#------------------------------------------------------------------------------ #$Date: 2021-05-19 01:21:31 +0300 (Wed, 19 May 2021) $ #$Revision: 265313 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/00/39/4003941.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4003941 loop_ _publ_author_name 'Cho, Jung' 'Yun, Yifeng' 'Xu, Hongyi' 'Sun, Junliang' 'Burton, Allen W.' 'Strohmaier, Karl G.' 'Terefenko, Gene' 'Vroman, Hilda' 'Afeworki, Mobae' 'Cao, Guang' 'Wang, Hao' 'Zou, Xiaodong' 'Willhammar, Tom' _publ_section_title ; EMM-25: The Structure of Two-Dimensional 11 \\times 10 Medium-Pore Borosilicate Zeolite Unraveled Using 3D Electron Diffraction ; _journal_name_full 'Chemistry of Materials' _journal_paper_doi 10.1021/acs.chemmater.1c00892 _journal_year 2021 _chemical_formula_moiety 'O232 Si116' _chemical_formula_sum 'O232 Si116' _chemical_formula_weight 6969.74 _space_group_crystal_system orthorhombic _space_group_IT_number 63 _space_group_name_Hall '-C 2c 2' _space_group_name_H-M_alt 'C m c m' _audit_creation_date 2021-02-26 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6257) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 1 _cell_length_a 11.055(2) _cell_length_b 22.912(5) _cell_length_c 24.914(5) _cell_measurement_temperature 293(2) _cell_volume 6311(2) _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.964 _diffrn_measurement_device_type JEOL-2100 _diffrn_radiation_type electron _diffrn_radiation_wavelength 0.02508 _diffrn_reflns_av_R_equivalents 0.2266 _diffrn_reflns_av_unetI/netI 0.1109 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.964 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 45467 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.964 _diffrn_reflns_theta_full 0.862 _diffrn_reflns_theta_max 0.904 _diffrn_reflns_theta_min 0.058 _exptl_absorpt_coefficient_mu 0.000 _exptl_crystal_density_diffrn 1.834 _exptl_crystal_description 'needle-like nanocrystal' _exptl_crystal_F_000 1135 _refine_diff_density_max 0.296 _refine_diff_density_min -0.433 _refine_diff_density_rms 0.101 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.685 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 189 _refine_ls_number_reflns 3419 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.685 _refine_ls_R_factor_all 0.2133 _refine_ls_R_factor_gt 0.1938 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.4486 _refine_ls_wR_factor_ref 0.4635 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2640 _reflns_number_total 3419 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cm1c00892_si_002.cif _cod_data_source_block cal _cod_database_code 4003941 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Others Fixed Sof: Si1(0.25) Si2(0.25) Si3(0.25) Si4(0.25) Si5(0.25) Si6(0.5) Si7(0.5) Si8(0.5) Si9(0.5) Si10(0.5) Si11(0.5) Si12(0.5) Si13(0.5) Si14(0.5) Si15(0.5) O1(0.25) O2(0.25) O3(0.25) O4(0.25) O5(0.25) O6(0.5) O7(0.5) O8(0.5) O9(0.5) O10(0.5) O11(0.5) O12(0.5) O13(0.5) O14(0.5) O15(0.5) O16(0.5) O17(0.5) O18(0.5) O19(0.5) O20(0.5) O21(0.5) O22(0.5) O23(0.5) O24(0.5) O25(0.5) O26(0.5) O28(0.5) O29(0.25) O30(0.25) O31(0.25) O32(0.25) O33(0.25) O34(0.25) O35(0.25) ; _shelx_res_file ; TITL cmcm_Dchain_TW cal.res created by SHELXL-2018/3 at 14:04:19 on 26-Feb-2021 CELL 0.02508 11.055 22.912 24.914 90 90 90 ZERR 1 0.0023 0.0047 0.0051 0 0 0 LATT 7 SYMM -X,-Y,0.5+Z SYMM -X,+Y,0.5-Z SYMM +X,-Y,-Z SFAC O 0.455 23.78 0.917 7.622 0.472 2.144 0.138 0.296 0 0 0 0 0.73 15.999 SFAC SI 2.129 57.775 2.533 16.476 0.835 2.88 0.322 0.386 0 0 0 0 1.11 28.086 UNIT 232 116 L.S. 20 PLAN 1 CONF LIST 6 MORE -1 fmap 2 acta REM REM REM WGHT 0.200000 FVAR 0.40578 SI1 2 0.500000 0.464283 0.069557 10.25000 0.02443 SI2 2 0.000000 0.049838 0.164958 10.25000 0.02371 SI3 2 0.500000 0.475888 0.266910 10.25000 0.02692 SI4 2 0.000000 0.053498 0.366627 10.25000 0.02165 SI5 2 0.500000 0.470262 0.460052 10.25000 0.02781 SI6 2 0.242607 0.122556 0.343842 10.50000 0.02247 SI7 2 0.358206 0.056709 0.439801 10.50000 0.01519 SI8 2 0.236355 0.438868 0.441007 10.50000 0.01780 SI9 2 0.141103 0.368676 0.157358 10.50000 0.02246 SI10 2 0.143390 0.239538 0.191242 10.50000 0.02230 SI11 2 0.239305 0.120113 0.148071 10.50000 0.01522 SI12 2 0.356213 0.066658 0.055163 10.50000 0.02522 SI13 2 0.239491 0.429778 0.056699 10.50000 0.02961 SI14 2 0.138644 0.363590 0.349535 10.50000 0.01875 SI15 2 0.138779 0.235996 0.315987 10.50000 0.01891 SI16 2 0.242663 0.434847 0.250000 10.50000 0.02724 SI17 2 0.359388 0.062233 0.250000 10.50000 0.02187 O1 1 0.000000 0.015116 0.023931 10.25000 0.04334 O2 1 0.500000 0.495102 0.125265 10.25000 0.04775 O3 1 0.000000 0.028776 0.224864 10.25000 0.05356 O4 1 0.500000 0.501822 0.325929 10.25000 0.04357 O5 1 0.000000 0.030016 0.425264 10.25000 0.05780 O6 1 0.176505 0.301486 0.165763 10.50000 0.02580 O7 1 0.219793 0.191330 0.153501 10.50000 0.02441 O8 1 0.331901 0.110684 0.102828 10.50000 0.03103 O9 1 0.382736 0.425425 0.065708 10.50000 0.03558 O10 1 0.196948 0.500162 0.082107 10.50000 0.04006 O11 1 0.168955 0.423551 0.495663 10.50000 0.04075 O12 1 0.168044 0.387918 0.092267 10.50000 0.02509 O13 1 0.118451 0.088062 0.157500 10.50000 0.03812 O14 1 0.337765 0.094983 0.194209 10.50000 0.03724 O15 1 0.181932 0.397005 0.292259 10.50000 0.06475 O16 1 0.164064 0.294765 0.346176 10.50000 0.02891 O17 1 0.226675 0.187797 0.333128 10.50000 0.02400 O18 1 0.295270 0.110041 0.407980 10.50000 0.02767 O19 1 0.381459 0.433563 0.450866 10.50000 0.03469 O20 1 0.297997 -0.000424 0.430002 10.50000 0.03042 O21 1 0.295352 0.081195 0.495416 10.50000 0.04912 O22 1 0.213110 0.390095 0.395201 10.50000 0.04613 O23 1 0.111128 0.094696 0.361932 10.50000 0.03829 O24 1 0.292899 0.097365 0.292706 10.50000 0.06047 O25 1 0.220190 0.405608 0.192810 10.50000 0.03996 O26 1 0.194936 0.499443 0.239681 10.50000 0.05283 O27 1 0.170170 0.241763 0.250000 10.50000 0.03791 O28 1 0.386592 0.435310 0.261221 10.50000 0.04252 O29 1 0.000000 0.220343 0.183520 10.25000 0.03035 O30 1 0.000000 0.377234 0.166985 10.25000 0.02354 O31 1 0.000000 0.225518 0.325174 10.25000 0.03833 O32 1 0.000000 0.371005 0.358765 10.25000 0.04263 O33 1 0.500000 0.058005 0.066112 10.25000 0.04862 O34 1 0.500000 0.056187 0.450692 10.25000 0.04336 O35 1 0.500000 0.058433 0.261061 10.25000 0.05259 HKLF 4 REM cmcm_Dchain_TW REM wR2 = 0.4635, GooF = S = 1.685, Restrained GooF = 1.685 for all data REM R1 = 0.1938 for 2640 Fo > 4sig(Fo) and 0.2133 for all 3419 data REM 189 parameters refined using 0 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 0.296, deepest hole -0.433, 1-sigma level 0.101 Q1 1 0.5000 0.2065 0.0881 10.50000 0.05 0.30 ; _shelx_res_checksum 36154 _shelx_hkl_file ; 0 0 2 826.42 236.58 0 0 2 748.03 250.67 0 0 4 129.19 44.10 0 0 -4 144.69 41.80 0 0 -4 154.18 52.29 0 0 -4 155.58 27.60 0 0 6 403.36 135.69 0 0 6 413.36 118.49 0 0 -6 505.45 144.89 0 0 -6 503.45 89.09 0 0 -6 419.96 141.09 0 0 8 502.25 168.88 0 0 8 994.00 284.57 0 0 8 787.82 139.39 0 0 -8 855.51 245.08 0 0 -8 927.31 163.98 0 0 -8 525.95 176.68 0 0 10 3029.30 1014.10 0 0 10 5354.96 1532.95 0 0 10 3683.93 651.53 0 0 -10 4898.11 1402.26 0 0 -10 3486.05 616.64 0 0 -10 3640.04 1218.78 0 0 12 359.36 120.99 0 0 12 662.53 189.78 0 0 12 794.42 140.59 0 0 -12 747.33 214.08 0 0 -12 915.61 161.98 0 0 -12 430.46 144.79 0 0 14 90.49 31.50 0 0 14 116.39 33.50 0 0 14 94.89 16.90 0 0 -14 95.29 27.50 0 0 -14 111.79 19.90 0 0 -14 138.89 47.40 0 0 16 379.86 127.69 0 0 16 306.87 87.89 0 0 16 257.47 45.60 0 0 -16 280.67 80.49 0 0 -16 242.88 43.00 0 0 -16 322.77 108.69 0 0 18 160.78 46.20 0 0 18 100.99 34.80 0 0 18 119.99 21.30 0 0 -18 124.99 36.10 0 0 -18 73.59 25.90 0 0 20 596.84 200.28 0 0 20 985.20 282.17 0 0 20 638.84 113.09 0 0 -20 711.83 203.88 0 0 -20 549.45 97.29 0 0 -20 813.52 272.87 0 0 22 59.69 17.60 0 0 22 22.20 9.70 0 0 -22 27.40 9.00 0 0 24 44.30 13.40 0 0 24 27.60 10.80 0 0 -24 37.80 11.40 0 0 26 0.50 3.70 0 0 26 2.60 3.90 0 0 26 2.70 1.40 0 0 -26 5.30 3.50 0 0 -26 4.90 1.60 0 0 28 7.40 4.70 0 0 28 6.50 1.80 0 0 -28 8.50 4.20 0 0 -28 11.00 2.40 0 0 30 4.50 4.60 0 0 30 9.80 2.30 0 0 -30 5.20 4.90 0 0 -30 16.50 3.30 0 -2 0 1450.35 366.46 0 2 1 92.79 23.80 0 -2 1 79.49 20.60 0 -2 -2 684.73 172.98 0 2 2 1244.98 417.06 0 -2 2 949.31 239.98 0 -2 -3 13.70 4.40 0 2 3 121.89 35.40 0 -2 3 3.70 2.20 0 -2 -4 765.42 219.28 0 -2 -4 846.72 283.87 0 -2 -5 933.91 235.98 0 -2 -5 561.84 160.98 0 -2 -5 758.82 254.27 0 2 5 766.12 193.58 0 2 5 767.32 257.27 0 2 -5 600.74 201.38 0 -2 -6 3877.01 1110.09 0 -2 -6 3720.63 939.81 0 -2 -6 3583.84 1199.78 0 2 6 5071.59 1451.85 0 -2 6 3552.04 1189.68 0 2 -6 2865.61 959.30 0 -2 -7 10.60 8.80 0 -2 -7 18.70 7.60 0 -2 -7 4.20 3.20 0 -2 -7 21.00 6.00 0 2 7 11.20 5.00 0 2 7 15.40 10.50 0 -2 7 26.80 11.50 0 2 -7 10.00 2.50 0 2 -7 13.40 8.30 0 -2 -8 -1.50 4.30 0 -2 -8 4.60 4.60 0 -2 -8 1.00 8.60 0 2 8 7.80 9.20 0 2 8 6.30 3.60 0 -2 8 5.90 7.20 0 2 -8 4.30 7.50 0 -2 -9 18.90 11.20 0 -2 -9 3.60 3.90 0 -2 -9 1.40 4.00 0 -2 -9 11.50 2.90 0 2 9 8.80 5.70 0 2 9 14.10 9.80 0 -2 9 10.40 7.80 0 -2 9 7.10 2.10 0 2 -9 14.60 3.10 0 -2 -10 1657.83 555.24 0 -2 -10 2069.39 592.44 0 -2 -10 1230.78 217.68 0 -2 10 1435.76 481.05 0 -2 10 1013.80 179.38 0 2 -10 1382.46 395.96 0 2 -10 1497.05 264.77 0 2 -10 1563.04 523.55 0 -2 -11 27.60 12.90 0 -2 -11 4.50 4.50 0 -2 -11 7.60 2.40 0 2 11 -0.10 2.10 0 2 11 4.70 4.80 0 2 11 9.50 8.20 0 2 11 5.90 2.60 0 -2 11 7.30 2.20 0 -2 11 36.90 13.30 0 2 -11 2.00 4.90 0 2 -11 11.10 2.60 0 2 -11 4.30 7.20 0 -2 -12 5.60 6.10 0 -2 -12 3.90 4.50 0 -2 -12 3.30 2.00 0 2 12 10.00 9.00 0 2 12 4.60 2.30 0 2 12 1.10 4.20 0 -2 12 8.30 2.50 0 -2 12 26.30 11.70 0 -2 12 17.60 8.10 0 2 -12 2.00 4.90 0 2 -12 0.90 1.40 0 2 -12 14.90 9.20 0 -2 -13 -0.10 3.90 0 -2 -13 2.20 1.70 0 2 13 0.30 8.00 0 2 13 3.20 3.50 0 2 13 0.20 2.10 0 -2 13 3.30 6.60 0 -2 13 3.50 1.90 0 -2 13 10.80 8.10 0 2 -13 -0.20 3.30 0 2 -13 5.10 7.80 0 2 -13 0.40 1.60 0 -2 -14 213.08 61.19 0 -2 -14 294.17 99.09 0 -2 -14 150.08 26.70 0 2 14 239.98 80.99 0 2 14 312.97 89.79 0 2 14 223.38 39.60 0 -2 14 178.48 31.70 0 -2 14 248.98 83.89 0 2 -14 226.68 65.09 0 2 -14 179.48 31.80 0 2 -14 250.37 84.49 0 -2 -15 18.90 9.20 0 -2 -15 22.60 7.10 0 -2 -15 22.30 4.30 0 2 15 11.40 7.30 0 2 15 12.60 2.90 0 2 15 34.70 10.30 0 -2 15 21.30 4.20 0 -2 15 17.80 8.10 0 2 -15 23.90 7.40 0 2 -15 10.20 7.00 0 -2 -16 402.16 135.09 0 -2 -16 388.16 111.29 0 -2 -16 232.18 41.20 0 2 16 360.56 121.29 0 2 16 276.07 79.09 0 2 16 282.17 49.99 0 -2 16 307.77 54.49 0 -2 16 321.97 108.19 0 2 -16 288.77 82.79 0 2 -16 252.37 44.70 0 2 -16 328.37 110.39 0 -2 -17 5.50 7.50 0 -2 -17 4.80 3.20 0 -2 -17 7.50 2.00 0 2 17 10.50 7.50 0 2 17 3.70 2.80 0 2 17 7.30 1.90 0 -2 17 7.80 1.90 0 -2 17 4.70 4.50 0 -2 17 4.60 5.40 0 2 -17 1.50 2.80 0 2 -17 7.90 2.20 0 -2 -18 48.50 14.40 0 -2 -18 31.60 12.50 0 -2 -18 35.00 6.50 0 2 18 29.90 11.90 0 2 18 56.39 16.50 0 2 18 33.60 6.20 0 -2 18 37.00 11.90 0 -2 18 39.30 7.20 0 -2 18 30.30 11.40 0 2 -18 34.30 10.60 0 2 -18 42.50 7.70 0 -2 -19 11.10 6.90 0 -2 -19 12.00 4.90 0 -2 -19 9.40 2.40 0 2 19 9.20 6.40 0 2 19 11.10 4.60 0 2 19 6.40 2.00 0 -2 19 8.30 1.90 0 -2 19 9.90 5.80 0 2 -19 -0.40 3.40 0 2 -19 7.60 1.80 0 -2 -20 28.60 9.00 0 -2 -20 22.30 10.30 0 -2 -20 16.10 3.30 0 2 20 -1.60 5.30 0 2 20 25.50 8.10 0 2 20 7.40 1.90 0 -2 20 9.80 2.20 0 -2 20 12.50 6.40 0 -2 20 0.20 5.00 0 2 -20 15.10 6.30 0 2 -20 10.40 2.30 0 2 -20 7.70 6.20 0 -2 -21 1.60 4.00 0 -2 -21 2.70 6.60 0 -2 -21 4.80 1.70 0 2 21 -2.80 5.50 0 2 21 2.60 1.40 0 2 21 4.80 3.60 0 -2 21 -5.30 6.00 0 -2 21 1.00 1.40 0 -2 21 -1.00 4.50 0 2 -21 3.10 4.90 0 2 -21 -1.10 5.20 0 2 -21 1.70 1.50 0 -2 -22 9.30 4.50 0 -2 -22 10.50 7.20 0 -2 -22 4.80 1.60 0 2 22 12.10 4.90 0 2 22 7.50 1.90 0 -2 22 4.00 1.40 0 -2 22 4.00 6.00 0 -2 22 8.20 6.00 0 2 -22 9.80 5.70 0 2 -22 5.70 1.70 0 2 -22 3.40 5.60 0 -2 -23 2.10 5.70 0 -2 -23 3.00 4.30 0 -2 -23 0.60 1.50 0 2 23 3.00 3.50 0 2 23 2.10 1.70 0 -2 23 2.70 1.20 0 -2 23 4.00 5.40 0 -2 23 8.00 5.40 0 2 -23 0.00 4.30 0 2 -23 1.60 1.20 0 2 -23 0.50 5.30 0 -2 -24 -1.20 4.10 0 -2 -24 5.70 5.70 0 -2 -24 2.20 1.70 0 2 24 0.10 3.90 0 2 24 2.80 1.70 0 -2 24 2.20 1.20 0 -2 24 -4.90 4.70 0 -2 24 1.70 4.20 0 2 -24 2.10 1.20 0 2 -24 0.10 4.70 0 -2 -25 3.90 5.60 0 -2 -25 0.40 3.40 0 -2 -25 3.20 1.60 0 2 25 4.40 3.70 0 2 25 4.80 1.80 0 -2 25 1.30 1.20 0 -2 25 0.90 3.90 0 -2 25 2.20 4.10 0 2 -25 0.80 4.10 0 2 -25 1.10 1.10 0 2 -25 1.00 4.70 0 -2 -26 22.80 9.80 0 -2 -26 37.10 11.30 0 -2 -26 31.50 5.80 0 2 26 31.20 11.80 0 2 26 27.20 8.70 0 2 26 30.80 5.70 0 -2 26 28.70 5.30 0 -2 26 20.10 7.20 0 -2 26 29.60 11.00 0 2 -26 25.10 9.90 0 2 -26 29.90 5.50 0 -2 -27 0.30 5.20 0 -2 -27 -1.40 3.20 0 -2 -27 2.60 1.30 0 2 27 0.20 3.60 0 2 27 1.60 1.20 0 2 27 6.90 4.50 0 -2 27 -2.60 3.80 0 -2 27 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0 -12 0 525.45 133.19 0 -12 0 609.54 204.18 0 12 0 524.95 132.99 0 12 0 393.36 131.89 0 -12 -1 9.40 4.40 0 -12 -1 22.10 8.40 0 12 1 13.00 6.50 0 12 1 6.90 4.70 0 -12 1 3.40 3.90 0 -12 1 5.20 2.70 0 12 -1 8.00 6.50 0 12 -1 7.80 3.50 0 -12 -2 14.20 5.30 0 -12 -2 16.80 7.00 0 12 2 6.50 5.40 0 12 2 14.80 5.70 0 -12 2 8.30 4.30 0 -12 2 16.90 6.30 0 12 -2 6.30 6.10 0 12 -2 15.80 6.10 0 -12 -3 103.39 26.60 0 -12 -3 87.19 29.70 0 12 3 112.09 28.80 0 12 3 81.79 28.20 0 -12 -4 864.31 218.48 0 -12 -4 854.01 286.07 0 12 4 1067.79 357.66 0 -12 -5 51.69 13.60 0 -12 -5 37.90 13.80 0 12 5 55.99 14.60 0 -12 5 103.09 26.60 0 12 -5 45.30 13.10 0 -12 -6 141.29 36.10 0 -12 -6 165.28 55.79 0 12 6 138.59 35.40 0 -12 6 138.59 35.60 0 12 -6 108.79 28.80 0 -12 -7 9.30 3.60 0 -12 -7 16.00 7.30 0 -12 7 8.30 5.30 0 12 -7 12.40 6.30 0 12 8 57.89 15.00 0 -12 8 35.40 11.30 0 12 -8 40.20 12.00 0 -12 -9 48.10 17.10 0 -12 -9 92.89 23.70 0 12 9 128.79 43.70 0 -12 9 143.29 37.10 0 -12 9 62.19 12.10 0 12 -9 100.09 26.50 0 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18.10 3.90 -5 5 -6 14.40 8.60 -5 5 -6 36.80 7.30 5 5 7 24.40 7.00 5 5 7 6.00 1.90 5 -5 -7 -4.60 9.60 5 -5 -7 5.20 4.60 5 -5 -7 10.60 3.60 5 5 -7 18.90 7.40 5 5 -7 15.40 7.90 5 5 -7 15.60 5.20 5 5 -7 12.30 2.90 5 -5 7 15.80 4.20 5 -5 7 13.40 7.90 -5 -5 -7 26.80 7.20 -5 -5 -7 17.70 7.10 -5 -5 -7 6.90 2.30 -5 5 7 10.90 3.10 -5 5 7 5.90 4.70 -5 5 7 0.40 7.80 -5 -5 7 13.70 6.40 -5 -5 7 14.40 6.00 -5 -5 7 13.20 5.20 -5 5 -7 12.90 3.60 5 5 8 8.30 4.90 5 -5 -8 -0.90 5.50 5 -5 -8 -0.90 2.20 5 -5 -8 6.40 5.10 5 5 -8 -2.00 3.50 5 5 -8 6.60 5.80 5 5 -8 16.20 6.70 5 -5 8 6.20 3.10 -5 -5 -8 0.90 2.10 -5 -5 -8 3.70 5.50 -5 5 8 3.20 4.40 -5 5 8 -1.10 6.90 -5 -5 8 0.90 5.80 -5 -5 8 2.00 1.70 -5 -5 8 3.20 3.30 -5 5 -8 -1.30 7.40 -5 5 -8 2.40 2.70 5 -5 -9 15.00 3.50 5 5 -9 18.70 7.60 5 5 -9 15.80 6.50 5 5 -9 2.10 6.50 5 5 -9 12.50 2.90 5 -5 9 9.90 3.50 -5 -5 -9 17.50 3.80 -5 -5 -9 2.20 6.00 -5 5 9 13.80 9.60 -5 5 9 18.30 4.00 -5 5 9 9.70 5.80 -5 -5 9 13.10 7.40 -5 -5 9 14.10 3.20 -5 5 -9 14.20 4.00 5 5 10 74.79 13.50 5 -5 -10 51.29 18.10 5 -5 -10 97.39 24.70 5 -5 -10 48.10 8.90 5 5 -10 84.09 21.90 5 5 -10 28.10 10.80 5 -5 10 61.89 11.60 -5 -5 -10 38.10 7.10 -5 -5 -10 47.20 15.00 -5 5 10 107.09 27.20 -5 5 10 51.39 9.50 -5 5 10 62.09 21.80 -5 -5 10 54.59 19.00 -5 -5 10 39.00 13.20 -5 -5 10 46.10 8.50 -5 5 -10 20.30 9.60 -5 5 -10 61.49 11.60 5 5 11 24.10 8.50 5 -5 -11 31.30 10.90 5 -5 -11 28.20 11.10 5 -5 -11 42.80 8.10 5 5 -11 34.30 12.40 5 5 -11 48.90 9.00 5 5 -11 14.60 8.00 5 -5 11 59.59 11.30 -5 -5 -11 44.40 8.30 -5 5 11 38.70 14.30 -5 5 11 29.50 11.10 -5 5 11 44.30 8.20 -5 -5 11 8.90 6.60 -5 -5 11 77.69 26.80 -5 -5 11 38.90 7.20 5 5 12 0.40 2.90 5 5 12 19.10 7.40 5 5 12 9.70 2.70 5 -5 -12 0.30 7.00 5 -5 -12 0.90 4.80 5 -5 -12 -0.90 3.70 5 -5 -12 10.90 2.70 5 5 -12 3.90 4.00 5 5 -12 8.00 2.20 5 -5 12 -1.80 5.80 -5 -5 -12 4.50 2.20 -5 -5 -12 5.80 2.30 -5 -5 -12 31.80 11.30 -5 5 12 2.80 7.80 -5 5 12 12.10 3.10 -5 5 12 5.00 5.00 -5 -5 12 16.40 7.70 -5 -5 12 6.90 5.10 -5 -5 12 9.30 2.50 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25 -2.10 2.70 -5 -5 -25 3.60 2.60 -5 -5 -25 -11.50 14.40 -5 5 25 -0.40 5.50 -5 5 25 8.20 2.10 -5 -5 25 -0.40 4.30 -5 -5 25 3.40 1.60 -5 5 -25 7.10 7.40 -5 5 -25 4.90 1.30 5 5 26 5.60 3.90 5 5 26 -0.80 5.30 5 -5 -26 12.90 7.50 5 -5 -26 5.80 1.80 5 5 -26 5.70 1.80 5 5 -26 1.60 4.20 5 -5 26 12.80 2.40 -5 -5 -26 11.40 4.30 -5 5 26 12.40 7.00 -5 5 26 4.60 1.70 -5 5 -26 7.40 1.60 5 5 27 6.50 3.90 5 -5 -27 -1.80 6.20 5 -5 -27 3.30 1.60 5 5 -27 3.20 1.40 5 5 -27 1.00 4.50 5 -5 27 3.10 0.90 5 -5 27 1.70 2.80 -5 -5 -27 5.70 14.20 -5 -5 -27 0.00 2.60 -5 5 27 2.30 1.50 -5 -5 27 3.30 1.50 -5 5 -27 5.70 7.10 -5 5 -27 2.60 0.80 5 5 28 0.90 4.50 5 -5 -28 1.10 1.40 5 5 -28 1.10 1.20 5 -5 28 0.30 0.70 -5 -5 -28 3.00 3.00 -5 -5 -28 -0.30 1.30 -5 5 28 0.20 1.50 -5 -5 28 -0.40 1.20 -5 5 -28 0.80 0.70 5 7 0 362.56 104.19 5 7 0 294.87 52.29 5 -7 0 376.96 108.49 -5 -7 0 313.47 90.09 -5 -7 0 319.57 80.99 -5 -7 0 233.18 41.40 -5 7 0 385.06 110.79 -5 7 0 286.57 96.29 -5 7 0 213.08 38.10 5 7 1 64.69 19.70 5 7 1 53.79 14.10 5 7 1 91.09 16.40 5 -7 -1 56.99 20.60 5 -7 -1 61.19 20.10 5 7 -1 63.59 19.20 5 -7 1 72.89 14.00 5 -7 1 63.59 19.90 -5 -7 -1 54.39 16.50 -5 -7 -1 114.59 20.60 -5 7 1 86.59 29.80 -5 -7 1 53.89 16.40 -5 -7 1 62.99 16.40 -5 -7 1 68.19 12.40 -5 7 -1 81.49 24.80 -5 7 -1 68.49 12.70 5 7 2 12.90 6.70 5 7 2 3.70 3.30 5 7 2 5.20 2.30 5 -7 -2 9.90 6.30 5 -7 -2 10.00 4.00 5 7 -2 10.00 6.70 5 7 -2 5.20 2.20 5 7 -2 9.70 3.80 5 -7 2 2.90 7.70 -5 -7 -2 8.00 5.00 -5 -7 -2 3.30 2.60 -5 -7 -2 3.90 2.70 -5 7 2 3.50 7.60 -5 7 2 12.00 4.60 -5 -7 2 13.10 6.20 -5 -7 2 12.80 4.40 -5 7 -2 7.10 8.40 -5 7 -2 7.10 3.70 5 7 3 5.40 5.50 5 -7 -3 -3.30 8.50 5 -7 -3 75.09 25.90 5 -7 -3 6.60 4.50 5 7 -3 7.90 2.50 5 7 -3 8.70 6.40 5 7 -3 10.40 4.10 5 -7 3 1.70 8.50 5 -7 3 2.10 3.50 -5 -7 -3 4.80 4.40 -5 -7 -3 3.30 2.50 -5 -7 -3 4.90 2.30 -5 7 3 -1.60 3.50 -5 7 3 5.90 7.50 -5 7 3 24.70 9.70 -5 -7 3 5.90 4.70 -5 -7 3 5.50 3.40 -5 -7 3 8.40 2.70 -5 7 -3 -5.80 7.80 -5 7 -3 3.20 3.80 5 7 4 53.79 16.50 5 -7 -4 60.99 11.70 5 -7 -4 53.99 17.50 5 7 -4 46.60 14.60 5 7 -4 60.69 11.20 5 7 -4 44.50 11.90 