0.073707 0.800594 0.049 Uiso 1 1 calc R U . . . H22C H 1.058552 -0.081175 0.815942 0.049 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I3 0.02345(14) 0.03474(17) 0.03197(16) -0.00742(12) -0.00701(11) 0.00417(11) I1 0.03059(16) 0.02950(17) 0.0494(2) -0.00247(14) -0.01488(13) 0.00504(12) I2 0.0474(2) 0.03731(19) 0.0425(2) -0.01649(15) -0.00669(15) 0.00257(15) Fe1 0.0176(3) 0.0190(3) 0.0168(3) -0.0041(2) -0.00360(19) 0.0024(2) S1 0.0473(7) 0.0474(8) 0.0309(6) -0.0112(5) -0.0122(5) 0.0185(6) F3 0.0382(14) 0.0323(14) 0.0349(14) -0.0099(11) -0.0100(11) 0.0107(11) F2 0.0353(14) 0.0404(16) 0.0434(16) -0.0122(13) -0.0151(12) 0.0157(12) O1 0.0225(13) 0.0244(15) 0.0185(13) -0.0053(11) -0.0039(10) 0.0015(11) O3 0.0214(13) 0.0261(15) 0.0185(13) -0.0062(11) -0.0052(10) 0.0043(11) F1 0.0493(16) 0.0358(15) 0.0405(15) -0.0058(12) -0.0254(13) 0.0021(13) O4 0.0259(15) 0.0351(18) 0.0369(17) -0.0093(14) -0.0160(13) 0.0107(13) O2 0.0308(16) 0.0262(16) 0.0381(17) -0.0091(13) 0.0010(13) -0.0084(13) N3 0.0173(14) 0.0176(16) 0.0178(15) -0.0016(12) -0.0023(12) 0.0023(12) N4 0.0195(15) 0.0247(18) 0.0189(15) -0.0017(13) -0.0055(12) 0.0000(13) N1 0.0180(15) 0.0190(16) 0.0178(15) 0.0010(12) -0.0009(12) 0.0026(12) N2 0.0212(15) 0.0199(16) 0.0173(15) -0.0047(12) -0.0078(12) 0.0014(12) C25 0.0189(17) 0.026(2) 0.0183(17) -0.0075(15) -0.0024(14) 0.0044(15) C34 0.0208(18) 0.0188(19) 0.0163(17) -0.0025(14) -0.0014(14) -0.0026(14) C19 0.0255(19) 0.025(2) 0.0179(18) -0.0054(15) -0.0071(15) 0.0025(16) C23 0.0203(18) 0.023(2) 0.0228(19) -0.0037(15) -0.0019(15) 0.0036(15) C26 0.0207(18) 0.027(2) 0.0141(17) -0.0033(15) -0.0036(14) 0.0024(15) C8 0.0229(18) 0.0197(19) 0.0180(17) -0.0030(14) -0.0032(14) 0.0008(15) C17 0.0218(18) 0.023(2) 0.0173(17) -0.0040(14) -0.0062(14) 0.0024(15) C18 0.0208(18) 0.0188(19) 0.0201(18) -0.0032(14) -0.0063(14) -0.0004(14) C24 0.0201(18) 0.022(2) 0.0195(18) -0.0053(15) -0.0045(14) 0.0033(15) C7 0.0187(17) 0.023(2) 0.0228(19) -0.0030(15) -0.0059(14) 0.0003(15) C9 0.0181(17) 0.0208(19) 0.0197(18) -0.0032(15) -0.0036(14) -0.0010(14) C6 0.0218(18) 0.022(2) 0.0232(19) -0.0010(15) -0.0047(15) 0.0007(15) C13 0.0222(19) 0.026(2) 0.0206(18) -0.0024(16) -0.0065(15) -0.0028(16) C21 0.0180(18) 0.024(2) 0.029(2) -0.0073(16) -0.0077(15) 0.0010(15) C4 0.0241(19) 0.023(2) 0.027(2) -0.0072(16) -0.0078(16) -0.0018(16) C38 0.032(2) 0.024(2) 