#------------------------------------------------------------------------------ #$Date: 2019-11-11 16:44:33 +0200 (Mon, 11 Nov 2019) $ #$Revision: 226604 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/03/51/4035118.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4035118 loop_ _publ_author_name 'Wang, Xu' 'Li, Jiawei' 'Huang, Yubing' 'Zhu, Jiayi' 'Hu, Rongrong' 'Wu, Wanqing' 'Jiang, Huanfeng' _publ_section_title ; Facile Synthesis of \p-Conjugated Quinazoline-Substituted Ethenes from 2-Ethynylanilines and Benzonitriles under Transition-Metal-Free Conditions. ; _journal_issue 17 _journal_name_full 'The Journal of organic chemistry' _journal_page_first 10453 _journal_page_last 10464 _journal_paper_doi 10.1021/acs.joc.8b01494 _journal_volume 83 _journal_year 2018 _chemical_formula_moiety 'C46 H30 F6 N4' _chemical_formula_sum 'C46 H30 F6 N4' _chemical_formula_weight 752.74 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2017-06-12 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5337) ; _cell_angle_alpha 90 _cell_angle_beta 109.358(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.8214(2) _cell_length_b 16.8165(2) _cell_length_c 16.3527(3) _cell_measurement_reflns_used 8312 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 73.3820 _cell_measurement_theta_min 4.2750 _cell_volume 3585.94(10) _computing_cell_refinement 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2684 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.990 _diffrn_measured_fraction_theta_max 0.965 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -1.00 32.00 1.00 1.00 -- -40.46 37.00 -90.00 33 2 \w -51.00 -16.00 1.00 1.00 -- -40.46 37.00 -90.00 35 3 \w -70.00 34.00 1.00 1.00 -- -40.46 57.00 60.00 104 4 \w -53.00 -6.00 1.00 1.00 -- -40.46 125.00 90.00 47 5 \w 58.00 97.00 1.00 1.00 -- 40.46-125.00-120.00 39 6 \w 86.00 138.00 1.00 2.00 -- 107.48 -61.00 60.00 52 7 \w 80.00 136.00 1.00 2.00 -- 107.48 45.00 0.00 56 8 \w 103.00 157.00 1.00 2.00 -- 107.48 111.00 60.00 54 9 \w 110.00 136.00 1.00 2.00 -- 107.48 77.00 90.00 26 10 \w 77.00 155.00 1.00 2.00 -- 107.48 77.00 -60.00 78 11 \w 143.00 176.00 1.00 2.00 -- 107.48 45.00-180.00 33 12 \w 87.00 170.00 1.00 2.00 -- 107.48 45.00-150.00 83 13 \w 29.00 82.00 1.00 2.00 -- 107.48 -94.00 90.00 53 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0490985000 _diffrn_orient_matrix_UB_12 -0.0595578000 _diffrn_orient_matrix_UB_13 -0.0460823000 _diffrn_orient_matrix_UB_21 0.1063610000 _diffrn_orient_matrix_UB_22 0.0364852000 _diffrn_orient_matrix_UB_23 0.0468547000 _diffrn_orient_matrix_UB_31 0.0158630000 _diffrn_orient_matrix_UB_32 -0.0591311000 _diffrn_orient_matrix_UB_33 0.0752344000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0243 _diffrn_reflns_av_unetI/netI 0.0306 _diffrn_reflns_Laue_measured_fraction_full 0.990 _diffrn_reflns_Laue_measured_fraction_max 0.965 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 14077 _diffrn_reflns_point_group_measured_fraction_full 0.990 _diffrn_reflns_point_group_measured_fraction_max 0.965 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.546 _diffrn_reflns_theta_min 3.641 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.874 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.72570 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43f (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.394 _exptl_crystal_description block _exptl_crystal_F_000 1552 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.303 _refine_diff_density_min -0.330 _refine_diff_density_rms 0.050 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 507 _refine_ls_number_reflns 6968 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0464 _refine_ls_R_factor_gt 0.0420 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0553P)^2^+1.5988P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1086 _refine_ls_wR_factor_ref 0.1129 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6266 _reflns_number_total 6968 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL exp_645_a.res in P2(1)/n exp_645.res created by SHELXL-2016/6 at 16:57:13 on 12-Jun-2017 REM Old TITL exp_645 in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.132, Rweak 0.008, Alpha 0.023, Orientation as input REM Formula found by SHELXT: C46 N4 F6 CELL 1.54184 13.8214 16.8165 16.3527 90 109.358 90 ZERR 4 0.0002 0.0002 0.0003 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H F N UNIT 184 120 24 16 L.S. 20 PLAN 20 SIZE 0.18 0.14 0.12 BOND $H list 4 fmap 2 acta REM REM REM WGHT 0.055300 1.598800 FVAR 0.33174 F2' 3 0.781337 0.383877 1.136275 11.00000 0.03279 0.02664 = 0.02080 0.00195 0.00350 0.00156 F1' 3 0.813237 0.325057 1.031204 11.00000 0.03459 0.03787 = 0.03233 -0.00425 0.00672 0.01343 F3' 3 0.845496 0.449961 1.053617 11.00000 0.02710 0.04167 = 0.03877 0.00952 0.00261 -0.00865 F2 3 -0.313388 0.872129 0.686807 11.00000 0.02777 0.04555 = 0.05136 0.00255 0.01342 0.01291 F1 3 -0.344814 0.754421 0.633423 11.00000 0.02139 0.05862 = 0.04231 -0.00862 0.00644 -0.00405 F3 3 -0.309278 0.773262 0.770514 11.00000 0.02906 0.08208 = 0.03878 0.01326 0.01938 0.00223 N1' 4 0.376999 0.519366 0.751039 11.00000 0.02537 0.01788 = 0.01883 -0.00102 0.00753 -0.00053 N2 4 0.211598 0.795391 0.822602 11.00000 0.02252 0.01859 = 0.02062 -0.00035 0.00905 0.00010 N1 4 0.171341 0.721142 0.690048 11.00000 0.02038 0.01692 = 0.01968 0.00152 0.00797 0.00136 N2' 4 0.293005 0.439005 0.828558 11.00000 0.02540 0.01776 = 0.02136 -0.00073 0.00804 -0.00136 C9 1 0.269307 0.710160 0.702170 11.00000 0.02031 0.01491 = 0.01952 0.00332 0.00760 0.00010 C16 1 0.146850 0.762432 0.752976 11.00000 0.02177 0.01531 = 0.01984 0.00275 0.00845 0.00126 C17 1 0.035519 0.769590 0.739649 11.00000 0.02150 0.01721 = 0.02114 0.00389 0.00844 0.00187 C2 1 0.320628 0.728776 0.570232 11.00000 0.02016 0.01651 = 0.01656 -0.00214 0.00498 -0.00139 C16' 1 0.375038 0.469075 0.816282 11.00000 0.02572 0.01581 = 0.01883 -0.00220 0.00768 -0.00105 C15 1 0.313475 0.783142 0.836411 11.00000 0.02249 0.01711 = 0.02128 0.00096 0.00816 -0.00137 C1 1 0.295118 0.671225 0.629496 11.00000 0.01604 0.01998 = 0.01753 -0.00004 0.00414 0.00125 C17' 1 0.477777 0.448006 0.878610 11.00000 0.02474 0.01619 = 0.01941 -0.00206 0.00707 -0.00074 C10' 1 0.193794 0.510543 0.698342 11.00000 0.02617 0.01627 = 0.02334 -0.00207 0.00896 0.00003 C9' 1 0.288317 0.539161 0.693422 11.00000 0.02598 0.01510 = 0.01987 -0.00288 0.00867 0.00110 C10 1 0.347617 0.738611 0.777659 11.00000 0.02142 0.01718 = 0.01900 0.00183 0.00725 -0.00015 C19' 1 0.585253 0.393246 1.014968 11.00000 0.02845 0.01786 = 0.01918 0.00064 0.00805 -0.00086 AFIX 43 H19' 2 0.592062 0.368770 1.067583 11.00000 -1.20000 AFIX 0 C18 1 0.002746 0.803534 0.803896 11.00000 0.02323 0.02395 = 0.02080 -0.00047 0.00799 0.00115 AFIX 43 H18 2 0.050854 0.821222 0.855213 11.00000 -1.20000 AFIX 0 C15' 1 0.200421 0.460042 0.769278 11.00000 0.02538 0.01712 = 0.02262 -0.00204 0.00833 -0.00066 C7 1 0.410277 0.721261 0.549309 11.00000 0.01946 0.02369 = 0.02441 0.00207 0.00660 0.00237 AFIX 43 H7 2 0.454618 0.679088 0.571894 11.00000 -1.20000 AFIX 0 C20' 1 0.671804 0.412639 0.993916 11.00000 0.02530 0.01823 = 0.02128 -0.00231 0.00593 0.00032 C20 1 -0.172569 0.783939 0.715094 11.00000 0.02086 0.02743 = 0.02577 0.00434 0.00886 0.00251 C1' 1 0.295371 0.591668 0.621401 11.00000 0.02053 0.01997 = 0.01945 0.00115 0.00681 0.00136 C22' 1 0.565371 0.467300 0.858405 11.00000 0.02881 0.02369 = 0.02144 0.00364 0.01023 0.00012 AFIX 43 H22' 2 0.558884 0.492446 0.806200 11.00000 -1.20000 AFIX 0 C3 1 0.257152 0.793760 0.537185 11.00000 0.02112 0.02073 = 0.02367 0.00037 0.00884 0.00275 AFIX 43 H3 2 0.198495 0.801246 0.552172 11.00000 -1.20000 AFIX 0 C11 1 0.453615 0.725106 0.795709 11.00000 0.02235 0.02365 = 0.02176 0.00045 0.00861 -0.00046 AFIX 43 H11 2 0.476255 0.695939 0.757233 11.00000 -1.20000 AFIX 0 C2' 1 0.307218 0.549456 0.545260 11.00000 0.03371 0.01835 = 0.02220 -0.00029 0.01270 0.00065 C21' 1 0.661732 0.449340 0.915355 11.00000 0.02542 0.02477 = 0.02587 0.00143 0.01056 -0.00128 AFIX 43 H21' 2 0.719762 0.461795 0.901134 11.00000 -1.20000 AFIX 0 C14 1 0.386703 0.814124 0.912528 11.00000 0.02809 0.02363 = 0.02166 -0.00451 0.00978 -0.00410 AFIX 43 H14 2 0.365434 0.844046 0.951288 11.00000 -1.20000 AFIX 0 C22 1 -0.037185 0.741938 0.663772 11.00000 0.02376 0.02767 = 0.02170 -0.00290 0.00825 0.00250 AFIX 43 H22 2 -0.015887 0.718470 0.621123 11.00000 -1.20000 AFIX 0 C12 1 0.523054 0.755159 0.870191 11.00000 0.01976 0.02878 = 0.02506 0.00088 0.00715 -0.00244 AFIX 43 H12 2 0.592782 0.746140 0.882198 11.00000 -1.20000 AFIX 0 C18' 1 0.488613 0.410524 0.957213 11.00000 0.02502 0.01746 = 0.02156 -0.00125 0.00912 -0.00229 AFIX 43 H18' 2 0.430626 0.397010 0.971019 11.00000 -1.20000 AFIX 0 C5 1 0.369167 0.839468 0.459957 11.00000 0.02708 0.02385 = 0.02225 0.00122 0.00734 -0.00411 C14' 1 0.109194 0.431258 0.780270 11.00000 0.02821 0.02233 = 0.02886 0.00153 0.01092 -0.00297 AFIX 43 H14' 2 0.112443 0.398225 0.826718 11.00000 -1.20000 AFIX 0 C3' 1 0.255576 0.575042 0.461168 11.00000 0.02119 0.02687 = 0.02361 -0.00328 0.00564 0.00054 AFIX 43 H3' 2 0.210950 0.618042 0.452216 11.00000 -1.20000 AFIX 0 C21 1 -0.141155 0.749095 0.651235 11.00000 0.02241 0.03173 = 0.02389 -0.00105 0.00571 0.00083 AFIX 43 H21 2 -0.189406 0.730656 0.600376 11.00000 -1.20000 AFIX 0 C4 1 0.280720 0.847404 0.482096 11.00000 0.02828 0.02125 = 0.02795 0.00420 0.00853 0.00417 AFIX 43 H4 2 0.236423 0.889593 0.459473 11.00000 -1.20000 AFIX 0 C19 1 -0.100857 0.811042 0.791743 11.00000 0.02632 0.02992 = 0.02366 0.00048 0.01192 0.00385 AFIX 43 H19 2 -0.122386 0.834038 0.834501 11.00000 -1.20000 AFIX 0 C11' 1 0.096518 0.531139 0.638733 11.00000 0.02744 0.02129 = 0.02846 0.00352 0.00699 0.00079 AFIX 43 H11' 2 0.091833 0.563909 0.591760 11.00000 -1.20000 AFIX 0 C13 1 0.488964 0.799780 0.928729 11.00000 0.02509 0.03013 = 0.02195 -0.00286 0.00560 -0.00762 AFIX 43 H13 2 0.536729 0.819712 0.979036 11.00000 -1.20000 AFIX 0 C4' 1 0.269600 0.537452 0.390550 11.00000 0.02919 0.02840 = 0.02108 -0.00199 0.00749 -0.00616 AFIX 43 H4' 2 0.234227 0.555855 0.335028 11.00000 -1.20000 AFIX 0 C6 1 0.434026 0.775677 0.495461 11.00000 0.02041 0.03136 = 0.02556 0.00121 0.00933 -0.00124 AFIX 43 H6 2 0.494355 0.769639 0.482675 11.00000 -1.20000 AFIX 0 C23' 1 0.777158 0.393135 1.053596 11.00000 0.02745 0.02337 = 0.02559 0.00029 0.00794 -0.00077 C12' 1 0.009508 0.502477 0.650759 11.00000 0.02489 0.02863 = 0.03545 0.00457 0.00450 0.00069 AFIX 43 H12' 2 -0.054440 0.515987 0.611844 11.00000 -1.20000 AFIX 0 C23 1 -0.284108 0.795261 0.701486 11.00000 0.02475 0.04093 = 0.02837 0.00149 0.01072 0.00132 C13' 1 0.016202 0.452427 0.722006 11.00000 0.02475 0.02903 = 0.03888 0.00287 0.01169 -0.00382 AFIX 43 H13' 2 -0.043627 0.433581 0.729381 11.00000 -1.20000 AFIX 0 C8 1 0.395314 0.898009 0.400697 11.00000 0.03769 0.03603 = 0.04186 0.01318 0.01882 -0.00054 AFIX 137 H8A 2 0.333544 0.922243 0.363416 11.00000 -1.50000 H8B 2 0.429144 0.870760 0.366204 11.00000 -1.50000 H8C 2 0.439912 0.938316 0.434721 11.00000 -1.50000 AFIX 0 C5' 1 0.334521 0.473649 0.400637 11.00000 0.08969 0.03019 = 0.02942 0.00352 0.03071 0.01771 C7' 1 0.369164 0.483322 0.555267 11.00000 0.13827 0.04917 = 0.02748 0.01698 0.03680 0.05982 AFIX 43 H7' 2 0.401598 0.462934 0.610460 11.00000 -1.20000 AFIX 0 C6' 1 0.383760 0.446806 0.484184 11.00000 0.19269 0.06546 = 0.03611 0.02077 0.05287 0.09167 AFIX 43 H6' 2 0.427596 0.403326 0.492840 11.00000 -1.20000 AFIX 0 C8' 1 0.351596 0.436074 0.322390 11.00000 0.16059 0.05328 = 0.03553 0.00799 0.04952 0.04867 AFIX 137 H8'A 2 0.313512 0.387336 0.308244 11.00000 -1.50000 H8'B 2 0.423289 0.425166 0.335250 11.00000 -1.50000 H8'C 2 0.328813 0.471896 0.274063 11.00000 -1.50000 AFIX 0 HKLF 4 REM exp_645_a.res in P2(1)/n REM R1 = 0.0420 for 6266 Fo > 4sig(Fo) and 0.0464 for all 6968 data REM 507 parameters refined using 0 restraints END WGHT 0.0548 1.6064 REM Highest difference peak 0.303, deepest hole -0.330, 1-sigma level 0.050 Q1 1 0.3858 0.3814 0.3312 11.00000 0.05 0.30 Q2 1 0.4656 0.8974 0.4013 11.00000 0.05 0.28 Q3 1 0.3416 0.4364 0.4816 11.00000 0.05 0.27 Q4 1 0.4208 0.4627 0.4964 11.00000 0.05 0.27 Q5 1 -0.2185 0.7892 0.7103 11.00000 0.05 0.23 Q6 1 0.0171 0.7955 0.7649 11.00000 0.05 0.23 Q7 1 0.4802 0.4216 0.4987 11.00000 0.05 0.23 Q8 1 0.0803 0.7733 0.7401 11.00000 0.05 0.22 Q9 1 0.2847 0.6889 0.6636 11.00000 0.05 0.22 Q10 1 0.3168 0.8345 0.4593 11.00000 0.05 0.20 Q11 1 0.3350 0.7524 0.8140 11.00000 0.05 0.19 Q12 1 0.0931 0.7539 0.7553 11.00000 0.05 0.19 Q13 1 0.3072 0.6975 0.5974 11.00000 0.05 0.19 Q14 1 0.5217 0.4730 0.8805 11.00000 0.05 0.19 Q15 1 0.3993 0.5026 0.5601 11.00000 0.05 0.19 Q16 1 0.1536 0.4370 0.7665 11.00000 0.05 0.19 Q17 1 0.3598 0.7247 0.5585 11.00000 0.05 0.19 Q18 1 0.4363 0.4607 0.8566 11.00000 0.05 0.18 Q19 1 0.4570 0.4869 0.6338 11.00000 0.05 0.18 Q20 1 -0.1579 0.7776 0.6831 11.00000 0.05 0.18 REM The information below was added by Olex2. REM REM R1 = 0.0420 for 6266 Fo > 4sig(Fo) and 0.0464 for all 14423 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.30, deepest hole -0.33 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0464 REM R1_gt = 0.0420 REM wR_ref = 0.1129 REM GOOF = 1.033 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 14423 REM Reflections_gt = 6266 REM Parameters = n/a REM Hole = -0.33 REM Peak = 0.30 REM Flack = n/a ; _cod_data_source_file jo8b01494_si_002.cif _cod_data_source_block exp_645 _cod_database_code 4035118 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.902 _shelx_estimated_absorpt_t_min 0.859 _reflns_odcompleteness_completeness 98.99 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C19'(H19'), C18(H18), C7(H7), C22'(H22'), C3(H3), C11(H11), C21'(H21'), C14(H14), C22(H22), C12(H12), C18'(H18'), C14'(H14'), C3'(H3'), C21(H21), C4(H4), C19(H19), C11'(H11'), C13(H13), C4'(H4'), C6(H6), C12'(H12'), C13'(H13'), C7'(H7'), C6'(H6') 2.b Idealised Me refined as rotating group: C8(H8A,H8B,H8C), C8'(H8'A,H8'B,H8'C) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.351 _oxdiff_exptl_absorpt_empirical_full_min 0.702 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn F2' F 0.78134(7) 0.38388(5) 1.13627(5) 0.0281(2) Uani 1 1 d . F1' F 0.81324(7) 0.32506(6) 1.03120(6) 0.0360(2) Uani 1 1 d . F3' F 0.84550(7) 0.44996(6) 1.05362(7) 0.0379(2) Uani 1 1 d . F2 F -0.31339(7) 0.87213(7) 0.68681(7) 0.0415(3) Uani 1 1 d . F1 F -0.34481(7) 0.75442(7) 0.63342(7) 0.0418(3) Uani 1 1 d . F3 F -0.30928(8) 0.77326(8) 0.77051(7) 0.0480(3) Uani 1 1 d . N1' N 0.37700(9) 0.51937(7) 0.75104(8) 0.0206(2) Uani 1 1 d . N2 N 0.21160(9) 0.79539(7) 0.82260(8) 0.0201(2) Uani 1 1 d . N1 N 0.17134(9) 0.72114(7) 0.69005(7) 0.0187(2) Uani 1 1 d . N2' N 0.29300(9) 0.43900(7) 0.82856(8) 0.0214(2) Uani 1 1 d . C9 C 0.26931(10) 0.71016(8) 0.70217(9) 0.0180(3) Uani 1 1 d . C16 C 0.14685(10) 0.76243(8) 0.75298(9) 0.0186(3) Uani 1 1 d . C17 C 0.03552(10) 0.76959(8) 0.73965(9) 0.0196(3) Uani 1 1 d . C2 C 0.32063(10) 0.72878(8) 0.57023(9) 0.0180(3) Uani 1 1 d . C16' C 0.37504(11) 0.46908(8) 0.81628(9) 0.0200(3) Uani 1 1 d . C15 C 0.31348(11) 0.78314(8) 0.83641(9) 0.0201(3) Uani 1 1 d . C1 C 0.29512(10) 0.67123(8) 0.62950(9) 0.0182(3) Uani 1 1 d . C17' C 0.47778(11) 0.44801(8) 0.87861(9) 0.0202(3) Uani 1 1 d . C10' C 0.19379(11) 0.51054(8) 0.69834(9) 0.0217(3) Uani 1 1 d . C9' C 0.28832(11) 0.53916(8) 0.69342(9) 0.0200(3) Uani 1 1 d . C10 C 0.34762(10) 0.73861(8) 0.77766(9) 0.0191(3) Uani 1 1 d . C19' C 0.58525(11) 0.39325(8) 1.01497(9) 0.0218(3) Uani 1 1 d . H19' H 0.592062 0.368770 1.067583 0.026 Uiso 1 1 calc R C18 C 0.00275(11) 0.80353(9) 0.80390(9) 0.0225(3) Uani 1 1 d . H18 H 0.050854 0.821222 0.855213 0.027 Uiso 1 1 calc R C15' C 0.20042(11) 0.46004(8) 0.76928(9) 0.0216(3) Uani 1 1 d . C7 C 0.41028(11) 0.72126(9) 0.54931(9) 0.0227(3) Uani 1 1 d . H7 H 0.454618 0.679088 0.571894 0.027 Uiso 1 1 calc R C20' C 0.67180(11) 0.41264(8) 0.99392(9) 0.0220(3) Uani 1 1 d . C20 C -0.17257(11) 0.78394(9) 0.71509(10) 0.0244(3) Uani 1 1 d . C1' C 0.29537(10) 0.59167(9) 0.62140(9) 0.0199(3) Uani 1 1 d . C22' C 0.56537(11) 0.46730(9) 0.85840(10) 0.0242(3) Uani 1 1 d . H22' H 0.558884 0.492446 0.806200 0.029 Uiso 1 1 calc R C3 C 0.25715(11) 0.79376(8) 0.53718(9) 0.0215(3) Uani 1 1 d . H3 H 0.198495 0.801246 0.552172 0.026 Uiso 1 1 calc R C11 C 0.45361(11) 0.72511(9) 0.79571(9) 0.0223(3) Uani 1 1 d . H11 H 0.476255 0.695939 0.757233 0.027 Uiso 1 1 calc R C2' C 0.30722(12) 0.54946(9) 0.54526(10) 0.0239(3) Uani 1 1 d . C21' C 0.66173(11) 0.44934(9) 0.91536(10) 0.0248(3) Uani 1 1 d . H21' H 0.719762 0.461795 0.901134 0.030 Uiso 1 1 calc R C14 C 0.38670(11) 0.81412(9) 0.91253(9) 0.0241(3) Uani 1 1 d . H14 H 0.365434 0.844046 0.951288 0.029 Uiso 1 1 calc R C22 C -0.03719(11) 0.74194(9) 0.66377(10) 0.0242(3) Uani 1 1 d . H22 H -0.015887 0.718470 0.621123 0.029 Uiso 1 1 calc R C12 C 0.52305(11) 0.75516(9) 0.87019(10) 0.0246(3) Uani 1 1 d . H12 H 0.592782 0.746140 0.882198 0.030 Uiso 1 1 calc R C18' C 0.48861(11) 0.41052(8) 0.95721(9) 0.0210(3) Uani 1 1 d . H18' H 0.430626 0.397010 0.971019 0.025 Uiso 1 1 calc R C5 C 0.36917(11) 0.83947(9) 0.45996(9) 0.0246(3) Uani 1 1 d . C14' C 0.10919(11) 0.43126(9) 0.78027(10) 0.0261(3) Uani 1 1 d . H14' H 0.112443 0.398225 0.826718 0.031 Uiso 1 1 calc R C3' C 0.25558(11) 0.57504(9) 0.46117(9) 0.0243(3) Uani 1 1 d . H3' H 0.210950 0.618042 0.452216 0.029 Uiso 1 1 calc R C21 C -0.14116(11) 0.74909(10) 0.65124(10) 0.0265(3) Uani 1 1 d . H21 H -0.189406 0.730656 0.600376 0.032 Uiso 1 1 calc R C4 C 0.28072(12) 0.84740(9) 0.48210(10) 0.0260(3) Uani 1 1 d . H4 H 0.236423 0.889593 0.459473 0.031 Uiso 1 1 calc R C19 C -0.10086(11) 0.81104(9) 0.79174(10) 0.0257(3) Uani 1 1 d . H19 H -0.122386 0.834038 0.834501 0.031 Uiso 1 1 calc R C11' C 0.09652(12) 0.53114(9) 0.63873(10) 0.0263(3) Uani 1 1 d . H11' H 0.091833 0.563909 0.591760 0.032 Uiso 1 1 calc R C13 C 0.48896(11) 0.79978(9) 0.92873(10) 0.0263(3) Uani 1 1 d . H13 H 0.536729 0.819712 0.979036 0.032 Uiso 1 1 calc R C4' C 0.26960(12) 0.53745(9) 0.39055(10) 0.0264(3) Uani 1 1 d . H4' H 0.234227 0.555855 0.335028 0.032 Uiso 1 1 calc R C6 C 0.43403(11) 0.77568(9) 0.49546(10) 0.0254(3) Uani 1 1 d . H6 H 0.494355 0.769639 0.482675 0.030 Uiso 1 1 calc R C23' C 0.77716(12) 0.39314(9) 1.05360(10) 0.0257(3) Uani 1 1 d . C12' C 0.00951(12) 0.50248(10) 0.65076(11) 0.0310(3) Uani 1 1 d . H12' H -0.054440 0.515987 0.611844 0.037 Uiso 1 1 calc R C23 C -0.28411(12) 0.79526(11) 0.70149(11) 0.0309(3) Uani 1 1 d . C13' C 0.01620(12) 0.45243(10) 0.72201(11) 0.0306(3) Uani 1 1 d . H13' H -0.043627 0.433581 0.729381 0.037 Uiso 1 1 calc R C8 C 0.39531(14) 0.89801(11) 0.40070(12) 0.0371(4) Uani 1 1 d . H8A H 0.333544 0.922243 0.363416 0.056 Uiso 1 1 calc GR H8B H 0.429144 0.870760 0.366204 0.056 Uiso 1 1 calc GR H8C H 0.439912 0.938316 0.434721 0.056 Uiso 1 1 calc GR C5' C 0.33452(19) 0.47365(11) 0.40064(12) 0.0470(5) Uani 1 1 d . C7' C 0.3692(2) 0.48332(14) 0.55527(13) 0.0693(8) Uani 1 1 d . H7' H 0.401598 0.462934 0.610460 0.083 Uiso 1 1 calc R C6' C 0.3838(3) 0.44681(16) 0.48418(15) 0.0944(13) Uani 1 1 d . H6' H 0.427596 0.403326 0.492840 0.113 Uiso 1 1 calc R C8' C 0.3516(3) 0.43607(15) 0.32239(14) 0.0789(10) Uani 1 1 d . H8'A H 0.313512 0.387336 0.308244 0.118 Uiso 1 1 calc GR H8'B H 0.423289 0.425166 0.335250 0.118 Uiso 1 1 calc GR H8'C H 0.328813 0.471896 0.274063 0.118 Uiso 1 1 calc GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F2' 0.0328(5) 0.0266(4) 0.0208(4) 0.0020(3) 0.0035(4) 0.0016(4) F1' 0.0346(5) 0.0379(5) 0.0323(5) -0.0042(4) 0.0067(4) 0.0134(4) F3' 0.0271(5) 0.0417(6) 0.0388(6) 0.0095(4) 0.0026(4) -0.0087(4) F2 0.0278(5) 0.0455(6) 0.0514(6) 0.0025(5) 0.0134(4) 0.0129(4) F1 0.0214(5) 0.0586(7) 0.0423(6) -0.0086(5) 0.0064(4) -0.0040(4) F3 0.0291(5) 0.0821(9) 0.0388(6) 0.0133(6) 0.0194(4) 0.0022(5) N1' 0.0254(6) 0.0179(5) 0.0188(6) -0.0010(4) 0.0075(5) -0.0005(5) N2 0.0225(6) 0.0186(6) 0.0206(6) -0.0003(4) 0.0091(5) 0.0001(4) N1 0.0204(5) 0.0169(5) 0.0197(6) 0.0015(4) 0.0080(5) 0.0014(4) N2' 0.0254(6) 0.0178(6) 0.0214(6) -0.0007(5) 0.0080(5) -0.0014(5) C9 