5 -7 4 42.90 8.90 5 -7 4 69.39 21.90 -5 -7 -4 51.09 15.60 -5 -7 -4 45.00 8.40 -5 7 4 55.89 10.70 -5 7 4 62.09 19.30 -5 7 4 62.69 21.70 -5 -7 4 50.99 15.70 -5 -7 4 44.30 11.70 -5 -7 4 69.19 12.60 5 7 5 168.28 48.70 5 -7 -5 141.09 47.70 5 -7 -5 212.68 61.79 5 7 -5 126.89 42.90 5 7 -5 135.49 34.50 5 7 -5 157.38 45.70 5 7 -5 121.89 21.80 5 -7 5 136.39 24.70 -5 7 5 144.59 26.00 -5 7 5 202.28 58.69 -5 -7 5 174.98 50.59 -5 -7 5 132.59 23.70 -5 -7 5 212.38 53.99 -5 7 -5 160.18 46.70 5 7 6 70.49 18.40 5 7 6 107.69 31.40 5 -7 -6 89.39 30.40 5 -7 -6 99.19 29.40 5 -7 -6 128.39 23.20 5 7 -6 75.99 19.70 5 7 -6 107.19 31.60 5 -7 6 135.99 24.60 -5 -7 -6 78.59 20.10 -5 7 6 116.59 29.70 -5 7 6 96.39 17.70 -5 7 6 98.79 33.60 -5 -7 6 112.39 32.90 -5 -7 6 76.29 19.90 -5 -7 6 143.69 25.70 5 7 7 27.70 8.10 5 7 7 22.00 8.70 5 7 7 19.60 4.40 5 -7 -7 17.00 7.20 5 -7 -7 21.40 5.20 5 -7 -7 27.10 7.80 5 7 -7 25.90 7.60 5 7 -7 17.30 3.80 5 7 -7 29.90 10.90 5 -7 7 22.50 5.50 -5 -7 -7 34.70 11.80 -5 -7 -7 26.10 7.10 -5 7 7 17.90 4.40 -5 7 7 12.10 8.60 -5 7 7 25.30 6.70 -5 -7 7 29.80 10.50 -5 -7 7 25.30 7.40 -5 -7 7 17.60 3.90 -5 7 -7 32.50 12.10 -5 7 -7 13.80 5.20 5 7 8 2.10 3.20 5 7 8 5.00 2.20 5 -7 -8 0.90 6.90 5 -7 -8 3.00 4.10 5 -7 -8 2.80 3.40 5 7 -8 6.50 2.50 5 7 -8 3.00 4.20 5 -7 8 2.50 5.90 5 -7 8 2.60 3.00 -5 -7 -8 -6.70 5.00 -5 -7 -8 1.30 2.20 -5 -7 -8 2.90 2.20 -5 7 8 1.20 2.60 -5 7 8 -3.90 8.00 -5 7 8 17.00 7.50 -5 7 8 2.20 1.80 -5 -7 8 -3.70 5.70 -5 -7 8 1.50 1.70 -5 -7 8 -1.90 3.40 5 7 9 4.30 3.50 5 7 9 3.50 4.70 5 -7 -9 6.70 2.40 5 -7 -9 2.90 2.70 5 -7 -9 -3.30 6.50 5 7 -9 0.70 4.20 5 7 -9 2.30 1.70 -5 -7 -9 1.30 2.20 -5 -7 -9 4.20 2.40 -5 -7 -9 4.00 5.10 -5 7 9 -6.90 8.60 -5 7 9 3.90 2.50 -5 7 9 6.20 5.00 -5 7 9 6.20 2.10 -5 -7 9 0.40 5.70 -5 -7 9 1.90 1.70 -5 7 -9 6.80 8.40 5 7 10 21.30 6.20 5 7 10 12.50 6.10 5 7 10 15.40 3.70 5 -7 -10 73.79 25.50 5 -7 -10 15.60 4.10 5 -7 -10 19.30 4.50 5 7 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11.40 4.50 5 -15 8 -1.20 23.10 -5 -15 -8 13.30 4.40 -5 15 8 -0.20 12.50 -5 15 8 6.10 3.60 -5 15 8 11.30 5.80 -5 15 8 2.90 8.40 -5 -15 8 25.90 5.70 -5 -15 8 23.30 14.40 -5 -15 8 13.60 5.20 -5 -15 8 8.60 5.10 -5 15 -8 33.00 33.10 5 15 9 38.20 10.40 5 -15 -9 58.49 11.80 5 -15 -9 39.90 11.10 5 -15 -9 26.90 10.80 5 15 -9 49.30 9.30 5 15 -9 37.90 11.50 5 15 -9 31.30 12.40 5 -15 9 10.20 22.20 -5 15 9 -5.90 9.50 -5 15 9 40.10 10.70 -5 15 9 46.40 16.50 -5 -15 9 49.90 18.90 -5 -15 9 57.19 19.50 -5 -15 9 34.80 10.10 -5 -15 9 51.29 9.80 -5 15 -9 -33.10 31.60 5 15 10 80.29 20.80 5 -15 -10 95.49 24.60 5 -15 -10 112.79 34.20 5 -15 -10 35.70 8.90 5 15 -10 51.69 9.60 5 15 -10 95.29 25.70 5 15 -10 125.29 37.40 5 15 -10 73.39 24.90 -5 -15 -10 79.49 20.50 -5 15 10 63.89 22.30 -5 15 10 67.49 17.50 -5 -15 10 66.79 12.30 -5 -15 10 56.19 15.30 5 -15 -11 30.10 8.50 5 -15 -11 29.50 8.30 5 15 -11 36.20 13.00 5 15 -11 13.80 3.20 5 15 -11 8.40 3.90 5 -15 11 -7.90 14.30 -5 -15 -11 19.60 5.80 -5 -15 -11 9.50 6.80 -5 15 11 10.20 10.30 -5 15 11 9.30 5.80 -5 15 11 22.70 6.50 -5 -15 11 12.20 3.10 -5 -15 11 29.40 9.20 -5 15 -11 -3.90 22.70 5 -15 -12 14.60 5.10 5 -15 -12 21.40 9.10 5 15 -12 24.90 8.90 5 15 -12 26.00 5.10 5 15 -12 29.00 10.90 5 -15 12 -0.50 10.20 -5 -15 -12 0.30 6.20 -5 15 12 23.60 6.50 -5 15 12 -0.50 12.70 -5 15 12 -4.80 9.20 -5 15 12 39.60 14.40 -5 -15 12 10.40 8.40 -5 -15 12 27.50 5.50 -5 -15 12 12.60 5.90 -5 -15 12 26.50 8.50 5 15 13 0.50 5.10 5 -15 -13 5.10 5.60 5 -15 -13 1.10 3.00 5 -15 -13 2.80 3.60 5 15 -13 1.40 6.80 5 15 -13 2.40 3.60 -5 15 13 -0.80 2.10 -5 15 13 10.90 10.20 -5 15 13 0.70 8.10 -5 15 13 -0.50 4.20 -5 -15 13 -7.00 8.70 -5 -15 13 2.30 3.20 -5 -15 13 3.60 2.10 -5 15 -13 -4.00 16.30 5 -15 -14 3.70 5.30 5 -15 -14 1.80 2.70 5 -15 -14 1.90 3.10 5 15 -14 -0.70 3.00 5 15 -14 2.50 1.80 -5 15 14 -0.10 1.90 -5 15 14 1.30 6.60 -5 -15 14 0.50 7.70 -5 -15 14 -1.20 3.00 -5 15 -14 -17.90 16.40 5 15 15 3.80 4.50 5 15 15 5.40 3.90 5 -15 -15 5.90 2.30 5 -15 -15 2.80 9.10 5 15 -15 6.50 6.50 5 15 -15 2.50 1.90 5 15 -15 -1.80 2.90 -5 15 15 8.00 4.80 -5 15 15 16.70 12.40 -5 15 15 0.70 4.30 -5 15 15 6.10 2.70 -5 -15 15 4.70 6.30 -5 -15 15 3.60 2.00 5 15 16 19.70 6.70 5 15 16 4.90 4.20 5 -15 -16 3.00 4.70 5 -15 -16 59.29 19.50 5 -15 -16 17.00 4.80 5 -15 -16 9.70 3.70 5 15 -16 12.20 3.00 5 15 -16 17.60 8.80 5 15 -16 9.10 4.50 -5 -15 -16 16.40 5.00 -5 -15 -16 -0.80 5.60 -5 15 16 14.00 12.00 -5 15 16 21.20 5.90 -5 15 16 8.50 5.30 -5 15 16 15.10 4.70 -5 -15 16 6.30 7.30 -5 -15 16 16.90 3.80 -5 15 -16 -1.20 13.20 5 15 17 0.40 3.80 5 -15 -17 4.20 4.60 5 -15 -17 -3.30 6.30 5 -15 -17 2.80 2.80 5 -15 -17 4.30 2.20 5 15 -17 5.90 6.30 5 15 -17 6.20 2.10 5 15 -17 8.70 4.20 -5 -15 -17 7.20 3.10 -5 -15 -17 5.50 5.70 -5 15 17 4.70 2.20 -5 -15 17 4.50 6.80 -5 -15 17 5.60 1.90 -5 -15 17 3.60 3.40 -5 -15 17 9.90 5.80 -5 15 -17 3.20 11.90 5 15 18 1.20 4.00 5 15 18 4.40 5.20 5 -15 -18 3.20 5.60 5 -15 -18 4.20 2.00 5 15 -18 4.30 8.50 5 15 -18 5.40 2.10 5 15 -18 3.10 3.10 5 15 -18 2.80 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5.60 -5 -17 3 9.90 4.50 -5 -17 3 4.90 4.80 -5 17 -3 -6.10 30.00 5 17 4 13.60 5.70 5 -17 -4 18.70 6.30 5 -17 -4 17.60 18.50 5 17 -4 -1.60 7.50 5 17 -4 18.10 7.10 5 17 -4 9.00 3.90 5 -17 4 28.70 27.60 5 -17 4 5.70 6.40 -5 -17 -4 5.70 7.60 -5 -17 -4 35.70 9.90 -5 17 4 15.10 6.20 -5 17 4 15.70 30.20 -5 -17 4 14.80 4.80 -5 17 -4 -3.10 32.00 -5 17 -4 28.60 9.00 5 17 5 15.10 5.50 5 -17 -5 38.20 20.10 5 17 -5 15.10 6.40 5 17 -5 14.50 4.50 5 17 -5 -1.00 8.10 5 -17 5 17.00 25.30 -5 -17 -5 -4.20 6.80 -5 -17 -5 20.70 6.30 -5 17 5 22.40 27.70 -5 17 5 26.40 9.70 -5 -17 5 15.20 4.70 -5 17 -5 5.20 29.30 -5 17 -5 25.50 8.30 5 17 6 211.98 53.99 5 -17 -6 215.38 72.59 5 17 -6 241.48 61.69 5 17 -6 202.18 67.79 5 17 -6 262.57 46.90 -5 -17 -6 209.08 53.19 -5 17 6 170.58 43.70 -5 17 6 196.18 65.99 -5 -17 6 221.18 39.60 -5 -17 6 219.88 73.79 -5 17 -6 26.80 27.80 5 17 7 3.70 3.70 5 -17 -7 -1.80 4.00 5 -17 -7 6.40 13.10 5 17 -7 10.30 6.00 5 17 -7 -0.30 7.20 5 17 -7 3.50 2.50 5 17 -7 -0.70 2.60 5 -17 7 9.30 16.70 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6 160.98 29.10 6 -14 -6 171.58 50.49 6 -14 -6 189.08 63.79 6 -14 -6 169.88 43.60 6 14 -6 168.58 43.10 6 14 -6 157.18 28.20 6 14 -6 219.98 63.89 6 14 -6 144.59 48.60 6 -14 6 198.88 60.59 -6 14 6 142.79 27.80 -6 14 6 164.18 49.10 -6 14 6 150.98 50.99 -6 14 6 213.88 54.39 -6 -14 6 247.28 71.69 -6 -14 6 141.69 25.50 -6 -14 6 170.78 57.39 6 14 7 74.99 19.50 6 14 7 93.79 28.40 6 -14 -7 69.79 18.60 6 -14 -7 58.89 11.50 6 -14 -7 91.09 28.30 6 -14 -7 85.49 29.30 6 14 -7 63.39 17.00 6 14 -7 59.99 11.20 6 14 -7 62.99 21.50 6 -14 7 143.19 45.80 -6 -14 -7 67.99 13.70 -6 -14 -7 108.39 32.70 -6 -14 -7 90.49 23.40 -6 14 7 109.29 34.00 -6 -14 7 97.19 29.60 -6 -14 7 68.99 12.80 -6 -14 7 62.39 21.20 -6 14 -7 14.00 25.80 6 14 8 7.80 4.20 6 14 8 14.30 9.00 6 -14 -8 15.30 7.10 6 -14 -8 2.00 8.60 6 -14 -8 4.70 3.70 6 14 -8 10.90 3.20 6 14 -8 7.60 5.40 6 14 -8 19.10 9.10 6 14 -8 16.40 6.10 6 -14 8 -20.20 19.70 -6 -14 -8 13.00 7.80 -6 -14 -8 17.30 6.80 -6 -14 -8 7.90 3.60 -6 14 8 12.20 6.30 -6 -14 8 18.30 9.70 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8 -6 -6 50.09 17.70 8 6 -6 41.70 14.90 8 6 -6 38.90 10.50 8 6 -6 66.39 22.90 8 6 -6 39.40 7.40 8 -6 6 37.80 7.50 8 -6 6 33.10 11.90 -8 -6 -6 41.10 11.00 -8 -6 -6 43.00 8.10 -8 6 6 20.10 13.00 -8 6 6 46.00 16.30 -8 -6 6 41.20 15.60 -8 -6 6 49.30 9.30 -8 -6 6 58.09 20.30 -8 6 -6 58.19 19.20 -8 6 -6 55.99 10.40 8 6 7 19.00 6.40 8 6 7 40.20 13.30 8 6 7 24.30 4.80 8 -6 -7 20.40 4.40 8 -6 -7 29.80 13.30 8 -6 -7 53.79 18.80 8 6 -7 27.90 7.90 8 6 -7 44.30 15.70 8 6 -7 35.80 7.10 8 6 -7 34.50 12.50 8 -6 7 27.10 5.50 8 -6 7 49.50 16.10 -8 -6 -7 23.30 4.80 -8 -6 -7 26.30 7.40 -8 6 7 4.30 12.20 -8 6 7 55.39 19.40 -8 6 7 25.50 5.30 -8 -6 7 53.49 18.30 -8 -6 7 31.20 6.20 -8 6 -7 36.80 14.00 -8 6 -7 33.40 6.50 8 6 8 115.49 33.90 8 6 8 95.09 17.10 8 -6 -8 112.09 38.10 8 -6 -8 128.49 38.50 8 6 -8 125.49 37.60 8 6 -8 86.09 29.30 8 6 -8 113.79 20.50 8 -6 8 71.59 13.10 -8 -6 -8 92.69 23.80 -8 -6 -8 106.59 19.10 -8 6 8 98.59 17.80 -8 6 8 71.89 24.70 -8 6 8 291.17 73.89 -8 6 8 124.09 42.20 -8 -6 8 109.29 37.10 -8 -6 8 186.28 54.59 -8 -6 8 118.09 30.30 -8 -6 8 96.79 17.50 -8 6 -8 165.18 49.00 -8 6 -8 96.69 17.40 8 6 9 10.80 6.80 8 6 9 14.60 3.30 8 -6 -9 3.80 5.90 8 -6 -9 24.10 11.70 8 -6 -9 9.40 3.10 8 6 -9 13.50 4.90 8 6 -9 19.30 4.20 8 6 -9 29.40 12.90 8 -6 9 13.00 3.50 8 -6 9 2.30 7.30 -8 -6 -9 8.50 2.70 -8 -6 -9 27.20 10.90 -8 6 9 11.60 3.10 -8 6 9 17.00 15.80 -8 6 9 14.60 6.90 -8 6 9 11.00 5.00 -8 -6 9 7.50 9.80 -8 -6 9 20.30 4.60 -8 -6 9 18.80 7.70 -8 -6 9 9.10 4.10 -8 6 -9 15.30 11.60 -8 6 -9 13.90 3.60 8 6 10 184.38 32.80 8 -6 -10 256.07 74.29 8 -6 -10 171.78 30.70 8 6 -10 307.07 88.99 8 6 -10 142.39 48.10 8 6 -10 153.78 27.50 8 6 -10 168.58 43.00 8 -6 10 329.57 95.09 8 -6 10 204.98 36.50 -8 -6 -10 171.28 30.50 -8 -6 -10 363.56 104.69 -8 6 10 401.16 116.19 -8 6 10 185.98 33.20 -8 6 10 269.17 90.59 -8 6 10 492.25 124.49 -8 -6 10 160.08 28.60 -8 6 -10 176.28 31.40 8 6 11 6.50 2.20 8 -6 -11 3.20 4.50 8 -6 -11 2.80 8.60 8 -6 -11 0.90 3.80 8 -6 -11 2.20 2.20 8 6 -11 10.00 5.10 8 6 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18.90 -8 8 -2 46.80 8.80 8 8 3 21.10 9.50 8 -8 -3 19.90 8.60 8 -8 -3 -2.90 7.10 8 -8 -3 2.80 3.10 8 8 -3 3.10 3.50 8 8 -3 -0.40 2.60 8 8 -3 24.60 10.90 8 -8 3 5.00 6.50 -8 -8 -3 1.60 2.20 -8 8 3 11.20 6.50 -8 -8 3 14.40 9.10 -8 -8 3 0.30 2.00 -8 -8 3 1.10 2.80 -8 8 -3 3.80 9.30 -8 8 -3 3.70 2.90 8 8 4 122.49 36.10 8 -8 -4 160.08 47.00 8 -8 -4 157.28 28.20 8 -8 -4 117.69 40.00 8 8 -4 140.39 25.20 8 8 -4 158.68 46.60 8 -8 4 169.58 49.50 8 -8 4 183.78 32.90 -8 -8 -4 131.89 23.70 -8 8 4 152.68 51.69 -8 8 4 222.48 65.19 -8 8 4 136.89 24.60 -8 -8 4 129.59 38.30 -8 -8 4 112.89 28.80 -8 8 -4 145.79 26.10 8 8 5 47.90 15.50 8 8 5 78.79 20.50 8 8 5 83.19 15.10 8 8 -5 56.99 18.80 8 8 -5 79.69 14.50 8 8 -5 62.49 16.20 8 8 -5 58.79 20.30 8 -8 5 84.69 25.80 -8 -8 -5 91.79 16.60 -8 8 5 61.49 21.70 -8 8 5 76.69 14.00 -8 8 5 50.79 17.90 -8 -8 5 34.40 12.50 -8 -8 5 63.39 22.00 -8 -8 5 67.59 12.40 -8 8 -5 46.40 15.90 8 8 6 1062.39 268.77 8 8 6 814.02 233.38 8 8 6 1060.49 187.68 8 -8 -6 932.71 165.18 8 8 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8 25.80 5.20 -8 8 -8 21.50 5.00 8 8 9 0.60 4.00 8 8 9 10.50 6.80 8 -8 -9 8.70 5.20 8 -8 -9 5.60 2.90 8 -8 -9 -11.60 10.40 8 8 -9 15.80 10.50 8 8 -9 10.30 4.80 8 8 -9 3.70 3.90 8 -8 9 1.20 2.20 -8 -8 -9 4.50 2.80 -8 -8 -9 8.10 2.90 -8 8 9 6.20 2.60 -8 8 9 -5.00 11.20 -8 8 9 8.30 5.30 -8 -8 9 10.60 8.90 -8 -8 9 9.30 4.90 -8 -8 9 5.20 2.20 -8 -8 9 11.00 4.70 -8 8 -9 10.80 11.20 -8 8 -9 3.70 2.20 8 8 10 92.69 24.30 8 8 10 48.20 15.50 8 8 10 44.10 8.10 8 -8 -10 53.39 18.60 8 8 -10 75.69 20.20 8 8 -10 48.50 9.00 8 8 -10 41.60 15.40 8 -8 10 37.70 14.20 -8 -8 -10 24.70 10.90 -8 -8 -10 52.59 13.80 -8 -8 -10 52.29 9.60 -8 8 10 48.80 9.20 -8 8 10 16.10 11.70 -8 8 10 53.79 19.00 -8 -8 10 45.20 15.30 -8 -8 10 36.20 13.00 -8 -8 10 53.59 10.00 -8 8 -10 79.59 25.80 -8 8 -10 49.40 9.30 8 8 11 4.00 4.10 8 8 11 12.70 2.90 8 -8 -11 13.10 9.00 8 -8 -11 0.90 2.90 8 8 -11 12.70 6.00 8 8 -11 5.20 4.80 8 8 -11 2.70 2.20 8 8 -11 38.50 13.70 8 -8 11 3.80 8.40 8 -8 11 0.30 2.70 -8 -8 -11 2.30 2.40 -8 -8 -11 2.60 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12.10 6.10 8 -8 14 7.60 3.20 8 -8 14 13.70 8.20 -8 -8 -14 5.20 5.80 -8 -8 -14 4.00 1.80 -8 8 14 11.50 3.30 -8 8 14 5.40 8.10 -8 8 14 4.90 5.10 -8 -8 14 7.40 5.60 -8 -8 14 9.30 5.70 -8 -8 14 8.50 2.80 -8 8 -14 10.40 10.10 -8 8 -14 5.80 3.20 8 8 15 7.70 4.80 8 8 15 3.60 1.90 8 -8 -15 0.70 5.50 8 -8 -15 8.00 2.70 8 -8 -15 3.00 4.60 8 8 -15 6.20 2.20 8 8 -15 0.30 5.60 8 8 -15 2.90 7.20 8 -8 15 6.80 7.30 8 -8 15 2.70 2.50 -8 -8 -15 3.40 1.90 -8 -8 -15 0.60 5.40 -8 8 15 5.00 8.70 -8 8 15 7.00 2.50 -8 -8 15 2.80 4.00 -8 -8 15 2.80 5.50 -8 -8 15 0.70 4.00 -8 8 -15 2.40 3.70 8 8 16 67.29 20.00 8 8 16 114.79 20.60 8 -8 -16 85.29 29.70 8 -8 -16 82.49 24.90 8 8 -16 48.40 14.20 8 8 -16 35.60 12.80 8 8 -16 99.09 17.80 8 -8 16 56.99 18.20 8 -8 16 129.99 23.40 -8 -8 -16 70.49 12.80 -8 8 16 43.30 15.90 -8 8 16 107.59 19.40 -8 -8 16 45.00 14.30 -8 -8 16 103.69 18.60 -8 -8 16 41.90 15.00 -8 -8 16 80.79 21.10 8 8 17 6.20 4.20 8 8 17 2.20 1.60 8 -8 -17 6.00 4.40 8 -8 -17 -2.10 2.50 8 -8 -17 4.50 6.80 8 -8 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5 10.40 5.70 -8 -12 5 3.50 7.40 -8 -12 5 3.20 3.20 -8 12 -5 10.70 11.70 -8 12 -5 -0.30 7.50 8 12 6 24.20 9.50 8 -12 -6 9.80 6.10 8 -12 -6 12.20 10.30 8 -12 -6 2.90 2.90 8 12 -6 19.80 7.40 8 12 -6 23.30 9.40 8 12 -6 13.90 5.40 8 12 -6 9.00 3.10 8 -12 6 3.20 4.70 8 -12 6 -5.60 9.80 -8 -12 -6 14.20 7.80 -8 12 6 18.30 11.40 -8 12 6 6.50 3.30 -8 12 6 10.60 5.70 -8 -12 6 10.60 4.20 -8 -12 6 7.40 8.60 -8 -12 6 12.60 3.40 -8 -12 6 21.80 8.60 -8 12 -6 5.10 11.80 -8 12 -6 11.60 8.40 8 12 7 4.30 6.10 8 12 7 3.90 2.40 8 -12 -7 6.90 5.10 8 -12 -7 5.30 3.40 8 12 -7 4.20 3.70 8 12 -7 7.10 4.20 8 12 -7 2.70 2.20 8 12 -7 -2.60 6.60 8 -12 7 -0.50 9.70 8 -12 7 1.50 5.60 -8 -12 -7 0.10 2.30 -8 12 7 3.70 4.60 -8 12 7 6.70 9.40 -8 12 7 0.90 2.60 -8 -12 7 3.40 2.40 -8 -12 7 -2.90 7.60 -8 -12 7 8.40 4.80 -8 -12 7 1.70 2.90 8 12 8 -0.60 6.50 8 -12 -8 3.30 4.30 8 -12 -8 8.80 8.80 8 -12 -8 10.30 3.80 8 12 -8 2.60 2.10 8 12 -8 1.10 3.40 8 12 -8 4.50 6.80 8 -12 8 -10.40 8.60 8 -12 8 -1.50 4.30 -8 12 8 5.30 8.90 -8 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41.20 9.10 8 -16 1 66.89 22.70 -8 -16 -1 6.00 5.80 -8 -16 -1 16.50 5.00 -8 16 1 14.50 6.90 -8 -16 1 7.30 6.10 -8 -16 1 28.10 7.90 -8 16 -1 8.40 13.80 -8 16 -1 51.79 18.30 8 16 2 1.20 4.80 8 -16 -2 1.20 4.50 8 -16 -2 -9.60 9.70 8 16 -2 -3.90 6.00 8 16 -2 45.60 12.40 8 16 -2 2.10 2.50 8 -16 2 -4.10 9.90 8 -16 2 0.70 4.00 -8 -16 -2 -2.90 5.10 -8 -16 -2 3.30 3.20 -8 16 2 3.10 9.40 -8 -16 2 5.20 5.40 -8 -16 2 1.20 2.60 -8 -16 2 43.90 11.70 -8 16 -2 -2.40 7.40 8 16 3 3.30 4.30 8 16 3 4.80 3.40 8 16 3 5.00 2.50 8 -16 -3 -1.70 4.60 8 -16 -3 2.90 3.60 8 -16 -3 -5.30 9.60 8 16 -3 1.70 2.10 8 16 -3 -5.50 5.70 8 16 -3 3.70 3.70 8 -16 3 -4.80 10.80 -8 -16 -3 2.60 2.50 -8 -16 -3 1.60 2.60 -8 -16 -3 0.80 4.90 -8 16 3 -7.00 11.20 -8 16 3 1.30 7.90 -8 -16 3 0.70 4.80 -8 -16 3 2.10 2.60 -8 -16 3 2.60 2.70 -8 16 -3 4.30 13.60 -8 16 -3 -0.30 6.70 8 16 4 -0.50 2.80 8 16 4 3.10 5.30 8 -16 -4 6.10 4.80 8 -16 -4 -1.90 8.30 8 -16 -4 -0.30 3.10 8 16 -4 3.60 5.50 8 16 -4 -0.80 3.40 8 16 -4 1.00 2.10 8 -16 4 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44.20 8.40 10 -8 -4 16.80 7.60 10 8 -4 40.80 11.00 10 8 -4 28.90 5.80 10 8 -4 35.50 13.60 10 -8 4 29.20 12.50 10 -8 4 34.20 6.90 -10 -8 -4 26.50 5.40 -10 -8 -4 31.10 11.40 -10 -8 4 45.60 15.70 -10 -8 4 46.40 12.20 -10 -8 4 33.50 6.60 -10 8 -4 51.99 19.00 -10 8 -4 35.70 6.90 10 8 5 29.70 11.20 10 8 5 15.10 6.40 10 8 5 14.20 3.30 10 -8 -5 14.80 7.20 10 -8 -5 -1.60 6.80 10 -8 -5 9.90 3.20 10 8 -5 34.60 9.50 10 8 -5 12.90 3.20 10 8 -5 29.30 11.90 10 -8 5 10.90 8.10 10 -8 5 10.80 3.70 -10 -8 -5 17.20 8.80 -10 -8 -5 21.10 6.20 -10 8 5 14.30 9.80 -10 8 5 18.60 4.20 -10 -8 5 32.10 12.30 -10 -8 5 9.60 3.10 -10 -8 5 7.70 5.70 -10 8 -5 16.40 11.80 10 8 6 164.58 29.50 10 -8 -6 181.28 61.29 10 8 -6 161.08 28.80 10 8 -6 167.98 56.69 10 8 -6 190.48 48.40 10 8 -6 228.08 66.49 10 -8 6 176.88 31.60 10 -8 6 227.88 66.19 -10 -8 -6 132.59 33.90 -10 -8 -6 238.38 69.09 -10 8 6 185.18 33.10 -10 8 6 229.68 66.79 -10 -8 6 159.58 53.99 -10 -8 6 205.78 60.09 -10 -8 6 175.78 44.70 -10 -8 6 188.58 33.70 -10 8 -6 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6.30 -11 -1 -5 50.59 13.70 -11 1 5 24.90 5.10 -11 1 5 31.70 13.20 -11 1 5 37.60 10.00 -11 1 5 21.70 8.90 -11 -1 5 32.60 12.40 -11 -1 5 39.10 14.90 -11 -1 5 27.80 5.50 -11 1 -5 35.00 14.00 -11 1 -5 42.90 13.50 11 1 6 18.10 7.60 11 1 6 40.60 13.30 11 1 6 15.00 3.20 11 -1 -6 21.30 8.70 11 -1 -6 49.30 16.90 11 -1 -6 11.60 5.20 11 -1 -6 13.60 3.50 11 1 -6 16.10 3.60 11 1 -6 22.30 9.70 11 -1 6 15.00 3.20 11 -1 6 20.30 8.60 -11 -1 -6 18.90 6.90 -11 -1 -6 21.50 10.20 -11 -1 -6 12.50 2.80 -11 1 6 14.40 7.60 -11 1 6 20.60 9.90 -11 1 6 13.40 3.30 -11 -1 6 24.40 9.70 -11 -1 6 14.30 9.10 -11 -1 6 14.30 3.30 -11 1 -6 11.20 9.60 -11 1 -6 34.00 12.00 -11 1 -6 13.50 3.00 11 1 7 45.50 15.50 11 1 7 14.30 3.10 11 -1 -7 8.80 5.20 11 -1 -7 8.80 8.20 11 -1 -7 9.80 4.70 11 -1 -7 13.20 3.50 11 1 -7 16.30 8.30 11 1 -7 13.10 3.30 11 -1 7 16.40 3.40 11 -1 7 7.50 7.50 11 -1 7 14.70 7.70 -11 -1 -7 -0.60 5.90 -11 -1 -7 14.20 3.10 -11 -1 -7 19.20 9.10 -11 1 7 7.80 7.10 -11 1 7 11.10 3.50 -11 1 7 14.90 3.50 -11 -1 7 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2.50 9.10 11 -5 8 4.30 1.70 11 -5 8 10.00 8.90 -11 -5 -8 12.30 6.90 -11 -5 -8 2.40 1.70 -11 5 8 18.00 8.10 -11 5 8 10.70 5.80 -11 5 8 6.60 2.50 -11 -5 8 7.60 6.40 -11 -5 8 8.60 3.20 -11 5 -8 -4.70 8.70 -11 5 -8 0.30 13.60 -11 5 -8 5.80 1.90 11 5 9 39.80 12.90 11 5 9 42.20 7.90 11 -5 -9 20.30 8.10 11 -5 -9 12.00 8.20 11 -5 -9 8.00 4.70 11 5 -9 28.50 10.50 11 -5 9 39.50 14.20 11 -5 9 29.00 5.50 11 -5 9 5.80 7.70 -11 -5 -9 29.40 5.60 -11 -5 -9 26.40 9.90 -11 5 9 18.30 8.10 -11 5 9 21.80 8.70 -11 5 9 29.80 5.80 -11 -5 9 12.50 7.20 -11 -5 9 23.40 6.40 -11 5 -9 -0.40 15.70 -11 5 -9 35.50 6.60 11 5 10 13.30 6.90 11 5 10 6.20 1.90 11 -5 -10 8.60 5.20 11 5 -10 11.20 5.10 11 5 -10 7.30 3.30 11 5 -10 27.00 10.20 11 -5 10 7.40 2.10 11 -5 10 10.70 8.80 -11 -5 -10 7.90 2.00 -11 5 10 7.70 2.70 -11 5 10 9.60 5.30 -11 -5 10 13.00 3.10 -11 -5 10 27.10 10.20 -11 5 -10 0.60 8.20 -11 5 -10 8.60 2.20 -11 5 -10 -11.20 13.10 11 5 11 47.60 15.30 11 5 11 18.60 4.00 11 -5 -11 38.30 13.70 11 5 -11 29.60 10.60 11 5 -11 21.40 4.90 11 -5 11 16.40 9.60 11 -5 11 20.90 4.10 -11 -5 -11 27.10 5.20 -11 -5 -11 39.80 13.20 -11 5 11 27.20 10.20 -11 5 11 23.30 4.70 -11 5 11 26.30 6.90 -11 -5 11 28.00 5.60 -11 -5 11 21.00 8.80 -11 -5 11 29.30 8.10 -11 5 -11 30.50 5.80 -11 5 -11 -1.00 13.30 11 5 12 4.40 5.30 11 5 12 -3.20 4.40 11 5 12 2.60 1.60 11 -5 -12 0.60 2.20 11 -5 -12 -0.60 