0.030(2) -0.0066(17) -0.0025(17) -0.0020(17) C27 0.027(2) 0.027(2) 0.024(2) -0.0059(16) -0.0066(16) 0.0037(16) C20 0.026(2) 0.031(2) 0.0220(19) -0.0078(16) -0.0112(16) -0.0027(17) C2 0.0206(18) 0.032(2) 0.0204(19) -0.0050(16) -0.0026(15) 0.0003(16) C1 0.0195(17) 0.026(2) 0.0180(17) -0.0031(15) -0.0080(14) 0.0002(15) C28 0.037(2) 0.029(2) 0.0207(19) -0.0054(17) -0.0079(17) 0.0026(18) N5 0.060(3) 0.050(3) 0.040(2) -0.019(2) -0.014(2) 0.017(2) C12 0.0199(19) 0.029(2) 0.032(2) -0.0073(18) 0.0006(16) -0.0049(16) C33 0.0234(19) 0.023(2) 0.025(2) -0.0023(16) -0.0058(15) 0.0029(16) C36 0.024(2) 0.029(2) 0.029(2) -0.0016(17) -0.0081(16) 0.0016(17) C41 0.030(2) 0.023(2) 0.027(2) -0.0033(16) -0.0060(17) 0.0040(17) C16 0.028(2) 0.024(2) 0.0216(19) -0.0059(16) -0.0061(15) 0.0046(16) C32 0.026(2) 0.027(2) 0.029(2) 0.0022(17) -0.0079(17) 0.0054(17) C30 0.0213(18) 0.029(2) 0.0210(19) -0.0011(16) -0.0033(15) -0.0012(16) C10 0.0230(19) 0.024(2) 0.029(2) -0.0086(17) -0.0015(16) 0.0006(16) C3 0.0196(18) 0.031(2) 0.027(2) -0.0008(17) -0.0044(15) -0.0070(16) C39 0.026(2) 0.028(2) 0.036(2) -0.0033(19) -0.0054(17) 0.0042(17) C15 0.032(2) 0.021(2) 0.031(2) -0.0042(17) -0.0114(17) -0.0063(17) C11 0.026(2) 0.034(2) 0.031(2) -0.0120(19) 0.0010(17) 0.0011(18) C29 0.030(2) 0.035(2) 0.022(2) 0.0005(17) -0.0103(16) -0.0016(18) C37 0.032(2) 0.024(2) 0.030(2) 0.0045(17) -0.0117(17) 0.0010(17) C35 0.057(3) 0.040(3) 0.023(2) -0.016(2) -0.018(2) 0.033(3) C40 0.027(2) 0.031(2) 0.029(2) -0.0012(18) -0.0068(17) -0.0007(18) C14 0.028(2) 0.027(2) 0.029(2) -0.0016(17) -0.0062(17) -0.0081(17) C31 0.030(2) 0.031(2) 0.025(2) 0.0015(17) -0.0108(17) 0.0043(18) C5 0.036(2) 0.020(2) 0.037(2) -0.0071(18) -0.0068(19) -0.0051(18) C22 0.030(2) 0.035(3) 0.032(2) -0.0040(19) -0.0076(18) 0.0118(19) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Fe1 N3 88.08(12) . . ? O1 Fe1 N4 90.39(12) . . ? O1 Fe1 N1 94.62(13) . . ? O1 Fe1 N2 176.29(12) . . ? O3 Fe1 O1 92.25(12) . . ? O3 Fe1 N3 94.26(12) . . ? O3 Fe1 N4 175.84(13) . . ? O3 Fe1 N1 88.90(12) . . ? O3 Fe1 N2 90.00(12) . . ? N3 Fe1 N4 82.61(13) . . ? N3 Fe1 N2 94.70(13) . . ? N4 Fe1 N2 87.54(13) . . ? N1 Fe1 N3 175.77(14) . . ? N1 Fe1 N4 94.10(13) . . ? N1 Fe1 N2 82.47(13) . . ? C1 O1 Fe1 125.5(2) . . ? C18 O3 Fe1 126.0(2) . . ? C21 O4 C22 116.1(3) . . ? C4 O2 C5 116.5(3) . . ? C25 N3 Fe1 125.2(3) . . ? C25 N3 