0.0203(6) 0.0149(6) 0.0195(7) 0.0033(5) 0.0076(5) 0.0001(5) C16 0.0218(7) 0.0153(6) 0.0198(7) 0.0027(5) 0.0085(5) 0.0013(5) C17 0.0215(7) 0.0172(6) 0.0211(7) 0.0039(5) 0.0084(5) 0.0019(5) C2 0.0202(6) 0.0165(6) 0.0166(6) -0.0021(5) 0.0050(5) -0.0014(5) C16' 0.0257(7) 0.0158(6) 0.0188(7) -0.0022(5) 0.0077(5) -0.0011(5) C15 0.0225(7) 0.0171(6) 0.0213(7) 0.0010(5) 0.0082(5) -0.0014(5) C1 0.0160(6) 0.0200(7) 0.0175(6) 0.0000(5) 0.0041(5) 0.0012(5) C17' 0.0247(7) 0.0162(6) 0.0194(7) -0.0021(5) 0.0071(5) -0.0007(5) C10' 0.0262(7) 0.0163(6) 0.0233(7) -0.0021(5) 0.0090(6) 0.0000(5) C9' 0.0260(7) 0.0151(6) 0.0199(7) -0.0029(5) 0.0087(5) 0.0011(5) C10 0.0214(7) 0.0172(6) 0.0190(7) 0.0018(5) 0.0073(5) -0.0001(5) C19' 0.0284(7) 0.0179(6) 0.0192(7) 0.0006(5) 0.0080(6) -0.0009(5) C18 0.0232(7) 0.0240(7) 0.0208(7) -0.0005(5) 0.0080(5) 0.0012(5) C15' 0.0254(7) 0.0171(6) 0.0226(7) -0.0020(5) 0.0083(6) -0.0007(5) C7 0.0195(6) 0.0237(7) 0.0244(7) 0.0021(6) 0.0066(6) 0.0024(5) C20' 0.0253(7) 0.0182(6) 0.0213(7) -0.0023(5) 0.0059(6) 0.0003(5) C20 0.0209(7) 0.0274(7) 0.0258(7) 0.0043(6) 0.0089(6) 0.0025(6) C1' 0.0205(6) 0.0200(7) 0.0194(7) 0.0011(5) 0.0068(5) 0.0014(5) C22' 0.0288(7) 0.0237(7) 0.0214(7) 0.0036(6) 0.0102(6) 0.0001(6) C3 0.0211(6) 0.0207(7) 0.0237(7) 0.0004(5) 0.0088(5) 0.0028(5) C11 0.0223(7) 0.0236(7) 0.0218(7) 0.0004(5) 0.0086(6) -0.0005(5) C2' 0.0337(8) 0.0184(7) 0.0222(7) -0.0003(5) 0.0127(6) 0.0006(6) C21' 0.0254(7) 0.0248(7) 0.0259(7) 0.0014(6) 0.0106(6) -0.0013(6) C14 0.0281(7) 0.0236(7) 0.0217(7) -0.0045(6) 0.0098(6) -0.0041(6) C22 0.0238(7) 0.0277(7) 0.0217(7) -0.0029(6) 0.0083(6) 0.0025(6) C12 0.0198(7) 0.0288(8) 0.0251(7) 0.0009(6) 0.0071(6) -0.0024(5) C18' 0.0250(7) 0.0175(6) 0.0216(7) -0.0012(5) 0.0091(6) -0.0023(5) C5 0.0271(7) 0.0238(7) 0.0222(7) 0.0012(6) 0.0073(6) -0.0041(6) C14' 0.0282(7) 0.0223(7) 0.0289(8) 0.0015(6) 0.0109(6) -0.0030(6) C3' 0.0212(7) 0.0269(7) 0.0236(7) -0.0033(6) 0.0056(6) 0.0005(6) C21 0.0224(7) 0.0317(8) 0.0239(7) -0.0011(6) 0.0057(6) 0.0008(6) C4 0.0283(7) 0.0212(7) 0.0279(8) 0.0042(6) 0.0085(6) 0.0042(6) C19 0.0263(7) 0.0299(8) 0.0237(7) 0.0005(6) 0.0119(6) 0.0038(6) C11' 0.0274(7) 0.0213(7) 0.0285(8) 0.0035(6) 0.0070(6) 0.0008(6) C13 0.0251(7) 0.0301(8) 0.0219(7) -0.0029(6) 0.0056(6) -0.0076(6) C4' 0.0292(7) 0.0284(8) 0.0211(7) -0.0020(6) 0.0075(6) -0.0062(6) C6 0.0204(7) 0.0314(8) 0.0256(7) 0.0012(6) 0.0093(6) -0.0012(6) C23' 0.0275(7) 0.0234(7) 0.0256(7) 0.0003(6) 0.0079(6) -0.0008(6) C12' 0.0249(7) 0.0286(8) 0.0355(9) 0.0046(7) 0.0045(6) 0.0007(6) C23 0.0248(7) 0.0409(9) 0.0284(8) 0.0015(7) 0.0107(6) 0.0013(6) C13' 0.0248(7) 0.0290(8) 0.0389(9) 0.0029(7) 0.0117(7) -0.0038(6) C8 0.0377(9) 0.0360(9) 0.0419(10) 0.0132(8) 0.0188(8) -0.0005(7) C5' 0.0897(15) 0.0302(9) 0.0294(9) 0.0035(7) 0.0307(10) 0.0177(9) C7' 0.138(2) 0.0492(12) 0.0275(10) 0.0170(9) 0.0368(12) 0.0598(15) C6' 0.193(3) 0.0655(16) 0.0361(12) 0.0208(11) 0.0529(17) 0.092(2) C8' 0.161(3) 0.0533(14) 0.0355(11) 0.0080(10) 0.0495(15) 0.0487(16) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C9' N1' C16' 117.36(12) C16 N2 C15 116.62(12) C9 N1 C16 117.08(12) C16' N2' C15' 116.25(12) N1 C9 C1 116.45(12) N1 C9 C10 122.07(12) C10 C9 C1 121.34(12) N2 C16 N1 126.57(12) N2 C16 C17 117.87(12) N1 C16 C17 115.56(12) C18 C17 C16 120.08(13) C22 C17 C16 120.67(13) C22 C17 C18 119.25(13) C7 C2 C1 121.36(12) C3 C2 C1 120.44(12) C3 C2 C7 118.15(13) N1' C16' C17' 114.80(12) N2' C16' N1' 126.65(13) N2' C16' C17' 118.55(12) N2 C15 C10 121.63(13) N2 C15 C14 119.12(13) C10 C15 C14 119.23(13) C2 C1 C9 113.64(11) C1' C1 C9 121.43(12) C1' C1 C2 124.93(12) C22' C17' C16' 119.19(13) C18' C17' C16' 121.65(13) C18' C17' C22' 119.15(13) C15' C10' C9' 116.04(13) C15' C10' C11' 119.94(13) C11' C10' C9' 124.01(14) N1' C9' C10' 121.97(13) N1' C9' C1' 115.02(12) C10' C9' C1' 122.99(13) C15 C10 C9 115.85(12) C11 C10 C9 124.25(13) C11 C10 C15 119.90(13) C20' C19' H19' 120.1 C18' C19' H19' 120.1 C18' C19' C20' 119.75(13) C17 C18 H18 119.8 C19 C18 C17 120.48(14) C19 C18 H18 119.8 N2' C15' C10' 121.72(13) N2' C15' C14' 118.91(13) C10' C15' C14' 119.36(13) C2 C7 H7 119.6 C6 C7 C2 120.89(13) C6 C7 H7 119.6 C19' C20' C21' 120.18(13) C19' C20' C23' 121.26(13) C21' C20' C23' 118.55(13) C21 C20 C19 120.61(13) C21 C20 C23 120.44(14) C19 C20 C23 118.93(14) C1 C1' C9' 120.34(12) C1 C1' C2' 124.15(13) C2' C1' C9' 115.44(12) C17' C22' H22' 119.7 C21' C22' C17' 120.52(14) C21' C22' H22' 119.7 C2 C3 H3 119.7 C4 C3 C2 120.56(13) C4 C3 H3 119.7 C10 C11 H11 120.1 C12 C11 C10 119.83(13) C12 C11 H11 120.1 C3' C2' C1' 121.11(13) C7' C2' C1' 121.41(14) C7' C2' C3' 117.48(15) C20' C21' H21' 120.0 C22' C21' C20' 119.92(14) C22' C21' H21' 120.0 C15 C14 H14 120.1 C13 C14 C15 119.70(13) C13 C14 H14 120.1 C17 C22 H22 119.7 C21 C22 C17 120.58(14) C21 C22 H22 119.7 C11 C12 H12 119.9 C11 C12 C13 120.26(13) C13 C12 H12 119.9 C17' C18' H18' 119.8 C19' C18' C17' 120.48(13) C19' C18' H18' 119.8 C4 C5 C6 117.65(13) C4 C5 C8 121.55(14) C6 C5 C8 120.79(14) C15' C14' H14' 120.2 C13' C14' C15' 119.51(14) C13' C14' H14' 120.2 C2' C3' H3' 119.5 C4' C3' C2' 121.01(14) C4' C3' H3' 119.5 C20 C21 C22 119.52(14) C20 C21 H21 120.2 C22 C21 H21 120.2 C3 C4 C5 121.46(14) C3 C4 H4 119.3 C5 C4 H4 119.3 C18 C19 C20 119.55(14) C18 C19 H19 120.2 C20 C19 H19 120.2 C10' C11' H11' 120.2 C12' C11' C10' 119.56(14) C12' C11' H11' 120.2 C14 C13 C12 121.08(14) C14 C13 H13 119.5 C12 C13 H13 119.5 C3' C4' H4' 119.2 C5' C4' C3' 121.52(15) C5' C4' H4' 119.2 C7 C6 C5 121.23(13) C7 C6 H6 119.4 C5 C6 H6 119.4 F2' C23' F1' 106.19(12) F2' C23' F3' 106.65(12) F2' C23' C20' 112.95(12) F1' C23' C20' 112.15(12) F3' C23' F1' 106.32(12) F3' C23' C20' 112.11(12) C11' C12' H12' 119.8 C11' C12' C13' 120.45(15) C13' C12' H12' 119.8 F2 C23 C20 112.42(14) F1 C23 F2 105.93(13) F1 C23 C20 112.91(13) F3 C23 F2 105.53(13) F3 C23 F1 107.01(14) F3 C23 C20 112.50(13) C14' C13' C12' 121.17(14) C14' C13' H13' 119.4 C12' C13' H13' 119.4 C5 C8 H8A 109.5 C5 C8 H8B 109.5 C5 C8 H8C 109.5 H8A C8 H8B 109.5 H8A C8 H8C 109.5 H8B C8 H8C 109.5 C4' C5' C6' 117.46(16) C4' C5' C8' 120.22(17) C6' C5' C8' 122.31(19) C2' C7' H7' 119.5 C2' C7' C6' 120.95(18) C6' C7' H7' 119.5 C5' C6' C7' 121.47(19) C5' C6' H6' 119.3 C7' C6' H6' 119.3 C5' C8' H8'A 109.5 C5' C8' H8'B 109.5 C5' C8' H8'C 109.5 H8'A C8' H8'B 109.5 H8'A C8' H8'C 109.5 H8'B C8' H8'C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance F2' C23' 1.3430(18) F1' C23' 1.3470(18) F3' C23' 1.3435(18) F2 C23 1.352(2) F1 C23 1.340(2) F3 C23 1.3388(19) N1' C16' 1.3687(18) N1' C9' 1.3173(19) N2 C16 1.3149(19) N2 C15 1.3658(18) N1 C9 1.3149(17) N1 C16 1.3735(18) N2' C16' 1.3162(19) N2' C15' 1.3711(19) C9 C1 1.4998(18) C9 C10 1.4278(19) C16 C17 1.4857(19) C17 C18 1.397(2) C17 C22 1.392(2) C2 C1 1.4922(19) C2 C7 1.3962(19) C2 C3 1.3934(19) C16' C17' 1.4904(19) C15 C10 1.4167(19) C15 C14 1.418(2) C1 C1' 1.345(2) C17' C22' 1.395(2) C17' C18' 1.394(2) C10' C9' 1.419(2) C10' C15' 1.416(2) C10' C11' 1.417(2) C9' C1' 1.5008(19) C10 C11 1.4136(19) C19' H19' 0.9300 C19' C20' 1.389(2) C19' C18' 1.387(2) C18 H18 0.9300 C18 C19 1.385(2) C15' C14' 1.417(2) C7 H7 0.9300 C7 C6 1.383(2) C20' C21' 1.390(2) C20' C23' 1.496(2) C20 C21 1.387(2) C20 C19 1.392(2) C20 C23 1.495(2) C1' C2' 1.4887(19) C22' H22' 0.9300 C22' C21' 1.382(2) C3 H3 0.9300 C3 C4 1.388(2) C11 H11 0.9300 C11 C12 1.373(2) C2' C3' 1.391(2) C2' C7' 1.380(2) C21' H21' 0.9300 C14 H14 0.9300 C14 C13 1.370(2) C22 H22 0.9300 C22 C21 1.388(2) C12 H12 0.9300 C12 C13 1.414(2) C18' H18' 0.9300 C5 C4 1.392(2) C5 C6 1.395(2) C5 C8 1.507(2) C14' H14' 0.9300 C14' C13' 1.369(2) C3' H3' 0.9300 C3' C4' 1.385(2) C21 H21 0.9300 C4 H4 0.9300 C19 H19 0.9300 C11' H11' 0.9300 C11' C12' 1.369(2) C13 H13 0.9300 C4' H4' 0.9300 C4' C5' 1.373(2) C6 H6 0.9300 C12' H12' 0.9300 C12' C13' 1.415(2) C13' H13' 0.9300 C8 H8A 0.9600 C8 H8B 0.9600 C8 H8C 0.9600 C5' C6' 1.385(3) C5' C8' 1.514(2) C7' H7' 0.9300 C7' C6' 1.387(3) C6' H6' 0.9300 C8' H8'A 0.9600 C8' H8'B 0.9600 C8' H8'C 0.9600 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 2 887.92 21.39 0 0 3 0.13 0.09 0 0 3 0.11 0.15 0 0 4 256.64 6.52 0 0 4 285.76 7.52 0 0 5 0.1 0.09 0 0 5 -0.13 0.22 0 0 6 430.28 10.62 0 0 6 447.43 12.19 0 0 7 0.73 0.41 0 0 8 74.82 3.83 0 0 9 0.28 0.42 0 0 10 68.86 4.2 0 0 10 73.65 3.94 0 0 11 -0.26 0.5 0 0 12 379.89 10.5 0 0 12 351.65 13.15 0 0 13 -0.27 0.42 0 0 13 0.36 0.9 0 0 14 2.91 0.59 0 0 15 0.07 0.3 0 0 18 17.67 1.13 0 0 19 -0.11 0.19 0 -1 1 160.71 4.08 0 -1 -1 167.12 4.15 0 -1 2 143.16 3.73 0 -1 2 152.32 4.11 0 -1 3 593 14.33 0 -1 3 605.85 14.95 0 -1 4 644.53 16.18 0 -1 4 624.36 15.26 0 1 4 652.15 16.32 0 -1 5 85.64 2.52 0 1 5 88.97 3.51 0 -1 5 89.22 3.42 0 1 6 197.48 6.53 0 1 6 189.81 5.11 0 -1 6 196.9 5.12 0 -1 6 211.27 6.51 0 1 7 23.8 1.91 0 -1 7 28.56 2.02 0 -1 8 10.56 1.31 0 1 8 9.9 1.35 0 -1 9 6.59 1.06 0 -1 9 4.67 0.93 0 1 9 5.66 1.1 0 1 10 95.91 5.07 0 -1 10 88.33 4.78 0 -1 10 87.43 4.55 0 -1 11 17.24 2.11 0 -1 11 15.18 1.81 0 1 11 17.02 2.16 0 1 12 -0.01 0.55 0 1 12 0.44 0.3 0 -1 12 0.36 0.29 0 1 13 27.2 1.72 0 1 13 26.27 3.01 0 -1 13 26.87 1.78 0 1 14 97.97 3.79 0 -1 14 95.24 3.83 0 -1 15 3.68 0.67 0 -1 18 -0.38 0.27 0 1 18 0.25 0.27 0 1 19 9.3 0.66 0 -1 19 9.52 0.65 0 -2 0 725.75 17.48 0 -2 1 375.52 9.18 0 -2 -1 366.26 9.3 0 -2 -2 904.38 22.67 0 -2 2 957.8 22.28 0 -2 2 943.05 22.52 0 -2 3 1913.89 45.73 0 -2 3 1908.65 45.16 0 -2 4 433.33 10.88 0 -2 4 450.32 11.66 0 -2 5 8.67 0.58 0 -2 5 8.74 0.92 0 2 6 59.42 3.02 0 -2 6 60.72 2.86 0 -2 6 57.24 2.78 0 -2 6 54.91 1.94 0 -2 7 2.51 0.64 0 2 7 2.22 0.65 0 -2 7 1.58 0.54 0 2 8 8.91 1.29 0 -2 8 10.38 1.29 0 -2 8 9.66 1.25 0 -2 9 500.07 15.19 0 -2 9 519.59 15.16 0 2 9 513.16 15.64 0 -2 10 1.77 0.75 0 -2 10 3.76 0.9 0 2 10 1.53 0.73 0 -2 11 40.97 3.15 0 -2 11 40.68 2.13 0 2 11 36.71 3.29 0 2 12 1.84 0.48 0 2 12 4.57 1.32 0 2 12 4.01 0.62 0 -2 12 3.23 0.61 0 -2 13 12.9 1.21 0 2 13 16.06 1.26 0 2 14 68.11 2.91 0 -2 14 68.85 3.11 0 -2 15 1.58 0.49 0 -2 18 13.37 0.93 0 2 18 11.18 0.89 0 2 19 0.37 0.18 0 -3 0 5.66 0.5 0 -3 -1 922.52 23.7 0 -3 1 