7.50 11 -5 -12 0.00 1.70 11 5 -12 2.70 3.30 11 5 -12 6.30 2.40 11 5 -12 5.30 5.70 11 -5 12 3.50 1.60 -11 -5 -12 3.10 6.60 -11 -5 -12 0.90 1.40 -11 5 12 1.50 1.60 -11 -5 12 6.30 2.50 -11 -5 12 2.90 2.50 -11 5 -12 -0.40 14.90 -11 5 -12 2.10 1.60 11 5 13 8.10 6.70 11 5 13 2.90 4.90 11 5 13 1.10 1.40 11 -5 -13 -1.00 1.60 11 -5 -13 2.10 2.00 11 -5 -13 -3.70 7.10 11 5 -13 0.50 1.70 11 5 -13 0.40 3.30 11 5 -13 -2.00 5.80 11 -5 13 2.70 6.80 11 -5 13 1.30 1.50 -11 -5 -13 1.30 1.20 -11 5 13 -0.70 6.00 -11 5 13 1.10 1.50 -11 5 -13 -6.50 9.60 -11 5 -13 0.60 1.20 -11 5 -13 4.80 14.30 11 5 14 -1.30 6.30 11 5 14 1.30 1.50 11 -5 -14 0.70 6.70 11 -5 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3.30 1.40 11 5 17 3.90 6.40 11 5 17 5.60 1.70 11 -5 -17 5.70 2.10 11 5 -17 5.40 6.70 11 5 -17 7.50 2.30 11 -5 17 -4.30 5.90 11 -5 17 5.50 1.70 -11 -5 -17 10.50 2.40 -11 5 17 3.20 2.60 -11 5 17 4.70 1.90 -11 -5 17 6.60 2.10 -11 -5 17 -1.50 3.90 -11 5 -17 3.70 1.40 11 7 0 5.60 6.60 11 -7 0 3.40 7.30 -11 -7 0 5.30 2.00 -11 -7 0 0.70 6.40 -11 7 0 10.20 2.80 -11 7 0 -6.00 10.10 11 7 1 14.20 7.10 11 7 1 12.00 2.90 11 -7 -1 27.00 11.00 11 -7 -1 15.50 3.60 11 7 -1 7.30 2.30 11 7 -1 10.50 7.00 11 -7 1 10.60 2.90 11 -7 1 6.60 7.70 -11 -7 -1 11.10 2.80 -11 -7 -1 37.90 13.10 -11 7 1 1.70 8.70 -11 7 1 -7.50 12.60 -11 7 1 10.90 2.80 -11 -7 1 21.20 9.30 -11 -7 1 17.50 4.00 -11 7 -1 -3.80 8.30 -11 7 -1 12.80 3.30 11 7 2 3.30 5.70 11 7 2 1.80 4.00 11 7 2 0.00 1.60 11 -7 -2 -1.60 6.70 11 -7 -2 0.20 2.00 11 7 -2 3.30 1.90 11 7 -2 -4.00 6.20 11 -7 2 2.40 1.80 -11 -7 -2 2.60 1.80 -11 7 2 -0.30 1.70 -11 7 2 2.70 8.70 -11 7 2 10.00 17.00 -11 7 2 -0.10 5.20 -11 -7 2 7.70 7.90 -11 -7 2 3.00 2.10 -11 -7 2 4.50 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82.09 14.90 -11 -9 0 97.09 24.90 11 9 1 16.20 7.60 11 -9 -1 -1.20 7.90 11 9 -1 9.90 4.10 11 9 -1 24.80 9.90 11 -9 1 0.70 10.00 11 -9 1 7.20 2.80 -11 -9 -1 8.40 2.40 -11 -9 -1 20.00 8.60 -11 9 1 15.70 3.70 -11 9 1 18.00 8.70 -11 9 1 0.60 11.90 -11 -9 1 30.30 11.20 -11 -9 1 11.50 3.80 -11 9 -1 7.00 2.50 11 9 2 -4.30 5.40 11 9 2 0.20 1.60 11 -9 -2 -16.60 8.80 11 -9 -2 2.90 3.50 11 -9 -2 0.30 2.40 11 9 -2 -1.00 2.80 11 9 -2 1.60 1.70 11 9 -2 0.10 5.70 11 -9 2 3.20 2.50 -11 -9 -2 5.50 5.90 -11 9 2 -5.00 10.10 -11 9 2 0.30 1.80 -11 -9 2 6.10 6.60 -11 -9 2 5.60 2.60 -11 9 -2 -8.40 10.70 -11 9 -2 1.50 1.90 11 9 3 -5.50 5.60 11 9 3 2.10 1.90 11 -9 -3 -1.00 3.40 11 -9 -3 0.00 2.30 11 9 -3 -1.40 2.60 11 9 -3 4.50 2.00 11 9 -3 3.10 6.00 11 -9 3 -2.80 7.80 -11 -9 -3 1.10 1.70 -11 -9 -3 2.10 6.60 -11 9 3 -0.90 5.00 -11 9 3 0.60 9.50 -11 9 3 0.10 1.80 -11 -9 3 -0.40 1.80 -11 -9 3 2.30 6.60 -11 -9 3 3.50 1.90 -11 9 -3 -0.40 10.20 -11 9 -3 2.40 2.00 11 9 4 0.70 3.70 11 9 4 -1.50 5.00 11 -9 -4 1.60 4.70 11 -9 -4 1.50 6.30 11 -9 -4 3.40 2.20 11 9 -4 3.80 2.70 11 9 -4 2.70 2.00 11 9 -4 3.60 6.20 11 -9 4 4.60 7.80 -11 -9 -4 2.60 1.80 -11 9 4 6.10 8.40 -11 9 4 3.80 4.40 -11 9 4 2.10 1.90 -11 -9 4 0.40 1.70 -11 -9 4 4.00 2.40 -11 -9 4 -3.30 6.50 -11 9 -4 -5.80 10.60 -11 9 -4 2.90 2.10 11 9 5 1.30 4.80 11 9 5 -2.10 5.20 11 -9 -5 -2.40 7.30 11 -9 -5 2.20 2.30 11 9 -5 11.30 4.20 11 9 -5 -2.10 6.10 11 -9 5 4.20 7.10 11 -9 5 2.40 2.60 -11 -9 -5 2.50 2.70 -11 9 5 5.80 2.50 -11 9 5 17.50 7.90 -11 -9 5 9.20 6.90 -11 -9 5 10.20 2.90 -11 9 -5 19.10 12.30 11 9 6 11.90 5.90 11 9 6 10.40 6.20 11 9 6 3.50 1.90 11 -9 -6 10.80 5.60 11 -9 -6 -11.20 7.70 11 -9 -6 15.70 3.80 11 9 -6 12.40 4.70 11 9 -6 7.30 6.90 11 9 -6 9.80 2.70 11 -9 6 11.10 3.20 11 -9 6 9.60 7.80 -11 -9 -6 6.70 2.40 -11 -9 -6 18.90 5.60 -11 9 6 0.80 8.20 -11 9 6 15.50 7.30 -11 -9 6 8.90 6.70 -11 -9 6 9.20 3.80 -11 -9 6 9.00 6.00 11 9 7 7.30 5.80 11 9 7 13.60 6.20 11 9 7 4.70 1.80 11 -9 -7 -2.60 7.90 11 -9 -7 6.50 2.70 11 9 -7 9.20 2.60 11 9 -7 10.00 4.20 11 9 -7 4.90 6.80 11 -9 7 2.40 2.40 -11 -9 -7 4.20 2.60 -11 9 7 6.90 9.10 -11 9 7 7.50 2.50 -11 -9 7 4.40 5.70 -11 -9 7 8.30 2.40 -11 9 -7 13.20 11.60 -11 9 -7 6.90 2.40 11 9 8 2.20 4.80 11 9 8 3.00 5.90 11 -9 -8 -1.90 6.20 11 9 -8 7.60 3.70 11 9 -8 4.60 2.10 11 9 -8 -0.40 6.70 11 -9 8 0.60 6.80 11 -9 8 0.90 2.50 -11 9 8 1.80 8.30 -11 9 8 7.50 2.40 -11 -9 8 2.70 5.60 -11 -9 8 5.80 2.20 -11 9 -8 15.20 11.50 -11 9 -8 5.40 2.50 11 9 9 -0.30 4.70 11 9 9 3.80 7.10 11 9 9 0.70 1.40 11 -9 -9 -0.30 2.10 11 9 -9 5.50 3.60 11 9 -9 -1.60 7.10 11 -9 9 0.40 6.40 11 -9 9 1.40 2.70 -11 -9 -9 3.40 1.90 -11 -9 -9 0.70 2.30 -11 9 9 -4.50 8.40 -11 9 9 0.20 1.70 -11 -9 9 3.00 6.00 -11 -9 9 -0.30 1.70 -11 -9 9 2.40 2.70 -11 9 -9 -10.50 9.80 -11 9 -9 1.00 2.20 11 9 10 14.70 7.30 11 9 10 14.70 3.20 11 -9 -10 10.80 7.40 11 -9 -10 16.10 3.70 11 9 -10 15.40 5.40 11 9 -10 16.90 9.30 11 9 -10 17.60 3.80 11 -9 10 14.00 3.50 11 -9 10 26.50 11.80 -11 -9 -10 30.70 8.80 -11 -9 -10 16.00 3.50 -11 9 10 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1.80 13 1 -2 3.60 4.90 13 1 -2 0.20 1.60 13 -1 2 2.30 7.50 13 -1 2 1.50 1.70 13 -1 2 -3.60 6.30 -13 -1 -2 1.10 8.10 -13 1 2 -3.60 6.10 -13 1 2 0.90 1.60 -13 -1 2 0.90 1.60 -13 -1 2 2.50 8.30 -13 -1 2 1.60 2.80 -13 1 -2 3.50 7.70 -13 1 -2 0.70 1.60 13 1 3 4.50 6.20 13 -1 -3 -3.30 6.60 13 -1 -3 0.00 1.70 13 1 -3 0.30 1.60 13 1 -3 6.10 7.30 13 -1 3 1.00 8.20 13 -1 3 -3.30 6.60 -13 -1 -3 0.70 7.90 -13 -1 -3 0.20 1.90 -13 1 3 1.00 1.60 -13 -1 3 -4.70 8.10 -13 -1 3 -0.60 2.70 -13 -1 3 1.20 1.60 -13 1 -3 -4.90 7.70 -13 1 -3 1.30 1.70 13 1 4 9.50 6.80 13 1 4 -1.60 4.90 13 1 4 9.20 2.60 13 -1 -4 13.20 8.40 13 -1 -4 5.30 2.10 13 1 -4 1.80 5.10 13 1 -4 4.50 2.00 13 1 -4 8.00 7.40 13 -1 4 0.20 7.20 13 -1 4 5.10 1.90 13 -1 4 8.10 7.30 -13 -1 -4 13.20 9.40 -13 -1 -4 9.60 2.60 -13 1 4 3.60 1.80 -13 1 4 4.50 3.40 -13 1 4 -1.50 7.70 -13 -1 4 4.10 1.90 -13 -1 4 9.80 4.10 -13 1 -4 5.00 8.00 -13 1 -4 3.60 1.90 13 1 5 5.50 6.20 13 1 5 10.30 2.60 13 -1 -5 7.70 8.20 13 -1 -5 11.50 3.00 13 1 -5 16.60 7.00 13 1 -5 16.60 3.70 13 1 -5 17.70 9.50 13 -1 5 16.70 8.40 13 -1 5 15.80 3.50 13 -1 5 -2.20 7.60 -13 1 5 12.20 2.90 -13 1 5 10.20 8.30 -13 1 5 14.30 4.80 -13 -1 5 16.10 3.50 -13 -1 5 13.20 5.00 13 1 6 7.30 6.80 13 1 6 9.50 2.40 13 -1 -6 13.80 6.70 13 -1 -6 10.40 8.20 13 -1 -6 10.00 2.80 13 1 -6 9.60 8.20 13 1 -6 6.90 4.70 13 1 -6 12.00 3.10 13 -1 6 3.70 6.30 13 -1 6 9.60 2.60 13 -1 6 19.90 9.50 -13 -1 -6 12.40 10.10 -13 -1 -6 10.90 3.00 -13 1 6 1.80 7.90 -13 1 6 25.00 7.20 -13 1 6 10.80 2.70 -13 -1 6 12.10 2.90 -13 -1 6 4.30 8.80 -13 1 -6 9.70 2.80 13 1 7 9.50 8.00 13 1 7 9.10 2.40 13 -1 -7 2.20 4.40 13 -1 -7 9.60 8.20 13 -1 -7 11.40 3.00 13 1 -7 8.20 8.40 13 1 -7 8.80 4.30 13 1 -7 14.50 3.50 13 -1 7 1.20 7.20 13 -1 7 10.20 2.80 -13 -1 -7 9.80 9.10 -13 -1 -7 13.40 3.20 -13 1 7 0.90 8.40 -13 1 7 10.40 2.70 -13 1 7 11.70 4.10 -13 -1 7 13.20 3.00 -13 1 -7 5.20 9.20 -13 1 -7 7.50 2.50 13 1 8 2.40 7.20 13 1 8 1.60 6.30 13 1 8 6.90 2.10 13 -1 -8 5.70 2.40 13 -1 -8 2.50 4.10 13 -1 -8 11.80 8.20 13 1 -8 6.00 2.40 13 1 -8 3.90 8.20 13 -1 8 5.90 7.00 13 -1 8 -1.70 6.00 13 -1 8 8.20 2.60 -13 -1 -8 5.90 2.00 -13 1 8 3.30 2.40 -13 1 8 6.20 2.20 -13 -1 8 6.10 2.10 -13 1 -8 6.30 2.50 13 1 9 -7.10 7.30 13 1 9 0.60 1.50 13 -1 -9 -0.40 7.20 13 -1 -9 -1.10 2.10 13 1 -9 2.90 8.40 13 -1 9 1.80 1.90 13 -1 9 1.90 7.20 13 -1 9 -2.80 7.20 -13 -1 -9 0.80 1.60 -13 1 9 2.50 1.90 -13 -1 9 1.30 1.70 13 3 0 8.80 6.30 13 3 0 2.70 5.80 13 3 0 0.60 1.90 13 -3 0 4.30 7.80 13 -3 0 2.40 1.70 -13 -3 0 -2.60 7.00 -13 3 0 5.60 9.00 -13 3 0 1.70 1.40 13 3 1 1.80 5.00 13 3 1 4.40 6.10 13 -3 -1 0.70 1.50 13 -3 -1 -1.50 8.30 13 -3 -1 -2.70 5.30 13 3 -1 -0.30 1.80 13 3 -1 2.90 4.70 13 3 -1 11.70 7.20 13 -3 1 1.00 6.30 13 -3 1 5.20 7.70 13 -3 1 0.30 1.50 -13 -3 -1 1.30 1.80 -13 -3 -1 10.00 8.00 -13 3 1 -4.70 8.60 -13 3 1 0.50 1.40 -13 3 1 4.20 5.00 -13 -3 1 2.40 8.00 -13 -3 1 0.80 1.70 -13 3 -1 -4.20 8.30 -13 3 -1 -0.20 1.40 -13 3 -1 1.10 5.70 13 3 2 -0.50 5.40 13 3 2 -0.80 2.00 13 -3 -2 4.10 6.70 13 -3 -2 0.50 1.50 13 -3 -2 -1.90 8.90 13 3 -2 -0.70 1.80 13 3 -2 -0.80 4.40 13 3 -2 2.60 5.70 13 -3 2 2.70 6.10 13 -3 2 -5.40 7.50 13 -3 2 0.50 1.50 -13 -3 -2 1.50 1.70 -13 -3 -2 -8.70 7.60 -13 3 2 -0.40 1.30 -13 3 2 0.70 3.70 -13 -3 2 -4.10 7.80 -13 -3 2 -0.70 1.50 -13 3 -2 2.90 8.20 -13 3 -2 -0.70 1.40 13 3 3 8.50 6.60 13 -3 -3 3.50 6.80 13 -3 -3 6.00 6.80 13 -3 -3 5.00 1.90 13 3 -3 5.30 2.10 13 3 -3 3.40 4.20 13 -3 3 9.80 7.50 13 -3 3 3.90 6.90 -13 -3 -3 4.20 1.90 -13 -3 -3 0.10 7.20 -13 3 3 6.50 8.30 -13 3 3 3.10 1.60 -13 -3 3 1.60 8.10 -13 -3 3 3.00 1.70 -13 3 -3 -3.50 7.90 -13 3 -3 3.70 1.60 13 3 4 4.90 6.20 13 -3 -4 -5.70 6.70 13 -3 -4 1.10 5.30 13 -3 -4 1.40 1.60 13 3 -4 3.10 2.00 13 3 -4 1.10 4.40 13 -3 4 3.00 1.60 13 -3 4 1.70 6.40 -13 -3 -4 2.00 1.70 -13 3 4 -2.70 8.60 -13 3 4 1.20 1.50 -13 -3 4 1.50 7.90 -13 -3 4 1.40 1.50 -13 3 -4 3.00 7.60 -13 3 -4 2.90 1.70 13 3 5 1.80 5.40 13 3 5 0.20 1.70 13 -3 -5 -14.80 7.90 13 -3 -5 2.30 1.70 13 3 -5 1.30 2.00 13 3 -5 -10.10 8.10 13 -3 5 -6.90 6.90 13 -3 5 1.90 1.50 13 -3 5 -6.00 6.90 -13 3 5 6.60 8.80 -13 3 5 0.50 1.50 -13 -3 5 -5.30 7.30 -13 -3 5 0.40 1.60 -13 3 -5 -8.30 7.80 13 3 6 1.10 1.70 13 -3 -6 5.60 7.30 13 -3 -6 0.80 1.70 13 3 -6 -0.90 7.40 13 3 -6 0.60 1.90 13 -3 6 0.80 6.50 13 -3 6 1.00 1.40 13 -3 6 2.40 6.40 -13 -3 -6 3.30 9.00 -13 3 6 1.10 1.50 -13 3 6 2.40 8.30 -13 -3 6 0.50 1.60 -13 3 -6 2.10 1.70 13 3 7 1.00 2.00 13 -3 -7 -2.20 7.30 13 -3 -7 1.20 1.70 13 3 -7 0.30 2.10 13 3 -7 -8.30 8.80 13 -3 7 0.00 1.40 -13 -3 -7 -0.40 1.90 -13 3 7 0.00 2.50 -13 3 7 0.20 1.50 -13 -3 7 0.40 1.60 -13 3 -7 1.40 1.60 13 3 8 -0.60 6.60 13 3 8 1.60 2.10 13 -3 -8 1.40 1.80 13 3 -8 2.80 9.00 13 -3 8 -3.00 6.30 13 -3 8 2.10 1.50 13 -3 8 -3.90 7.70 -13 -3 -8 1.00 2.10 -13 3 8 1.60 1.60 -13 3 8 0.20 2.50 -13 -3 8 0.10 1.60 -13 3 -8 1.60 1.70 13 5 0 87.09 15.90 13 -5 0 56.19 19.20 13 -5 0 82.79 15.10 -13 -5 0 38.10 14.00 -13 -5 0 109.99 19.90 -13 5 0 72.19 13.10 13 5 1 3.60 5.10 13 5 1 1.30 6.80 13 5 1 2.80 2.30 13 -5 -1 0.50 1.80 13 -5 -1 -2.00 7.10 13 -5 -1 4.00 8.30 13 5 -1 0.30 4.60 13 5 -1 0.10 1.80 13 5 -1 -6.50 6.30 13 -5 1 -1.50 6.50 13 -5 1 3.60 2.10 -13 -5 -1 -2.00 7.40 -13 -5 -1 3.00 1.90 -13 5 1 0.80 1.60 -13 5 1 -3.40 5.90 -13 -5 1 2.10 2.10 -13 -5 1 1.90 7.30 -13 5 -1 -5.10 7.90 -13 5 -1 3.40 1.80 13 5 2 7.70 7.20 13 5 2 1.30 4.90 13 5 2 -1.00 1.90 13 -5 -2 -2.70 7.90 13 -5 -2 -3.90 8.60 13 -5 -2 1.00 1.70 13 5 -2 3.90 4.00 13 5 -2 8.10 6.30 13 5 -2 0.00 1.90 13 -5 2 -1.10 6.70 13 -5 2 -1.40 8.40 13 -5 2 0.60 1.90 -13 -5 -2 2.90 6.90 -13 -5 -2 -0.30 1.70 -13 5 2 1.30 7.60 -13 5 2 0.90 1.60 -13 5 2 -3.10 6.00 -13 -5 2 3.60 7.70 -13 -5 2 0.70 1.50 -13 5 -2 -0.50 8.70 -13 5 -2 0.80 1.70 13 5 3 1.70 5.40 13 5 3 -6.40 6.70 13 5 3 0.90 1.90 13 -5 -3 1.20 1.70 13 -5 -3 -0.90 6.60 13 -5 -3 5.40 8.80 13 5 -3 0.50 2.00 13 5 -3 8.30 6.30 13 -5 3 13.40 9.60 13 -5 3 -4.00 6.60 -13 -5 -3 1.20 1.60 -13 5 3 -3.20 7.40 -13 5 3 1.40 1.60 -13 5 3 2.20 5.60 -13 -5 3 1.90 7.90 -13 -5 3 0.30 1.60 -13 5 -3 -0.80 9.80 -13 5 -3 1.20 1.80 13 5 4 -0.50 5.40 13 5 4 6.00 6.70 13 -5 -4 -4.20 6.70 13 -5 -4 2.00 1.80 13 -5 -4 -1.80 7.70 13 5 -4 1.90 5.90 13 5 -4 3.40 2.20 13 -5 4 1.40 1.90 13 -5 4 -5.50 9.60 13 -5 4 1.10 6.70 -13 -5 -4 1.40 1.60 -13 5 4 2.30 1.70 -13 5 4 0.10 4.80 -13 -5 4 0.70 1.60 -13 5 -4 -1.80 11.20 -13 5 -4 5.80 2.30 13 5 5 16.80 9.30 13 5 5 3.00 1.90 13 -5 -5 3.20 7.40 13 -5 -5 1.40 1.80 13 -5 -5 0.10 5.50 13 5 -5 26.10 10.40 13 5 -5 0.50 2.20 13 -5 5 0.10 1.90 13 -5 5 -0.60 7.70 13 -5 5 -5.00 8.50 -13 -5 -5 7.10 2.50 -13 5 5 3.50 1.90 -13 5 5 1.40 5.40 -13 -5 5 2.10 1.70 -13 5 -5 -5.80 10.70 13 5 6 11.80 3.10 13 -5 -6 -0.40 6.00 13 -5 -6 0.40 1.80 13 -5 6 4.30 8.60 -13 5 6 -0.40 4.00 -13 5 6 2.70 1.80 -13 -5 6 2.00 1.80 13 5 7 1.30 1.70 13 -5 -7 -5.80 6.10 13 -5 -7 -0.10 8.00 13 -5 -7 -0.10 1.90 13 -5 7 -1.00 8.70 -13 -5 -7 1.00 1.90 -13 5 7 2.10 1.90 -13 5 7 2.70 2.50 -13 -5 7 3.10 2.20 -13 5 -7 1.30 2.20 13 7 0 41.30 13.80 13 -7 0 47.90 16.30 13 -7 0 55.59 10.30 -13 -7 0 45.50 8.60 -13 7 0 42.90 8.00 13 7 1 4.50 4.90 13 7 1 21.00 8.80 13 7 1 6.20 2.50 13 -7 -1 1.20 5.70 13 -7 -1 7.50 2.40 13 -7 -1 7.40 7.80 13 7 -1 -0.40 5.70 13 7 -1 6.00 2.20 13 -7 1 -1.60 5.10 13 -7 1 5.70 2.30 13 -7 1 16.00 8.90 -13 -7 -1 4.70 1.90 -13 7 1 6.10 2.00 -13 7 1 0.50 9.20 -13 -7 1 5.50 2.10 -13 7 -1 4.40 1.90 13 7 2 4.00 5.30 13 7 2 6.50 6.00 13 7 2 9.10 2.60 13 -7 -2 8.10 2.40 13 -7 -2 -1.10 5.50 13 -7 -2 10.60 8.40 13 7 -2 14.80 3.40 13 7 -2 7.00 5.90 13 -7 2 9.30 2.70 13 -7 2 8.20 9.30 13 -7 2 2.80 5.30 -13 -7 -2 11.30 2.80 -13 7 2 9.80 2.60 -13 7 2 -1.10 10.00 -13 -7 2 10.20 2.60 -13 7 -2 6.40 2.20 13 7 3 -5.50 5.30 13 7 3 0.10 1.70 13 -7 -3 -3.00 7.40 13 -7 -3 -4.30 6.40 13 -7 -3 -0.30 1.70 13 7 -3 1.30 1.80 13 7 -3 0.40 5.90 13 -7 3 1.90 5.10 -13 -7 -3 1.80 1.70 -13 7 3 0.20 1.70 -13 7 3 -1.30 7.60 -13 -7 3 1.70 1.60 -13 7 -3 -0.80 1.80 13 7 4 4.90 6.00 13 -7 -4 -1.70 5.20 13 -7 -4 8.60 2.60 13 7 -4 9.10 2.80 13 7 -4 12.50 7.60 13 -7 4 11.60 8.40 -13 -7 -4 12.20 3.00 -13 7 4 9.60 2.70 -13 7 4 -1.90 8.70 -13 -7 4 6.20 2.10 13 -7 -5 10.70 9.60 13 -7 -5 4.30 2.10 13 7 -5 2.40 6.30 13 -7 5 -4.50 8.70 13 -7 5 6.40 2.30 -13 -7 -5 1.80 2.00 -13 7 5 1.10 2.20 -13 -7 5 6.00 2.20 -13 7 -5 2.90 2.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 89236 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y, -z-1/2' 'x, -y, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' 'x+1/2, -y+1/2, z-1/2' '-x+1/2, y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si 0.500000 0.4643(5) 0.0696(4) 0.024(2) Uiso 0.5 2 d S . P . . Si2 Si 0.000000 0.0498(5) 0.1650(4) 0.024(2) Uiso 0.5 2 d S . P . . Si3 Si 0.500000 0.4759(5) 0.2669(3) 0.027(2) Uiso 0.5 2 d S . P . . Si4 Si 0.000000 0.0535(4) 0.3666(4) 0.0216(19) Uiso 0.5 2 d S . P . . Si5 Si 0.500000 0.4703(5) 0.4601(4) 0.028(2) Uiso 0.5 2 d S . P . . Si6 Si 0.2426(11) 0.1226(6) 0.3438(5) 0.022(4) Uiso 0.5 1 d . . P . . Si7 Si 0.3582(8) 0.0567(5) 0.4398(4) 0.015(3) Uiso 0.5 1 d . . P . . Si8 Si 0.2364(11) 0.4389(6) 0.4410(5) 0.018(3) Uiso 0.5 1 d . . P . . Si9 Si 0.1411(11) 0.3687(6) 0.1574(5) 0.022(4) Uiso 0.5 1 d . . P . . Si10 Si 0.1434(11) 0.2395(6) 0.1912(5) 0.022(4) Uiso 0.5 1 d . . P . . Si11 Si 0.2393(9) 0.1201(5) 0.1481(5) 0.015(3) Uiso 0.5 1 d . . P . . Si12 Si 0.3562(10) 0.0667(5) 0.0552(4) 0.025(4) Uiso 0.5 1 d . . P . . Si13 Si 0.2395(13) 0.4298(6) 0.0567(5) 0.030(5) Uiso 0.5 1 d . . P . . Si14 Si 0.1386(10) 0.3636(6) 0.3495(5) 0.019(3) Uiso 0.5 1 d . . P . . Si15 Si 0.1388(11) 0.2360(6) 0.3160(5) 0.019(4) Uiso 0.5 1 d . . P . . Si16 Si 0.2427(5) 0.4348(2) 0.250000 0.0272(12) Uiso 1 2 d S . P . . Si17 Si 0.3594(4) 0.0622(2) 0.250000 0.0219(11) Uiso 1 2 d S . P . . O1 O 0.000000 0.0151(9) 0.0239(7) 0.043(4) Uiso 0.5 2 d S . P . . O2 O 0.500000 0.4951(9) 0.1253(7) 0.048(4) Uiso 0.5 2 d S . P . . O3 O 0.000000 0.0288(10) 0.2249(8) 0.054(5) Uiso 0.5 2 d S . P . . O4 O 0.500000 0.5018(9) 0.3259(7) 0.044(4) Uiso 0.5 2 d S . P . . O5 O 0.000000 0.0300(10) 0.4253(8) 0.058(5) Uiso 0.5 2 d S . P . . O6 O 0.1765(11) 0.3015(6) 0.1658(5) 0.026(3) Uiso 0.5 1 d . . P . . O7 O 0.2198(11) 0.1913(6) 0.1535(5) 0.024(3) Uiso 0.5 1 d . . P . . O8 O 0.3319(13) 0.1107(5) 0.1028(5) 0.031(3) Uiso 0.5 1 d . . P . . O9 O 0.3827(12) 0.4254(6) 0.0657(6) 0.036(3) Uiso 0.5 1 d . . P . . O10 O 0.1969(15) 0.5002(8) 0.0821(8) 0.040(5) Uiso 0.5 1 d . . P . . O11 O 0.1690(14) 0.4236(7) 0.4957(6) 0.041(3) Uiso 0.5 1 d . . P . . O12 O 0.1680(11) 0.3879(5) 0.0923(4) 0.025(2) Uiso 0.5 1 d . . P . . O13 O 0.1185(12) 0.0881(6) 0.1575(6) 0.038(3) Uiso 0.5 1 d . . P . . O14 O 0.3378(13) 0.0950(6) 0.1942(5) 0.037(3) Uiso 0.5 1 d . . P . . O15 O 0.1819(19) 0.3970(8) 0.2923(8) 0.065(5) Uiso 0.5 1 d . . P . . O16 O 0.1641(13) 0.2948(7) 0.3462(6) 0.029(4) Uiso 0.5 1 d . . P . . O17 O 0.2267(11) 0.1878(6) 0.3331(5) 0.024(3) Uiso 0.5 1 d . . P . . O18 O 0.2953(12) 0.1100(5) 0.4080(5) 0.028(3) Uiso 0.5 1 d . . P . . O19 O 0.3815(12) 0.4336(6) 0.4509(6) 0.035(3) Uiso 0.5 1 d . . P . . O20 O 0.2980(13) -0.0004(7) 0.4300(7) 0.030(4) Uiso 0.5 1 d . . P . . O21 O 0.2954(15) 0.0812(8) 0.4954(6) 0.049(4) Uiso 0.5 1 d . . P . . O22 O 0.2131(15) 0.3901(7) 0.3952(6) 0.046(3) Uiso 0.5 1 d . . P . . O23 O 0.1111(11) 0.0947(6) 0.3619(6) 0.038(3) Uiso 0.5 1 d . . P . . O24 O 0.2929(18) 0.0974(8) 0.2927(7) 0.060(4) Uiso 0.5 1 d . . P . . O25 O 0.2202(13) 0.4056(6) 0.1928(5) 0.040(3) Uiso 0.5 1 d . . P . . O26 O 0.1949(10) 0.4994(6) 0.2397(6) 0.053(4) Uiso 0.5 1 d . . P . . O27 O 0.1702(8) 0.2418(4) 0.250000 0.0379(19) Uiso 1 2 d S . P . . O28 O 0.3866(10) 0.4353(5) 0.2612(4) 0.043(3) Uiso 0.5 1 d . . P . . O29 O 0.000000 0.2203(12) 0.1835(11) 0.030(8) Uiso 0.5 2 d S . P . . O30 O 0.000000 0.3772(7) 0.1670(6) 0.024(3) Uiso 0.5 2 d S . P . . O31 O 0.000000 0.2255(14) 0.3252(12) 0.038(10) Uiso 0.5 2 d S . P . . O32 O 0.000000 0.3710(9) 0.3588(8) 0.043(4) Uiso 0.5 2 d S . P . . O33 O 0.500000 0.0580(11) 0.0661(11) 0.049(6) Uiso 0.5 2 d S . P . . O34 O 0.500000 0.0562(11) 0.4507(10) 0.043(6) Uiso 0.5 2 d S . P . . O35 O 0.500000 0.0584(8) 0.2611(8) 0.053(5) Uiso 0.5 2 d S . P . . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O O 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Si5 Si1 Si4 117.4(14) 10_556 14_556 ? Si5 Si1 O1 35.2(12) 10_556 5 ? Si5 Si1 O2 142.5(17) 10_556 . ? Si5 Si1 O5 84.4(15) 10_556 14_556 ? Si5 Si1 O9 92.5(9) 10_556 12_655 ? Si5 Si1 O9 92.5(9) 10_556 . ? Si5 Si1 O19 76.3(9) 10_556 10_556 ? Si5 Si1 O19 76.3(9) 10_556 3_655 ? O1 Si1 Si4 82.2(8) 5 14_556 ? O2 Si1 Si4 25.2(8) . 14_556 ? O2 Si1 O1 107.3(11) . 5 ? O2 Si1 O9 108.1(7) . 12_655 ? O2 Si1 O9 108.1(7) . . ? O2 Si1 O19 119.4(7) . 10_556 ? O2 Si1 O19 119.4(7) . 3_655 ? O5 Si1 Si4 33.0(9) 14_556 14_556 ? O5 Si1 O1 49.2(11) 14_556 5 ? O5 Si1 O2 58.1(12) 14_556 . ? O5 Si1 O9 124.6(6) 14_556 . ? O5 Si1 O9 124.6(6) 14_556 12_655 ? O5 Si1 O19 118.3(7) 14_556 3_655 ? O5 Si1 O19 118.3(7) 14_556 10_556 ? O9 Si1 Si4 118.9(6) 12_655 14_556 ? O9 Si1 Si4 118.9(6) . 14_556 ? O9 Si1 O1 111.2(8) 12_655 5 ? O9 Si1 O1 111.2(8) . 5 ? O9 Si1 O9 110.7(12) . 