Crystallography Open Database

Information card for entry 4024585

Preview

Coordinates	4024585.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H27 N2 O5 S
Calculated formula	C21 H29 N2 O5 S
Title of publication	Diastereoselective Synthesis of 2,3,6-Trisubstituted Piperidines
Authors of publication	John M. Humphrey; Eric P. Arnold; Thomas A. Chappie; John B. Feltenberger; Arthur Nagel; Wendy Simon; Melani Suarez-Contreras; Norma J. Tom; Brian T. O'Neill
Journal of publication	Journal of Organic Chemistry
Year of publication	2009
Journal volume	74
Pages of publication	4525 - 4536
a	6.213 ± 0.001 Å
b	7.676 ± 0.001 Å
c	21.575 ± 0.004 Å
α	96.05 ± 0.1°
β	90.61 ± 0.2°
γ	96.21 ± 0.1°
Cell volume	1016.95 Å³
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4024585.cif
120074	2014-07-11	Adding DOIs to range 4/02 structures.	4024585.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4024585.cif
966	2010-01-30	cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated.	4024585.cif
948	2010-01-19	cif/ Adding CIFs for the Acta-Cryst-B-2009_06/ Acta-Cryst-C-2009_12/ Acta-Cryst-E-2009_12/ J-Appl-Cryst-2009_06/ J-Org-Chem-2009/ deposition.	4024585.cif