1031.57 23.66 0 -3 2 120.13 3.05 0 -3 2 123.84 3.59 0 -3 -2 131.09 3.84 0 -3 3 1150.62 27.68 0 -3 4 1768.62 43.48 0 -3 4 1807.79 42.75 0 -3 5 327.1 8.64 0 -3 5 342.21 9.63 0 -3 6 48.12 2.58 0 -3 6 43.8 1.78 0 3 7 195.6 7.28 0 -3 7 208.93 7.11 0 3 8 168.79 6.87 0 -3 8 177.2 6.67 0 3 9 37.56 2.97 0 -3 9 40.26 2.87 0 -3 10 3.76 0.93 0 3 10 4.32 1.11 0 -3 11 48.11 3.6 0 3 11 57.94 4.22 0 -3 11 55.78 2.58 0 3 12 98.07 4.09 0 -3 12 94.29 3.78 0 3 12 93.84 5.82 0 3 13 95.35 3.96 0 -3 13 83.04 3.59 0 -3 14 42.94 2.36 0 -3 15 12.29 1.17 0 -3 18 51.43 2 0 3 18 50.41 2.07 0 -4 0 9999 234.29 0 -4 -1 176.59 5.24 0 -4 1 179.42 5.17 0 -4 2 5116.19 122 0 -4 -2 5275.57 122.34 0 -4 3 21.55 1.2 0 -4 4 1.09 0.27 0 -4 4 1.45 0.47 0 -4 5 0.91 0.26 0 -4 5 0.5 0.27 0 -4 6 230.15 6.64 0 -4 6 238.73 7.7 0 -4 7 1.27 0.54 0 4 8 0.77 0.57 0 -4 8 0.05 0.47 0 4 9 115.52 5.82 0 -4 9 124.18 5.71 0 -4 10 47.6 3.49 0 4 10 54.49 3.91 0 -4 11 63.4 2.81 0 4 11 63.71 3.11 0 -4 11 57.22 4.05 0 4 11 56.61 4.28 0 -4 12 14.22 2.04 0 -4 12 15.21 1.3 0 4 12 17.73 2.44 0 4 12 15.17 1.4 0 -4 13 0.72 0.38 0 4 13 0.53 0.44 0 4 14 23.29 1.77 0 -4 14 24.34 1.7 0 -4 15 3.07 0.63 0 4 17 16.11 1.14 0 4 18 0.41 0.24 0 -4 18 0.75 0.27 0 -5 0 0.31 0.24 0 -5 1 2864.66 67.08 0 -5 -1 2809.7 67.06 0 -5 1 2753.91 66.89 0 -5 2 3271.39 79.91 0 -5 -2 3254.77 79.89 0 -5 3 1673.25 39.17 0 -5 -3 1551.14 39.5 0 -5 3 1609.43 39.59 0 -5 4 20.1 1.28 0 -5 4 19.06 1.5 0 -5 5 0.98 0.32 0 -5 5 0.8 0.41 0 -5 6 16.14 1.57 0 -5 6 16.49 1.21 0 -5 7 82.85 4.1 0 -5 7 75.39 3.06 0 5 8 331.3 11.42 0 -5 8 326.49 10.96 0 5 9 58.72 4.01 0 -5 9 62.5 3.93 0 -5 10 2.07 0.49 0 -5 10 1.56 0.81 0 5 10 1.16 0.79 0 -5 11 64.11 2.87 0 -5 11 58.97 4.23 0 5 11 67.49 3.27 0 5 11 61.03 4.5 0 -5 12 25.3 2.79 0 5 12 26.03 1.94 0 -5 12 25.31 1.71 0 5 12 26.45 3 0 -5 13 9.67 1.01 0 5 13 10.21 1.21 0 -5 14 11.64 1.17 0 5 14 10.74 1.18 0 -5 15 67.73 2.97 0 5 15 63.21 2.99 0 5 17 2.96 0.49 0 -5 17 2.1 0.39 0 5 18 0.02 0.19 0 -6 0 2502.74 60.2 0 -6 1 1273.04 31.34 0 -6 -1 1266.71 31.53 0 -6 -2 65.88 2.99 0 -6 2 68.68 2.86 0 -6 2 63.79 2.96 0 -6 3 3.36 0.58 0 -6 -3 3.67 0.71 0 -6 3 3.43 0.65 0 -6 4 5.02 0.83 0 -6 4 5.86 0.74 0 -6 5 46.49 2.74 0 -6 5 51.13 2.45 0 -6 6 9.15 0.96 0 -6 6 10.71 1.34 0 -6 7 389.22 12.32 0 -6 7 390.03 10.95 0 -6 8 127.51 5.88 0 6 9 68.59 4.58 0 -6 9 83.05 4.71 0 -6 10 39.59 2.08 0 -6 10 36.85 3.2 0 6 10 41.14 3.58 0 6 10 41.04 2.48 0 -6 11 0.28 0.33 0 6 11 0.55 0.38 0 6 11 -0.1 0.6 0 -6 11 0.07 0.58 0 -6 12 3.76 0.66 0 6 12 2.49 0.7 0 6 13 0.38 0.51 0 -6 13 0.76 0.43 0 6 14 8.95 1.1 0 -6 14 8.9 1 0 -6 15 36.62 2.06 0 6 15 34.34 2.07 0 6 16 3.5 0.57 0 6 17 6.73 0.65 0 -7 0 1.55 0.45 0 -7 -1 74.87 3.4 0 -7 1 77.78 3.32 0 -7 -2 57.11 2.97 0 -7 2 56.06 2.73 0 -7 -3 143.64 5.51 0 -7 3 150.56 5.19 0 -7 3 141.35 5.34 0 -7 4 188.81 6.72 0 -7 4 200.5 6.46 0 -7 5 71.53 3.24 0 -7 5 70.81 3.63 0 -7 6 222.97 7.17 0 -7 6 219.63 7.99 0 -7 7 4.49 1 0 -7 7 5.35 0.84 0 -7 8 58.33 3.83 0 7 9 153.92 5.72 0 -7 9 162.29 7.24 0 7 9 150.46 7.39 0 -7 10 78 4.94 0 7 10 77.6 3.71 0 -7 10 80.8 3.24 0 7 10 74.29 5.04 0 7 11 37.01 3.58 0 7 11 40.61 2.55 0 -7 11 40.02 2.16 0 -7 11 39.48 3.49 0 -7 12 2.52 0.57 0 7 12 2.87 0.75 0 -7 13 33.59 1.99 0 7 13 30 2.14 0 7 14 1.03 0.52 0 -7 14 1.76 0.5 0 7 15 2.37 0.52 0 7 15 1.83 0.48 0 7 16 16.03 1.16 0 7 16 15.6 1.08 0 7 17 1.85 0.36 0 -8 0 120.86 4.8 0 -8 1 29.33 2.04 0 -8 -1 27.91 2.07 0 -8 -2 371.73 11.29 0 -8 2 369.45 10.94 0 -8 3 88.53 3.89 0 -8 -3 87.5 4.21 0 -8 4 190.5 6.87 0 -8 4 190 6.58 0 -8 5 383.18 11.18 0 -8 5 361.69 11.56 0 -8 6 8.5 1.13 0 -8 6 8.4 1.25 0 -8 7 86.18 3.96 0 -8 7 86.24 4.67 0 -8 8 399.36 13.39 0 -8 9 254.12 9.81 0 8 9 232.07 7.99 0 -8 9 246.36 7.26 0 8 10 107.54 6.42 0 -8 10 111.07 6.1 0 -8 10 115.31 4.13 0 8 10 106.48 4.69 0 -8 11 3.46 0.64 0 8 11 3.92 0.85 0 8 12 37.83 2.46 0 -8 12 36.39 2.1 0 -8 13 29.76 1.83 0 8 13 29.14 1.76 0 8 13 27.83 2.06 0 8 14 37.35 2.27 0 -8 14 37.18 2.07 0 8 14 39.66 2.02 0 8 15 2.69 0.49 0 8 15 3.27 0.61 0 8 16 32.25 1.67 0 -9 0 0.21 0.42 0 -9 1 10.69 1.28 0 -9 -1 11.21 1.39 0 -9 2 498.8 14.25 0 -9 -2 481.28 14.54 0 -9 3 35.08 2.45 0 -9 4 234.91 8.07 0 -9 5 6.29 1 0 -9 6 4.67 0.95 0 -9 6 5.1 1.06 0 -9 7 75.54 4.47 0 -9 7 80.16 3.99 0 -9 -8 8.44 0.86 0 -9 8 8.58 1.51 0 9 8 9.94 1.24 0 -9 -9 260.67 7.71 0 -9 9 273.69 7.82 0 -9 9 247.26 10.22 0 9 9 271.08 8.84 0 9 10 210.71 7.44 0 -9 10 215.6 6.54 0 9 10 198.55 9.45 0 -9 -10 202.43 6.34 0 -9 -11 0.38 0.25 0 -9 11 0.7 0.36 0 9 11 0.02 0.42 0 9 12 3.26 0.78 0 -9 12 2.46 0.51 0 -9 13 1.79 0.47 0 9 13 1.54 0.54 0 9 14 8.64 1.04 0 9 15 16.65 1.28 0 9 16 20.04 1.22 0 -10 0 85.99 4.38 0 -10 -1 15.68 1.75 0 -10 1 15.42 1.7 0 -10 2 13.78 1.6 0 -10 -2 12.18 1.63 0 -10 3 29.48 2.39 0 -10 4 27.87 2.33 0 -10 5 3.97 0.86 0 -10 6 7.82 1.24 0 10 6 7.5 1.1 0 -10 -7 4 0.61 0 10 7 3.92 0.81 0 10 8 146.22 5.75 0 -10 -8 140.79 4.81 0 -10 9 106.1 3.8 0 10 9 97.82 4.54 0 -10 -9 95.48 3.69 0 -10 -10 121.01 4.29 0 10 10 118.84 5.17 0 -10 10 124.52 4.37 0 -10 11 3.2 0.61 0 10 11 2.37 0.66 0 -10 -11 4.58 0.64 0 10 12 4.3 0.86 0 -10 12 4.68 0.7 0 10 13 28.23 2.02 0 10 14 5.01 0.76 0 10 15 23.59 1.49 0 10 16 2.16 0.37 0 -11 0 2.94 0.93 0 -11 1 1.4 0.66 0 -11 -1 1.96 0.65 0 -11 2 97.53 5.01 0 -11 3 312.3 10.79 0 -11 4 0.64 0.48 0 -11 -5 13.32 1.15 0 -11 5 15.24 1.81 0 11 5 12.84 1.42 0 -11 -6 232.06 7.08 0 11 6 228.21 8 0 -11 6 247.39 9 0 -11 -7 3.71 0.62 0 11 7 3.96 0.86 0 11 8 11.51 1.44 0 -11 -8 12.49 1.13 0 -11 -9 54.13 2.53 0 11 9 52.21 3.18 0 11 10 69.5 3.68 0 -11 -10 65.53 2.84 0 11 11 0.63 0.47 0 -11 -11 0.97 0.36 0 11 12 37.41 2.45 0 11 13 7.39 1 0 11 14 18.74 1.42 0 11 15 31.82 1.68 0 -12 0 378.6 12.92 0 -12 1 83.53 4.83 0 -12 2 188.98 8.01 0 -12 2 192.88 6.42 0 -12 3 51.79 2.68 0 -12 -3 49.41 2.45 0 -12 3 47.86 3.58 0 -12 4 0.67 0.42 0 -12 4 1.03 0.54 0 -12 -4 0.77 0.34 0 12 4 0.41 0.37 0 -12 5 23.95 2.5 0 -12 -5 23.29 1.6 0 12 5 22.22 1.92 0 -12 6 -0.09 0.65 0 -12 -6 0.34 0.39 0 12 6 0.25 0.51 0 -12 -7 364.78 10.46 0 12 7 382.36 11.71 0 12 8 275.03 9.24 0 -12 -8 269.17 8.07 0 -12 -9 205.76 6.46 0 12 9 207.81 7.54 0 -12 -10 97.22 3.66 0 12 10 98.67 4.56 0 12 11 5.16 0.97 0 -12 -11 5.47 0.7 0 12 12 1.62 0.56 0 12 13 19.73 1.55 0 12 14 0.69 0.38 0 12 15 3.85 0.5 0 -13 0 -0.09 0.29 0 -13 1 15.5 1.37 0 -13 -1 14.86 1.27 0 -13 1 18.04 2.21 0 -13 2 0.38 0.5 0 -13 2 0.83 0.43 0 13 3 32.79 2.38 0 -13 3 35.73 3.23 0 -13 3 37.17 2.29 0 -13 4 39.91 3.41 0 13 4 34.63 2.53 0 -13 5 66.34 4.46 0 -13 -5 63.26 2.93 0 13 5 63.77 3.55 0 13 6 260.57 8.83 0 -13 -6 248.14 7.68 0 13 7 28.45 2.3 0 -13 -7 23.22 1.65 0 13 8 19.47 1.87 0 -13 -8 18.25 1.4 0 13 9 151.99 5.27 0 -13 -9 138.57 4.87 0 13 9 150.47 5.98 0 -13 -10 5.47 0.72 0 13 10 7.53 1.09 0 13 11 29.85 2.12 0 13 12 30.07 2.01 0 13 13 0.19 0.29 0 13 14 0.36 0.31 0 -14 0 123.75 4.74 0 -14 -1 299.67 8.99 0 -14 1 302.69 9.26 0 -14 2 23.47 1.8 0 14 2 22.61 2 0 -14 3 0.59 0.38 0 14 3 0.37 0.48 0 14 4 186.85 7.02 0 14 5 4.7 0.97 0 14 6 36.36 2.65 0 14 7 2.96 0.82 0 14 8 223.77 7.94 0 14 9 143.76 5.12 0 14 9 154.52 5.91 0 14 10 29.46 2.14 0 14 11 41.54 2.42 0 14 12 4.28 0.7 0 14 13 3.33 0.55 0 14 14 0.92 0.26 0 -15 0 0.64 0.38 0 -15 1 39.34 2.37 0 -15 -1 43.29 2.39 0 15 1 38.32 2.7 0 -15 2 19.68 1.66 0 15 2 21.12 1.94 0 15 3 38.09 2.67 0 15 4 6.67 1.12 0 15 5 102.06 4.74 0 15 6 39.37 2.71 0 15 7 6.32 1.08 0 15 8 66 3.47 0 15 8 65.05 3.09 0 15 9 1.58 0.44 0 15 9 1.06 0.54 0 15 10 36.43 2.27 0 15 11 0.52 0.45 0 15 12 0 0.26 0 15 13 3.77 0.5 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2 -5 10 16.75 2 2 -5 11 257.49 7.98 2 5 11 275.46 11.23 2 -5 12 28.56 1.9 2 -5 13 52.27 2.6 2 -5 14 45.75 2.38 2 -5 15 127.21 4.44 2 5 17 8.07 0.66 2 -5 17 7.31 0.57 -2 6 18 6.84 0.65 -2 6 17 44.53 2.07 -2 6 16 1.16 0.44 -2 6 16 1.6 0.44 -2 6 15 0.42 0.39 -2 6 15 0.12 0.34 -2 6 14 24.51 1.71 -2 6 14 21.96 1.82 -2 -6 13 4 0.69 -2 6 13 3.51 0.78 -2 -6 12 2.67 0.6 -2 6 12 3.11 1.14 -2 -6 12 1.63 0.91 -2 6 12 0.98 0.49 -2 -6 11 6.86 1.39 -2 6 11 6.26 0.98 -2 -6 11 6.05 0.79 -2 6 11 3.66 1.09 -2 6 10 78.58 4.84 -2 -6 10 78.5 4.82 -2 6 10 78.12 3.6 -2 6 9 0.44 0.45 -2 -6 9 0.49 0.59 -2 -6 8 131.73 5.95 -2 -6 7 5.64 1.03 -2 -6 6 12.04 1.11 -2 -6 6 11.77 1.41 -2 -6 5 243.63 7.38 2 -6 -5 232.51 7.42 -2 -6 5 237.49 7.97 -2 -6 5 247.62 6.7 -2 -6 4 51.04 2.7 2 -6 -4 48.96 2.49 -2 -6 4 49.64 2.44 -2 -6 3 625.85 16.65 -2 -6 3 622.66 15.87 2 -6 -3 658.62 16.73 -2 -6 3 646.3 16.88 -2 -6 2 3.76 0.63 -2 -6 2 3.5 0.62 2 -6 -2 3.56 0.6 -2 -6 2 3.52 0.5 -2 -6 1 51.48 2.45 2 -6 -1 55.98 2.56 2 -6 0 12.04 1.06 2 -6 1 13.44 1.16 2 -6 2 189.35 6.08 2 -6 3 183.62 6.01 2 -6 4 132.76 4.82 2 -6 5 12.01 1.2 2 -6 5 11.95 1.33 2 -6 6 50.99 3.12 2 -6 6 52.87 2.76 2 -6 7 6.94 0.95 2 -6 7 8.36 1.3 2 6 8 3.17 0.97 2 -6 8 3.12 0.85 2 -6 9 595.18 17.71 2 -6 9 579.9 15.24 2 6 9 579.57 15.82 2 -6 10 4.85 0.75 2 6 10 5.45 1.47 2 6 10 4.73 0.82 2 -6 11 21.54 1.58 2 6 11 22.59 1.78 2 -6 12 59.62 2.83 2 -6 13 69.67 3.12 2 -6 14 14.12 1.19 2 -6 15 7.09 0.81 2 6 16 0.48 0.2 -2 7 18 15.24 0.89 -2 7 17 2.87 0.47 -2 7 17 3.81 0.58 -2 7 16 37.1 2.15 -2 7 16 36.23 1.91 -2 7 15 10.39 1.04 -2 7 15 9.82 1.23 -2 7 14 3.02 0.72 -2 7 14 2.35 0.49 -2 7 13 22.7 1.63 -2 7 13 20.23 1.8 -2 7 12 42.88 2.66 -2 7 12 42.75 2.27 -2 -7 12 39.76 2.2 -2 7 12 38.63 3.63 -2 -7 11 3.02 0.58 -2 7 11 2.56 0.95 -2 7 11 2.81 0.64 -2 -7 11 4.26 1.26 -2 7 10 15.02 1.47 -2 7 10 14.03 2.01 -2 -7 10 14.41 2.04 -2 -7 10 16.6 1.25 -2 -7 9 14.96 1.95 -2 -7 8 280.69 10.16 -2 -7 7 2.16 0.7 -2 -7 6 1453.37 36.81 -2 -7 6 1518.79 38.02 -2 -7 5 12.58 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13.27 1.63 -4 5 8 0.06 0.45 -4 -5 8 -0.07 0.22 -4 -5 7 0.24 0.32 4 -5 -6 183.8 5.74 4 -5 -5 18.21 1.31 -4 5 5 19.97 1.64 -4 -5 4 14.39 1.19 -4 -5 4 15.15 1.34 -4 5 4 15.31 1.32 4 -5 -4 14.05 1.13 -4 -5 3 116.69 4.21 -4 -5 3 110.84 4.1 -4 5 3 117.58 4.12 4 -5 -3 108.76 4.05 -4 -5 2 589.47 15.5 -4 -5 2 627.71 15.86 -4 5 2 619.41 15.44 -4 -5 1 8.4 0.76 -4 5 1 7.13 0.68 4 -5 -1 6.9 0.84 -4 5 0 21.99 1.11 4 -5 0 20.24 1.48 4 -5 1 0.4 0.29 4 -5 2 110.72 4.32 4 -5 3 