12_655 ? O19 Si1 Si4 123.5(6) 3_655 14_556 ? O19 Si1 Si4 123.5(6) 10_556 14_556 ? O19 Si1 O1 95.4(8) 10_556 5 ? O19 Si1 O1 95.4(8) 3_655 5 ? O19 Si1 O9 114.4(8) 3_655 . ? O19 Si1 O9 16.6(6) 10_556 . ? O19 Si1 O9 114.4(8) 10_556 12_655 ? O19 Si1 O9 16.6(6) 3_655 12_655 ? O19 Si1 O19 112.9(11) 10_556 3_655 ? Si4 Si2 Si3 141.1(12) 10_556 14_446 ? Si4 Si2 O2 57.8(12) 10_556 5_445 ? Si4 Si2 O3 168.2(16) 10_556 . ? Si4 Si2 O4 107.7(16) 10_556 14_446 ? Si4 Si2 O5 17.5(11) 10_556 10_556 ? Si4 Si2 O13 79.9(8) 10_556 12 ? Si4 Si2 O13 79.9(8) 10_556 . ? Si4 Si2 O23 63.5(8) 10_556 10_556 ? Si4 Si2 O23 63.5(8) 10_556 3 ? O2 Si2 Si3 83.3(9) 5_445 14_446 ? O2 Si2 O5 40.3(9) 5_445 10_556 ? O2 Si2 O23 103.1(8) 5_445 3 ? O2 Si2 O23 103.1(8) 5_445 10_556 ? O3 Si2 Si3 27.0(9) . 14_446 ? O3 Si2 O2 110.3(12) . 5_445 ? O3 Si2 O5 150.7(12) . 10_556 ? O3 Si2 O13 106.3(8) . 12 ? O3 Si2 O13 106.3(8) . . ? O3 Si2 O23 123.3(7) . 10_556 ? O3 Si2 O23 123.3(7) . 3 ? O4 Si2 Si3 33.4(10) 14_446 14_446 ? O4 Si2 O2 49.9(13) 14_446 5_445 ? O4 Si2 O3 60.4(13) 14_446 . ? O4 Si2 O5 90.2(12) 14_446 10_556 ? O4 Si2 O13 124.4(6) 14_446 12 ? O4 Si2 O13 124.4(6) 14_446 . ? O4 Si2 O23 131.1(7) 14_446 3 ? O4 Si2 O23 131.1(7) 14_446 10_556 ? O5 Si2 Si3 123.6(8) 10_556 14_446 ? O13 Si2 Si3 118.2(6) . 14_446 ? O13 Si2 Si3 118.2(6) 12 14_446 ? O13 Si2 O2 111.2(7) . 5_445 ? O13 Si2 O2 111.2(7) 12 5_445 ? O13 Si2 O5 89.7(7) . 10_556 ? O13 Si2 O5 89.7(7) 12 10_556 ? O13 Si2 O13 111.3(12) . 12 ? O13 Si2 O23 102.2(9) 12 10_556 ? O13 Si2 O23 17.0(5) . 10_556 ? O13 Si2 O23 102.2(9) . 3 ? O13 Si2 O23 17.0(5) 12 3 ? O23 Si2 Si3 133.7(5) 3 14_446 ? O23 Si2 Si3 133.7(5) 10_556 14_446 ? O23 Si2 O5 74.9(7) 10_556 10_556 ? O23 Si2 O5 74.9(7) 3 10_556 ? O23 Si2 O23 90.1(11) 10_556 3 ? Si3 Si3 Si2 135.0(3) 10_556 14_556 ? Si3 Si3 O3 99.6(10) 10_556 14_556 ? Si3 Si3 O3 49.2(8) 10_556 5 ? Si3 Si3 O4 158.0(8) 10_556 . ? Si3 Si3 O28 65.8(5) 10_556 3_655 ? Si3 Si3 O28 84.8(5) 10_556 12_655 ? Si3 Si3 O28 65.8(5) 10_556 10_556 ? Si3 Si3 O28 84.8(5) 10_556 . ? O3 Si3 Si2 35.5(10) 14_556 14_556 ? O3 Si3 Si2 85.9(9) 5 14_556 ? O3 Si3 O3 50.4(17) 14_556 5 ? O3 Si3 O4 58.4(12) 14_556 . ? O3 Si3 O28 127.2(7) 14_556 10_556 ? O3 Si3 O28 98.2(7) 5 3_655 ? O3 Si3 O28 126.9(5) 14_556 . ? O3 Si3 O28 98.2(7) 5 10_556 ? O3 Si3 O28 127.2(7) 14_556 3_655 ? O3 Si3 O28 126.9(6) 14_556 12_655 ? O4 Si3 Si2 22.9(8) . 14_556 ? O4 Si3 O3 108.8(12) . 5 ? O4 Si3 O28 125.7(6) . 10_556 ? O4 Si3 O28 125.7(6) . 3_655 ? O28 Si3 Si2 118.9(5) 12_655 14_556 ? O28 Si3 Si2 132.4(5) 3_655 14_556 ? O28 Si3 Si2 132.4(5) 10_556 14_556 ? O28 Si3 Si2 118.9(5) . 14_556 ? O28 Si3 O3 112.9(7) 12_655 5 ? O28 Si3 O3 112.9(7) . 5 ? O28 Si3 O4 107.8(7) 12_655 . ? O28 Si3 O4 107.8(7) . . ? O28 Si3 O28 94.2(9) 10_556 3_655 ? O28 Si3 O28 19.0(7) . 10_556 ? O28 Si3 O28 103.1(10) . 3_655 ? O28 Si3 O28 106.3(11) 12_655 . ? O28 Si3 O28 103.1(10) 12_655 10_556 ? O28 Si3 O28 19.0(7) 12_655 3_655 ? Si2 Si4 Si1 121.8(12) 10_556 14_446 ? Si2 Si4 O2 92.5(14) 10_556 14_446 ? Si2 Si4 O4 43.3(11) 10_556 5_445 ? Si2 Si4 O5 153.7(16) 10_556 . ? Si2 Si4 O13 71.8(8) 10_556 3 ? Si2 Si4 O13 71.8(8) 10_556 10_556 ? Si2 Si4 O23 89.4(9) 10_556 . ? Si2 Si4 O23 89.4(9) 10_556 12 ? O2 Si4 Si1 29.3(8) 14_446 14_446 ? O2 Si4 O4 49.2(12) 14_446 5_445 ? O2 Si4 O5 61.2(12) 14_446 . ? O2 Si4 O13 122.1(7) 14_446 10_556 ? O2 Si4 O13 122.1(7) 14_446 3 ? O2 Si4 O23 127.7(6) 14_446 12 ? O2 Si4 O23 127.7(6) 14_446 . ? O4 Si4 Si1 78.5(9) 5_445 14_446 ? O4 Si4 O13 97.4(8) 5_445 10_556 ? O4 Si4 O13 97.4(8) 5_445 3 ? O5 Si4 Si1 31.9(9) . 14_446 ? O5 Si4 O4 110.4(13) . 5_445 ? O5 Si4 O13 120.6(7) . 3 ? O5 Si4 O13 120.6(7) . 10_556 ? O13 Si4 Si1 127.2(5) 10_556 14_446 ? O13 Si4 Si1 127.2(5) 3 14_446 ? O13 Si4 O13 105.6(11) 10_556 3 ? O23 Si4 Si1 121.7(6) 12 14_446 ? O23 Si4 Si1 121.7(6) . 14_446 ? O23 Si4 O4 114.4(8) 12 5_445 ? O23 Si4 O4 114.4(8) . 5_445 ? O23 Si4 O5 106.3(8) 12 . ? O23 Si4 O5 106.3(8) . . ? O23 Si4 O13 18.2(6) . 10_556 ? O23 Si4 O13 108.0(8) 12 10_556 ? O23 Si4 O13 18.2(6) 12 3 ? O23 Si4 O13 108.0(8) . 3 ? O23 Si4 O23 104.5(12) 12 . ? Si1 Si5 Si5 156.1(16) 10_556 9_666 ? Si1 Si5 O1 178.6(17) 10_556 6 ? Si1 Si5 O1 121.7(18) 10_556 14_556 ? Si1 Si5 O2 25.5(12) 10_556 10_556 ? Si1 Si5 O5 68.2(14) 10_556 5 ? Si1 Si5 O9 62.5(8) 10_556 10_556 ? Si1 Si5 O9 62.5(8) 10_556 3_655 ? Si1 Si5 O19 76.1(9) 10_556 12_655 ? Si1 Si5 O19 76.1(9) 10_556 . ? O1 Si5 Si5 22.5(7) 6 9_666 ? O1 Si5 Si5 34.4(10) 14_556 9_666 ? O1 Si5 O1 56.9(16) 14_556 6 ? O1 Si5 O2 96.2(13) 14_556 10_556 ? O1 Si5 O2 153.1(11) 6 10_556 ? O1 Si5 O5 53.5(13) 14_556 5 ? O1 Si5 O9 118.2(7) 6 10_556 ? O1 Si5 O9 118.2(7) 6 3_655 ? O1 Si5 O9 132.1(6) 14_556 3_655 ? O1 Si5 O9 132.1(6) 14_556 10_556 ? O1 Si5 O19 123.4(6) 14_556 12_655 ? O1 Si5 O19 123.4(6) 14_556 . ? O2 Si5 Si5 130.6(9) 10_556 9_666 ? O5 Si5 Si5 87.9(10) 5 9_666 ? O5 Si5 O1 110.4(13) 5 6 ? O5 Si5 O2 42.7(10) 5 10_556 ? O5 Si5 O9 107.2(8) 5 10_556 ? O5 Si5 O9 107.2(8) 5 3_655 ? O9 Si5 Si5 128.7(6) 3_655 9_666 ? O9 Si5 Si5 128.7(6) 10_556 9_666 ? O9 Si5 O2 78.5(7) 10_556 10_556 ? O9 Si5 O2 78.5(7) 3_655 10_556 ? O9 Si5 O9 93.9(11) 10_556 3_655 ? O19 Si5 Si5 115.0(7) 12_655 9_666 ? O19 Si5 Si5 114.9(7) . 9_666 ? O19 Si5 O1 104.6(8) . 6 ? O19 Si5 O1 104.6(8) 12_655 6 ? O19 Si5 O2 89.9(7) 12_655 10_556 ? O19 Si5 O2 89.9(7) . 10_556 ? O19 Si5 O5 111.9(7) . 5 ? O19 Si5 O5 111.9(7) 12_655 5 ? O19 Si5 O9 104.3(9) 12_655 10_556 ? O19 Si5 O9 104.3(9) . 3_655 ? O19 Si5 O9 14.0(6) . 10_556 ? O19 Si5 O9 14.0(6) 12_655 3_655 ? O19 Si5 O19 112.8(13) 12_655 . ? Si11 Si6 O7 101(6) 10_556 10_556 ? Si11 Si6 O8 46(6) 10_556 10_556 ? Si11 Si6 O13 75(6) 10_556 10_556 ? Si11 Si6 O14 126(6) 10_556 10_556 ? Si11 Si6 O17 114(7) 10_556 . ? Si11 Si6 O18 30(5) 10_556 . ? Si11 Si6 O23 59(6) 10_556 . ? Si11 Si6 O24 140(7) 10_556 . ? O7 Si6 O8 102.7(9) 10_556 10_556 ? O7 Si6 O18 100.3(9) 10_556 . ? O7 Si6 O23 103.4(10) 10_556 . ? O8 Si6 O18 16.4(5) 10_556 . ? O13 Si6 O7 110.9(10) 10_556 10_556 ? O13 Si6 O8 116.5(10) 10_556 10_556 ? O13 Si6 O18 103.2(9) 10_556 . ? O13 Si6 O23 18.1(6) 10_556 . ? O14 Si6 O7 122.3(10) 10_556 10_556 ? O14 Si6 O8 91.1(10) 10_556 10_556 ? O14 Si6 O13 111.8(11) 10_556 10_556 ? O14 Si6 O18 105.6(10) 10_556 . ? O14 Si6 O23 127.4(11) 10_556 . ? O17 Si6 O7 12.7(6) . 10_556 ? O17 Si6 O8 111.4(10) . 10_556 ? O17 Si6 O13 112.6(10) . 10_556 ? O17 Si6 O14 111.7(10) . 10_556 ? O17 Si6 O18 111.3(10) . . ? O17 Si6 O23 108.9(10) . . ? O23 Si6 O8 103.8(10) . 10_556 ? O23 Si6 O18 88.9(9) . . ? O24 Si6 O7 118.1(12) . 10_556 ? O24 Si6 O8 113.0(12) . 10_556 ? O24 Si6 O13 96.4(12) . 10_556 ? O24 Si6 O14 22.4(7) . 10_556 ? O24 Si6 O17 105.6(11) . . ? O24 Si6 O18 126.6(12) . . ? O24 Si6 O23 114.1(12) . . ? Si12 Si7 O8 69(4) 10_556 10_556 ? Si12 Si7 O10 151(5) 10_556 7_545 ? Si12 Si7 O11 45(4) 10_556 13_556 ? Si12 Si7 O18 63(4) 10_556 . ? Si12 Si7 O20 144(5) 10_556 . ? Si12 Si7 O21 43(4) 10_556 . ? Si12 Si7 O33 96(4) 10_556 10_556 ? Si12 Si7 O34 90(4) 10_556 . ? O8 Si7 O11 112.2(9) 10_556 13_556 ? O10 Si7 O8 109.5(10) 7_545 10_556 ? O10 Si7 O11 119.5(11) 7_545 13_556 ? O10 Si7 O18 107.1(10) 7_545 . ? O10 Si7 O21 114.8(11) 7_545 . ? O10 Si7 O33 112.3(13) 7_545 10_556 ? O10 Si7 O34 116.5(13) 7_545 . ? O18 Si7 O8 17.1(5) . 10_556 ? O18 Si7 O11 100.8(9) . 13_556 ? O18 Si7 O21 88.5(9) . . ? O20 Si7 O8 118.2(10) . 10_556 ? O20 Si7 O10 11.5(9) . 7_545 ? O20 Si7 O11 108.1(10) . 13_556 ? O20 Si7 O18 113.1(9) . . ? O20 Si7 O21 104.4(11) . . ? O20 Si7 O33 116.5(13) . 10_556 ? O20 Si7 O34 117.5(12) . . ? O21 Si7 O8 102.2(10) . 10_556 ? O21 Si7 O11 15.9(7) . 13_556 ? O33 Si7 O8 95.8(12) 10_556 10_556 ? O33 Si7 O11 105.1(12) 10_556 13_556 ? O33 Si7 O18 111.6(12) 10_556 . ? O33 Si7 O21 119.5(13) 10_556 . ? O33 Si7 O34 15.3(11) 10_556 . ? O34 Si7 O8 106.7(12) . 10_556 ? O34 Si7 O11 90.8(11) . 13_556 ? O34 Si7 O18 120.9(12) . . ? O34 Si7 O21 105.9(12) . . ? Si13 Si8 O9 72(6) 10_556 10_556 ? Si13 Si8 O10 170(7) 10_556 10_556 ? Si13 Si8 O11 69(6) 10_556 . ? Si13 Si8 O12 61(6) 10_556 10_556 ? Si13 Si8 O19 75(7) 10_556 . ? Si13 Si8 O20 173(7) 10_556 16 ? Si13 Si8 O21 62(6) 10_556 13_556 ? Si13 Si8 O22 63(6) 10_556 . ? O9 Si8 O21 104.3(10) 10_556 13_556 ? O10 Si8 O9 113.5(11) 10_556 10_556 ? O10 Si8 O11 112.3(11) 10_556 . ? O10 Si8 O12 109.0(11) 10_556 10_556 ? O10 Si8 O19 113.2(11) 10_556 . ? O10 Si8 O21 121.8(12) 10_556 13_556 ? O10 Si8 O22 108.3(11) 10_556 . ? O11 Si8 O9 120.2(11) . 10_556 ? O11 Si8 O12 93.5(9) . 10_556 ? O11 Si8 O19 108.4(10) . . ? O11 Si8 O21 16.0(7) . 13_556 ? O11 Si8 O22 112.1(11) . . ? O12 Si8 O9 105.7(10) 10_556 10_556 ? O12 Si8 O19 118.9(10) 10_556 . ? O12 Si8 O21 100.8(10) 10_556 13_556 ? O19 Si8 O9 15.8(6) . 10_556 ? O19 Si8 O21 92.5(10) . 13_556 ? O20 Si8 O9 114.2(11) 16 10_556 ? O20 Si8 O10 10.8(9) 16 10_556 ? O20 Si8 O11 104.3(11) 16 . ? O20 Si8 O12 117.8(10) 16 10_556 ? O20 Si8 O19 110.7(11) 16 . ? O20 Si8 O21 112.3(12) 16 13_556 ? O20 Si8 O22 118.8(11) 16 . ? O22 Si8 O9 87.4(10) . 10_556 ? O22 Si8 O12 21.0(6) . 10_556 ? O22 Si8 O19 102.2(10) . . ? O22 Si8 O21 116.2(11) . 13_556 ? Si14 Si9 O6 67(7) 10_556 . ? Si14 Si9 O12 52(7) 10_556 . ? Si14 Si9 O15 168(7) 10_556 10_556 ? Si14 Si9 O16 55(7) 10_556 10_556 ? Si14 Si9 O22 64(7) 10_556 10_556 ? Si14 Si9 O25 151(7) 10_556 . ? Si14 Si9 O30 94(6) 10_556 . ? Si14 Si9 O32 72(6) 10_556 10_556 ? O6 Si9 O12 109.3(9) . . ? O6 Si9 O16 11.9(6) . 10_556 ? O6 Si9 O22 106.2(10) . 10_556 ? O6 Si9 O32 107.5(11) . 10_556 ? O12 Si9 O16 100.4(9) . 10_556 ? O15 Si9 O6 103.6(12) 10_556 . ? O15 Si9 O12 129.6(13) 10_556 . ? O15 Si9 O16 115.5(12) 10_556 10_556 ? O15 Si9 O22 113.9(14) 10_556 10_556 ? O15 Si9 O25 23.0(8) 10_556 . ? O15 Si9 O30 96.7(12) 10_556 . ? O15 Si9 O32 119.4(13) 10_556 10_556 ? O22 Si9 O12 20.2(6) 10_556 . ? O22 Si9 O16 100.7(9) 10_556 10_556 ? O22 Si9 O32 105.4(12) 10_556 10_556 ? O25 Si9 O6 108.8(11) . . ? O25 Si9 O12 108.1(11) . . ? O25 Si9 O16 120.0(11) . 10_556 ? O25 Si9 O22 91.1(11) . 10_556 ? O25 Si9 O30 114.4(11) . . ? O25 Si9 O32 133.7(13) . 10_556 ? O30 Si9 O6 109.8(10) . . ? O30 Si9 O12 106.4(10) . . ? O30 Si9 O16 105.9(10) . 10_556 ? O30 Si9 O22 124.8(11) . 10_556 ? O30 Si9 O32 23.7(7) . 10_556 ? O32 Si9 O12 85.6(10) 10_556 . ? O32 Si9 O16 99.4(11) 10_556 10_556 ? Si15 Si10 O6 93(7) 10_556 . ? Si15 Si10 O7 51(7) 10_556 . ? Si15 Si10 O16 80(7) 10_556 10_556 ? Si15 Si10 O17 61(7) 10_556 10_556 ? Si15 Si10 O27 158(8) 10_556 . ? Si15 Si10 O29 63(7) 10_556 . ? Si15 Si10 O31 58(7) 10_556 10_556 ? O6 Si10 O7 104.3(10) . . ? O6 Si10 O17 111.8(10) . 10_556 ? O6 Si10 O29 114.1(13) . . ? O6 Si10 O31 106.9(14) . 10_556 ? O16 Si10 O6 13.0(6) 10_556 . ? O16 Si10 O7 97.1(10) 10_556 . ? O16 Si10 O17 106.3(10) 10_556 10_556 ? O16 Si10 O29 106.3(13) 10_556 . ? O16 Si10 O31 98.4(14) 10_556 10_556 ? O17 Si10 O7 12.1(6) 10_556 . ? O17 Si10 O29 107.8(12) 10_556 . ? O17 Si10 O31 107.9(13) 10_556 10_556 ? O27 Si10 O6 108.3(10) . . ? O27 Si10 O7 118.1(10) . . ? O27 Si10 O16 121.3(11) . 10_556 ? O27 Si10 O17 106.2(10) . 10_556 ? O27 Si10 O29 108.2(12) . . ? O27 Si10 O31 115.8(13) . 10_556 ? O29 Si10 O7 104.0(12) . . ? O29 Si10 O31 8.5(15) . 10_556 ? O31 Si10 O7 102.4(13) 10_556 . ? Si6 Si11 O7 72(6) 10_556 . ? Si6 Si11 O8 128(6) 10_556 . ? Si6 Si11 O13 97(6) 10_556 . ? Si6 Si11 O14 48(6) 10_556 . ? Si6 Si11 O17 59(6) 10_556 10_556 ? Si6 Si11 O18 146(6) 10_556 10_556 ? Si6 Si11 O23 114(6) 10_556 10_556 ? Si6 Si11 O24 35(6) 10_556 10_556 ? O7 Si11 O14 111.5(9) . . ? O7 Si11 O24 106.4(10) . 10_556 ? O8 Si11 O7 106.6(9) . . ? O8 Si11 O13 128.4(10) . . ? O8 Si11 O14 91.3(9) . . ? O8 Si11 O17 113.7(9) . 10_556 ? O8 Si11 O18 18.2(6) . 10_556 ? O8 Si11 O23 115.9(10) . 10_556 ? O8 Si11 O24 111.5(11) . 10_556 ? O13 Si11 O7 110.2(9) . . ? O13 Si11 O14 107.0(10) . . ? O13 Si11 O17 109.6(9) . 10_556 ? O13 Si11 O18 114.4(10) . 10_556 ? O13 Si11 O23 19.1(6) . 10_556 ? O13 Si11 O24 91.4(10) . 10_556 ? O17 Si11 O7 12.3(6) 10_556 . ? O17 Si11 O14 100.7(9) 10_556 . ? O17 Si11 O24 94.2(10) 10_556 10_556 ? O18 Si11 O7 105.9(9) 10_556 . ? O18 Si11 O14 107.9(9) 10_556 . ? O18 Si11 O17 115.9(10) 10_556 10_556 ? O18 Si11 O23 99.5(10) 10_556 10_556 ? O18 Si11 O24 127.5(12) 10_556 10_556 ? O23 Si11 O7 105.3(9) 10_556 . ? O23 Si11 O14 124.8(10) 10_556 . ? O23 Si11 O17 109.0(9) 10_556 10_556 ? O23 Si11 O24 110.4(11) 10_556 10_556 ? O24 Si11 O14 20.4(6) 10_556 . ? Si7 Si12 O8 102(4) 10_556 . ? Si7 Si12 O10 25(4) 10_556 16_545 ? Si7 Si12 O11 128(5) 10_556 6_554 ? Si7 Si12 O18 109(4) 10_556 10_556 ? Si7 Si12 O20 31(4) 10_556 10_556 ? Si7 Si12 O21 130(5) 10_556 10_556 ? Si7 Si12 O33 74(4) 10_556 . ? Si7 Si12 O34 80(4) 10_556 10_556 ? O8 Si12 O10 102.0(10) . 16_545 ? O8 Si12 O20 110.4(10) . 10_556 ? O8 Si12 O33 96.8(12) . . ? O8 Si12 O34 109.3(12) . 10_556 ? O11 Si12 O8 127.2(11) 6_554 . ? O11 Si12 O10 115.8(11) 6_554 16_545 ? O11 Si12 O20 105.9(10) 6_554 10_556 ? O11 Si12 O33 111.1(13) 6_554 . ? O11 Si12 O34 96.5(12) 6_554 10_556 ? O18 Si12 O8 17.9(6) 10_556 . ? O18 Si12 O10 100.8(9) 10_556 16_545 ? O18 Si12 O11 114.4(11) 10_556 6_554 ? O18 Si12 O20 107.0(10) 10_556 10_556 ? O18 Si12 O33 114.5(13) 10_556 . ? O18 Si12 O34 126.3(13) 10_556 10_556 ? O20 Si12 O10 10.0(8) 10_556 16_545 ? O21 Si12 O8 115.0(12) 10_556 . ? O21 Si12 O10 111.7(12) 10_556 16_545 ? O21 Si12 O11 17.8(8) 10_556 6_554 ? O21 Si12 O18 99.7(11) 10_556 10_556 ? O21 Si12 O20 102.6(11) 10_556 10_556 ? O21 Si12 O33 128.4(14) 10_556 . ? O21 Si12 O34 114.1(13) 10_556 10_556 ? O33 Si12 O10 99.0(12) . 16_545 ? O33 Si12 O20 102.9(12) . 10_556 ? O34 Si12 O10 103.5(12) 10_556 16_545 ? O34 Si12 O20 104.9(12) 10_556 10_556 ? O34 Si12 O33 14.9(11) 10_556 . ? Si8 Si13 O9 100(7) 10_556 . ? Si8 Si13 O10 8(6) 10_556 . ? Si8 Si13 O11 103(7) 10_556 10_556 ? Si8 Si13 O12 111(7) 10_556 . ? Si8 Si13 O19 98(7) 10_556 10_556 ? Si8 Si13 O20 6(6) 10_556 7 ? Si8 Si13 O21 111(7) 10_556 6_554 ? Si8 Si13 O22 109(7) 10_556 10_556 ? O9 Si13 O10 105.4(11) . . ? O9 Si13 O20 105.9(11) . 7 ? O11 Si13 O9 128.2(12) 10_556 . ? O11 Si13 O10 104.6(12) 10_556 . ? O11 Si13 O19 114.2(12) 10_556 10_556 ? O11 Si13 O20 97.5(11) 10_556 7 ? O11 Si13 O21 17.0(8) 10_556 6_554 ? O11 Si13 O22 121.0(13) 10_556 10_556 ? O12 Si13 O9 113.0(11) . . ? O12 Si13 O10 103.0(10) . . ? O12 Si13 O11 100.0(11) . 10_556 ? O12 Si13 O19 128.1(12) . 10_556 ? O12 Si13 O20 110.8(11) . 7 ? O12 Si13 O21 109.4(11) . 6_554 ? O12 Si13 O22 22.2(6) . 10_556 ? O19 Si13 O9 16.3(6) 10_556 . ? O19 Si13 O10 104.6(11) 10_556 . ? O19 Si13 O20 102.4(10) 10_556 7 ? O19 Si13 O21 97.7(11) 10_556 6_554 ? O20 Si13 O10 9.5(8) 7 . ? O21 Si13 O9 111.3(12) 6_554 . ? O21 Si13 O10 114.6(12) 6_554 . ? O21 Si13 O20 106.2(12) 6_554 7 ? O22 Si13 O9 92.4(11) 10_556 . ? O22 Si13 O10 102.0(11) 10_556 . ? O22 Si13 O19 108.3(12) 10_556 10_556 ? O22 Si13 O20 111.3(11) 10_556 7 ? O22 Si13 O21 127.5(13) 10_556 6_554 ? Si9 Si14 O6 106(7) 10_556 10_556 ? Si9 Si14 O12 122(7) 10_556 10_556 ? Si9 Si14 O15 11(6) 10_556 . ? Si9 Si14 O16 119(7) 10_556 . ? Si9 Si14 O22 109(7) 10_556 . ? Si9 Si14 O25 26(6) 10_556 10_556 ? Si9 Si14 O30 79(6) 10_556 10_556 ? Si9 Si14 O32 101(6) 10_556 . ? O6 Si14 O12 119.8(10) 10_556 10_556 ? O6 Si14 O15 97.7(11) 10_556 . ? O6 Si14 O16 13.0(6) 10_556 . ? O6 Si14 O25 103.2(10) 10_556 10_556 ? O6 Si14 O30 112.0(10) 10_556 10_556 ? O6 Si14 O32 114.0(12) 10_556 . ? O12 Si14 O15 123.7(12) 10_556 . ? O12 Si14 O16 110.9(9) 10_556 . ? O12 Si14 O25 105.1(10) 10_556 10_556 ? O12 Si14 O30 111.0(10) 10_556 10_556 ? O15 Si14 O25 20.4(7) . 10_556 ? O16 Si14 O15 110.6(11) . . ? O16 Si14 O25 115.7(10) . 10_556 ? O16 Si14 O30 110.0(10) . 10_556 ? O22 Si14 O6 114.0(10) . 10_556 ? O22 Si14 O12 21.7(6) . 10_556 ? O22 Si14 O15 107.2(12) . . ? O22 Si14 O16 109.6(10) . . ? O22 Si14 O25 87.2(11) . 10_556 ? O22 Si14 O30 128.5(11) . 10_556 ? O22 Si14 O32 112.1(12) . . ? O30 Si14 O15 88.0(10) 10_556 . ? O30 Si14 O25 103.7(10) 10_556 10_556 ? O32 Si14 O12 91.6(11) . 10_556 ? O32 Si14 O15 110.7(12) . . ? O32 Si14 O16 106.7(12) . . ? O32 Si14 O25 123.7(12) . 10_556 ? O32 Si14 O30 23.8(7) . 10_556 ? Si10 Si15 O6 79(7) 10_556 10_556 ? Si10 Si15 O7 123(7) 10_556 10_556 ? Si10 Si15 O16 92(7) 10_556 . ? Si10 Si15 O17 112(7) 10_556 . ? Si10 Si15 O27 19(7) 10_556 . ? Si10 Si15 O29 110(7) 10_556 10_556 ? Si10 Si15 O31 116(7) 10_556 . ? O6 Si15 O27 98.5(9) 10_556 . ? O7 Si15 O6 108.8(10) 10_556 10_556 ? O7 Si15 O16 103.2(10) 10_556 . ? O7 Si15 O27 114.1(9) 10_556 . ? O7 Si15 O29 114.0(13) 10_556 10_556 ? O7 Si15 O31 113.0(14) 10_556 . ? O16 Si15 O6 12.9(6) . 10_556 ? O16 Si15 O27 111.3(10) . . ? O16 Si15 O29 111.4(14) . 10_556 ? O16 Si15 O31 103.6(14) . . ? O17 Si15 O6 115.2(10) . 10_556 ? O17 Si15 O7 13.0(6) . 10_556 ? O17 Si15 O16 111.9(10) . . ? O17 Si15 O27 101.4(9) . . ? O17 Si15 O29 116.8(13) . 10_556 ? O17 Si15 O31 118.0(14) . . ? O29 Si15 O6 117.3(13) 10_556 10_556 ? O29 Si15 O27 103.1(12) 10_556 . ? O31 Si15 O6 110.6(14) . 10_556 ? O31 Si15 O27 110.8(13) . . ? O31 Si15 O29 9.0(16) . 10_556 ? O15 Si16 O15 87.7(16) 10_556 . ? O15 Si16 O25 21.9(7) . 10_556 ? O15 Si16 O25 21.9(7) 10_556 . ? O15 Si16 O25 108.1(12) . . ? O15 Si16 O25 108.1(12) 10_556 10_556 ? O15 Si16 O26 119.7(9) . . ? O15 Si16 O26 119.7(9) 10_556 10_556 ? O15 Si16 O26 105.8(9) . 10_556 ? O15 Si16 O26 105.8(9) 10_556 . ? O15 Si16 O28 124.0(9) 10_556 . ? O15 Si16 O28 108.6(9) 10_556 10_556 ? O15 Si16 O28 124.0(9) . 10_556 ? O15 Si16 O28 108.6(9) . . ? O25 Si16 O25 126.7(12) . 10_556 ? O25 Si16 O28 90.1(7) . 10_556 ? O25 Si16 O28 108.1(7) . . ? O25 Si16 O28 90.1(7) 10_556 . ? O25 Si16 O28 108.1(7) 10_556 10_556 ? O26 Si16 O25 118.9(7) . 10_556 ? O26 Si16 O25 118.9(7) 10_556 . ? O26 Si16 O25 101.2(7) 10_556 10_556 ? O26 Si16 O25 101.2(7) . . ? O26 Si16 O26 18.6(10) . 10_556 ? O26 Si16 O28 110.4(7) 10_556 10_556 ? O26 Si16 O28 107.0(7) . 10_556 ? O26 Si16 O28 107.0(7) 10_556 . ? O26 Si16 O28 110.4(7) . . ? O28 Si16 O28 19.9(8) . 10_556 ? O14 Si17 O14 120.9(10) 10_556 . ? O24 Si17 O14 106.7(10) . . ? O24 Si17 O14 21.9(7) 10_556 . ? O24 Si17 O14 106.7(10) 10_556 10_556 ? O24 Si17 O14 21.9(7) . 10_556 ? O24 Si17 O24 88.6(15) 10_556 . ? O24 Si17 O26 114.3(9) . 