#------------------------------------------------------------------------------ #$Date: 2019-11-11 16:43:52 +0200 (Mon, 11 Nov 2019) $ #$Revision: 226602 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/03/51/4035116.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4035116 loop_ _publ_author_name 'Liu, Zhi-Wen' 'Zhang, Jian' 'Li, Song-Tao' 'Liu, Ming-Qun' 'Huang, Xiao-Jun' 'Ao, Yun-Lin' 'Fan, Chun-Lin' 'Zhang, Dong-Mei' 'Zhang, Qing-Wen' 'Ye, Wen-Cai' 'Zhang, Xiao-Qi' _publ_section_title ; Ervadivamines A and B, Two Unusual Trimeric Monoterpenoid Indole Alkaloids from Ervatamia divaricata. ; _journal_issue 17 _journal_name_full 'The Journal of organic chemistry' _journal_page_first 10613 _journal_page_last 10618 _journal_paper_doi 10.1021/acs.joc.8b01371 _journal_volume 83 _journal_year 2018 _chemical_absolute_configuration ad _chemical_formula_moiety 'C62 H78 N6 O5' _chemical_formula_sum 'C62 H78 N6 O5' _chemical_formula_weight 987.30 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _audit_creation_date 2018-03-25 _audit_creation_method ; Olex2 1.2 (compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.6557(2) _cell_length_b 17.4453(3) _cell_length_c 29.2029(5) _cell_measurement_reflns_used 27848 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 73.4600 _cell_measurement_theta_min 4.6020 _cell_volume 6447.49(19) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _diffrn_ambient_temperature 100.00(10) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0617 _diffrn_reflns_av_unetI/netI 0.0393 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 35 _diffrn_reflns_limit_l_min -36 _diffrn_reflns_number 60833 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.987 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.768 _diffrn_reflns_theta_min 3.807 _diffrn_source 'micro-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 0.508 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.68705 _exptl_absorpt_correction_type multi-scan _exptl_crystal_colour colorless? _exptl_crystal_density_diffrn 1.017 _exptl_crystal_description block _exptl_crystal_F_000 2128 _exptl_crystal_size_max 0.29 _exptl_crystal_size_mid 0.26 _exptl_crystal_size_min 0.25 _refine_diff_density_max 0.209 _refine_diff_density_min -0.163 _refine_diff_density_rms 0.037 _refine_ls_abs_structure_details ; Flack x determined using 4787 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.95(9) _refine_ls_extinction_coef 0.00024(7) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_goodness_of_fit_ref 1.029 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 667 _refine_ls_number_reflns 12883 _refine_ls_number_restraints 7 _refine_ls_restrained_S_all 1.035 _refine_ls_R_factor_all 0.0461 _refine_ls_R_factor_gt 0.0423 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0579P)^2^+0.7029P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1084 _refine_ls_wR_factor_ref 0.1116 _reflns_Friedel_coverage 0.809 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.981 _reflns_number_gt 11907 _reflns_number_total 12883 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jo8b01371_si_003.cif _cod_data_source_block e_l_2_sq _cod_original_cell_volume 6447.47(18) _cod_database_code 4035116 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2. Rigid bond restraints C3, C14 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 3. Uiso/Uaniso restraints and constraints C3 \\sim C14: within 1.7A with sigma of 0.01 and sigma for terminal atoms of 0.08 4.a Ternary CH refined with riding coordinates: C3*(H3*), C21(H21), C3'(H3'), C5'(H5'), C5*(H5*), C16'(H16'), C16*(H16*), C15* (H15*), C15'(H15'), C16(H16), C20*(H20*), C20(H20), C20'(H20'), C14(H14) 4.b Secondary CH2 refined with riding coordinates: C6'(H6'A,H6'B), C21*(H21A,H21B), C6*(H6*A,H6*B), C14*(H14A,H14B), C14'(H14C, H14D), C21'(H21C,H21D), C19*(H19A,H19B), C19'(H19C,H19D), C19(H19E,H19F), C6(H6A,H6B), C5(H5A,H5B), C15(H15A,H15B), C17(H17A,H17B), C3(H3A,H3B) 4.c Aromatic/amide H refined with riding coordinates: N1*(H1*), N1'(H1'), C12(H12), C9*(H9*), C12*(H12*), C9(H9), C10*(H10*), C12'(H12'), C9'(H9'), C11*(H11*), C11'(H11'), C10'(H10') 4.d Idealised Me refined as rotating group: C23*(H23A,H23B,H23C), C24*(H24A,H24B,H24C), C24'(H24D,H24E,H24F), C18(H18A, H18B,H18C), C23'(H23D,H23E,H23F), C18*(H18D,H18E,H18F), C22(H22A,H22B,H22C), C18'(H18G,H18H,H18I) ; _platon_squeeze_void_probe_radius 1.20 _shelx_res_file ; e_l_2_sq.res created by SHELXL-2014/7 TITL e_l_2_a.res in P2(1)2(1)2(1) REM Old TITL E_L_2 in P212121 #19 REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.145, Rweak 0.039, Alpha 0.007, Orientation as input REM Flack x = 0.157 ( 0.085 ) from Parsons' quotients REM Formula found by SHELXT: C62 N8 O7 CELL 1.54184 12.655664 17.445297 29.202915 90 90 90 ZERR 4 0.000214 0.00025 0.000461 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 248 312 24 20 DELU C3 C14 SIMU 0.01 0.08 1.7 C3 C14 L.S. 30 0 81 PLAN 20 BOND $H MORE -1 CONF ABIN fmap 2 53 acta REM REM REM WGHT 0.057900 0.702900 EXTI 0.000241 FVAR 0.34191 O1* 4 0.727863 0.421082 0.540102 11.00000 0.04120 0.02598 = 0.04919 -0.00172 0.00875 0.00127 O1' 4 0.375640 0.936074 0.684620 11.00000 0.05329 0.03240 = 0.03588 -0.00434 -0.00888 0.01073 O2' 4 0.547804 0.965096 0.692598 11.00000 0.05767 0.02817 = 0.04070 0.00389 0.00437 -0.00203 O2* 4 0.856753 0.495447 0.568267 11.00000 0.03662 0.03953 = 0.04275 -0.00021 0.00699 0.00175 O1 4 0.166168 0.728863 0.651381 11.00000 0.03294 0.04243 = 0.05149 -0.00936 0.00494 0.00458 N1* 3 0.596333 0.514388 0.637811 11.00000 0.02970 0.02692 = 0.02899 0.00423 0.00295 -0.00464 AFIX 43 H1* 2 0.552349 0.478503 0.644473 11.00000 -1.20000 AFIX 0 N1 3 0.426944 0.516628 0.570967 11.00000 0.02993 0.02353 = 0.02728 -0.00177 0.00031 -0.00047 N1' 3 0.472239 0.828882 0.593767 11.00000 0.04176 0.02629 = 0.02653 0.00083 0.00144 0.00328 AFIX 43 H1' 2 0.416843 0.831487 0.576782 11.00000 -1.20000 AFIX 0 N4' 3 0.606719 0.796787 0.785798 11.00000 0.04377 0.03686 = 0.02664 -0.00164 -0.00167 0.00667 N4* 3 0.795495 0.674378 0.480380 11.00000 0.05278 0.03365 = 0.03060 -0.00065 0.01036 -0.01134 C13 1 0.372202 0.576170 0.591455 11.00000 0.03331 0.02549 = 0.02221 0.00020 0.00059 -0.00015 C11 1 0.337703 0.693103 0.631036 11.00000 0.03305 0.02683 = 0.02343 0.00103 0.00166 0.00108 C2' 1 0.476014 0.795630 0.637025 11.00000 0.03858 0.02042 = 0.02490 -0.00155 0.00426 0.00140 C12 1 0.409194 0.644205 0.610917 11.00000 0.03207 0.02624 = 0.02228 0.00279 0.00077 -0.00012 AFIX 43 H12 2 0.480777 0.656208 0.610283 11.00000 -1.20000 AFIX 0 C3* 1 0.538514 0.519795 0.557070 11.00000 0.02999 0.02326 = 0.02784 -0.00094 0.00398 -0.00116 AFIX 13 H3* 2 0.560709 0.466843 0.551324 11.00000 -1.20000 AFIX 0 C2* 1 0.606030 0.549211 0.595506 11.00000 0.03007 0.02295 = 0.02574 0.00043 0.00328 0.00431 C8 1 0.264894 0.555926 0.592006 11.00000 0.03019 0.03237 = 0.02948 0.00041 -0.00275 -0.00040 C8' 1 0.638270 0.841657 0.618976 11.00000 0.04051 0.02976 = 0.02946 -0.00607 0.00628 -0.00229 C13' 1 0.569401 0.856754 0.582261 11.00000 0.05450 0.02389 = 0.02832 -0.00452 0.00595 -0.00166 C7 1 0.255376 0.482321 0.571258 11.00000 0.03270 0.03545 = 0.03306 -0.00459 -0.00195 -0.00245 C7' 1 0.577814 0.801939 0.653507 11.00000 0.03750 0.02690 = 0.02751 -0.00454 0.00363 0.00152 C22' 1 0.459652 0.922732 0.701311 11.00000 0.05078 0.02551 = 0.02651 -0.00596 0.00148 0.00779 C7* 1 0.684895 0.603693 0.597114 11.00000 0.03181 0.02425 = 0.02885 -0.00263 0.00478 0.00001 C9* 1 0.808459 0.640218 0.664737 11.00000 0.03310 0.03707 = 0.03508 -0.00437 0.00488 -0.00562 AFIX 43 H9* 2 0.847792 0.676831 0.649077 11.00000 -1.20000 AFIX 0 C2 1 0.355525 0.459514 0.558565 11.00000 0.03229 0.02534 = 0.03006 0.00040 -0.00021 -0.00384 C21 1 0.341005 0.314514 0.557354 11.00000 0.03864 0.03059 = 0.03800 -0.00328 -0.00091 -0.00807 AFIX 13 H21 2 0.350275 0.316257 0.590654 11.00000 -1.20000 AFIX 0 C8* 1 0.726384 0.601517 0.642807 11.00000 0.02946 0.02883 = 0.03147 -0.00317 0.00471 -0.00008 C13* 1 0.667842 0.546093 0.667397 11.00000 0.03093 0.02952 = 0.02921 -0.00125 0.00213 -0.00142 C10 1 0.228670 0.674500 0.630772 11.00000 0.03201 0.03610 = 0.03051 -0.00071 0.00368 0.00463 C3' 1 0.375898 0.764247 0.656796 11.00000 0.03383 0.02609 = 0.02796 -0.00155 0.00218 0.00467 AFIX 13 H3' 2 0.321262 0.803801 0.654111 11.00000 -1.20000 AFIX 0 N4 3 0.229039 0.306478 0.547029 11.00000 0.04011 0.04703 = 0.08044 -0.02644 -0.00068 -0.00829 C5' 1 0.594055 0.831878 0.739438 11.00000 0.03722 0.03109 = 0.02636 -0.00124 0.00048 0.00304 AFIX 13 H5' 2 0.642690 0.875508 0.737824 11.00000 -1.20000 AFIX 0 C6' 1 0.621740 0.777623 0.698866 11.00000 0.03601 0.03073 = 0.03237 -0.00182 0.00236 0.00521 AFIX 23 H6'A 2 0.698021 0.774268 0.696329 11.00000 -1.20000 H6'B 2 0.595490 0.726719 0.705880 11.00000 -1.20000 AFIX 0 C5* 1 0.791523 0.625295 0.521742 11.00000 0.03954 0.02930 = 0.03287 -0.00041 0.00849 -0.00717 AFIX 13 H5* 2 0.863816 0.620891 0.533476 11.00000 -1.20000 AFIX 0 C16' 1 0.481425 0.864497 0.738416 11.00000 0.04028 0.02765 = 0.02524 -0.00400 0.00116 0.00459 AFIX 13 H16' 2 0.477069 0.894567 0.766699 11.00000 -1.20000 AFIX 0 C22* 1 0.775183 0.481328 0.540074 11.00000 0.03575 0.03355 = 0.03701 -0.00368 0.01045 0.00344 C16* 1 0.757204 0.545246 0.505843 11.00000 0.03612 0.03122 = 0.03224 -0.00499 0.01054 -0.00232 AFIX 13 H16* 2 0.806229 0.533300 0.480866 11.00000 -1.20000 AFIX 0 C12* 1 0.689221 0.530061 0.713663 11.00000 0.04299 0.04067 = 0.03221 0.00623 -0.00183 -0.00404 AFIX 43 H12* 2 0.649577 0.494291 0.729861 11.00000 -1.20000 AFIX 0 C9 1 0.191751 0.607236 0.611957 11.00000 0.02838 0.03990 = 0.03800 -0.00302 0.00003 -0.00014 AFIX 43 H9 2 0.119987 0.595789 0.612373 11.00000 -1.20000 AFIX 0 C15* 1 0.648403 0.543484 0.482914 11.00000 0.04261 0.03070 = 0.02846 -0.00244 0.00752 -0.00677 AFIX 13 H15* 2 0.638169 0.491632 0.470788 11.00000 -1.20000 AFIX 0 C21* 1 0.693570 0.677756 0.456492 11.00000 0.05740 0.03851 = 0.02962 0.00599 0.00999 -0.00372 AFIX 23 H21A 2 0.700820 0.710230 0.429713 11.00000 -1.20000 H21B 2 0.641789 0.701246 0.476562 11.00000 -1.20000 AFIX 0 C10* 1 0.830729 0.623574 0.710011 11.00000 0.03718 0.04699 = 0.03815 -0.00414 -0.00203 -0.00534 AFIX 43 H10* 2 0.886036 0.648763 0.724615 11.00000 -1.20000 AFIX 0 C6* 1 0.722279 0.658766 0.560881 11.00000 0.04355 0.02526 = 0.02952 -0.00120 0.00690 -0.00826 AFIX 23 H6*A 2 0.762232 0.699066 0.575845 11.00000 -1.20000 H6*B 2 0.660608 0.682461 0.547146 11.00000 -1.20000 AFIX 0 C14* 1 0.550522 0.562910 0.511781 11.00000 0.03540 0.03332 = 0.02779 0.00195 0.00162 -0.00308 AFIX 23 H14A 2 0.551804 0.617395 0.518383 11.00000 -1.20000 H14B 2 0.488225 0.553035 0.493352 11.00000 -1.20000 AFIX 0 C14' 1 0.383326 0.740465 0.707647 11.00000 0.03900 0.02994 = 0.02760 -0.00124 0.00271 -0.00142 AFIX 23 H14C 2 0.443009 0.705957 0.710708 11.00000 -1.20000 H14D 2 0.320349 0.711229 0.714953 11.00000 -1.20000 AFIX 0 C15' 1 0.395267 0.803722 0.744409 11.00000 0.03731 0.03211 = 0.02669 -0.00138 0.00219 0.00067 AFIX 13 H15' 2 0.327536 0.830782 0.746215 11.00000 -1.20000 AFIX 0 C16 1 0.390220 0.386885 0.536179 11.00000 0.04559 0.02697 = 0.04101 -0.00481 0.00667 -0.00435 AFIX 13 H16 2 0.466994 0.383057 0.539910 11.00000 -1.20000 AFIX 0 C20* 1 0.652420 0.598753 0.441347 11.00000 0.04981 0.04234 = 0.02727 0.00034 0.00756 -0.00970 AFIX 13 H20* 2 0.579522 0.605979 0.430885 11.00000 -1.20000 AFIX 0 C12' 1 0.603147 0.895635 0.542862 11.00000 0.06226 0.03307 = 0.03072 -0.00066 0.00773 -0.00180 AFIX 43 H12' 2 0.557244 0.904515 0.518565 11.00000 -1.20000 AFIX 0 C21' 1 0.527651 0.736337 0.795324 11.00000 0.05860 0.03120 = 0.02574 0.00094 -0.00049 0.00436 AFIX 23 H21C 2 0.539001 0.716902 0.826054 11.00000 -1.20000 H21D 2 0.538623 0.694242 0.774151 11.00000 -1.20000 AFIX 0 C20 1 0.399917 0.244441 0.538355 11.00000 0.04378 0.02833 = 0.04295 -0.00459 -0.00154 -0.00388 AFIX 13 H20 2 0.475602 0.252027 0.543816 11.00000 -1.20000 AFIX 0 C19* 1 0.715565 0.566911 0.400460 11.00000 0.05840 0.05387 = 0.02876 -0.00337 0.01218 -0.01410 AFIX 23 H19A 2 0.715284 0.604863 0.376185 11.00000 -1.20000 H19B 2 0.788332 0.559632 0.409944 11.00000 -1.20000 AFIX 0 C20' 1 0.413036 0.763923 0.791183 11.00000 0.04729 0.03333 = 0.02792 0.00122 0.00379 -0.00127 AFIX 13 H20' 2 0.368407 0.718017 0.791397 11.00000 -1.20000 AFIX 0 C9' 1 0.743017 0.866948 0.616522 11.00000 0.04608 0.04321 = 0.03739 -0.01012 0.00779 -0.01030 AFIX 43 H9' 2 0.789345 0.857697 0.640616 11.00000 -1.20000 AFIX 0 C11* 1 0.771287 0.569401 0.734169 11.00000 0.04378 0.05203 = 0.03097 0.00430 -0.00573 -0.00112 AFIX 43 H11* 2 0.787363 0.559660 0.764694 11.00000 -1.20000 AFIX 0 C19' 1 0.377481 0.813745 0.831806 11.00000 0.05353 0.04565 = 0.02904 -0.00303 0.00772 0.00413 AFIX 23 H19C 2 0.430641 0.852731 0.837296 11.00000 -1.20000 H19D 2 0.312403 0.839682 0.823571 11.00000 -1.20000 AFIX 0 C23* 1 0.871898 0.440164 0.604404 11.00000 0.04156 0.04931 = 0.04605 0.00324 0.00601 0.00917 AFIX 137 H23A 2 0.894548 0.392313 0.591474 11.00000 -1.50000 H23B 2 0.806543 0.432792 0.620500 11.00000 -1.50000 H23C 2 0.924682 0.458595 0.625288 11.00000 -1.50000 AFIX 0 C19 1 0.367289 0.169632 0.561412 11.00000 0.05540 0.03358 = 0.04543 -0.00260 -0.00146 -0.01272 AFIX 23 H19E 2 0.366904 0.176985 0.594336 11.00000 -1.20000 H19F 2 0.295932 0.156749 0.552043 11.00000 -1.20000 AFIX 0 C24* 1 0.831711 0.751798 0.492063 11.00000 0.07022 0.03569 = 0.03458 -0.00212 0.01350 -0.01835 AFIX 137 H24A 2 0.780371 0.776183 0.511388 11.00000 -1.50000 H24B 2 0.840442 0.781205 0.464536 11.00000 -1.50000 H24C 2 0.898028 0.748686 0.507914 11.00000 -1.50000 AFIX 0 C6 1 0.154005 0.439719 0.563691 11.00000 0.03448 0.04835 = 0.05403 -0.01393 -0.00224 -0.00565 AFIX 23 H6A 2 0.132255 0.447669 0.532197 11.00000 -1.20000 H6B 2 0.100275 0.462364 0.583136 11.00000 -1.20000 AFIX 0 C11' 1 0.706264 0.920189 0.541325 11.00000 0.07726 0.03611 = 0.03768 -0.00081 0.01715 -0.01473 AFIX 43 H11' 2 0.729897 0.946768 0.515689 11.00000 -1.20000 AFIX 0 C24' 1 0.713212 0.769126 0.793619 11.00000 0.05263 0.05354 = 0.03511 -0.00520 -0.00757 0.01776 AFIX 137 H24D 2 0.726469 0.725606 0.774338 11.00000 -1.50000 H24E 2 0.720834 0.754427 0.825125 11.00000 -1.50000 H24F 2 0.762857 0.809026 0.786573 11.00000 -1.50000 AFIX 0 C18 1 0.440152 0.103297 0.549775 11.00000 0.06281 0.02874 = 0.06535 0.00187 -0.01056 -0.00766 AFIX 137 H18A 2 0.444590 0.097850 0.517119 11.00000 -1.50000 H18B 2 0.412685 0.056918 0.562865 11.00000 -1.50000 H18C 2 0.509255 0.113177 0.561981 11.00000 -1.50000 AFIX 0 C5 1 0.156252 0.353923 0.572789 11.00000 0.03939 0.04703 = 0.07997 -0.01518 0.00969 -0.01519 AFIX 23 H5A 2 0.171593 0.346651 0.605041 11.00000 -1.20000 H5B 2 0.085576 0.334312 0.567504 11.00000 -1.20000 AFIX 0 C15 1 0.381651 0.242770 0.485530 11.00000 0.05516 0.03536 = 0.04252 -0.00903 0.00319 -0.00438 AFIX 23 H15A 2 0.449044 0.244961 0.469764 11.00000 -1.20000 H15B 2 0.346646 0.195424 0.476974 11.00000 -1.20000 AFIX 0 C10' 1 0.777373 0.906081 0.577722 11.00000 0.05593 0.04807 = 0.04681 -0.01012 0.01691 -0.01733 AFIX 43 H10' 2 0.846951 0.922910 0.575746 11.00000 -1.20000 AFIX 0 C23' 1 0.536017 1.023857 0.658070 11.00000 0.09230 0.03269 = 0.04543 0.00863 0.00835 -0.00123 AFIX 137 H23D 2 0.532550 1.000439 0.628359 11.00000 -1.50000 H23E 2 0.595437 1.058003 0.659287 11.00000 -1.50000 H23F 2 0.472236 1.052152 0.663633 11.00000 -1.50000 AFIX 0 C18* 1 0.674315 0.491668 0.381247 11.00000 0.07384 0.06075 = 0.03877 -0.01060 0.00874 -0.02269 AFIX 137 H18D 2 0.709547 0.480543 0.352903 11.00000 -1.50000 H18E 2 0.599661 0.495753 0.375956 11.00000 -1.50000 H18F 2 0.687685 0.451186 0.402748 11.00000 -1.50000 AFIX 0 C14 1 0.314602 0.310087 0.471743 11.00000 0.09356 0.06145 = 0.04196 -0.01877 -0.02100 0.02341 AFIX 13 H14 2 0.301487 0.308465 0.438683 11.00000 -1.20000 AFIX 0 C22 1 0.055196 0.716365 0.649828 11.00000 0.03222 0.06199 = 0.07492 -0.01467 0.00744 0.00562 AFIX 137 H22A 2 0.032877 0.711927 0.618522 11.00000 -1.50000 H22B 2 0.019472 0.758743 0.663974 11.00000 -1.50000 H22C 2 0.038319 0.669988 0.665940 11.00000 -1.50000 AFIX 0 C18' 1 0.359831 0.770113 0.875166 11.00000 0.10436 0.06539 = 0.03268 0.00298 0.01824 0.01078 AFIX 137 H18G 2 0.303991 0.733618 0.870723 11.00000 -1.50000 H18H 2 0.340638 0.805037 0.899171 11.00000 -1.50000 H18I 2 0.423525 0.743651 0.883464 11.00000 -1.50000 AFIX 0 C17 1 0.366349 0.384885 0.484190 11.00000 0.20165 0.03445 = 0.03656 -0.00386 0.00871 0.01054 AFIX 23 H17A 2 0.319955 0.427080 0.476209 11.00000 -1.20000 H17B 2 0.431558 0.390701 0.467084 11.00000 -1.20000 AFIX 0 C3 1 0.210808 0.306225 0.497236 11.00000 0.07169 0.15279 = 0.09755 -0.08348 -0.04301 0.03769 AFIX 23 H3A 2 0.167305 0.349820 0.488894 11.00000 -1.20000 H3B 2 0.173334 0.259904 0.488643 11.00000 -1.20000 AFIX 0 HKLF 4 REM e_l_2_a.res in P2(1)2(1)2(1) REM R1 = 0.0423 for 11907 Fo > 4sig(Fo) and 0.0461 for all 12883 data REM 667 parameters refined using 7 restraints END WGHT 0.0579 0.7013 REM Highest difference peak 0.209, deepest hole -0.163, 1-sigma level 0.037 Q1 1 0.5631 0.8804 0.8242 11.00000 0.05 0.21 Q2 1 0.5997 0.8382 0.7999 11.00000 0.05 0.20 Q3 1 0.5341 0.9023 0.8339 11.00000 0.05 0.19 Q4 1 0.1226 0.1634 0.5005 11.00000 0.05 0.18 Q5 1 0.4008 0.4343 0.6654 11.00000 0.05 0.16 Q6 1 0.1862 0.2187 0.5075 11.00000 0.05 0.15 Q7 1 0.4240 0.3791 0.5007 11.00000 0.05 0.15 Q8 1 0.3189 0.5782 0.5845 11.00000 0.05 0.15 Q9 1 0.2464 0.5216 0.5814 11.00000 0.05 0.14 Q10 1 0.3662 0.6538 0.6358 11.00000 0.05 0.14 Q11 1 0.3948 0.5584 0.5834 11.00000 0.05 0.14 Q12 1 0.2082 0.2811 0.5056 11.00000 0.05 0.14 Q13 1 0.3280 0.3812 0.5580 11.00000 0.05 0.14 Q14 1 0.5843 0.6816 0.8423 11.00000 0.05 0.14 Q15 1 0.4284 0.8158 0.7956 11.00000 0.05 0.14 Q16 1 0.7843 0.5822 0.5189 11.00000 0.05 0.14 Q17 1 0.4319 0.8394 0.7410 11.00000 0.05 0.13 Q18 1 0.4852 0.8929 0.7271 11.00000 0.05 0.13 Q19 1 0.3033 0.4582 0.5799 11.00000 0.05 0.13 Q20 1 0.2842 0.7024 0.6159 11.00000 0.05 0.13 ; _shelx_res_checksum 93800 _shelx_hkl_file ; 0 0 3 0.35 0.49 0 0 -3 0.43 0.43 0 0 -3 0.16 0.40 0 0 -4 175.49 5.25 0 0 4 206.84 5.20 0 0 5 0.08 0.53 0 0 -5 0.38 0.63 0 0 -5 0.80 0.79 0 0 6 51.95 3.37 0 0 -6 53.99 4.06 0 0 -7 0.78 0.58 0 0 -7 1.02 1.23 0 0 7 1.68 0.93 0 0 -7 -0.65 0.94 0 0 -8 823.61 16.31 0 0 -8 807.32 11.18 0 0 9 1.13 1.23 0 0 -9 -0.69 1.03 0 0 -9 0.12 0.59 0 0 -9 1.82 1.23 0 0 -10 102.54 6.78 0 0 10 137.17 6.73 0 0 -10 84.01 3.94 0 0 -10 117.85 7.25 0 0 -11 -0.79 1.53 0 0 -11 0.07 0.49 0 0 11 0.09 0.97 0 0 -11 1.07 1.13 0 0 -12 1211.07 25.09 0 0 -12 1217.61 15.10 0 0 -12 1233.05 25.20 0 0 13 -0.43 1.40 0 0 -13 0.62 1.07 0 0 13 0.25 1.16 0 0 -13 0.07 1.25 0 0 -14 920.07 23.96 0 0 14 762.26 19.12 0 0 14 784.51 23.62 0 0 -14 984.46 24.83 0 0 -15 -0.24 1.33 0 0 15 0.90 1.14 0 0 -15 1.57 1.74 0 0 15 -0.76 1.99 0 0 -16 197.73 12.71 0 0 16 222.94 11.68 0 0 -16 247.74 13.83 0 0 16 233.77 14.36 0 0 -16 219.38 12.71 0 0 -17 -0.68 1.27 0 0 -17 -1.01 1.23 0 0 17 -0.26 1.42 0 0 -17 0.29 1.70 0 0 17 -0.28 1.31 0 0 18 48.78 7.49 0 0 -18 38.13 6.10 0 0 -18 27.73 4.97 0 0 18 45.92 6.00 0 0 -18 38.59 6.19 0 0 19 -0.76 1.53 0 0 -19 -0.73 1.92 0 0 19 0.18 1.48 0 0 -19 -1.60 1.70 0 0 20 415.39 21.91 0 0 20 400.85 18.40 0 0 -20 417.67 19.92 0 0 -21 2.76 2.39 0 0 -21 0.17 1.03 0 0 -21 0.44 1.35 0 0 21 4.41 2.26 0 0 21 0.08 1.53 0 0 -22 325.89 15.47 0 0 -22 331.63 15.15 0 0 22 345.67 21.26 0 0 -23 -1.81 1.58 0 0 -23 0.81 1.59 0 0 23 -1.32 1.90 0 0 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39.30 5.72 0 -1 -18 47.30 7.03 0 1 18 51.71 6.70 0 1 -18 40.10 6.21 0 1 -18 45.57 6.54 0 -1 18 49.17 7.02 0 1 -18 33.55 5.42 0 1 18 55.80 7.53 0 -1 18 51.12 5.89 0 1 -19 56.22 7.73 0 1 -19 56.28 7.14 0 -1 19 77.93 7.65 0 1 -19 61.17 7.67 0 -1 -19 54.83 7.89 0 -1 19 70.68 8.98 0 1 19 62.84 7.40 0 -1 -19 63.39 7.59 0 1 19 75.84 9.11 0 1 -20 221.85 15.50 0 1 20 303.06 19.07 0 -1 20 288.44 18.04 0 -1 -20 221.33 16.10 0 -1 -20 187.52 13.39 0 1 20 247.60 14.96 0 1 -21 272.20 13.46 0 -1 -21 265.08 13.43 0 1 21 307.58 17.36 0 -1 -21 288.59 13.58 0 1 -21 252.86 13.13 0 1 21 336.40 20.44 0 -1 21 332.73 19.94 0 -1 -21 291.69 18.59 0 -1 -22 34.97 4.91 0 -1 -22 37.20 6.82 0 -1 22 40.31 7.21 0 1 -22 30.20 4.80 0 1 22 37.24 5.03 0 1 22 37.22 6.17 0 1 -22 37.29 5.16 0 -1 -22 31.58 5.07 0 1 22 40.91 7.39 0 -1 -23 167.44 11.17 0 -1 23 194.38 16.04 0 1 23 167.79 10.55 0 1 -23 152.61 10.90 0 1 23 171.91 13.95 0 -1 -23 174.32 11.12 0 1 -23 172.62 11.41 0 1 23 191.13 16.24 0 1 -24 56.82 6.87 0 1 24 89.58 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5.99 0 -6 -2 73.01 6.53 0 6 -2 37.74 4.20 0 6 -2 38.08 4.95 0 6 2 39.17 4.26 0 6 -2 65.36 3.44 0 -6 2 69.72 5.98 0 6 2 64.60 4.77 0 -6 2 80.26 6.15 0 -6 -3 15.08 2.96 0 6 3 80.37 6.20 0 -6 3 15.49 3.09 0 6 3 23.36 3.23 0 6 -3 88.37 6.75 0 6 -3 71.34 5.83 0 -6 -3 21.01 3.84 0 -6 3 26.19 4.20 0 6 3 82.20 6.51 0 6 4 429.13 14.44 0 6 -4 429.89 14.91 0 -6 -4 479.10 16.93 0 -6 4 494.61 15.99 0 6 4 495.31 13.95 0 -6 4 484.79 14.52 0 -6 -4 501.95 16.89 0 6 -4 397.52 13.42 0 6 4 412.18 14.62 0 -6 5 65.42 5.94 0 6 -5 106.40 7.46 0 6 5 92.14 6.90 0 -6 -5 52.52 5.94 0 6 -5 90.19 6.55 0 6 5 94.52 6.97 0 6 5 60.84 5.24 0 -6 5 62.98 5.23 0 6 6 1198.90 23.38 0 6 6 1210.24 25.03 0 6 -6 1196.58 25.45 0 -6 -6 1209.57 27.38 0 -6 6 1232.38 25.97 0 6 -6 1138.76 23.90 0 -6 7 1266.96 27.06 0 6 7 1317.35 26.80 0 6 -7 1317.84 26.24 0 6 7 1206.63 24.53 0 6 -7 1265.76 26.13 0 -6 -7 1208.82 28.30 0 -6 -8 4.04 2.35 0 6 8 0.25 1.21 0 6 8 3.74 1.90 0 -6 8 0.91 1.35 0 6 -8 5.60 2.57 0 6 -8 3.63 1.86 0 6 -8 0.53 1.51 0 6 9 117.66 8.33 0 6 -9 145.44 9.74 0 6 -9 172.48 11.47 0 -6 9 112.65 8.86 0 -6 -9 93.59 8.71 0 6 9 166.46 10.10 0 6 -9 170.83 9.68 0 6 -10 898.38 24.59 0 6 10 958.26 24.28 0 6 -10 938.38 22.88 0 -6 -10 1013.17 28.75 0 -6 10 1051.53 27.09 0 6 10 877.66 23.83 0 6 -10 963.95 27.88 0 6 -11 620.77 21.37 0 6 -11 654.36 23.33 0 6 11 549.44 18.85 0 -6 -11 546.63 21.24 0 6 -11 673.47 19.24 0 -6 11 591.74 21.04 0 6 11 606.44 20.33 0 -6 12 42.76 5.95 0 6 -12 32.84 5.90 0 -6 -12 37.00 5.90 0 6 12 21.43 4.09 0 6 12 32.32 4.91 0 6 -12 22.87 3.75 0 6 -12 29.18 4.96 0 6 -13 1.39 1.18 0 -6 -13 2.16 1.71 0 6 -13 1.08 1.72 0 6 13 2.15 1.99 0 -6 13 2.25 2.28 0 6 13 1.33 1.53 0 6 -13 1.43 1.44 0 6 -14 62.18 8.44 0 -6 -14 37.24 6.56 0 -6 14 42.68 6.51 0 6 14 45.00 6.31 0 6 14 49.68 6.35 0 6 -14 54.66 7.10 0 6 -15 101.05 9.92 0 6 15 121.43 10.12 0 -6 -15 114.36 11.21 0 6 -15 97.90 11.37 0 -6 15 117.75 10.99 0 6 15 99.70 9.03 0 -6 16 755.56 28.45 0 6 16 653.47 23.84 0 -6 -16 652.48 27.18 0 6 16 685.40 24.87 0 6 -16 771.42 31.31 0 6 -16 750.74 27.53 0 -6 -17 14.55 4.58 0 6 -17 14.94 5.63 0 6 17 12.59 3.95 0 6 17 11.52 3.49 0 6 -17 13.41 4.19 0 -6 17 13.60 4.68 0 -6 -18 10.31 3.96 0 6 -18 4.54 1.96 0 6 18 3.19 1.67 0 6 18 4.83 2.13 0 -6 18 5.40 2.74 0 6 -18 7.60 4.23 0 6 -18 3.68 2.48 0 6 -18 7.11 2.33 0 -6 -19 2.42 1.37 0 -6 -19 1.70 2.95 0 6 19 0.70 1.40 0 6 -19 2.39 1.36 0 6 -19 3.23 3.50 0 6 -19 0.55 1.21 0 6 19 0.71 2.12 0 6 -19 0.38 1.51 0 -6 -19 -1.16 2.13 0 6 -19 -2.72 2.21 0 -6 19 1.81 2.17 0 6 -20 439.58 26.95 0 6 -20 400.89 16.38 0 -6 -20 376.42 22.85 0 6 -20 419.04 17.13 0 -6 -20 412.11 18.15 0 6 20 426.93 22.31 0 -6 20 486.52 25.82 0 -6 -20 464.07 16.70 0 -6 21 324.21 21.55 0 -6 -21 273.75 15.06 0 -6 -21 326.50 14.46 0 -6 -21 247.50 19.10 0 6 -21 304.20 22.94 0 6 -21 296.59 14.96 0 6 -21 295.87 14.59 0 6 21 291.59 18.93 0 -6 22 67.18 10.24 0 -6 -22 46.19 6.41 0 6 -22 62.79 6.98 0 6 -22 70.26 7.43 0 -6 -22 70.29 6.87 0 6 22 60.88 9.42 0 -6 -22 47.98 8.85 0 6 -22 74.76 11.75 0 6 -23 0.77 3.16 0 6 23 5.35 2.89 0 6 -23 6.01 2.38 0 6 -23 0.94 1.73 0 -6 -23 3.54 2.15 0 -6 -23 6.52 2.12 0 -6 -24 31.36 5.48 0 6 -24 33.53 5.22 0 6 -24 34.25 5.25 0 6 -25 0.76 1.46 0 -6 -25 0.29 1.92 0 6 -25 0.95 1.45 0 6 -26 1.38 1.52 0 6 -26 3.80 2.14 0 -6 -26 2.28 1.70 0 -6 -27 37.02 5.76 0 6 -27 35.50 5.29 0 6 -27 36.51 5.34 0 6 -28 4.63 2.38 0 -6 -28 2.20 2.10 0 6 -28 2.92 2.02 0 -6 -29 2.66 1.93 0 6 -29 2.06 1.71 0 6 -29 -0.37 1.38 0 6 -30 0.43 1.81 0 6 -30 0.56 1.37 0 -6 -30 0.81 1.49 0 -6 30 -1.25 1.80 0 -6 -31 1.42 1.71 0 6 -31 0.37 1.10 0 -6 31 1.23 1.58 0 6 -31 1.73 1.41 0 -6 32 16.62 3.37 0 6 -32 18.72 3.11 0 -6 -32 14.28 3.00 0 -6 -33 3.44 1.77 0 6 -33 1.42 0.99 0 6 -33 2.87 1.26 0 6 -34 2.95 1.28 0 -6 -34 1.07 1.21 0 -6 34 0.50 0.77 0 7 0 0.62 0.93 0 7 0 1.43 1.82 0 -7 0 0.74 1.39 0 -7 0 -0.90 1.71 0 7 0 -0.81 1.13 0 7 1 1.69 1.87 0 -7 -1 11.56 3.14 0 7 -1 9.70 1.66 0 7 1 1.12 1.26 0 7 -1 1.08 1.64 0 -7 1 13.65 3.15 0 7 -1 2.53 2.21 0 -7 1 12.12 3.04 0 -7 -1 15.37 3.06 0 7 1 11.65 2.04 0 -7 -2 3.60 1.84 0 -7 2 2.45 2.08 0 7 2 5.22 2.13 0 7 -2 1.45 0.96 0 7 -2 6.14 2.45 0 7 -2 7.12 2.71 0 7 2 5.10 2.31 0 -7 2 2.25 1.81 0 -7 -2 0.91 1.73 0 7 2 1.65 1.27 0 7 3 127.05 8.99 0 -7 -3 89.89 7.86 0 7 3 88.40 6.07 0 -7 3 84.97 7.43 0 7 -3 139.74 9.33 0 7 3 125.59 8.42 0 -7 3 85.81 6.86 0 -7 -3 75.23 6.97 0 7 -3 78.18 3.40 0 7 -3 121.65 8.20 0 -7 4 1.67 2.09 0 7 4 2.53 1.66 0 7 4 7.62 2.43 0 -7 -4 0.93 1.32 0 -7 -4 1.02 1.47 0 7 4 7.29 2.33 0 7 -4 2.07 1.48 0 -7 4 4.21 2.01 0 7 -4 6.51 2.34 0 7 5 174.58 10.23 0 7 -5 161.03 9.99 0 -7 5 236.93 12.39 0 -7 -5 243.87 13.32 0 7 -5 164.85 10.50 0 7 5 232.26 10.63 0 -7 5 264.51 11.72 0 7 -6 816.98 22.78 0 7 6 782.64 21.79 0 7 -6 751.46 20.79 0 7 6 733.76 19.49 0 -7 -6 672.88 22.06 0 -7 6 738.86 22.07 0 7 -7 264.55 12.93 0 7 7 232.62 11.51 0 7 -7 233.00 12.17 0 -7 -7 218.40 13.08 0 -7 7 237.12 12.76 0 7 7 244.38 12.32 0 7 -8 73.63 7.03 0 7 8 98.71 7.74 0 7 8 68.21 6.83 0 -7 -8 108.59 9.40 0 -7 8 101.30 8.63 0 7 -8 69.53 7.01 0 7 -8 71.24 7.93 0 7 9 505.93 18.53 0 -7 -9 533.92 21.46 0 7 -9 519.03 18.29 0 7 -9 505.70 18.93 0 7 9 522.11 18.27 0 -7 9 558.80 20.40 0 7 -9 511.26 20.54 0 7 -10 401.42 17.47 0 7 10 385.17 16.58 0 7 -10 396.85 16.22 0 -7 10 439.13 18.58 0 7 -10 396.47 18.53 0 -7 -10 399.80 19.12 0 7 10 405.25 16.68 0 7 -11 29.40 5.08 0 7 11 32.90 5.27 0 -7 -11 14.27 4.11 0 7 -11 34.81 6.00 0 7 -11 37.32 5.08 0 -7 11 17.26 4.43 0 7 11 17.53 4.20 0 7 12 26.16 4.74 0 7 -12 42.58 5.38 0 7 12 39.13 5.69 0 -7 -12 21.21 5.13 0 7 -12 44.83 7.15 0 7 -12 41.38 6.26 0 -7 12 27.84 5.23 0 -7 13 88.33 9.26 0 -7 -13 62.04 8.28 0 7 13 115.70 9.65 0 7 -13 133.35 9.54 0 7 -13 124.38 10.81 0 7 13 78.78 8.16 0 7 -13 120.13 11.89 0 -7 -14 426.56 21.61 0 7 -14 441.19 20.73 0 7 -14 424.08 22.33 0 7 14 438.86 19.09 0 -7 14 466.84 21.94 0 7 14 428.55 19.30 0 7 -15 11.40 3.80 0 7 -15 14.05 4.36 0 -7 15 10.48 3.94 0 7 15 10.55 3.08 0 -7 -15 7.78 3.37 0 7 15 7.25 2.95 0 7 -16 322.03 18.79 0 -7 16 302.43 18.62 0 7 -16 331.43 21.69 0 7 16 293.19 16.17 0 7 16 280.03 16.71 0 -7 -16 251.39 17.58 0 -7 -17 35.23 6.97 0 -7 17 38.55 7.07 0 7 -17 22.23 3.95 0 7 -17 19.09 4.85 0 7 -17 11.84 4.42 0 7 17 33.14 6.13 0 7 17 16.46 4.12 0 -7 18 5.77 3.08 0 7 -18 1.66 1.86 0 7 -18 2.61 3.53 0 7 18 1.56 1.73 0 7 -18 1.76 1.32 0 7 18 2.31 2.58 0 -7 -18 7.08 2.65 0 -7 -18 5.18 2.59 0 7 -18 2.07 2.43 0 7 -18 3.29 1.98 0 7 -19 315.98 16.23 0 -7 -19 284.64 20.23 0 7 -19 370.80 24.92 0 -7 19 352.70 21.94 0 7 -19 335.67 14.90 0 7 19 366.55 18.74 0 7 19 331.29 19.83 0 -7 -19 323.88 15.77 0 7 -19 341.05 15.27 0 -7 20 2.50 2.73 0 7 -20 5.28 4.36 0 7 -20 2.65 2.21 0 -7 -20 0.60 3.03 0 7 -20 1.67 2.02 0 7 20 -0.31 2.00 0 7 -20 0.54 1.71 0 -7 -20 3.98 2.98 0 -7 -21 53.06 6.99 0 7 -21 51.86 6.31 0 7 21 57.49 9.17 0 7 -21 65.28 11.12 0 -7 -21 47.26 8.48 0 -7 21 58.58 9.39 0 7 -21 55.31 6.57 0 7 -22 4.89 2.46 0 -7 -22 11.63 4.47 0 7 -22 3.16 2.11 0 -7 22 3.50 2.78 0 7 22 6.32 3.28 0 -7 -22 4.49 2.42 0 7 -22 1.15 3.40 0 7 -23 48.22 6.37 0 7 -23 52.72 6.60 0 -7 -23 49.20 6.57 0 -7 -24 64.58 7.46 0 7 -24 50.06 6.43 0 7 -24 55.34 6.55 0 7 -25 0.40 1.87 0 -7 -25 -0.25 1.56 0 7 -25 0.69 1.37 0 7 -26 226.24 12.99 0 -7 -26 205.02 13.21 0 7 -26 227.48 13.20 0 -7 -27 88.85 8.57 0 7 -27 88.16 7.89 0 7 -27 88.41 8.11 0 7 -28 18.32 3.74 0 7 -28 21.37 3.89 0 -7 -28 25.44 4.64 0 7 -29 3.11 1.49 0 -7 -29 2.74 2.31 0 7 -29 2.08 1.87 0 -7 30 14.92 3.34 0 7 -30 12.26 2.88 0 7 -30 14.12 2.96 0 -7 -30 11.22 2.96 0 7 -31 2.12 1.78 0 -7 -31 0.50 1.38 0 7 -31 -0.14 1.05 0 -7 31 0.52 1.52 0 7 -32 45.01 4.46 0 -7 -32 43.93 4.72 0 -7 32 46.60 4.93 0 -7 -33 1.46 1.27 0 -7 33 4.11 1.59 0 7 33 2.07 1.13 0 7 -33 4.16 1.50 0 -7 34 26.84 3.00 0 -7 -34 18.32 2.49 0 7 -34 27.74 2.88 0 -8 0 708.97 22.01 0 -8 0 694.40 23.23 0 8 0 721.70 22.79 0 8 0 646.28 14.48 0 8 0 696.86 21.11 0 8 -1 9.93 3.97 0 -8 1 46.83 5.68 0 -8 1 37.00 5.88 0 8 -1 33.33 3.05 0 -8 -1 45.15 5.75 0 8 -1 12.92 3.76 0 8 1 30.55 3.44 0 8 1 9.55 3.36 0 -8 -1 38.19 6.00 0 8 1 11.72 3.60 0 -8 2 2.31 1.20 0 8 2 4.21 1.51 0 -8 -2 2.18 1.49 0 8 -2 4.92 2.15 0 8 2 5.75 2.31 0 8 -2 4.81 2.43 0 -8 -2 1.38 1.83 0 8 2 5.23 2.46 0 -8 2 2.76 2.00 0 -8 -3 2.41 1.33 0 -8 3 7.87 2.54 0 8 3 0.99 1.58 0 8 3 1.50 1.35 0 -8 3 3.84 2.12 0 8 3 2.81 1.28 0 8 -3 0.80 1.27 0 -8 -3 1.69 2.06 0 8 -3 2.30 2.07 0 -8 4 11.07 2.82 0 8 -4 9.00 2.85 0 8 -4 9.97 3.26 0 8 4 8.89 2.56 0 8 4 9.84 2.29 0 -8 -4 11.66 3.09 0 8 4 7.64 2.69 0 -8 4 9.67 2.89 0 -8 -4 11.81 3.52 0 -8 5 0.68 1.11 0 -8 5 2.71 2.37 0 8 5 0.61 1.49 0 -8 -5 -1.46 2.21 0 8 5 1.01 1.30 0 8 -5 1.05 1.55 0 8 -5 1.65 1.60 0 8 -6 2.92 2.08 0 8 6 1.03 1.51 0 8 6 0.54 1.18 0 -8 6 0.92 1.69 0 -8 6 1.62 1.57 0 -8 -6 0.88 1.47 0 8 -6 4.02 1.92 0 8 7 216.64 11.68 0 8 -7 185.42 11.57 0 -8 -7 217.74 13.53 0 8 7 185.96 11.59 0 8 -7 180.62 12.11 0 -8 7 228.10 13.83 0 8 -7 195.14 12.30 0 8 8 2.74 1.94 0 8 -8 0.37 1.46 0 -8 8 10.37 3.32 0 -8 -8 10.26 3.49 0 8 -8 4.48 3.27 0 8 8 5.81 2.45 0 8 -8 2.12 2.30 0 8 -9 18.25 3.88 0 -8 -9 10.06 3.50 0 8 9 15.99 3.72 0 8 9 11.43 2.82 0 8 -9 17.20 3.73 0 -8 9 10.18 2.90 0 8 -9 15.26 3.88 0 8 -10 6.84 3.40 0 -8 10 5.36 1.86 0 -8 -10 3.47 2.52 0 8 -10 5.11 2.42 0 8 10 3.15 2.18 0 8 10 5.51 2.20 0 8 -10 9.44 3.11 0 8 11 72.46 7.70 0 8 -11 69.50 8.80 0 8 11 78.43 7.92 0 8 -11 73.01 7.71 0 -8 11 86.71 9.17 0 8 -11 70.66 7.99 0 -8 -11 75.85 9.07 0 -8 -12 325.03 18.69 0 8 -12 266.85 17.35 0 8 12 264.98 15.00 0 8 12 302.40 16.05 0 8 -12 275.98 16.22 0 8 -12 261.82 14.47 0 -8 12 353.09 18.73 0 8 -13 238.03 15.63 0 8 -13 229.26 16.49 0 -8 13 269.24 17.12 0 -8 -13 244.88 16.81 0 8 13 225.12 14.24 0 8 -13 247.12 14.04 0 8 13 246.07 14.84 0 -8 14 304.08 18.60 0 8 14 216.23 13.97 0 -8 -14 283.49 18.75 0 8 14 271.52 16.18 0 8 -14 243.90 16.24 0 8 -14 236.82 17.51 0 8 -15 0.57 1.55 0 8 15 0.56 1.40 0 -8 -15 2.47 2.73 0 8 15 1.93 2.07 0 -8 15 -0.22 1.94 0 8 -15 -1.31 2.41 0 8 16 48.14 6.90 0 -8 -16 25.72 5.95 0 8 -16 34.15 4.64 0 -8 16 34.75 6.60 0 8 -16 47.64 7.62 0 8 -16 40.58 4.90 0 8 16 32.05 6.12 0 8 -16 48.65 8.99 0 8 -17 137.16 9.47 0 -8 -17 126.63 13.34 0 8 -17 155.62 13.79 0 -8 17 125.63 9.28 0 8 -17 169.19 16.38 0 -8 17 144.01 13.70 0 8 17 151.46 13.26 0 8 -17 147.55 9.46 0 -8 -17 125.59 9.57 0 8 -17 127.95 9.88 0 8 17 155.43 12.45 0 8 -18 5.12 3.53 0 -8 18 6.45 2.57 0 -8 -18 3.30 2.07 0 8 -18 0.67 1.26 0 -8 -18 4.41 2.88 0 8 18 0.52 1.56 0 -8 18 6.88 3.62 0 8 18 3.68 3.09 0 8 -18 2.15 1.45 0 8 -18 2.21 2.43 0 8 -18 2.37 1.66 0 8 -19 66.61 6.87 0 8 -19 61.60 7.18 0 -8 -19 59.84 6.89 0 8 -19 76.49 11.93 0 -8 -19 53.70 9.25 0 8 19 64.33 7.99 0 -8 19 69.31 10.02 0 8 -19 64.85 6.55 0 -8 19 68.85 7.06 0 8 19 59.92 8.93 0 8 20 28.50 6.52 0 -8 -20 23.14 6.14 0 8 -20 24.68 4.35 0 8 -20 27.07 5.07 0 -8 -20 26.25 4.87 0 8 -20 32.80 7.99 0 8 -20 27.43 4.55 0 -8 20 32.88 7.24 0 -8 -21 9.32 3.21 0 -8 21 10.75 4.71 0 8 -21 -1.62 3.99 0 8 21 11.90 5.02 0 -8 -21 7.34 3.65 0 8 -21 4.36 2.19 0 8 -21 4.38 2.53 0 8 -22 358.06 16.49 0 -8 -22 389.67 18.20 0 8 -22 362.50 16.16 0 8 -23 39.84 5.54 0 8 -23 43.30 5.86 0 -8 -23 44.30 6.35 0 -8 -24 12.65 3.45 0 8 -24 14.61 3.33 0 8 -24 11.37 3.40 0 -8 -25 22.87 4.74 0 8 -25 20.25 4.27 0 8 -25 17.95 3.83 0 8 -26 125.95 9.56 0 -8 -26 103.24 9.12 0 8 -26 127.29 9.58 0 -8 -27 12.71 3.59 0 8 -27 13.94 3.46 0 8 -27 14.94 3.33 0 8 -28 41.58 5.19 0 8 -28 48.08 5.66 0 8 -29 0.13 1.13 0 8 -29 0.72 1.52 0 -8 30 21.52 3.83 0 -8 -30 12.77 2.95 0 8 -30 18.44 3.28 0 8 -30 19.86 3.35 0 8 31 8.22 2.01 0 -8 31 11.12 2.63 0 8 -31 7.72 2.02 0 -8 -31 7.53 2.23 0 8 -31 9.21 2.11 0 8 32 52.18 4.08 0 -8 32 63.15 5.48 0 -8 -32 46.97 4.48 0 8 -32 59.54 4.88 0 -8 33 50.13 4.34 0 -8 -33 42.21 3.83 0 8 -33 47.59 3.92 0 -9 0 1.59 1.99 0 9 0 -0.06 2.03 0 9 0 1.24 2.15 0 -9 0 0.44 2.29 0 9 0 -0.05 1.00 0 9 1 6.77 2.96 0 -9 1 7.95 2.95 0 9 -1 3.87 2.01 0 9 1 11.69 2.27 0 -9 -1 11.06 2.93 0 9 1 5.24 2.28 0 9 -1 5.18 2.62 0 -9 1 7.96 2.68 0 -9 -1 12.22 3.57 0 9 2 100.18 9.51 0 9 2 101.30 8.70 0 -9 2 83.93 8.93 0 9 2 84.05 6.23 0 -9 -2 75.26 7.93 0 -9 -2 82.88 8.91 0 -9 2 87.58 8.27 0 9 -2 101.99 9.53 0 9 -2 98.18 8.64 0 9 3 10.91 2.85 0 9 3 6.54 1.69 0 -9 3 8.25 2.94 0 -9 3 8.12 2.65 0 9 -3 11.83 3.33 0 9 3 7.74 2.77 0 -9 -3 6.13 2.15 0 -9 -3 7.29 3.09 0 9 -3 9.60 2.97 0 -9 4 11.44 3.43 0 9 -4 26.98 4.46 0 9 -4 30.26 5.14 0 -9 -4 11.12 3.43 0 9 4 30.70 4.99 0 -9 -4 13.01 3.86 0 9 4 14.77 3.00 0 -9 4 13.97 3.46 0 -9 -5 187.34 12.98 0 -9 5 183.71 11.61 0 9 5 152.08 11.09 0 9 -5 150.97 11.71 0 9 -5 149.48 11.17 0 9 5 172.31 10.09 0 -9 5 179.48 13.25 0 9 -6 52.31 6.52 0 -9 6 58.80 7.49 0 -9 -6 53.16 7.32 0 9 -6 54.18 7.04 0 9 6 57.09 6.93 0 9 -6 52.32 6.71 0 9 6 53.14 5.86 0 -9 6 57.49 6.45 0 9 -7 44.19 6.41 0 9 7 16.45 3.87 0 -9 -7 11.50 3.98 0 9 -7 34.91 5.32 0 9 -7 37.02 6.22 0 9 7 41.73 5.88 0 -9 7 14.91 4.29 0 -9 -8 26.14 5.39 0 9 -8 23.16 4.73 0 9 -8 18.89 4.80 0 9 -8 20.40 4.48 0 9 8 26.62 4.92 0 9 8 26.26 4.50 0 -9 8 26.30 5.23 0 9 -9 2.31 1.73 0 9 -9 2.80 1.68 0 9 9 5.02 2.48 0 9 9 3.80 2.28 0 9 -9 3.65 2.84 0 -9 -9 3.92 2.42 0 -9 9 6.76 3.51 0 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4.14 0 -9 -24 22.65 4.31 0 9 -25 4.28 2.30 0 9 -25 4.84 2.46 0 -9 -25 0.33 1.77 0 -9 -26 102.64 8.77 0 9 -26 105.93 8.47 0 9 -26 108.62 8.66 0 9 -27 3.80 2.04 0 9 -27 7.75 2.43 0 -9 -27 1.68 1.60 0 9 -28 -0.48 1.29 0 9 -28 1.83 1.70 0 -9 -28 1.39 1.58 0 9 -29 3.60 1.92 0 9 -29 0.61 1.18 0 -9 -29 6.23 2.23 0 9 29 2.88 1.46 0 9 -30 22.43 3.39 0 9 30 24.46 3.22 0 -9 30 23.87 3.69 0 9 -30 24.62 3.49 0 -9 -30 22.58 3.43 0 9 31 2.26 1.07 0 -9 -31 0.48 1.14 0 -9 31 3.52 1.68 0 9 -31 1.70 0.88 0 9 -31 4.69 1.63 0 9 -32 32.68 3.32 0 -9 32 37.22 3.93 0 9 32 32.07 2.93 0 -9 -32 30.00 3.29 0 -9 33 3.04 1.26 0 -10 0 81.06 9.47 0 10 0 130.51 11.11 0 -10 0 78.01 8.72 0 10 0 140.69 12.20 0 -10 -1 229.42 14.75 0 -10 1 237.64 14.84 0 10 1 207.44 13.96 0 10 -1 216.26 14.14 0 -10 -1 216.71 15.69 0 10 1 201.59 14.71 0 10 -1 213.72 15.19 0 -10 1 224.05 15.74 0 -10 2 92.22 9.14 0 10 -2 142.95 11.93 0 10 2 131.19 11.22 0 10 -2 127.70 10.73 0 10 2 106.51 7.26 0 -10 -2 87.21 9.16 0 -10 2 105.07 11.03 0 -10 -2 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5.84 0 10 -9 38.06 6.42 0 10 9 36.53 6.18 0 10 -10 909.98 33.33 0 -10 -10 1067.42 36.22 0 -10 10 1177.81 37.73 0 10 10 1107.52 31.42 0 10 10 1021.56 32.25 0 10 -10 1050.61 33.45 0 10 -10 1039.89 33.35 0 10 -11 2.36 2.18 0 -10 11 2.88 3.27 0 10 -11 2.94 2.59 0 -10 -11 3.69 3.08 0 10 11 4.24 2.81 0 10 11 2.84 2.97 0 10 -11 1.28 2.81 0 -10 -12 378.71 22.46 0 10 12 392.78 20.09 0 -10 12 405.29 23.25 0 -10 12 404.71 16.74 0 10 12 387.58 19.75 0 10 -12 412.81 21.05 0 10 -12 392.30 21.42 0 10 -12 374.27 22.32 0 -10 13 86.36 11.21 0 10 -13 83.27 6.62 0 10 -13 90.62 11.52 0 10 -13 73.24 7.24 0 10 -13 87.02 10.40 0 10 -13 101.83 10.39 0 10 -13 78.26 6.84 0 10 13 83.75 9.65 0 10 13 80.84 9.38 0 -10 13 70.78 7.31 0 -10 -13 61.28 9.34 0 10 14 37.04 6.60 0 10 -14 35.96 4.74 0 10 14 32.84 6.03 0 10 -14 32.10 6.98 0 -10 -14 45.09 5.63 0 -10 -14 43.09 5.27 0 -10 14 47.30 8.49 0 -10 14 40.48 5.75 0 10 -14 36.08 7.04 0 10 -14 36.15 5.24 0 -10 -14 40.94 7.70 0 10 -14 33.59 4.34 0 10 -15 2.34 1.51 0 10 -15 2.52 2.72 0 10 15 3.86 2.22 0 -10 15 2.32 2.36 0 -10 -15 8.33 4.22 0 -10 15 6.26 2.47 0 10 -15 2.45 1.40 0 -10 -15 10.20 3.03 0 10 15 2.39 2.15 0 10 -15 5.09 2.09 0 10 -15 -0.16 1.46 0 -10 -15 10.95 2.74 0 -10 16 -2.38 2.93 0 -10 -16 -2.13 2.96 0 -10 16 -1.17 2.00 0 10 -16 -0.88 1.84 0 10 16 1.28 2.06 0 10 -16 1.98 2.06 0 10 -16 1.37 1.05 0 -10 -16 0.38 1.62 0 10 -16 0.92 2.27 0 10 -16 -0.53 1.74 0 10 16 1.89 2.23 0 10 17 221.79 15.85 0 10 -17 191.87 12.68 0 -10 -17 193.88 11.95 0 -10 17 180.92 11.95 0 10 -17 235.82 20.73 0 -10 -17 166.87 16.50 0 10 -17 217.82 11.77 0 -10 17 193.34 17.65 0 10 -17 196.61 11.71 0 10 -17 229.70 17.92 0 10 17 198.55 16.15 0 10 -18 91.98 7.77 0 -10 18 95.55 