604.98 16.34 4 -5 4 4.65 0.8 4 -5 5 6.65 0.97 4 -5 6 4.53 0.83 4 5 6 3.66 0.98 4 -5 7 65.66 3.41 4 5 7 59.28 4.08 4 5 8 1.17 0.71 4 -5 8 0.23 0.27 4 -5 9 102.26 4.02 4 5 9 92.47 5.7 4 -5 10 0.81 0.41 4 -5 11 6.17 0.87 4 -5 12 9.47 1.05 4 -5 13 8.2 0.94 4 -5 14 0.22 0.31 4 -5 15 0.01 0.21 4 5 16 17.32 0.9 -4 6 19 74.28 2.48 -4 6 18 0.75 0.34 -4 6 17 7.09 0.8 -4 6 17 8.03 0.98 -4 6 16 15.21 1.41 -4 6 16 14.33 1.25 -4 6 15 -0.02 0.41 -4 6 15 0.28 0.42 -4 6 14 50.2 2.91 -4 6 14 49.34 2.6 -4 6 13 12.24 1.22 -4 6 13 12 1.35 -4 6 12 32.4 1.95 -4 6 12 29.87 2.95 -4 -6 12 33.21 3.28 -4 6 12 29.7 2.14 -4 6 11 6.53 1.43 -4 6 11 7.29 1.02 -4 6 11 7.93 0.91 -4 -6 11 6.04 1.36 -4 -6 10 17.09 2.19 -4 6 10 21.91 2.28 -4 6 10 21.79 1.73 -4 -6 9 4 1.01 -4 6 9 3.29 0.93 -4 -6 8 357.53 11.85 -4 -6 7 294.06 10.24 -4 -6 7 319.69 9.2 -4 -6 6 1.09 0.53 4 -6 -6 0.65 0.3 4 -6 -5 13.69 1.18 -4 -6 5 9.14 1.18 -4 -6 4 193.88 5.97 4 -6 -4 173.33 5.95 -4 -6 4 184.27 6.38 -4 -6 3 764.82 20.86 4 -6 -3 804.41 20.81 -4 -6 2 38.11 2.14 -4 6 2 40.7 1.98 -4 -6 2 34.05 2 4 -6 -2 33.84 2.01 4 -6 -1 444.08 12.51 -4 -6 1 426.38 11.82 4 -6 0 -0.04 0.34 4 -6 1 251.39 7.87 4 -6 2 49.2 2.68 4 -6 3 19.57 1.65 4 -6 4 53.47 2.97 4 -6 5 29.67 2.16 4 6 6 119.56 6.07 4 -6 6 130.85 5.28 4 -6 7 83.76 3.39 4 6 7 73.4 4.75 4 -6 7 78.61 3.94 4 -6 8 15.37 1.3 4 6 8 12.56 2.03 4 -6 9 304.55 9.09 4 6 9 303.9 11.91 4 -6 10 52.08 2.68 4 -6 11 7.51 0.99 4 -6 12 25.08 1.74 4 -6 13 2.32 0.53 4 -6 14 50.63 2.26 4 -6 15 81.58 2.93 -4 -6 -15 84.96 2.77 -4 7 18 2.6 0.43 -4 7 17 0.24 0.37 -4 7 17 -0.14 0.27 -4 7 16 1.86 0.49 -4 7 16 0.9 0.32 -4 7 15 19.38 1.7 -4 7 15 18.08 1.46 -4 7 14 113.77 4.85 -4 7 14 118.54 4.44 -4 7 13 1.82 0.65 -4 7 13 1.04 0.43 -4 7 12 76.58 3.75 -4 7 12 73.04 4.93 -4 7 12 76.27 3.3 -4 -7 11 5.54 1.37 -4 7 11 4.47 1.33 -4 7 11 4.92 0.87 -4 7 11 6.13 0.83 -4 -7 10 11.18 1.77 -4 7 10 9.76 0.98 -4 7 10 10.22 1.22 -4 7 10 10.86 1.71 -4 7 9 11.51 1.65 -4 -7 9 11.29 1.68 -4 -7 8 5.57 1.08 -4 -7 7 264.35 9.39 -4 -7 6 52.44 3.25 4 -7 -6 56.47 2.92 -4 -7 5 0.27 0.33 4 -7 -5 0.92 0.42 4 -7 -4 130.09 5.03 -4 -7 4 139.34 5.37 -4 -7 4 138.08 4.83 -4 -7 3 14.58 1.3 -4 -7 3 18.15 1.59 4 -7 -3 17.26 1.45 -4 -7 2 280.55 8.42 4 -7 -2 268.86 8.46 -4 -7 2 277.29 8.33 4 -7 -1 10.98 1.16 4 -7 0 111.63 4.47 4 -7 1 6.06 0.93 4 -7 2 9.65 1.24 4 -7 3 1.48 0.54 4 -7 4 1 0.45 4 -7 5 1.15 0.52 4 -7 6 1.46 0.58 4 -7 7 7.61 1.17 4 -7 7 6.42 0.85 4 7 7 6.85 1.39 4 7 8 176.52 8.51 4 -7 8 199.45 6.35 4 7 9 60.71 4.66 4 -7 9 67.11 3.03 4 -7 10 8.58 1.01 4 -7 11 1.63 0.44 4 -7 12 60.8 2.81 4 -7 13 26.35 1.64 4 -7 14 79.86 3 -4 -7 -14 79.94 2.92 4 -7 15 14.16 0.95 -4 8 18 2.69 0.36 -4 8 17 1.07 0.36 -4 8 17 1.23 0.42 -4 8 16 20.02 1.36 -4 8 16 20.47 1.59 -4 8 15 0.68 0.5 -4 8 15 1.16 0.46 -4 8 14 116.75 4.89 -4 8 14 118.25 4.39 -4 8 13 41.97 2.32 -4 8 13 44.46 2.78 -4 8 12 11.19 1.34 -4 8 12 7.86 0.93 -4 -8 11 67.83 4.83 -4 8 11 71.36 3.08 -4 8 11 70.91 4.8 -4 8 11 68.64 3.55 -4 -8 10 -0.03 0.5 -4 8 10 1.13 0.65 -4 8 10 0.53 0.35 -4 8 10 0.9 0.54 -4 8 10 0.88 0.33 -4 -8 9 3.06 0.95 -4 8 9 3.06 0.63 -4 8 9 3.64 0.76 -4 -8 8 -0.31 0.6 -4 -8 7 313.17 10.93 -4 -8 6 49.64 3.29 4 -8 -6 51.27 2.9 -4 -8 5 65.19 3.66 4 -8 -5 61.22 3.25 -4 -8 4 16.78 1.35 4 -8 -4 15.76 1.57 -4 -8 4 17.27 1.67 4 -8 -3 74.26 3.68 -4 -8 3 76.51 3.33 -4 -8 3 75.28 3.59 4 -8 -2 64.19 3.3 -4 -8 2 58.48 2.96 4 -8 -1 15.63 1.49 4 -8 0 108.17 4.62 4 -8 1 2.83 0.72 4 -8 2 454.08 13.36 4 -8 3 4.11 0.9 4 -8 4 19.61 1.86 4 -8 5 135.05 5.75 4 -8 6 91.08 3.53 4 -8 6 91.84 4.55 4 8 6 83.61 3.87 4 8 7 187.35 6.52 4 -8 7 182.49 5.94 4 8 7 169.66 8.25 4 -8 8 1.56 0.39 4 8 8 2.38 1.04 4 8 8 2.59 0.7 4 -8 9 144.97 5.08 4 -8 10 6.69 0.87 4 -8 11 19.89 1.48 4 -8 12 24.17 1.57 -4 -8 -13 0.36 0.27 4 -8 13 0.57 0.33 -4 -8 -14 0.16 0.22 4 -8 14 0.02 0.22 -4 9 17 0.24 0.24 -4 9 16 5.75 0.81 -4 9 16 6.65 0.71 -4 9 15 1.16 0.59 -4 9 15 1.44 0.42 -4 9 14 3.38 0.77 -4 9 14 3.92 0.65 -4 9 13 53.16 2.57 -4 9 13 52.24 3.02 -4 9 12 19.23 1.81 -4 9 12 18.1 1.4 -4 9 11 76.59 3.83 -4 9 11 76.13 3.33 -4 -9 10 53.24 4.16 -4 9 10 57.4 2.84 -4 9 10 57.35 3.21 -4 9 10 60.45 4.39 -4 -9 9 34.73 3.19 -4 9 9 37.78 2.48 -4 9 9 37.32 2.18 -4 -9 8 22.23 2.47 -4 -9 8 21.82 1.61 -4 9 8 22.33 1.82 -4 9 8 19.8 1.56 -4 -9 7 3.41 0.91 4 -9 -6 340.9 10.73 -4 -9 6 320.52 11.23 -4 -9 5 107.69 5.19 4 -9 -5 120.08 5.11 4 -9 -4 35.52 2.52 -4 -9 4 32.94 2.49 4 -9 -3 76.65 3.97 -4 -9 3 71.12 3.69 4 -9 -2 172.3 6.56 -4 -9 2 175.56 6.14 4 -9 -1 272.01 9.06 4 -9 0 1.63 0.57 4 -9 1 5.63 1 4 -9 2 128.1 5.55 4 -9 3 100.72 4.87 4 -9 4 47.1 3.15 4 -9 5 61.27 3.72 4 9 5 57.46 3.12 4 -9 6 70.72 4.1 4 -9 6 73.48 3.02 4 9 6 67.56 3.49 4 -9 7 311.67 8.96 4 9 7 294.5 11.99 4 9 7 308.46 9.75 4 -9 8 36.92 2.05 4 9 8 34.29 2.35 4 9 9 79.73 3.74 4 -9 9 78.87 3.32 4 -9 10 10.06 1.03 4 -9 11 156.85 5.22 4 -9 12 5.26 0.7 -4 -9 -12 6.99 0.8 -4 -9 -13 6.12 0.69 4 -9 13 6.08 0.67 -4 -9 -14 0.78 0.26 4 -9 14 0.76 0.26 -4 10 17 8.25 0.78 -4 10 16 2.23 0.49 -4 10 15 251.65 7.89 -4 10 14 19.09 1.66 -4 10 13 20.82 1.83 -4 10 12 1.95 0.67 -4 10 11 52.69 2.69 -4 10 11 51.75 3.07 -4 10 10 37.87 2.25 -4 10 10 35.1 2.46 -4 10 10 33.5 3.41 -4 -10 9 5.41 1.29 -4 10 9 8.12 1.02 -4 10 9 7.84 1.12 -4 -10 8 24.53 2.63 -4 -10 8 27.72 1.92 -4 10 8 26.69 1.88 -4 10 8 29.39 2.13 -4 -10 7 29.29 1.94 -4 10 7 29.81 1.96 -4 10 7 29.78 2.13 -4 -10 7 30.27 2.82 -4 -10 6 11.7 1.15 -4 -10 6 9.84 1.51 -4 10 6 11.65 1.21 4 -10 -6 13.46 1.65 -4 -10 5 6.19 1.19 4 -10 -5 4.4 0.93 4 -10 -4 20.01 1.98 4 -10 -3 28.27 2.35 4 -10 -2 86.28 4.42 4 -10 -1 72.4 3.99 -4 -10 1 70.05 3.54 4 -10 0 316.02 10.6 4 -10 1 3.78 0.92 4 -10 2 24.42 2.25 -4 -10 -3 2.58 0.48 4 -10 3 2.07 0.67 4 -10 4 18.18 2.02 4 -10 5 30.42 2.67 4 10 5 27.45 2.11 4 -10 6 122.02 5.78 4 10 6 100.72 4.67 4 -10 7 466.35 12.35 4 10 7 434.6 13.32 4 -10 8 226.41 6.77 4 10 8 204.42 7.47 4 -10 9 6.8 0.81 4 10 9 6.21 0.99 4 -10 10 144.16 4.82 4 10 10 139.5 5.26 -4 -10 -10 141.74 4.95 4 -10 11 50.79 2.3 -4 -10 -11 47.4 2.34 4 -10 12 46.08 2.06 -4 -10 -12 43.18 2.06 -4 -10 -13 1.05 0.3 4 -10 13 0.71 0.27 -4 11 17 -0.13 0.21 -4 11 16 85.38 3.25 -4 11 15 0.41 0.41 -4 11 14 33.33 2.17 -4 11 13 2.63 0.71 -4 11 12 5.57 1.02 -4 11 11 -0.09 0.32 -4 11 11 0.07 0.5 -4 11 10 116.21 5.15 -4 11 10 128.14 4.82 -4 11 9 1.08 0.51 -4 11 9 0.67 0.51 -4 -11 8 0.7 0.84 -4 -11 8 1.54 0.54 -4 11 8 0.42 0.33 -4 11 8 0.43 0.52 -4 -11 7 2.33 0.9 -4 -11 7 3.19 0.69 -4 11 7 3.53 0.7 -4 11 7 2.68 0.62 -4 -11 6 8 1.01 4 -11 -6 6.09 1.24 -4 11 6 7.98 1.03 -4 11 6 8.62 1.14 -4 -11 5 35.36 2.13 4 -11 -5 38.92 3.03 4 -11 -4 3.98 1.04 -4 -11 4 4.65 0.72 -4 -11 3 1.76 0.45 4 -11 -3 1.44 0.59 -4 -11 2 2.41 0.51 4 -11 -2 1.83 0.68 4 -11 -1 5.33 1.1 -4 -11 1 5.46 0.78 4 -11 0 169.01 7.2 -4 -11 0 178.09 5.71 -4 -11 0 172.61 5.59 -4 -11 -1 3.13 0.58 -4 -11 -1 3.19 0.59 4 -11 1 2.49 0.81 4 -11 2 74.34 4.36 -4 -11 -2 70.69 2.99 -4 -11 -2 70.36 3 -4 -11 -3 3.83 0.64 -4 -11 -3 2.88 0.55 4 -11 3 2.76 0.96 -4 -11 -4 8.07 0.93 4 -11 4 7.84 1.34 -4 -11 -4 7.23 0.84 4 -11 5 50.18 3.62 4 11 5 45.65 2.94 -4 -11 -5 48.21 2.44 -4 -11 -6 6.38 0.85 4 11 6 7.74 1.22 4 11 7 339.94 10.88 -4 -11 -7 348.06 9.97 -4 -11 -8 0.04 0.45 4 11 8 1.12 0.55 4 -11 9 11.04 0.97 4 11 9 10.48 1.26 -4 -11 -9 10.38 1.07 -4 -11 -10 6.33 0.82 4 -11 10 5.5 0.67 -4 -11 -10 6.03 0.71 4 11 10 5.08 0.79 -4 -11 -11 0.09 0.27 4 -11 11 -0.01 0.22 -4 -11 -12 26.36 1.46 4 -11 12 27.96 1.42 -4 -11 -13 9.42 0.73 -4 12 16 1.02 0.36 -4 12 15 -0.07 0.28 -4 12 14 0.34 0.39 -4 12 13 21 1.7 -4 12 12 69.19 2.98 -4 12 12 66.42 3.41 -4 12 11 52.65 2.7 -4 12 11 53.64 3.07 -4 12 10 41.28 2.67 -4 12 10 37.39 2.32 -4 12 9 41.05 2.51 -4 12 9 39.9 2.67 -4 12 8 22.96 1.95 -4 12 8 17.87 1.61 -4 -12 7 14.69 1.47 -4 12 7 11.94 1.32 -4 12 7 14.95 1.59 -4 -12 6 21.58 1.73 -4 12 6 17.52 1.59 -4 12 6 18.44 1.73 4 -12 -5 0.21 0.79 -4 12 5 0.69 0.58 -4 -12 5 0.11 0.47 -4 12 5 0.54 0.4 -4 -12 4 1.85 0.49 4 -12 -4 1.28 0.73 -4 -12 3 61.02 2.92 4 -12 -3 52.84 3.77 -4 -12 2 15.25 1.35 4 -12 -2 16.64 1.99 4 -12 -1 0.49 0.6 -4 -12 1 0.42 0.39 -4 -12 0 118.12 4.38 4 -12 0 118.44 5.88 -4 12 0 113.96 4.47 -4 -12 0 118.29 4.3 4 -12 1 30.5 2.82 -4 -12 -1 28.73 1.82 -4 -12 -1 29.83 1.83 4 -12 2 186.59 7.97 -4 -12 -2 180.75 5.98 -4 -12 -2 190.55 6.07 4 -12 3 26.58 2.63 -4 -12 -3 27.17 1.73 -4 -12 -3 27.26 1.77 4 -12 4 18.11 2.22 -4 -12 -4 19.8 1.45 4 12 4 20.11 1.91 -4 -12 -4 18.27 1.44 -4 -12 -5 1.96 0.56 -4 -12 -5 2.49 0.59 4 12 5 1.63 0.6 -4 -12 -6 94.32 3.71 -4 -12 -6 99.41 3.88 4 12 6 98.68 4.64 -4 -12 -7 118.19 4.3 4 12 7 125.32 5.31 -4 -12 -7 126.72 4.57 -4 -12 -8 22.59 1.47 4 12 8 20.66 1.9 -4 -12 -8 23.71 1.63 -4 -12 -9 22.03 1.38 4 12 9 21.26 1.75 -4 -12 -9 20.06 1.47 -4 -12 -10 3.33 0.58 4 12 10 2.2 0.6 4 12 11 44.19 2.17 -4 -12 -11 46.56 2.09 -4 -12 -12 5.48 0.58 -4 13 15 1.71 0.38 -4 13 14 13.95 1.19 -4 13 13 9.15 1.06 -4 13 12 1.96 0.43 -4 13 12 1.7 0.64 -4 13 11 165.53 5.65 -4 13 11 167.5 6.13 -4 13 10 10.78 1.2 -4 13 10 9.41 1.24 -4 13 9 108.74 4.8 -4 13 9 112.54 4.61 -4 13 8 9.48 1.27 -4 13 8 9.92 1.22 -4 -13 7 41.07 2.55 -4 13 7 43.46 2.68 -4 13 7 45.93 2.81 -4 -13 6 2.18 0.63 -4 13 6 2.02 0.63 -4 13 6 2.69 0.72 -4 -13 5 4.79 0.84 -4 13 5 3.99 0.83 4 -13 -5 3.64 1.17 -4 13 5 4.86 0.92 -4 -13 4 13.14 1.33 -4 13 4 11.68 1.33 4 -13 -4 9.64 1.63 -4 -13 3 30.97 2.03 4 -13 -3 26.76 2.76 -4 13 3 29.26 2.09 -4 -13 2 31.81 2.05 4 -13 -2 31.72 3.01 4 -13 -1 4.37 1.21 -4 13 1 3.69 0.69 -4 -13 1 5.55 0.83 -4 -13 0 2.95 0.63 -4 13 0 2.91 0.65 4 -13 0 3.15 1.07 -4 -13 -1 34.2 2.06 4 -13 1 33.55 3.08 -4 -13 -1 36.61 2.09 -4 -13 -2 21.32 1.55 -4 -13 -2 20.34 1.52 -4 -13 -3 62.13 2.87 -4 -13 -3 63.06 2.92 -4 -13 -4 0.02 0.4 -4 -13 -4 -0.07 0.29 4 13 4 0.59 0.55 4 13 5 60.62 3.49 -4 -13 -5 56.43 2.67 -4 -13 -5 59.68 2.8 -4 -13 -6 136.27 4.72 -4 -13 -6 136.18 4.88 4 13 6 138.56 5.77 -4 -13 -7 279.48 8.13 4 13 7 281.3 9.25 -4 -13 -7 279.95 8.33 4 13 8 17.16 1.64 -4 -13 -8 16.73 1.21 -4 -13 -8 16.88 1.32 4 13 9 12.91 1.3 -4 -13 -9 15.3 1.07 -4 -13 -9 13.43 1.12 4 13 10 0.18 0.29 -4 -13 -10 0.91 0.34 -4 -13 -11 