16_545 ? O24 Si17 O26 114.3(9) 10_556 7_545 ? O24 Si17 O26 100.6(9) 10_556 16_545 ? O24 Si17 O26 100.6(9) . 7_545 ? O24 Si17 O35 112.4(11) 10_556 10_556 ? O24 Si17 O35 128.7(11) 10_556 . ? O24 Si17 O35 112.4(11) . . ? O24 Si17 O35 128.7(11) . 10_556 ? O26 Si17 O14 120.8(7) 7_545 . ? O26 Si17 O14 103.2(7) 7_545 10_556 ? O26 Si17 O14 120.8(7) 16_545 10_556 ? O26 Si17 O14 103.2(7) 16_545 . ? O26 Si17 O26 18.7(10) 16_545 7_545 ? O26 Si17 O35 110.6(9) 7_545 10_556 ? O26 Si17 O35 110.6(9) 16_545 . ? O26 Si17 O35 107.2(8) 7_545 . ? O26 Si17 O35 107.2(8) 16_545 10_556 ? O35 Si17 O14 108.9(9) 10_556 10_556 ? O35 Si17 O14 108.9(9) . . ? O35 Si17 O14 91.2(9) . 10_556 ? O35 Si17 O14 91.2(9) 10_556 . ? O35 Si17 O35 20.1(14) . 10_556 ? Si5 O1 Si1 23.1(8) 14_446 5_445 ? Si5 O1 Si1 146.2(14) 6_554 5_445 ? Si5 O1 Si5 123.1(16) 14_446 6_554 ? Si5 O1 O1 81.1(19) 14_446 9 ? Si5 O1 O5 83.9(17) 14_446 10_556 ? O1 O1 Si1 104(2) 9 5_445 ? O1 O1 Si5 42.0(12) 9 6_554 ? O5 O1 Si1 60.8(13) 10_556 5_445 ? O5 O1 Si5 153.0(19) 10_556 6_554 ? O5 O1 O1 165(3) 10_556 9 ? Si1 O2 Si2 155.2(15) . 5 ? Si1 O2 Si5 12.0(5) . 10_556 ? Si2 O2 Si5 143.2(13) 5 10_556 ? Si4 O2 Si1 125.6(15) 14_556 . ? Si4 O2 Si2 29.7(6) 14_556 5 ? Si4 O2 Si5 113.6(12) 14_556 10_556 ? Si4 O2 O5 66.2(13) 14_556 14_556 ? O4 O2 Si1 160.3(19) 10_556 . ? O4 O2 Si2 44.5(11) 10_556 5 ? O4 O2 Si4 74.2(14) 10_556 14_556 ? O4 O2 Si5 172.2(17) 10_556 10_556 ? O4 O2 O5 140(2) 10_556 14_556 ? O5 O2 Si1 59.4(12) 14_556 . ? O5 O2 Si2 95.8(15) 14_556 5 ? O5 O2 Si5 47.4(11) 14_556 10_556 ? Si2 O3 Si3 148.8(16) . 5_445 ? Si3 O3 Si2 117.5(16) 14_446 . ? Si3 O3 Si3 31.2(8) 14_446 5_445 ? Si3 O3 O3 80.4(10) 14_446 10_556 ? Si3 O3 O4 73.6(15) 14_446 14_446 ? O3 O3 Si2 162.1(9) 10_556 . ? O3 O3 Si3 49.2(8) 10_556 5_445 ? O3 O3 O4 154.0(12) 10_556 14_446 ? O4 O3 Si2 43.9(11) 14_446 . ? O4 O3 Si3 104.8(16) 14_446 5_445 ? Si2 O4 Si3 123.7(16) 14_556 . ? Si2 O4 Si4 28.9(7) 14_556 5 ? Si2 O4 O2 85.6(16) 14_556 10_556 ? Si2 O4 O3 75.6(15) 14_556 14_556 ? Si4 O4 Si3 152.6(15) 5 . ? O2 O4 Si3 150.8(18) 10_556 . ? O2 O4 Si4 56.6(12) 10_556 5 ? O2 O4 O3 161(2) 10_556 14_556 ? O3 O4 Si3 48.0(11) 14_556 . ? O3 O4 Si4 104.6(16) 14_556 5 ? Si1 O5 Si2 106.3(12) 14_446 10_556 ? Si1 O5 Si4 115.1(15) 14_446 . ? Si1 O5 Si5 27.4(6) 14_446 5_445 ? Si4 O5 Si2 8.8(5) . 10_556 ? Si4 O5 Si5 142.6(16) . 5_445 ? Si5 O5 Si2 133.8(13) 5_445 10_556 ? O1 O5 Si1 70.0(14) 10_556 14_446 ? O1 O5 Si2 176.3(19) 10_556 10_556 ? O1 O5 Si4 175(2) 10_556 . ? O1 O5 Si5 42.6(11) 10_556 5_445 ? O1 O5 O2 132(2) 10_556 14_446 ? O2 O5 Si1 62.5(12) 14_446 14_446 ? O2 O5 Si2 43.9(10) 14_446 10_556 ? O2 O5 Si4 52.7(11) 14_446 . ? O2 O5 Si5 89.9(15) 14_446 5_445 ? Si9 O6 Si15 149.6(10) . 10_556 ? Si10 O6 Si9 148.2(11) . . ? Si10 O6 Si15 7.2(7) . 10_556 ? Si14 O6 Si9 7.2(7) 10_556 . ? Si14 O6 Si10 149.5(11) 10_556 . ? Si14 O6 Si15 149.2(11) 10_556 10_556 ? O16 O6 Si9 102(4) 10_556 . ? O16 O6 Si10 82(4) 10_556 . ? O16 O6 Si14 95(4) 10_556 10_556 ? O16 O6 Si15 75(4) 10_556 10_556 ? Si6 O7 Si10 134.9(11) 10_556 . ? Si6 O7 Si11 7.2(7) 10_556 . ? Si11 O7 Si10 139.6(10) . . ? Si15 O7 Si6 135.9(11) 10_556 10_556 ? Si15 O7 Si10 5.8(7) 10_556 . ? Si15 O7 Si11 139.8(11) 10_556 . ? O17 O7 Si6 72(4) 10_556 10_556 ? O17 O7 Si10 74(4) 10_556 . ? O17 O7 Si11 80(4) 10_556 . ? O17 O7 Si15 79(4) 10_556 10_556 ? Si7 O8 Si6 137.1(10) 10_556 10_556 ? Si11 O8 Si6 5.7(7) . 10_556 ? Si11 O8 Si7 133.8(10) . 10_556 ? Si11 O8 Si12 138.9(11) . . ? Si12 O8 Si6 143.0(11) . 10_556 ? Si12 O8 Si7 8.9(6) . 10_556 ? O18 O8 Si6 87(2) 10_556 10_556 ? O18 O8 Si7 77(2) 10_556 10_556 ? O18 O8 Si11 82(2) 10_556 . ? O18 O8 Si12 73(2) 10_556 . ? Si1 O9 Si5 25.0(4) . 10_556 ? Si1 O9 Si8 134.8(11) . 10_556 ? Si1 O9 Si13 141.9(12) . . ? Si8 O9 Si5 124.7(10) 10_556 10_556 ? Si13 O9 Si5 129.4(11) . 10_556 ? Si13 O9 Si8 7.5(8) . 10_556 ? O19 O9 Si1 81(3) 10_556 . ? O19 O9 Si5 57(3) 10_556 10_556 ? O19 O9 Si8 79(3) 10_556 10_556 ? O19 O9 Si13 79(3) 10_556 . ? Si7 O10 Si8 137.0(15) 7 10_556 ? Si7 O10 Si12 4.1(7) 7 16 ? Si7 O10 Si13 137.6(14) 7 . ? Si8 O10 Si12 136.1(14) 10_556 16 ? Si8 O10 Si13 1.2(9) 10_556 . ? Si12 O10 Si13 136.7(14) 16 . ? O20 O10 Si7 76(6) 7 7 ? O20 O10 Si8 63(6) 7 10_556 ? O20 O10 Si12 74(6) 7 16 ? O20 O10 Si13 64(6) 7 . ? Si8 O11 Si7 146.6(12) . 13_556 ? Si12 O11 Si7 7.0(7) 6 13_556 ? Si12 O11 Si8 152.2(13) 6 . ? Si12 O11 Si13 155.5(13) 6 10_556 ? Si13 O11 Si7 151.1(12) 10_556 13_556 ? Si13 O11 Si8 7.7(8) 10_556 . ? O21 O11 Si7 76(3) 13_556 13_556 ? O21 O11 Si8 94(3) 13_556 . ? O21 O11 Si12 74(3) 13_556 6 ? O21 O11 Si13 90(3) 13_556 10_556 ? Si8 O12 Si9 139.0(10) 10_556 . ? Si13 O12 Si8 7.2(8) . 10_556 ? Si13 O12 Si9 143.6(11) . . ? Si13 O12 Si14 149.0(11) . 10_556 ? Si14 O12 Si8 144.8(10) 10_556 10_556 ? Si14 O12 Si9 6.0(8) 10_556 . ? O22 O12 Si8 79(2) 10_556 10_556 ? O22 O12 Si9 70.5(19) 10_556 . ? O22 O12 Si13 79(2) 10_556 . ? O22 O12 Si14 73.7(19) 10_556 10_556 ? Si2 O13 Si4 28.3(5) . 10_556 ? Si6 O13 Si2 173.3(12) 10_556 . ? Si6 O13 Si4 157.3(11) 10_556 10_556 ? Si11 O13 Si2 174.7(12) . . ? Si11 O13 Si4 149.7(11) . 10_556 ? Si11 O13 Si6 7.6(7) . 10_556 ? O23 O13 Si2 98(2) 10_556 . ? O23 O13 Si4 71(2) 10_556 10_556 ? O23 O13 Si6 88(2) 10_556 10_556 ? O23 O13 Si11 82(2) 10_556 . ? Si6 O14 Si11 5.8(7) 10_556 . ? Si6 O14 Si17 145.6(11) 10_556 . ? Si17 O14 Si11 148.3(11) . . ? O24 O14 Si6 74(2) 10_556 10_556 ? O24 O14 Si11 79(2) 10_556 . ? O24 O14 Si17 72(2) 10_556 . ? Si9 O15 Si14 1.5(9) 10_556 . ? Si9 O15 Si16 165.9(17) 10_556 . ? Si16 O15 Si14 165.7(16) . . ? O25 O15 Si9 80(3) 10_556 10_556 ? O25 O15 Si14 80(2) 10_556 . ? O25 O15 Si16 86(3) 10_556 . ? Si10 O16 Si9 137.3(11) 10_556 10_556 ? Si10 O16 Si14 142.1(11) 10_556 . ? Si14 O16 Si9 6.1(7) . 10_556 ? Si15 O16 Si9 142.9(11) . 10_556 ? Si15 O16 Si10 7.4(7) . 10_556 ? Si15 O16 Si14 147.0(11) . . ? O6 O16 Si9 66(4) 10_556 10_556 ? O6 O16 Si10 85(4) 10_556 10_556 ? O6 O16 Si14 72(4) 10_556 . ? O6 O16 Si15 92(4) 10_556 . ? Si6 O17 Si10 147.9(10) . 10_556 ? Si6 O17 Si11 6.9(7) . 10_556 ? Si6 O17 Si15 145.8(11) . . ? Si10 O17 Si11 148.8(10) 10_556 10_556 ? Si15 O17 Si10 6.7(7) . 10_556 ? Si15 O17 Si11 145.3(10) . 10_556 ? O7 O17 Si6 95(4) 10_556 . ? O7 O17 Si10 94(4) 10_556 10_556 ? O7 O17 Si11 88(4) 10_556 10_556 ? O7 O17 Si15 88(4) 10_556 . ? Si7 O18 Si6 136.6(10) . . ? Si11 O18 Si6 3.9(7) 10_556 . ? Si11 O18 Si7 136.9(10) 10_556 . ? Si12 O18 Si6 145.3(10) 10_556 . ? Si12 O18 Si7 8.8(6) 10_556 . ? Si12 O18 Si11 145.7(11) 10_556 10_556 ? O8 O18 Si6 76(2) 10_556 . ? O8 O18 Si7 86(2) 10_556 . ? O8 O18 Si11 80(2) 10_556 10_556 ? O8 O18 Si12 89(2) 10_556 10_556 ? Si1 O19 Si5 27.6(5) 10_556 . ? Si1 O19 Si8 137.7(10) 10_556 . ? Si1 O19 Si13 144.3(11) 10_556 10_556 ? Si5 O19 Si8 143.4(11) . . ? Si5 O19 Si13 150.7(12) . 10_556 ? Si13 O19 Si8 7.7(8) 10_556 . ? O9 O19 Si1 82(3) 10_556 10_556 ? O9 O19 Si5 109(3) 10_556 . ? O9 O19 Si8 86(3) 10_556 . ? O9 O19 Si13 84(3) 10_556 10_556 ? Si7 O20 Si12 5.2(7) . 10_556 ? Si7 O20 Si13 155.8(13) . 7_545 ? Si8 O20 Si7 156.7(14) 16_545 . ? Si8 O20 Si12 155.6(14) 16_545 10_556 ? Si8 O20 Si13 0.9(9) 16_545 7_545 ? Si13 O20 Si12 154.8(13) 7_545 10_556 ? O10 O20 Si7 92(6) 7_545 . ? O10 O20 Si8 106(6) 7_545 16_545 ? O10 O20 Si12 96(6) 7_545 10_556 ? O10 O20 Si13 106(6) 7_545 7_545 ? Si7 O21 Si8 141.7(13) . 13_556 ? Si12 O21 Si7 6.9(7) 10_556 . ? Si12 O21 Si8 147.2(14) 10_556 13_556 ? Si12 O21 Si13 153.8(15) 10_556 6 ? Si13 O21 Si7 148.5(14) 6 . ? Si13 O21 Si8 6.9(8) 6 13_556 ? O11 O21 Si7 88(3) 13_556 . ? O11 O21 Si8 70(3) 13_556 13_556 ? O11 O21 Si12 88(3) 13_556 10_556 ? O11 O21 Si13 73(3) 13_556 6 ? Si9 O22 Si8 149.7(12) 10_556 . ? Si13 O22 Si8 7.3(8) 10_556 . ? Si13 O22 Si9 155.7(13) 10_556 10_556 ? Si14 O22 Si8 152.2(13) . . ? Si14 O22 Si9 7.1(8) . 10_556 ? Si14 O22 Si13 156.9(14) . 10_556 ? O12 O22 Si8 80(2) 10_556 . ? O12 O22 Si9 89(2) 10_556 10_556 ? O12 O22 Si13 78(2) 10_556 10_556 ? O12 O22 Si14 85(2) 10_556 . ? Si4 O23 Si2 27.1(5) . 10_556 ? Si4 O23 Si6 162.2(12) . . ? Si6 O23 Si2 138.3(11) . 10_556 ? Si11 O23 Si2 143.7(11) 10_556 10_556 ? Si11 O23 Si4 164.1(12) 10_556 . ? Si11 O23 Si6 6.7(7) 10_556 . ? O13 O23 Si2 65(2) 10_556 10_556 ? O13 O23 Si4 91(3) 10_556 . ? O13 O23 Si6 74(2) 10_556 . ? O13 O23 Si11 79(2) 10_556 10_556 ? Si6 O24 Si11 4.7(8) . 10_556 ? Si6 O24 Si17 166.4(16) . . ? Si17 O24 Si11 162.1(14) . 10_556 ? O14 O24 Si6 83(2) 10_556 . ? O14 O24 Si11 81(2) 10_556 10_556 ? O14 O24 Si17 86(2) 10_556 . ? Si9 O25 Si14 3.5(8) . 10_556 ? Si9 O25 Si16 148.5(12) . . ? Si16 O25 Si14 151.8(12) . 10_556 ? O15 O25 Si9 77(3) 10_556 . ? O15 O25 Si14 80(3) 10_556 10_556 ? O15 O25 Si16 72(2) 10_556 . ? Si17 O26 Si16 161.1(10) 7 . ? O26 O26 Si16 80.7(5) 10_556 . ? O26 O26 Si17 80.6(5) 10_556 7 ? Si10 O27 Si10 156.8(12) . 10_556 ? Si10 O27 Si15 155.8(7) . . ? Si10 O27 Si15 2.6(9) 10_556 . ? Si10 O27 Si15 155.8(7) 10_556 10_556 ? Si10 O27 Si15 2.6(9) . 10_556 ? Si15 O27 Si15 154.5(10) 10_556 . ? Si3 O28 Si3 29.4(6) . 10_556 ? Si3 O28 Si16 143.8(9) . . ? Si16 O28 Si3 130.9(8) . 10_556 ? O28 O28 Si3 65.8(5) 10_556 10_556 ? O28 O28 Si3 95.2(5) 10_556 . ? O28 O28 Si16 80.0(4) 10_556 . ? Si10 O29 Si10 146(2) 12 . ? Si15 O29 Si10 6.6(7) 3 12 ? Si15 O29 Si10 150.5(19) 3 . ? Si15 O29 Si10 150.5(19) 10_556 12 ? Si15 O29 Si10 6.6(7) 10_556 . ? Si15 O29 Si15 154(2) 10_556 3 ? O31 O29 Si10 89(4) 10_556 . ? O31 O29 Si10 89(4) 10_556 12 ? O31 O29 Si15 84(3) 10_556 3 ? O31 O29 Si15 84(3) 10_556 10_556 ? Si9 O30 Si9 157.5(14) 12 . ? Si9 O30 Si14 150.1(12) . 3 ? Si9 O30 Si14 7.4(7) 12 3 ? Si9 O30 Si14 7.4(7) . 10_556 ? Si9 O30 Si14 150.1(12) 12 10_556 ? Si14 O30 Si14 142.7(13) 3 10_556 ? O32 O30 Si9 80.0(7) 10_556 . ? O32 O30 Si9 80.0(7) 10_556 12 ? O32 O30 Si14 73.1(7) 10_556 3 ? O32 O30 Si14 73.1(7) 10_556 10_556 ? Si10 O31 Si10 144(2) 3 10_556 ? Si15 O31 Si10 6.3(8) . 10_556 ? Si15 O31 Si10 150(2) 12 10_556 ? Si15 O31 Si10 6.3(8) 12 3 ? Si15 O31 Si10 150(2) . 3 ? Si15 O31 Si15 156(2) 12 . ? O29 O31 Si10 83(4) 10_556 10_556 ? O29 O31 Si10 83(4) 10_556 3 ? O29 O31 Si15 87(3) 10_556 12 ? O29 O31 Si15 87(3) 10_556 . ? Si9 O32 Si9 150.9(16) 3 10_556 ? Si14 O32 Si9 155.7(14) 12 10_556 ? Si14 O32 Si9 7.3(7) . 10_556 ? Si14 O32 Si9 155.7(14) . 3 ? Si14 O32 Si9 7.3(7) 12 3 ? Si14 O32 Si14 158.9(17) . 12 ? O30 O32 Si9 76.3(8) 10_556 10_556 ? O30 O32 Si9 76.3(8) 10_556 3 ? O30 O32 Si14 83.1(9) 10_556 . ? O30 O32 Si14 83.1(9) 10_556 12 ? Si7 O33 Si7 169(2) 10_556 3_655 ? Si7 O33 Si12 163.8(19) 10_556 12_655 ? Si7 O33 Si12 163.8(19) 3_655 . ? Si7 O33 Si12 9.2(6) 10_556 . ? Si7 O33 Si12 9.2(6) 3_655 12_655 ? Si12 O33 Si12 156(2) . 12_655 ? O34 O33 Si7 84.5(10) 10_556 3_655 ? O34 O33 Si7 84.5(10) 10_556 10_556 ? O34 O33 Si12 81.1(13) 10_556 12_655 ? O34 O33 Si12 81.1(13) 10_556 . ? Si7 O34 Si7 160.3(19) . 12_655 ? Si7 O34 Si12 162.5(18) . 3_655 ? Si7 O34 Si12 9.3(6) . 10_556 ? Si7 O34 Si12 162.5(18) 12_655 10_556 ? Si7 O34 Si12 9.3(6) 12_655 3_655 ? Si12 O34 Si12 160.0(19) 3_655 10_556 ? O33 O34 Si7 80.2(9) 10_556 12_655 ? O33 O34 Si7 80.2(9) 10_556 . ? O33 O34 Si12 84.0(13) 10_556 3_655 ? O33 O34 Si12 84.0(13) 10_556 10_556 ? Si17 O35 Si17 158.9(14) . 3_655 ? O35 O35 Si17 80.0(7) 10_556 3_655 ? O35 O35 Si17 80.0(7) 10_556 . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si1 Si4 2.590(14) 14_556 ? Si1 Si5 0.750(11) 10_556 ? Si1 O1 1.63(2) 5 ? Si1 O2 1.56(2) . ? Si1 O5 1.51(3) 14_556 ? Si1 O9 1.576(15) 12_655 ? Si1 O9 1.576(15) . ? Si1 O19 1.572(14) 10_556 ? Si1 O19 1.572(14) 3_655 ? Si2 Si3 2.398(14) 14_446 ? Si2 Si4 0.791(11) 10_556 ? Si2 O2 1.60(2) 5_445 ? Si2 O3 1.57(2) . ? Si2 O4 1.12(2) 14_446 ? Si2 O5 2.29(2) 10_556 ? Si2 O13 1.586(15) 12 ? Si2 O13 1.586(15) . ? Si2 O23 1.736(15) 3 ? Si2 O23 1.736(15) 10_556 ? Si3 Si3 0.843(17) 10_556 ? Si3 O3 1.23(2) 14_556 ? Si3 O3 1.60(2) 5 ? Si3 O4 1.59(2) . ? Si3 O28 1.567(13) 12_655 ? Si3 O28 1.711(13) 10_556 ? Si3 O28 1.567(13) . ? Si3 O28 1.711(13) 3_655 ? Si4 O2 1.35(2) 14_446 ? Si4 O4 1.56(2) 5_445 ? Si4 O5 1.56(2) . ? Si4 O13 1.644(15) 3 ? Si4 O13 1.644(15) 10_556 ? Si4 O23 1.554(14) 12 ? Si4 O23 1.554(14) . ? Si5 Si5 2.41(2) 9_666 ? Si5 O1 1.10(2) 14_556 ? Si5 O1 1.63(2) 6 ? Si5 O2 2.20(2) 10_556 ? Si5 O5 1.62(2) 5 ? Si5 O9 1.774(16) 10_556 ? Si5 O9 1.774(16) 3_655 ? Si5 O19 1.574(15) . ? Si5 O19 1.574(15) 12_655 ? Si6 Si11 0.212(19) 10_556 ? Si6 O7 1.597(19) 10_556 ? Si6 O8 1.677(17) 10_556 ? Si6 O13 1.584(18) 10_556 ? Si6 O14 1.551(17) 10_556 ? Si6 O17 1.529(18) . ? Si6 O18 1.725(17) . ? Si6 O23 1.650(18) . ? Si6 O24 1.51(2) . ? Si7 Si12 0.261(17) 10_556 ? Si7 O8 1.656(16) 10_556 ? Si7 O10 1.53(2) 7_545 ? Si7 O11 1.697(18) 13_556 ? Si7 O18 1.614(15) . ? Si7 O20 1.489(19) . ? Si7 O21 1.648(18) . ? Si7 O33 1.575(10) 10_556 ? Si7 O34 1.591(10) . ? Si8 Si13 0.22(2) 10_556 ? Si8 O9 1.656(18) 10_556 ? Si8 O10 1.58(2) 10_556 ? Si8 O11 1.591(18) . ? Si8 O12 1.619(16) 10_556 ? Si8 O19 1.627(18) . ? Si8 O20 1.47(2) 16 ? Si8 O21 1.69(2) 13_556 ? Si8 O22 1.618(19) . ? Si9 Si14 0.21(2) 10_556 ? Si9 O6 1.602(19) . ? Si9 O12 1.707(17) . ? Si9 O15 1.48(2) 10_556 ? Si9 O16 1.71(2) 10_556 ? Si9 O22 1.609(18) 10_556 ? Si9 O25 1.504(19) . ? Si9 O30 1.590(13) . ? Si9 O32 1.612(13) 10_556 ? Si10 Si15 0.20(2) 10_556 ? Si10 O6 1.597(19) . ? Si10 O7 1.679(18) . ? Si10 O16 1.588(19) 10_556 ? Si10 O17 1.619(18) 10_556 ? Si10 O27 1.494(13) . ? Si10 O29 1.656(15) . ? Si10 O31 1.668(16) 10_556 ? Si11 O7 1.651(17) . ? Si11 O8 1.538(16) . ? Si11 O13 1.543(17) . ? Si11 O14 1.685(16) . ? Si11 O17 1.626(17) 10_556 ? Si11 O18 1.545(15) 10_556 ? Si11 O23 1.552(16) 10_556 ? Si11 O24 1.67(2) 10_556 ? Si12 O8 1.581(16) . ? Si12 O10 1.77(2) 16_545 ? Si12 O11 1.525(18) 6_554 ? Si12 O18 1.512(16) 10_556 ? Si12 O20 1.71(2) 10_556 ? Si12 O21 1.467(19) 10_556 ? Si12 O33 1.625(12) . ? Si12 O34 1.614(12) 10_556 ? Si13 O9 1.60(2) . ? Si13 O10 1.80(2) . ? Si13 O11 1.53(2) 10_556 ? Si13 O12 1.526(18) . ? Si13 O19 1.583(19) 10_556 ? Si13 O20 1.68(2) 7 ? Si13 O21 1.59(2) 6_554 ? Si13 O22 1.53(2) 10_556 ? Si14 O6 1.531(19) 10_556 ? Si14 O12 1.587(15) 10_556 ? Si14 O15 1.69(2) . ? Si14 O16 1.60(2) . ? Si14 O22 1.530(19) . ? Si14 O25 1.689(18) 10_556 ? Si14 O30 1.617(13) 10_556 ? Si14 O32 1.559(12) . ? Si15 O6 1.622(18) 10_556 ? Si15 O7 1.558(18) 10_556 ? Si15 O16 1.567(19) . ? Si15 O17 1.532(18) . ? Si15 O27 1.685(12) . ? Si15 O29 1.576(13) 10_556 ? Si15 O31 1.570(14) . ? Si16 O15 1.520(19) 10_556 ? Si16 O15 1.520(19) . ? Si16 O25 1.594(13) . ? Si16 O25 1.594(13) 10_556 ? Si16 O26 1.592(14) 10_556 ? Si16 O26 1.592(14) . ? Si16 O28 1.616(12) . ? Si16 O28 1.616(12) 10_556 ? Si17 O14 1.597(13) 10_556 ? Si17 O14 1.598(13) . ? Si17 O24 1.523(18) 10_556 ? Si17 O24 1.523(18) . ? Si17 O26 1.580(13) 16_545 ? Si17 O26 1.580(13) 7_545 ? Si17 O35 1.581(6) . ? Si17 O35 1.581(6) 10_556 ? O1 O1 1.38(4) 9 ? O1 O5 1.31(3) 10_556 ? O2 O4 1.23(3) 10_556 ? O2 O5 1.49(3) 14_556 ? O3 O3 1.25(4) 10_556 ? O3 O4 1.41(3) 14_446 ? O6 O16 0.362(18) 10_556 ? O7 O17 0.351(17) 10_556 ? O8 O18 0.487(15) 10_556 ? O9 O19 0.453(16) 10_556 ? O10 O20 0.31(2) 7 ? O11 O21 0.47(2) 13_556 ? O12 O22 0.590(15) 10_556 ? O13 O23 0.514(15) 10_556 ? O14 O24 0.596(18) 10_556 ? O15 O25 0.597(19) 10_556 ? O26 O26 0.51(3) 10_556 ? O28 O28 0.56(2) 10_556 ? O29 O31 0.25(4) 10_556 ? O30 O32 0.657(19) 10_556 ? O33 O34 0.42(3) 10_556 ? O35 O35 0.55(4) 10_556 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Si1 Si4 O5 Si2 0.000(15) 14_446 . . 10_556 ? Si1 Si4 O5 Si5 0.000(2) 14_446 . . 5_445 ? Si1 Si4 O5 O2 0.000(4) 14_446 . . 14_446 ? Si1 Si4 O23 Si2 127.8(11) 14_446 . . 10_556 ? Si1 Si4 O23 Si6 84(4) 14_446 . . . ? Si1 Si4 O23 Si11 61(5) 14_446 . . 10_556 ? Si1 Si4 O23 O13 113(2) 14_446 . . 10_556 ? Si1 Si5 O19 Si8 -96(2) 10_556 . . . ? Si1 Si5 O19 Si13 -100(3) 10_556 . . 10_556 ? Si1 Si5 O19 O9 13(3) 10_556 . . 10_556 ? Si2 Si3 O4 Si4 0.000(5) 14_556 . . 5 ? Si2 Si3 O4 O2 180.000(15) 14_556 . . 10_556 ? Si2 Si3 O4 O3 0.000(11) 14_556 . . 14_556 ? Si2 Si3 O28 Si3 139.6(5) 14_556 . . 10_556 ? Si2 Si3 O28 Si16 59.4(15) 14_556 . . . ? Si2 Si3 O28 O28 139.6(5) 14_556 . . 10_556 ? Si2 Si4 O5 Si1 0.000(6) 10_556 . . 14_446 ? Si2 Si4 O5 Si5 0.000(7) 10_556 . . 5_445 ? Si2 Si4 O5 O2 0.000(5) 10_556 . . 14_446 ? Si2 Si4 O23 Si6 -44(4) 10_556 . . . ? Si2 Si4 O23 Si11 -66(4) 10_556 . . 10_556 ? Si2 Si4 O23 O13 -14(3) 10_556 . . 10_556 ? Si3 Si2 O3 Si3 0.000(1) 14_446 . . 5_445 ? Si3 Si2 O3 O3 180.000(9) 14_446 . . 10_556 ? Si3 Si2 O3 O4 0.000(3) 14_446 . . 14_446 ? Si3 Si2 O13 Si4 143.3(12) 14_446 . . 10_556 ? Si3 Si2 O13 O23 158(2) 14_446 . . 10_556 ? Si3 Si3 O4 Si2 0.000(11) 10_556 . . 14_556 ? Si3 Si3 O4 Si4 0.000(14) 10_556 . . 5 ? Si3 Si3 O4 O2 180.000(10) 10_556 . . 10_556 ? Si3 Si3 O4 O3 0.000(9) 10_556 . . 14_556 ? Si3 Si3 O28 Si16 -80.2(13) 10_556 . . . ? Si3 Si3 O28 O28 0.000(2) 10_556 . . 10_556 ? Si4 Si1 O2 Si2 0.000(4) 14_556 . . 5 ? Si4 Si1 O2 Si5 0.000(14) 14_556 . . 10_556 ? Si4 Si1 O2 O4 180.000(14) 14_556 . . 10_556 ? Si4 Si1 O2 O5 0.000(7) 14_556 . . 14_556 ? Si4 Si1 O9 Si5 123.3(13) 14_556 . . 10_556 ? Si4 Si1 O9 Si8 46.7(17) 14_556 . . 10_556 ? Si4 Si1 O9 Si13 51(2) 14_556 . . . ? Si4 Si1 O9 O19 111(3) 14_556 . . 10_556 ? Si4 Si2 O3 Si3 0.000(7) 10_556 . . 5_445 ? Si4 Si2 O3 Si3 0.000(7) 10_556 . . 14_446 ? Si4 Si2 O3 O3 180.000(4) 10_556 . . 10_556 ? Si4 Si2 O3 O4 0.000(5) 10_556 . . 14_446 ? Si4 Si2 O13 O23 15(3) 10_556 . . 10_556 ? Si5 Si1 O2 Si2 0.000(8) 10_556 . . 5 ? Si5 Si1 O2 Si4 0.000(5) 10_556 . . 14_556 ? Si5 Si1 O2 O4 180.000(10) 10_556 . . 10_556 ? Si5 Si1 O2 O5 0.000(4) 10_556 . . 14_556 ? Si5 Si1 O9 Si8 -76.6(18) 10_556 . . 10_556 ? Si5 Si1 O9 Si13 -73(2) 10_556 . . . ? Si5 Si1 O9 O19 -12(3) 10_556 . . 10_556 ? Si5 Si5 O19 Si1 157.5(16) 9_666 . . 10_556 ? Si5 Si5 O19 Si8 62(2) 9_666 . . . ? Si5 Si5 O19 Si13 57(3) 9_666 . . 10_556 ? Si5 Si5 O19 O9 171(3) 9_666 . . 10_556 ? Si6 Si11 O7 Si10 -52(6) 10_556 . . . ? Si6 Si11 O7 Si15 -61(6) 10_556 . . 10_556 ? Si6 Si11 O7 O17 -2(7) 10_556 . . 10_556 ? Si6 Si11 O8 Si7 128(8) 10_556 . . 10_556 ? Si6 Si11 O8 Si12 138(8) 10_556 . . . ? Si6 Si11 O8 O18 -170(9) 10_556 . . 