12.59 0 -10 -18 84.25 8.05 0 10 -18 90.89 13.33 0 -10 -18 79.49 11.60 0 10 18 96.83 10.57 0 -10 18 79.25 8.05 0 10 18 87.10 11.03 0 10 -18 80.11 8.55 0 10 -18 86.91 7.86 0 -10 19 10.96 3.75 0 10 -19 4.78 2.72 0 -10 -19 15.15 3.99 0 10 -19 11.84 4.08 0 10 -19 5.42 2.44 0 -10 20 4.96 2.26 0 -10 -20 1.59 1.98 0 10 -20 2.65 2.06 0 10 -20 5.93 3.71 0 10 -20 0.96 1.32 0 -10 -21 52.64 6.64 0 10 -21 39.20 5.33 0 10 -21 44.86 5.69 0 -10 21 51.04 6.37 0 10 -21 45.41 6.35 0 -10 -22 16.71 3.58 0 10 -22 22.35 3.85 0 10 -22 23.00 4.32 0 -10 22 18.98 4.04 0 10 -23 5.26 2.11 0 -10 -23 8.78 2.98 0 10 -23 6.67 2.77 0 -10 -24 1.19 1.95 0 10 -24 2.89 2.04 0 10 -24 2.96 1.67 0 10 -25 3.51 1.99 0 -10 -25 5.35 2.20 0 10 -25 4.15 1.98 0 10 -26 4.38 2.01 0 10 -26 3.07 2.04 0 -10 -26 0.11 1.42 0 10 -27 26.07 3.98 0 10 -27 26.45 4.05 0 -10 -27 23.86 4.14 0 10 27 27.59 3.93 0 10 -28 60.58 5.78 0 -10 -28 63.07 5.98 0 10 28 64.10 5.50 0 10 -28 65.09 5.91 0 10 -29 22.10 3.41 0 10 29 20.44 3.10 0 10 -29 22.44 3.32 0 -10 29 22.02 3.65 0 -10 -29 14.90 2.83 0 10 -30 -0.18 1.00 0 -10 30 0.40 0.97 0 10 30 0.07 0.74 0 10 -30 0.29 0.93 0 -10 -30 0.34 0.87 0 10 31 0.59 0.67 0 10 -31 -0.54 1.07 0 -10 31 0.96 0.87 0 10 -31 -0.97 0.82 0 -10 -31 0.21 0.71 0 -10 32 0.57 0.77 0 11 0 26.76 6.13 0 11 0 15.47 6.78 0 11 0 18.69 5.88 0 -11 0 20.38 5.90 0 -11 0 20.24 6.55 0 -11 -1 25.37 5.78 0 11 -1 30.80 5.49 0 11 1 22.49 5.07 0 11 1 29.52 5.13 0 -11 -1 30.55 6.01 0 11 -1 26.63 5.54 0 11 -1 26.62 6.51 0 11 1 19.57 4.96 0 -11 1 26.85 5.68 0 -11 1 29.40 6.80 0 11 -2 69.06 8.08 0 11 -2 96.02 10.91 0 -11 -2 66.67 9.50 0 11 2 80.32 9.48 0 -11 2 75.38 8.84 0 11 -2 82.90 9.44 0 -11 -2 60.32 8.32 0 -11 2 72.59 9.83 0 11 -3 146.99 13.41 0 -11 -3 103.77 11.78 0 -11 3 115.39 12.61 0 11 -3 124.37 11.06 0 11 -3 146.62 12.33 0 -11 -3 112.64 11.32 0 -11 3 123.36 11.07 0 11 3 149.30 12.88 0 -11 4 29.53 6.25 0 11 -4 24.69 5.24 0 11 -4 32.02 6.42 0 -11 -4 26.98 5.76 0 11 -4 29.91 5.44 0 -11 4 31.67 5.66 0 11 4 30.09 5.99 0 -11 5 18.44 4.90 0 11 -5 11.25 3.44 0 11 5 13.78 4.22 0 11 -5 11.17 3.82 0 -11 -5 14.72 4.56 0 -11 5 23.69 4.90 0 11 -5 13.23 4.33 0 11 5 14.48 3.28 0 11 6 91.76 8.21 0 11 -6 66.34 8.63 0 11 -6 77.21 9.24 0 11 6 83.04 9.40 0 -11 6 94.04 11.14 0 11 -6 72.96 9.49 0 -11 -6 96.01 10.85 0 11 7 30.49 5.20 0 -11 -7 22.14 5.58 0 11 -7 47.38 7.57 0 11 -7 36.44 6.62 0 11 -7 35.43 6.50 0 11 7 41.28 6.89 0 -11 7 24.99 5.98 0 11 8 8.06 3.44 0 11 8 9.67 3.06 0 -11 -8 5.44 3.29 0 11 -8 8.66 4.34 0 11 -8 5.86 3.11 0 -11 8 8.35 4.20 0 11 -8 9.83 4.35 0 11 -9 69.41 9.02 0 11 9 69.35 8.04 0 -11 9 72.09 10.18 0 -11 -9 69.41 9.72 0 11 -9 61.53 9.05 0 11 -9 72.54 9.80 0 11 9 74.11 6.47 0 -11 9 80.51 7.63 0 11 9 72.94 9.12 0 -11 10 55.62 6.69 0 11 10 44.28 5.35 0 11 -10 51.84 8.07 0 11 -10 43.46 8.08 0 11 -10 50.07 8.23 0 -11 10 50.83 8.91 0 11 10 45.38 7.30 0 11 10 49.63 6.99 0 -11 -10 45.26 7.95 0 11 -10 48.71 5.97 0 -11 -10 51.33 5.87 0 11 -11 200.62 15.95 0 11 -11 187.19 16.09 0 11 11 176.09 13.41 0 -11 -11 167.81 15.40 0 11 11 194.15 14.96 0 -11 11 192.24 12.04 0 11 -11 185.61 10.32 0 11 -11 186.86 9.63 0 11 -11 203.89 16.02 0 11 11 185.00 10.55 0 -11 11 181.38 11.52 0 -11 -11 180.91 11.06 0 11 -11 195.91 11.74 0 -11 11 196.85 17.00 0 11 -12 3.31 2.17 0 11 -12 2.69 2.01 0 11 12 0.50 1.91 0 11 12 4.29 2.01 0 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11 15 92.50 10.84 0 -11 -15 108.57 8.63 0 -11 -16 2.35 2.01 0 -11 16 2.29 1.83 0 -11 -16 3.00 1.73 0 11 16 0.93 1.60 0 11 -16 1.96 2.40 0 -11 -16 0.54 1.83 0 11 -16 3.08 1.71 0 11 16 0.23 1.93 0 11 -16 2.37 1.64 0 11 -16 5.28 4.81 0 -11 16 7.31 4.16 0 11 -16 3.42 1.81 0 11 -17 30.42 5.30 0 11 -17 23.18 4.09 0 11 17 18.83 4.88 0 11 17 32.77 6.77 0 11 -17 24.97 4.36 0 -11 17 36.51 5.67 0 -11 -17 37.26 5.23 0 11 -18 57.89 6.43 0 -11 -18 80.18 7.75 0 11 -18 66.44 7.52 0 -11 18 68.69 7.86 0 11 -18 57.25 6.20 0 -11 19 1.99 1.91 0 11 -19 3.43 1.71 0 -11 -19 2.13 1.95 0 11 -19 2.36 2.11 0 11 -19 5.31 2.63 0 11 -20 149.45 10.42 0 11 -20 152.54 10.29 0 11 -20 139.67 10.88 0 -11 -20 149.42 10.65 0 -11 20 145.93 11.05 0 -11 -21 11.73 3.43 0 11 -21 10.71 3.42 0 11 -21 6.37 2.62 0 11 -21 12.44 3.36 0 -11 21 13.33 3.66 0 11 -22 0.26 1.75 0 -11 22 -1.13 1.93 0 -11 -22 -1.80 1.85 0 11 -22 -0.40 1.36 0 11 22 0.06 1.38 0 11 23 12.25 3.07 0 11 -23 11.95 3.00 0 -11 -23 10.27 3.01 0 11 -23 9.20 2.78 0 -11 23 9.11 2.85 0 11 24 16.51 3.25 0 -11 -24 19.68 3.93 0 11 -24 17.03 3.52 0 11 -24 14.20 3.25 0 -11 -25 20.83 3.89 0 11 -25 24.09 4.01 0 11 25 23.91 3.81 0 11 -25 18.84 3.73 0 11 -26 4.84 2.04 0 11 26 4.34 1.95 0 -11 -26 7.21 2.48 0 11 -26 3.87 1.81 0 11 -27 3.33 1.81 0 -11 -27 -1.04 1.41 0 11 27 0.64 1.24 0 11 -27 2.07 1.33 0 -11 -28 2.25 1.56 0 11 28 2.51 1.27 0 11 -28 2.30 1.35 0 11 -28 2.88 1.73 0 -11 -29 36.22 3.81 0 11 -29 35.18 3.74 0 11 29 41.18 3.90 0 11 -29 38.34 4.03 0 -11 29 41.60 4.56 0 11 -30 2.15 1.08 0 11 -30 2.75 1.04 0 -11 -30 1.54 0.92 0 -11 30 2.95 1.46 0 11 30 3.47 1.41 0 -11 31 0.64 0.90 0 -12 0 56.55 9.16 0 -12 0 51.57 8.01 0 12 -1 57.96 8.35 0 12 -1 58.23 7.65 0 12 1 66.09 8.80 0 -12 1 60.80 8.43 0 -12 1 56.81 9.39 0 12 -1 61.07 9.40 0 -12 -1 54.16 9.07 0 -12 -1 60.24 8.83 0 -12 -2 178.38 16.33 0 12 -2 186.02 14.21 0 12 2 199.43 15.32 0 12 -2 207.60 17.10 0 -12 2 208.53 17.57 0 12 -2 210.45 15.64 0 -12 -2 196.40 15.70 0 -12 2 220.82 15.77 0 12 -3 17.79 4.49 0 -12 3 20.43 4.93 0 12 -3 16.85 4.87 0 -12 -3 19.37 5.17 0 12 -3 15.44 4.97 0 -12 3 17.36 5.84 0 12 3 20.38 5.11 0 -12 -4 11.91 3.48 0 12 -4 9.66 4.18 0 -12 -4 11.43 4.78 0 -12 4 15.21 5.51 0 -12 4 13.33 4.05 0 12 -4 9.57 4.29 0 12 4 7.40 3.78 0 12 -4 9.25 4.21 0 12 5 202.34 15.96 0 12 -5 169.99 14.31 0 12 5 186.44 10.57 0 -12 5 182.47 16.85 0 -12 -5 172.58 15.27 0 12 -5 210.81 17.01 0 -12 5 181.73 11.30 0 -12 -5 197.87 11.74 0 12 -5 208.11 15.75 0 12 -6 158.05 10.23 0 -12 6 174.59 11.11 0 -12 -6 147.75 14.49 0 -12 6 164.56 15.83 0 12 -6 150.88 13.46 0 12 6 159.61 13.90 0 12 -6 133.17 12.82 0 12 -6 158.65 14.79 0 12 6 169.45 10.17 0 -12 -6 180.31 11.42 0 12 7 114.01 12.55 0 -12 7 116.25 13.93 0 -12 -7 118.38 12.91 0 12 -7 111.94 12.18 0 12 -7 112.12 7.30 0 -12 -7 114.62 9.23 0 12 -7 114.52 11.93 0 -12 7 103.85 8.88 0 12 -7 115.01 12.85 0 12 7 123.17 8.83 0 -12 7 117.71 9.45 0 12 -7 116.24 8.97 0 12 -8 46.71 4.96 0 12 8 56.87 7.30 0 -12 -8 59.61 9.87 0 12 8 61.18 6.43 0 12 -8 60.57 6.79 0 12 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13.22 3.28 0 -12 16 13.56 3.72 0 12 -16 1.66 1.39 0 12 16 6.84 2.66 0 -12 -16 12.51 3.36 0 12 -16 5.10 2.47 0 -12 -17 88.96 7.96 0 12 -17 86.97 7.59 0 12 -17 84.28 7.88 0 -12 -17 84.09 7.54 0 12 -17 84.33 8.58 0 -12 17 81.91 8.59 0 12 17 87.66 7.94 0 12 -18 12.48 3.03 0 12 18 14.17 3.43 0 -12 18 8.39 2.93 0 12 -18 13.06 2.88 0 12 -18 10.23 2.81 0 -12 -18 10.26 3.13 0 -12 -19 29.94 4.82 0 12 19 37.08 5.21 0 -12 19 25.22 4.74 0 12 -19 26.53 4.83 0 12 -19 36.49 5.07 0 12 -19 33.76 4.81 0 -12 -20 0.36 1.34 0 12 -20 -1.41 1.69 0 12 20 -1.18 1.45 0 -12 20 0.62 1.81 0 12 -20 2.22 1.26 0 12 -20 -0.63 1.20 0 12 -21 1.30 1.42 0 12 -21 -2.03 1.71 0 -12 -21 2.25 1.71 0 12 -21 -0.76 1.24 0 12 21 2.26 2.16 0 -12 21 0.81 1.49 0 -12 -22 4.87 2.12 0 -12 22 5.23 2.88 0 12 -22 6.25 2.20 0 12 22 4.47 2.10 0 12 -22 4.04 2.06 0 -12 23 -0.13 1.31 0 12 -23 0.22 1.20 0 12 23 1.41 1.64 0 12 -23 1.20 1.28 0 -12 -23 1.47 1.19 0 12 -24 4.24 1.88 0 12 -24 6.09 2.10 0 12 24 9.23 2.66 0 -12 -24 6.79 2.26 0 12 -25 2.42 1.64 0 -12 -25 3.08 1.88 0 12 -25 3.78 1.83 0 12 25 4.48 2.15 0 12 26 14.17 2.68 0 12 -26 14.86 2.80 0 12 -26 11.07 2.39 0 -12 -26 12.76 2.61 0 12 -27 14.26 2.61 0 12 -27 11.72 2.42 0 -12 -27 17.78 2.94 0 12 27 11.08 2.33 0 12 -28 0.37 0.97 0 -12 28 0.81 1.03 0 -12 -28 -0.75 0.82 0 12 -28 0.17 1.06 0 12 28 0.84 0.97 0 -12 29 2.69 1.18 0 12 29 3.67 1.20 0 12 -29 0.20 0.64 0 12 -29 2.71 1.15 0 -12 30 20.10 2.60 0 13 0 0.16 1.07 0 13 0 0.03 2.27 0 13 0 -0.15 1.18 0 -13 0 -1.96 2.35 0 -13 0 0.87 1.46 0 -13 0 2.16 1.84 0 -13 0 0.04 2.36 0 13 -1 30.72 3.89 0 13 1 29.31 3.68 0 13 1 25.03 4.26 0 -13 1 19.78 3.71 0 13 -1 24.16 4.20 0 13 -1 36.40 6.97 0 -13 -1 14.71 3.40 0 13 1 39.54 7.47 0 -13 1 16.85 4.92 0 -13 -1 22.25 6.31 0 -13 1 17.85 4.00 0 -13 -1 21.15 5.54 0 -13 1 18.67 5.94 0 13 -2 9.43 2.65 0 -13 -2 6.00 3.26 0 -13 -2 8.72 4.02 0 -13 -2 10.03 2.98 0 -13 2 8.32 3.63 0 -13 2 13.08 5.38 0 13 2 4.48 2.57 0 13 -2 6.04 1.92 0 13 -2 8.36 3.68 0 -13 2 11.64 3.51 0 13 2 3.78 1.75 0 -13 3 8.16 2.88 0 -13 -3 9.60 2.91 0 -13 3 10.27 4.22 0 13 3 4.91 2.16 0 -13 3 9.61 3.12 0 13 -3 7.04 2.60 0 -13 -3 4.22 2.63 0 13 3 5.34 3.09 0 13 -3 3.03 1.66 0 13 -3 2.07 1.85 0 13 -3 2.44 2.10 0 13 -4 4.19 2.55 0 13 4 7.04 3.17 0 13 -4 5.35 1.79 0 13 4 12.86 3.08 0 -13 -4 12.73 4.69 0 -13 4 9.40 2.87 0 -13 4 9.36 3.04 0 -13 -4 15.51 3.83 0 -13 4 15.72 5.45 0 13 -4 5.93 3.01 0 13 -4 8.33 2.27 0 13 -5 137.78 13.62 0 13 5 134.53 13.70 0 13 -5 120.58 7.65 0 13 -5 126.06 14.09 0 -13 5 110.91 9.20 0 13 -5 106.47 12.13 0 13 5 110.51 8.60 0 -13 -5 108.68 9.30 0 -13 -5 94.44 11.87 0 13 -5 107.35 8.61 0 -13 5 106.66 9.22 0 -13 5 111.46 13.87 0 13 -6 -0.30 1.44 0 13 6 0.24 1.59 0 -13 6 -0.09 1.98 0 -13 -6 1.77 1.37 0 -13 6 0.63 1.36 0 13 6 0.32 2.05 0 -13 -6 -1.79 2.03 0 13 -6 1.47 1.88 0 13 -6 -1.58 3.82 0 13 -6 2.46 2.40 0 -13 6 2.61 1.89 0 -13 -7 34.74 5.25 0 13 -7 12.23 4.66 0 -13 -7 28.96 6.88 0 13 -7 8.91 4.15 0 13 7 20.59 3.85 0 13 -7 20.08 4.10 0 -13 7 24.96 4.92 0 -13 7 32.63 5.34 0 13 7 13.71 4.43 0 13 -7 11.59 2.61 0 13 -7 6.32 3.89 0 -13 7 17.50 6.50 0 -13 8 75.81 7.89 0 13 8 71.41 10.16 0 -13 8 66.13 10.87 0 13 -8 69.56 6.14 0 -13 -8 65.67 10.17 0 -13 8 75.03 7.89 0 13 -8 71.22 10.49 0 13 -8 75.39 10.44 0 13 -8 55.42 9.08 0 13 8 65.06 6.90 0 -13 -8 75.74 7.65 0 13 -8 65.08 7.00 0 -13 9 -0.05 1.67 0 -13 9 -2.16 2.51 0 13 -9 -0.68 1.87 0 -13 -9 -0.46 1.94 0 13 -9 1.82 1.71 0 13 -9 -0.18 2.23 0 13 -9 -0.41 1.27 0 -13 9 0.01 1.50 0 13 9 1.07 1.74 0 13 9 0.01 1.56 0 -13 -9 -2.36 2.06 0 13 -9 -0.98 2.71 0 -13 10 0.06 1.49 0 13 -10 -0.06 1.46 0 -13 -10 -1.18 2.57 0 13 10 0.56 2.38 0 13 10 1.35 1.45 0 13 -10 0.86 1.28 0 -13 10 1.03 1.48 0 -13 10 -2.43 3.21 0 13 -10 2.35 3.43 0 -13 -10 0.70 1.90 0 13 -10 0.09 3.16 0 13 -11 28.89 4.20 0 -13 -11 37.90 5.57 0 13 -11 28.37 6.54 0 -13 11 45.92 6.36 0 -13 -11 34.08 7.79 0 13 11 30.96 6.59 0 13 -11 31.22 5.06 0 13 -11 31.30 7.92 0 -13 11 33.92 8.31 0 13 11 36.92 5.29 0 -13 11 38.76 6.05 0 -13 12 28.28 5.76 0 13 -12 15.00 5.03 0 13 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20.20 4.38 0 -13 19 6.57 2.87 0 13 -19 5.31 2.15 0 13 -19 7.02 2.91 0 -13 -19 7.32 2.28 0 13 -19 6.10 2.29 0 13 19 8.24 2.74 0 -13 20 2.90 2.13 0 13 -20 1.17 1.55 0 -13 -20 2.86 1.62 0 13 20 1.55 1.88 0 13 -20 3.05 2.16 0 13 -20 1.71 1.17 0 13 -21 -0.04 1.12 0 13 -21 -1.30 1.37 0 13 21 -0.48 1.55 0 -13 21 4.15 1.98 0 -13 -21 -0.49 1.39 0 13 -22 39.37 4.84 0 13 -22 44.89 5.21 0 -13 -22 33.58 4.49 0 -13 22 38.85 5.46 0 13 22 40.01 5.02 0 -13 -23 6.33 2.24 0 13 23 6.60 2.37 0 13 -23 5.65 1.96 0 13 -23 6.26 2.11 0 -13 23 9.00 2.96 0 13 24 10.75 2.70 0 13 -24 12.32 2.71 0 13 -24 14.76 2.86 0 -13 24 11.57 2.75 0 -13 -24 9.92 2.31 0 -13 -25 44.31 4.48 0 13 -25 43.30 4.51 0 13 -25 41.63 4.33 0 13 25 45.42 4.77 0 13 -26 2.47 1.27 0 13 -26 1.77 1.19 0 13 26 3.44 1.43 0 -13 -26 2.55 1.16 0 13 27 2.90 1.25 0 13 -27 1.02 0.93 0 13 -27 0.92 0.88 0 -13 -27 2.60 1.16 0 -13 27 0.64 0.91 0 -13 28 6.68 1.65 0 13 28 6.94 1.50 0 -14 0 115.51 9.80 0 -14 0 127.88 9.40 0 14 0 186.28 16.46 0 14 0 176.08 9.40 0 14 0 135.91 9.92 0 -14 0 112.89 14.81 0 -14 1 39.61 5.91 0 14 -1 30.85 3.94 0 14 -1 32.25 7.02 0 -14 1 33.88 8.02 0 14 1 27.94 3.80 0 -14 1 35.07 5.23 0 14 1 29.54 6.92 0 -14 -1 40.30 5.25 0 14 -1 31.83 4.91 0 14 1 31.22 5.05 0 -14 -1 43.39 6.18 0 -14 -1 31.40 7.07 0 -14 2 200.84 12.17 0 -14 -2 214.71 13.30 0 14 2 259.05 19.62 0 14 -2 212.97 12.43 0 14 -2 237.62 10.90 0 14 2 206.85 12.30 0 14 2 226.15 10.62 0 -14 -2 182.21 16.40 0 -14 2 197.06 12.93 0 -14 2 189.96 18.93 0 14 -2 251.21 19.16 0 -14 -3 1.03 2.02 0 14 -3 1.83 1.17 0 -14 3 6.27 2.76 0 14 -3 2.04 2.10 0 14 3 3.18 2.53 0 14 3 0.28 1.99 0 -14 3 9.37 3.18 0 -14 3 1.70 3.77 0 -14 -3 7.44 3.15 0 14 -3 2.96 2.15 0 14 -4 223.13 18.02 0 -14 4 206.02 13.06 0 14 4 220.16 18.16 0 -14 4 211.03 12.74 0 14 -4 220.38 10.55 0 -14 -4 189.41 17.32 0 -14 -4 207.39 13.09 0 14 4 207.38 12.25 0 -14 4 208.16 19.81 0 14 -4 197.08 12.08 0 14 5 39.93 7.82 0 14 -5 43.49 7.98 0 -14 5 31.87 5.21 0 14 5 36.94 5.28 0 -14 5 26.67 5.05 0 -14 -5 26.27 6.58 0 14 -5 36.65 5.66 0 14 -5 42.85 4.79 0 -14 -5 34.37 5.56 0 -14 5 36.44 8.67 0 14 -5 44.12 8.31 0 14 6 77.89 10.88 0 -14 6 59.70 10.87 0 -14 6 51.60 6.89 0 14 -6 79.20 6.55 0 14 -6 67.54 10.09 0 14 -6 64.82 7.22 0 -14 -6 46.55 9.02 0 14 6 62.08 6.88 0 -14 -6 52.25 6.81 0 14 -6 84.50 11.36 0 -14 6 65.96 7.42 0 -14 -7 0.42 1.77 0 -14 -7 0.94 1.61 0 14 -7 -0.44 1.83 0 -14 7 0.39 2.13 0 14 7 -0.53 2.23 0 14 -7 -2.23 3.71 0 -14 7 0.60 1.79 0 14 7 0.69 2.29 0 -14 7 0.01 2.20 0 14 -7 2.12 2.03 0 14 -7 1.32 1.49 0 -14 8 1.28 1.79 0 -14 -8 0.50 2.72 0 14 8 0.73 1.43 0 -14 -8 0.46 1.58 0 14 -8 4.89 2.28 0 -14 8 -1.61 2.69 0 14 -8 1.06 1.49 0 14 8 2.90 2.00 0 14 -8 5.54 3.56 0 14 -8 6.07 2.22 0 -14 8 6.85 5.06 0 -14 9 21.25 4.82 0 14 -9 20.28 5.78 0 14 -9 18.91 3.92 0 14 9 15.85 3.62 0 -14 9 20.43 4.42 0 -14 -9 20.41 4.17 0 14 -9 18.74 3.39 0 14 -10 5.49 2.18 0 14 10 8.89 3.25 0 -14 10 2.82 2.47 0 -14 10 1.65 2.45 0 -14 -10 2.19 2.06 0 14 11 206.86 12.40 0 -14 11 200.76 13.58 0 -14 11 185.04 12.97 0 14 -11 188.17 12.51 0 -14 -11 178.18 11.95 0 14 -11 235.14 11.80 0 -14 12 50.04 7.11 0 14 -12 47.07 5.57 0 -14 12 46.15 6.44 0 14 -12 41.18 6.05 0 14 12 45.17 5.73 0 -14 -12 45.24 6.20 0 14 -13 90.44 9.11 0 -14 13 112.18 10.25 0 -14 -13 116.81 9.46 0 -14 13 132.51 10.68 0 14 -13 81.66 7.21 0 14 13 100.92 8.76 0 -14 -14 5.62 2.59 0 -14 14 2.50 2.04 0 14 14 3.99 2.59 0 14 -14 5.49 2.42 0 14 -14 1.87 1.17 0 -14 14 10.25 3.40 0 14 -14 4.52 2.57 0 14 -15 55.24 7.02 0 -14 -15 66.24 6.90 0 14 15 51.32 6.25 0 -14 15 63.22 7.71 0 14 -15 43.71 5.41 0 14 -15 38.14 5.04 0 -14 16 2.81 1.89 0 14 -16 3.45 2.08 0 -14 -16 7.07 2.78 0 14 16 2.95 2.03 0 14 -16 7.92 3.32 0 14 -16 2.56 1.69 0 -14 17 3.98 2.20 0 14 -17 13.85 3.16 0 -14 -17 6.29 2.49 0 14 -17 6.81 2.63 0 14 -17 11.63 2.79 0 14 17 8.78 2.75 0 14 -18 2.68 2.03 0 14 18 4.74 2.68 0 -14 -18 10.29 3.31 0 -14 18 1.04 1.75 0 14 -18 3.05 1.75 0 14 -18 6.93 2.60 0 -14 19 3.92 2.67 0 14 -19 0.97 1.38 0 14 -19 5.16 2.07 0 14 19 1.29 1.55 0 14 -19 3.41 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3 4.23 2.70 0 -15 3 3.75 2.24 0 15 -3 2.78 1.43 0 15 3 1.02 1.36 0 15 3 2.16 1.38 0 -15 -3 4.36 2.51 0 15 -4 132.71 8.34 0 15 -4 124.05 9.99 0 15 4 126.34 9.89 0 -15 4 135.52 10.53 0 -15 4 133.03 10.91 0 15 4 122.58 7.95 0 -15 -4 138.27 10.70 0 15 5 12.64 3.50 0 -15 5 14.77 3.64 0 -15 -5 21.52 4.61 0 15 -5 18.52 4.13 0 15 -5 22.58 3.71 0 -15 5 19.12 4.39 0 -15 6 180.70 12.38 0 -15 -6 195.28 12.90 0 15 -6 171.62 11.56 0 15 -6 166.32 9.52 0 -15 6 184.33 12.58 0 15 6 170.43 11.44 0 -15 -7 54.71 6.94 0 -15 7 49.61 6.86 0 -15 7 52.75 6.80 0 15 -7 41.65 5.88 0 15 -7 44.42 5.07 0 15 7 43.57 5.86 0 -15 8 13.93 4.18 0 15 -8 11.53 3.24 0 15 8 11.14 3.27 0 -15 -8 18.61 4.08 0 15 -8 11.53 2.73 0 -15 8 19.69 4.26 0 15 -9 123.29 8.42 0 -15 9 111.88 9.93 0 15 9 112.99 9.32 0 15 -9 104.77 9.26 0 -15 9 113.57 10.16 0 -15 -9 111.61 9.71 0 -15 10 17.19 3.89 0 15 -10 18.41 3.41 0 15 10 18.24 3.75 0 -15 -10 21.12 4.56 0 -15 10 24.00 5.20 0 15 -10 15.55 3.74 0 15 -11 47.92 5.31 0 15 -11 42.69 6.08 0 -15 11 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83.73 10.66 1 12 -11 75.47 10.87 1 -12 11 97.60 8.73 1 12 -10 115.12 9.03 1 12 -10 109.67 12.64 1 12 -10 105.68 7.54 -1 -12 -10 109.84 13.00 -1 12 10 117.23 8.93 1 -12 10 124.67 9.81 1 -12 10 116.47 13.72 1 12 -10 108.63 12.50 1 12 -10 94.19 11.82 -1 12 10 112.63 10.75 -1 -12 -10 130.05 9.43 -1 -12 -10 122.16 9.20 -1 12 10 104.07 11.68 1 -12 9 66.58 10.48 -1 -12 -9 65.45 6.67 1 12 -9 71.24 7.02 1 12 -9 65.48 10.17 1 -12 9 64.68 6.92 -1 12 9 67.29 8.32 -1 -12 -9 63.82 6.67 1 12 -9 75.39 6.27 -1 -12 -9 56.74 9.22 1 12 -9 74.65 10.07 1 12 -9 88.81 11.16 -1 12 9 71.87 9.71 -1 12 9 70.62 6.81 1 12 -8 109.71 12.35 -1 12 8 118.32 12.35 -1 -12 -8 93.53 8.13 1 12 -8 98.10 11.54 1 12 -8 100.28 7.11 -1 12 8 102.12 8.35 1 12 -8 108.00 12.02 -1 -12 -8 90.99 12.06 -1 -12 -8 97.68 8.07 1 -12 8 88.58 8.33 1 -12 8 100.57 12.54 1 12 -8 104.55 8.48 1 -12 7 0.97 2.42 1 12 -7 3.81 3.08 -1 -12 -7 2.01 2.53 -1 -12 -7 3.35 3.62 -1 12 7 3.75 1.97 1 12 -7 6.65 3.83 1 -12 7 2.98 2.19 1 12 -7 2.20 1.37 -1 12 7 1.63 2.20 1 12 -7 1.47 1.92 1 12 -7 3.80 2.79 -1 12 6 14.36 3.20 1 12 -6 11.73 4.28 -1 -12 -6 16.58 4.98 1 12 -6 12.92 2.60 1 12 -6 16.36 4.62 1 -12 6 15.03 4.69 1 12 -6 8.47 3.87 -1 -12 -6 20.13 3.84 1 -12 6 19.96 3.73 -1 12 6 8.67 3.13 -1 12 5 13.44 3.33 -1 -12 -5 10.99 3.04 -1 12 5 17.17 4.92 1 12 -5 22.27 5.67 -1 -12 -5 11.13 4.15 1 12 -5 17.84 4.79 1 -12 5 13.22 5.21 1 12 -5 19.04 5.29 1 -12 4 171.97 15.81 1 12 -4 178.70 15.37 -1 12 4 170.16 14.48 -1 -12 -4 180.02 11.24 -1 -12 -4 150.40 14.65 -1 12 4 169.80 10.32 1 12 -4 176.15 14.56 -1 -12 -3 62.33 9.50 1 12 -3 65.18 9.23 1 12 -3 61.41 9.11 1 -12 3 59.85 9.68 -1 12 3 64.97 9.15 -1 -12 -2 53.84 9.25 -1 12 2 66.46 9.17 1 12 -2 67.19 9.46 -1 -12 -2 57.33 8.66 1 -12 2 71.61 10.76 1 12 -2 64.16 8.73 -1 -12 -1 98.20 12.29 -1 -12 -1 107.41 11.75 1 12 -1 111.95 12.24 1 -12 1 96.95 12.05 1 -12 1 113.00 11.12 1 12 -1 108.84 11.44 -1 12 1 106.60 11.34 -1 -12 0 11.15 4.07 1 -12 0 15.43 4.96 1 -12 0 17.07 4.67 -1 -12 0 19.80 5.50 1 12 0 17.91 4.99 1 12 0 25.68 5.54 -1 12 0 22.54 5.64 1 -12 -1 105.95 11.00 -1 12 -1 94.47 10.44 -1 -12 1 96.06 12.06 -1 -12 1 105.88 11.47 1 12 1 108.15 11.46 1 12 1 103.05 11.81 1 -12 -1 92.50 11.57 1 12 2 70.50 9.25 1 12 2 61.41 9.29 -1 12 -2 64.35 8.71 -1 -12 2 68.82 10.70 1 -12 -2 65.87 9.90 1 -12 -2 63.55 8.82 -1 -12 2 68.89 9.33 -1 12 -2 59.97 8.41 -1 12 -3 67.86 9.17 1 12 3 65.30 9.29 1 12 3 62.38 9.68 -1 -12 3 67.70 10.51 -1 12 -3 61.51 8.57 1 -12 -3 65.80 8.95 -1 -12 3 69.05 9.33 1 -12 -3 67.23 7.01 -1 12 -4 159.80 14.02 -1 -12 4 175.89 11.09 -1 -12 4 172.34 14.55 -1 12 -4 168.66 10.41 -1 12 -4 177.72 14.23 1 -12 -4 170.17 11.15 -1 -12 4 158.74 15.82 1 -12 -4 161.17 14.41 1 12 4 176.80 14.87 -1 -12 5 11.90 4.91 -1 -12 5 8.22 2.68 1 12 5 12.20 2.85 1 -12 -5 10.03 3.83 1 -12 -5 12.52 3.16 -1 12 -5 16.77 4.37 -1 12 -5 16.19 4.91 -1 -12 5 16.58 3.60 1 12 5 17.20 4.64 -1 12 -5 12.54 3.12 1 12 6 13.95 4.65 -1 12 -6 18.37 3.57 -1 12 -6 6.31 2.87 -1 -12 6 25.50 4.36 -1 -12 6 18.38 5.92 -1 -12 6 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8.18 -2 -11 -4 52.01 8.17 -2 11 4 44.21 6.87 2 11 -4 44.55 7.05 -2 -11 -3 53.67 8.39 2 11 -3 59.65 8.41 2 -11 3 59.41 8.77 -2 11 3 53.57 7.55 2 11 -3 53.64 7.81 -2 11 2 18.02 5.07 -2 -11 -2 5.72 3.88 2 11 -2 15.41 4.31 -2 -11 -2 4.43 3.26 2 11 -2 24.35 5.67 2 -11 2 6.57 4.02 -2 -11 -1 84.73 10.86 -2 11 1 77.26 9.06 2 -11 1 86.33 10.19 -2 -11 -1 95.07 10.75 2 11 -1 81.52 9.77 2 11 -1 77.98 9.24 2 -11 0 201.56 15.59 -2 11 0 167.91 13.37 -2 -11 0 186.76 16.40 2 -11 0 227.28 14.59 2 11 0 171.62 13.49 -2 -11 0 230.02 16.85 2 11 0 160.07 13.49 2 11 1 85.66 9.58 -2 -11 1 82.91 10.86 -2 11 -1 87.64 9.50 2 -11 -1 91.69 9.41 2 -11 -1 88.56 10.36 2 11 1 86.40 9.94 -2 -11 1 90.94 10.38 2 11 2 14.87 4.21 2 -11 -2 5.92 2.97 -2 -11 2 6.90 3.61 -2 11 -2 16.71 4.42 2 11 2 23.19 5.54 -2 -11 2 8.30 4.26 2 -11 -2 4.83 2.95 -2 11 -2 24.33 5.54 2 11 3 54.17 8.11 2 -11 -3 53.94 8.10 2 -11 -3 53.80 7.84 -2 11 -3 59.77 7.84 -2 -11 3 54.62 8.79 -2 11 -3 64.92 8.62 -2 -11 3 49.80 7.75 2 11 3 61.74 8.16 2 11 3 58.53 6.46 -2 11 -4 45.17 6.87 2 11 4 45.98 7.22 -2 -11 4 57.12 8.27 2 -11 -4 50.09 7.58 -2 11 -4 47.97 7.89 2 11 4 46.43 6.21 -2 -11 4 56.66 9.04 2 11 4 40.71 7.17 2 11 5 0.97 1.57 -2 11 -5 3.52 2.52 -2 -11 5 4.41 4.07 2 -11 -5 1.49 1.93 2 11 5 4.16 2.88 2 11 5 4.01 2.37 -2 11 -5 6.59 3.51 -2 11 -6 178.20 13.42 2 11 6 175.93 13.73 -2 11 -6 164.39 14.88 2 11 6 161.36 14.04 2 11 6 172.86 11.89 2 -11 -6 168.63 13.96 -2 -11 6 189.39 16.47 -2 11 -7 9.35 4.13 2 11 7 4.44 3.06 -2 11 -7 6.40 3.10 2 -11 -7 2.82 2.88 -2 -11 7 7.10 4.39 2 11 7 8.91 3.35 2 -11 -8 139.93 9.92 -2 -11 8 132.47 9.75 2 -11 -8 118.09 12.30 -2 11 -8 135.36 14.24 -2 -11 8 127.95 13.60 2 11 8 134.05 11.22 -2 11 -8 130.20 9.24 2 11 8 133.45 12.11 -2 11 -8 145.40 12.65 2 -11 -9 140.75 9.81 -2 11 -9 109.35 12.85 2 11 9 111.79 11.27 2 -11 -9 103.34 11.82 -2 -11 9 121.72 13.32 -2 11 -9 119.58 8.54 2 11 9 120.30 10.84 -2 -11 9 134.57 9.91 -2 -11 9 136.51 9.99 -2 11 -9 125.05 9.27 2 11 9 129.17 8.60 -2 11 -9 124.80 11.66 2 11 10 87.39 7.38 2 11 10 82.23 9.54 2 -11 -10 84.96 8.21 -2 -11 10 90.63 8.30 2 -11 -10 80.27 10.49 -2 -11 10 81.94 8.11 -2 11 -10 86.54 9.80 -2 11 -10 75.03 10.87 -2 -11 10 89.06 11.86 -2 11 -10 79.38 7.10 2 11 10 79.25 8.98 -2 11 -10 82.57 7.85 2 11 11 225.37 11.73 2 11 11 194.83 14.47 2 -11 -11 278.14 14.02 -2 -11 11 242.61 19.45 -2 -11 11 238.82 13.69 2 -11 -11 223.07 17.84 -2 -11 11 260.33 14.21 -2 11 -11 192.53 17.71 -2 11 -11 195.60 11.31 2 11 11 226.36 15.45 -2 11 -11 216.84 12.74 -2 11 -11 194.66 14.84 2 -11 -12 29.41 4.82 2 11 12 29.06 6.81 2 11 12 29.18 5.98 -2 -11 12 25.09 5.11 -2 11 -12 30.06 6.25 -2 -11 12 28.89 7.07 -2 11 -12 22.29 4.03 -2 -11 12 20.39 4.41 -2 11 -12 24.50 6.58 2 -11 -12 18.38 5.35 -2 11 -12 29.37 5.02 -2 -11 13 73.62 7.77 2 -11 -13 65.64 10.40 -2 -11 13 89.37 12.15 -2 -11 13 80.92 8.18 -2 11 -13 84.71 7.71 2 11 13 79.67 9.66 2 -11 -13 76.99 7.57 2 11 13 95.60 10.13 -2 11 -13 81.91 8.20 -2 11 -13 84.20 12.23 -2 -11 14 65.12 7.47 2 -11 -14 70.28 7.31 -2 11 -14 51.06 6.69 -2 -11 14 51.89 9.87 -2 11 -14 42.05 8.83 2 -11 -14 54.08 9.68 -2 11 -14 48.51 5.88 2 11 14 60.99 8.77 -2 -11 14 68.15 7.54 -2 -11 15 31.63 5.39 2 -11 -15 32.94 5.53 2 -11 -15 28.99 8.27 -2 -11 15 29.32 5.29 -2 11 -15 29.09 4.82 -2 -11 15 36.53 8.38 2 11 15 33.96 7.13 -2 11 -15 20.60 6.67 -2 11 -15 26.19 5.38 -2 -11 16 67.83 7.62 -2 -11 16 81.13 8.27 2 -11 -16 72.46 7.40 -2 -11 16 53.56 9.44 -2 11 -16 19.88 6.70 -2 11 -16 37.17 5.27 2 -11 -16 51.88 9.46 2 11 16 51.01 8.23 -2 11 -16 42.31 6.32 2 -11 -17 41.24 5.68 -2 11 -17 43.82 6.02 -2 -11 17 48.43 6.68 -2 11 -17 44.58 6.60 -2 11 -18 16.48 3.64 2 -11 -18 17.67 3.83 -2 -11 18 19.30 4.42 -2 11 -18 19.55 4.31 -2 11 -19 8.32 2.47 2 -11 -19 3.52 2.28 -2 -11 19 3.20 2.26 -2 11 -19 5.77 2.49 -2 11 -19 4.97 2.38 -2 -11 20 34.07 5.53 -2 11 -20 31.66 5.07 -2 11 -20 25.43 4.99 2 -11 -20 27.45 4.47 -2 11 -20 31.63 4.62 2 -11 -21 16.54 3.48 -2 11 -21 17.55 3.79 -2 11 -21 15.93 3.89 -2 11 -21 19.70 3.79 -2 -11 21 19.05 4.26 -2 11 -22 11.38 3.15 -2 11 -22 9.83 2.85 -2 11 -22 13.19 3.80 -2 -11 22 13.49 3.65 -2 11 -23 2.26 1.56 -2 11 -23 5.99 2.20 -2 -11 23 2.60 1.64 -2 -11 24 26.26 4.39 -2 11 -24 22.79 4.02 -2 11 -24 21.91 3.55 2 11 25 4.17 1.75 -2 11 -25 3.65 1.58 -2 11 -25 1.19 1.47 -2 11 -26 14.84 3.02 2 11 26 13.07 2.75 -2 -11 26 16.33 3.20 -2 11 -26 14.81 2.79 -2 -11 27 2.37 1.54 2 11 27 2.58 1.10 -2 11 -27 5.65 1.85 -2 11 -27 3.64 1.36 2 11 28 0.93 1.27 -2 -11 28 3.06 1.44 -2 11 -28 1.53 1.33 2 11 29 4.90 1.48 -2 -11 29 4.73 1.73 -2 11 -29 4.61 1.60 -2 -11 30 9.68 2.00 -2 11 -30 9.41 1.88 2 11 30 8.50 1.69 -2 -12 -29 14.66 2.17 2 12 -29 12.97 2.13 -2 12 28 13.93 2.07 2 12 -28 18.04 2.80 -2 -12 -28 12.93 2.35 2 12 -27 11.06 2.48 -2 -12 -27 13.37 2.50 -2 12 27 13.64 2.29 2 12 -27 12.84 1.95 -2 12 26 20.12 2.93 2 12 -26 20.80 3.00 -2 -12 -26 22.01 3.65 2 12 -26 19.53 3.34 -2 12 25 0.12 0.96 -2 -12 -25 2.85 1.57 2 12 -25 2.22 1.66 2 12 -25 0.79 1.25 2 12 -24 22.10 3.43 -2 -12 -24 14.46 3.06 2 12 -24 12.62 2.72 -2 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134.32 9.46 2 -12 4 130.92 13.67 -2 -12 -4 126.56 9.23 -2 -12 -4 123.53 13.56 2 12 -4 136.13 8.21 2 12 -4 137.87 13.36 2 12 -4 147.16 14.01 -2 12 3 11.74 4.17 2 12 -3 10.48 2.33 2 12 -3 12.97 4.34 -2 12 3 11.44 2.97 2 -12 3 15.53 5.17 -2 -12 -3 15.79 3.37 -2 -12 -3 11.28 4.57 2 12 -3 11.54 4.09 -2 12 2 22.38 3.99 2 12 -2 26.09 5.75 -2 -12 -2 27.59 4.50 2 12 -2 25.16 3.49 -2 -12 -2 28.96 6.61 2 -12 2 21.12 5.79 -2 -12 -2 20.63 5.79 -2 12 2 24.78 5.86 2 12 -2 29.26 6.14 -2 -12 -1 76.22 7.12 2 -12 1 81.26 10.52 -2 -12 -1 68.00 10.43 -2 12 1 91.89 10.64 2 12 -1 94.19 10.74 -2 -12 -1 70.19 9.81 -2 12 1 83.67 7.38 2 12 -1 89.35 10.85 2 12 0 18.23 5.12 -2 12 0 22.98 5.08 -2 -12 0 20.09 5.35 -2 -12 0 17.95 5.46 2 12 0 15.03 4.46 -2 -12 0 24.68 4.31 -2 12 0 25.99 4.37 2 -12 0 19.24 5.21 2 12 1 94.36 10.59 2 12 1 89.85 10.77 -2 12 -1 97.43 10.87 -2 -12 1 74.02 7.06 -2 -12 1 74.77 11.37 -2 12 -1 87.67 7.68 -2 -12 1 75.47 9.97 2 -12 -1 74.46 10.09 2 -12 -1 72.34 7.48 2 -12 -2 25.59 5.45 2 -12 -2 28.66 4.85 2 12 2 22.96 5.54 -2 12 -2 28.63 5.75 -2 -12 2 30.35 6.48 2 12 2 23.71 5.36 -2 -12 2 31.84 4.82 2 -12 -2 25.40 6.09 -2 -12 2 23.35 6.71 -2 12 -2 26.44 4.20 2 -12 -3 20.64 3.94 -2 12 -3 16.70 4.73 -2 -12 3 13.47 4.36 2 -12 -3 14.93 4.31 2 12 3 15.06 4.46 -2 -12 3 17.18 5.37 2 12 3 8.81 3.46 -2 12 -3 12.46 3.13 -2 -12 3 19.87 3.94 2 12 4 144.96 13.23 -2 -12 4 130.06 14.73 2 -12 -4 121.06 9.87 -2 12 -4 141.66 12.59 -2 12 -4 138.20 9.66 2 -12 -4 125.40 12.28 -2 -12 4 133.97 9.74 2 12 4 140.76 13.80 -2 12 -4 149.73 13.90 -2 -12 4 129.02 13.08 -2 -12 4 115.61 9.08 2 12 5 230.40 16.76 2 -12 -5 216.60 12.50 2 12 5 215.74 17.44 -2 -12 5 206.83 12.36 2 -12 -5 204.89 16.23 -2 -12 5 222.51 12.69 -2 12 -5 247.03 16.69 -2 -12 5 218.55 18.64 -2 12 -5 236.03 17.83 -2 12 -5 219.62 12.19 2 12 5 215.46 11.15 2 12 6 20.87 3.67 -2 -12 6 13.55 2.90 -2 -12 6 12.78 3.39 -2 12 -6 24.91 5.31 2 12 6 12.50 3.46 2 12 6 25.88 5.70 -2 -12 6 16.28 3.83 2 -12 -6 11.07 3.29 -2 12 -6 25.47 6.65 2 -12 -6 15.50 5.16 -2 -12 6 20.10 6.26 -2 12 -6 17.63 3.45 -2 12 -6 16.79 3.83 2 12 7 124.75 12.28 -2 12 -7 123.14 13.78 2 -12 -7 127.93 9.89 -2 -12 7 117.87 8.69 -2 -12 7 115.65 9.40 2 12 7 120.87 8.63 2 -12 -7 106.14 12.11 -2 12 -7 120.68 8.77 2 12 7 99.13 9.77 -2 12 -7 122.94 9.37 -2 -12 7 116.53 13.99 -2 -12 7 105.58 8.99 -2 12 -7 135.84 12.67 -2 -12 8 281.86 13.32 -2 -12 8 277.29 14.67 2 12 8 271.51 18.00 -2 12 -8 264.33 13.04 2 -12 -8 246.24 18.41 -2 -12 8 266.30 20.97 -2 -12 8 285.33 14.85 2 -12 -8 293.31 14.80 2 12 8 247.48 15.59 -2 12 -8 257.64 20.30 -2 12 -8 281.84 18.30 -2 12 -8 284.18 14.29 2 12 8 282.20 13.14 2 12 9 17.32 3.43 -2 12 -9 13.26 4.24 -2 -12 9 23.79 4.13 -2 12 -9 15.84 3.37 2 -12 -9 29.43 5.14 2 -12 -9 17.67 5.28 2 12 9 16.37 4.22 -2 -12 9 31.54 5.18 -2 -12 9 23.79 4.55 -2 -12 9 24.48 6.57 -2 12 -9 24.44 4.39 -2 12 -9 13.53 5.39 2 12 9 11.47 4.01 2 12 10 289.24 18.80 2 12 10 241.59 15.97 -2 -12 10 271.58 21.41 -2 -12 10 253.84 14.67 2 12 10 281.20 13.52 2 -12 -10 224.88 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31.31 6.39 -2 -12 14 35.93 5.83 -2 -12 14 31.34 5.42 2 12 15 0.25 1.30 -2 -12 15 1.46 1.71 -2 -12 15 4.25 2.44 -2 12 -15 4.09 2.33 2 -12 -15 2.02 2.04 -2 12 -15 1.03 1.96 -2 -12 16 26.52 4.96 -2 -12 16 23.41 4.59 -2 12 -16 25.26 4.62 2 12 16 24.94 4.38 2 -12 -16 24.50 4.64 -2 12 -16 21.12 4.51 2 12 17 47.56 6.01 -2 -12 17 46.18 6.73 2 -12 -17 52.13 6.63 -2 12 -17 39.06 5.44 -2 12 -17 42.33 6.47 2 12 18 17.84 3.86 2 -12 -18 22.65 4.50 -2 -12 18 18.42 4.39 -2 12 -18 15.54 3.86 -2 12 -18 16.09 3.65 2 12 19 24.80 4.37 -2 -12 19 26.42 5.05 -2 12 -19 20.16 4.04 -2 12 -19 24.67 4.83 2 -12 -19 27.81 4.83 2 12 20 3.82 2.13 -2 12 -20 2.84 1.79 2 -12 -20 1.44 1.33 -2 12 -20 0.27 1.71 -2 -12 20 2.55 1.88 2 12 21 2.39 1.79 -2 -12 21 1.16 1.62 -2 12 -21 0.30 1.68 2 -12 -21 4.75 2.06 -2 12 -21 0.70 1.63 2 12 22 33.57 4.63 -2 -12 22 27.57 4.70 -2 12 -22 36.52 5.06 2 12 23 29.70 4.43 -2 12 -23 26.07 4.25 -2 -12 23 21.61 4.04 2 12 24 15.39 3.21 -2 -12 24 14.00 3.16 -2 12 -24 16.41 3.32 2 12 25 1.64 1.83 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16.79 5.18 4 -9 -8 12.23 3.99 4 9 8 20.71 4.67 -4 9 -9 21.37 5.89 4 -9 -9 13.18 4.20 -4 -9 9 14.86 4.59 4 9 9 23.00 4.71 4 9 9 14.94 4.64 4 -9 -10 128.94 12.78 -4 -9 10 152.63 13.73 -4 9 -10 152.43 16.02 4 9 10 141.81 12.62 -4 -9 11 1.48 1.49 -4 9 -11 -0.31 2.91 4 -9 -11 1.26 1.53 -4 -9 11 3.38 1.88 4 -9 -11 2.92 2.15 -4 -9 11 6.26 3.47 -4 9 -11 3.40 1.77 -4 -9 11 3.00 1.31 4 9 11 2.97 2.06 -4 9 -11 3.21 1.40 4 -9 -12 65.87 6.83 -4 -9 12 59.55 6.93 4 -9 -12 56.78 8.90 -4 -9 12 63.22 9.09 -4 9 -12 63.42 6.22 -4 9 -12 64.39 6.51 -4 9 -12 82.49 12.33 4 9 12 65.00 8.76 -4 -9 12 55.23 6.84 -4 9 -12 59.76 6.89 -4 -9 13 164.14 11.51 4 -9 -13 195.72 11.80 -4 -9 13 178.19 12.18 4 9 13 173.39 14.70 4 -9 -13 161.44 15.35 -4 -9 13 173.81 15.25 -4 9 -13 171.69 10.82 -4 9 -13 157.88 17.24 -4 9 -13 172.11 11.82 -4 9 -13 173.84 10.18 4 -9 -14 68.38 7.21 -4 9 -14 68.11 6.49 -4 -9 14 66.77 7.65 4 -9 -14 60.74 9.95 -4 9 -14 72.29 7.21 -4 9 -14 69.84 11.66 4 9 14 67.50 9.46 -4 9 -14 59.18 7.07 -4 -9 14 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71.17 9.52 -4 -13 5 17.32 3.81 4 13 5 29.09 6.19 -4 -13 5 16.50 4.18 4 -13 -5 18.00 4.21 -4 -13 5 23.18 5.49 4 13 5 37.46 7.64 -4 -13 5 18.87 6.20 -4 13 -5 22.29 4.48 4 13 6 23.58 3.90 -4 -13 6 20.65 4.28 4 -13 -6 25.66 4.90 -4 -13 6 22.57 4.70 4 13 6 24.23 6.33 -4 -13 6 17.69 5.86 -4 13 -6 20.57 4.05 4 13 6 28.15 5.98 -4 13 -6 26.19 4.70 -4 -13 6 26.64 4.96 4 13 7 12.31 3.04 -4 -13 7 15.05 4.00 -4 -13 7 13.69 3.94 -4 -13 7 20.40 4.94 -4 -13 7 17.98 7.26 4 -13 -7 17.77 4.38 -4 13 -7 11.77 3.21 -4 13 -7 14.84 4.01 4 -13 -8 115.37 10.19 -4 -13 8 107.65 9.96 -4 -13 8 104.25 9.20 -4 -13 8 112.10 10.18 -4 -13 8 99.59 13.88 -4 13 -8 86.79 8.00 -4 13 -8 92.17 8.91 4 13 8 103.13 8.24 -4 -13 9 30.24 5.07 -4 -13 9 22.31 4.74 4 -13 -9 30.16 5.27 -4 -13 9 29.46 5.73 -4 13 -9 30.04 4.91 -4 13 -9 36.44 5.89 4 13 9 38.28 4.93 4 13 10 3.18 1.79 -4 -13 10 4.61 2.90 4 -13 -10 4.66 3.13 -4 -13 10 10.53 3.85 -4 13 -10 2.08 1.31 -4 13 -10 4.94 2.66 4 -13 -11 103.53 9.55 -4 -13 11 96.40 9.55 -4 13 -11 91.72 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161.37 11.69 -4 14 -4 183.94 12.62 -4 -14 5 104.10 9.73 4 -14 -5 99.45 9.50 -4 -14 5 100.96 8.90 -4 -14 5 92.48 9.00 -4 14 -5 69.38 7.13 -4 14 -5 88.05 8.78 4 14 5 87.01 7.59 -4 -14 6 47.03 6.88 -4 -14 6 57.25 7.01 -4 -14 6 60.02 7.47 -4 14 -6 73.20 7.46 -4 14 -6 69.01 7.94 4 14 6 71.48 6.92 4 -14 -6 57.73 7.31 -4 -14 7 31.96 5.86 4 -14 -7 37.42 6.17 -4 -14 7 34.76 5.37 -4 -14 7 33.98 5.56 -4 14 -7 35.31 5.03 -4 14 -7 37.74 5.84 4 14 7 36.12 4.92 4 14 8 18.05 3.40 -4 -14 8 13.14 3.46 -4 -14 8 14.13 3.46 -4 -14 8 20.21 4.36 4 -14 -8 12.83 3.77 -4 14 -8 19.52 3.73 -4 14 -8 15.48 3.71 4 14 9 9.89 2.80 4 -14 -9 6.97 2.80 -4 -14 9 5.47 2.80 -4 14 -9 8.71 2.83 -4 14 -9 9.55 3.36 -4 -14 9 3.88 2.29 4 -14 -10 115.00 10.23 -4 -14 10 118.64 10.54 -4 14 -10 102.44 8.69 -4 -14 10 119.29 10.75 -4 14 -10 121.35 10.38 4 14 10 111.66 8.68 4 -14 -11 9.08 3.25 4 14 11 2.52 1.38 -4 -14 11 5.00 2.50 -4 -14 11 3.60 2.79 -4 14 -11 1.83 2.06 -4 14 -11 1.94 2.80 4 14 12 19.41 3.79 -4 -14 12 20.20 4.47 -4 -14 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10.65 3.10 5 12 -8 10.93 4.50 -5 -12 -8 7.74 2.53 -5 -12 -8 12.90 4.71 -5 12 8 10.49 4.23 5 12 -8 10.29 2.72 5 12 -8 10.94 4.31 -5 12 8 7.17 2.33 -5 -12 -7 74.97 7.66 -5 12 7 70.88 7.21 -5 12 7 75.53 10.19 5 12 -7 71.03 6.60 -5 -12 -7 73.69 10.98 5 12 -7 84.28 11.81 5 12 -7 71.64 10.76 -5 12 7 71.22 6.95 -5 12 6 14.46 3.53 5 12 -6 26.22 6.80 -5 -12 -6 10.55 2.89 -5 12 6 12.23 4.26 -5 -12 -6 9.27 2.39 5 12 -6 16.95 3.43 -5 -12 -6 12.56 4.71 5 12 -6 17.45 5.72 -5 12 6 15.34 3.33 -5 12 5 96.82 8.52 -5 -12 -5 114.78 9.00 -5 -12 -5 114.33 9.44 -5 12 5 89.15 10.80 5 12 -5 91.76 7.48 -5 -12 -5 94.20 12.40 5 12 -5 89.55 11.70 5 12 -5 87.13 11.48 -5 12 5 96.56 8.11 -5 12 4 65.08 6.99 -5 -12 -4 52.55 6.03 -5 12 4 83.83 10.37 -5 -12 -4 63.28 7.09 5 12 -4 73.53 6.61 -5 -12 -4 56.73 9.80 5 12 -4 74.51 10.77 5 12 -4 69.64 10.15 -5 12 4 68.41 6.94 -5 12 3 46.54 5.97 5 -12 3 42.68 5.66 -5 12 3 52.12 8.15 -5 -12 -3 43.32 5.90 -5 -12 -3 40.49 8.17 5 12 -3 54.56 9.08 5 12 -3 50.41 5.64 5 12 -3 46.09 7.89 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38.77 5.30 -5 13 9 2.65 1.72 -5 -13 -9 3.56 2.66 -5 13 9 6.79 2.37 -5 13 8 25.41 4.55 5 13 -8 29.15 4.43 -5 -13 -8 27.05 4.87 -5 13 8 26.20 4.47 -5 13 7 12.25 3.27 -5 -13 -7 7.29 2.24 -5 -13 -7 10.67 2.96 5 13 -7 11.91 2.97 -5 13 7 9.86 2.68 -5 13 6 5.99 2.57 -5 -13 -6 7.03 2.22 -5 -13 -6 8.62 2.83 5 13 -6 11.32 2.91 -5 13 6 6.98 2.52 -5 13 5 17.68 3.73 -5 -13 -5 16.99 2.98 -5 -13 -5 19.47 4.08 5 13 -5 17.54 3.49 -5 13 5 16.51 3.73 -5 13 4 29.48 4.92 -5 -13 -4 20.78 3.98 -5 -13 -4 24.49 4.65 -5 13 4 36.12 7.23 5 13 -4 39.01 8.16 5 13 -4 38.66 5.07 -5 13 4 31.70 5.11 5 13 -4 36.34 7.68 -5 13 3 56.73 6.56 -5 -13 -3 87.49 14.75 5 -13 3 77.70 7.77 -5 13 3 53.81 8.67 -5 -13 -3 64.68 7.28 5 13 -3 52.16 5.70 -5 -13 -3 66.59 10.62 5 13 -3 60.47 10.13 5 13 -3 43.03 8.02 -5 13 3 63.03 6.83 -5 13 2 83.53 8.03 -5 -13 -2 76.30 8.00 -5 13 2 95.50 11.49 -5 -13 -2 91.15 8.73 5 -13 2 83.57 8.36 5 13 -2 110.72 8.19 -5 -13 -2 81.49 11.83 5 13 -2 120.23 13.76 5 13 -2 95.40 12.01 -5 13 2 90.26 8.17 5 13 -1 24.54 6.15 5 -13 1 18.95 4.18 -5 13 1 22.08 4.35 -5 -13 -1 14.15 3.94 -5 -13 -1 20.07 4.37 -5 13 1 30.04 6.22 5 13 -1 28.02 4.22 -5 -13 -1 12.96 4.70 5 13 -1 29.54 6.88 -5 13 1 21.52 4.07 -5 13 0 53.19 8.30 -5 -13 0 53.77 6.80 5 -13 0 61.67 7.28 -5 -13 0 60.63 7.09 5 13 0 55.26 6.09 5 13 0 59.10 9.60 5 13 0 49.61 8.52 -5 13 0 53.98 6.36 5 13 1 24.11 5.88 -5 -13 1 20.17 4.19 -5 -13 1 17.58 4.07 -5 13 -1 29.41 6.23 -5 -13 1 19.40 4.44 5 13 1 25.06 3.83 5 13 1 23.83 6.27 -5 13 -1 20.02 4.04 5 -13 -1 18.17 4.14 -5 -13 2 80.69 8.30 5 -13 -2 81.57 8.45 -5 -13 2 86.67 8.55 -5 -13 2 83.07 8.57 -5 13 -2 87.59 8.43 5 13 2 88.06 10.96 5 13 2 110.83 13.17 -5 -13 3 74.92 7.96 -5 -13 3 65.61 7.51 5 -13 -3 80.82 8.45 -5 -13 3 63.44 7.54 -5 13 -3 69.31 7.71 5 13 3 44.12 7.59 5 13 3 48.13 8.65 5 13 4 43.23 8.23 -5 -13 4 20.22 4.89 -5 -13 4 23.01 4.90 5 -13 -4 24.00 4.91 -5 -13 4 24.43 6.93 -5 -13 4 21.42 4.38 -5 13 -4 31.31 5.15 -5 -13 5 20.34 4.28 5 -13 -5 23.82 4.75 -5 -13 5 20.59 4.59 -5 -13 5 20.56 4.33 5 13 5 15.25 5.20 -5 13 -5 18.17 4.39 -5 -13 6 8.83 3.22 -5 -13 6 7.70 2.98 -5 -13 6 6.75 2.71 5 -13 -6 7.09 3.16 -5 13 -6 9.04 2.79 -5 13 -6 12.13 3.63 -5 -13 7 9.69 3.47 5 -13 -7 6.64 3.02 -5 -13 7 9.40 2.85 -5 -13 7 9.31 3.30 -5 13 -7 10.65 3.26 -5 13 -7 6.91 2.74 -5 -13 8 19.57 4.57 5 -13 -8 23.78 4.73 -5 -13 8 25.13 4.74 -5 -13 8 27.93 5.33 -5 13 -8 24.55 4.56 -5 13 -8 24.97 4.62 -5 -13 9 0.34 1.92 -5 -13 9 3.07 2.43 5 -13 -9 5.29 2.55 -5 -13 9 3.07 2.28 -5 13 -9 7.27 2.53 -5 13 -9 3.64 2.24 5 -13 -10 33.38 5.63 -5 -13 10 27.74 5.15 -5 -13 10 33.36 5.96 -5 13 -10 42.43 5.92 -5 13 -10 38.29 5.84 5 13 10 48.23 5.55 5 -13 -11 78.07 8.24 -5 -13 11 66.26 8.20 -5 13 -11 69.81 7.32 -5 -13 11 66.03 7.95 -5 13 -11 67.43 7.91 5 13 11 76.82 6.93 5 -13 -12 118.05 10.14 -5 -13 12 118.11 10.63 -5 13 -12 130.24 9.86 -5 13 -12 127.36 10.63 -5 -13 12 92.70 9.49 5 13 12 133.20 9.11 5 -13 -13 65.62 7.60 -5 -13 13 56.21 7.27 -5 13 -13 40.88 5.50 -5 13 -13 54.39 7.20 5 13 13 53.19 5.69 5 13 14 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5.95 -5 14 13 46.05 5.84 -5 -14 -12 21.25 4.15 5 14 -12 15.60 3.55 -5 14 12 21.93 4.12 -5 -14 -11 4.64 2.37 5 14 -11 10.97 2.93 -5 14 11 6.65 2.65 -5 -14 -10 12.29 3.58 5 14 -10 8.64 2.70 -5 14 10 8.28 2.79 -5 14 9 60.71 6.55 5 14 -9 72.87 7.07 -5 -14 -9 66.11 7.38 -5 14 9 73.00 7.31 -5 14 8 5.02 2.44 -5 -14 -8 3.15 2.26 5 14 -8 7.21 2.42 -5 14 8 5.53 2.61 -5 14 7 21.77 4.10 -5 -14 -7 17.33 3.45 -5 -14 -7 19.33 4.29 5 14 -7 27.78 4.34 -5 14 7 23.97 4.33 -5 14 6 16.75 3.51 -5 -14 -6 20.30 4.10 5 14 -6 20.89 3.58 -5 -14 -6 18.44 3.98 -5 14 6 17.20 3.68 -5 14 5 67.83 7.14 -5 -14 -5 74.34 7.68 -5 -14 -5 69.58 7.30 5 14 -5 76.14 6.84 -5 14 5 77.10 7.63 -5 14 4 13.71 3.64 -5 -14 -4 17.25 3.92 5 -14 4 18.11 3.81 -5 -14 -4 16.69 3.80 5 14 -4 12.80 3.18 -5 14 4 15.76 3.87 5 -14 3 45.74 6.04 -5 -14 -3 45.93 6.35 -5 -14 -3 49.40 6.39 5 14 -3 43.41 5.35 -5 14 3 43.89 6.01 -5 -14 -2 3.77 2.42 5 -14 2 2.68 2.21 -5 -14 -2 5.97 3.05 5 14 -2 8.38 2.58 -5 14 2 6.22 2.98 -5 -14 -1 55.41 6.84 5 -14 1 54.54 6.92 -5 -14 -1 52.58 6.59 5 14 -1 44.30 5.44 -5 14 1 51.38 6.50 5 -14 0 0.84 1.75 -5 -14 0 3.23 2.35 -5 -14 0 2.73 1.91 -5 14 0 6.59 2.59 -5 -14 1 48.82 