C26 120.6(3) . . ? C26 N3 Fe1 114.1(2) . . ? C34 N4 Fe1 112.9(2) . . ? C33 N4 Fe1 128.6(3) . . ? C33 N4 C34 118.5(3) . . ? C8 N1 Fe1 125.1(3) . . ? C8 N1 C9 120.4(3) . . ? C9 N1 Fe1 114.5(3) . . ? C17 N2 Fe1 112.6(3) . . ? C16 N2 Fe1 129.0(3) . . ? C16 N2 C17 118.4(3) . . ? N3 C25 H25 117.3 . . ? N3 C25 C24 125.3(3) . . ? C24 C25 H25 117.3 . . ? N4 C34 C26 116.4(3) . . ? N4 C34 C30 122.9(3) . . ? C26 C34 C30 120.7(3) . . ? C18 C19 H19 119.1 . . ? C20 C19 H19 119.1 . . ? C20 C19 C18 121.9(4) . . ? C24 C23 H23 119.6 . . ? C21 C23 H23 119.6 . . ? C21 C23 C24 120.7(4) . . ? C34 C26 N3 113.7(3) . . ? C27 C26 N3 127.0(4) . . ? C27 C26 C34 119.4(3) . . ? N1 C8 H8 117.6 . . ? N1 C8 C7 124.7(4) . . ? C7 C8 H8 117.6 . . ? N2 C17 C9 117.0(3) . . ? N2 C17 C13 122.3(4) . . ? C9 C17 C13 120.8(3) . . ? O3 C18 C19 118.1(3) . . ? O3 C18 C24 125.4(3) . . ? C19 C18 C24 116.5(3) . . ? C23 C24 C25 116.7(3) . . ? C23 C24 C18 120.7(4) . . ? C18 C24 C25 122.5(3) . . ? C6 C7 C8 115.9(3) . . ? C6 C7 C1 121.0(4) . . ? C1 C7 C8 123.0(4) . . ? C17 C9 N1 112.9(3) . . ? C10 C9 N1 127.5(4) . . ? C10 C9 C17 119.7(3) . . ? C7 C6 H6 119.7 . . ? C4 C6 C7 120.5(4) . . ? C4 C6 H6 119.7 . . ? C17 C13 C14 117.0(4) . . ? C12 C13 C17 118.4(4) . . ? C12 C13 C14 124.6(4) . . ? O4 C21 C20 116.2(4) . . ? C23 C21 O4 125.0(4) . . ? C23 C21 C20 118.8(4) . . ? O2 C4 C6 124.8(4) . . ? O2 C4 C3 116.4(3) . . ? C6 C4 C3 118.8(4) . . ? C39 C38 I2 121.4(3) . . ? C37 C38 I2 121.4(3) . . ? C37 C38 C39 117.1(4) . . ? C26 C27 H27 120.2 . . ? C26 C27 C28 119.6(4) . . ? C28 C27 H27 120.2 . . ? C19 C20 C21 121.4(4) . . ? C19 C20 H20 119.3 . . ? C21 C20 H20 119.3 . . ? C1 C2 H2 119.3 . . ? C3 C2 H2 119.3 . . ? C3 C2 C1 121.3(4) . . ? O1 C1 C7 125.6(3) . . ? O1 C1 C2 117.6(3) . . ? C7 C1 C2 116.7(4) . . ? C27 C28 H28 119.2 . . ? C29 C28 C27 121.6(4) . . ? C29 C28 H28 119.2 . . ? C13 C12 H12 120.2 . . ? C11 C12 C13 119.5(4) . . ? C11 C12 H12 120.2 . . ? N4 C33 H33 118.9 . . ? N4 C33 C32 122.2(4) . . ? C32 C33 H33 118.9 . . ? C41 C36 I1 122.5(3) . . ? C37 C36 I1 120.0(3) . . ? C37 C36 C41 117.3(4) . . ? F3 C41 C36 118.6(4) . . ? F3 C41 C40 118.8(4) . . ? C40 C41 C36 122.7(4) . . ? N2 C16 H16 118.5 . . ? N2 C16 C15 122.9(4) . . ? C15 C16 H16 118.5 . . ? C33 C32 H32 119.9 . . ? C31 C32 C33 120.3(4) . . ? C31 C32 H32 119.9 . . ? C34 C30 C31 116.9(4) . . ? C29 C30 C34 118.1(4) . . ? C29 