10_556 ? Si6 Si11 O13 Si4 176(6) 10_556 . . 10_556 ? Si6 Si11 O13 O23 152(7) 10_556 . . 10_556 ? Si6 Si11 O14 Si17 66(8) 10_556 . . . ? Si6 Si11 O14 O24 43(8) 10_556 . . 10_556 ? Si7 Si12 O8 Si6 -53(5) 10_556 . . 10_556 ? Si7 Si12 O8 Si11 -59(5) 10_556 . . . ? Si7 Si12 O8 O18 -113(5) 10_556 . . 10_556 ? Si7 Si12 O33 Si7 139(8) 10_556 . . 3_655 ? Si7 Si12 O33 Si12 154(5) 10_556 . . 12_655 ? Si7 Si12 O33 O34 112(7) 10_556 . . 10_556 ? Si8 Si13 O9 Si1 -22(7) 10_556 . . . ? Si8 Si13 O9 Si5 -53(7) 10_556 . . 10_556 ? Si8 Si13 O9 O19 -83(7) 10_556 . . 10_556 ? Si8 Si13 O10 Si7 63(44) 10_556 . . 7 ? Si8 Si13 O10 Si12 57(44) 10_556 . . 16 ? Si8 Si13 O10 O20 40(44) 10_556 . . 7 ? Si8 Si13 O12 Si9 -54(8) 10_556 . . . ? Si8 Si13 O12 Si14 -59(8) 10_556 . . 10_556 ? Si8 Si13 O12 O22 -89(7) 10_556 . . 10_556 ? Si9 Si14 O15 Si16 101(37) 10_556 . . . ? Si9 Si14 O15 O25 110(37) 10_556 . . 10_556 ? Si9 Si14 O16 Si10 -42(8) 10_556 . . 10_556 ? Si9 Si14 O16 Si15 -52(8) 10_556 . . . ? Si9 Si14 O16 O6 13(8) 10_556 . . 10_556 ? Si9 Si14 O22 Si8 76(8) 10_556 . . . ? Si9 Si14 O22 Si13 89(8) 10_556 . . 10_556 ? Si9 Si14 O22 O12 131(7) 10_556 . . 10_556 ? Si9 Si14 O32 Si9 55(8) 10_556 . . 3 ? Si9 Si14 O32 Si14 72(10) 10_556 . . 12 ? Si9 Si14 O32 O30 23(8) 10_556 . . 10_556 ? Si10 Si15 O16 Si9 44(7) 10_556 . . 10_556 ? Si10 Si15 O16 Si14 52(7) 10_556 . . . ? Si10 Si15 O16 O6 -7(8) 10_556 . . 10_556 ? Si10 Si15 O17 Si6 -113(8) 10_556 . . . ? Si10 Si15 O17 Si11 -125(7) 10_556 . . 10_556 ? Si10 Si15 O17 O7 152(8) 10_556 . . 10_556 ? Si10 Si15 O27 Si10 -116(20) 10_556 . . . ? Si10 Si15 O27 Si15 -121(18) 10_556 . . 10_556 ? Si10 Si15 O31 Si10 -19(9) 10_556 . . 3 ? Si10 Si15 O31 Si15 -24(11) 10_556 . . 12 ? Si10 Si15 O31 O29 52(15) 10_556 . . 10_556 ? Si11 Si6 O17 Si10 -103(7) 10_556 . . 10_556 ? Si11 Si6 O17 Si15 -91(7) 10_556 . . . ? Si11 Si6 O17 O7 2(7) 10_556 . . 10_556 ? Si11 Si6 O18 Si7 96(12) 10_556 . . . ? Si11 Si6 O18 Si12 98(12) 10_556 . . 10_556 ? Si11 Si6 O18 O8 165(12) 10_556 . . 10_556 ? Si11 Si6 O23 Si2 -146(7) 10_556 . . 10_556 ? Si11 Si6 O23 Si4 -117(7) 10_556 . . . ? Si11 Si6 O23 O13 -148(8) 10_556 . . 10_556 ? Si11 Si6 O24 Si17 -24(13) 10_556 . . . ? Si11 Si6 O24 O14 -61(10) 10_556 . . 10_556 ? Si12 Si7 O18 Si6 174(5) 10_556 . . . ? Si12 Si7 O18 Si11 180(5) 10_556 . . 10_556 ? Si12 Si7 O18 O8 108(5) 10_556 . . 10_556 ? Si12 Si7 O20 Si8 -83(8) 10_556 . . 16_545 ? Si12 Si7 O20 Si13 -84(8) 10_556 . . 7_545 ? Si12 Si7 O20 O10 135(9) 10_556 . . 7_545 ? Si12 Si7 O21 Si8 -146(6) 10_556 . . 13_556 ? Si12 Si7 O21 Si13 -144(6) 10_556 . . 6 ? Si12 Si7 O21 O11 -92(7) 10_556 . . 13_556 ? Si12 Si7 O34 Si7 -117(6) 10_556 . . 12_655 ? Si12 Si7 O34 Si12 -88(7) 10_556 . . 3_655 ? Si12 Si7 O34 O33 -113(7) 10_556 . . 10_556 ? Si13 Si8 O11 Si7 131(7) 10_556 . . 13_556 ? Si13 Si8 O11 Si12 122(7) 10_556 . . 6 ? Si13 Si8 O11 O21 61(8) 10_556 . . 13_556 ? Si13 Si8 O19 Si1 153(6) 10_556 . . 10_556 ? Si13 Si8 O19 Si5 -164(6) 10_556 . . . ? Si13 Si8 O19 O9 79(7) 10_556 . . 10_556 ? Si13 Si8 O22 Si9 149(7) 10_556 . . 10_556 ? Si13 Si8 O22 Si14 136(7) 10_556 . . . ? Si13 Si8 O22 O12 79(7) 10_556 . . 10_556 ? Si14 Si9 O6 Si10 -107(7) 10_556 . . . ? Si14 Si9 O6 Si15 -93(7) 10_556 . . 10_556 ? Si14 Si9 O6 O16 -12(8) 10_556 . . 10_556 ? Si14 Si9 O12 Si8 -167(7) 10_556 . . 10_556 ? Si14 Si9 O12 Si13 -158(7) 10_556 . . . ? Si14 Si9 O12 O22 -121(8) 10_556 . . 10_556 ? Si14 Si9 O25 Si16 -163(15) 10_556 . . . ? Si14 Si9 O25 O15 -156(16) 10_556 . . 10_556 ? Si14 Si9 O30 Si9 5(10) 10_556 . . 12 ? Si14 Si9 O30 Si14 4(7) 10_556 . . 3 ? Si14 Si9 O30 O32 -22(8) 10_556 . . 10_556 ? Si15 Si10 O6 Si9 107(7) 10_556 . . . ? Si15 Si10 O6 Si14 93(7) 10_556 . . 10_556 ? Si15 Si10 O6 O16 7(8) 10_556 . . 10_556 ? Si15 Si10 O7 Si6 -103(9) 10_556 . . 10_556 ? Si15 Si10 O7 Si11 -95(9) 10_556 . . . ? Si15 Si10 O7 O17 -147(10) 10_556 . . 10_556 ? Si15 Si10 O27 Si10 -70(20) 10_556 . . 10_556 ? Si15 Si10 O27 Si15 -64(19) 10_556 . . . ? Si15 Si10 O29 Si10 -133(8) 10_556 . . 12 ? Si15 Si10 O29 Si15 -124(9) 10_556 . . 3 ? Si15 Si10 O29 O31 -48(14) 10_556 . . 10_556 ? O1 Si1 O2 Si2 0.000(5) 5 . . 5 ? O1 Si1 O2 Si4 0.000(2) 5 . . 14_556 ? O1 Si1 O2 Si5 0.000(9) 5 . . 10_556 ? O1 Si1 O2 O4 180.000(10) 5 . . 10_556 ? O1 Si1 O2 O5 0.000(3) 5 . . 14_556 ? O1 Si1 O9 Si5 30.6(11) 5 . . 10_556 ? O1 Si1 O9 Si8 -46.0(18) 5 . . 10_556 ? O1 Si1 O9 Si13 -42(2) 5 . . . ? O1 Si1 O9 O19 18(3) 5 . . 10_556 ? O1 Si5 O19 Si1 178.8(15) 6 . . 10_556 ? O1 Si5 O19 Si1 119(2) 14_556 . . 10_556 ? O1 Si5 O19 Si8 23(3) 14_556 . . . ? O1 Si5 O19 Si8 83(2) 6 . . . ? O1 Si5 O19 Si13 79(3) 6 . . 10_556 ? O1 Si5 O19 Si13 19(3) 14_556 . . 10_556 ? O1 Si5 O19 O9 -168(3) 6 . . 10_556 ? O1 Si5 O19 O9 133(3) 14_556 . . 10_556 ? O2 Si1 O9 Si5 148.2(15) . . . 10_556 ? O2 Si1 O9 Si8 71.6(17) . . . 10_556 ? O2 Si1 O9 Si13 75(2) . . . . ? O2 Si1 O9 O19 136(3) . . . 10_556 ? O2 Si2 O3 Si3 0.000(1) 5_445 . . 14_446 ? O2 Si2 O3 Si3 0.000(3) 5_445 . . 5_445 ? O2 Si2 O3 O3 180.000(7) 5_445 . . 10_556 ? O2 Si2 O3 O4 0.000(1) 5_445 . . 14_446 ? O2 Si2 O13 Si4 49.5(11) 5_445 . . 10_556 ? O2 Si2 O13 O23 64(3) 5_445 . . 10_556 ? O2 Si4 O5 Si1 0.000(1) 14_446 . . 14_446 ? O2 Si4 O5 Si2 0.000(13) 14_446 . . 10_556 ? O2 Si4 O5 Si5 0.000(2) 14_446 . . 5_445 ? O2 Si4 O23 Si2 92.7(16) 14_446 . . 10_556 ? O2 Si4 O23 Si6 49(4) 14_446 . . . ? O2 Si4 O23 Si11 26(5) 14_446 . . 10_556 ? O2 Si4 O23 O13 78(3) 14_446 . . 10_556 ? O2 Si5 O19 Si1 21.7(10) 10_556 . . 10_556 ? O2 Si5 O19 Si8 -74.1(19) 10_556 . . . ? O2 Si5 O19 Si13 -78(2) 10_556 . . 10_556 ? O2 Si5 O19 O9 35(3) 10_556 . . 10_556 ? O3 Si2 O13 Si4 169.7(14) . . . 10_556 ? O3 Si2 O13 O23 -176(3) . . . 10_556 ? O3 Si3 O4 Si2 0.000(4) 5 . . 14_556 ? O3 Si3 O4 Si2 0.000(3) 14_556 . . 14_556 ? O3 Si3 O4 Si4 0.000(5) 14_556 . . 5 ? O3 Si3 O4 Si4 0.000(7) 5 . . 5 ? O3 Si3 O4 O2 180.000(10) 14_556 . . 10_556 ? O3 Si3 O4 O2 180.000(9) 5 . . 10_556 ? O3 Si3 O4 O3 0.000(5) 5 . . 14_556 ? O3 Si3 O28 Si3 41.3(9) 5 . . 10_556 ? O3 Si3 O28 Si3 98.1(14) 14_556 . . 10_556 ? O3 Si3 O28 Si16 -38.9(17) 5 . . . ? O3 Si3 O28 Si16 18(2) 14_556 . . . ? O3 Si3 O28 O28 41.3(9) 5 . . 10_556 ? O3 Si3 O28 O28 98.1(14) 14_556 . . 10_556 ? O4 Si2 O3 Si3 0.000(1) 14_446 . . 14_446 ? O4 Si2 O3 Si3 0.000(2) 14_446 . . 5_445 ? O4 Si2 O3 O3 180.000(8) 14_446 . . 10_556 ? O4 Si2 O13 Si4 104.7(18) 14_446 . . 10_556 ? O4 Si2 O13 O23 119(3) 14_446 . . 10_556 ? O4 Si3 O28 Si3 161.6(8) . . . 10_556 ? O4 Si3 O28 Si16 81.4(15) . . . . ? O4 Si3 O28 O28 161.6(8) . . . 10_556 ? O4 Si4 O5 Si1 0.000(2) 5_445 . . 14_446 ? O4 Si4 O5 Si2 0.000(11) 5_445 . . 10_556 ? O4 Si4 O5 Si5 0.000(4) 5_445 . . 5_445 ? O4 Si4 O5 O2 0.000(2) 5_445 . . 14_446 ? O4 Si4 O23 Si2 36.6(10) 5_445 . . 10_556 ? O4 Si4 O23 Si6 -7(4) 5_445 . . . ? O4 Si4 O23 Si11 -30(5) 5_445 . . 10_556 ? O4 Si4 O23 O13 22(3) 5_445 . . 10_556 ? O5 Si1 O2 Si2 0.000(4) 14_556 . . 5 ? O5 Si1 O2 Si4 0.000(2) 14_556 . . 14_556 ? O5 Si1 O2 Si5 0.000(11) 14_556 . . 10_556 ? O5 Si1 O2 O4 180.000(12) 14_556 . . 10_556 ? O5 Si1 O9 Si5 84.9(16) 14_556 . . 10_556 ? O5 Si1 O9 Si8 8(2) 14_556 . . 10_556 ? O5 Si1 O9 Si13 12(2) 14_556 . . . ? O5 Si1 O9 O19 72(3) 14_556 . . 10_556 ? O5 Si2 O3 Si3 0.000(3) 10_556 . . 14_446 ? O5 Si2 O3 Si3 0.000(4) 10_556 . . 5_445 ? O5 Si2 O3 O3 180.000(6) 10_556 . . 10_556 ? O5 Si2 O3 O4 0.000(2) 10_556 . . 14_446 ? O5 Si2 O13 Si4 14.6(9) 10_556 . . 10_556 ? O5 Si2 O13 O23 29(3) 10_556 . . 10_556 ? O5 Si4 O23 Si2 158.6(13) . . . 10_556 ? O5 Si4 O23 Si6 115(4) . . . . ? O5 Si4 O23 Si11 92(4) . . . 10_556 ? O5 Si4 O23 O13 144(3) . . . 10_556 ? O5 Si5 O19 Si1 59.2(13) 5 . . 10_556 ? O5 Si5 O19 Si8 -37(2) 5 . . . ? O5 Si5 O19 Si13 -41(3) 5 . . 10_556 ? O5 Si5 O19 O9 73(3) 5 . . 10_556 ? O6 Si9 O12 Si8 -129.9(14) . . . 10_556 ? O6 Si9 O12 Si13 -120.9(17) . . . . ? O6 Si9 O12 Si14 37(7) . . . 10_556 ? O6 Si9 O12 O22 -85(2) . . . 10_556 ? O6 Si9 O25 Si14 76(15) . . . 10_556 ? O6 Si9 O25 Si16 -87(2) . . . . ? O6 Si9 O25 O15 -81(3) . . . 10_556 ? O6 Si9 O30 Si9 -61(4) . . . 12 ? O6 Si9 O30 Si14 -67(7) . . . 10_556 ? O6 Si9 O30 Si14 -63(2) . . . 3 ? O6 Si9 O30 O32 -89(2) . . . 10_556 ? O6 Si10 O7 Si6 173.8(13) . . . 10_556 ? O6 Si10 O7 Si11 -178.1(14) . . . . ? O6 Si10 O7 Si15 -83(9) . . . 10_556 ? O6 Si10 O7 O17 130(4) . . . 10_556 ? O6 Si10 O27 Si10 118(3) . . . 10_556 ? O6 Si10 O27 Si15 -172(20) . . . 10_556 ? O6 Si10 O27 Si15 124.1(17) . . . . ? O6 Si10 O29 Si10 -52(4) . . . 12 ? O6 Si10 O29 Si15 81(8) . . . 10_556 ? O6 Si10 O29 Si15 -42(4) . . . 3 ? O6 Si10 O29 O31 33(13) . . . 10_556 ? O6 Si14 O15 Si9 143(37) 10_556 . . 10_556 ? O6 Si14 O15 Si16 -116(6) 10_556 . . . ? O6 Si14 O15 O25 -107(3) 10_556 . . 10_556 ? O6 Si14 O16 Si9 -13(8) 10_556 . . 10_556 ? O6 Si14 O16 Si10 -55(3) 10_556 . . 10_556 ? O6 Si14 O16 Si15 -65(4) 10_556 . . . ? O6 Si14 O22 Si8 -166(2) 10_556 . . . ? O6 Si14 O22 Si9 118(8) 10_556 . . 10_556 ? O6 Si14 O22 Si13 -153(3) 10_556 . . 10_556 ? O6 Si14 O22 O12 -111(2) 10_556 . . 10_556 ? O6 Si14 O32 Si9 -58(4) 10_556 . . 3 ? O6 Si14 O32 Si9 -113(8) 10_556 . . 10_556 ? O6 Si14 O32 Si14 -41(5) 10_556 . . 12 ? O6 Si14 O32 O30 -90(2) 10_556 . . 10_556 ? O6 Si15 O16 Si9 52(3) 10_556 . . 10_556 ? O6 Si15 O16 Si10 7(8) 10_556 . . 10_556 ? O6 Si15 O16 Si14 60(4) 10_556 . . . ? O6 Si15 O17 Si6 158.6(17) 10_556 . . . ? O6 Si15 O17 Si10 -88(8) 10_556 . . 10_556 ? O6 Si15 O17 Si11 146.5(17) 10_556 . . 10_556 ? O6 Si15 O17 O7 63(4) 10_556 . . 10_556 ? O6 Si15 O27 Si10 -123.2(18) 10_556 . . . ? O6 Si15 O27 Si10 -7(19) 10_556 . . 10_556 ? O6 Si15 O27 Si15 -129(2) 10_556 . . 10_556 ? O6 Si15 O31 Si10 69(4) 10_556 . . 3 ? O6 Si15 O31 Si10 88(8) 10_556 . . 10_556 ? O6 Si15 O31 Si15 64(6) 10_556 . . 12 ? O6 Si15 O31 O29 139(12) 10_556 . . 10_556 ? O7 Si6 O17 Si10 -105(4) 10_556 . . 10_556 ? O7 Si6 O17 Si11 -2(8) 10_556 . . 10_556 ? O7 Si6 O17 Si15 -93(4) 10_556 . . . ? O7 Si6 O18 Si7 -169.4(13) 10_556 . . . ? O7 Si6 O18 Si11 95(12) 10_556 . . 10_556 ? O7 Si6 O18 Si12 -167.8(17) 10_556 . . 10_556 ? O7 Si6 O18 O8 -100(3) 10_556 . . 10_556 ? O7 Si6 O23 Si2 119.2(14) 10_556 . . 10_556 ? O7 Si6 O23 Si4 148(3) 10_556 . . . ? O7 Si6 O23 Si11 -95(7) 10_556 . . 10_556 ? O7 Si6 O23 O13 117(3) 10_556 . . 10_556 ? O7 Si6 O24 Si11 168(10) 10_556 . . 10_556 ? O7 Si6 O24 Si17 144(6) 10_556 . . . ? O7 Si6 O24 O14 107(3) 10_556 . . 10_556 ? O7 Si10 O6 Si9 158(2) . . . . ? O7 Si10 O6 Si14 144(2) . . . 10_556 ? O7 Si10 O6 Si15 50(6) . . . 10_556 ? O7 Si10 O6 O16 58(4) . . . 10_556 ? O7 Si10 O27 Si10 -124(3) . . . 10_556 ? O7 Si10 O27 Si15 -117.8(18) . . . . ? O7 Si10 O27 Si15 -54(19) . . . 10_556 ? O7 Si10 O29 Si10 -165(3) . . . 12 ? O7 Si10 O29 Si15 -155(4) . . . 3 ? O7 Si10 O29 Si15 -32(7) . . . 10_556 ? O7 Si10 O29 O31 -80(12) . . . 10_556 ? O7 Si11 O8 Si6 79(8) . . . 10_556 ? O7 Si11 O8 Si7 -152.9(13) . . . 10_556 ? O7 Si11 O8 Si12 -142.3(15) . . . . ? O7 Si11 O8 O18 -90(3) . . . 10_556 ? O7 Si11 O13 Si4 103(2) . . . 10_556 ? O7 Si11 O13 Si6 -73(6) . . . 10_556 ? O7 Si11 O13 O23 79(3) . . . 10_556 ? O7 Si11 O14 Si6 36(8) . . . 10_556 ? O7 Si11 O14 Si17 101.9(19) . . . . ? O7 Si11 O14 O24 79(3) . . . 10_556 ? O7 Si15 O16 Si9 169.3(17) 10_556 . . 10_556 ? O7 Si15 O16 Si10 125(7) 10_556 . . 10_556 ? O7 Si15 O16 Si14 177(2) 10_556 . . . ? O7 Si15 O16 O6 118(4) 10_556 . . 10_556 ? O7 Si15 O17 Si6 95(4) 10_556 . . . ? O7 Si15 O17 Si10 -152(8) 10_556 . . 10_556 ? O7 Si15 O17 Si11 83(4) 10_556 . . 10_556 ? O7 Si15 O27 Si10 121.6(19) 10_556 . . . ? O7 Si15 O27 Si10 -123(20) 10_556 . . 10_556 ? O7 Si15 O27 Si15 116(2) 10_556 . . 10_556 ? O7 Si15 O31 Si10 -150(9) 10_556 . . 10_556 ? O7 Si15 O31 Si10 -169(4) 10_556 . . 3 ? O7 Si15 O31 Si15 -174(5) 10_556 . . 12 ? O7 Si15 O31 O29 -98(13) 10_556 . . 10_556 ? O8 Si6 O17 Si10 -153.1(19) 10_556 . . 10_556 ? O8 Si6 O17 Si11 -50(6) 10_556 . . 10_556 ? O8 Si6 O17 Si15 -141.4(18) 10_556 . . . ? O8 Si6 O17 O7 -48(4) 10_556 . . 10_556 ? O8 Si6 O18 Si7 -69(2) 10_556 . . . ? O8 Si6 O18 Si11 -165(12) 10_556 . . 10_556 ? O8 Si6 O18 Si12 -68(3) 10_556 . . 10_556 ? O8 Si6 O23 Si2 -133.9(13) 10_556 . . 10_556 ? O8 Si6 O23 Si4 -105(4) 10_556 . . . ? O8 Si6 O23 Si11 12(7) 10_556 . . 10_556 ? O8 Si6 O23 O13 -136(3) 10_556 . . 10_556 ? O8 Si6 O24 Si11 48(9) 10_556 . . 10_556 ? O8 Si6 O24 Si17 24(7) 10_556 . . . ? O8 Si6 O24 O14 -13(3) 10_556 . . 10_556 ? O8 Si7 O18 Si6 66(2) 10_556 . . . ? O8 Si7 O18 Si11 71(2) 10_556 . . 10_556 ? O8 Si7 O18 Si12 -108(5) 10_556 . . 10_556 ? O8 Si7 O20 Si8 -176(3) 10_556 . . 16_545 ? O8 Si7 O20 Si12 -93(8) 10_556 . . 10_556 ? O8 Si7 O20 Si13 -177(3) 10_556 . . 7_545 ? O8 Si7 O20 O10 42(6) 10_556 . . 7_545 ? O8 Si7 O21 Si8 175.2(18) 10_556 . . 13_556 ? O8 Si7 O21 Si12 -39(6) 10_556 . . 10_556 ? O8 Si7 O21 Si13 177(2) 10_556 . . 6 ? O8 Si7 O21 O11 -131(3) 10_556 . . 13_556 ? O8 Si7 O34 Si7 -49(6) 10_556 . . 12_655 ? O8 Si7 O34 Si12 -20(6) 10_556 . . 3_655 ? O8 Si7 O34 Si12 68(4) 10_556 . . 10_556 ? O8 Si7 O34 O33 -45(6) 10_556 . . 10_556 ? O8 Si11 O7 Si6 -126(6) . . . 10_556 ? O8 Si11 O7 Si10 -177.5(14) . . . . ? O8 Si11 O7 Si15 173.4(15) . . . 10_556 ? O8 Si11 O7 O17 -127(4) . . . 10_556 ? O8 Si11 O13 Si4 -30(3) . . . 10_556 ? O8 Si11 O13 Si6 154(7) . . . 10_556 ? O8 Si11 O13 O23 -54(3) . . . 10_556 ? O8 Si11 O14 Si6 144(8) . . . 10_556 ? O8 Si11 O14 Si17 -149.7(18) . . . . ? O8 Si11 O14 O24 -172(3) . . . 10_556 ? O8 Si12 O33 Si7 -120(7) . . . 3_655 ? O8 Si12 O33 Si7 101(4) . . . 10_556 ? O8 Si12 O33 Si12 -105(5) . . . 12_655 ? O8 Si12 O33 O34 -148(6) . . . 10_556 ? O9 Si1 O2 Si2 -120.1(7) . . . 5 ? O9 Si1 O2 Si2 120.1(7) 12_655 . . 5 ? O9 Si1 O2 Si4 120.1(7) 12_655 . . 14_556 ? O9 Si1 O2 Si4 -120.1(7) . . . 14_556 ? O9 Si1 O2 Si5 120.1(7) 12_655 . . 10_556 ? O9 Si1 O2 Si5 -120.1(7) . . . 10_556 ? O9 Si1 O2 O4 -59.9(7) 12_655 . . 10_556 ? O9 Si1 O2 O4 59.9(7) . . . 10_556 ? O9 Si1 O2 O5 120.1(7) 12_655 . . 14_556 ? O9 Si1 O2 O5 -120.1(7) . . . 14_556 ? O9 Si1 O9 Si5 -93.6(14) 12_655 . . 10_556 ? O9 Si1 O9 Si8 -170.2(8) 12_655 . . 10_556 ? O9 Si1 O9 Si13 -166.3(11) 12_655 . . . ? O9 Si1 O9 O19 -106(3) 12_655 . . 10_556 ? O9 Si5 O19 Si1 -13(3) 10_556 . . 10_556 ? O9 Si5 O19 Si1 -56.4(10) 3_655 . . 10_556 ? O9 Si5 O19 Si8 -152.2(16) 3_655 . . . ? O9 Si5 O19 Si8 -109(4) 10_556 . . . ? O9 Si5 O19 Si13 -113(4) 10_556 . . 10_556 ? O9 Si5 O19 Si13 -156(2) 3_655 . . 10_556 ? O9 Si5 O19 O9 -43(3) 3_655 . . 10_556 ? O9 Si8 O11 Si7 78(2) 10_556 . . 13_556 ? O9 Si8 O11 Si12 69(3) 10_556 . . 6 ? O9 Si8 O11 Si13 -53(7) 10_556 . . 10_556 ? O9 Si8 O11 O21 8(4) 10_556 . . 13_556 ? O9 Si8 O19 Si1 73(3) 10_556 . . 10_556 ? O9 Si8 O19 Si5 116(4) 10_556 . . . ? O9 Si8 O19 Si13 -79(7) 10_556 . . 10_556 ? O9 Si8 O22 Si9 -139(3) 10_556 . . 10_556 ? O9 Si8 O22 Si13 71(7) 10_556 . . 10_556 ? O9 Si8 O22 Si14 -153(3) 10_556 . . . ? O9 Si8 O22 O12 150(2) 10_556 . . 10_556 ? O9 Si13 O10 Si7 117.4(18) . . . 7 ? O9 Si13 O10 Si8 54(44) . . . 10_556 ? O9 Si13 O10 Si12 111.5(17) . . . 16 ? O9 Si13 O10 O20 95(6) . . . 7 ? O9 Si13 O12 Si8 112(8) . . . 10_556 ? O9 Si13 O12 Si9 58(2) . . . . ? O9 Si13 O12 Si14 53(2) . . . 10_556 ? O9 Si13 O12 O22 23(2) . . . 10_556 ? O10 Si7 O18 Si6 -35.2(18) 7_545 . . . ? O10 Si7 O18 Si11 -29.4(19) 7_545 . . 10_556 ? O10 Si7 O18 Si12 151(5) 7_545 . . 10_556 ? O10 Si7 O18 O8 -101(2) 7_545 . . 10_556 ? O10 Si7 O20 Si8 142(8) 7_545 . . 16_545 ? O10 Si7 O20 Si12 -135(9) 7_545 . . 10_556 ? O10 Si7 O20 Si13 141(8) 7_545 . . 7_545 ? O10 Si7 O21 Si8 57(2) 7_545 . . 13_556 ? O10 Si7 O21 Si12 -157(6) 7_545 . . 10_556 ? O10 Si7 O21 Si13 59(3) 7_545 . . 6 ? O10 Si7 O21 O11 111(3) 7_545 . . 13_556 ? O10 Si7 O34 Si7 74(6) 7_545 . . 12_655 ? O10 Si7 O34 Si12 -169(5) 7_545 . . 10_556 ? O10 Si7 O34 Si12 103(6) 7_545 . . 3_655 ? O10 Si7 O34 O33 77(6) 7_545 . . 10_556 ? O10 Si8 O11 Si7 -60(3) 10_556 . . 13_556 ? O10 Si8 O11 Si12 -68(3) 10_556 . . 6 ? O10 Si8 O11 Si13 170(8) 10_556 . . 10_556 ? O10 Si8 O11 O21 -130(3) 10_556 . . 13_556 ? O10 Si8 O19 Si1 -21(2) 10_556 . . 10_556 ? O10 Si8 O19 Si5 22(2) 10_556 . . . ? O10 Si8 O19 Si13 -174(7) 10_556 . . 10_556 ? O10 Si8 O19 O9 -95(3) 10_556 . . 10_556 ? O10 Si8 O22 Si9 -26(3) 10_556 . . 10_556 ? O10 Si8 O22 Si13 -175(8) 10_556 . . 10_556 ? O10 Si8 O22 Si14 -39(3) 10_556 . . . ? O10 Si8 O22 O12 -96(2) 10_556 . . 10_556 ? O10 Si12 O8 Si6 -27(2) 16_545 . . 10_556 ? O10 Si12 O8 Si7 25(4) 16_545 . . 10_556 ? O10 Si12 O8 Si11 -33.6(19) 16_545 . . . ? O10 Si12 O8 O18 -88(2) 16_545 . . 10_556 ? O10 Si12 O33 Si7 137(7) 16_545 . . 3_655 ? O10 Si12 O33 Si7 -3(4) 16_545 . . 10_556 ? O10 Si12 O33 Si12 151(5) 16_545 . . 12_655 ? O10 Si12 O33 O34 109(6) 16_545 . . 10_556 ? O10 Si13 O9 Si1 -29(2) . . . . ? O10 Si13 O9 Si5 -60.2(16) . . . 10_556 ? O10 Si13 O9 Si8 -7(6) . . . 10_556 ? O10 Si13 O9 O19 -90(3) . . . 10_556 ? O10 Si13 O12 Si8 -1(7) . . . 10_556 ? O10 Si13 O12 Si9 -55(2) . . . . ? O10 Si13 O12 Si14 -60(2) . . . 10_556 ? O10 Si13 O12 O22 -90(2) . . . 10_556 ? O11 Si7 O18 Si6 -160.8(13) 13_556 . . . ? O11 Si7 O18 Si11 -155.1(14) 13_556 . . 10_556 ? O11 Si7 O18 Si12 25(4) 13_556 . . 10_556 ? O11 Si7 O18 O8 134(2) 13_556 . . 10_556 ? O11 Si7 O20 Si8 -47(4) 13_556 . . 16_545 ? O11 Si7 O20 Si12 36(7) 13_556 . . 10_556 ? O11 Si7 O20 Si13 -48(3) 13_556 . . 7_545 ? O11 Si7 O20 O10 171(5) 13_556 . . 7_545 ? O11 Si7 O21 Si8 -54(3) 13_556 . . 13_556 ? O11 Si7 O21 Si12 92(7) 13_556 . . 10_556 ? O11 Si7 O21 Si13 -52(3) 13_556 . . 6 ? O11 Si7 O34 Si7 -162(5) 13_556 . . 12_655 ? O11 Si7 O34 Si12 -133(6) 13_556 . . 3_655 ? O11 Si7 O34 Si12 -45(4) 13_556 . . 10_556 ? O11 Si7 O34 O33 -159(6) 13_556 . . 10_556 ? O11 Si8 O19 Si1 -146.4(16) . . . 10_556 ? O11 Si8 O19 Si5 -103.3(19) . . . . ? O11 Si8 O19 Si13 61(6) . . . 10_556 ? O11 Si8 O19 O9 140(3) . . . 10_556 ? O11 Si8 O22 Si9 99(3) . . . 10_556 ? O11 Si8 O22 Si13 -50(7) . . . 10_556 ? O11 Si8 O22 Si14 85(3) . . . . ? O11 Si8 O22 O12 29(2) . . . 10_556 ? O11 Si12 O8 Si6 108.9(19) 6_554 . . 10_556 ? O11 Si12 O8 Si7 162(5) 6_554 . . 10_556 ? O11 Si12 O8 Si11 102.6(18) 6_554 . . . ? O11 Si12 O8 O18 48(3) 6_554 . . 