6.57 5 -14 -1 49.60 6.66 -5 -14 1 43.44 5.88 -5 -14 1 47.74 6.37 5 14 1 44.91 5.46 -5 14 -1 49.18 6.62 -5 -14 2 4.40 2.63 5 -14 -2 4.24 1.91 -5 -14 2 8.93 3.07 5 14 2 10.48 2.96 -5 -14 2 0.83 2.13 -5 14 -2 8.64 3.61 5 -14 -3 39.89 6.07 -5 -14 3 46.67 6.25 -5 -14 3 40.36 5.69 -5 14 -3 38.65 5.88 -5 -14 3 40.67 6.03 -5 -14 4 16.97 4.00 5 -14 -4 15.97 3.84 -5 -14 4 15.21 3.92 -5 -14 4 13.38 3.75 -5 14 -4 19.10 4.64 -5 -14 5 69.45 8.01 5 -14 -5 76.30 8.35 -5 -14 5 70.69 7.93 -5 -14 5 75.73 8.32 -5 14 -5 74.52 7.57 -5 14 -5 76.83 8.05 -5 -14 6 22.46 4.46 5 -14 -6 18.67 4.42 -5 -14 6 23.50 4.86 -5 -14 6 19.38 4.36 -5 14 -6 18.47 3.81 -5 14 -6 19.47 4.41 -5 -14 7 12.79 3.98 5 -14 -7 18.40 4.52 -5 -14 7 18.86 4.15 -5 -14 7 20.40 4.78 -5 14 -7 21.64 4.16 -5 14 -7 20.65 4.43 -5 -14 8 1.26 1.80 -5 -14 8 1.33 2.11 5 -14 -8 4.89 2.81 -5 -14 8 4.15 2.59 -5 14 -8 5.53 2.27 -5 14 -8 1.50 1.60 -5 -14 9 57.38 7.32 5 -14 -9 58.25 7.42 -5 14 -9 65.30 7.04 -5 -14 9 54.59 7.17 -5 14 -9 70.30 7.98 -5 -14 10 12.24 3.73 5 -14 -10 12.72 3.86 -5 -14 10 10.79 3.55 -5 14 -10 7.55 2.73 -5 14 -10 8.38 3.02 5 14 11 4.17 1.70 5 -14 -11 3.26 2.11 -5 -14 11 4.36 2.71 -5 14 -11 5.63 2.47 -5 14 -11 4.84 2.12 -5 -14 11 2.89 2.35 5 14 12 19.10 3.51 5 -14 -12 25.11 4.85 -5 -14 12 22.61 4.62 -5 14 -12 17.87 3.91 -5 14 -12 20.40 4.50 5 -14 -13 46.75 6.40 -5 -14 13 41.96 6.24 -5 14 -13 48.99 6.02 -5 14 -13 44.41 6.34 5 14 13 46.76 5.26 5 -14 -14 66.71 7.40 -5 -14 14 61.07 7.30 -5 14 -14 48.42 5.89 -5 14 -14 51.47 6.90 5 14 14 60.45 5.93 5 -14 -15 77.60 8.19 -5 -14 15 83.67 8.52 -5 14 -15 88.11 7.86 -5 14 -15 75.41 8.00 5 14 15 87.25 7.08 5 14 16 9.70 2.52 5 -14 -16 14.37 3.51 -5 -14 16 5.61 2.27 -5 14 -16 10.69 3.15 -5 14 -16 9.35 3.18 5 14 17 14.48 2.87 5 -14 -17 12.58 3.58 -5 -14 17 14.26 3.58 -5 14 -17 13.25 3.18 -5 14 -17 8.09 2.22 5 14 18 1.87 1.27 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13 -23 3.69 1.50 6 -13 -24 6.36 1.65 -6 -13 24 7.35 1.68 -6 13 -25 0.09 0.59 6 14 -24 4.70 1.16 -6 -14 -24 2.00 0.97 6 14 -23 13.66 2.25 -6 -14 -23 19.73 2.61 6 14 -22 4.63 1.56 -6 -14 -22 3.94 1.41 6 14 -21 12.24 2.44 -6 -14 -21 10.44 2.43 -6 -14 -20 5.20 1.81 6 14 -20 2.29 1.64 6 -14 20 3.38 1.68 -6 -14 -19 7.77 2.38 6 14 -19 12.60 2.85 6 -14 19 8.47 2.47 6 14 -18 54.12 5.54 -6 -14 -18 48.92 5.23 6 -14 18 48.72 5.55 -6 -14 -17 2.39 1.87 6 14 -17 1.67 1.69 6 -14 17 3.80 2.32 -6 -14 -16 10.74 2.80 6 14 -16 11.25 2.88 6 -14 16 13.10 3.55 -6 -14 -15 32.33 4.80 6 14 -15 39.51 5.02 -6 14 14 31.17 5.05 6 14 -14 21.53 3.53 -6 -14 -14 23.17 4.25 -6 14 13 11.02 2.65 6 14 -13 13.13 2.92 -6 -14 -13 11.27 3.11 6 14 -13 11.02 2.98 -6 14 13 13.67 3.09 -6 14 12 8.95 2.61 -6 -14 -12 8.46 2.92 6 14 -12 17.18 3.70 -6 14 12 10.25 2.68 -6 14 11 47.87 5.55 -6 -14 -11 64.25 6.88 6 14 -11 54.08 6.08 -6 14 11 58.36 6.13 -6 14 10 11.75 2.92 -6 -14 -10 15.26 3.72 6 14 -10 11.52 2.85 -6 14 10 12.85 3.10 -6 14 9 11.11 3.03 -6 -14 -9 12.48 3.46 6 14 -9 14.79 3.42 -6 14 9 12.04 2.80 -6 14 8 59.19 6.58 6 14 -8 72.89 6.92 -6 -14 -8 67.38 7.31 -6 14 8 70.05 6.85 -6 14 7 0.58 1.41 -6 -14 -7 4.18 2.46 6 14 -7 1.28 1.21 -6 14 7 0.68 1.34 -6 14 6 42.19 5.69 -6 -14 -6 36.79 5.67 6 14 -6 44.65 5.39 -6 14 6 38.97 5.40 -6 14 5 53.18 6.43 -6 -14 -5 51.09 6.09 -6 -14 -5 52.96 6.73 6 14 -5 66.65 6.39 -6 14 5 56.11 6.42 -6 14 4 11.51 3.50 -6 -14 -4 17.83 3.85 -6 -14 -4 21.20 4.55 6 14 -4 10.85 2.91 -6 14 4 12.66 3.52 -6 14 3 51.36 6.51 -6 -14 -3 50.83 6.33 -6 -14 -3 53.81 6.81 6 14 -3 55.50 6.19 -6 14 3 52.94 6.48 -6 -14 -2 176.07 11.96 6 -14 2 176.85 11.59 -6 -14 -2 172.41 11.81 6 14 -2 167.74 10.29 -6 14 2 160.86 10.93 -6 -14 -1 9.16 3.15 6 -14 1 6.17 2.68 -6 -14 -1 6.49 2.34 6 14 -1 7.48 2.50 -6 14 1 10.92 3.92 -6 -14 0 24.18 4.82 6 -14 0 20.59 4.47 -6 -14 0 20.95 4.31 6 14 0 17.77 3.53 -6 14 0 17.45 4.01 -6 -14 1 4.36 2.72 6 -14 -1 6.46 2.63 -6 -14 1 4.66 2.79 6 14 1 7.50 2.97 -6 14 -1 6.55 3.12 -6 -14 2 158.43 11.50 -6 -14 2 165.65 11.89 6 -14 -2 174.47 12.21 -6 -14 2 165.63 11.70 6 14 2 163.73 10.35 -6 14 -2 163.68 11.50 -6 -14 3 49.04 6.75 6 -14 -3 51.32 6.82 -6 -14 3 53.36 6.87 -6 -14 3 44.92 6.19 6 14 3 55.13 6.29 -6 14 -3 59.16 6.94 6 -14 -4 14.97 3.85 -6 -14 4 15.29 3.89 -6 -14 4 16.17 3.74 -6 -14 4 12.39 3.31 6 14 4 6.48 2.33 -6 14 -4 12.78 3.58 -6 -14 5 53.62 6.92 6 -14 -5 55.64 7.07 -6 -14 5 59.72 7.36 -6 -14 5 56.92 7.03 -6 14 -5 63.14 7.03 -6 14 -5 59.13 7.02 -6 -14 6 32.38 5.43 6 -14 -6 36.92 5.79 -6 -14 6 35.72 5.49 -6 -14 6 31.21 5.33 -6 14 -6 41.82 5.63 -6 14 -6 37.15 5.86 -6 -14 7 3.47 1.64 6 -14 -7 3.99 2.78 -6 -14 7 3.78 1.89 -6 -14 7 0.94 2.18 -6 14 -7 0.91 1.82 -6 14 -7 3.39 2.20 -6 -14 8 65.84 7.82 6 -14 -8 67.74 7.66 -6 -14 8 70.32 7.58 -6 -14 8 63.94 7.64 -6 14 -8 62.69 6.90 -6 14 -8 69.42 7.78 -6 -14 9 15.12 3.94 6 -14 -9 15.37 4.47 -6 -14 9 12.56 3.69 -6 14 -9 10.87 2.80 -6 14 -9 15.18 4.11 6 -14 -10 12.95 3.52 -6 -14 10 10.86 3.36 -6 14 -10 12.90 3.14 -6 14 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10.85 7 7 -5 114.98 11.77 7 7 -4 56.83 8.37 -7 7 4 52.23 6.87 -7 -7 -4 63.97 8.65 7 7 -4 52.55 7.83 7 7 -3 5.00 3.09 -7 7 3 2.97 1.79 7 7 -3 1.82 1.19 7 7 -2 47.44 7.98 -7 7 2 47.02 6.19 7 7 -2 43.77 6.81 7 7 -1 16.64 4.89 7 7 -1 15.89 3.97 7 7 0 111.70 11.14 7 7 1 14.28 4.41 7 7 2 47.23 7.33 -7 7 -3 3.93 2.86 7 7 3 0.12 1.45 7 7 4 48.92 7.12 -7 7 -4 42.56 7.35 -7 7 -5 103.23 8.19 -7 7 -5 106.27 8.36 -7 7 -5 108.90 11.87 -7 7 -6 454.08 17.32 -7 -7 6 431.58 16.70 -7 7 -6 459.99 17.09 -7 -7 6 477.64 20.51 -7 7 -6 473.58 25.44 -7 -7 7 22.00 4.12 7 -7 -7 45.11 6.06 -7 -7 7 45.95 5.62 -7 7 -7 17.90 5.70 -7 7 -7 28.70 4.62 -7 -7 7 43.90 6.57 7 -7 -8 74.01 7.44 -7 -7 8 71.24 7.01 -7 7 -8 41.80 8.30 -7 7 -8 59.68 6.38 -7 -7 8 72.81 8.46 7 -7 -8 72.21 9.51 7 7 8 65.37 8.98 -7 -7 8 44.52 5.94 -7 -7 9 36.34 5.17 -7 7 -9 38.11 8.12 -7 7 -9 36.04 4.97 7 -7 -9 37.34 5.45 -7 -7 9 39.35 6.45 7 -7 -9 36.14 7.05 -7 7 -9 32.30 4.49 -7 7 -9 32.94 4.47 7 7 9 32.37 6.62 -7 7 -9 33.98 4.94 -7 -7 9 36.79 5.10 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26.52 4.46 7 12 -15 28.36 4.23 -7 12 14 24.16 4.27 7 12 -14 21.70 4.02 -7 -12 -14 24.86 4.35 7 12 -14 24.97 4.01 -7 12 13 18.73 3.61 7 12 -13 24.93 4.42 -7 -12 -13 23.61 4.31 7 12 -13 21.19 3.81 -7 12 13 23.82 3.84 -7 12 12 -0.73 1.95 -7 -12 -12 -0.21 2.02 7 12 -12 -1.01 1.69 -7 12 12 2.03 1.80 -7 12 11 15.39 3.65 7 12 -11 13.34 3.24 -7 12 11 17.37 3.44 -7 12 10 5.69 2.19 -7 -12 -10 8.86 3.61 7 12 -10 11.18 2.78 -7 12 10 6.57 2.23 -7 12 9 147.82 10.55 -7 -12 -9 144.25 10.96 7 12 -9 175.55 10.63 -7 12 9 153.59 9.86 -7 12 8 92.36 8.46 -7 -12 -8 103.22 9.20 7 12 -8 104.11 8.18 -7 12 8 97.90 7.91 -7 12 7 50.18 6.42 -7 -12 -7 53.18 6.98 7 12 -7 52.28 5.82 -7 12 7 45.83 5.47 -7 12 6 138.14 10.61 -7 -12 -6 150.22 11.19 7 12 -6 142.35 9.52 -7 12 6 134.84 9.35 -7 12 5 49.66 6.42 -7 12 5 40.72 5.29 7 12 -5 43.67 5.34 -7 12 4 27.50 4.80 -7 -12 -4 28.57 5.29 -7 12 4 30.24 4.59 7 12 -4 42.40 5.20 -7 12 3 4.97 2.25 -7 -12 -3 13.16 3.23 -7 -12 -3 14.44 3.67 -7 12 3 6.15 2.48 7 12 -3 5.04 2.14 -7 12 3 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39.84 8.42 -8 -4 12 31.37 5.92 -8 4 -12 35.19 4.89 8 4 12 34.85 6.71 -8 -4 13 21.03 4.45 8 -4 -13 19.57 4.29 -8 4 -13 14.97 4.89 -8 4 -13 17.00 3.68 -8 -4 13 20.91 4.68 8 4 13 16.98 4.56 -8 4 -13 15.81 3.41 8 -4 -14 21.44 4.48 -8 4 -14 32.43 8.00 -8 4 -14 24.74 4.54 -8 -4 14 20.42 4.76 -8 4 -14 22.43 4.37 8 4 14 20.80 5.36 -8 -4 15 54.60 6.50 8 -4 -15 43.18 6.42 -8 -4 15 35.95 6.57 8 -4 -15 88.34 12.79 -8 4 -15 57.25 6.50 8 -4 -15 44.77 9.22 8 4 15 49.76 8.18 -8 4 -15 72.28 11.97 8 -4 -16 16.92 4.00 -8 -4 16 12.11 3.22 -8 4 -16 14.61 3.52 -8 -4 16 17.27 4.47 8 -4 -17 5.02 2.50 -8 -4 17 3.35 1.82 -8 4 -17 8.21 2.53 -8 -4 17 4.02 2.61 8 -4 -18 22.34 4.79 -8 -4 18 19.99 4.21 -8 4 -18 20.97 3.75 -8 -4 18 22.11 4.94 -8 -4 19 61.17 7.15 8 -4 -19 54.10 7.28 -8 4 -19 66.88 6.81 -8 -4 19 55.26 7.34 8 -4 -20 19.50 4.46 -8 4 -20 8.24 2.70 -8 -4 20 8.81 3.03 -8 -4 20 13.60 3.78 8 -4 -21 19.14 4.32 -8 -4 21 12.45 3.05 -8 4 -21 11.95 2.89 -8 -4 21 18.09 4.13 8 -4 -22 24.09 4.71 -8 -4 22 19.54 3.87 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16.60 3.67 -8 -5 8 17.94 3.55 -8 5 -8 27.67 4.44 -8 5 -8 26.87 6.62 -8 -5 8 18.71 4.32 8 -5 -8 21.08 5.13 -8 5 -8 23.81 4.08 -8 -5 9 32.39 5.10 8 -5 -9 27.03 4.90 -8 5 -9 27.92 4.47 -8 5 -9 35.12 7.65 -8 -5 9 32.00 6.00 8 -5 -9 30.50 6.52 -8 5 -9 33.30 4.40 -8 5 -9 29.73 4.30 -8 -5 10 13.63 3.29 8 -5 -10 12.45 3.66 -8 5 -10 12.26 4.55 -8 5 -10 11.09 3.12 -8 -5 10 16.04 4.61 8 -5 -10 12.49 4.52 -8 5 -10 12.24 2.78 8 5 10 8.06 3.82 -8 5 -10 10.89 3.03 8 -5 -11 70.74 7.93 -8 5 -11 73.73 7.33 -8 -5 11 75.08 8.78 8 -5 -11 85.25 11.86 -8 5 -11 74.73 6.55 8 5 11 78.91 10.21 -8 5 -11 75.35 6.89 -8 5 -11 66.29 10.84 -8 -5 11 86.46 8.30 8 -5 -12 37.07 6.17 -8 5 -12 70.66 7.42 -8 -5 12 40.81 7.02 8 -5 -12 45.14 8.99 -8 5 -12 73.09 6.55 8 5 12 52.02 8.53 -8 5 -12 60.15 6.54 -8 5 -12 78.72 12.26 -8 -5 12 77.00 8.22 -8 -5 13 27.66 5.08 8 -5 -13 36.65 5.91 -8 5 -13 23.51 7.10 -8 5 -13 27.31 4.66 -8 -5 13 33.79 6.01 8 -5 -13 30.48 7.34 -8 5 -13 20.58 3.45 -8 5 -13 21.61 3.86 8 5 13 28.89 6.00 8 -5 -14 35.35 5.87 -8 5 -14 33.22 5.14 -8 5 -14 44.19 9.44 -8 -5 14 31.94 5.81 8 -5 -14 25.00 6.71 -8 5 -14 40.91 5.01 8 5 14 40.31 7.38 8 -5 -15 69.53 8.04 -8 5 -15 65.43 7.23 -8 -5 15 64.29 8.29 -8 5 -15 67.06 6.49 8 -5 -16 18.64 4.33 -8 -5 16 12.09 3.03 -8 5 -16 9.59 2.72 -8 -5 16 14.10 4.28 -8 5 -16 11.68 2.98 -8 -5 17 79.31 7.88 8 -5 -17 79.24 8.71 -8 5 -17 79.61 7.75 -8 -5 17 68.86 8.79 -8 5 -17 76.57 6.92 -8 -5 18 36.36 5.49 8 -5 -18 25.11 5.56 -8 5 -18 39.75 5.53 -8 -5 18 23.76 5.22 -8 5 -18 38.38 4.93 8 -5 -19 16.47 4.03 -8 -5 19 9.74 2.94 -8 5 -19 10.64 2.99 -8 -5 19 16.91 4.22 -8 5 -19 7.93 2.49 8 -5 -20 30.77 5.34 -8 -5 20 31.83 4.84 -8 5 -20 33.53 4.88 -8 -5 20 25.66 5.04 8 -5 -21 12.47 3.73 -8 5 -21 3.35 1.94 -8 -5 21 7.99 2.71 -8 -5 21 7.93 2.74 8 -5 -22 8.14 3.60 -8 -5 22 7.34 2.17 -8 5 -22 5.49 1.89 -8 -5 22 1.08 1.92 -8 -5 23 10.31 3.27 8 -5 -23 10.24 3.35 -8 -5 23 8.08 2.56 -8 5 -23 11.94 2.88 -8 -5 23 4.91 2.25 -8 -5 24 2.22 2.07 8 -5 -24 0.77 2.06 -8 -5 24 2.86 1.76 -8 -5 25 1.75 1.33 8 -5 -25 2.36 1.92 -8 -5 26 2.66 1.30 8 -5 -26 4.63 2.22 -8 -5 26 4.57 1.62 -8 -5 27 18.92 3.19 -8 -5 27 21.94 3.15 8 -5 -27 19.35 3.18 -8 -5 28 5.54 1.75 -8 -5 28 6.93 1.72 8 -5 -28 5.44 1.55 -8 -5 29 23.16 2.68 -8 -5 29 27.16 3.03 -8 6 29 4.14 1.29 -8 6 28 5.29 1.56 8 6 -28 4.72 1.46 -8 6 27 48.94 4.64 -8 6 26 1.21 1.28 -8 -6 -26 2.58 1.31 -8 6 25 12.90 2.82 -8 -6 -25 11.34 2.36 -8 -6 -24 3.07 1.68 -8 6 24 3.75 1.55 -8 6 23 0.36 1.65 8 6 -23 0.34 1.58 -8 -6 -23 1.62 1.33 -8 6 22 11.35 2.87 8 6 -22 12.27 3.44 -8 -6 -22 12.21 2.88 -8 6 21 6.00 2.75 8 6 -21 6.08 2.92 -8 -6 -21 4.75 2.11 -8 6 20 16.52 3.76 8 6 -20 13.72 3.78 -8 -6 -20 10.09 2.98 -8 6 19 52.91 6.64 8 6 -19 58.45 7.09 -8 -6 -19 57.72 6.37 -8 6 18 41.25 5.94 8 6 -18 40.42 6.43 -8 -6 -18 45.77 5.77 -8 6 17 47.90 6.60 8 6 -17 50.75 6.75 -8 -6 -17 55.17 6.23 -8 6 16 21.53 4.51 8 6 -16 26.38 4.82 -8 -6 -16 23.93 4.23 -8 6 15 21.50 4.70 8 6 -15 15.63 4.27 -8 -6 -15 13.80 3.33 -8 6 14 8.31 2.73 8 6 -14 5.06 2.85 -8 -6 -14 6.65 2.65 -8 6 13 158.07 11.72 8 6 -13 146.41 11.13 -8 -6 -13 145.56 9.87 -8 6 13 156.28 15.24 8 6 -13 150.84 16.48 -8 -6 -13 171.67 9.95 8 6 -13 180.64 17.56 -8 6 12 115.56 9.79 8 6 -12 141.58 10.74 -8 -6 -12 122.92 9.02 -8 6 12 99.17 11.88 8 6 -12 94.34 12.74 -8 -6 -12 115.63 8.21 8 6 -12 118.32 13.99 -8 6 11 80.55 8.24 -8 -6 -11 71.81 6.80 -8 6 11 85.28 10.81 8 6 -11 79.29 11.30 -8 -6 -11 87.10 7.08 8 6 -11 87.58 11.68 -8 6 10 89.16 8.42 -8 -6 -10 81.00 7.19 -8 6 10 99.85 11.32 8 6 -10 89.53 11.81 -8 -6 -10 94.55 7.43 8 6 -10 109.31 12.85 8 6 -9 38.82 7.69 -8 6 9 17.20 3.79 -8 -6 -9 13.90 3.14 -8 6 9 34.60 6.62 -8 -6 -9 26.60 4.11 8 6 -9 33.52 7.17 -8 6 8 57.37 6.56 -8 -6 -8 64.47 6.44 -8 6 8 47.18 7.38 8 6 -8 44.28 7.97 -8 -6 -8 49.26 5.45 8 6 -8 54.43 9.21 -8 6 7 56.84 6.59 -8 -6 -7 58.53 6.18 -8 6 7 49.52 7.43 8 6 -7 49.35 8.24 -8 -6 -7 54.10 5.81 8 6 -7 56.22 9.41 8 6 -6 26.16 6.24 -8 6 6 15.38 3.47 -8 -6 -6 10.17 2.94 -8 6 6 23.90 4.98 8 6 -6 17.00 4.61 -8 -6 -6 18.57 3.63 8 6 -5 12.85 4.67 -8 6 5 20.99 4.10 8 6 -5 14.79 4.68 -8 -6 -5 14.71 2.94 -8 6 4 44.72 5.64 -8 -6 -4 36.76 4.75 8 6 -4 47.17 7.28 -8 -6 -4 41.38 4.99 8 6 -4 49.57 8.03 -8 6 3 17.07 3.57 -8 -6 -3 12.87 2.83 -8 -6 -3 17.69 3.39 -8 6 2 42.20 5.54 -8 6 2 42.54 5.23 -8 -6 -2 44.36 5.06 8 6 -2 47.74 7.96 -8 6 1 50.40 5.85 -8 6 1 49.54 5.69 -8 -6 -1 48.67 5.58 8 6 -1 55.85 8.45 8 6 0 79.60 9.74 -8 6 0 66.82 6.66 -8 6 0 66.95 6.65 -8 -6 0 75.71 6.93 8 6 1 62.31 8.52 -8 6 -1 45.76 5.62 -8 -6 1 37.50 5.65 -8 6 -1 47.38 5.64 -8 -6 1 53.57 5.90 -8 6 -2 41.47 5.36 8 6 2 51.27 7.71 -8 -6 2 39.57 4.95 -8 6 -2 44.51 5.48 -8 -6 2 42.30 5.90 -8 -6 2 44.32 5.45 -8 -6 3 23.15 4.14 -8 6 -3 18.56 3.67 8 6 3 19.62 4.58 -8 -6 3 17.58 3.43 -8 6 -3 25.75 5.63 -8 -6 3 15.93 4.31 -8 6 -3 17.17 3.29 -8 6 -4 39.14 5.00 -8 -6 4 38.20 5.87 8 6 4 42.68 6.72 -8 -6 4 35.23 4.71 -8 6 -4 35.98 4.84 -8 6 -4 36.43 6.80 -8 -6 4 44.79 5.73 -8 -6 5 16.43 3.70 -8 6 -5 19.82 3.67 8 -6 -5 32.08 4.66 -8 -6 5 31.49 4.67 -8 6 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8.98 -8 -6 12 133.47 12.26 8 -6 -12 115.94 14.09 -8 6 -12 105.81 8.10 8 6 12 113.32 12.50 -8 6 -12 114.65 9.31 -8 6 -12 98.60 13.77 -8 -6 12 102.89 9.42 8 -6 -13 147.40 11.59 -8 6 -13 157.93 10.70 -8 -6 13 149.64 12.68 8 -6 -13 123.48 14.79 -8 6 -13 145.65 9.49 8 6 13 152.29 14.82 -8 6 -13 132.83 10.19 -8 6 -13 148.09 17.41 -8 -6 13 158.41 11.50 -8 -6 14 10.32 3.26 8 -6 -14 6.68 2.94 -8 6 -14 9.82 3.22 -8 -6 14 2.97 2.13 -8 6 -14 10.36 2.85 -8 6 -14 4.72 2.39 8 -6 -15 16.48 4.00 -8 6 -15 23.68 4.28 -8 -6 15 13.88 4.38 -8 6 -15 25.24 4.27 8 -6 -16 20.89 4.64 -8 6 -16 23.85 4.24 -8 -6 16 17.44 4.34 -8 6 -16 28.76 4.37 -8 6 -17 44.73 5.73 8 -6 -17 50.78 6.90 -8 -6 17 49.27 7.24 -8 6 -17 32.88 4.59 8 -6 -18 39.58 6.04 -8 6 -18 46.04 5.71 -8 -6 18 37.66 6.05 -8 6 -18 44.49 5.41 -8 -6 19 54.79 6.08 8 -6 -19 63.00 7.59 -8 6 -19 57.08 6.08 -8 -6 19 52.89 7.22 -8 6 -19 48.19 5.40 8 -6 -20 10.27 3.45 -8 -6 20 12.94 3.20 -8 6 -20 14.10 2.99 -8 -6 20 11.51 3.71 -8 6 -20 17.13 3.28 8 -6 -21 8.89 3.08 -8 -6 21 6.30 2.25 -8 6 -21 4.28 1.90 -8 -6 21 2.42 2.23 -8 6 -21 8.81 2.45 -8 -6 22 12.51 3.72 8 -6 -22 13.85 3.50 -8 -6 22 13.76 2.92 -8 6 -22 12.52 2.73 -8 -6 22 9.68 2.85 -8 6 -22 14.93 2.81 -8 -6 23 2.92 2.21 8 -6 -23 2.66 2.37 -8 -6 23 3.20 1.68 -8 6 -23 3.75 2.21 -8 -6 23 1.11 1.18 -8 6 -23 4.97 1.80 -8 -6 24 3.41 1.77 8 -6 -24 2.17 1.36 -8 -6 24 2.50 1.67 -8 6 -24 3.33 1.29 -8 -6 25 11.08 2.73 8 -6 -25 12.73 2.80 -8 -6 26 4.38 2.03 8 -6 -26 0.89 1.55 -8 -6 26 3.81 1.65 -8 -6 27 49.55 4.30 8 -6 -27 36.70 4.06 -8 -6 27 50.29 4.67 -8 -6 28 5.70 1.67 8 -6 -28 4.62 1.47 -8 -6 28 5.42 1.34 -8 -6 29 4.13 1.42 -8 7 28 11.06 1.94 -8 7 27 1.67 1.32 -8 -7 -27 1.01 1.07 -8 7 26 15.48 2.86 -8 -7 -26 14.96 2.44 -8 7 25 6.93 2.15 -8 -7 -25 6.54 2.03 -8 7 24 2.60 1.77 8 7 -24 2.50 1.54 -8 -7 -24 4.41 1.73 -8 7 23 -0.99 1.56 8 7 -23 1.13 1.13 8 7 -23 1.54 1.64 -8 -7 -23 1.39 1.23 -8 7 22 7.08 2.55 8 7 -22 8.75 2.81 8 7 -22 6.01 2.20 -8 -7 -22 7.04 2.22 8 7 -21 30.77 5.44 -8 7 21 28.18 4.58 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211.35 18.20 -8 7 9 206.92 12.80 -8 -7 -9 196.29 11.53 -8 7 9 189.94 15.35 8 7 -9 182.52 17.01 -8 7 8 66.70 7.23 -8 -7 -8 63.85 6.56 -8 7 8 86.46 10.13 8 7 -8 69.47 10.32 -8 -7 -8 79.20 6.79 8 7 -7 174.76 16.52 -8 7 7 169.60 11.52 -8 -7 -7 158.54 10.21 -8 7 7 158.98 13.31 8 7 -7 154.55 14.98 -8 -7 -7 162.70 9.69 -8 7 6 30.30 4.90 8 7 -6 21.39 6.09 -8 -7 -6 37.40 4.88 -8 -7 -6 26.82 4.09 8 7 -6 19.95 5.58 8 7 -5 325.88 21.54 -8 7 5 306.15 14.99 -8 -7 -5 282.37 13.53 8 7 -5 287.89 19.40 -8 -7 -5 272.96 12.67 8 7 -4 199.85 17.21 -8 7 4 210.93 12.43 -8 -7 -4 183.08 10.93 -8 -7 -4 185.07 10.54 8 7 -3 70.99 9.87 -8 7 3 74.63 7.37 -8 -7 -3 79.39 7.22 -8 -7 -3 61.68 5.99 8 7 -2 97.84 11.49 -8 7 2 76.27 7.72 -8 -7 -2 67.32 6.65 -8 7 2 79.01 7.46 -8 -7 -2 81.30 6.95 -8 7 1 128.72 9.53 8 7 -1 127.92 12.86 -8 -7 -1 118.97 8.83 -8 -7 -1 120.45 9.62 -8 7 1 112.83 8.79 -8 -7 -1 114.18 8.33 -8 -7 0 27.15 4.06 -8 7 0 36.75 5.19 8 7 0 29.37 6.19 -8 -7 0 36.85 4.85 -8 -7 0 39.25 5.75 -8 7 0 25.21 4.03 -8 7 -1 118.41 9.10 8 7 1 115.70 11.96 -8 -7 1 122.06 8.85 -8 7 -1 119.40 8.97 -8 -7 1 118.45 9.87 -8 -7 1 115.85 8.65 -8 7 -2 86.42 7.86 -8 -7 2 71.10 7.01 -8 7 -2 77.26 7.47 8 7 2 84.40 10.40 -8 -7 2 85.41 7.64 -8 -7 2 74.23 8.04 -8 7 -3 65.74 6.96 8 7 3 68.48 8.90 -8 -7 3 84.32 7.51 -8 7 -3 63.39 6.77 -8 -7 3 88.97 8.92 -8 -7 3 68.07 6.66 -8 7 -4 194.43 11.86 8 -7 -4 179.39 11.19 8 7 4 205.10 15.04 -8 -7 4 182.92 11.03 -8 7 -4 176.59 11.11 -8 -7 4 198.98 13.50 -8 -7 4 193.58 11.64 -8 7 -5 284.72 14.43 8 -7 -5 280.49 14.09 -8 -7 5 280.22 13.71 -8 7 -5 274.93 13.81 -8 -7 5 312.03 17.30 -8 -7 5 289.85 14.47 -8 7 -5 275.26 19.68 -8 -7 6 24.18 4.26 -8 7 -6 27.67 4.54 8 -7 -6 39.58 5.47 -8 -7 6 37.23 5.09 -8 7 -6 16.69 4.94 -8 -7 6 44.11 6.82 -8 7 -6 24.92 4.33 -8 -7 7 164.12 10.69 -8 7 -7 164.89 10.78 -8 -7 7 184.52 13.68 -8 -7 7 165.73 11.18 -8 7 -7 159.20 15.76 8 -7 -7 162.02 11.13 8 -7 -8 55.39 6.84 -8 -7 8 62.46 6.85 -8 7 -8 66.99 6.99 -8 -7 8 73.34 9.01 -8 7 -8 71.54 6.67 8 7 8 64.84 9.53 -8 7 -8 66.41 6.52 -8 7 -8 78.15 11.55 -8 -7 8 72.40 7.64 8 -7 -9 210.24 12.83 -8 -7 9 193.39 11.80 -8 7 -9 190.33 11.51 -8 -7 9 216.06 15.23 -8 7 -9 177.21 10.51 8 7 9 186.06 16.15 -8 7 -9 189.21 10.51 -8 7 -9 184.51 18.03 -8 -7 9 185.69 12.07 -8 -7 10 34.18 5.42 8 -7 -10 23.58 4.77 -8 7 -10 35.01 5.28 -8 7 -10 39.63 9.03 -8 -7 10 25.51 5.59 -8 7 -10 30.63 4.49 -8 7 -10 41.69 5.15 8 7 10 25.35 6.09 8 -7 -11 58.24 7.26 -8 7 -11 51.08 6.18 -8 7 -11 47.63 9.64 -8 -7 11 57.79 8.25 -8 7 -11 48.46 5.58 8 7 11 51.19 8.58 -8 7 -11 48.56 6.16 -8 -7 11 52.10 6.55 -8 -7 12 11.58 3.14 8 -7 -12 7.01 3.22 -8 7 -12 15.11 5.64 -8 7 -12 10.33 2.80 -8 -7 12 9.96 3.65 -8 7 -12 11.52 2.72 8 7 12 9.76 4.37 -8 7 -12 6.70 2.52 8 -7 -13 108.68 9.78 -8 7 -13 98.32 8.58 -8 -7 13 108.63 11.12 -8 7 -13 85.74 7.39 -8 7 -13 80.66 8.17 -8 -7 13 87.30 8.49 -8 -7 14 21.37 4.36 8 -7 -14 13.29 3.85 -8 7 -14 20.51 4.27 -8 -7 14 10.09 3.69 -8 7 -14 21.13 3.81 -8 7 -14 10.99 3.14 8 -7 -15 87.60 9.06 -8 7 -15 78.62 7.76 -8 -7 15 70.40 8.76 -8 7 -15 66.35 6.67 -8 7 -15 70.41 7.71 -8 -7 15 68.24 7.69 8 -7 -16 103.91 9.76 -8 7 -16 134.76 9.99 -8 -7 16 104.81 10.74 -8 7 -16 138.63 9.43 -8 -7 16 137.19 10.81 -8 -7 17 -0.84 1.85 8 -7 -17 6.63 2.61 -8 7 -17 2.16 2.00 -8 -7 17 3.26 2.88 -8 7 -17 0.66 1.27 8 -7 -18 40.37 6.27 -8 7 -18 37.98 5.21 -8 -7 18 37.20 6.28 -8 7 -18 37.84 4.89 -8 -7 18 38.29 5.83 -8 -7 19 29.23 5.21 8 -7 -19 30.94 5.33 -8 7 -19 30.84 4.89 -8 -7 19 27.85 5.26 -8 7 -19 24.12 3.99 -8 -7 20 5.51 2.73 8 -7 -20 4.41 2.29 -8 7 -20 5.83 2.41 -8 -7 20 5.97 2.58 -8 7 -20 3.36 1.83 -8 -7 21 34.17 5.17 8 -7 -21 20.46 4.13 -8 7 -21 30.53 4.34 -8 -7 21 20.36 4.32 -8 7 -21 29.78 4.09 -8 -7 22 8.26 2.57 8 -7 -22 8.13 3.00 -8 -7 22 6.27 2.03 -8 7 -22 4.09 1.77 -8 -7 22 5.71 2.13 -8 7 -22 6.99 2.05 -8 -7 23 0.73 1.57 8 -7 -23 2.13 1.70 -8 -7 23 2.21 1.50 -8 7 -23 1.82 1.86 -8 -7 23 -1.44 1.77 -8 7 -23 2.08 1.38 -8 -7 24 1.62 1.76 8 -7 -24 3.73 1.82 -8 -7 24 2.68 1.29 -8 -7 24 0.88 1.37 -8 7 -24 3.01 1.44 -8 -7 25 5.70 1.90 8 -7 -25 5.65 1.98 -8 -7 25 6.88 1.69 -8 7 -25 6.57 1.66 -8 -7 26 15.12 2.57 8 -7 -26 20.18 3.24 -8 -7 26 15.01 2.38 -8 -7 27 0.23 1.03 8 -7 -27 2.78 1.21 -8 -7 27 0.15 0.65 -8 -7 28 11.72 2.06 8 -7 -28 7.46 1.61 -8 8 27 12.21 2.01 -8 -8 -27 8.96 1.62 -8 8 26 26.61 3.24 -8 -8 -26 22.29 2.83 -8 8 25 1.24 1.22 8 8 -25 -0.50 1.00 -8 -8 -25 0.87 1.03 -8 8 24 0.19 1.12 8 8 -24 1.68 1.34 -8 -8 -24 0.01 1.22 -8 8 23 28.67 4.11 8 8 -23 26.55 3.56 8 8 -23 34.18 4.61 -8 -8 -23 30.42 4.07 -8 8 22 31.37 4.50 8 8 -22 30.73 3.94 8 8 -22 25.65 4.30 -8 -8 -22 25.43 3.90 -8 8 21 37.89 5.08 8 8 -21 43.32 5.02 8 8 -21 37.04 5.20 -8 -8 -21 40.13 4.88 -8 8 20 31.50 5.02 8 8 -20 27.16 4.20 8 8 -20 37.67 5.53 -8 -8 -20 34.36 4.75 -8 8 19 38.70 5.69 8 8 -19 41.59 5.21 8 8 -19 34.17 5.37 -8 -8 -19 33.63 4.74 -8 8 18 3.99 2.47 8 8 -18 6.07 2.45 8 8 -18 5.05 2.06 -8 -8 -18 4.80 2.07 -8 8 17 5.95 2.56 8 8 -17 7.31 3.07 8 8 -17 11.99 2.79 -8 -8 -17 5.10 2.01 -8 8 16 6.03 2.28 8 8 -16 15.50 3.78 -8 -8 -16 14.03 2.94 8 8 -16 5.98 2.12 -8 8 15 4.88 2.06 8 8 -15 8.25 3.10 -8 -8 -15 4.75 2.21 8 8 -15 6.07 2.07 -8 8 14 16.82 4.13 8 8 -14 24.17 4.71 -8 -8 -14 21.44 4.12 8 8 -14 15.83 3.25 -8 8 13 82.19 8.37 8 8 -13 79.14 8.14 8 8 -13 73.64 6.74 -8 -8 -13 83.25 7.80 -8 8 12 40.59 5.97 8 8 -12 31.31 4.49 -8 -8 -12 43.78 5.67 -8 8 11 59.33 7.21 -8 -8 -11 42.47 5.72 -8 8 10 81.43 8.12 8 8 -10 79.98 11.88 -8 -8 -10 87.42 7.88 8 8 -10 78.38 6.73 -8 8 10 84.38 10.66 8 8 -10 71.77 11.22 -8 8 9 44.00 6.14 8 8 -9 48.57 8.99 -8 8 9 46.73 7.97 -8 -8 -9 37.73 5.26 8 8 -9 51.73 5.45 8 8 -9 46.27 8.70 -8 8 8 91.40 8.64 8 8 -8 104.33 13.13 -8 -8 -8 101.00 8.48 -8 8 8 100.99 11.08 8 8 -8 108.22 7.64 8 8 -8 99.47 12.49 -8 8 7 9.41 3.23 8 8 -7 23.49 6.32 -8 8 7 34.55 8.52 -8 -8 -7 6.31 2.72 8 8 -7 23.07 3.60 8 8 -7 21.50 6.12 -8 8 6 40.19 5.84 -8 -8 -6 40.94 5.37 8 8 -6 30.88 6.88 8 8 -6 30.90 4.04 8 8 -6 22.75 5.99 -8 8 5 107.46 9.27 8 8 -5 112.39 13.22 -8 -8 -5 115.51 8.99 8 8 -5 107.42 7.26 8 8 -5 97.55 11.62 -8 8 4 62.91 7.04 8 8 -4 92.25 11.91 -8 -8 -4 43.04 5.70 -8 8 4 70.03 7.36 8 8 -4 87.51 6.53 -8 8 3 20.41 4.22 -8 -8 -3 24.24 4.08 8 8 -3 9.33 3.97 -8 8 3 16.14 3.57 8 8 -3 13.43 2.43 -8 -8 -3 11.86 2.81 -8 8 2 8.97 2.89 -8 -8 -2 7.97 2.72 -8 8 2 9.40 2.83 8 8 -2 12.15 2.39 -8 -8 -2 9.62 2.26 -8 8 1 164.63 11.18 -8 -8 -1 149.49 10.22 -8 -8 -1 149.79 10.91 -8 8 1 147.14 10.35 8 8 -1 165.80 15.45 8 8 -1 163.41 8.92 -8 -8 -1 150.13 9.59 -8 8 0 68.12 7.30 8 8 0 90.30 11.04 -8 -8 0 48.73 6.01 -8 8 0 77.02 7.67 -8 -8 0 54.25 6.81 8 8 0 87.81 6.57 -8 -8 0 78.67 7.13 -8 8 -1 156.29 11.18 8 8 1 175.28 15.25 -8 -8 1 144.77 9.99 -8 8 -1 148.10 10.29 -8 -8 1 147.74 11.14 8 8 1 147.60 8.58 -8 -8 1 142.89 9.66 -8 -8 2 13.55 3.20 -8 8 -2 8.78 3.17 -8 -8 2 4.26 2.16 -8 8 -2 9.30 2.76 -8 -8 2 8.76 3.24 -8 -8 3 18.01 3.65 -8 8 -3 24.06 4.33 8 -8 -3 31.11 4.70 -8 -8 3 25.68 4.35 -8 8 -3 17.02 3.47 -8 -8 3 24.35 4.53 8 8 3 14.52 4.36 -8 8 -4 54.19 6.66 8 -8 -4 35.16 5.16 -8 -8 4 39.08 5.60 -8 8 -4 57.15 6.62 -8 -8 4 39.80 6.56 -8 8 -5 105.61 9.14 8 -8 -5 122.00 9.38 -8 -8 5 120.40 9.27 -8 8 -5 112.51 9.03 -8 -8 5 128.35 11.47 -8 -8 5 103.42 8.60 8 -8 -6 38.60 5.52 -8 -8 6 45.43 5.88 -8 8 -6 36.82 5.14 -8 -8 6 51.61 7.22 8 8 6 41.27 7.68 -8 -8 6 34.97 5.11 -8 -8 7 17.92 3.90 8 -8 -7 2.70 2.31 -8 -8 7 5.75 2.81 -8 8 -7 18.50 6.20 -8 8 -7 14.66 3.57 -8 -8 7 6.49 3.39 8 8 7 6.26 3.37 8 -8 -8 92.41 8.59 -8 -8 8 91.39 8.38 -8 8 -8 92.69 8.33 -8 -8 8 97.71 10.44 -8 8 -8 94.34 7.95 8 8 8 86.55 11.24 -8 8 -8 100.04 13.24 -8 -8 8 96.02 8.61 8 -8 -9 37.32 5.79 -8 -8 9 33.02 5.16 -8 8 -9 39.15 5.51 -8 8 -9 41.89 8.95 -8 -8 9 34.95 6.64 -8 8 -9 34.34 4.80 8 8 9 36.10 7.59 -8 -8 9 43.46 5.72 8 -8 -10 86.77 8.68 -8 8 -10 81.36 7.86 -8 -8 10 89.74 10.08 -8 8 -10 76.64 7.10 8 8 10 76.36 10.39 -8 8 -10 83.78 8.22 -8 8 -10 76.98 12.16 -8 -8 10 75.65 7.82 8 -8 -11 36.34 6.06 -8 8 -11 60.29 6.83 -8 -8 11 41.78 7.10 -8 8 -11 64.50 6.71 -8 8 -11 45.95 6.35 -8 -8 11 70.38 7.77 -8 -8 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2.52 -8 -14 1 6.70 2.85 8 14 1 10.78 2.82 -8 14 -1 7.29 2.26 8 -14 -2 15.87 3.59 -8 -14 2 14.18 3.20 8 14 2 13.93 2.95 -8 14 -2 15.73 3.37 8 -14 -3 37.13 5.17 -8 -14 3 40.60 5.47 -8 -14 3 37.04 5.37 8 14 3 39.77 4.93 -8 14 -3 42.93 5.34 8 -14 -4 9.63 2.97 -8 -14 4 11.01 3.35 -8 -14 4 7.04 2.55 8 14 4 8.90 2.73 -8 14 -4 10.66 3.29 -8 14 -4 11.29 3.28 8 -14 -5 24.59 4.11 -8 -14 5 28.38 4.72 -8 14 -5 26.22 3.88 -8 -14 5 22.90 4.29 8 14 5 29.32 4.28 -8 14 -5 26.60 4.75 -8 14 -5 24.26 4.02 8 -14 -6 42.86 5.56 -8 -14 6 55.76 6.59 -8 14 -6 55.88 5.30 -8 -14 6 47.52 6.17 8 14 6 63.69 6.09 -8 14 -6 61.26 6.55 -8 14 -6 53.42 6.01 8 -14 -7 6.31 2.32 -8 14 -7 5.02 1.68 -8 -14 7 9.77 2.99 8 14 7 5.92 2.44 -8 14 -7 7.91 3.01 -8 14 -7 7.01 2.50 8 -14 -8 12.91 3.26 -8 14 -8 11.28 2.33 -8 -14 8 6.59 2.87 8 14 8 17.96 3.12 -8 14 -8 15.12 3.57 -8 14 -8 12.35 3.11 8 -14 -9 6.51 2.71 -8 14 -9 6.03 1.82 -8 -14 9 7.25 2.70 8 14 9 8.25 2.21 -8 14 -9 8.14 2.57 -8 14 -9 7.56 2.49 8 -14 -10 18.74 3.83 -8 14 -10 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6.96 -10 -4 1 79.25 7.83 10 4 1 86.95 10.48 -10 4 -2 89.90 7.90 -10 4 -2 93.84 8.35 -10 -4 2 87.13 8.86 -10 4 -2 91.23 7.67 -10 -4 2 92.99 8.34 -10 4 -3 101.35 8.20 -10 4 -3 90.41 8.12 -10 4 -3 94.16 7.79 -10 -4 3 89.51 8.36 -10 -4 4 3.45 2.14 -10 4 -4 7.96 2.48 -10 4 -4 3.61 1.65 -10 4 -4 5.04 2.18 -10 4 -5 62.97 7.01 -10 -4 5 46.67 6.92 -10 4 -5 72.73 7.20 -10 -4 5 72.59 7.99 10 -4 -6 33.91 5.14 -10 4 -6 39.04 5.52 -10 -4 6 34.87 6.42 -10 4 -6 45.79 5.78 -10 -4 6 49.12 6.61 10 -4 -7 46.78 6.05 -10 4 -7 39.33 5.23 -10 -4 7 45.51 7.09 -10 4 -7 39.64 5.03 -10 -4 7 47.17 6.17 -10 -4 8 1.12 2.07 10 -4 -8 1.78 1.40 -10 4 -8 -0.10 1.52 -10 -4 8 0.67 1.90 -10 4 -8 1.23 1.25 -10 -4 9 8.45 3.38 10 -4 -9 3.19 2.55 -10 4 -9 2.17 2.00 -10 -4 9 3.05 2.48 -10 4 -9 6.36 2.73 10 -4 -10 102.99 9.48 -10 4 -10 90.41 7.99 -10 -4 10 95.60 10.27 -10 4 -10 89.65 7.79 -10 -4 10 94.22 9.08 10 -4 -11 66.36 7.81 -10 4 -11 75.64 7.46 -10 -4 11 75.06 9.14 -10 4 -11 69.01 7.37 -10 -4 11 78.72 8.60 10 -4 -12 39.53 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5.75 2.30 -10 -4 23 2.83 2.02 -10 -4 23 2.34 1.06 10 -4 -23 4.14 2.18 -10 -4 24 33.64 3.42 10 -4 -24 35.58 4.47 -10 -4 24 32.59 3.74 -10 -4 25 3.60 1.61 -10 -4 25 3.98 1.41 10 -4 -25 6.18 1.90 10 -4 -26 32.77 3.51 -10 -4 26 25.32 2.78 10 -4 -27 13.99 2.11 -10 5 26 5.43 1.58 10 5 -26 6.22 1.66 -10 5 25 13.19 2.42 10 5 -25 14.27 2.68 -10 5 24 25.51 3.48 -10 5 23 41.20 4.76 -10 5 22 14.13 3.15 -10 5 21 1.28 1.65 10 5 -21 -0.01 1.88 -10 5 20 17.47 3.76 10 5 -20 8.61 2.83 -10 5 19 10.17 2.95 10 5 -19 12.37 3.35 -10 5 18 36.80 5.42 10 5 -18 23.50 4.76 -10 5 17 2.88 2.07 10 5 -17 4.46 2.45 -10 5 16 14.31 3.61 10 5 -16 6.34 2.47 -10 -5 -16 10.72 3.00 -10 5 15 44.30 5.98 -10 -5 -15 54.72 5.71 -10 5 14 3.53 1.99 10 5 -14 1.81 2.05 -10 -5 -14 3.41 1.87 -10 5 13 14.36 3.63 10 5 -13 12.99 3.50 -10 -5 -13 16.51 3.40 -10 5 12 11.70 3.24 10 5 -12 10.11 3.08 -10 -5 -12 18.31 3.63 -10 5 11 30.56 4.96 10 5 -11 22.08 4.73 -10 5 10 32.40 5.07 10 5 -10 38.94 5.69 -10 -5 -10 34.33 4.83 -10 5 9 10.75 3.02 10 5 -9 6.77 2.54 -10 -5 -9 11.05 2.79 -10 5 8 37.54 5.59 10 5 -8 30.96 5.13 -10 -5 -8 41.82 5.16 -10 5 7 79.93 7.84 -10 -5 -7 75.67 7.00 -10 5 6 44.98 6.20 -10 -5 -6 41.20 5.63 -10 5 5 151.14 10.71 -10 5 5 153.13 10.67 -10 -5 -5 157.03 10.42 -10 5 4 168.36 11.29 -10 5 4 152.96 10.86 -10 -5 -4 161.67 10.75 10 5 -4 155.21 15.92 -10 5 3 124.43 9.66 -10 -5 -3 122.50 10.06 -10 5 3 125.59 9.81 -10 -5 -3 123.68 9.62 10 5 -3 148.87 14.97 -10 5 2 164.02 10.89 -10 -5 -2 149.80 11.35 -10 5 2 150.35 10.66 -10 -5 -2 153.66 10.49 10 5 -2 167.49 15.66 -10 5 1 70.64 7.85 -10 -5 -1 65.10 7.82 -10 5 1 50.26 6.08 -10 5 1 64.52 6.25 -10 -5 -1 67.25 7.25 10 5 -1 57.89 9.03 -10 5 0 23.93 4.36 10 5 0 16.63 4.84 -10 -5 0 22.34 4.70 -10 5 0 15.91 3.06 -10 5 0 18.61 3.37 -10 -5 0 19.16 3.69 10 5 1 58.76 8.76 -10 5 -1 59.15 6.73 -10 5 -1 49.92 5.99 -10 -5 1 60.02 7.40 -10 5 -1 60.34 6.07 -10 -5 1 62.44 6.76 -10 5 -2 149.05 10.39 -10 5 -2 140.41 10.26 -10 -5 2 149.74 11.68 -10 5 -2 150.33 9.48 -10 -5 2 155.32 11.04 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6.89 1.93 -11 -7 -13 9.05 2.22 -11 7 12 15.24 3.37 11 7 -12 22.51 4.36 -11 7 12 17.18 3.42 -11 -7 -12 19.37 3.25 -11 7 11 7.80 3.07 11 7 -11 3.35 2.11 -11 7 11 3.26 1.74 -11 -7 -11 4.84 2.20 -11 7 10 29.03 4.65 11 7 -10 28.03 4.65 -11 7 10 32.55 4.89 -11 -7 -10 34.59 4.38 -11 7 9 9.40 2.74 11 7 -9 18.04 3.94 -11 7 9 10.96 2.89 -11 -7 -9 9.19 2.73 -11 7 8 17.81 3.73 11 7 -8 23.10 4.27 -11 7 8 23.03 4.54 -11 -7 -8 20.24 3.65 -11 7 7 75.48 7.60 11 7 -7 63.51 7.04 -11 7 7 86.95 7.97 -11 -7 -7 85.77 7.28 -11 7 6 39.67 5.59 -11 7 6 34.54 5.47 -11 -7 -6 30.51 4.58 -11 7 5 88.42 8.36 -11 7 5 98.20 8.71 -11 -7 -5 94.86 7.91 -11 7 4 96.51 8.45 -11 7 4 89.45 8.36 -11 -7 -4 80.45 7.35 -11 7 3 40.73 5.78 -11 7 3 40.28 6.13 -11 -7 -3 37.70 5.39 -11 7 2 44.97 6.01 -11 7 2 47.82 6.42 -11 -7 -2 45.89 5.91 -11 7 1 45.68 5.92 -11 -7 -1 56.05 6.90 -11 7 1 35.09 5.49 -11 -7 -1 41.70 5.58 -11 7 0 9.58 3.00 -11 -7 0 7.90 3.30 -11 7 0 11.53 3.33 -11 -7 0 11.40 3.15 -11 7 -1 36.14 5.43 -11 -7 1 48.27 6.67 -11 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-15 -2 5 29.75 3.19 -15 -2 6 5.65 1.59 -15 -2 7 2.56 1.16 -15 -2 8 0.02 0.71 -15 -2 9 0.94 0.78 -15 -3 -8 6.26 1.56 -15 -3 -7 8.10 1.77 -15 -3 -6 3.09 1.17 -15 -3 -5 8.61 1.89 -15 -3 -4 5.19 1.48 -15 -3 -3 8.17 1.82 -15 -3 -2 6.50 1.80 -15 3 1 4.85 1.29 -15 -3 -1 2.66 1.39 -15 3 0 1.24 0.65 -15 -3 0 1.75 1.07 -15 3 -1 3.90 1.20 -15 -3 1 3.97 1.43 -15 3 -2 5.96 1.44 -15 -3 2 4.55 1.67 -15 3 -3 5.87 1.35 -15 -3 3 6.60 1.72 -15 -3 4 3.04 1.42 -15 -3 5 6.62 1.85 -15 -3 6 -0.11 0.80 -15 -3 7 6.90 1.55 -15 -3 8 1.46 0.85 -15 -3 9 3.19 1.05 -15 -4 -7 3.09 1.13 -15 -4 -6 10.49 1.74 -15 -4 -5 8.75 1.71 -15 -4 -4 5.89 1.62 -15 -4 -3 10.98 2.02 -15 -4 -2 6.01 1.64 -15 4 1 0.84 0.80 -15 -4 -1 4.86 1.76 -15 4 0 2.17 1.01 -15 -4 0 1.18 1.16 -15 -4 1 0.75 0.76 -15 -4 2 3.89 1.25 -15 -4 3 6.47 1.61 -15 -4 4 2.18 1.18 -15 -4 5 7.54 1.73 -15 -4 6 8.64 1.83 -15 -4 7 0.90 0.90 -15 -4 8 0.23 0.72 -15 -5 -5 8.66 1.54 -15 -5 -4 0.92 0.90 -15 -5 -3 3.00 1.24 -15 -5 -2 4.12 1.29 -15 -5 -1 4.89 1.31 -15 -5 0 0.12 0.76 -15 -5 1 3.72 1.31 -15 -5 2 4.44 1.25 -15 -5 3 2.93 1.16 -15 -5 4 -0.11 0.71 -15 -5 5 3.95 1.26 -15 -5 6 3.45 1.15 -15 -6 -1 -0.33 0.57 -15 -6 0 -0.13 0.57 -15 -6 1 1.90 1.02 -15 -6 2 5.25 1.36 -15 -6 3 1.99 0.94 0 0 0 0.00 0.00 TITL E_L_2 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 12.655664 17.445297 29.202915 90.0000 90.0000 90.0000 ZERR 28.00 0.000214 0.000250 0.000461 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 308.00 280.00 28.00 28.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 14259 _shelx_fab_checksum 40364 _shelx_fab_file ; 0 0 4 40.60 -0.34 0 0 6 26.62 -0.32 0 0 8 -14.47 0.73 0 0 10 1.88 -0.14 0 0 12 -20.75 -0.35 0 0 14 30.64 0.42 0 0 16 -27.96 0.46 0 0 18 8.33 -0.77 0 0 20 -0.87 0.29 0 0 22 -5.66 -0.05 0 0 24 9.05 -0.30 0 0 26 -7.60 -0.16 0 0 28 2.31 0.32 0 0 30 1.20 -0.45 0 0 32 -1.60 0.29 0 0 34 -1.33 0.32 0 0 36 2.13 -0.38 0 1 2 -0.17 -6.65 0 1 3 -0.03 65.20 0 1 4 0.49 28.99 0 1 5 -0.07 -23.68 0 1 6 -0.47 -23.44 0 1 7 0.18 -12.61 0 1 8 0.23 -1.24 0 1 9 -0.09 8.39 0 1 10 0.00 23.33 0 1 11 -0.11 9.49 0 1 12 -0.13 -13.66 0 1 13 0.67 -6.13 0 1 14 -0.36 -5.12 0 1 15 -0.62 1.19 0 1 16 0.82 12.54 0 1 17 0.81 4.43 0 1 18 -0.81 -4.13 0 1 19 -0.66 2.40 0 1 20 0.07 -4.02 0 1 21 0.02 -2.04 0 1 22 0.20 -1.25 0 1 23 0.14 0.44 0 1 24 -0.18 8.30 0 1 25 -0.35 0.61 0 1 26 0.12 -10.22 0 1 27 0.03 0.13 0 1 28 0.03 5.25 0 1 29 0.03 -0.13 0 1 30 0.23 1.57 0 1 31 -0.06 -1.19 0 1 32 -0.21 -5.43 0 1 33 0.09 3.08 0 1 34 0.11 3.59 0 1 35 0.15 -2.01 0 1 36 0.02 -1.28 0 2 0 71.86 -0.25 0 2 1 -20.01 0.10 0 2 2 -64.00 0.37 0 2 3 30.46 -0.41 0 2 4 24.17 -0.04 0 2 5 -4.40 0.18 0 2 6 12.16 -0.41 0 2 7 -20.93 0.18 0 2 8 -22.97 0.40 0 2 9 35.03 -0.56 0 2 10 11.01 0.07 0 2 11 -18.22 0.37 0 2 12 1.32 -0.26 0 2 13 9.48 0.15 0 2 14 3.90 -0.22 0 2 15 -10.59 -0.19 0 2 16 -6.64 -0.05 0 2 17 14.56 0.04 0 2 18 5.66 0.14 0 2 19 -7.82 0.28 0 2 20 3.70 0.21 0 2 21 -7.62 0.26 0 2 22 -8.58 -0.21 0 2 23 11.56 -0.37 0 2 24 8.82 0.12 0 2 25 -7.36 0.18 0 2 26 -3.72 0.01 0 2 27 0.08 -0.11 0 2 28 -1.41 0.10 0 2 29 2.23 -0.16 0 2 30 2.34 -0.06 0 2 31 -1.24 -0.09 0 2 32 -0.71 0.06 0 2 33 -0.94 0.08 0 2 34 -0.08 -0.02 0 2 35 0.16 -0.05 0 2 36 0.01 -0.21 0 3 1 -0.09 -17.36 0 3 2 -0.51 -31.98 0 3 3 0.10 32.74 0 3 4 0.27 24.49 0 3 5 -0.09 -9.87 0 3 6 -0.05 -10.37 0 3 7 -0.02 -24.55 0 3 8 -0.25 -8.93 0 3 9 0.15 35.52 0 3 10 0.20 -0.14 0 3 11 -0.38 -17.30 0 3 12 -0.16 4.74 0 3 13 1.38 -5.09 0 3 14 -0.17 -10.37 0 3 15 -2.79 11.11 0 3 16 0.66 8.75 0 3 17 2.52 -6.48 0 3 18 -0.39 -5.33 0 3 19 -0.93 1.78 0 3 20 0.38 2.78 0 3 21 -0.11 -1.92 0 3 22 0.02 2.86 0 3 23 0.25 2.86 0 3 24 -0.13 -2.59 0 3 25 -0.14 -3.93 0 3 26 -0.01 1.82 0 3 27 -0.14 2.81 0 3 28 -0.06 0.22 0 3 29 0.21 0.85 0 3 30 -0.02 1.23 0 3 31 0.08 -3.39 0 3 32 -0.32 -2.56 0 3 33 -0.21 3.53 0 3 34 0.27 2.95 0 3 35 0.10 -1.74 0 3 36 -0.14 -0.27 0 4 0 -8.10 0.30 0 4 1 -44.62 0.48 0 4 2 6.15 -0.30 0 4 3 14.88 0.33 0 4 4 -8.49 0.09 0 4 5 9.14 -0.37 0 4 6 5.23 0.07 0 4 7 -23.65 0.33 0 4 8 -7.17 -0.18 0 4 9 7.39 -0.26 0 4 10 11.22 0.25 0 4 11 -1.41 0.39 0 4 12 -8.05 -0.44 0 4 13 0.97 -0.03 0 4 14 2.94 0.22 0 4 15 -12.16 -0.27 0 4 16 5.75 0.28 0 4 17 17.94 0.02 0 4 18 -7.19 -0.46 0 4 19 -13.21 -0.30 0 4 20 5.54 0.07 0 4 21 4.06 0.21 0 4 22 -2.68 0.19 0 4 23 6.36 0.08 0 4 24 1.55 0.01 0 4 25 -6.83 -0.32 0 4 26 -0.31 0.13 0 4 27 3.43 0.26 0 4 28 -1.06 -0.12 0 4 29 1.48 0.00 0 4 30 2.55 0.12 0 4 31 -1.53 0.08 0 4 32 -2.31 -0.21 0 4 33 -0.03 0.05 0 4 34 1.62 0.12 0 4 35 1.72 0.03 0 5 1 0.16 -10.39 0 5 2 0.60 -0.30 0 5 3 -0.14 19.34 0 5 4 -0.44 10.15 0 5 5 -0.20 10.44 0 5 6 0.43 -14.79 0 5 7 0.18 -31.32 0 5 8 -0.07 17.94 0 5 9 0.06 28.40 0 5 10 -0.23 -3.67 0 5 11 -0.29 -11.35 0 5 12 0.50 -8.08 0 5 13 0.27 -5.79 0 5 14 -0.32 15.50 0 5 15 -0.67 4.80 0 5 16 -0.10 -11.44 0 5 17 0.80 -5.29 0 5 18 0.09 5.23 0 5 19 -0.44 2.73 0 5 20 -0.27 -0.86 0 5 21 -0.13 -2.73 0 5 22 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21 -0.38 -0.76 6 16 21 -0.50 0.14 7 16 21 0.50 -0.22 4 17 21 0.34 -0.15 5 17 21 -1.24 -0.18 6 17 21 0.50 -0.45 0 18 21 -0.17 -0.08 1 18 21 0.44 0.14 2 18 21 -0.01 -0.38 3 18 21 0.45 -0.33 4 18 21 0.21 0.05 0 19 21 -0.01 1.02 13 0 22 0.67 0.07 13 1 22 0.56 -0.48 13 2 22 0.49 0.05 13 3 22 0.71 -0.01 13 4 22 -0.85 -0.03 13 5 22 0.75 -0.27 12 6 22 0.23 1.29 12 7 22 0.81 -0.83 12 8 22 -0.38 0.22 11 9 22 -0.33 -0.37 11 10 22 0.05 0.68 10 11 22 -0.50 0.34 10 12 22 -0.09 0.34 9 13 22 0.05 0.26 8 14 22 -0.08 -0.05 7 15 22 -0.07 -0.73 8 15 22 0.67 0.21 5 16 22 -0.58 0.70 6 16 22 0.78 -0.53 2 17 22 -0.81 0.02 3 17 22 0.21 -0.58 4 17 22 -0.76 -0.60 5 17 22 0.07 -0.23 0 18 22 0.86 -0.04 1 18 22 0.66 -0.52 2 18 22 -0.04 0.46 3 18 22 1.03 0.11 13 0 23 0.01 -0.23 13 1 23 0.61 -0.42 13 2 23 -0.37 0.12 13 3 23 0.34 -0.89 12 4 23 1.65 0.58 12 5 23 -0.03 0.16 12 6 23 0.08 -0.15 12 7 23 0.52 0.22 11 8 23 -0.37 1.67 11 9 23 0.42 -0.52 10 10 23 -0.35 -0.34 11 10 23 1.11 -1.25 10 11 23 0.67 0.65 9 12 23 -1.52 -0.06 8 13 23 0.82 -0.31 9 13 23 0.23 0.00 7 14 23 -1.10 0.63 8 14 23 0.08 0.21 6 15 23 0.34 -0.88 7 15 23 0.14 0.20 4 16 23 -0.11 1.25 5 16 23 -0.62 0.49 6 16 23 -0.06 0.12 0 17 23 -0.05 -0.03 1 17 23 -0.52 -0.07 2 17 23 -0.97 -0.25 3 17 23 -0.11 0.04 4 17 23 -0.80 -0.59 0 18 23 0.22 -0.03 1 18 23 -0.26 -0.55 12 0 24 1.04 0.13 12 1 24 0.78 0.75 12 2 24 0.20 0.02 12 3 24 0.94 0.30 12 4 24 -0.60 -1.54 12 5 24 1.10 -0.77 12 6 24 -0.12 -0.60 11 7 24 0.64 0.40 11 8 24 0.50 -0.29 10 9 24 0.43 0.58 11 9 24 1.17 1.15 10 10 24 -2.26 -0.34 9 11 24 -0.03 -1.26 10 11 24 -0.18 -0.18 8 12 24 -0.54 0.81 9 12 24 -0.51 -0.87 8 13 24 1.00 0.11 7 14 24 -0.06 0.05 5 15 24 0.31 -1.15 6 15 24 0.86 0.22 3 16 24 0.29 0.80 4 16 24 -0.23 -0.01 5 16 24 0.38 -0.07 0 17 24 0.04 -0.70 1 17 24 -0.29 -0.47 2 17 24 0.33 0.02 3 17 24 -0.12 -0.55 12 0 25 -0.01 -0.48 12 1 25 0.47 -0.25 12 2 25 -0.03 -0.90 12 3 25 0.61 -0.65 12 4 25 -0.54 0.09 11 5 25 0.85 0.52 11 6 25 0.40 -0.37 11 7 25 0.55 0.17 10 8 25 -0.55 0.31 11 8 25 -0.20 -0.88 10 9 25 0.94 -1.51 9 10 25 0.59 0.07 10 10 25 0.52 0.03 8 11 25 -0.08 0.17 9 11 25 -0.20 0.41 8 12 25 0.01 -0.28 7 13 25 0.60 1.15 8 13 25 0.22 0.83 6 14 25 -0.69 0.26 7 14 25 0.14 -0.40 4 15 25 -0.08 0.01 5 15 25 0.89 -0.50 6 15 25 -0.18 0.47 0 16 25 0.21 0.15 1 16 25 -0.08 1.33 2 16 25 0.54 0.44 3 16 25 -0.69 -0.54 4 16 25 -0.08 -0.35 0 17 25 0.02 -0.38 1 17 25 -0.40 -0.16 2 17 25 0.63 0.05 11 0 26 0.07 -0.11 12 0 26 -0.70 -0.10 11 1 26 0.24 0.08 12 1 26 -0.22 -0.26 11 2 26 -0.50 -0.42 12 2 26 0.00 -0.20 11 3 26 0.26 -0.03 11 4 26 0.32 -0.12 11 5 26 0.22 -0.64 11 6 26 -0.45 -0.45 10 7 26 -0.01 0.57 10 8 26 0.92 0.53 9 9 26 -1.90 0.54 10 9 26 -0.49 0.21 9 10 26 -0.13 -0.07 8 11 26 -0.66 0.05 9 11 26 -0.49 0.71 7 12 26 0.80 -0.59 8 12 26 -0.10 -0.77 6 13 26 -0.23 1.10 7 13 26 