C30 C31 124.9(4) . . ? C9 C10 H10 120.4 . . ? C9 C10 C11 119.1(4) . . ? C11 C10 H10 120.4 . . ? C4 C3 H3 119.2 . . ? C2 C3 C4 121.6(4) . . ? C2 C3 H3 119.2 . . ? F2 C39 C38 118.7(4) . . ? F2 C39 C40 118.2(4) . . ? C38 C39 C40 123.1(4) . . ? C16 C15 H15 119.9 . . ? C14 C15 C16 120.1(4) . . ? C14 C15 H15 119.9 . . ? C12 C11 C10 122.4(4) . . ? C12 C11 H11 118.8 . . ? C10 C11 H11 118.8 . . ? C28 C29 C30 120.5(4) . . ? C28 C29 H29 119.7 . . ? C30 C29 H29 119.7 . . ? F1 C37 C38 118.3(4) . . ? F1 C37 C36 118.6(4) . . ? C36 C37 C38 123.1(4) . . ? N5 C35 S1 179.8(5) . . ? C41 C40 I3 122.5(3) . . ? C41 C40 C39 116.7(4) . . ? C39 C40 I3 120.7(3) . . ? C13 C14 H14 120.4 . . ? C15 C14 C13 119.3(4) . . ? C15 C14 H14 120.4 . . ? C32 C31 C30 119.2(4) . . ? C32 C31 H31 120.4 . . ? C30 C31 H31 120.4 . . ? O2 C5 H5A 109.5 . . ? O2 C5 H5B 109.5 . . ? O2 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? O4 C22 H22A 109.5 . . ? O4 C22 H22B 109.5 . . ? O4 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I3 C40 2.100(4) . ? I1 C36 2.086(4) . ? I2 C38 2.076(4) . ? Fe1 O1 1.877(3) . ? Fe1 O3 1.876(3) . ? Fe1 N3 1.940(3) . ? Fe1 N4 1.987(3) . ? Fe1 N1 1.934(3) . ? Fe1 N2 1.989(3) . ? S1 C35 1.654(6) . ? F3 C41 1.344(5) . ? F2 C39 1.349(5) . ? O1 C1 1.317(5) . ? O3 C18 1.318(4) . ? F1 C37 1.343(5) . ? O4 C21 1.375(5) . ? O4 C22 1.419(5) . ? O2 C4 1.373(5) . ? O2 C5 1.423(5) . ? N3 C25 1.297(5) . ? N3 C26 1.416(5) . ? N4 C34 1.369(5) . ? N4 C33 1.322(5) . ? N1 C8 1.308(5) . ? N1 C9 1.420(5) . ? N2 C17 1.368(5) . ? N2 C16 1.321(5) . ? C25 H25 0.9500 . ? C25 C24 1.425(5) . ? C34 C26 1.413(5) . ? C34 C30 1.415(5) . ? C19 H19 0.9500 . ? C19 C18 1.414(5) . ? C19 C20 1.364(6) . ? C23 H23 0.9500 . ? C23 C24 1.416(5) . ? C23 C21 1.372(6) . ? C26 C27 1.383(5) . ? C8 H8 0.9500 . ? C8 C7 1.425(5) . ? C17 C9 1.411(5) . ? C17 C13 1.417(5) . ? C18 C24 1.422(5) . ? C7 C6 1.409(6) . ? C7 C1 1.416(5) . ? C9 C10 1.381(5) . ? C6 H6 0.9500 . ? C6 C4 1.378(5) . ? C13 C12 1.415(6) . ? C13 C14 1.421(6) . ? C21 C20 1.403(5) . ? C4 C3 1.404(6) . ? C38 C39 1.384(6) . ? C38 C37 1.378(6) . ? C27 H27 0.9500 . ? C27 C28 1.398(6) . ? C20 H20 0.9500 . ? C2 H2 0.9500 . ? C2 C1 1.422(5) . ? C2 C3 1.363(6) . ? C28 H28 0.9500 . ? C28 C29 1.368(6) . ? N5 C35 1.167(7) . ? C12 H12 0.9500 . ? C12 C11 1.367(6) . ? C33 H33 0.9500 . ? C33 C32 1.415(6) . ? C36 C41 