10_556 ? O11 Si12 O33 Si7 -125(5) 6_554 . . 10_556 ? O11 Si12 O33 Si7 14(7) 6_554 . . 3_655 ? O11 Si12 O33 Si12 29(5) 6_554 . . 12_655 ? O11 Si12 O33 O34 -13(6) 6_554 . . 10_556 ? O11 Si13 O9 Si1 95(2) 10_556 . . . ? O11 Si13 O9 Si5 63(2) 10_556 . . 10_556 ? O11 Si13 O9 Si8 116(7) 10_556 . . 10_556 ? O11 Si13 O9 O19 34(3) 10_556 . . 10_556 ? O11 Si13 O10 Si7 -20(2) 10_556 . . 7 ? O11 Si13 O10 Si8 -83(44) 10_556 . . 10_556 ? O11 Si13 O10 Si12 -26(2) 10_556 . . 16 ? O11 Si13 O10 O20 -43(6) 10_556 . . 7 ? O11 Si13 O12 Si8 -109(7) 10_556 . . 10_556 ? O11 Si13 O12 Si9 -163.0(15) 10_556 . . . ? O11 Si13 O12 Si14 -167.4(18) 10_556 . . 10_556 ? O11 Si13 O12 O22 162(2) 10_556 . . 10_556 ? O12 Si8 O11 Si7 -172(2) 10_556 . . 13_556 ? O12 Si8 O11 Si12 180(3) 10_556 . . 6 ? O12 Si8 O11 Si13 57(7) 10_556 . . 10_556 ? O12 Si8 O11 O21 118(3) 10_556 . . 13_556 ? O12 Si8 O19 Si1 108.7(17) 10_556 . . 10_556 ? O12 Si8 O19 Si5 151.9(16) 10_556 . . . ? O12 Si8 O19 Si13 -44(6) 10_556 . . 10_556 ? O12 Si8 O19 O9 35(3) 10_556 . . 10_556 ? O12 Si8 O22 Si9 70(3) 10_556 . . 10_556 ? O12 Si8 O22 Si13 -79(7) 10_556 . . 10_556 ? O12 Si8 O22 Si14 56(3) 10_556 . . . ? O12 Si9 O6 Si10 -137(2) . . . . ? O12 Si9 O6 Si14 -31(6) . . . 10_556 ? O12 Si9 O6 Si15 -124(2) . . . 10_556 ? O12 Si9 O6 O16 -43(4) . . . 10_556 ? O12 Si9 O25 Si14 -43(15) . . . 10_556 ? O12 Si9 O25 Si16 154.4(18) . . . . ? O12 Si9 O25 O15 161(3) . . . 10_556 ? O12 Si9 O30 Si9 57(4) . . . 12 ? O12 Si9 O30 Si14 52(7) . . . 10_556 ? O12 Si9 O30 Si14 55(2) . . . 3 ? O12 Si9 O30 O32 29(2) . . . 10_556 ? O12 Si13 O9 Si1 -140.4(16) . . . . ? O12 Si13 O9 Si5 -171.9(10) . . . 10_556 ? O12 Si13 O9 Si8 -119(7) . . . 10_556 ? O12 Si13 O9 O19 159(3) . . . 10_556 ? O12 Si13 O10 Si7 -123.9(18) . . . 7 ? O12 Si13 O10 Si8 173(45) . . . 10_556 ? O12 Si13 O10 Si12 -129.8(16) . . . 16 ? O12 Si13 O10 O20 -147(6) . . . 7 ? O12 Si14 O15 Si9 -83(37) 10_556 . . 10_556 ? O12 Si14 O15 Si16 18(6) 10_556 . . . ? O12 Si14 O15 O25 27(3) 10_556 . . 10_556 ? O12 Si14 O16 Si9 -149(8) 10_556 . . 10_556 ? O12 Si14 O16 Si10 169.1(16) 10_556 . . 10_556 ? O12 Si14 O16 Si15 159.6(19) 10_556 . . . ? O12 Si14 O16 O6 -135(4) 10_556 . . 10_556 ? O12 Si14 O22 Si8 -55(3) 10_556 . . . ? O12 Si14 O22 Si9 -131(7) 10_556 . . 10_556 ? O12 Si14 O22 Si13 -42(3) 10_556 . . 10_556 ? O12 Si14 O32 Si9 178(4) 10_556 . . 3 ? O12 Si14 O32 Si9 123(8) 10_556 . . 10_556 ? O12 Si14 O32 Si14 -165(5) 10_556 . . 12 ? O12 Si14 O32 O30 146(2) 10_556 . . 10_556 ? O13 Si2 O3 Si3 120.7(7) 12 . . 5_445 ? O13 Si2 O3 Si3 -120.7(7) . . . 5_445 ? O13 Si2 O3 Si3 120.7(7) 12 . . 14_446 ? O13 Si2 O3 Si3 -120.7(7) . . . 14_446 ? O13 Si2 O3 O3 59.3(7) . . . 10_556 ? O13 Si2 O3 O3 -59.3(7) 12 . . 10_556 ? O13 Si2 O3 O4 -120.7(7) . . . 14_446 ? O13 Si2 O3 O4 120.7(7) 12 . . 14_446 ? O13 Si2 O13 Si4 -74.9(12) 12 . . 10_556 ? O13 Si2 O13 O23 -60(3) 12 . . 10_556 ? O13 Si4 O5 Si1 -112.2(10) 10_556 . . 14_446 ? O13 Si4 O5 Si1 112.2(10) 3 . . 14_446 ? O13 Si4 O5 Si2 -112.2(10) 10_556 . . 10_556 ? O13 Si4 O5 Si2 112.2(10) 3 . . 10_556 ? O13 Si4 O5 Si5 -112.2(10) 10_556 . . 5_445 ? O13 Si4 O5 Si5 112.2(10) 3 . . 5_445 ? O13 Si4 O5 O2 -112.2(10) 10_556 . . 14_446 ? O13 Si4 O5 O2 112.2(10) 3 . . 14_446 ? O13 Si4 O23 Si2 -70.6(11) 3 . . 10_556 ? O13 Si4 O23 Si2 14(3) 10_556 . . 10_556 ? O13 Si4 O23 Si6 -29(3) 10_556 . . . ? O13 Si4 O23 Si6 -114(3) 3 . . . ? O13 Si4 O23 Si11 -137(4) 3 . . 10_556 ? O13 Si4 O23 Si11 -52(4) 10_556 . . 10_556 ? O13 Si4 O23 O13 -85(3) 3 . . 10_556 ? O13 Si6 O17 Si10 -20(3) 10_556 . . 10_556 ? O13 Si6 O17 Si11 83(6) 10_556 . . 10_556 ? O13 Si6 O17 Si15 -8(3) 10_556 . . . ? O13 Si6 O17 O7 85(4) 10_556 . . 10_556 ? O13 Si6 O18 Si7 76.1(16) 10_556 . . . ? O13 Si6 O18 Si11 -20(12) 10_556 . . 10_556 ? O13 Si6 O18 Si12 78(2) 10_556 . . 10_556 ? O13 Si6 O18 O8 145(2) 10_556 . . 10_556 ? O13 Si6 O23 Si2 2.4(19) 10_556 . . 10_556 ? O13 Si6 O23 Si4 31(3) 10_556 . . . ? O13 Si6 O23 Si11 148(8) 10_556 . . 10_556 ? O13 Si6 O24 Si11 -74(10) 10_556 . . 10_556 ? O13 Si6 O24 Si17 -98(7) 10_556 . . . ? O13 Si6 O24 O14 -135(2) 10_556 . . 10_556 ? O13 Si11 O7 Si6 91(6) . . . 10_556 ? O13 Si11 O7 Si10 39.3(19) . . . . ? O13 Si11 O7 Si15 30(2) . . . 10_556 ? O13 Si11 O7 O17 90(4) . . . 10_556 ? O13 Si11 O8 Si6 -147(9) . . . 10_556 ? O13 Si11 O8 Si7 -19(2) . . . 10_556 ? O13 Si11 O8 Si12 -8(2) . . . . ? O13 Si11 O8 O18 44(3) . . . 10_556 ? O13 Si11 O14 Si6 -85(8) . . . 10_556 ? O13 Si11 O14 Si17 -19(2) . . . . ? O13 Si11 O14 O24 -41(3) . . . 10_556 ? O14 Si6 O17 Si10 107(2) 10_556 . . 10_556 ? O14 Si6 O17 Si11 -150(7) 10_556 . . 10_556 ? O14 Si6 O17 Si15 118(2) 10_556 . . . ? O14 Si6 O17 O7 -149(4) 10_556 . . 10_556 ? O14 Si6 O18 Si7 -41.4(18) 10_556 . . . ? O14 Si6 O18 Si11 -138(12) 10_556 . . 10_556 ? O14 Si6 O18 Si12 -40(2) 10_556 . . 10_556 ? O14 Si6 O18 O8 28(3) 10_556 . . 10_556 ? O14 Si6 O23 Si2 -32(2) 10_556 . . 10_556 ? O14 Si6 O23 Si4 -3(4) 10_556 . . . ? O14 Si6 O23 Si11 114(7) 10_556 . . 10_556 ? O14 Si6 O23 O13 -34(3) 10_556 . . 10_556 ? O14 Si6 O24 Si11 61(10) 10_556 . . 10_556 ? O14 Si6 O24 Si17 37(5) 10_556 . . . ? O14 Si11 O7 Si6 -27(6) . . . 10_556 ? O14 Si11 O7 Si10 -79.4(17) . . . . ? O14 Si11 O7 Si15 -88.4(17) . . . 10_556 ? O14 Si11 O7 O17 -29(4) . . . 10_556 ? O14 Si11 O8 Si6 -34(8) . . . 10_556 ? O14 Si11 O8 Si7 94.3(15) . . . 10_556 ? O14 Si11 O8 Si12 104.8(17) . . . . ? O14 Si11 O8 O18 157(2) . . . 10_556 ? O14 Si11 O13 Si4 -136(2) . . . 10_556 ? O14 Si11 O13 Si6 48(6) . . . 10_556 ? O14 Si11 O13 O23 -160(2) . . . 10_556 ? O14 Si17 O14 Si6 -68(2) 10_556 . . 10_556 ? O14 Si17 O14 Si11 -77(2) 10_556 . . . ? O14 Si17 O14 O24 -54(3) 10_556 . . 10_556 ? O14 Si17 O24 Si6 -37(5) 10_556 . . . ? O14 Si17 O24 Si6 -171(6) . . . . ? O14 Si17 O24 Si11 -177(4) . . . 10_556 ? O14 Si17 O24 Si11 -43(4) 10_556 . . 10_556 ? O14 Si17 O24 O14 -134(3) . . . 10_556 ? O14 Si17 O35 Si17 -11(4) . . . 3_655 ? O14 Si17 O35 Si17 -135(4) 10_556 . . 3_655 ? O14 Si17 O35 O35 -29.1(6) . . . 10_556 ? O14 Si17 O35 O35 -152.6(5) 10_556 . . 10_556 ? O15 Si9 O6 Si10 81(2) 10_556 . . . ? O15 Si9 O6 Si14 -172(7) 10_556 . . 10_556 ? O15 Si9 O6 Si15 95(2) 10_556 . . 10_556 ? O15 Si9 O6 O16 176(4) 10_556 . . 10_556 ? O15 Si9 O12 Si8 -2(2) 10_556 . . 10_556 ? O15 Si9 O12 Si13 7(3) 10_556 . . . ? O15 Si9 O12 Si14 164(9) 10_556 . . 10_556 ? O15 Si9 O12 O22 43(3) 10_556 . . 10_556 ? O15 Si9 O25 Si14 156(16) 10_556 . . 10_556 ? O15 Si9 O25 Si16 -6(2) 10_556 . . . ? O15 Si9 O30 Si9 -169(3) 10_556 . . 12 ? O15 Si9 O30 Si14 -170(2) 10_556 . . 3 ? O15 Si9 O30 Si14 -174(8) 10_556 . . 10_556 ? O15 Si9 O30 O32 164(2) 10_556 . . 10_556 ? O15 Si14 O16 Si9 -8(7) . . . 10_556 ? O15 Si14 O16 Si10 -50(2) . . . 10_556 ? O15 Si14 O16 Si15 -59(3) . . . . ? O15 Si14 O16 O6 6(4) . . . 10_556 ? O15 Si14 O22 Si8 87(3) . . . . ? O15 Si14 O22 Si9 11(7) . . . 10_556 ? O15 Si14 O22 Si13 100(3) . . . 10_556 ? O15 Si14 O22 O12 142(2) . . . 10_556 ? O15 Si14 O32 Si9 -4(7) . . . 10_556 ? O15 Si14 O32 Si9 51(4) . . . 3 ? O15 Si14 O32 Si14 68(5) . . . 12 ? O15 Si14 O32 O30 18(3) . . . 10_556 ? O15 Si16 O15 Si9 174(6) 10_556 . . 10_556 ? O15 Si16 O15 Si14 167(5) 10_556 . . . ? O15 Si16 O15 O25 159(2) 10_556 . . 10_556 ? O15 Si16 O25 Si9 29(2) . . . . ? O15 Si16 O25 Si9 7(2) 10_556 . . . ? O15 Si16 O25 Si14 4(2) 10_556 . . 10_556 ? O15 Si16 O25 Si14 27(2) . . . 10_556 ? O15 Si16 O25 O15 22(2) . . . 10_556 ? O15 Si16 O26 Si17 132(3) 10_556 . . 7 ? O15 Si16 O26 Si17 35(3) . . . 7 ? O15 Si16 O26 O26 44.4(10) . . . 10_556 ? O15 Si16 O26 O26 140.9(9) 10_556 . . 10_556 ? O15 Si16 O28 Si3 -171.4(12) . . . 10_556 ? O15 Si16 O28 Si3 128.3(15) 10_556 . . . ? O15 Si16 O28 Si3 88.6(15) 10_556 . . 10_556 ? O15 Si16 O28 Si3 -131.6(15) . . . . ? O15 Si16 O28 O28 43.2(10) 10_556 . . 10_556 ? O15 Si16 O28 O28 143.2(9) . . . 10_556 ? O16 Si9 O6 Si10 -94(4) 10_556 . . . ? O16 Si9 O6 Si14 12(8) 10_556 . . 10_556 ? O16 Si9 O6 Si15 -81(4) 10_556 . . 10_556 ? O16 Si9 O12 Si8 -138.1(14) 10_556 . . 10_556 ? O16 Si9 O12 Si13 -129.2(16) 10_556 . . . ? O16 Si9 O12 Si14 28(7) 10_556 . . 10_556 ? O16 Si9 O12 O22 -93(2) 10_556 . . 10_556 ? O16 Si9 O25 Si14 71(15) 10_556 . . 10_556 ? O16 Si9 O25 Si16 -91(2) 10_556 . . . ? O16 Si9 O25 O15 -85(3) 10_556 . . 10_556 ? O16 Si9 O30 Si9 -50(4) 10_556 . . 12 ? O16 Si9 O30 Si14 -55(7) 10_556 . . 10_556 ? O16 Si9 O30 Si14 -51(2) 10_556 . . 3 ? O16 Si9 O30 O32 -77(2) 10_556 . . 10_556 ? O16 Si10 O6 Si9 100(4) 10_556 . . . ? O16 Si10 O6 Si14 86(4) 10_556 . . 10_556 ? O16 Si10 O6 Si15 -7(8) 10_556 . . 10_556 ? O16 Si10 O7 Si6 -175.1(13) 10_556 . . 10_556 ? O16 Si10 O7 Si11 -167.1(14) 10_556 . . . ? O16 Si10 O7 Si15 -72(8) 10_556 . . 10_556 ? O16 Si10 O7 O17 141(4) 10_556 . . 10_556 ? O16 Si10 O27 Si10 117(3) 10_556 . . 10_556 ? O16 Si10 O27 Si15 -173(20) 10_556 . . 10_556 ? O16 Si10 O27 Si15 123.0(18) 10_556 . . . ? O16 Si10 O29 Si10 -63(4) 10_556 . . 12 ? O16 Si10 O29 Si15 -53(4) 10_556 . . 3 ? O16 Si10 O29 Si15 70(8) 10_556 . . 10_556 ? O16 Si10 O29 O31 22(13) 10_556 . . 10_556 ? O16 Si14 O15 Si9 141(37) . . . 10_556 ? O16 Si14 O15 Si16 -117(6) . . . . ? O16 Si14 O15 O25 -109(3) . . . 10_556 ? O16 Si14 O22 Si8 -153(2) . . . . ? O16 Si14 O22 Si9 131(8) . . . 10_556 ? O16 Si14 O22 Si13 -140(3) . . . 10_556 ? O16 Si14 O22 O12 -98(2) . . . 10_556 ? O16 Si14 O32 Si9 -70(4) . . . 3 ? O16 Si14 O32 Si9 -125(8) . . . 10_556 ? O16 Si14 O32 Si14 -52(5) . . . 12 ? O16 Si14 O32 O30 -102(2) . . . 10_556 ? O16 Si15 O17 Si6 145.0(18) . . . . ? O16 Si15 O17 Si10 -102(8) . . . 10_556 ? O16 Si15 O17 Si11 132.9(18) . . . 10_556 ? O16 Si15 O17 O7 50(4) . . . 10_556 ? O16 Si15 O27 Si10 -6(19) . . . 10_556 ? O16 Si15 O27 Si10 -122.1(19) . . . . ? O16 Si15 O27 Si15 -127(2) . . . 10_556 ? O16 Si15 O31 Si10 99(8) . . . 10_556 ? O16 Si15 O31 Si10 80(4) . . . 3 ? O16 Si15 O31 Si15 75(6) . . . 12 ? O16 Si15 O31 O29 151(12) . . . 10_556 ? O17 Si6 O18 Si7 -162.8(13) . . . . ? O17 Si6 O18 Si11 101(12) . . . 10_556 ? O17 Si6 O18 Si12 -161.2(17) . . . 10_556 ? O17 Si6 O18 O8 -94(3) . . . 10_556 ? O17 Si6 O23 Si2 107.4(15) . . . 10_556 ? O17 Si6 O23 Si4 136(3) . . . . ? O17 Si6 O23 Si11 -107(7) . . . 10_556 ? O17 Si6 O23 O13 105(3) . . . 10_556 ? O17 Si6 O24 Si11 170(10) . . . 10_556 ? O17 Si6 O24 Si17 146(6) . . . . ? O17 Si6 O24 O14 109(2) . . . 10_556 ? O17 Si10 O6 Si9 167.5(19) 10_556 . . . ? O17 Si10 O6 Si14 154(2) 10_556 . . 10_556 ? O17 Si10 O6 Si15 60(7) 10_556 . . 10_556 ? O17 Si10 O6 O16 67(4) 10_556 . . 10_556 ? O17 Si10 O7 Si6 44(3) 10_556 . . 10_556 ? O17 Si10 O7 Si11 52(3) 10_556 . . . ? O17 Si10 O7 Si15 147(10) 10_556 . . 10_556 ? O17 Si10 O27 Si10 -122(3) 10_556 . . 10_556 ? O17 Si10 O27 Si15 -115.6(17) 10_556 . . . ? O17 Si10 O27 Si15 -52(19) 10_556 . . 10_556 ? O17 Si10 O29 Si10 -177(3) 10_556 . . 12 ? O17 Si10 O29 Si15 -44(7) 10_556 . . 10_556 ? O17 Si10 O29 Si15 -167(4) 10_556 . . 3 ? O17 Si10 O29 O31 -92(12) 10_556 . . 10_556 ? O17 Si11 O7 Si6 2(7) 10_556 . . 10_556 ? O17 Si11 O7 Si10 -50(3) 10_556 . . . ? O17 Si11 O7 Si15 -59(3) 10_556 . . 10_556 ? O17 Si11 O8 Si6 69(8) 10_556 . . 10_556 ? O17 Si11 O8 Si7 -163.5(12) 10_556 . . 10_556 ? O17 Si11 O8 Si12 -153.0(14) 10_556 . . . ? O17 Si11 O8 O18 -101(3) 10_556 . . 10_556 ? O17 Si11 O13 Si4 116(2) 10_556 . . 10_556 ? O17 Si11 O13 Si6 -60(6) 10_556 . . 10_556 ? O17 Si11 O13 O23 92(3) 10_556 . . 10_556 ? O17 Si11 O14 Si6 30(8) 10_556 . . 10_556 ? O17 Si11 O14 Si17 95.9(19) 10_556 . . . ? O17 Si11 O14 O24 73(3) 10_556 . . 10_556 ? O17 Si15 O16 Si9 159.1(16) . . . 10_556 ? O17 Si15 O16 Si10 115(7) . . . 10_556 ? O17 Si15 O16 Si14 167.1(19) . . . . ? O17 Si15 O16 O6 108(4) . . . 10_556 ? O17 Si15 O27 Si10 118.8(18) . . . . ? O17 Si15 O27 Si10 -125(20) . . . 10_556 ? O17 Si15 O27 Si15 113(2) . . . 10_556 ? O17 Si15 O31 Si10 -155(4) . . . 3 ? O17 Si15 O31 Si10 -137(9) . . . 10_556 ? O17 Si15 O31 Si15 -160(5) . . . 12 ? O17 Si15 O31 O29 -85(13) . . . 10_556 ? O18 Si6 O17 Si10 -135.5(19) . . . 10_556 ? O18 Si6 O17 Si11 -33(6) . . . 10_556 ? O18 Si6 O17 Si15 -123.9(19) . . . . ? O18 Si6 O17 O7 -31(4) . . . 10_556 ? O18 Si6 O23 Si2 -140.5(14) . . . 10_556 ? O18 Si6 O23 Si4 -112(4) . . . . ? O18 Si6 O23 Si11 5(7) . . . 10_556 ? O18 Si6 O23 O13 -143(3) . . . 10_556 ? O18 Si6 O24 Si11 38(9) . . . 10_556 ? O18 Si6 O24 Si17 14(7) . . . . ? O18 Si6 O24 O14 -24(3) . . . 10_556 ? O18 Si7 O20 Si8 -158(3) . . . 16_545 ? O18 Si7 O20 Si12 -75(8) . . . 10_556 ? O18 Si7 O20 Si13 -159(3) . . . 7_545 ? O18 Si7 O20 O10 60(6) . . . 7_545 ? O18 Si7 O21 Si8 165.0(19) . . . 13_556 ? O18 Si7 O21 Si12 -49(6) . . . 10_556 ? O18 Si7 O21 Si13 167(2) . . . 6 ? O18 Si7 O21 O11 -141(3) . . . 13_556 ? O18 Si7 O34 Si7 -59(6) . . . 12_655 ? O18 Si7 O34 Si12 -30(6) . . . 3_655 ? O18 Si7 O34 Si12 58(4) . . . 10_556 ? O18 Si7 O34 O33 -56(6) . . . 10_556 ? O18 Si11 O7 Si6 -144(6) 10_556 . . 10_556 ? O18 Si11 O7 Si10 163.5(14) 10_556 . . . ? O18 Si11 O7 Si15 154.5(15) 10_556 . . 10_556 ? O18 Si11 O7 O17 -146(3) 10_556 . . 10_556 ? O18 Si11 O8 Si6 170(9) 10_556 . . 10_556 ? O18 Si11 O8 Si7 -62(2) 10_556 . . 10_556 ? O18 Si11 O8 Si12 -52(2) 10_556 . . . ? O18 Si11 O13 Si4 -16(3) 10_556 . . 10_556 ? O18 Si11 O13 Si6 168(7) 10_556 . . 10_556 ? O18 Si11 O13 O23 -41(3) 10_556 . . 10_556 ? O18 Si11 O14 Si6 152(8) 10_556 . . 10_556 ? O18 Si11 O14 Si17 -142.2(17) 10_556 . . . ? O18 Si11 O14 O24 -165(2) 10_556 . . 10_556 ? O18 Si12 O8 Si6 61(2) 10_556 . . 10_556 ? O18 Si12 O8 Si7 113(5) 10_556 . . 10_556 ? O18 Si12 O8 Si11 54(2) 10_556 . . . ? O18 Si12 O33 Si7 -117(7) 10_556 . . 3_655 ? O18 Si12 O33 Si7 104(5) 10_556 . . 10_556 ? O18 Si12 O33 Si12 -102(5) 10_556 . . 12_655 ? O18 Si12 O33 O34 -145(6) 10_556 . . 10_556 ? O19 Si1 O2 Si2 106.8(10) 3_655 . . 5 ? O19 Si1 O2 Si2 -106.8(10) 10_556 . . 5 ? O19 Si1 O2 Si4 106.8(10) 3_655 . . 14_556 ? O19 Si1 O2 Si4 -106.8(10) 10_556 . . 14_556 ? O19 Si1 O2 Si5 106.8(10) 3_655 . . 10_556 ? O19 Si1 O2 Si5 -106.8(10) 10_556 . . 10_556 ? O19 Si1 O2 O4 73.2(10) 10_556 . . 10_556 ? O19 Si1 O2 O4 -73.2(10) 3_655 . . 10_556 ? O19 Si1 O2 O5 -106.8(10) 10_556 . . 14_556 ? O19 Si1 O2 O5 106.8(10) 3_655 . . 14_556 ? O19 Si1 O9 Si5 12(3) 10_556 . . 10_556 ? O19 Si1 O9 Si5 -76.1(13) 3_655 . . 10_556 ? O19 Si1 O9 Si8 -152.7(12) 3_655 . . 10_556 ? O19 Si1 O9 Si8 -64(3) 10_556 . . 10_556 ? O19 Si1 O9 Si13 -60(3) 10_556 . . . ? O19 Si1 O9 Si13 -148.8(15) 3_655 . . . ? O19 Si1 O9 O19 -89(3) 3_655 . . 10_556 ? O19 Si5 O19 Si1 -68.1(13) 12_655 . . 10_556 ? O19 Si5 O19 Si8 -163.9(11) 12_655 . . . ? O19 Si5 O19 Si13 -168.1(16) 12_655 . . 10_556 ? O19 Si5 O19 O9 -55(4) 12_655 . . 10_556 ? O19 Si8 O11 Si7 66(2) . . . 13_556 ? O19 Si8 O11 Si12 58(3) . . . 6 ? O19 Si8 O11 Si13 -65(7) . . . 10_556 ? O19 Si8 O11 O21 -4(4) . . . 13_556 ? O19 Si8 O22 Si9 -145(2) . . . 10_556 ? O19 Si8 O22 Si13 66(7) . . . 10_556 ? O19 Si8 O22 Si14 -159(3) . . . . ? O19 Si8 O22 O12 145(2) . . . 10_556 ? O19 Si13 O9 Si1 61(3) 10_556 . . . ? O19 Si13 O9 Si5 29(2) 10_556 . . 10_556 ? O19 Si13 O9 Si8 83(7) 10_556 . . 10_556 ? O19 Si13 O10 Si7 100.5(19) 10_556 . . 7 ? O19 Si13 O10 Si8 37(44) 10_556 . . 10_556 ? O19 Si13 O10 Si12 94.6(18) 10_556 . . 16 ? O19 Si13 O10 O20 78(6) 10_556 . . 7 ? O19 Si13 O12 Si8 119(8) 10_556 . . 10_556 ? O19 Si13 O12 Si9 65(2) 10_556 . . . ? O19 Si13 O12 Si14 61(3) 10_556 . . 10_556 ? O19 Si13 O12 O22 31(2) 10_556 . . 10_556 ? O20 Si7 O18 Si6 -45.7(18) . . . . ? O20 Si7 O18 Si11 -39.9(19) . . . 10_556 ? O20 Si7 O18 Si12 140(5) . . . 10_556 ? O20 Si7 O18 O8 -111(2) . . . 10_556 ? O20 Si7 O21 Si8 52(2) . . . 13_556 ? O20 Si7 O21 Si12 -163(6) . . . 10_556 ? O20 Si7 O21 Si13 53(3) . . . 6 ? O20 Si7 O21 O11 106(3) . . . 13_556 ? O20 Si7 O34 Si7 87(6) . . . 12_655 ? O20 Si7 O34 Si12 -156(5) . . . 10_556 ? O20 Si7 O34 Si12 116(6) . . . 3_655 ? O20 Si7 O34 O33 90(6) . . . 10_556 ? O20 Si8 O11 Si7 -52(2) 16 . . 13_556 ? O20 Si8 O11 Si12 -60(3) 16 . . 6 ? O20 Si8 O11 Si13 177(7) 16 . . 10_556 ? O20 Si8 O11 O21 -122(3) 16 . . 13_556 ? O20 Si8 O19 Si1 -33(2) 16 . . 10_556 ? O20 Si8 O19 Si5 11(2) 16 . . . ? O20 Si8 O19 Si13 175(7) 16 . . 10_556 ? O20 Si8 O19 O9 -106(3) 16 . . 10_556 ? O20 Si8 O22 Si9 -23(3) 16 . . 10_556 ? O20 Si8 O22 Si13 -172(8) 16 . . 10_556 ? O20 Si8 O22 Si14 -37(3) 16 . . . ? O20 Si8 O22 O12 -93(2) 16 . . 10_556 ? O20 Si12 O8 Si6 -22(2) 10_556 . . 10_556 ? O20 Si12 O8 Si7 31(4) 10_556 . . 10_556 ? O20 Si12 O8 Si11 -28(2) 10_556 . . . ? O20 Si12 O8 O18 -82(2) 10_556 . . 10_556 ? O20 Si12 O33 Si7 -12(4) 10_556 . . 10_556 ? O20 Si12 O33 Si7 127(7) 10_556 . . 3_655 ? O20 Si12 O33 Si12 142(5) 10_556 . . 12_655 ? O20 Si12 O33 O34 100(6) 10_556 . . 10_556 ? O20 Si13 O9 Si1 -19(2) 7 . . . ? O20 Si13 O9 Si5 -50.4(16) 7 . . 10_556 ? O20 Si13 O9 Si8 3(6) 7 . . 10_556 ? O20 Si13 O9 O19 -80(3) 7 . . 10_556 ? O20 Si13 O10 Si7 23(5) 7 . . 7 ? O20 Si13 O10 Si8 -40(44) 7 . . 10_556 ? O20 Si13 O10 Si12 17(5) 7 . . 16 ? O20 Si13 O12 Si8 -7(7) 7 . . 10_556 ? O20 Si13 O12 Si9 -61(2) 7 . . . ? O20 Si13 O12 Si14 -65(2) 7 . . 10_556 ? O20 Si13 O12 O22 -96(2) 7 . . 10_556 ? O21 Si7 O18 Si6 -150.7(14) . . . . ? O21 Si7 O18 Si11 -144.9(15) . . . 10_556 ? O21 Si7 O18 Si12 35(5) . . . 10_556 ? O21 Si7 O18 O8 144(2) . . . 10_556 ? O21 Si7 O20 Si8 -63(3) . . . 16_545 ? O21 Si7 O20 Si12 20(7) . . . 10_556 ? O21 Si7 O20 Si13 -64(3) . . . 7_545 ? O21 Si7 O20 O10 155(5) . . . 7_545 ? O21 Si7 O34 Si7 -157(5) . . . 12_655 ? O21 Si7 O34 Si12 -128(6) . . . 3_655 ? O21 Si7 O34 Si12 -40(4) . . . 10_556 ? O21 Si7 O34 O33 -154(6) . . . 10_556 ? O21 Si8 O11 Si7 70(4) 13_556 . . 13_556 ? O21 Si8 O11 Si12 62(4) 13_556 . . 6 ? O21 Si8 O11 Si13 -61(8) 13_556 . . 10_556 ? O21 Si8 O19 Si1 -147.6(17) 13_556 . . 10_556 ? O21 Si8 O19 Si5 -104.4(19) 13_556 . . . ? O21 Si8 O19 Si13 60(6) 13_556 . . 10_556 ? O21 Si8 O19 O9 139(3) 13_556 . . 10_556 ? O21 Si8 O22 Si9 116(2) 13_556 . . 10_556 ? O21 Si8 O22 Si13 -33(7) 13_556 . . 10_556 ? O21 Si8 O22 Si14 102(3) 13_556 . . . ? O21 Si8 O22 O12 46(2) 13_556 . . 10_556 ? O21 Si12 O8 Si6 93.8(19) 10_556 . . 10_556 ? O21 Si12 O8 Si7 146(5) 10_556 . . 