Crystallography Open Database

Information card for entry 4030873

Preview

Coordinates	4030873.cif

Structure parameters

Formula	C60 H63 Li N4 Sn4
Title of publication	[Li(NH3)4][Sn(SnPh3)3].C6H6, crystal structure of a stannide with trigonal pyramidal tin skeleton
Authors of publication	Flacke, F.; Jacobs, H.
Journal of publication	European Journal of Solid State and Inorganic Chemistry
Year of publication	1997
Journal volume	34
Pages of publication	495 - 501
a	12.305 ± 0.003 Å
b	12.421 ± 0.003 Å
c	20.448 ± 0.002 Å
α	78.84 ± 0.01°
β	89.58 ± 0.01°
γ	73.37 ± 0.02°
Cell volume	2934.1 ± 1.1 Å³
Ambient diffraction temperature	293 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.066
Weighted residual factors for significantly intense reflections	0.155
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	No
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
191028 (current)	2017-01-27	cif/ (antanas@echidna.ibt.lt) Changing atom parameters to '?' in entries 1519045, 1519046, 1519049, 1519058, 1520510, 4030776, 4030873 to indicate that atomic coordinates in these entries are unknown.	4030873.cif
176467	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4030873.cif
134418	2015-03-26	cif/ Adding structures of 4030873 via cif-deposit CGI script.	4030873.cif