1.395(6) . ? C36 C37 1.378(6) . ? C41 C40 1.382(6) . ? C16 H16 0.9500 . ? C16 C15 1.394(6) . ? C32 H32 0.9500 . ? C32 C31 1.361(6) . ? C30 C29 1.405(6) . ? C30 C31 1.424(6) . ? C10 H10 0.9500 . ? C10 C11 1.407(6) . ? C3 H3 0.9500 . ? C39 C40 1.394(6) . ? C15 H15 0.9500 . ? C15 C14 1.358(6) . ? C11 H11 0.9500 . ? C29 H29 0.9500 . ? C14 H14 0.9500 . ? C31 H31 0.9500 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag I1 C36 C41 F3 -3.8(6) . . . . ? I1 C36 C41 C40 176.7(3) . . . . ? I1 C36 C37 F1 4.5(6) . . . . ? I1 C36 C37 C38 -175.5(3) . . . . ? I2 C38 C39 F2 4.7(6) . . . . ? I2 C38 C39 C40 -175.9(3) . . . . ? I2 C38 C37 F1 -4.3(6) . . . . ? I2 C38 C37 C36 175.7(3) . . . . ? Fe1 O1 C1 C7 -10.6(5) . . . . ? Fe1 O1 C1 C2 173.2(3) . . . . ? Fe1 O3 C18 C19 174.1(3) . . . . ? Fe1 O3 C18 C24 -8.4(6) . . . . ? Fe1 N3 C25 C24 7.3(6) . . . . ? Fe1 N3 C26 C34 4.6(4) . . . . ? Fe1 N3 C26 C27 -174.4(3) . . . . ? Fe1 N4 C34 C26 -2.6(4) . . . . ? Fe1 N4 C34 C30 178.9(3) . . . . ? Fe1 N4 C33 C32 -179.7(3) . . . . ? Fe1 N1 C8 C7 7.6(5) . . . . ? Fe1 N1 C9 C17 7.7(4) . . . . ? Fe1 N1 C9 C10 -171.8(3) . . . . ? Fe1 N2 C17 C9 -2.2(4) . . . . ? Fe1 N2 C17 C13 177.2(3) . . . . ? Fe1 N2 C16 C15 -179.6(3) . . . . ? F3 C41 C40 I3 -4.0(6) . . . . ? F3 C41 C40 C39 178.6(4) . . . . ? F2 C39 C40 I3 2.7(6) . . . . ? F2 C39 C40 C41 -179.8(4) . . . . ? O1 Fe1 O3 C18 -76.3(3) . . . . ? O3 Fe1 O1 C1 -76.2(3) . . . . ? O3 C18 C24 C25 -0.1(6) . . . . ? O3 C18 C24 C23 -176.5(4) . . . . ? O4 C21 C20 C19 -177.5(4) . . . . ? O2 C4 C3 C2 -177.2(4) . . . . ? N3 Fe1 O1 C1 -170.4(3) . . . . ? N3 Fe1 O3 C18 11.9(3) . . . . ? N3 C25 C24 C23 177.0(4) . . . . ? N3 C25 C24 C18 0.4(7) . . . . ? N3 C26 C27 C28 -178.5(4) . . . . ? N4 Fe1 O1 C1 107.0(3) . . . . ? N4 C34 C26 N3 -1.3(5) . . . . ? N4 C34 C26 C27 177.8(4) . . . . ? N4 C34 C30 C29 -179.3(4) . . . . ? N4 C34 C30 C31 1.6(6) . . . . ? N4 C33 C32 C31 0.1(6) . . . . ? N1 Fe1 O1 C1 12.9(3) . . . . ? N1 Fe1 O3 C18 -170.9(3) . . . . ? N1 C8 C7 C6 176.0(4) . . . . ? N1 C8 C7 C1 -1.0(6) . . . . ? N1 C9 C10 C11 -178.8(4) . . . . ? N2 Fe1 O3 C18 106.6(3) . . . . ? N2 C17 C9 N1 -3.4(5) . . . . ? N2 C17 C9 C10 176.1(4) . . . . ? N2 C17 C13 C12 -176.5(4) . . . . ? N2 C17 C13 C14 3.5(6) . . . . ? N2 C16 C15 C14 1.3(6) . . . . ? C25 N3 C26 C34 -171.6(4) . . . . ? C25 N3 C26 C27 9.4(6) . . . . ? C34 N4 C33 C32 0.3(6) . . . . ? C34 