42.75 1.87 4 13 11 42.84 1.98 -4 14 15 32.26 1.47 -4 14 14 0.36 0.28 -4 14 13 4.78 0.68 -4 14 12 0.83 0.32 -4 14 12 1.35 0.46 -4 14 11 1.36 0.41 -4 14 11 0.98 0.46 -4 14 10 0.24 0.38 -4 14 10 -0.28 0.41 -4 14 9 32.34 2.15 -4 14 9 34.98 2.38 -4 14 8 64.6 3.28 -4 14 8 68.05 3.5 -4 14 7 7.64 1.1 -4 14 7 8.62 1.19 -4 -14 6 31.05 2.19 -4 14 6 28.76 2.12 -4 14 6 29.46 2.18 -4 -14 5 40.28 2.52 -4 14 5 36.29 2.48 -4 14 5 41.67 2.61 -4 -14 4 1.01 0.56 -4 14 4 0.45 0.36 -4 -14 3 -0.18 0.47 -4 14 3 0.11 0.4 -4 -14 2 49.19 2.68 -4 14 2 48.24 2.72 -4 -14 1 17.97 1.52 -4 14 1 15.52 1.47 -4 -14 0 66.77 3.18 -4 14 0 72.03 3.34 -4 -14 -1 -0.36 0.46 -4 -14 -2 60.66 2.83 -4 -14 -2 53.8 2.7 -4 -14 -3 0.6 0.32 4 14 3 0.05 0.56 -4 -14 -3 0.07 0.45 -4 -14 -4 2.53 0.52 4 14 4 2.25 0.78 -4 -14 -4 2.4 0.52 -4 -14 -5 210.85 6.64 4 14 5 216.43 7.81 -4 -14 -5 218.62 6.82 -4 -14 -6 122.57 4.3 4 14 6 115.58 5.13 -4 -14 -6 123.95 4.45 -4 -14 -7 57.06 2.49 4 14 7 61.05 3.27 -4 -14 -7 57.64 2.66 -4 -14 -8 22.32 1.32 4 14 8 20.48 1.71 -4 -14 -8 18.86 1.35 4 14 9 1.61 0.45 -4 -14 -9 1.98 0.42 4 14 10 0.51 0.29 -4 -14 -10 1.12 0.36 -4 15 14 11.99 0.83 -4 15 13 106.75 3.67 -4 15 12 34.12 1.63 -4 15 12 35.15 1.92 -4 15 11 4.88 0.68 -4 15 11 3.81 0.71 -4 15 10 51.52 2.51 -4 15 10 45.77 2.56 -4 15 9 56.3 2.86 -4 15 9 56.6 2.96 -4 15 8 0.22 0.43 -4 15 8 0.29 0.47 -4 15 7 5.43 0.97 -4 15 7 3.42 0.77 -4 -15 6 43.17 2.61 -4 15 6 48.88 2.76 -4 15 6 43.33 2.66 -4 -15 5 12.66 1.36 -4 15 5 11.46 1.35 -4 -15 4 -0.09 0.56 -4 15 4 -0.16 0.47 -4 15 3 2.55 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5 1 6 8.06 1.16 5 -1 6 9.81 1.24 5 1 7 349.41 11.72 5 1 7 362.7 11.31 5 -1 7 355.1 11.15 5 1 8 0.61 0.29 5 -1 8 0.15 0.29 5 1 8 0.15 0.46 5 -1 9 115.11 4.47 5 1 9 114.15 4.36 5 1 9 120.1 6.1 5 1 10 9.19 1.06 5 -1 10 8.59 1.06 5 -1 11 21.02 1.61 5 1 11 21.03 1.56 5 1 12 23.93 1.6 5 -1 12 22.51 1.61 5 1 13 64.47 2.73 5 -1 13 67.41 2.87 5 1 14 10.67 0.88 5 -1 14 9.57 0.89 5 -1 15 10.35 0.79 -5 2 20 33.62 1.46 -5 -2 19 30.16 1.48 -5 2 19 31.45 1.61 -5 -2 18 2.21 0.48 -5 2 18 2 0.49 -5 2 17 12.42 1.21 -5 -2 17 11.29 1.06 -5 2 16 3.09 0.6 -5 -2 16 2.52 0.53 -5 2 15 82.61 3.62 -5 2 15 78.31 3.76 -5 -2 15 82.01 3.45 -5 2 14 4.28 0.86 -5 2 14 4.61 0.76 -5 -2 14 4.12 0.68 -5 2 13 111.4 5.68 -5 2 13 96.91 4.25 -5 2 13 103.84 4.08 -5 -2 13 98.46 3.88 -5 -2 12 257.3 7.63 -5 2 12 264.52 9.68 -5 2 12 251.95 8.13 -5 2 12 256.29 7.8 -5 2 11 161.45 6.74 -5 -2 10 327.23 10.77 -5 2 10 321.01 10.51 -5 2 9 236.49 7.98 -5 -2 9 236.63 8.22 -5 2 9 227.29 8.47 -5 -2 8 123.96 5.18 -5 2 8 140.19 5.77 -5 2 8 138.31 5.11 -5 -2 7 1.93 0.55 -5 2 7 1.96 0.65 -5 2 7 1.64 0.47 -5 2 6 6.18 0.71 5 -2 -6 5.13 0.56 -5 2 5 45.47 1.9 5 -2 -5 43.86 1.97 -5 2 5 42.61 2.31 -5 -2 4 0.01 0.23 -5 2 4 0.56 0.19 5 -2 -4 0.52 0.24 5 -2 -3 1.51 0.39 -5 -2 3 1.45 0.42 -5 -2 2 292.43 8.32 5 -2 -2 271.87 8.13 -5 2 1 114.92 3.96 5 -2 -1 111.18 4.08 -5 -2 1 107.19 4.08 5 -2 0 0.23 0.29 -5 2 0 0.76 0.3 5 2 1 151.06 4.63 -5 2 -1 142.69 4.81 5 -2 1 154.18 5.26 5 2 2 504.7 13.72 5 -2 2 524.96 14.29 -5 2 -2 536.25 13.93 5 2 3 17.7 1.41 5 -2 3 15.58 1.44 5 2 4 326.69 10 5 -2 4 335.53 10.09 5 -2 5 65.63 3.36 5 2 5 62.47 3.4 5 2 6 -0.31 0.4 5 -2 6 0.02 0.26 5 -2 7 45.42 2.83 5 2 7 37.04 2.9 5 2 7 40.14 2.79 5 -2 8 46.29 2.52 5 2 8 47.89 2.44 5 2 8 54.05 3.72 5 -2 9 13.37 1.27 5 2 9 13.84 2.01 5 2 9 14.85 1.26 5 2 10 215.91 6.83 5 -2 10 220.05 7.16 5 2 11 57.27 2.65 5 -2 11 54.64 2.77 5 -2 12 2.96 0.62 5 2 12 2.91 0.54 5 -2 13 84.37 3.37 5 2 13 82.39 3.11 5 -2 14 0.89 0.34 5 -2 15 4.99 0.57 -5 3 20 9.88 0.7 -5 -3 19 21.28 1.13 -5 3 19 20.95 1.27 -5 -3 18 6.72 0.71 -5 3 18 7.48 0.85 -5 3 17 -0.88 0.57 -5 -3 17 0.52 0.33 -5 3 16 7.6 0.98 -5 -3 16 7.51 0.88 -5 3 15 114.15 4.82 -5 3 15 126.08 4.71 -5 -3 15 118.79 4.39 -5 -3 14 -0.02 0.32 -5 3 14 0.28 0.44 -5 3 14 0.88 0.47 -5 -3 13 27.66 3.04 -5 3 13 30.61 2.87 -5 3 13 30.48 2.13 -5 3 13 31.85 1.99 -5 -3 13 29.27 1.8 -5 3 12 20.51 2.25 -5 3 12 19.35 1.65 -5 3 12 20.17 1.51 -5 -3 12 19.12 1.39 -5 3 11 484.29 15.15 -5 3 11 492.57 13.75 -5 3 11 498.47 13.32 -5 3 10 3.13 0.84 -5 -3 10 3.46 0.81 -5 -3 9 696.38 19.59 -5 3 9 729.7 19.66 -5 -3 8 51.54 2.89 -5 3 8 53.55 2.86 -5 3 8 52.93 3.25 -5 3 7 192.91 6.89 -5 3 7 192.27 6.3 -5 -3 7 179.97 6.38 -5 3 6 6.86 0.81 -5 3 6 5.56 0.91 5 -3 -6 7.06 0.72 -5 3 5 10.52 1.11 -5 3 5 11.14 0.93 5 -3 -5 10.92 0.91 -5 -3 4 34.63 1.99 5 -3 -4 34.29 1.79 -5 3 4 30.96 1.86 -5 -3 3 18.82 1.43 5 -3 -3 19.89 1.37 -5 -3 2 15.62 1.36 5 -3 -2 16.21 1.26 5 -3 -1 9.64 0.99 -5 3 0 64.63 2.61 5 -3 0 66.35 3.01 5 -3 1 114.39 4.42 -5 3 -1 118.01 4.01 -5 3 -2 668.96 17.09 5 -3 2 664.8 17.82 -5 3 -3 167.71 5.37 5 3 3 165.21 5.86 5 -3 3 165.38 5.92 5 3 4 17.92 1.64 5 -3 4 19.53 1.67 5 3 5 22.66 2.01 5 -3 5 22.03 1.86 5 -3 6 99.99 4.55 5 3 6 106.43 5.1 5 3 7 156 6.38 5 3 7 156.49 6.89 5 -3 7 156.56 6.14 5 -3 8 1.26 0.4 5 3 8 1.65 0.78 5 -3 9 -0.3 0.33 5 3 9 1.36 0.83 5 -3 10 0.56 0.3 5 -3 11 68.1 3.23 5 -3 12 54.07 2.65 5 -3 13 68.18 2.93 5 -3 14 3.34 0.55 5 -3 15 15.57 1.01 -5 4 19 23.5 1.31 -5 -4 18 3.78 0.52 -5 4 18 3.86 0.59 -5 4 17 0.95 0.43 -5 -4 17 0.49 0.31 -5 4 16 41.24 2.3 -5 4 16 36.39 2.35 -5 -4 16 36.82 1.97 -5 4 15 131.31 4.85 -5 -4 15 122.69 4.46 -5 4 15 126.72 5.08 -5 4 14 182.26 6.63 -5 4 14 189.96 6.35 -5 -4 14 184.88 5.97 -5 -4 13 0.83 0.64 -5 4 13 0.39 0.33 -5 4 13 0.31 0.35 -5 -4 13 0.61 0.35 -5 -4 12 25.03 2.79 -5 4 12 26.82 2.61 -5 4 12 34.05 2.31 -5 4 12 31.25 1.94 -5 -4 12 31.44 1.77 -5 4 11 0.77 0.54 -5 4 11 0.02 0.38 -5 4 11 0.59 0.43 -5 -4 10 37.28 2.65 -5 4 10 33.53 2.63 -5 4 9 5.83 1.02 -5 -4 9 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13 4.54 0.66 5 -5 14 3.26 0.5 5 -5 15 27.88 1.35 -5 -5 -15 28.13 1.25 -5 6 19 10.51 0.75 -5 6 18 30.93 1.61 -5 6 17 48.48 2.5 -5 6 17 45.27 2.24 -5 6 16 14.95 1.46 -5 6 16 18.3 1.41 -5 6 15 36.43 2.38 -5 6 15 35.77 2.16 -5 6 14 0.3 0.43 -5 6 14 1.54 0.52 -5 6 13 0.25 0.39 -5 6 13 0.59 0.48 -5 -6 12 62.78 4.63 -5 6 12 56.57 4.09 -5 6 12 63.28 3.28 -5 6 12 65.05 2.98 -5 -6 11 26.4 2.81 -5 6 11 27.2 1.99 -5 6 11 28.14 2.66 -5 6 11 26.12 1.72 -5 -6 10 92.68 5.4 -5 6 10 100.2 5.21 -5 6 10 103.66 4.26 -5 6 10 105.74 3.89 -5 -6 9 145.93 6.76 -5 6 9 157.58 6.53 -5 -6 8 174.63 6.14 -5 -6 8 158.02 6.89 -5 6 8 175.29 6.79 -5 -6 7 0.27 0.35 -5 -6 7 -0.34 0.48 5 -6 -6 225.22 6.99 -5 -6 6 201.05 7.58 -5 -6 5 19.58 1.76 -5 6 5 20.67 1.74 -5 -6 5 21.48 1.67 5 -6 -5 20.27 1.56 -5 -6 4 112.46 4.56 -5 -6 4 119.38 4.51 -5 6 4 112.55 4.45 5 -6 -4 109.21 4.32 -5 -6 3 0.26 0.26 5 -6 -3 0.89 0.36 -5 6 3 0.34 0.21 -5 -6 2 5.72 0.77 5 -6 -2 5.49 0.82 -5 6 2 6.4 0.76 -5 -6 2 5.82 0.9 -5 6 1 385.94 10.31 5 -6 -1 377.26 11.13 5 -6 0 148.27 5.51 5 -6 1 51.34 2.84 5 -6 2 252.54 8.31 5 -6 3 24.34 1.99 5 -6 4 15.21 1.6 5 6 5 112.86 5.7 5 -6 5 121.07 5.21 5 6 6 9.18 1.58 5 -6 6 10.16 1.34 5 -6 6 6.68 0.83 5 -6 7 3.38 0.64 5 6 7 3.69 1.2 5 -6 7 3.99 0.82 5 -6 8 30.75 1.97 5 6 8 23.61 2.69 5 -6 9 3.64 0.7 5 -6 10 72.04 3.25 5 -6 11 3.2 0.62 5 -6 12 17.98 1.38 5 -6 13 0.39 0.32 5 -6 14 7 0.73 5 -6 15 43.05 1.72 -5 7 18 7.96 0.72 -5 7 17 1.88 0.5 -5 7 17 2.4 0.51 -5 7 16 25.18 1.82 -5 7 16 20.8 1.5 -5 7 15 0.38 0.45 -5 7 15 0.13 0.33 -5 7 14 4.17 0.9 -5 7 14 3.8 0.71 -5 7 13 303.21 9.46 -5 7 13 284.9 8.78 -5 7 12 18.39 1.7 -5 7 12 16.9 1.42 -5 -7 11 30.06 3.03 -5 7 11 32.68 2.99 -5 7 11 29.07 1.85 -5 7 11 32.17 2.21 -5 7 11 29.72 1.85 -5 -7 10 59.62 4.32 -5 7 10 72.08 4.4 -5 7 10 72.29 3.14 -5 7 10 71.57 3.47 -5 7 10 72.96 3.09 -5 -7 9 0.81 0.67 -5 7 9 -0.16 0.6 -5 -7 8 5.64 1.14 -5 -7 7 11.95 1.61 -5 -7 6 19.5 1.95 5 -7 -6 23.96 1.83 5 -7 -5 62.23 3.13 -5 -7 5 51.5 3.15 -5 -7 5 57.75 2.92 -5 -7 4 6.69 0.97 -5 -7 4 8.89 1.12 5 -7 -4 7.35 1 -5 -7 3 35.8 2.34 -5 -7 3 43.97 2.47 5 -7 -3 37.97 2.41 -5 -7 2 7.19 1.02 5 -7 -2 10.32 1.19 5 -7 -1 156.25 5.87 5 -7 0 713.74 19.3 5 -7 1 31.55 2.26 5 -7 2 82.59 3.99 5 -7 3 125.29 5.32 5 -7 4 3.1 0.77 5 -7 5 52.77 3.28 5 7 6 78.63 4.89 5 -7 6 80.03 3.4 5 -7 6 77.14 4.17 5 -7 7 152.05 5.26 5 7 7 132.95 7 5 -7 8 10.14 1.11 5 -7 9 61.53 2.96 5 -7 10 3.18 0.63 5 -7 11 26.71 1.75 5 -7 12 1.01 0.4 5 -7 13 35.25 1.81 5 -7 14 10.76 0.84 -5 -7 -14 10.66 0.82 -5 8 18 0.22 0.18 -5 8 17 17.89 1.17 -5 8 17 21.58 1.47 -5 8 16 3.73 0.71 -5 8 16 3.3 0.57 -5 8 15 1.22 0.54 -5 8 15 1.99 0.49 -5 8 14 35.96 2.36 -5 8 14 29.25 1.9 -5 8 13 154.09 5.98 -5 8 13 160.82 5.5 -5 8 12 119.24 5 -5 8 12 120.38 4.47 -5 8 11 0.33 0.29 -5 -8 11 0.9 0.77 -5 8 11 0.23 0.62 -5 8 11 0.36 0.36 -5 8 10 0.73 0.74 -5 8 10 -0.06 0.3 -5 8 10 1.11 0.51 -5 8 10 0.73 0.3 -5 -8 9 14.33 1.98 -5 8 9 17.89 2.12 -5 8 9 18.73 1.49 -5 8 9 18.84 1.42 -5 8 9 18.06 1.58 -5 -8 8 21.45 2.3 -5 -8 7 0.18 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9 9 39.09 2.29 -5 -9 8 132.12 4.74 -5 9 8 127.53 4.78 -5 9 8 126.79 4.99 -5 -9 7 86.91 4.97 -5 -9 7 96.66 3.77 -5 9 7 91.96 3.84 -5 -9 6 27.9 2.48 5 -9 -6 32.43 2.47 -5 -9 5 67.81 3.88 5 -9 -5 72.69 3.97 5 -9 -4 70.82 3.96 -5 -9 4 67.87 3.67 5 -9 -3 92.16 4.48 -5 -9 3 89.75 4.1 5 -9 -2 261.44 9.01 -5 -9 2 259.06 8.64 -5 -9 1 132.01 5.55 5 -9 -1 138.37 5.75 5 -9 0 584.17 16.92 5 -9 1 93.98 4.64 5 -9 2 13.68 1.67 5 -9 3 55.73 3.53 5 -9 4 186.92 7.53 5 -9 5 43.91 2.24 5 9 5 41.61 2.61 5 -9 5 41.44 3.13 5 -9 6 147.56 6.45 5 9 6 126.06 6.94 5 -9 6 139.45 4.86 5 9 6 134.54 5.38 5 -9 7 112.25 4.23 5 9 7 110.06 4.68 5 -9 8 2.06 0.52 5 -9 9 14.46 1.25 5 -9 10 23.9 1.59 5 -9 11 1.42 0.41 5 -9 12 26.92 1.52 -5 -9 -12 26.44 1.52 -5 -9 -13 4.38 0.53 5 -9 13 4.83 0.58 -5 10 17 22.89 1.37 -5 10 16 13.08 1.18 -5 10 15 1.17 0.45 -5 10 14 37.76 2.4 -5 10 13 -0.22 0.55 -5 10 12 172.52 6.47 -5 10 12 176.2 5.91 -5 10 11 4.75 0.77 -5 10 11 6.52 1.05 -5 10 10 0.01 0.33 -5 10 10 -0.18 0.52 -5 10 9 0.41 0.34 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0.2 0.21 -8 6 19 0.02 0.18 -8 6 18 5.67 0.67 -8 6 17 27.41 1.66 -8 6 16 22.2 1.58 -8 6 15 62.79 3.16 -8 6 15 65.57 3.07 -8 6 14 75 3.55 -8 6 14 70.24 3.32 -8 6 13 104.2 4.04 -8 6 13 101.61 4.38 -8 6 13 100.56 4.19 -8 6 12 152.16 5.4 -8 6 12 155.14 5.71 -8 6 12 145.52 