10_556 ? O21 Si12 O8 Si11 87.5(19) 10_556 . . . ? O21 Si12 O8 O18 33(3) 10_556 . . 10_556 ? O21 Si12 O33 Si7 -130(5) 10_556 . . 10_556 ? O21 Si12 O33 Si7 10(8) 10_556 . . 3_655 ? O21 Si12 O33 Si12 24(6) 10_556 . . 12_655 ? O21 Si12 O33 O34 -18(7) 10_556 . . 10_556 ? O21 Si13 O9 Si1 96.0(19) 6_554 . . . ? O21 Si13 O9 Si5 64.6(17) 6_554 . . 10_556 ? O21 Si13 O9 Si8 118(7) 6_554 . . 10_556 ? O21 Si13 O9 O19 35(3) 6_554 . . 10_556 ? O21 Si13 O10 Si7 -5(2) 6_554 . . 7 ? O21 Si13 O10 Si8 -68(44) 6_554 . . 10_556 ? O21 Si13 O10 Si12 -11(2) 6_554 . . 16 ? O21 Si13 O10 O20 -28(6) 6_554 . . 7 ? O21 Si13 O12 Si8 -123(8) 6_554 . . 10_556 ? O21 Si13 O12 Si9 -177.6(14) 6_554 . . . ? O21 Si13 O12 Si14 178.0(17) 6_554 . . 10_556 ? O21 Si13 O12 O22 148(2) 6_554 . . 10_556 ? O22 Si8 O11 Si7 178.1(18) . . . 13_556 ? O22 Si8 O11 Si12 170(2) . . . 6 ? O22 Si8 O11 Si13 48(7) . . . 10_556 ? O22 Si8 O11 O21 108(4) . . . 13_556 ? O22 Si8 O19 Si1 95.0(18) . . . 10_556 ? O22 Si8 O19 Si5 138.2(18) . . . . ? O22 Si8 O19 Si13 -58(6) . . . 10_556 ? O22 Si8 O19 O9 22(3) . . . 10_556 ? O22 Si9 O6 Si10 -158(2) 10_556 . . . ? O22 Si9 O6 Si14 -52(6) 10_556 . . 10_556 ? O22 Si9 O6 Si15 -145(2) 10_556 . . 10_556 ? O22 Si9 O6 O16 -64(4) 10_556 . . 10_556 ? O22 Si9 O12 Si8 -45(2) 10_556 . . 10_556 ? O22 Si9 O12 Si13 -36(2) 10_556 . . . ? O22 Si9 O12 Si14 121(8) 10_556 . . 10_556 ? O22 Si9 O25 Si14 -32(15) 10_556 . . 10_556 ? O22 Si9 O25 Si16 165.5(19) 10_556 . . . ? O22 Si9 O25 O15 172(3) 10_556 . . 10_556 ? O22 Si9 O30 Si9 66(4) 10_556 . . 12 ? O22 Si9 O30 Si14 65(2) 10_556 . . 3 ? O22 Si9 O30 Si14 61(7) 10_556 . . 10_556 ? O22 Si9 O30 O32 39(3) 10_556 . . 10_556 ? O22 Si13 O9 Si1 -131.8(17) 10_556 . . . ? O22 Si13 O9 Si5 -163.3(12) 10_556 . . 10_556 ? O22 Si13 O9 Si8 -110(7) 10_556 . . 10_556 ? O22 Si13 O9 O19 167(3) 10_556 . . 10_556 ? O22 Si13 O10 Si7 -146.7(18) 10_556 . . 7 ? O22 Si13 O10 Si8 150(45) 10_556 . . 10_556 ? O22 Si13 O10 Si12 -152.6(16) 10_556 . . 16 ? O22 Si13 O10 O20 -169(6) 10_556 . . 7 ? O22 Si13 O12 Si8 89(7) 10_556 . . 10_556 ? O22 Si13 O12 Si9 34.6(19) 10_556 . . . ? O22 Si13 O12 Si14 30(2) 10_556 . . 10_556 ? O22 Si14 O15 Si9 -99(37) . . . 10_556 ? O22 Si14 O15 Si16 2(6) . . . . ? O22 Si14 O15 O25 11(3) . . . 10_556 ? O22 Si14 O16 Si9 -126(8) . . . 10_556 ? O22 Si14 O16 Si10 -167.8(17) . . . 10_556 ? O22 Si14 O16 Si15 -177(2) . . . . ? O22 Si14 O16 O6 -112(4) . . . 10_556 ? O22 Si14 O32 Si9 170(3) . . . 3 ? O22 Si14 O32 Si9 115(8) . . . 10_556 ? O22 Si14 O32 Si14 -172(4) . . . 12 ? O22 Si14 O32 O30 138(2) . . . 10_556 ? O23 Si2 O3 Si3 122.1(9) 3 . . 5_445 ? O23 Si2 O3 Si3 122.1(9) 3 . . 14_446 ? O23 Si2 O3 Si3 -122.1(9) 10_556 . . 5_445 ? O23 Si2 O3 Si3 -122.1(9) 10_556 . . 14_446 ? O23 Si2 O3 O3 -57.9(9) 3 . . 10_556 ? O23 Si2 O3 O3 57.9(9) 10_556 . . 10_556 ? O23 Si2 O3 O4 -122.1(9) 10_556 . . 14_446 ? O23 Si2 O3 O4 122.1(9) 3 . . 14_446 ? O23 Si2 O13 Si4 -15(3) 10_556 . . 10_556 ? O23 Si2 O13 Si4 -59.8(9) 3 . . 10_556 ? O23 Si2 O13 O23 -45(3) 3 . . 10_556 ? O23 Si4 O5 Si1 -124.5(7) . . . 14_446 ? O23 Si4 O5 Si1 124.5(7) 12 . . 14_446 ? O23 Si4 O5 Si2 -124.5(7) . . . 10_556 ? O23 Si4 O5 Si2 124.5(7) 12 . . 10_556 ? O23 Si4 O5 Si5 124.5(7) 12 . . 5_445 ? O23 Si4 O5 Si5 -124.5(7) . . . 5_445 ? O23 Si4 O5 O2 -124.5(7) . . . 14_446 ? O23 Si4 O5 O2 124.5(7) 12 . . 14_446 ? O23 Si4 O23 Si2 -89.2(12) 12 . . 10_556 ? O23 Si4 O23 Si6 -133(3) 12 . . . ? O23 Si4 O23 Si11 -156(4) 12 . . 10_556 ? O23 Si4 O23 O13 -104(2) 12 . . 10_556 ? O23 Si6 O17 Si10 -39(2) . . . 10_556 ? O23 Si6 O17 Si11 64(6) . . . 10_556 ? O23 Si6 O17 Si15 -27(2) . . . . ? O23 Si6 O17 O7 66(4) . . . 10_556 ? O23 Si6 O18 Si7 87.3(15) . . . . ? O23 Si6 O18 Si11 -9(12) . . . 10_556 ? O23 Si6 O18 Si12 89(2) . . . 10_556 ? O23 Si6 O18 O8 157(3) . . . 10_556 ? O23 Si6 O24 Si11 -70(10) . . . 10_556 ? O23 Si6 O24 Si17 -94(7) . . . . ? O23 Si6 O24 O14 -131(2) . . . 10_556 ? O23 Si11 O7 Si6 111(6) 10_556 . . 10_556 ? O23 Si11 O7 Si10 58.7(18) 10_556 . . . ? O23 Si11 O7 Si15 49.7(19) 10_556 . . 10_556 ? O23 Si11 O7 O17 109(4) 10_556 . . 10_556 ? O23 Si11 O8 Si6 -164(9) 10_556 . . 10_556 ? O23 Si11 O8 Si7 -36.0(19) 10_556 . . 10_556 ? O23 Si11 O8 Si12 -25(2) 10_556 . . . ? O23 Si11 O8 O18 26(3) 10_556 . . 10_556 ? O23 Si11 O13 Si4 24(2) 10_556 . . 10_556 ? O23 Si11 O13 Si6 -152(7) 10_556 . . 10_556 ? O23 Si11 O14 Si6 -92(8) 10_556 . . 10_556 ? O23 Si11 O14 Si17 -26(2) 10_556 . . . ? O23 Si11 O14 O24 -49(3) 10_556 . . 10_556 ? O24 Si6 O17 Si10 84(2) . . . 10_556 ? O24 Si6 O17 Si11 -173(7) . . . 10_556 ? O24 Si6 O17 Si15 95(2) . . . . ? O24 Si6 O17 O7 -171(4) . . . 10_556 ? O24 Si6 O18 Si7 -32(2) . . . . ? O24 Si6 O18 Si11 -128(13) . . . 10_556 ? O24 Si6 O18 Si12 -31(3) . . . 10_556 ? O24 Si6 O18 O8 37(3) . . . 10_556 ? O24 Si6 O23 Si2 -10(2) . . . 10_556 ? O24 Si6 O23 Si4 18(4) . . . . ? O24 Si6 O23 Si11 135(8) . . . 10_556 ? O24 Si6 O23 O13 -13(3) . . . 10_556 ? O24 Si11 O7 Si6 -6(6) 10_556 . . 10_556 ? O24 Si11 O7 Si10 -58.4(18) 10_556 . . . ? O24 Si11 O7 Si15 -67.4(19) 10_556 . . 10_556 ? O24 Si11 O7 O17 -8(4) 10_556 . . 10_556 ? O24 Si11 O8 Si6 -36(8) 10_556 . . 10_556 ? O24 Si11 O8 Si7 91.4(16) 10_556 . . 10_556 ? O24 Si11 O8 Si12 102.0(17) 10_556 . . . ? O24 Si11 O8 O18 154(2) 10_556 . . 10_556 ? O24 Si11 O13 Si4 -149(2) 10_556 . . 10_556 ? O24 Si11 O13 Si6 35(6) 10_556 . . 10_556 ? O24 Si11 O13 O23 -173(3) 10_556 . . 10_556 ? O24 Si11 O14 Si6 -43(8) 10_556 . . 10_556 ? O24 Si11 O14 Si17 23(2) 10_556 . . . ? O24 Si17 O14 Si6 -49.4(19) . . . 10_556 ? O24 Si17 O14 Si6 -14(2) 10_556 . . 10_556 ? O24 Si17 O14 Si11 -24(2) 10_556 . . . ? O24 Si17 O14 Si11 -58.8(18) . . . . ? O24 Si17 O14 O24 -35(2) . . . 10_556 ? O24 Si17 O24 Si6 177(6) 10_556 . . . ? O24 Si17 O24 Si11 170(4) 10_556 . . 10_556 ? O24 Si17 O24 O14 -146(2) 10_556 . . 10_556 ? O24 Si17 O35 Si17 -22(5) 10_556 . . 3_655 ? O24 Si17 O35 Si17 -129(4) . . . 3_655 ? O24 Si17 O35 O35 -39.9(10) 10_556 . . 10_556 ? O24 Si17 O35 O35 -147.2(9) . . . 10_556 ? O25 Si9 O6 Si10 105(2) . . . . ? O25 Si9 O6 Si14 -149(7) . . . 10_556 ? O25 Si9 O6 Si15 118(2) . . . 10_556 ? O25 Si9 O6 O16 -161(4) . . . 10_556 ? O25 Si9 O12 Si8 -11.6(19) . . . 10_556 ? O25 Si9 O12 Si13 -3(2) . . . . ? O25 Si9 O12 Si14 155(8) . . . 10_556 ? O25 Si9 O12 O22 34(2) . . . 10_556 ? O25 Si9 O30 Si9 176(3) . . . 12 ? O25 Si9 O30 Si14 175(2) . . . 3 ? O25 Si9 O30 Si14 171(8) . . . 10_556 ? O25 Si9 O30 O32 149(2) . . . 10_556 ? O25 Si14 O15 Si9 -110(37) 10_556 . . 10_556 ? O25 Si14 O15 Si16 -9(4) 10_556 . . . ? O25 Si14 O16 Si9 -29(7) 10_556 . . 10_556 ? O25 Si14 O16 Si10 -71(2) 10_556 . . 10_556 ? O25 Si14 O16 Si15 -81(2) 10_556 . . . ? O25 Si14 O16 O6 -16(4) 10_556 . . 10_556 ? O25 Si14 O22 Si8 91(3) 10_556 . . . ? O25 Si14 O22 Si9 15(7) 10_556 . . 10_556 ? O25 Si14 O22 Si13 104(3) 10_556 . . 10_556 ? O25 Si14 O22 O12 146(2) 10_556 . . 10_556 ? O25 Si14 O32 Si9 13(7) 10_556 . . 10_556 ? O25 Si14 O32 Si9 69(4) 10_556 . . 3 ? O25 Si14 O32 Si14 86(5) 10_556 . . 12 ? O25 Si14 O32 O30 36(3) 10_556 . . 10_556 ? O25 Si16 O15 Si9 165(6) . . . 10_556 ? O25 Si16 O15 Si9 15(5) 10_556 . . 10_556 ? O25 Si16 O15 Si14 9(4) 10_556 . . . ? O25 Si16 O15 Si14 159(6) . . . . ? O25 Si16 O15 O25 151(3) . . . 10_556 ? O25 Si16 O25 Si9 42(3) 10_556 . . . ? O25 Si16 O25 Si14 40(3) 10_556 . . 10_556 ? O25 Si16 O25 O15 35(3) 10_556 . . 10_556 ? O25 Si16 O26 Si17 10(3) 10_556 . . 7 ? O25 Si16 O26 Si17 154(3) . . . 7 ? O25 Si16 O26 O26 162.9(6) . . . 10_556 ? O25 Si16 O26 O26 19.2(7) 10_556 . . 10_556 ? O25 Si16 O28 Si3 111.3(14) . . . . ? O25 Si16 O28 Si3 -159.4(11) 10_556 . . 10_556 ? O25 Si16 O28 Si3 -119.7(14) 10_556 . . . ? O25 Si16 O28 Si3 71.6(12) . . . 10_556 ? O25 Si16 O28 O28 26.2(6) . . . 10_556 ? O25 Si16 O28 O28 155.2(6) 10_556 . . 10_556 ? O26 Si16 O15 Si9 -66(7) 10_556 . . 10_556 ? O26 Si16 O15 Si9 -80(7) . . . 10_556 ? O26 Si16 O15 Si14 -72(6) 10_556 . . . ? O26 Si16 O15 Si14 -86(6) . . . . ? O26 Si16 O15 O25 -81(3) 10_556 . . 10_556 ? O26 Si16 O15 O25 -94(3) . . . 10_556 ? O26 Si16 O25 Si9 -98(2) . . . . ? O26 Si16 O25 Si9 -92(2) 10_556 . . . ? O26 Si16 O25 Si14 -94(2) 10_556 . . 10_556 ? O26 Si16 O25 Si14 -100(2) . . . 10_556 ? O26 Si16 O25 O15 -104(3) . . . 10_556 ? O26 Si16 O25 O15 -98(3) 10_556 . . 10_556 ? O26 Si16 O26 Si17 -9(3) 10_556 . . 7 ? O26 Si16 O28 Si3 1.4(16) . . . . ? O26 Si16 O28 Si3 -57.6(12) 10_556 . . 10_556 ? O26 Si16 O28 Si3 -17.9(15) 10_556 . . . ? O26 Si16 O28 Si3 -38.3(12) . . . 10_556 ? O26 Si16 O28 O28 -103.0(6) 10_556 . . 10_556 ? O26 Si16 O28 O28 -83.7(6) . . . 10_556 ? O26 Si17 O14 Si6 64(2) 7_545 . . 10_556 ? O26 Si17 O14 Si6 71.4(19) 16_545 . . 10_556 ? O26 Si17 O14 Si11 61.9(19) 16_545 . . . ? O26 Si17 O14 Si11 55(2) 7_545 . . . ? O26 Si17 O14 O24 78(3) 7_545 . . 10_556 ? O26 Si17 O14 O24 85(3) 16_545 . . 10_556 ? O26 Si17 O24 Si6 76(7) 16_545 . . . ? O26 Si17 O24 Si6 62(7) 7_545 . . . ? O26 Si17 O24 Si11 69(5) 16_545 . . 10_556 ? O26 Si17 O24 Si11 56(5) 7_545 . . 10_556 ? O26 Si17 O24 O14 99(2) 7_545 . . 10_556 ? O26 Si17 O24 O14 113(2) 16_545 . . 10_556 ? O26 Si17 O35 Si17 102(4) 16_545 . . 3_655 ? O26 Si17 O35 Si17 121(4) 7_545 . . 3_655 ? O26 Si17 O35 O35 83.7(6) 16_545 . . 10_556 ? O26 Si17 O35 O35 103.2(6) 7_545 . . 10_556 ? O27 Si10 O6 Si9 -76(2) . . . . ? O27 Si10 O6 Si14 -90(2) . . . 10_556 ? O27 Si10 O6 Si15 177(7) . . . 10_556 ? O27 Si10 O6 O16 -176(4) . . . 10_556 ? O27 Si10 O7 Si6 53.6(18) . . . 10_556 ? O27 Si10 O7 Si11 61.7(19) . . . . ? O27 Si10 O7 Si15 157(9) . . . 10_556 ? O27 Si10 O7 O17 10(4) . . . 10_556 ? O27 Si10 O29 Si10 68(4) . . . 12 ? O27 Si10 O29 Si15 -158(8) . . . 10_556 ? O27 Si10 O29 Si15 78(4) . . . 3 ? O27 Si10 O29 O31 154(12) . . . 10_556 ? O27 Si15 O16 Si9 46(2) . . . 10_556 ? O27 Si15 O16 Si10 2(6) . . . 10_556 ? O27 Si15 O16 Si14 54(2) . . . . ? O27 Si15 O16 O6 -5(4) . . . 10_556 ? O27 Si15 O17 Si6 -96(2) . . . . ? O27 Si15 O17 Si10 17(7) . . . 10_556 ? O27 Si15 O17 Si11 -108.3(19) . . . 10_556 ? O27 Si15 O17 O7 168(4) . . . 10_556 ? O27 Si15 O31 Si10 -20(8) . . . 10_556 ? O27 Si15 O31 Si10 -39(5) . . . 3 ? O27 Si15 O31 Si15 -44(6) . . . 12 ? O27 Si15 O31 O29 31(13) . . . 10_556 ? O28 Si3 O4 Si2 115.6(9) 3_655 . . 14_556 ? O28 Si3 O4 Si2 -115.6(9) 10_556 . . 14_556 ? O28 Si3 O4 Si2 -122.8(7) . . . 14_556 ? O28 Si3 O4 Si2 122.8(7) 12_655 . . 14_556 ? O28 Si3 O4 Si4 122.8(7) 12_655 . . 5 ? O28 Si3 O4 Si4 115.6(9) 3_655 . . 5 ? O28 Si3 O4 Si4 -122.8(7) . . . 5 ? O28 Si3 O4 Si4 -115.6(9) 10_556 . . 5 ? O28 Si3 O4 O2 -64.4(9) 3_655 . . 10_556 ? O28 Si3 O4 O2 -57.2(7) 12_655 . . 10_556 ? O28 Si3 O4 O2 64.4(9) 10_556 . . 10_556 ? O28 Si3 O4 O2 57.2(7) . . . 10_556 ? O28 Si3 O4 O3 -115.6(9) 10_556 . . 14_556 ? O28 Si3 O4 O3 -122.8(7) . . . 14_556 ? O28 Si3 O4 O3 115.6(9) 3_655 . . 14_556 ? O28 Si3 O4 O3 122.8(7) 12_655 . . 14_556 ? O28 Si3 O28 Si3 -63.7(5) 3_655 . . 10_556 ? O28 Si3 O28 Si3 -83.1(7) 12_655 . . 10_556 ? O28 Si3 O28 Si3 0.000(5) 10_556 . . 10_556 ? O28 Si3 O28 Si16 -143.9(15) 3_655 . . . ? O28 Si3 O28 Si16 -163.2(7) 12_655 . . . ? O28 Si3 O28 Si16 -80.2(13) 10_556 . . . ? O28 Si3 O28 O28 -83.1(7) 12_655 . . 10_556 ? O28 Si3 O28 O28 -63.7(5) 3_655 . . 10_556 ? O28 Si16 O15 Si9 63(7) 10_556 . . 10_556 ? O28 Si16 O15 Si9 48(7) . . . 10_556 ? O28 Si16 O15 Si14 57(6) 10_556 . . . ? O28 Si16 O15 Si14 42(6) . . . . ? O28 Si16 O15 O25 34(3) . . . 10_556 ? O28 Si16 O15 O25 48(3) 10_556 . . 10_556 ? O28 Si16 O25 Si9 146(2) . . . . ? O28 Si16 O25 Si9 155(2) 10_556 . . . ? O28 Si16 O25 Si14 153(2) 10_556 . . 10_556 ? O28 Si16 O25 Si14 144(2) . . . 10_556 ? O28 Si16 O25 O15 140(3) . . . 10_556 ? O28 Si16 O25 O15 148(3) 10_556 . . 10_556 ? O28 Si16 O26 Si17 -92(3) . . . 7 ? O28 Si16 O26 Si17 -113(3) 10_556 . . 7 ? O28 Si16 O26 O26 -82.7(5) . . . 10_556 ? O28 Si16 O26 O26 -103.5(5) 10_556 . . 10_556 ? O28 Si16 O28 Si3 45.4(10) 10_556 . . 10_556 ? O28 Si16 O28 Si3 85.1(13) 10_556 . . . ? O29 Si10 O6 Si9 45(3) . . . . ? O29 Si10 O6 Si14 31(3) . . . 10_556 ? O29 Si10 O6 Si15 -62(7) . . . 10_556 ? O29 Si10 O6 O16 -55(4) . . . 10_556 ? O29 Si10 O7 Si6 -66.3(19) . . . 10_556 ? O29 Si10 O7 Si11 -58(2) . . . . ? O29 Si10 O7 Si15 37(8) . . . 10_556 ? O29 Si10 O7 O17 -110(4) . . . 10_556 ? O29 Si10 O27 Si10 -6(4) . . . 10_556 ? O29 Si10 O27 Si15 64(19) . . . 10_556 ? O29 Si10 O27 Si15 0(2) . . . . ? O29 Si15 O16 Si9 -68(2) 10_556 . . 10_556 ? O29 Si15 O16 Si10 -112(7) 10_556 . . 10_556 ? O29 Si15 O16 Si14 -60(3) 10_556 . . . ? O29 Si15 O16 O6 -120(4) 10_556 . . 10_556 ? O29 Si15 O17 Si6 15(3) 10_556 . . . ? O29 Si15 O17 Si10 128(8) 10_556 . . 10_556 ? O29 Si15 O17 Si11 3(3) 10_556 . . 10_556 ? O29 Si15 O17 O7 -80(4) 10_556 . . 10_556 ? O29 Si15 O27 Si10 113(19) 10_556 . . 10_556 ? O29 Si15 O27 Si10 -2(2) 10_556 . . . ? O29 Si15 O27 Si15 -8(3) 10_556 . . 10_556 ? O29 Si15 O31 Si10 -52(15) 10_556 . . 10_556 ? O29 Si15 O31 Si10 -70(12) 10_556 . . 3 ? O29 Si15 O31 Si15 -75(12) 10_556 . . 12 ? O30 Si9 O6 Si10 -21(3) . . . . ? O30 Si9 O6 Si14 85(7) . . . 10_556 ? O30 Si9 O6 Si15 -7(3) . . . 10_556 ? O30 Si9 O6 O16 73(4) . . . 10_556 ? O30 Si9 O12 Si8 111.7(15) . . . 10_556 ? O30 Si9 O12 Si13 120.6(17) . . . . ? O30 Si9 O12 Si14 -82(8) . . . 10_556 ? O30 Si9 O12 O22 157(2) . . . 10_556 ? O30 Si9 O25 Si14 -161(16) . . . 10_556 ? O30 Si9 O25 Si16 36(3) . . . . ? O30 Si9 O25 O15 43(3) . . . 10_556 ? O30 Si14 O15 Si9 31(36) 10_556 . . 10_556 ? O30 Si14 O15 Si16 132(6) 10_556 . . . ? O30 Si14 O15 O25 141(3) 10_556 . . 10_556 ? O30 Si14 O16 Si9 88(7) 10_556 . . 10_556 ? O30 Si14 O16 Si10 46(2) 10_556 . . 10_556 ? O30 Si14 O16 Si15 36(3) 10_556 . . . ? O30 Si14 O16 O6 101(4) 10_556 . . 10_556 ? O30 Si14 O22 Si8 -15(4) 10_556 . . . ? O30 Si14 O22 Si9 -90(7) 10_556 . . 10_556 ? O30 Si14 O22 Si13 -1(4) 10_556 . . 10_556 ? O30 Si14 O22 O12 41(3) 10_556 . . 10_556 ? O30 Si14 O32 Si9 32(3) 10_556 . . 3 ? O30 Si14 O32 Si9 -23(8) 10_556 . . 10_556 ? O30 Si14 O32 Si14 49(4) 10_556 . . 12 ? O31 Si10 O6 Si9 50(3) 10_556 . . . ? O31 Si10 O6 Si14 36(3) 10_556 . . 10_556 ? O31 Si10 O6 Si15 -57(7) 10_556 . . 10_556 ? O31 Si10 O6 O16 -50(4) 10_556 . . 10_556 ? O31 Si10 O7 Si6 -74.9(19) 10_556 . . 10_556 ? O31 Si10 O7 Si11 -67(2) 10_556 . . . ? O31 Si10 O7 Si15 29(8) 10_556 . . 10_556 ? O31 Si10 O7 O17 -119(4) 10_556 . . 10_556 ? O31 Si10 O27 Si10 -2(4) 10_556 . . 10_556 ? O31 Si10 O27 Si15 68(19) 10_556 . . 10_556 ? O31 Si10 O27 Si15 4(2) 10_556 . . . ? O31 Si10 O29 Si10 -85(13) 10_556 . . 12 ? O31 Si10 O29 Si15 48(14) 10_556 . . 10_556 ? O31 Si10 O29 Si15 -75(12) 10_556 . . 3 ? O31 Si15 O16 Si9 -73(2) . . . 10_556 ? O31 Si15 O16 Si10 -117(7) . . . 10_556 ? O31 Si15 O16 Si14 -65(3) . . . . ? O31 Si15 O16 O6 -124(4) . . . 10_556 ? O31 Si15 O17 Si6 25(3) . . . . ? O31 Si15 O17 Si10 138(8) . . . 10_556 ? O31 Si15 O17 Si11 13(3) . . . 10_556 ? O31 Si15 O17 O7 -70(4) . . . 10_556 ? O31 Si15 O27 Si10 109(20) . . . 10_556 ? O31 Si15 O27 Si10 -7(2) . . . . ? O31 Si15 O27 Si15 -13(3) . . . 10_556 ? O32 Si9 O6 Si10 -46(3) 10_556 . . . ? O32 Si9 O6 Si14 61(7) 10_556 . . 10_556 ? O32 Si9 O6 Si15 -32(3) 10_556 . . 10_556 ? O32 Si9 O6 O16 48(4) 10_556 . . 10_556 ? O32 Si9 O12 Si8 123.1(15) 10_556 . . 10_556 ? O32 Si9 O12 Si13 132.1(18) 10_556 . . . ? O32 Si9 O12 Si14 -70(8) 10_556 . . 10_556 ? O32 Si9 O12 O22 168(2) 10_556 . . 10_556 ? O32 Si9 O25 Si14 -145(16) 10_556 . . 10_556 ? O32 Si9 O25 Si16 53(3) 10_556 . . . ? O32 Si9 O25 O15 59(3) 10_556 . . 10_556 ? O32 Si9 O30 Si9 27(4) 10_556 . . 12 ? O32 Si9 O30 Si14 26(2) 10_556 . . 3 ? O32 Si9 O30 Si14 22(8) 10_556 . . 10_556 ? O32 Si14 O15 Si9 23(36) . . . 10_556 ? O32 Si14 O15 Si16 125(6) . . . . ? O32 Si14 O15 O25 133(3) . . . 10_556 ? O32 Si14 O16 Si9 113(8) . . . 10_556 ? O32 Si14 O16 Si10 71(2) . . . 10_556 ? O32 Si14 O16 Si15 61(3) . . . . ? O32 Si14 O16 O6 126(4) . . . 10_556 ? O32 Si14 O22 Si8 -35(3) . . . . ? O32 Si14 O22 Si9 -111(8) . . . 10_556 ? O32 Si14 O22 Si13 -22(4) . . . 10_556 ? O32 Si14 O22 O12 21(2) . . . 10_556 ? O33 Si7 O18 Si6 88.1(18) 10_556 . . . ? O33 Si7 O18 Si11 93.8(18) 10_556 . . 10_556 ? O33 Si7 O18 Si12 -86(5) 10_556 . . 10_556 ? O33 Si7 O18 O8 22(3) 10_556 . . 10_556 ? O33 Si7 O20 Si8 71(4) 10_556 . . 16_545 ? O33 Si7 O20 Si12 154(8) 10_556 . . 10_556 ? O33 Si7 O20 Si13 70(3) 10_556 . . 7_545 ? O33 Si7 O20 O10 -71(6) 10_556 . . 7_545 ? O33 Si7 O21 Si8 -81(2) 10_556 . . 13_556 ? O33 Si7 O21 Si12 65(6) 10_556 . . 10_556 ? O33 Si7 O21 Si13 -79(3) 10_556 . . 6 ? O33 Si7 O21 O11 -27(4) 10_556 . . 13_556 ? O33 Si7 O34 Si7 -3(4) 10_556 . . 12_655 ? O33 Si7 O34 Si12 26(4) 10_556 . . 3_655 ? O33 Si7 O34 Si12 113(7) 10_556 . . 10_556 ? O33 Si12 O8 Si6 -128.0(19) . . . 10_556 ? O33 Si12 O8 Si7 -75(4) . . . 10_556 ? O33 Si12 O8 Si11 -134.3(17) . . . . ? O33 Si12 O8 O18 171(3) . . . 10_556 ? O34 Si7 O18 Si6 101.6(18) . . . . ? O34 Si7 O18 Si11 107.3(18) . . . 10_556 ? O34 Si7 O18 Si12 -72(5) . . . 10_556 ? O34 Si7 O18 O8 36(3) . . . 10_556 ? O34 Si7 O20 Si8 54(4) . . . 16_545 ? O34 Si7 O20 Si12 137(8) . . . 10_556 ? O34 Si7 O20 Si13 53(4) . . . 7_545 ? O34 Si7 O20 O10 -88(6) . . . 7_545 ? O34 Si7 O21 Si8 -73(2) . . . 13_556 ? O34 Si7 O21 Si12 73(6) . . . 10_556 ? O34 Si7 O21 Si13 -71(3) . . . 6 ? O34 Si7 O21 O11 -19(4) . . . 13_556 ? O34 Si12 O8 Si6 -136.4(18) 10_556 . . 10_556 ? O34 Si12 O8 Si7 -84(5) 10_556 . . 10_556 ? O34 Si12 O8 Si11 -142.7(17) 10_556 . . . ? O34 Si12 O8 O18 163(2) 10_556 . . 10_556 ? O34 Si12 O33 Si7 28(4) 10_556 . . 3_655 ? O34 Si12 O33 Si7 -112(7) 10_556 . . 10_556 ? O34 Si12 O33 Si12 42(5) 10_556 . . 12_655 ? O35 Si17 O14 Si6 -171.0(18) . . . 10_556 ? O35 Si17 O14 Si6 179.4(19) 10_556 . . 10_556 ? O35 Si17 O14 Si11 169.9(19) 10_556 . . . ? O35 Si17 O14 Si11 179.5(18) . . . . ? O35 Si17 O14 O24 -157(2) . . . 10_556 ? O35 Si17 O14 O24 -167(3) 10_556 . . 10_556 ? O35 Si17 O24 Si6 -52(7) . . . . ? O35 Si17 O24 Si6 -65(7) 10_556 . . . ? O35 Si17 O24 Si11 -72(5) 10_556 . . 10_556 ? O35 Si17 O24 Si11 -58(5) . . . 10_556 ? O35 Si17 O24 O14 -28(3) 10_556 . . 10_556 ? O35 Si17 O24 O14 -15(3) . . . 10_556 ? O35 Si17 O35 Si17 18(4) 10_556 . . 3_655 ?