C26 C27 C28 2.6(6) . . . . ? C34 C30 C29 C28 0.1(6) . . . . ? C34 C30 C31 C32 -1.1(6) . . . . ? C19 C18 C24 C25 177.5(4) . . . . ? C19 C18 C24 C23 1.2(6) . . . . ? C23 C21 C20 C19 1.9(6) . . . . ? C26 N3 C25 C24 -176.9(4) . . . . ? C26 C34 C30 C29 2.3(6) . . . . ? C26 C34 C30 C31 -176.9(4) . . . . ? C26 C27 C28 C29 -0.3(7) . . . . ? C8 N1 C9 C17 -170.2(3) . . . . ? C8 N1 C9 C10 10.3(6) . . . . ? C8 C7 C6 C4 -175.5(4) . . . . ? C8 C7 C1 O1 2.4(6) . . . . ? C8 C7 C1 C2 178.6(3) . . . . ? C17 N2 C16 C15 0.4(6) . . . . ? C17 C9 C10 C11 1.8(6) . . . . ? C17 C13 C12 C11 -1.0(6) . . . . ? C17 C13 C14 C15 -1.8(6) . . . . ? C18 C19 C20 C21 -1.2(6) . . . . ? C24 C23 C21 O4 178.3(4) . . . . ? C24 C23 C21 C20 -1.0(6) . . . . ? C7 C6 C4 O2 176.3(4) . . . . ? C7 C6 C4 C3 -4.0(6) . . . . ? C9 N1 C8 C7 -174.7(3) . . . . ? C9 C17 C13 C12 2.9(6) . . . . ? C9 C17 C13 C14 -177.1(4) . . . . ? C9 C10 C11 C12 0.2(7) . . . . ? C6 C7 C1 O1 -174.4(4) . . . . ? C6 C7 C1 C2 1.8(6) . . . . ? C6 C4 C3 C2 3.1(6) . . . . ? C13 C17 C9 N1 177.1(3) . . . . ? C13 C17 C9 C10 -3.3(6) . . . . ? C13 C12 C11 C10 -0.6(7) . . . . ? C21 C23 C24 C25 -177.1(4) . . . . ? C21 C23 C24 C18 -0.5(6) . . . . ? C38 C39 C40 I3 -176.7(3) . . . . ? C38 C39 C40 C41 0.7(7) . . . . ? C27 C28 C29 C30 -1.1(7) . . . . ? C20 C19 C18 O3 177.5(4) . . . . ? C20 C19 C18 C24 -0.3(6) . . . . ? C1 C7 C6 C4 1.6(6) . . . . ? C1 C2 C3 C4 0.3(6) . . . . ? C12 C13 C14 C15 178.2(4) . . . . ? C33 N4 C34 C26 177.4(4) . . . . ? C33 N4 C34 C30 -1.2(6) . . . . ? C33 C32 C31 C30 0.3(6) . . . . ? C36 C41 C40 I3 175.5(3) . . . . ? C36 C41 C40 C39 -1.9(6) . . . . ? C41 C36 C37 F1 179.6(4) . . . . ? C41 C36 C37 C38 -0.4(7) . . . . ? C16 N2 C17 C9 177.8(3) . . . . ? C16 N2 C17 C13 -2.8(5) . . . . ? C16 C15 C14 C13 -0.5(6) . . . . ? C30 C34 C26 N3 177.3(3) . . . . ? C30 C34 C26 C27 -3.6(6) . . . . ? C3 C2 C1 O1 173.8(4) . . . . ? C3 C2 C1 C7 -2.7(6) . . . . ? C39 C38 C37 F1 179.3(4) . . . . ? C39 C38 C37 C36 -0.6(7) . . . . ? C29 C30 C31 C32 179.8(4) . . . . ? C37 C38 C39 F2 -178.9(4) . . . . ? C37 C38 C39 C40 0.5(7) . . . . ? C37 C36 C41 F3 -178.8(4) . . . . ? C37 C36 C41 C40 1.7(7) . . . . ? C14 C13 C12 C11 179.1(4) . . . . ? C31 C30 C29 C28 179.2(4) . . . . ? C5 O2 C4 C6 -13.8(6) . . . . ? C5 O2 C4 C3 166.5(4) . . . . ? C22 O4 C21 C23 -15.1(6) . . . . ? C22 O4 C21 C20 164.2(4) . . . . ?