5.42 -8 6 11 598.84 15.77 -8 6 11 594.87 15.99 -8 6 11 575.25 15.73 -8 -6 10 58.31 4.2 -8 -6 10 63.21 3.97 -8 6 10 69.27 3.2 -8 6 10 67.66 3.22 -8 6 10 66.47 3.21 -8 -6 9 58.17 3.69 -8 -6 9 51.01 3.74 -8 6 9 58.68 2.91 -8 6 9 59.98 2.98 -8 -6 8 22.63 2.31 -8 6 8 27.06 1.81 -8 6 8 26.11 2.68 -8 6 8 23.91 1.81 -8 -6 7 -0.18 0.35 -8 6 7 -0.05 0.29 -8 6 7 0.19 0.41 -8 6 7 0.12 0.47 -8 6 6 75.26 4.31 8 -6 -6 87.83 4.17 -8 6 5 321.34 10.27 8 -6 -5 305.27 9.96 -8 6 4 43.72 2.82 8 -6 -4 39.81 2.79 -8 -6 4 39.89 2.9 -8 -6 3 98.6 4.99 8 -6 -3 102.78 4.85 -8 -6 2 38.09 2.96 8 -6 -2 44.1 2.99 -8 -6 1 26.87 2.55 8 -6 -1 26.38 2.33 -8 -6 0 26.77 2.56 8 -6 0 28.23 2.47 8 -6 1 28.14 1.96 8 -6 1 24.47 2.33 -8 -6 -1 24.06 2.51 8 -6 2 1.55 0.55 8 -6 2 2.76 0.84 8 -6 2 2.51 0.6 8 6 3 128.62 5 8 -6 3 129.35 4.87 8 -6 3 127.7 5 8 -6 3 133.61 6.23 8 6 4 -0.41 0.41 8 -6 4 -0.11 0.32 8 -6 4 -0.04 0.52 8 -6 4 0.13 0.31 8 -6 5 13.32 1.31 8 -6 5 11.76 1.3 8 -6 6 12.81 1.3 8 -6 6 13.63 1.34 8 -6 7 237.1 7.71 8 -6 8 46.45 2.54 8 -6 9 138.2 4.94 8 -6 10 73.38 3.07 8 -6 11 6.48 0.72 8 -6 12 34.64 1.57 -8 7 18 0.13 0.22 -8 7 17 7.11 0.79 -8 7 16 2.66 0.56 -8 7 15 3.46 0.71 -8 7 15 4.08 0.75 -8 7 14 22.55 1.78 -8 7 14 17.45 1.5 -8 7 13 1.93 0.53 -8 7 13 2.7 0.66 -8 7 13 1.22 0.47 -8 7 12 190.8 6.3 -8 7 12 171.92 6.18 -8 7 12 188.75 6.54 -8 7 11 38.53 2.3 -8 7 11 38.24 2.3 -8 7 11 35.99 2.32 -8 -7 10 14.43 2 -8 7 10 17.87 1.54 -8 7 10 17.17 1.5 -8 7 10 18.52 1.58 -8 -7 9 3.61 1.01 -8 7 9 4.99 0.83 -8 7 9 4.41 0.8 -8 7 8 172.56 5.96 -8 7 8 176.1 6.11 -8 -7 8 177.09 7.08 -8 7 7 142.32 5.27 -8 7 7 155.13 5.6 8 -7 -6 5.25 0.81 -8 7 6 6.16 0.87 8 -7 -6 3.04 0.89 -8 7 6 3.18 0.68 -8 7 6 4.66 1.12 -8 -7 5 1.46 0.72 -8 7 5 2.88 0.65 8 -7 -5 1.62 0.61 -8 -7 4 1.64 0.73 8 -7 -4 2.23 0.72 -8 -7 3 48.04 3.32 8 -7 -3 49.35 3.27 -8 -7 2 27.82 2.53 8 -7 -2 28.73 2.48 -8 -7 1 12.87 1.8 8 -7 -1 13.19 1.67 -8 -7 0 59.07 3.97 8 -7 0 62.32 3.12 8 -7 0 56.75 3.71 8 -7 1 41.28 2.45 8 -7 1 38.87 3.04 -8 -7 -1 38.25 3.23 8 -7 2 14.04 1.4 8 -7 2 14.16 1.81 8 -7 3 7.68 1.1 8 -7 3 9.25 1.49 8 -7 4 0.52 0.5 8 -7 4 1.96 0.76 8 -7 5 43.83 2.55 8 -7 5 49.62 2.73 8 -7 6 0.01 0.37 8 -7 7 94.47 3.99 8 -7 8 2.06 0.62 8 -7 9 179.08 5.86 8 -7 10 3.96 0.58 8 -7 11 6.25 0.66 -8 -7 -12 0.08 0.2 8 -7 12 0.36 0.23 8 -8 -18 5.19 0.57 -8 8 18 4.71 0.48 -8 8 17 14.77 1.05 -8 8 16 1.18 0.38 -8 8 15 51.83 2.54 -8 8 15 57.49 2.84 -8 8 14 7.29 1.01 -8 8 14 6.66 0.89 -8 8 13 6.95 0.9 -8 8 13 8.77 1.17 -8 8 13 7.64 0.96 -8 8 12 1.9 0.57 -8 8 12 1.37 0.6 -8 8 12 1.89 0.57 -8 8 11 168.43 5.86 -8 8 11 151.02 5.6 -8 8 11 167.83 5.95 -8 8 10 155.54 5.55 -8 8 10 138.04 5.3 -8 8 10 153.94 5.53 -8 8 9 89.04 3.85 -8 8 9 83.65 3.74 -8 8 8 40.64 2.42 -8 8 8 40.88 2.44 -8 8 7 0.95 0.5 8 -8 -7 1.08 0.42 -8 8 7 1.37 0.57 -8 -8 6 12.64 1.09 -8 8 6 12.47 1.26 8 -8 -6 11.68 1.21 -8 -8 5 245.81 7.31 -8 8 5 236.64 7.68 8 -8 -5 258 7.84 -8 -8 5 238.64 8.95 8 -8 -5 251.32 9.03 -8 -8 4 -0.34 0.26 -8 -8 4 0.72 0.52 8 -8 -4 1.12 0.51 -8 8 4 0.14 0.31 8 -8 -4 0.08 0.49 -8 -8 3 4.48 0.64 8 -8 -3 2.43 0.66 -8 -8 3 2.97 0.9 -8 -8 2 56.02 2.52 -8 8 2 56.93 2.76 -8 -8 2 48.42 3.51 8 -8 -2 56.37 3.69 -8 -8 1 16.32 2.07 8 -8 -1 19.97 2.15 -8 -8 0 40.22 3.25 8 -8 0 36.42 2.36 8 -8 0 39.76 3.11 -8 -8 -1 27.12 2.7 8 -8 1 26.31 1.95 8 -8 1 26.6 2.58 8 -8 2 3.26 0.7 8 -8 2 4.21 1.07 -8 -8 -2 3.68 1.13 8 -8 3 27.99 2.02 8 -8 3 30.18 2.77 8 -8 4 48.18 2.72 8 -8 5 9.92 1.14 8 -8 6 0.24 0.36 8 -8 7 3.8 0.68 8 -8 8 76.74 3.29 8 -8 9 3.06 0.56 8 -8 10 48.99 2.2 8 -8 11 8.43 0.73 -8 -8 -11 9.66 0.78 8 -8 12 32.51 1.34 -8 -8 -12 32.82 1.36 8 -9 -17 6.29 0.65 -8 9 17 5.04 0.55 -8 9 16 18.03 1.19 -8 9 15 95.65 3.61 -8 9 15 100.68 3.94 -8 9 14 23.93 1.51 -8 9 14 19.95 1.45 -8 9 14 19.27 1.59 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97.27 5.4 -8 -10 1 87.76 3.53 -8 -10 1 82.17 4.85 8 -10 -1 82.22 4.91 -8 -10 0 11.21 1.71 -8 -10 0 11.02 1.07 8 -10 0 14.01 1.39 -8 -10 0 11.14 1.02 -8 -10 -1 53.19 2.6 8 -10 1 58.66 3.03 -8 -10 -1 53.69 2.5 8 -10 2 21.52 1.72 -8 -10 -2 22.48 1.5 8 -10 3 25.21 1.83 -8 -10 -3 23.43 1.57 8 -10 4 39.43 2.33 -8 -10 -4 39.23 2.11 8 -10 5 10.34 1.03 -8 -10 -5 10.32 1.04 -8 -10 -6 7.17 0.84 8 -10 6 6.16 0.79 8 -10 7 97.02 3.61 -8 -10 -7 101.34 3.67 8 -10 8 232.46 6.74 -8 -10 -8 230.67 6.79 -8 -10 -9 40.57 1.85 8 -10 9 43.94 1.89 -8 -10 -9 41.76 1.9 -8 -10 -10 7.74 0.65 8 -10 10 7.34 0.63 -8 -10 -10 6.7 0.64 -8 -10 -11 7.81 0.59 8 -11 -16 2.8 0.37 8 -11 -15 2.54 0.46 -8 11 15 2.02 0.44 -8 11 14 18.08 1.19 8 -11 -14 15.04 1.11 -8 11 14 17.29 1.33 -8 11 13 9.39 0.97 8 -11 -13 8.24 0.87 -8 11 13 9.74 1.05 -8 11 12 23.31 1.68 8 -11 -12 23.47 1.57 -8 11 12 23.97 1.72 -8 11 11 0.84 0.42 8 -11 -11 0.79 0.45 -8 11 11 0.53 0.35 -8 11 10 52.69 2.87 8 -11 -10 50.33 2.59 -8 -11 9 13.84 1.27 -8 11 9 15.22 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3.38 -9 8 8 74.73 3.53 9 -8 -8 74.75 3.51 -9 8 8 71.81 3.54 -9 8 7 9.8 1.15 9 -8 -7 7.73 1.07 -9 8 6 25.57 1.89 9 -8 -6 24.5 1.85 -9 -8 5 226.74 6.8 -9 8 5 211.24 7.2 9 -8 -5 228.37 7.43 -9 -8 5 220.72 8.75 9 -8 -5 225.41 8.67 -9 -8 4 0.86 0.39 -9 8 4 1.09 0.38 9 -8 -4 0.65 0.38 9 -8 -4 1.02 0.43 -9 -8 4 1.35 0.64 -9 -8 3 198.99 6.1 9 -8 -3 196.37 6.65 -9 8 3 189.49 6.45 -9 -8 3 188.18 8.04 9 -8 -3 181.78 7.79 -9 -8 2 53.45 2.52 -9 8 2 57.81 2.85 9 -8 -2 55.73 2.91 -9 -8 2 54.18 3.89 9 -8 -2 55.25 3.82 9 -8 -1 4.7 0.81 -9 -8 1 6.56 0.79 9 -8 -1 7.31 1.45 9 -8 -1 5.39 1 -9 -8 0 1.18 0.8 9 -8 0 0.3 0.53 9 -8 0 -0.03 0.38 9 -8 1 8.68 1.15 9 -8 2 45.87 2.69 9 -8 3 3.06 0.72 9 -8 4 180.37 6.34 9 -8 4 195.01 6.57 9 -8 5 -0.12 0.3 9 -8 6 191.3 6.36 9 -8 7 0.15 0.33 9 -8 8 7.88 0.85 9 -8 9 3.09 0.49 -9 -8 -10 2.34 0.37 9 -8 10 3.39 0.45 -9 -8 -11 15.13 0.83 9 -9 -17 3.13 0.44 9 -9 -16 15.61 1.09 -9 9 16 13.45 0.99 9 -9 -15 0.01 0.28 -9 9 15 0.11 0.26 -9 9 14 1.38 0.44 -9 9 14 1.56 0.45 -9 9 14 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2.36 10 -1 -4 27.78 2.4 10 -1 -3 5.77 1.14 10 1 -3 5.57 0.86 10 -1 -3 6.54 0.94 -10 -1 3 5.8 1.28 10 1 -3 5.37 1.15 10 -1 -3 5.97 0.94 -10 -1 2 112.97 5.56 10 1 -2 103.74 4.42 10 -1 -2 115.53 4.59 10 -1 -2 103.81 4.36 10 1 -2 111.15 5.53 10 -1 -2 107.1 5.43 -10 -1 1 1.76 0.81 10 1 -1 0.7 0.42 -10 1 1 2.58 0.87 10 -1 -1 1.31 0.69 10 1 -1 1.67 0.56 10 -1 -1 0.86 0.38 10 1 -1 0.38 0.47 10 -1 -1 0.34 0.37 -10 1 0 2.76 0.97 10 1 0 0.76 0.71 10 1 0 1.93 0.61 10 -1 0 1.23 0.45 10 -1 0 2.1 0.83 10 1 0 1.25 0.44 10 -1 0 1.88 0.67 -10 -1 0 1.75 0.78 -10 1 -1 100.85 5.21 10 1 1 101.69 4.49 10 -1 1 106.87 4.58 10 1 1 103.94 4.34 10 -1 1 104.49 4.5 10 1 1 107.89 5.86 10 -1 1 110.62 5.9 -10 -1 -1 99.48 5.46 10 1 2 24.88 2.03 10 -1 2 26.79 2.05 10 -1 2 27 2.05 10 1 2 29.04 2.9 -10 -1 -2 22.51 2.4 10 -1 2 25.86 2.68 10 1 3 23.66 1.95 10 -1 3 22.07 1.94 10 -1 3 21.9 1.87 10 1 4 6.4 1.11 10 -1 4 5.46 0.93 10 1 5 3 0.75 10 -1 5 3.77 0.86 10 1 6 1.13 0.61 10 -1 6 3.22 0.78 10 -1 7 1.55 0.51 10 1 7 1.1 0.39 10 1 8 0.49 0.32 10 -1 8 0.32 0.3 10 1 9 2.75 0.51 10 -1 9 3.16 0.52 10 1 10 -0.11 0.27 10 -1 10 0.09 0.19 10 -1 11 0.29 0.16 -10 2 19 2.15 0.38 10 -2 -18 0.4 0.29 -10 -2 18 0.36 0.23 -10 2 18 0.86 0.34 10 -2 -17 20.88 1.42 -10 -2 17 21.28 1.33 -10 2 17 23.02 1.52 -10 -2 16 4.76 0.71 -10 2 16 4.96 0.77 10 2 -15 49.05 2.39 -10 -2 15 47.67 2.41 -10 2 15 50.12 2.61 10 2 -14 0.65 0.4 -10 -2 14 0.19 0.33 -10 2 14 0.13 0.44 10 2 -13 13.99 1.32 -10 -2 13 10.91 1.13 -10 2 13 12.45 1.32 10 2 -12 11.97 1.25 -10 -2 12 9.54 1.09 -10 2 12 10.88 1.2 10 2 -11 7.67 1.07 -10 -2 11 7.26 0.93 -10 2 11 7.12 1.02 -10 -2 10 27.24 2.79 -10 2 10 31.31 3.08 10 2 -10 31.49 2.12 10 -2 -10 31.02 2.12 -10 -2 10 30.82 2 -10 2 10 28.87 2.08 -10 -2 9 513.57 16.29 -10 2 9 520.16 16.61 10 2 -9 522.46 14.22 10 -2 -9 495.86 14.22 -10 -2 9 484.29 13.89 -10 2 9 522.49 14.39 -10 2 8 501.74 16.43 -10 2 8 540.08 14.57 10 2 -8 520.32 14.59 10 -2 -8 514.76 14.58 -10 -2 8 503.69 14.4 -10 2 8 558.84 14.95 -10 -2 8 550.44 16.73 -10 2 7 41.78 3.22 10 2 -7 40.75 2.39 10 -2 -7 39.86 2.41 -10 2 7 42.29 2.4 -10 2 7 41.97 2.59 -10 2 6 12.5 1.23 10 2 -6 14.54 1.39 10 -2 -6 14.81 1.43 -10 2 6 12.63 1.72 10 2 -5 26.66 1.92 10 -2 -5 29.11 2 10 2 -5 28.48 2.41 10 -2 -5 33.17 2.56 -10 2 5 27.02 2.48 10 2 -4 94.09 4.07 10 -2 -4 106.29 4.28 10 2 -4 91.65 4.83 -10 -2 4 97.35 5.14 10 -2 -4 95.04 4.88 -10 -2 3 42.06 3.2 10 2 -3 39.41 2.41 10 -2 -3 42.95 2.52 10 2 -3 40.38 3.07 10 -2 -3 41.21 3.09 10 2 -2 2.56 0.77 10 2 -2 3.34 0.76 10 -2 -2 4.61 0.83 10 -2 -2 2.99 0.78 -10 -2 2 4.21 1.13 10 -2 -2 4.17 0.85 -10 -2 1 1.71 0.86 10 2 -1 1.08 0.8 10 2 -1 0.33 0.31 10 -2 -1 0.12 0.31 10 -2 -1 0.23 0.43 10 -2 -1 1 0.5 10 2 0 64.21 3.36 10 -2 0 72.95 3.53 10 2 0 69.29 3.2 10 2 0 70.48 4.53 10 -2 0 68.26 3.4 10 -2 0 72.19 4.47 -10 -2 0 73.7 4.64 10 2 1 136.69 5.29 10 -2 1 131.85 5.23 10 2 1 128.57 4.96 10 -2 1 117.61 5 10 2 1 138.17 6.78 -10 -2 -1 127.25 6.41 10 -2 1 130.96 6.51 10 2 2 500.05 14.14 10 -2 2 456.05 13.91 -10 -2 -2 484.9 16.21 10 -2 2 490.43 14.15 10 2 2 517.59 16.59 10 -2 2 517.78 16.36 10 2 3 253.94 8.72 10 -2 3 271.27 8.79 10 -2 3 282.44 8.89 10 -2 4 107.71 4.63 10 2 4 103.49 4.69 10 2 5 1.08 0.48 10 -2 5 1.32 0.55 10 2 6 153.26 5.82 10 -2 6 147.4 5.71 10 2 7 22.54 1.62 10 -2 7 24.16 1.76 10 -2 8 -0.77 0.38 10 2 8 0.22 0.25 10 2 9 17.41 1.15 10 -2 9 17.47 1.25 10 -2 10 1.71 0.33 10 -2 11 5.16 0.5 10 -3 -19 2.6 0.38 -10 3 19 1.95 0.34 10 -3 -18 7.76 0.77 -10 3 18 7.9 0.78 10 -3 -17 103.81 3.87 -10 3 17 114.32 4.03 -10 -3 16 58.17 2.5 -10 3 16 59.27 2.81 -10 -3 15 44.08 2.26 -10 3 15 48.25 2.55 -10 -3 14 26.18 1.69 -10 3 14 26.86 1.9 -10 -3 13 0.47 0.36 -10 3 13 1.34 0.54 -10 -3 12 9.35 1.02 -10 3 12 8.44 1.1 -10 -3 11 89.73 3.75 -10 3 11 92.84 4.02 -10 -3 10 54.73 3.92 -10 3 10 50.62 2.74 -10 3 10 51.54 4.03 10 -3 -10 50.52 2.8 -10 -3 10 48.44 2.58 -10 3 10 50.82 2.83 -10 3 9 6.29 0.9 10 3 -9 5.52 0.86 10 -3 -9 6.63 1.03 -10 -3 9 4.21 1.2 -10 3 9 4.22 1.17 -10 -3 9 5.31 0.83 -10 3 9 5.5 0.97 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1 17.89 2.27 -10 -3 -1 13.67 1.94 10 -3 1 16.36 2.08 10 -3 1 13.79 1.5 10 3 2 440.86 12.92 10 -3 2 432.6 12.78 -10 -3 -2 407.53 14.61 10 -3 2 448.03 12.89 10 3 2 445.08 15.24 10 -3 2 455.36 15.05 10 3 3 33.04 2.33 10 -3 3 33.76 2.3 10 3 4 84.39 4.05 10 -3 4 84.11 3.97 10 3 5 1.18 0.51 10 -3 5 0.14 0.37 10 -3 6 97.1 4.23 10 -3 7 0.13 0.41 10 3 7 0.19 0.37 10 3 8 35.44 1.84 10 -3 8 33.97 2 10 -3 9 18.8 1.3 10 -3 10 0.57 0.24 10 -3 11 21.91 1.08 -10 4 19 46.05 1.81 10 -4 -18 27.24 1.49 -10 4 18 26.49 1.49 10 -4 -17 47.9 2.28 -10 4 17 49.99 2.35 -10 4 16 2.49 0.59 -10 4 15 0.21 0.47 -10 4 14 0.87 0.52 -10 4 13 58.39 2.99 -10 4 12 42.8 2.53 -10 4 11 18.3 1.55 -10 4 11 16.57 1.55 -10 4 10 0.68 0.44 10 -4 -10 0.65 0.45 -10 4 9 321.28 9.72 -10 4 9 313.1 11.82 10 -4 -9 310.94 9.76 -10 4 9 318.29 9.94 -10 -4 9 330.17 11.65 -10 4 8 210.39 8.84 -10 4 8 214.62 7.12 10 -4 -8 202.76 7.1 -10 4 8 224.57 7.52 -10 -4 8 212.92 8.68 -10 4 7 85.62 5.05 -10 4 7 94.09 4.02 10 -4 -7 94.11 4.1 -10 4 6 0.39 0.32 10 -4 -6 0.24 0.32 -10 4 6 0.19 0.53 -10 4 5 46.1 3.29 -10 4 5 44.68 2.48 10 -4 -5 49.24 2.72 10 -4 -5 41.54 3.02 -10 4 4 28.14 1.85 10 4 -4 26.67 1.92 10 -4 -4 22.2 1.82 -10 -4 4 27.09 2.61 10 -4 -4 24.74 2.34 -10 4 4 31.07 2.58 -10 4 3 1.97 0.46 10 4 -3 2.41 0.66 10 -4 -3 1.97 0.57 10 -4 -3 1.73 0.7 -10 -4 3 0.99 0.67 -10 -4 2 11.91 1.85 10 4 -2 13.91 1.34 10 -4 -2 12.91 1.37 10 -4 -2 12.84 1.76 10 -4 -2 13.22 1.42 10 4 -1 384.08 11.62 10 -4 -1 408.2 11.89 10 -4 -1 402.83 11.93 -10 -4 1 410.97 13.87 10 -4 -1 418.1 13.64 10 4 0 133.05 5.14 10 -4 0 132.81 5.27 -10 -4 0 135.67 6.79 10 -4 0 125.08 5.16 10 -4 0 136.85 6.56 10 4 1 21.23 1.83 10 -4 1 22.61 1.89 -10 -4 -1 22.07 2.56 10 4 1 27.56 2.83 10 -4 1 23.56 2 10 -4 1 26.92 2.72 10 4 2 7.39 1.08 10 -4 2 8.84 1.2 10 -4 2 7.68 1.11 10 -4 3 3.53 0.78 10 -4 3 2.84 0.73 10 4 4 5.99 1.03 10 -4 4 5.53 0.9 10 4 5 27.61 2.12 10 -4 5 22.72 1.85 10 -4 6 3.47 0.72 10 -4 6 3.76 0.79 10 -4 7 27.47 1.86 10 -4 8 1.3 0.45 10 -4 9 25.23 1.52 10 -4 10 -0.44 0.28 10 -4 11 12.69 0.78 10 -5 -18 1.2 0.34 -10 5 18 0.3 0.23 10 -5 -17 51.4 2.37 -10 5 17 53.53 2.41 -10 5 16 28.4 1.79 -10 5 15 27.1 1.82 -10 5 14 10.19 1.11 -10 5 13 2.45 0.65 -10 5 12 0.13 0.35 -10 5 12 0.49 0.51 -10 5 11 50.19 2.71 -10 5 11 45.51 2.68 -10 5 10 22.27 1.77 10 -5 -10 24.26 1.89 -10 5 10 22.97 1.85 -10 5 9 3.93 0.79 10 -5 -9 4.42 0.86 -10 -5 9 2.73 0.96 -10 5 9 2.59 0.74 -10 5 9 4.64 1.18 -10 5 8 -0.08 0.33 10 -5 -8 1.01 0.6 -10 5 8 1.07 0.66 -10 5 8 0.12 0.66 -10 5 7 255.96 10.12 -10 5 7 281.77 8.63 10 -5 -7 271.87 8.67 -10 5 6 145.37 6.65 -10 5 6 135.18 5.13 10 -5 -6 134.76 5.25 -10 5 5 182.1 6.27 10 -5 -5 177.73 6.42 10 -5 -5 194.39 7.57 -10 5 4 30.7 2.01 -10 -5 4 34.84 3.03 10 -5 -4 33.15 2.24 10 -5 -4 31.75 2.69 -10 5 3 1.34 0.44 10 -5 -3 2.51 0.7 -10 -5 3 1.9 0.8 10 -5 -3 2.06 0.8 -10 5 2 80.5 3.5 10 -5 -2 74.16 3.62 10 -5 -2 82.59 4.72 -10 -5 2 88.33 5.19 10 5 -1 0.39 0.32 10 -5 -1 0.2 0.53 10 -5 -1 -0.51 0.54 -10 -5 1 0.73 0.65 10 -5 -1 0.2 0.38 10 5 0 66.03 3.26 10 -5 0 70.09 3.48 -10 -5 0 73.75 4.77 10 -5 0 64.96 3.49 10 -5 0 67.96 4.42 10 5 1 832.15 22.37 10 -5 1 805.7 22.38 -10 -5 -1 912.48 25.43 10 -5 1 877.28 22.68 10 -5 1 871.19 24.76 10 5 2 113.43 4.7 10 -5 2 108.79 4.56 10 -5 2 105.77 4.63 10 5 3 271.34 8.8 10 -5 3 269.69 8.76 10 -5 3 290.93 9.05 10 5 4 38.88 2.48 10 -5 4 44.31 2.59 10 -5 4 41.22 2.6 10 -5 5 22.94 1.81 10 -5 6 188.12 6.68 10 -5 6 219.05 6.89 10 -5 7 3.51 0.66 10 -5 8 3.6 0.64 10 -5 9 3.89 0.57 10 -5 10 1.3 0.3 10 -5 11 0.91 0.22 10 -6 -18 51.69 2.07 -10 6 18 47.76 1.98 10 -6 -17 0.15 0.29 -10 6 17 -0.42 0.31 10 -6 -16 15.89 1.27 -10 6 16 16.97 1.31 -10 6 15 9.26 1.01 -10 6 14 29.61 1.95 -10 6 13 3.38 0.63 -10 6 13 3.31 0.73 -10 6 12 -0.01 0.32 -10 6 12 0.32 0.38 -10 6 11 55.86 2.89 10 -6 -11 56.85 3.03 -10 6 11 51.06 2.85 -10 6 10 1.13 0.41 10 -6 -10 1.98 0.69 -10 6 10 2.94 0.64 -10 6 9 499.57 13.86 10 -6 -9 476.99 13.89 -10 6 9 484.96 14.02 -10 6 8 112.45 4.62 10 -6 -8 121.06 4.81 -10 6 8 116.32 6.23 -10 6 8 110.38 4.79 -10 6 7 54.03 2.89 10 -6 -7 55.29 3 -10 6 6 5.97 0.9 10 -6 -6 4.95 0.87 -10 6 5 87.43 3.81 10 -6 -5 84.05 3.91 10 -6 -5 94.42 4.89 -10 -6 4 0.48 0.47 -10 6 4 -0.51 0.36 10 -6 -4 -0.03 0.42 10 -6 -4 1.1 0.58 -10 -6 3 33.23 3.05 -10 6 3 36.39 2.19 10 -6 -3 35.16 2.31 10 -6 -3 29.2 2.7 -10 -6 2 4.33 0.64 -10 6 2 3.96 0.72 10 -6 -2 3.89 0.77 10 -6 -2 4.73 1.14 -10 -6 2 3.09 1.03 10 -6 -1 46.51 2.67 10 -6 -1 37.47 2.53 -10 -6 1 43.07 3.55 10 -6 -1 44.23 3.44 10 -6 0 175.5 6.34 -10 -6 0 190.29 8.32 10 -6 0 167.46 6.42 10 -6 0 179.02 7.87 10 6 1 130.28 5 10 -6 1 120.8 5 10 -6 1 131.5 5.23 10 6 2 129.61 4.98 10 -6 2 127.18 4.99 10 -6 2 122.15 5.06 10 6 3 304.29 9.38 10 -6 3 296.13 9.27 10 -6 3 294.75 9.45 10 -6 4 9.96 1.15 10 -6 4 8.81 1.14 10 -6 5 33.96 2.21 10 -6 5 33.67 2.2 10 -6 6 26.71 1.85 10 -6 7 24.65 1.68 10 -6 8 12.88 1.09 10 -6 9 2.92 0.5 10 -6 10 8.07 0.66 10 -7 -18 2.78 0.42 10 -7 -17 1.55 0.41 -10 7 17 1.58 0.41 10 -7 -16 1.08 0.35 -10 7 16 1.42 0.4 10 -7 -15 12.45 1.14 -10 7 15 10.45 1.08 10 -7 -14 0.8 0.44 -10 7 14 0.67 0.38 -10 7 13 1.91 0.53 10 -7 -13 2.15 0.67 -10 7 13 1.26 0.49 -10 7 12 84.52 3.64 10 -7 -12 82.67 3.73 -10 7 12 77.12 3.56 -10 7 11 6.61 0.94 10 -7 -11 9.42 1.2 -10 7 11 8.44 1.12 -10 7 10 3.28 0.7 10 -7 -10 2.21 0.69 -10 7 10 2.6 0.69 -10 7 9 108.19 4.49 10 -7 -9 112.23 4.63 -10 7 9 108.48 4.61 -10 7 8 212.83 7.24 10 -7 -8 222.07 7.42 -10 7 7 100.65 4.27 10 -7 -7 104.53 4.43 -10 7 6 290.59 9.06 10 -7 -6 295.89 9.27 -10 7 5 259.21 8.28 10 -7 -5 263.36 8.52 10 -7 -5 270.38 9.84 -10 7 4 56.29 2.87 -10 -7 4 52.97 3.9 10 -7 -4 52.77 2.95 10 -7 -4 56.1 3.8 -10 -7 3 51.35 3.82 -10 -7 3 52.07 2.38 -10 7 3 49.31 2.67 10 -7 -3 47.26 2.79 10 -7 -3 50.66 3.64 -10 -7 2 292.91 8.46 -10 7 2 304.55 9.05 10 -7 -2 291.11 9.23 -10 -7 2 295.61 11.18 10 -7 -2 283.26 10.78 10 -7 -1 4.71 0.82 10 -7 -1 4.88 0.92 10 -7 0 172.11 6.25 10 -7 0 180.76 6.52 10 -7 1 241.5 7.91 10 -7 1 243.92 8.13 10 -7 2 10.76 1.24 10 -7 2 9.69 1.26 10 -7 3 10.46 1.17 10 -7 3 9.66 1.18 10 -7 4 68.92 3.24 10 -7 5 105.59 4.37 10 -7 5 116.11 4.35 10 -7 6 1.28 0.48 10 -7 7 2.93 0.56 10 -7 8 1.29 0.4 10 -7 9 10.53 0.83 10 -7 10 15.04 0.88 -10 -7 -10 17.66 0.93 10 -8 -17 10.8 0.84 10 -8 -16 0.47 0.36 -10 8 16 -0.23 0.23 10 -8 -15 6.45 0.79 -10 8 15 4.53 0.65 10 -8 -14 0.8 0.43 -10 8 14 -0.09 0.4 -10 8 13 15.26 1.3 10 -8 -13 14.18 1.35 -10 8 13 13.49 1.26 -10 8 12 0.5 0.42 10 -8 -12 0.14 0.39 -10 8 12 -0.42 0.44 -10 8 11 43.63 2.51 10 -8 -11 42.22 2.5 -10 8 11 39.14 2.37 -10 8 10 12.21 1.29 10 -8 -10 11.75 1.28 -10 8 9 82.15 3.79 10 -8 -9 85.01 3.88 -10 8 8 51.16 2.86 10 -8 -8 56.34 3.03 -10 8 7 93.43 4.09 10 -8 -7 96.35 4.23 -10 8 6 -0.05 0.34 10 -8 -6 0.18 0.37 -10 8 5 414.33 12.14 10 -8 -5 429.6 12.4 -10 -8 4 9.28 0.93 -10 8 4 9.94 1.13 10 -8 -4 10 1.21 -10 -8 3 233.66 7.08 -10 8 3 233.72 7.57 10 -8 -3 237.51 7.8 -10 -8 2 8.17 0.9 -10 8 2 10.17 1.14 10 -8 -2 6.42 1 10 -8 -2 8.01 1.15 -10 -8 1 2.96 0.58 10 -8 -1 2.03 0.61 10 -8 -1 1.6 0.63 -10 -8 0 102.9 3.9 10 -8 0 109.68 4.41 10 -8 0 97.43 4.4 10 -8 1 163.06 5.77 10 -8 1 153.06 5.87 10 -8 2 435.3 12.74 10 -8 3 26.89 1.96 10 -8 4 4.96 0.78 10 -8 5 13.86 1.27 10 -8 6 0.99 0.34 10 -8 7 24.19 1.5 -10 -8 -8 1.78 0.35 10 -8 8 2.05 0.4 10 -8 9 5.04 0.53 -10 -8 -9 4.99 0.52 -10 -8 -9 5.44 0.52 10 -9 -16 2.77 0.45 10 -9 -15 10.18 0.91 10 -9 -14 25.05 1.6 -10 9 13 3.34 0.61 10 -9 -13 3.82 0.71 -10 9 12 60.7 2.91 10 -9 -12 59.09 2.91 -10 9 11 17.52 1.53 10 -9 -11 17.72 1.52 -10 9 10 2.99 0.68 10 -9 -10 2.54 0.69 -10 9 9 106.25 4.46 10 -9 -9 108.84 4.47 -10 9 8 24.02 1.88 10 -9 -8 24.91 1.93 -10 9 7 7.25 1.05 10 -9 -7 5.99 0.9 -10 9 6 323.38 10.07 10 -9 -6 347.92 10.27 -10 -9 5 108.19 3.97 -10 9 5 99.24 4.31 10 -9 -5 112.54 4.54 -10 -9 4 9.93 1 -10 9 4 9.56 1.11 10 -9 -4 10.84 1.22 -10 -9 3 135.56 4.76 -10 9 3 138.01 5.16 10 -9 -3 140.52 5.28 -10 -9 2 -0.02 0.28 -10 9 2 0.38 0.41 10 -9 -2 -0.21 0.47 -10 -9 1 6 0.78 10 -9 -1 5.49 0.94 -10 -9 0 19.24 1.43 10 -9 0 20.1 1.75 -10 -9 -1 12.95 1.14 10 -9 1 12.63 1.35 -10 -9 -2 8.65 0.95 10 -9 2 7.31 1.05 -10 -9 -2 8.88 0.91 10 -9 3 217.23 7.11 10 -9 3 230.9 7.5 -10 -9 -3 235.87 6.89 10 -9 4 38.67 2.14 -10 -9 -4 39.46 2.01 10 -9 5 19.4 1.39 -10 -9 -5 19.14 1.29 10 -9 6 26.7 1.58 -10 -9 -6 28.29 1.54 -10 -9 -7 13.94 1.01 10 -9 7 14.43 1.02 -10 -9 -7 13.44 0.97 -10 -9 -8 29.14 1.4 10 -9 8 25.63 1.32 -10 -9 -8 28.89 1.36 -10 -9 -9 17.59 0.93 -10 -9 -9 17.42 0.91 10 -10 -16 14.28 0.87 10 -10 -15 2.54 0.47 10 -10 -14 5.71 0.69 -10 10 13 10.6 1.02 10 -10 -13 10.21 1.02 -10 10 12 10.41 1.08 10 -10 -12 11.52 1.11 -10 10 11 37.05 2.22 10 -10 -11 34.24 2.08 -10 10 10 14.58 1.4 10 -10 -10 13.99 1.33 -10 10 9 105.01 4.34 10 -10 -9 102.18 4.23 -10 10 8 49.22 2.73 10 -10 -8 47.76 2.67 -10 10 7 0.96 0.5 10 -10 -7 0.61 0.41 -10 -10 6 45.58 2.3 -10 10 6 43.11 2.54 10 -10 -6 43.99 2.56 -10 -10 5 98.65 3.71 -10 10 5 88.02 3.92 -10 -10 4 102.68 3.84 -10 10 4 93.76 4.07 -10 -10 3 4.56 0.7 -10 10 3 3.75 0.72 -10 -10 2 31.39 1.88 10 -10 -2 30.96 2.23 -10 -10 1 5.01 0.72 10 -10 -1 4.99 0.85 -10 -10 0 258.65 7.75 10 -10 0 254.24 8.31 -10 -10 -1 3.71 0.64 10 -10 1 4.25 0.8 -10 -10 -2 7.9 0.9 10 -10 2 7.84 1.01 -10 -10 -2 10.09 0.92 -10 -10 -3 36.05 1.98 10 -10 3 36.27 2.17 -10 -10 -3 36.71 1.88 -10 -10 -4 4.48 0.61 -10 -10 -4 4.98 0.71 10 -10 4 4.7 0.64 -10 -10 -5 30.25 1.66 10 -10 5 27.07 1.53 -10 -10 -5 30.49 1.6 -10 -10 -6 10.13 0.87 10 -10 6 10.11 0.82 -10 -10 -6 12.01 0.9 -10 -10 -7 0.85 0.25 10 -10 7 0.93 0.26 -10 -10 -7 0.8 0.31 -10 -10 -8 0.31 0.18 -10 -10 -8 -0.24 0.2 10 -11 -14 11.45 0.87 -10 11 13 0.19 0.27 10 -11 -13 0.33 0.29 -10 11 12 2.63 0.58 10 -11 -12 3.29 0.57 -10 11 11 23.16 1.66 10 -11 -11 22.22 1.53 -10 11 10 14.14 1.32 10 -11 -10 14 1.23 -10 11 9 0.6 0.38 10 -11 -9 0.69 0.4 -10 11 8 14.23 1.39 -10 -11 7 13.67 1.2 -10 11 7 14.61 1.41 -10 -11 6 245.21 7.33 -10 11 6 233.74 7.7 -10 -11 5 69.16 2.98 -10 11 5 66.48 3.23 -10 -11 4 7.17 0.85 -10 11 4 6.74 0.9 -10 -11 3 107.41 4.1 -10 11 3 112.92 4.42 10 -11 -3 115.9 4.78 -10 -11 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