Crystallography Open Database

Information card for entry 4026610

Preview

Coordinates	4026610.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H39 N O7
Calculated formula	C25 H39 N O7
Title of publication	Asymmetric Synthesis of Cyclohexene Nucleoside Analogues
Authors of publication	Sylvain Dalençon; Ramzi Aït Youcef; Muriel Pipelier; Vincent Maisonneuve; Didier Dubreuil; François Huet; Stéphanie Legoupy
Journal of publication	Journal of Organic Chemistry
Year of publication	2011
Journal volume	76
Pages of publication	8059 - 8063
a	10.244 ± 0.003 Å
b	9.692 ± 0.009 Å
c	13.701 ± 0.015 Å
α	90°
β	97.53 ± 0.08°
γ	90°
Cell volume	1349 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0444
Residual factor for significantly intense reflections	0.037
Weighted residual factors for significantly intense reflections	0.1139
Weighted residual factors for all reflections included in the refinement	0.1295
Goodness-of-fit parameter for all reflections included in the refinement	1.216
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178445 (current)	2016-03-21	cif/4/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/02/66.	4026610.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4026610.cif
39727	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4026610 via cif-deposit CGI script.	4026610.cif