0.84 -0.35 5 14 26 0.12 -0.85 6 14 26 -0.23 -0.49 2 15 26 0.57 -0.13 3 15 26 -0.12 0.70 4 15 26 0.09 0.11 5 15 26 0.15 0.42 0 16 26 0.32 0.08 1 16 26 -0.43 0.36 2 16 26 -0.36 0.11 3 16 26 -0.98 -0.55 11 0 27 -0.07 1.23 11 1 27 0.77 -0.40 11 2 27 0.57 0.30 11 3 27 -0.44 -0.13 11 4 27 0.65 -0.31 10 5 27 -0.23 1.31 11 5 27 -0.63 -0.79 10 6 27 -0.06 -0.66 10 7 27 -0.51 0.16 9 8 27 0.36 -0.29 10 8 27 0.35 -0.41 9 9 27 -0.36 -0.05 8 10 27 0.88 -0.53 9 10 27 -0.23 0.39 7 11 27 0.06 0.22 8 11 27 -0.17 -0.20 6 12 27 -0.05 -1.24 7 12 27 1.19 -0.58 5 13 27 0.61 0.28 6 13 27 -0.28 0.29 3 14 27 -0.99 0.44 4 14 27 0.63 -0.34 5 14 27 -0.03 0.35 0 15 27 -0.01 -0.70 1 15 27 1.51 0.42 2 15 27 0.14 0.44 3 15 27 -0.26 0.68 4 15 27 0.27 0.59 0 16 27 -0.26 -0.13 1 16 27 -0.11 -0.37 10 0 28 -0.84 -0.05 11 0 28 0.60 0.03 10 1 28 0.23 0.41 11 1 28 0.18 -0.03 10 2 28 -0.52 -0.04 11 2 28 0.19 -0.62 10 3 28 0.98 0.48 11 3 28 -0.42 -0.11 10 4 28 0.31 0.27 10 5 28 0.61 -0.05 9 6 28 0.08 0.89 10 6 28 0.03 0.45 9 7 28 -0.60 1.57 10 7 28 -0.17 -0.58 9 8 28 0.63 -0.20 8 9 28 -0.38 -0.11 9 9 28 0.51 -0.17 7 10 28 0.69 -1.10 8 10 28 0.66 1.05 7 11 28 -0.24 0.15 6 12 28 -0.22 -0.17 7 12 28 0.09 -0.05 4 13 28 0.48 -0.38 5 13 28 -1.42 0.03 6 13 28 -0.28 -0.22 0 14 28 -0.91 0.02 1 14 28 0.33 0.21 2 14 28 -0.10 -0.29 3 14 28 0.15 -0.42 4 14 28 0.67 -0.53 0 15 28 0.09 0.40 1 15 28 0.67 0.70 2 15 28 -0.20 0.01 10 0 29 0.06 0.68 10 1 29 0.51 -0.49 10 2 29 -0.12 0.42 10 3 29 -0.48 -0.08 10 4 29 0.62 -0.05 9 5 29 0.20 0.03 10 5 29 -0.13 -0.82 9 6 29 -0.02 0.94 8 7 29 -0.12 0.16 9 7 29 0.21 0.85 8 8 29 -0.93 0.14 9 8 29 0.36 0.07 7 9 29 -0.01 -0.70 8 9 29 -0.96 0.28 7 10 29 0.12 -0.28 6 11 29 0.35 -0.70 7 11 29 -0.35 -0.60 4 12 29 0.33 -0.41 5 12 29 -0.24 0.32 6 12 29 0.38 0.54 0 13 29 0.01 0.57 1 13 29 0.27 -0.13 2 13 29 0.23 -0.07 3 13 29 0.10 -0.64 4 13 29 -0.15 -0.47 5 13 29 -0.61 -0.01 0 14 29 0.01 -0.04 1 14 29 0.74 -0.49 2 14 29 -0.11 -0.06 3 14 29 0.71 0.02 9 0 30 0.30 0.06 10 0 30 0.90 0.07 9 1 30 0.06 0.90 10 1 30 0.02 -0.34 9 2 30 0.04 0.65 10 2 30 0.23 -0.48 9 3 30 0.80 0.69 9 4 30 -0.08 0.09 8 5 30 -1.52 -0.05 9 5 30 -0.34 -0.13 8 6 30 -0.16 0.50 9 6 30 -0.33 -0.07 8 7 30 0.22 -0.32 7 8 30 0.12 0.66 8 8 30 -1.05 -0.23 6 9 30 0.10 -0.21 7 9 30 0.52 -0.85 6 10 30 0.82 0.52 7 10 30 -0.28 0.40 4 11 30 -1.45 0.84 5 11 30 -0.74 -0.69 6 11 30 -0.18 0.14 2 12 30 -0.39 -0.40 3 12 30 0.52 0.47 4 12 30 0.10 0.21 5 12 30 0.13 0.52 0 13 30 0.01 0.30 1 13 30 -0.43 -0.63 2 13 30 -1.47 0.04 3 13 30 -0.35 -0.50 0 14 30 0.78 -0.11 1 14 30 -0.22 -0.67 9 0 31 0.01 0.09 9 1 31 -0.11 -0.23 9 2 31 0.29 0.50 8 3 31 -0.03 0.97 9 3 31 0.81 -0.28 8 4 31 -0.41 0.20 9 4 31 0.90 -0.21 8 5 31 0.57 1.20 7 6 31 -0.09 0.66 8 6 31 -0.32 0.58 7 7 31 -0.62 -0.61 8 7 31 0.12 -0.34 6 8 31 1.08 -0.40 7 8 31 -0.85 0.80 5 9 31 0.05 -0.11 6 9 31 0.27 -1.24 7 9 31 -0.09 -0.04 4 10 31 -0.02 0.16 5 10 31 0.93 0.55 6 10 31 -0.10 -0.14 2 11 31 -1.40 0.40 3 11 31 0.49 0.69 4 11 31 -1.17 0.70 5 11 31 0.74 0.21 0 12 31 0.08 -0.06 1 12 31 -0.07 -0.43 2 12 31 0.02 0.19 3 12 31 -0.07 0.04 4 12 31 0.04 0.53 0 13 31 0.06 0.49 1 13 31 -0.34 -0.36 2 13 31 -0.16 0.12 8 0 32 -0.77 -0.01 9 0 32 0.01 0.05 8 1 32 0.09 -0.01 8 2 32 -0.25 0.26 8 3 32 0.64 -0.55 7 4 32 0.03 0.47 8 4 32 -0.42 -0.18 7 5 32 0.45 -0.06 8 5 32 0.68 -0.02 6 6 32 0.62 0.24 7 6 32 -0.77 0.28 6 7 32 -0.41 -0.77 7 7 32 -0.39 0.60 5 8 32 -0.26 -0.24 6 8 32 0.10 0.07 4 9 32 -0.50 -0.77 5 9 32 0.37 0.61 6 9 32 0.02 -0.82 2 10 32 0.69 0.39 3 10 32 0.13 -0.09 4 10 32 -0.85 -0.28 5 10 32 0.09 -0.11 0 11 32 0.08 -0.01 1 11 32 -0.59 0.22 2 11 32 0.75 -0.68 3 11 32 0.89 -0.18 4 11 32 0.30 -0.23 0 12 32 -0.41 0.01 1 12 32 0.29 0.25 2 12 32 0.16 1.01 7 0 33 -0.08 -1.21 8 0 33 0.00 0.42 7 1 33 -0.75 0.42 8 1 33 -0.25 -0.22 7 2 33 -0.58 -0.51 8 2 33 0.24 0.39 7 3 33 -0.56 0.02 8 3 33 0.07 -0.45 6 4 33 -0.26 -0.52 7 4 33 -1.10 0.31 6 5 33 0.38 -0.96 7 5 33 -0.15 -0.17 5 6 33 0.36 -0.15 6 6 33 -0.35 -0.28 7 6 33 -0.39 -0.39 5 7 33 0.32 0.65 6 7 33 0.07 0.23 4 8 33 -0.77 0.57 5 8 33 -0.26 0.11 1 9 33 -0.45 -0.83 2 9 33 1.31 -0.03 3 9 33 0.49 -0.19 4 9 33 0.82 -0.46 5 9 33 0.41 0.20 0 10 33 1.87 0.00 1 10 33 -0.52 0.00 2 10 33 0.39 0.91 3 10 33 -0.27 0.01 4 10 33 -0.61 0.28 0 11 33 0.03 -0.89 1 11 33 -0.42 -0.48 2 11 33 0.46 -0.40 6 0 34 -0.06 0.01 7 0 34 -1.15 0.07 6 1 34 0.42 -0.04 7 1 34 -0.15 0.52 6 2 34 0.08 0.42 7 2 34 -0.55 -0.02 6 3 34 0.03 -1.04 7 3 34 -0.06 -0.41 5 4 34 -0.48 0.17 6 4 34 0.03 0.50 5 5 34 0.68 -0.03 6 5 34 -0.28 0.08 4 6 34 0.18 0.31 5 6 34 -0.03 0.20 6 6 34 -0.91 -0.21 3 7 34 -0.26 -0.04 4 7 34 0.35 0.59 5 7 34 0.16 -0.26 0 8 34 0.29 0.03 1 8 34 -0.83 -0.27 2 8 34 -0.04 0.46 3 8 34 -1.12 0.44 4 8 34 0.02 0.34 0 9 34 -0.24 -0.89 1 9 34 -0.25 -0.64 2 9 34 0.55 -0.28 3 9 34 -0.22 -0.57 0 10 34 0.06 -0.02 1 10 34 -0.38 0.08 5 0 35 -0.09 -0.35 6 0 35 0.04 -0.43 5 1 35 0.75 -0.19 6 1 35 0.05 0.47 5 2 35 0.58 0.58 6 2 35 0.38 -0.14 4 3 35 -0.08 0.63 5 3 35 -0.60 0.21 6 3 35 -0.96 0.34 4 4 35 -1.22 0.22 5 4 35 0.32 -0.03 3 5 35 -0.79 -0.24 4 5 35 0.42 0.28 5 5 35 -0.10 0.36 0 6 35 -0.96 0.15 1 6 35 -0.62 0.50 2 6 35 -0.21 -1.33 3 6 35 -0.25 -1.16 4 6 35 -0.17 -0.27 0 7 35 0.02 -0.34 1 7 35 -0.26 0.47 2 7 35 0.96 0.17 3 7 35 -0.41 -0.27 4 7 35 0.15 0.25 0 8 35 -1.34 0.01 1 8 35 -0.29 0.56 2 8 35 0.14 0.19 3 8 35 -0.30 -0.01 0 9 35 -0.08 -0.29 3 0 36 1.43 -0.10 4 0 36 -1.29 0.07 5 0 36 0.08 -0.03 3 1 36 0.09 -1.28 4 1 36 0.34 0.15 5 1 36 0.03 -0.38 2 2 36 0.22 0.79 3 2 36 -0.63 -0.01 4 2 36 0.03 -0.27 5 2 36 0.11 -0.95 1 3 36 -0.80 -0.13 2 3 36 0.12 -0.14 3 3 36 0.69 -0.24 4 3 36 0.43 0.46 5 3 36 0.21 0.05 0 4 36 -0.46 -0.02 1 4 36 -0.71 0.02 2 4 36 -0.03 -0.03 3 4 36 -0.83 0.38 4 4 36 0.26 -0.53 0 5 36 -0.11 0.13 1 5 36 -0.59 -0.08 2 5 36 0.60 0.46 3 5 36 0.36 -0.19 4 5 36 0.56 0.87 0 6 36 -0.72 -0.04 1 6 36 -0.67 1.09 2 6 36 -0.46 -0.36 3 6 36 -0.68 0.12 0 7 36 0.12 0.02 1 7 36 0.82 0.16 2 7 36 0.12 0.43 1 0 37 -0.11 0.24 2 0 37 -0.04 -0.12 3 0 37 0.01 -0.10 4 0 37 0.00 -0.12 0 1 37 -0.04 0.16 1 1 37 -1.27 -0.32 2 1 37 -0.03 0.08 3 1 37 0.17 -0.67 4 1 37 -0.30 -0.02 0 2 37 -0.51 -0.06 1 2 37 -0.13 0.77 2 2 37 0.25 0.63 3 2 37 -0.11 0.11 0 3 37 -0.02 0.29 1 3 37 -0.46 0.38 2 3 37 0.50 -0.04 3 3 37 -0.26 0.14 0 4 37 -0.30 -0.08 1 4 37 -0.01 0.04 2 4 37 -0.04 0.24 0 5 37 0.00 0.48 1 5 37 0.49 0.14 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 91117) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.190 0.750 761 145 ' ' 2 0.500 0.448 0.250 761 144 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 1 1 2.951 0 0 2 3.026 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL e_l_2_a.res in P2(1)2(1)2(1) CELL 12.6557 17.4453 29.2029 90.00 90.00 90.00 SPGR P212121 # Solvent Accessible Volume = 1522 # Electrons Found in S.A.V. = 288 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.905 0.058 0.337 ! 10.60 eA-3 C102 0.408 0.511 0.207 ! 5.39 eA-3 C103 0.861 0.060 0.652 ! 3.85 eA-3 C104 0.964 0.348 0.701 ! 3.63 eA-3 C105 0.377 0.331 0.276 ! 3.35 eA-3 C106 0.485 0.808 0.150 ! 2.59 eA-3 C107 0.654 0.889 0.257 ! 2.15 eA-3 C108 0.452 0.084 0.212 ! 2.10 eA-3 C109 0.090 0.431 0.792 ! 1.92 eA-3 C110 0.077 0.896 0.720 ! 1.91 eA-3 C111 0.329 0.535 0.290 ! 1.87 eA-3 C112 0.484 0.558 0.290 ! 1.70 eA-3 C113 0.907 0.246 0.641 ! 1.64 eA-3 C114 0.938 0.663 0.823 ! 1.61 eA-3 Q115 0.894 0.667 0.976 ! 1.43 eA-3 C116 0.468 0.078 0.271 ! 1.27 eA-3 C117 0.719 0.946 0.264 ! 0.88 eA-3 C118 0.052 0.625 0.818 ! 0.88 eA-3 C119 0.705 0.027 0.752 ! 0.79 eA-3 Q120 0.404 0.393 0.210 ! 0.62 eA-3 Q121 0.062 0.294 0.614 ! 0.53 eA-3 C122 0.605 0.130 0.227 ! 0.52 eA-3 ) ; _shelx_shelxl_version_number 2014/7 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp O1* O 0.72786(16) 0.42108(9) 0.54010(7) 0.0388(4) Uani 1 1 d . . O1' O 0.37564(16) 0.93607(10) 0.68462(6) 0.0405(4) Uani 1 1 d . . O2' O 0.54780(17) 0.96510(10) 0.69260(7) 0.0422(5) Uani 1 1 d . . O2* O 0.85675(15) 0.49545(10) 0.56827(7) 0.0396(4) Uani 1 1 d . . O1 O 0.16617(15) 0.72886(11) 0.65138(7) 0.0423(4) Uani 1 1 d . . N1* N 0.59633(16) 0.51439(11) 0.63781(7) 0.0285(4) Uani 1 1 d . . H1* H 0.5523 0.4785 0.6445 0.034 Uiso 1 1 calc R . N1 N 0.42694(16) 0.51663(10) 0.57097(7) 0.0269(4) Uani 1 1 d . . N1' N 0.47224(18) 0.82888(11) 0.59377(7) 0.0315(4) Uani 1 1 d . . H1' H 0.4168 0.8315 0.5768 0.038 Uiso 1 1 calc R . N4' N 0.60672(19) 0.79679(12) 0.78580(7) 0.0358(5) Uani 1 1 d . . N4* N 0.7955(2) 0.67438(12) 0.48038(7) 0.0390(5) Uani 1 1 d . . C13 C 0.37220(19) 0.57617(13) 0.59146(7) 0.0270(5) Uani 1 1 d . . C11 C 0.33770(19) 0.69310(13) 0.63104(8) 0.0278(5) Uani 1 1 d . . C2' C 0.4760(2) 0.79563(12) 0.63702(8) 0.0280(5) Uani 1 1 d . . C12 C 0.4092(2) 0.64421(12) 0.61092(7) 0.0269(5) Uani 1 1 d . . H12 H 0.4808 0.6562 0.6103 0.032 Uiso 1 1 calc R . C3* C 0.53851(19) 0.51980(12) 0.55707(8) 0.0270(5) Uani 1 1 d . . H3* H 0.5607 0.4668 0.5513 0.032 Uiso 1 1 calc R . C2* C 0.60603(19) 0.54921(12) 0.59551(8) 0.0263(4) Uani 1 1 d . . C8 C 0.2649(2) 0.55593(13) 0.59201(8) 0.0307(5) Uani 1 1 d . . C8' C 0.6383(2) 0.84166(13) 0.61898(8) 0.0332(5) Uani 1 1 d . . C13' C 0.5694(2) 0.85675(13) 0.58226(8) 0.0356(6) Uani 1 1 d . . C7 C 0.2554(2) 0.48232(14) 0.57126(9) 0.0337(5) Uani 1 1 d . . C7' C 0.5778(2) 0.80194(13) 0.65351(8) 0.0306(5) Uani 1 1 d . . C22' C 0.4597(2) 0.92273(13) 0.70131(8) 0.0343(6) Uani 1 1 d . . C7* C 0.68490(19) 0.60369(13) 0.59711(8) 0.0283(5) Uani 1 1 d . . C9* C 0.8085(2) 0.64022(15) 0.66474(9) 0.0351(5) Uani 1 1 d . . H9* H 0.8478 0.6768 0.6491 0.042 Uiso 1 1 calc R . C2 C 0.3555(2) 0.45951(13) 0.55856(8) 0.0292(5) Uani 1 1 d . . C21 C 0.3410(2) 0.31451(14) 0.55735(9) 0.0357(5) Uani 1 1 d . . H21 H 0.3503 0.3163 0.5907 0.043 Uiso 1 1 calc R . C8* C 0.72638(19) 0.60152(13) 0.64281(8) 0.0299(5) Uani 1 1 d . . C13* C 0.6678(2) 0.54609(13) 0.66740(8) 0.0299(5) Uani 1 1 d . . C10 C 0.2287(2) 0.67450(14) 0.63077(8) 0.0329(5) Uani 1 1 d . . C3' C 0.3759(2) 0.76425(13) 0.65680(8) 0.0293(5) Uani 1 1 d . . H3' H 0.3213 0.8038 0.6541 0.035 Uiso 1 1 calc R . N4 N 0.2290(2) 0.30648(15) 0.54703(11) 0.0559(7) Uani 1 1 d . . C5' C 0.5941(2) 0.83188(14) 0.73944(8) 0.0316(5) Uani 1 1 d . . H5' H 0.6427 0.8755 0.7378 0.038 Uiso 1 1 calc R . C6' C 0.6217(2) 0.77762(14) 0.69887(8) 0.0330(5) Uani 1 1 d . . H6'A H 0.6980 0.7743 0.6963 0.040 Uiso 1 1 calc R . H6'B H 0.5955 0.7267 0.7059 0.040 Uiso 1 1 calc R . C5* C 0.7915(2) 0.62530(13) 0.52174(9) 0.0339(5) Uani 1 1 d . . H5* H 0.8638 0.6209 0.5335 0.041 Uiso 1 1 calc R . C16' C 0.4814(2) 0.86450(14) 0.73842(8) 0.0311(5) Uani 1 1 d . . H16' H 0.4771 0.8946 0.7667 0.037 Uiso 1 1 calc R . C22* C 0.7752(2) 0.48133(14) 0.54007(9) 0.0354(5) Uani 1 1 d . . C16* C 0.7572(2) 0.54525(13) 0.50584(9) 0.0332(5) Uani 1 1 d . . H16* H 0.8062 0.5333 0.4809 0.040 Uiso 1 1 calc R . C12* C 0.6892(2) 0.53006(15) 0.71366(9) 0.0386(6) Uani 1 1 d . . H12* H 0.6496 0.4943 0.7299 0.046 Uiso 1 1 calc R . C9 C 0.1918(2) 0.60724(15) 0.61196(9) 0.0354(5) Uani 1 1 d . . H9 H 0.1200 0.5958 0.6124 0.043 Uiso 1 1 calc R . C15* C 0.6484(2) 0.54348(14) 0.48291(8) 0.0339(5) Uani 1 1 d . . H15* H 0.6382 0.4916 0.4708 0.041 Uiso 1 1 calc R . C21* C 0.6936(2) 0.67776(15) 0.45649(9) 0.0418(6) Uani 1 1 d . . H21A H 0.7008 0.7102 0.4297 0.050 Uiso 1 1 calc R . H21B H 0.6418 0.7012 0.4766 0.050 Uiso 1 1 calc R . C10* C 0.8307(2) 0.62357(16) 0.71001(9) 0.0408(6) Uani 1 1 d . . H10* H 0.8860 0.6488 0.7246 0.049 Uiso 1 1 calc R . C6* C 0.7223(2) 0.65877(13) 0.56088(8) 0.0328(5) Uani 1 1 d . . H6*A H 0.7622 0.6991 0.5758 0.039 Uiso 1 1 calc R . H6*B H 0.6606 0.6825 0.5471 0.039 Uiso 1 1 calc R . C14* C 0.5505(2) 0.56291(14) 0.51178(8) 0.0322(5) Uani 1 1 d . . H14A H 0.5518 0.6174 0.5184 0.039 Uiso 1 1 calc R . H14B H 0.4882 0.5530 0.4934 0.039 Uiso 1 1 calc R . C14' C 0.3833(2) 0.74047(13) 0.70765(8) 0.0322(5) Uani 1 1 d . . H14C H 0.4430 0.7060 0.7107 0.039 Uiso 1 1 calc R . H14D H 0.3203 0.7112 0.7150 0.039 Uiso 1 1 calc R . C15' C 0.3953(2) 0.80372(14) 0.74441(8) 0.0320(5) Uani 1 1 d . . H15' H 0.3275 0.8308 0.7462 0.038 Uiso 1 1 calc R . C16 C 0.3902(2) 0.38688(13) 0.53618(9) 0.0379(6) Uani 1 1 d . . H16 H 0.4670 0.3831 0.5399 0.045 Uiso 1 1 calc R . C20* C 0.6524(3) 0.59875(15) 0.44135(9) 0.0398(6) Uani 1 1 d . . H20* H 0.5795 0.6060 0.4309 0.048 Uiso 1 1 calc R . C12' C 0.6031(3) 0.89563(15) 0.54286(9) 0.0420(6) Uani 1 1 d . . H12' H 0.5572 0.9045 0.5186 0.050 Uiso 1 1 calc R . C21' C 0.5277(2) 0.73634(14) 0.79532(9) 0.0385(6) Uani 1 1 d . . H21C H 0.5390 0.7169 0.8261 0.046 Uiso 1 1 calc R . H21D H 0.5386 0.6942 0.7742 0.046 Uiso 1 1 calc R . C20 C 0.3999(2) 0.24444(14) 0.53835(10) 0.0384(6) Uani 1 1 d . . H20 H 0.4756 0.2520 0.5438 0.046 Uiso 1 1 calc R . C19* C 0.7156(3) 0.56691(18) 0.40046(9) 0.0470(7) Uani 1 1 d . . H19A H 0.7153 0.6049 0.3762 0.056 Uiso 1 1 calc R . H19B H 0.7883 0.5596 0.4099 0.056 Uiso 1 1 calc R . C20' C 0.4130(2) 0.76392(15) 0.79118(8) 0.0362(5) Uani 1 1 d . . H20' H 0.3684 0.7180 0.7914 0.043 Uiso 1 1 calc R . C9' C 0.7430(2) 0.86695(16) 0.61652(10) 0.0422(6) Uani 1 1 d . . H9' H 0.7893 0.8577 0.6406 0.051 Uiso 1 1 calc R . C11* C 0.7713(2) 0.56940(17) 0.73417(9) 0.0423(6) Uani 1 1 d . . H11* H 0.7874 0.5597 0.7647 0.051 Uiso 1 1 calc R . C19' C 0.3775(3) 0.81374(17) 0.83181(9) 0.0427(6) Uani 1 1 d . . H19C H 0.4306 0.8527 0.8373 0.051 Uiso 1 1 calc R . H19D H 0.3124 0.8397 0.8236 0.051 Uiso 1 1 calc R . C23* C 0.8719(2) 0.44016(17) 0.60440(10) 0.0456(7) Uani 1 1 d . . H23A H 0.8945 0.3923 0.5915 0.068 Uiso 1 1 calc GR . H23B H 0.8065 0.4328 0.6205 0.068 Uiso 1 1 calc GR . H23C H 0.9247 0.4586 0.6253 0.068 Uiso 1 1 calc GR . C19 C 0.3673(3) 0.16963(15) 0.56141(10) 0.0448(7) Uani 1 1 d . . H19E H 0.3669 0.1770 0.5943 0.054 Uiso 1 1 calc R . H19F H 0.2959 0.1567 0.5520 0.054 Uiso 1 1 calc R . C24* C 0.8317(3) 0.75180(16) 0.49206(10) 0.0468(7) Uani 1 1 d . . H24A H 0.7804 0.7762 0.5114 0.070 Uiso 1 1 calc GR . H24B H 0.8404 0.7812 0.4645 0.070 Uiso 1 1 calc GR . H24C H 0.8980 0.7487 0.5079 0.070 Uiso 1 1 calc GR . C6 C 0.1540(2) 0.43972(17) 0.56369(11) 0.0456(7) Uani 1 1 d . . H6A H 0.1323 0.4477 0.5322 0.055 Uiso 1 1 calc R . H6B H 0.1003 0.4624 0.5831 0.055 Uiso 1 1 calc R . C11' C 0.7063(3) 0.92019(16) 0.54132(10) 0.0503(8) Uani 1 1 d . . H11' H 0.7299 0.9468 0.5157 0.060 Uiso 1 1 calc R . C24' C 0.7132(3) 0.76913(18) 0.79362(10) 0.0471(7) Uani 1 1 d . . H24D H 0.7265 0.7256 0.7743 0.071 Uiso 1 1 calc GR . H24E H 0.7208 0.7544 0.8251 0.071 Uiso 1 1 calc GR . H24F H 0.7629 0.8090 0.7866 0.071 Uiso 1 1 calc GR . C18 C 0.4402(3) 0.10330(15) 0.54977(12) 0.0523(8) Uani 1 1 d . . H18A H 0.4446 0.0978 0.5171 0.078 Uiso 1 1 calc GR . H18B H 0.4127 0.0569 0.5629 0.078 Uiso 1 1 calc GR . H18C H 0.5093 0.1132 0.5620 0.078 Uiso 1 1 calc GR . C5 C 0.1563(3) 0.35392(18) 0.57279(13) 0.0555(8) Uani 1 1 d . . H5A H 0.1716 0.3467 0.6050 0.067 Uiso 1 1 calc R . H5B H 0.0856 0.3343 0.5675 0.067 Uiso 1 1 calc R . C15 C 0.3817(3) 0.24277(15) 0.48553(10) 0.0443(6) Uani 1 1 d . . H15A H 0.4490 0.2450 0.4698 0.053 Uiso 1 1 calc R . H15B H 0.3466 0.1954 0.4770 0.053 Uiso 1 1 calc R . C10' C 0.7774(3) 0.90608(17) 0.57772(11) 0.0503(7) Uani 1 1 d . . H10' H 0.8470 0.9229 0.5757 0.060 Uiso 1 1 calc R . C23' C 0.5360(3) 1.02386(17) 0.65807(11) 0.0568(9) Uani 1 1 d . . H23D H 0.5326 1.0004 0.6284 0.085 Uiso 1 1 calc GR . H23E H 0.5954 1.0580 0.6593 0.085 Uiso 1 1 calc GR . H23F H 0.4722 1.0522 0.6636 0.085 Uiso 1 1 calc GR . C18* C 0.6743(3) 0.4917(2) 0.38125(11) 0.0578(9) Uani 1 1 d . . H18D H 0.7095 0.4805 0.3529 0.087 Uiso 1 1 calc GR . H18E H 0.5997 0.4958 0.3760 0.087 Uiso 1 1 calc GR . H18F H 0.6877 0.4512 0.4027 0.087 Uiso 1 1 calc GR . C14 C 0.3146(4) 0.3101(2) 0.47174(12) 0.0657(10) Uani 1 1 d . U H14 H 0.3015 0.3085 0.4387 0.079 Uiso 1 1 calc R . C22 C 0.0552(2) 0.7164(2) 0.64983(13) 0.0564(8) Uani 1 1 d . . H22A H 0.0329 0.7119 0.6185 0.085 Uiso 1 1 calc GR . H22B H 0.0195 0.7587 0.6640 0.085 Uiso 1 1 calc GR . H22C H 0.0383 0.6700 0.6659 0.085 Uiso 1 1 calc GR . C18' C 0.3598(4) 0.7701(2) 0.87517(11) 0.0675(11) Uani 1 1 d . . H18G H 0.3040 0.7336 0.8707 0.101 Uiso 1 1 calc GR . H18H H 0.3406 0.8050 0.8992 0.101 Uiso 1 1 calc GR . H18I H 0.4235 0.7437 0.8835 0.101 Uiso 1 1 calc GR . C17 C 0.3663(5) 0.38489(19) 0.48419(11) 0.0909(18) Uani 1 1 d . . H17A H 0.3200 0.4271 0.4762 0.109 Uiso 1 1 calc R . H17B H 0.4316 0.3907 0.4671 0.109 Uiso 1 1 calc R . C3 C 0.2108(4) 0.3062(4) 0.49724(18) 0.107(2) Uani 1 1 d . U H3A H 0.1673 0.3498 0.4889 0.129 Uiso 1 1 calc R . H3B H 0.1733 0.2599 0.4886 0.129 Uiso 1 1 calc R . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1* 0.0412(10) 0.0260(8) 0.0492(11) -0.0017(7) 0.0088(9) 0.0013(7) O1' 0.0533(12) 0.0324(9) 0.0359(9) -0.0043(7) -0.0089(9) 0.0107(8) O2' 0.0577(13) 0.0282(8) 0.0407(10) 0.0039(7) 0.0044(9) -0.0020(8) O2* 0.0366(10) 0.0395(9) 0.0428(10) -0.0002(8) 0.0070(8) 0.0017(8) O1 0.0329(10) 0.0424(10) 0.0515(11) -0.0094(8) 0.0049(8) 0.0046(8) N1* 0.0297(10) 0.0269(9) 0.0290(10) 0.0042(7) 0.0029(8) -0.0046(8) N1 0.0299(10) 0.0235(8) 0.0273(9) -0.0018(7) 0.0003(8) -0.0005(7) N1' 0.0418(12) 0.0263(9) 0.0265(10) 0.0008(8) 0.0014(9) 0.0033(8) N4' 0.0438(13) 0.0369(11) 0.0266(10) -0.0016(8) -0.0017(9) 0.0067(9) N4* 0.0528(14) 0.0337(11) 0.0306(10) -0.0006(9) 0.0104(10) -0.0113(10) C13 0.0333(12) 0.0255(10) 0.0222(10) 0.0002(8) 0.0006(9) -0.0002(9) C11 0.0331(12) 0.0268(10) 0.0234(10) 0.0010(8) 0.0017(9) 0.0011(9) C2' 0.0386(13) 0.0204(9) 0.0249(11) -0.0015(8) 0.0043(10) 0.0014(9) C12 0.0321(12) 0.0262(10) 0.0223(10) 0.0028(8) 0.0008(9) -0.0001(9) C3* 0.0300(12) 0.0233(10) 0.0278(11) -0.0009(8) 0.0040(9) -0.0012(9) C2* 0.0301(12) 0.0230(10) 0.0257(10) 0.0004(8) 0.0033(9) 0.0043(8) C8 0.0302(12) 0.0324(11) 0.0295(11) 0.0004(9) -0.0028(10) -0.0004(9) C8' 0.0405(14) 0.0298(11) 0.0295(12) -0.0061(9) 0.0063(10) -0.0023(10) C13' 0.0545(16) 0.0239(10) 0.0283(12) -0.0045(9) 0.0060(11) -0.0017(10) C7 0.0327(13) 0.0354(12) 0.0331(12) -0.0046(10) -0.0020(10) -0.0024(10) C7' 0.0375(13) 0.0269(10) 0.0275(11) -0.0045(9) 0.0036(10) 0.0015(10) C22' 0.0508(16) 0.0255(11) 0.0265(11) -0.0060(9) 0.0015(11) 0.0078(11) C7* 0.0318(12) 0.0243(10) 0.0288(11) -0.0026(8) 0.0048(9) 0.0000(9) C9* 0.0331(13) 0.0371(12) 0.0351(13) -0.0044(10) 0.0049(10) -0.0056(10) C2 0.0323(12) 0.0253(10) 0.0301(11) 0.0004(9) -0.0002(10) -0.0038(9) C21 0.0386(14) 0.0306(11) 0.0380(13) -0.0033(10) -0.0009(11) -0.0081(10) C8* 0.0295(12) 0.0288(10) 0.0315(12) -0.0032(9) 0.0047(10) -0.0001(9) C13* 0.0309(12) 0.0295(11) 0.0292(11) -0.0013(9) 0.0021(10) -0.0014(9) C10 0.0320(12) 0.0361(12) 0.0305(12) -0.0007(10) 0.0037(10) 0.0046(10) C3' 0.0338(13) 0.0261(10) 0.0280(11) -0.0015(9) 0.0022(9) 0.0047(9) N4 0.0401(14) 0.0470(13) 0.080(2) -0.0264(13) -0.0007(13) -0.0083(11) C5' 0.0372(13) 0.0311(11) 0.0264(11) -0.0012(9) 0.0005(10) 0.0030(10) C6' 0.0360(13) 0.0307(11) 0.0324(12) -0.0018(9) 0.0024(10) 0.0052(10) C5* 0.0395(14) 0.0293(11) 0.0329(12) -0.0004(9) 0.0085(11) -0.0072(10) C16' 0.0403(14) 0.0276(10) 0.0252(11) -0.0040(9) 0.0012(10) 0.0046(10) C22* 0.0357(13) 0.0336(12) 0.0370(13) -0.0037(10) 0.0105(11) 0.0034(10) C16* 0.0361(13) 0.0312(11) 0.0322(12) -0.0050(9) 0.0105(10) -0.0023(10) C12* 0.0430(15) 0.0407(13) 0.0322(12) 0.0062(10) -0.0018(11) -0.0040(11) C9 0.0284(12) 0.0399(13) 0.0380(13) -0.0030(11) 0.0000(10) -0.0001(10) C15* 0.0426(14) 0.0307(11) 0.0285(11) -0.0024(9) 0.0075(11) -0.0068(10) C21* 0.0574(18) 0.0385(13) 0.0296(12) 0.0060(11) 0.0100(12) -0.0037(12) C10* 0.0372(14) 0.0470(15) 0.0381(14) -0.0041(11) -0.0020(11) -0.0053(12) C6* 0.0435(14) 0.0253(10) 0.0295(12) -0.0012(9) 0.0069(10) -0.0083(10) C14* 0.0354(13) 0.0333(11) 0.0278(11) 0.0020(9) 0.0016(10) -0.0031(10) C14' 0.0390(14) 0.0299(11) 0.0276(11) -0.0012(9) 0.0027(10) -0.0014(10) C15' 0.0373(13) 0.0321(11) 0.0267(11) -0.0014(9) 0.0022(10) 0.0007(10) C16 0.0456(15) 0.0270(11) 0.0410(14) -0.0048(10) 0.0067(12) -0.0043(11) C20* 0.0498(16) 0.0423(14) 0.0273(12) 0.0003(10) 0.0076(11) -0.0097(12) C12' 0.0623(18) 0.0331(12) 0.0307(13) -0.0007(10) 0.0077(13) -0.0018(12) C21' 0.0586(17) 0.0312(12) 0.0257(11) 0.0009(10) -0.0005(12) 0.0044(12) C20 0.0438(15) 0.0283(11) 0.0430(14) -0.0046(10) -0.0015(12) -0.0039(10) C19* 0.0584(19) 0.0539(16) 0.0288(13) -0.0034(12) 0.0122(12) -0.0141(14) C20' 0.0473(15) 0.0333(12) 0.0279(12) 0.0012(10) 0.0038(11) -0.0013(11) C9' 0.0461(16) 0.0432(13) 0.0374(14) -0.0101(11) 0.0078(12) -0.0103(12) C11* 0.0438(15) 0.0520(15) 0.0310(13) 0.0043(11) -0.0057(11) -0.0011(13) C19' 0.0535(17) 0.0456(14) 0.0290(12) -0.0030(11) 0.0077(12) 0.0041(13) C23* 0.0416(16) 0.0493(15) 0.0460(16) 0.0032(12) 0.0060(13) 0.0092(13) C19 0.0554(18) 0.0336(13) 0.0454(15) -0.0026(11) -0.0015(13) -0.0127(12) C24* 0.070(2) 0.0357(13) 0.0346(13) -0.0021(11) 0.0135(14) -0.0183(13) C6 0.0345(14) 0.0484(15) 0.0540(16) -0.0139(13) -0.0022(13) -0.0056(12) C11' 0.077(2) 0.0361(13) 0.0377(14) -0.0008(11) 0.0172(15) -0.0147(14) C24' 0.0526(18) 0.0535(16) 0.0351(14) -0.0052(12) -0.0076(13) 0.0178(14) C18 0.063(2) 0.0287(12) 0.065(2) 0.0019(13) -0.0106(16) -0.0077(13) C5 0.0394(16) 0.0470(16) 0.080(2) -0.0152(15) 0.0097(16) -0.0152(13) C15 0.0552(18) 0.0354(13) 0.0425(15) -0.0090(11) 0.0032(13) -0.0044(12) C10' 0.0559(18) 0.0481(16) 0.0468(16) -0.0101(13) 0.0169(14) -0.0173(14) C23' 0.092(3) 0.0327(13) 0.0454(16) 0.0086(12) 0.0083(17) -0.0012(15) C18* 0.074(2) 0.0607(19) 0.0388(15) -0.0106(14) 0.0087(16) -0.0227(17) C14 0.094(3) 0.0615(19) 0.0420(17) -0.0188(15) -0.0210(17) 0.023(2) C22 0.0322(15) 0.0620(19) 0.075(2) -0.0147(16) 0.0074(15) 0.0056(14) C18' 0.104(3) 0.065(2) 0.0327(15) 0.0030(14) 0.0182(18) 0.011(2) C17 0.202(6) 0.0345(15) 0.0366(16) -0.0039(13) 0.009(3) 0.011(2) C3 0.072(3) 0.153(4) 0.098(3) -0.083(3) -0.043(2) 0.038(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C22' O2' C23' 115.5(2) C22* O2* C23* 115.3(2) C10 O1 C22 116.7(2) C2* N1* H1* 125.4 C13* N1* H1* 125.4 C13* N1* C2* 109.15(19) C13 N1 C3* 124.87(19) C13 N1 C2 108.9(2) C2 N1 C3* 125.32(19) C2' N1' H1' 125.0 C13' N1' H1' 125.0 C13' N1' C2' 110.0(2) C21' N4' C5' 112.9(2) C24' N4' C5' 112.3(2) C24' N4' C21' 111.2(2) C21* N4* C5* 112.4(2) C24* N4* C5* 110.7(2) C24* N4* C21* 110.4(2) N1 C13 C12 130.2(2) N1 C13 C8 107.5(2) C12 C13 C8 122.2(2) C12 C11 C10 119.7(2) C12 C11 C3' 120.4(2) C10 C11 C3' 119.7(2) N1' C2' C3' 118.3(2) C7' C2' N1' 108.4(2) C7' C2' C3' 133.3(2) C13 C12 H12 120.6 C11 C12 C13 118.7(2) C11 C12 H12 120.6 N1 C3* H3* 106.7 N1 C3* C2* 110.68(18) N1 C3* C14* 110.7(2) C2* C3* H3* 106.7 C2* C3* C14* 114.96(19) C14* C3* H3* 106.7 N1* C2* C3* 117.9(2) C7* C2* N1* 109.7(2) C7* C2* C3* 132.3(2) C13 C8 C7 107.7(2) C13 C8 C9 118.6(2) C9 C8 C7 133.7(2) C13' C8' C7' 107.1(2) C9' C8' C13' 119.3(2) C9' C8' C7' 133.6(3) N1' C13' C8' 107.7(2) N1' C13' C12' 130.5(3) C12' C13' C8' 121.8(3) C8 C7 C6 125.6(2) C2 C7 C8 107.3(2) C2 C7 C6 127.1(2) C2' C7' C8' 106.8(2) C2' C7' C6' 129.2(2) C8' C7' C6' 123.9(2) O1' C22' O2' 123.2(2) O1' C22' C16' 125.9(3) O2' C22' C16' 110.5(2) C2* C7* C8* 106.2(2) C2* C7* C6* 130.0(2) C8* C7* C6* 123.8(2) C8* C9* H9* 120.4 C10* C9* H9* 120.4 C10* C9* C8* 119.3(2) N1 C2 C16 122.0(2) C7 C2 N1 108.7(2) C7 C2 C16 129.3(2) N4 C21 H21 109.0 N4 C21 C16 113.0(2) N4 C21 C20 108.7(2) C16 C21 H21 109.0 C20 C21 H21 109.0 C20 C21 C16 108.2(2) C9* C8* C7* 133.4(2) C9* C8* C13* 119.2(2) C13* C8* C7* 107.4(2) N1* C13* C8* 107.6(2) N1* C13* C12* 130.8(2) C12* C13* C8* 121.5(2) O1 C10 C11 113.6(2) O1 C10 C9 124.6(2) C9 C10 C11 121.8(2) C11 C3' H3' 108.0 C11 C3' C14' 105.91(18) C2' C3' C11 112.01(19) C2' C3' H3' 108.0 C2' C3' C14' 114.7(2) C14' C3' H3' 108.0 C21 N4 C3 110.9(3) C5 N4 C21 117.2(2) C5 N4 C3 114.5(3) N4' C5' H5' 107.1 N4' C5' C6' 114.61(19) N4' C5' C16' 105.61(19) C6' C5' H5' 107.1 C16' C5' H5' 107.1 C16' C5' C6' 114.8(2) C7' C6' C5' 114.67(19) C7' C6' H6'A 108.6 C7' C6' H6'B 108.6 C5' C6' H6'A 108.6 C5' C6' H6'B 108.6 H6'A C6' H6'B 107.6 N4* C5* H5* 107.4 N4* C5* C16* 106.8(2) N4* C5* C6* 113.7(2) C16* C5* H5* 107.4 C16* C5* C6* 113.9(2) C6* C5* H5* 107.4 C22' C16' C5' 115.6(2) C22' C16' H16' 103.5 C22' C16' C15' 114.7(2) C5' C16' H16' 103.5 C15' C16' C5' 113.7(2) C15' C16' H16' 103.5 O1* C22* O2* 122.6(2) O1* C22* C16* 124.4(3) O2* C22* C16* 112.6(2) C5* C16* H16* 103.9 C22* C16* C5* 115.3(2) C22* C16* H16* 103.9 C22* C16* C15* 114.1(2) C15* C16* C5* 113.9(2) C15* C16* H16* 103.9 C13* C12* H12* 121.2 C11* C12* C13* 117.5(2) C11* C12* H12* 121.2 C8 C9 H9 120.6 C10 C9 C8 118.8(2) C10 C9 H9 120.6 C16* C15* H15* 107.2 C16* C15* C14* 118.7(2) C16* C15* C20* 107.5(2) C14* C15* H15* 107.2 C14* C15* C20* 108.6(2) C20* C15* H15* 107.2 N4* C21* H21A 108.9 N4* C21* H21B 108.9 N4* C21* C20* 113.5(2) H21A C21* H21B 107.7 C20* C21* H21A 108.9 C20* C21* H21B 108.9 C9* C10* H10* 119.5 C9* C10* C11* 121.0(3) C11* C10* H10* 119.5 C7* C6* C5* 117.02(19) C7* C6* H6*A 108.0 C7* C6* H6*B 108.0 C5* C6* H6*A 108.0 C5* C6* H6*B 108.0 H6*A C6* H6*B 107.3 C3* C14* C15* 116.5(2) C3* C14* H14A 108.2 C3* C14* H14B 108.2 C15* C14* H14A 108.2 C15* C14* H14B 108.2 H14A C14* H14B 107.3 C3' C14' H14C 107.6 C3' C14' H14D 107.6 C3' C14' C15' 118.8(2) H14C C14' H14D 107.1 C15' C14' H14C 107.6 C15' C14' H14D 107.6 C16' C15' C14' 119.0(2) C16' C15' H15' 107.2 C16' C15' C20' 107.9(2) C14' C15' H15' 107.2 C14' C15' C20' 107.85(19) C20' C15' H15' 107.2 C2 C16 C21 113.7(2) C2 C16 H16 107.5 C2 C16 C17 113.0(2) C21 C16 H16 107.5 C21 C16 C17 107.3(3) C17 C16 H16 107.5 C15* C20* H20* 107.0 C21* C20* C15* 110.1(2) C21* C20* H20* 107.0 C21* C20* C19* 111.7(2) C19* C20* C15* 113.5(2) C19* C20* H20* 107.0 C13' C12' H12' 121.1 C11' C12' C13' 117.8(3) C11' C12' H12' 121.1 N4' C21' H21C 108.8 N4' C21' H21D 108.8 N4' C21' C20' 113.7(2) H21C C21' H21D 107.7 C20' C21' H21C 108.8 C20' C21' H21D 108.8 C21 C20 H20 108.0 C21 C20 C15 107.5(2) C19 C20 C21 113.0(2) C19 C20 H20 108.0 C19 C20 C15 112.4(2) C15 C20 H20 108.0 C20* C19* H19A 108.6 C20* C19* H19B 108.6 H19A C19* H19B 107.5 C18* C19* C20* 114.8(3) C18* C19* H19A 108.6 C18* C19* H19B 108.6 C15' C20' H20' 106.8 C21' C20' C15' 110.3(2) C21' C20' H20' 106.8 C21' C20' C19' 113.2(2) C19' C20' C15' 112.6(2) C19' C20' H20' 106.8 C8' C9' H9' 120.3 C10' C9' C8' 119.5(3) C10' C9' H9' 120.3 C12* C11* C10* 121.4(2) C12* C11* H11* 119.3 C10* C11* H11* 119.3 C20' C19' H19C 108.7 C20' C19' H19D 108.7 H19C C19' H19D 107.6 C18' C19' C20' 114.2(2) C18' C19' H19C 108.7 C18' C19' H19D 108.7 O2* C23* H23A 109.5 O2* C23* H23B 109.5 O2* C23* H23C 109.5 H23A C23* H23B 109.5 H23A C23* H23C 109.5 H23B C23* H23C 109.5 C20 C19 H19E 109.0 C20 C19 H19F 109.0 H19E C19 H19F 107.8 C18 C19 C20 112.9(3) C18 C19 H19E 109.0 C18 C19 H19F 109.0 N4* C24* H24A 109.5 N4* C24* H24B 109.5 N4* C24* H24C 109.5 H24A C24* H24B 109.5 H24A C24* H24C 109.5 H24B C24* H24C 109.5 C7 C6 H6A 108.2 C7 C6 H6B 108.2 C7 C6 C5 116.5(3) H6A C6 H6B 107.3 C5 C6 H6A 108.2 C5 C6 H6B 108.2 C12' C11' H11' 119.2 C12' C11' C10' 121.7(3) C10' C11' H11' 119.2 N4' C24' H24D 109.5 N4' C24' H24E 109.5 N4' C24' H24F 109.5 H24D C24' H24E 109.5 H24D C24' H24F 109.5 H24E C24' H24F 109.5 C19 C18 H18A 109.5 C19 C18 H18B 109.5 C19 C18 H18C 109.5 H18A C18 H18B 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 N4 C5 C6 118.9(3) N4 C5 H5A 107.6 N4 C5 H5B 107.6 C6 C5 H5A 107.6 C6 C5 H5B 107.6 H5A C5 H5B 107.0 C20 C15 H15A 109.8 C20 C15 H15B 109.8 H15A C15 H15B 108.2 C14 C15 C20 109.5(2) C14 C15 H15A 109.8 C14 C15 H15B 109.8 C9' C10' C11' 119.9(3) C9' C10' H10' 120.1 C11' C10' H10' 120.1 O2' C23' H23D 109.5 O2' C23' H23E 109.5 O2' C23' H23F 109.5 H23D C23' H23E 109.5 H23D C23' H23F 109.5 H23E C23' H23F 109.5 C19* C18* H18D 109.5 C19* C18* H18E 109.5 C19* C18* H18F 109.5 H18D C18* H18E 109.5 H18D C18* H18F 109.5 H18E C18* H18F 109.5 C15 C14 H14 109.7 C15 C14 C17 111.5(3) C15 C14 C3 108.9(4) C17 C14 H14 109.7 C17 C14 C3 107.3(4) C3 C14 H14 109.7 O1 C22 H22A 109.5 O1 C22 H22B 109.5 O1 C22 H22C 109.5 H22A C22 H22B 109.5 H22A C22 H22C 109.5 H22B C22 H22C 109.5 C19' C18' H18G 109.5 C19' C18' H18H 109.5 C19' C18' H18I 109.5 H18G C18' H18H 109.5 H18G C18' H18I 109.5 H18H C18' H18I 109.5 C16 C17 H17A 109.7 C16 C17 H17B 109.7 C14 C17 C16 110.0(3) C14 C17 H17A 109.7 C14 C17 H17B 109.7 H17A C17 H17B 108.2 N4 C3 C14 110.5(3) N4 C3 H3A 109.6 N4 C3 H3B 109.6 C14 C3 H3A 109.6 C14 C3 H3B 109.6 H3A C3 H3B 108.1 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1* C22* 1.210(3) O1' C22' 1.193(3) O2' C22' 1.362(3) O2' C23' 1.446(3) O2* C22* 1.343(3) O2* C23* 1.442(3) O1 C10 1.374(3) O1 C22 1.422(4) N1* H1* 0.8600 N1* C2* 1.382(3) N1* C13* 1.368(3) N1 C13 1.385(3) N1 C3* 1.470(3) N1 C2 1.393(3) N1' H1' 0.8600 N1' C2' 1.391(3) N1' C13' 1.364(4) N4' C5' 1.494(3) N4' C21' 1.480(4) N4' C24' 1.450(4) N4* C5* 1.481(3) N4* C21* 1.468(4) N4* C24* 1.466(3) C13 C12 1.397(3) C13 C8 1.403(4) C11 C12 1.375(3) C11 C10 1.418(4) C11 C3' 1.530(3) C2' C7' 1.380(4) C2' C3' 1.496(3) C12 H12 0.9300 C3* H3* 0.9800 C3* C2* 1.501(3) C3* C14* 1.529(3) C2* C7* 1.379(3) C8 C7 1.425(3) C8 C9 1.413(4) C8' C13' 1.407(4) C8' C7' 1.443(3) C8' C9' 1.399(4) C13' C12' 1.402(4) C7 C2 1.379(4) C7 C6 1.499(4) C7' C6' 1.498(3) C22' C16' 1.511(3) C7* C8* 1.434(3) C7* C6* 1.505(3) C9* H9* 0.9300 C9* C8* 1.395(4) C9* C10* 1.383(4) C2 C16 1.492(3) C21 H21 0.9800 C21 N4 1.455(4) C21 C16 1.538(3) C21 C20 1.536(4) C8* C13* 1.414(3) C13* C12* 1.406(3) C10 C9 1.377(4) C3' H3' 0.9800 C3' C14' 1.545(3) N4 C5 1.449(4) N4 C3 1.472(6) C5' H5' 0.9800 C5' C6' 1.556(3) C5' C16' 1.535(4) C6' H6'A 0.9700 C6' H6'B 0.9700 C5* H5* 0.9800 C5* C16* 1.534(3) C5* C6* 1.554(3) C16' H16' 0.9800 C16' C15' 1.531(4) C22* C16* 1.515(4) C16* H16* 0.9800 C16* C15* 1.531(4) C12* H12* 0.9300 C12* C11* 1.381(4) C9 H9 0.9300 C15* H15* 0.9800 C15* C14* 1.536(3) C15* C20* 1.551(3) C21* H21A 0.9700 C21* H21B 0.9700 C21* C20* 1.538(4) C10* H10* 0.9300 C10* C11* 1.399(4) C6* H6*A 0.9700 C6* H6*B 0.9700 C14* H14A 0.9700 C14* H14B 0.9700 C14' H14C 0.9700 C14' H14D 0.9700 C14' C15' 1.547(3) C15' H15' 0.9800 C15' C20' 1.549(3) C16 H16 0.9800 C16 C17 1.548(4) C20* H20* 0.9800 C20* C19* 1.540(4) C12' H12' 0.9300 C12' C11' 1.374(5) C21' H21C 0.9700 C21' H21D 0.9700 C21' C20' 1.533(4) C20 H20 0.9800 C20 C19 1.525(4) C20 C15 1.560(4) C19* H19A 0.9700 C19* H19B 0.9700 C19* C18* 1.520(4) C20' H20' 0.9800 C20' C19' 1.538(4) C9' H9' 0.9300 C9' C10' 1.392(4) C11* H11* 0.9300 C19' H19C 0.9700 C19' H19D 0.9700 C19' C18' 1.494(4) C23* H23A 0.9600 C23* H23B 0.9600 C23* H23C 0.9600 C19 H19E 0.9700 C19 H19F 0.9700 C19 C18 1.518(4) C24* H24A 0.9600 C24* H24B 0.9600 C24* H24C 0.9600 C6 H6A 0.9700 C6 H6B 0.9700 C6 C5 1.520(4) C11' H11' 0.9300 C11' C10' 1.414(5) C24' H24D 0.9600 C24' H24E 0.9600 C24' H24F 0.9600 C18 H18A 0.9600 C18 H18B 0.9600 C18 H18C 0.9600 C5 H5A 0.9700 C5 H5B 0.9700 C15 H15A 0.9700 C15 H15B 0.9700 C15 C14 1.504(5) C10' H10' 0.9300 C23' H23D 0.9600 C23' H23E 0.9600 C23' H23F 0.9600 C18* H18D 0.9600 C18* H18E 0.9600 C18* H18F 0.9600 C14 H14 0.9800 C14 C17 1.505(6) C14 C3 1.511(7) C22 H22A 0.9600 C22 H22B 0.9600 C22 H22C 0.9600 C18' H18G 0.9600 C18' H18H 0.9600 C18' H18I 0.9600 C17 H17A 0.9700 C17 H17B 0.9700 C3 H3A 0.9700 C3 H3B 0.9700 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion O1* C22* C16* C5* 157.5(2) O1* C22* C16* C15* 22.8(3) O1' C22' C16' C5' 153.7(2) O1' C22' C16' C15' 18.3(3) O2' C22' C16' C5' -33.2(3) O2' C22' C16' C15' -168.59(19) O2* C22* C16* C5* -28.3(3) O2* C22* C16* C15* -163.0(2) O1 C10 C9 C8 -179.6(2) N1* C2* C7* C8* 0.6(3) N1* C2* C7* C6* -177.1(2) N1* C13* C12* C11* 176.6(3) N1 C13 C12 C11 -177.2(2) N1 C13 C8 C7 0.0(3) N1 C13 C8 C9 179.1(2) N1 C3* C2* N1* 51.6(3) N1 C3* C2* C7* -133.2(3) N1 C3* C14* C15* -155.2(2) N1 C2 C16 C21 133.3(2) N1 C2 C16 C17 -104.1(4) N1' C2' C7' C8' 0.7(2) N1' C2' C7' C6' 177.7(2) N1' C2' C3' C11 68.7(3) N1' C2' C3' C14' -170.57(19) N1' C13' C12' C11' 177.3(3) N4' C5' C6' C7' 161.4(2) N4' C5' C16' C22' 162.6(2) N4' C5' C16' C15' -61.6(2) N4' C21' C20' C15' 52.2(3) N4' C21' C20' C19' -75.0(3) N4* C5* C16* C22* 164.8(2) N4* C5* C16* C15* -60.5(3) N4* C5* C6* C7* 160.7(2) N4* C21* C20* C15* 54.1(3) N4* C21* C20* C19* -73.0(3) C13 N1 C3* C2* 49.7(3) C13 N1 C3* C14* -79.0(3) C13 N1 C2 C7 -0.2(3) C13 N1 C2 C16 -179.1(2) C13 C8 C7 C2 -0.1(3) C13 C8 C7 C6 -178.4(3) C13 C8 C9 C10 -1.1(4) C11 C10 C9 C8 -0.6(4) C11 C3' C14' C15' -166.3(2) C2' N1' C13' C8' -0.3(3) C2' N1' C13' C12' -178.9(2) C2' C7' C6' C5' -76.8(3) C2' C3' C14' C15' 69.6(3) C12 C13 C8 C7 -177.5(2) C12 C13 C8 C9 1.6(3) C12 C11 C10 O1 -179.0(2) C12 C11 C10 C9 1.9(4) C12 C11 C3' C2' 31.2(3) C12 C11 C3' C14' -94.5(2) C3* N1 C13 C12 -12.9(4) C3* N1 C13 C8 169.8(2) C3* N1 C2 C7 -169.9(2) C3* N1 C2 C16 11.2(3) C3* C2* C7* C8* -174.9(2) C3* C2* C7* C6* 7.4(4) C2* N1* C13* C8* -1.4(3) C2* N1* C13* C12* -179.5(3) C2* C3* C14* C15* 78.5(3) C2* C7* C8* C9* 177.2(3) C2* C7* C8* C13* -1.4(3) C2* C7* C6* C5* -75.7(4) C8 C13 C12 C11 -0.4(3) C8 C7 C2 N1 0.2(3) C8 C7 C2 C16 179.0(2) C8 C7 C6 C5 -139.3(3) C8' C13' C12' C11' -1.1(4) C8' C7' C6' C5' 99.7(3) C8' C9' C10' C11' 0.3(4) C13' N1' C2' C7' -0.3(2) C13' N1' C2' C3' 177.63(19) C13' C8' C7' C2' -0.9(3) C13' C8' C7' C6' -178.1(2) C13' C8' C9' C10' -0.4(4) C13' C12' C11' C10' 1.0(4) C7 C8 C9 C10 177.8(3) C7 C2 C16 C21 -45.4(4) C7 C2 C16 C17 77.3(4) C7 C6 C5 N4 -59.3(4) C7' C2' C3' C11 -114.0(3) C7' C2' C3' C14' 6.7(4) C7' C8' C13' N1' 0.7(3) C7' C8' C13' C12' 179.5(2) C7' C8' C9' C10' -178.5(3) C22' C16' C15' C14' 72.6(3) C22' C16' C15' C20' -164.3(2) C7* C8* C13* N1* 1.7(3) C7* C8* C13* C12* -180.0(2) C9* C8* C13* N1* -177.2(2) C9* C8* C13* C12* 1.1(4) C9* C10* C11* C12* 0.7(4) C2 N1 C13 C12 177.4(2) C2 N1 C13 C8 0.2(2) C2 N1 C3* C2* -142.3(2) C2 N1 C3* C14* 89.1(3) C2 C7 C6 C5 42.8(4) C2 C16 C17 C14 -132.2(3) C21 N4 C5 C6 70.4(4) C21 N4 C3 C14 3.1(5) C21 C16 C17 C14 -6.1(5) C21 C20 C19 C18 -168.4(2) C21 C20 C15 C14 0.7(3) C8* C7* C6* C5* 106.9(3) C8* C9* C10* C11* -0.9(4) C8* C13* C12* C11* -1.3(4) C13* N1* C2* C3* 176.7(2) C13* N1* C2* C7* 0.5(3) C13* C12* C11* C10* 0.4(4) C10 C11 C12 C13 -1.3(3) C10 C11 C3' C2' -153.5(2) C10 C11 C3' C14' 80.8(3) C3' C11 C12 C13 174.0(2) C3' C11 C10 O1 5.6(3) C3' C11 C10 C9 -173.5(2) C3' C2' C7' C8' -176.8(2) C3' C2' C7' C6' 0.2(4) C3' C14' C15' C16' -50.7(3) C3' C14' C15' C20' -173.9(2) N4 C21 C16 C2 71.3(3) N4 C21 C16 C17 -54.5(4) N4 C21 C20 C19 -64.2(3) N4 C21 C20 C15 60.3(3) C5' N4' C21' C20' -57.1(3) C5' C16' C15' C14' -63.7(3) C5' C16' C15' C20' 59.5(3) C6' C5' C16' C22' -70.2(3) C6' C5' C16' C15' 65.6(3) C5* N4* C21* C20* -58.2(3) C5* C16* C15* C14* -65.4(3) C5* C16* C15* C20* 58.2(3) C16' C5' C6' C7' 38.9(3) C16' C15' C20' C21' -51.6(3) C16' C15' C20' C19' 76.0(3) C22* C16* C15* C14* 69.9(3) C22* C16* C15* C20* -166.5(2) C16* C5* C6* C7* 38.1(3) C16* C15* C14* C3* -51.0(3) C16* C15* C20* C21* -52.0(3) C16* C15* C20* C19* 74.1(3) C9 C8 C7 C2 -179.1(3) C9 C8 C7 C6 2.6(5) C15* C20* C19* C18* 59.2(4) C21* N4* C5* C16* 58.2(3) C21* N4* C5* C6* -68.2(3) C21* C20* C19* C18* -175.6(3) C10* C9* C8* C7* -178.5(3) C10* C9* C8* C13* 0.0(4) C6* C7* C8* C9* -4.9(4) C6* C7* C8* C13* 176.5(2) C6* C5* C16* C22* -68.9(3) C6* C5* C16* C15* 65.9(3) C14* C3* C2* N1* 177.9(2) C14* C3* C2* C7* -7.0(4) C14* C15* C20* C21* 77.6(3) C14* C15* C20* C19* -156.3(2) C14' C15' C20' C21' 78.1(3) C14' C15' C20' C19' -154.3(2) C15' C20' C19' C18' 161.1(3) C16 C21 N4 C5 -77.3(3) C16 C21 N4 C3 56.8(4) C16 C21 C20 C19 172.8(2) C16 C21 C20 C15 -62.7(3) C20* C15* C14* C3* -174.1(2) C12' C11' C10' C9' -0.6(4) C21' N4' C5' C6' -69.0(3) C21' N4' C5' C16' 58.4(2) C21' C20' C19' C18' -72.9(4) C20 C21 N4 C5 162.7(3) C20 C21 N4 C3 -63.3(4) C20 C21 C16 C2 -168.3(2) C20 C21 C16 C17 65.9(3) C20 C15 C14 C17 59.7(4) C20 C15 C14 C3 -58.5(3) C9' C8' C13' N1' -177.9(2) C9' C8' C13' C12' 0.9(4) C9' C8' C7' C2' 177.4(3) C9' C8' C7' C6' 0.2(4) C23* O2* C22* O1* -11.2(3) C23* O2* C22* C16* 174.5(2) C19 C20 C15 C14 125.5(3) C24* N4* C5* C16* -177.8(2) C24* N4* C5* C6* 55.7(3) C24* N4* C21* C20* 177.7(2) C6 C7 C2 N1 178.5(3) C6 C7 C2 C16 -2.7(4) C24' N4' C5' C6' 57.7(3) C24' N4' C5' C16' -174.9(2) C24' N4' C21' C20' 175.6(2) C5 N4 C3 C14 138.4(3) C15 C20 C19 C18 69.9(3) C15 C14 C17 C16 -56.7(5) C15 C14 C3 N4 58.4(5) C23' O2' C22' O1' -5.6(3) C23' O2' C22' C16' -179.0(2) C22 O1 C10 C11 176.1(3) C22 O1 C10 C9 -4.8(4) C17 C14 C3 N4 -62.4(5) C3 N4 C5 C6 -62.1(5) C3 C14 C17 C16 62.5(5) loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.190 0.750 761 145 ' ' 2 0.500 0.448 0.250 761 144 ' '