#------------------------------------------------------------------------------ #$Date: 2019-11-11 20:38:07 +0200 (Mon, 11 Nov 2019) $ #$Revision: 227287 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/03/58/4035879.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4035879 loop_ _publ_author_name 'Mart\'inez-Pardo, Pablo' 'Blay, Gonzalo' 'Vila, Carlos' 'Sanz-Marco, Amparo' 'Mu\~noz, M Carmen' 'Pedro, Jos\'e R' _publ_section_title ; Enantioselective Synthesis of 5-Trifluoromethyl-2-oxazolines under Dual Silver/Organocatalysis. ; _journal_issue 1 _journal_name_full 'The Journal of organic chemistry' _journal_page_first 314 _journal_page_last 325 _journal_paper_doi 10.1021/acs.joc.8b02808 _journal_volume 84 _journal_year 2019 _chemical_absolute_configuration ad _chemical_formula_sum 'C11 H11 Br F3 N O3' _chemical_formula_weight 342.12 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens difmap _audit_creation_method SHELXL-2014 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 5.7871(2) _cell_length_b 13.5493(6) _cell_length_c 16.8357(6) _cell_measurement_reflns_used 2861 _cell_measurement_temperature 200(1) _cell_measurement_theta_max 23.8880 _cell_measurement_theta_min 3.7240 _cell_volume 1320.11(9) _computing_cell_refinement 'CrysAlisPro, Agilent Technologies' _computing_data_collection 'CrysAlisPro, Agilent Technologies' _computing_data_reduction 'CrysAlisPro, Agilent Technologies' _computing_structure_refinement 'SHELXL-2014 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-2014 (Sheldrick, 2014)' _diffrn_ambient_temperature 200(1) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.940 _diffrn_measurement_device_type 'SuperNova Sapphire3' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0548 _diffrn_reflns_av_unetI/netI 0.0664 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.940 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 11989 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.915 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 29.782 _diffrn_reflns_theta_min 3.241 _exptl_absorpt_coefficient_mu 3.153 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.54357 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Empirical absorption correction' _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.721 _exptl_crystal_description prismatic _exptl_crystal_F_000 680 _exptl_crystal_size_max 0.120 _exptl_crystal_size_mid 0.080 _exptl_crystal_size_min 0.080 _refine_diff_density_max 0.270 _refine_diff_density_min -0.408 _refine_diff_density_rms 0.070 _refine_ls_abs_structure_details ; Flack x determined using 764 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.005(8) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.896 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 216 _refine_ls_number_reflns 3447 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.896 _refine_ls_R_factor_all 0.0829 _refine_ls_R_factor_gt 0.0432 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0604P)^2^+0.3452P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0916 _refine_ls_wR_factor_ref 0.1144 _reflns_Friedel_coverage 0.681 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.880 _reflns_number_gt 2387 _reflns_number_total 3447 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jo8b02808_si_002.cif _cod_data_source_block shelx _cod_database_code 4035879 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.703 _shelx_estimated_absorpt_t_max 0.787 _shelxl_version_number 2014-1 _shelx_res_file ; TITL gon33 in P2(1)2(1)2(1) CELL 0.71073 5.7871 13.5493 16.8357 90.000 90.000 90.000 ZERR 4.00 0.0002 0.0006 0.0006 0.000 0.000 0.000 LATT -1 SYMM 1/2 - X, - Y, 1/2 + Z SYMM 1/2 + X, 1/2 - Y, - Z SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O BR F UNIT 44 44 4 12 4 12 MERG 2 FMAP 2 omit -3 180 acta 50 size 0.08 0.08 0.12 PLAN 25 L.S. 8 WGHT 0.060400 0.345200 FVAR 4.01255 BR 5 1.152484 0.847177 0.206875 11.00000 0.04268 0.07488 = 0.04125 0.01231 -0.00186 0.00734 O1 4 1.016924 1.083254 -0.035207 11.00000 0.02128 0.03472 = 0.06686 0.01786 0.00212 0.00385 O2 4 0.678379 1.217340 0.063906 11.00000 0.04110 0.03839 = 0.05475 -0.00820 -0.00129 -0.00738 O3 4 0.465690 1.083577 0.088784 11.00000 0.04356 0.03721 = 0.03562 -0.00257 0.00235 -0.00154 N 3 0.643933 1.187632 -0.095091 11.00000 0.04287 0.04479 = 0.04838 0.01012 0.00260 0.01861 F1 6 0.893306 1.057558 -0.187217 11.00000 0.07926 0.05688 = 0.04679 0.01424 0.02747 0.01917 F2 6 0.629500 0.952530 -0.160476 11.00000 0.08707 0.06542 = 0.04091 -0.00883 -0.00466 -0.00904 F3 6 0.986210 0.918022 -0.138143 11.00000 0.10408 0.05581 = 0.05407 0.00734 0.02899 0.04199 C1 1 0.810660 1.031695 -0.049222 11.00000 0.02387 0.02997 = 0.04096 0.00438 0.00307 0.00150 C2 1 0.828963 0.989722 -0.133916 11.00000 0.05583 0.03540 = 0.04517 0.00436 0.01170 0.01144 C3 1 0.601089 1.102883 -0.043043 11.00000 0.01997 0.03130 = 0.03462 0.00092 0.00019 0.00082 C4 1 0.588868 1.142287 0.041736 11.00000 0.01930 0.03157 = 0.03924 0.00172 -0.00276 -0.00060 C5 1 0.461185 1.112112 0.172324 11.00000 0.07903 0.05968 = 0.03271 0.00105 -0.00033 0.00395 C6 1 0.791616 0.946003 0.009788 11.00000 0.02668 0.02798 = 0.03230 0.00109 0.00281 0.00178 C7 1 0.609561 0.879737 0.005589 11.00000 0.03504 0.03549 = 0.03942 -0.00415 0.00084 -0.00547 C8 1 0.593309 0.803769 0.059800 11.00000 0.03960 0.03661 = 0.04500 0.00134 0.00184 -0.01040 C9 1 0.753114 0.793060 0.119218 11.00000 0.04820 0.03706 = 0.03882 0.00612 0.01345 -0.00106 C10 1 0.931304 0.859605 0.123355 11.00000 0.03188 0.04146 = 0.03588 0.00140 0.00611 0.00598 C11 1 0.956229 0.935929 0.069084 11.00000 0.02809 0.03047 = 0.04080 -0.00179 0.00601 0.00059 H7 2 0.496961 0.881570 -0.034120 11.00000 0.03438 H5A 2 0.365915 1.065244 0.197130 11.00000 0.07585 H8 2 0.465144 0.760282 0.057249 11.00000 0.03548 H3 2 0.463446 1.061662 -0.055486 11.00000 0.02372 H11 2 1.066307 0.985926 0.071957 11.00000 0.02186 H1O 2 0.997459 1.140019 -0.057298 11.00000 0.06031 H10 2 0.742681 0.745473 0.157191 11.00000 0.02263 H1N 2 0.606665 1.170753 -0.137833 11.00000 0.07896 H5B 2 0.613066 1.106066 0.192870 11.00000 0.09271 H5C 2 0.385689 1.177684 0.178159 11.00000 0.10014 H2N 2 0.559488 1.235034 -0.085859 11.00000 0.06492 HKLF 4 REM gon33 in P2(1)2(1)2(1) REM R1 = 0.0432 for 2387 Fo > 4sig(Fo) and 0.0829 for all 3447 data REM 216 parameters refined using 0 restraints END WGHT 0.0276 0.0000 REM Highest difference peak 0.270, deepest hole -0.408, 1-sigma level 0.070 Q1 1 1.1732 1.1565 -0.1016 11.00000 0.05 0.27 Q2 1 0.8224 0.8379 0.1387 11.00000 0.05 0.25 Q3 1 0.3640 1.2622 -0.1335 11.00000 0.05 0.25 Q4 1 0.4997 0.8259 0.1434 11.00000 0.05 0.25 Q5 1 0.9997 0.8729 0.1629 11.00000 0.05 0.24 Q6 1 1.3490 0.8521 0.1966 11.00000 0.05 0.24 Q7 1 0.8530 1.0196 0.1607 11.00000 0.05 0.24 Q8 1 0.3717 1.0596 -0.0072 11.00000 0.05 0.23 Q9 1 0.9839 0.8989 0.2051 11.00000 0.05 0.23 Q10 1 1.2872 0.9018 0.2443 11.00000 0.05 0.23 Q11 1 1.2695 0.8914 0.1622 11.00000 0.05 0.23 Q12 1 0.7937 0.8031 -0.0020 11.00000 0.05 0.23 Q13 1 1.0368 0.8749 0.2578 11.00000 0.05 0.22 Q14 1 1.1636 0.7451 0.2151 11.00000 0.05 0.22 Q15 1 0.7434 0.7555 0.0586 11.00000 0.05 0.22 Q16 1 1.1328 0.9784 -0.1679 11.00000 0.05 0.22 Q17 1 0.3217 1.0198 -0.1808 11.00000 0.05 0.22 Q18 1 0.9215 1.1911 -0.1216 11.00000 0.05 0.21 Q19 1 1.2011 1.0030 0.1234 11.00000 0.05 0.21 Q20 1 0.4483 1.2448 0.1210 11.00000 0.05 0.21 Q21 1 0.4600 1.0232 -0.1230 11.00000 0.05 0.21 Q22 1 1.1554 0.8986 0.2858 11.00000 0.05 0.21 Q23 1 0.9773 0.9698 -0.1359 11.00000 0.05 0.21 Q24 1 0.5064 1.2146 0.0605 11.00000 0.05 0.21 Q25 1 0.6855 1.1596 -0.0563 11.00000 0.05 0.20 ; _shelx_res_checksum 34788 _shelx_hkl_file ; 0 0 3 34.4694 114.573 3 0 0 -3 49.3039 97.9524 4 0 0 -3-36.0260 83.0554 2 0 0 -3 230.454 135.493 3 0 0 3 67.9397 91.9066 2 0 0 4 5290.89 543.462 3 0 0 -4 5337.82 516.783 3 0 0 -4 4823.06 530.299 4 0 0 4 4565.68 423.720 2 0 0 -4 5005.85 440.881 2 0 0 5 163.782 277.574 3 0 0 -5 30.8714 96.1502 2 0 0 5 232.736 161.789 2 0 0 -5 728.149 214.600 3 0 0 -5 144.808 145.693 4 0 0 6 13369.4 890.168 2 0 0 6 12457.4 1009.84 3 0 0 7 37.7933 186.246 2 0 0 7-82.9043 249.861 3 0 0 8 110140. 3909.08 3 0 0 -8 120619. 3211.72 6 0 0 8 121185. 3638.44 2 0 0 -9 235.358 168.731 6 0 0 9-98.7378 240.825 2 0 0 9 68.3779 290.286 3 0 0 10 20964.7 1684.17 3 0 0 -10 22541.9 1262.26 6 0 0 10 24031.2 1562.59 2 0 0 11 172.644 295.707 2 0 0 -11 295.887 235.656 6 0 0 11 283.609 341.826 3 0 0 -12 60708.5 2414.07 6 0 0 12 63626.1 2923.99 2 0 0 12 55835.2 3080.21 3 0 0 13-465.691 430.289 3 0 0 13-16.1481 285.761 2 0 0 -13 393.451 285.319 6 0 0 14 24671.2 1919.92 2 0 0 14 18885.5 1922.46 3 0 0 -14 23099.8 1539.11 6 0 0 15 8.38385 356.933 2 0 0 -15 63.6781 230.968 6 0 0 15-391.230 490.223 3 0 0 16 34.9584 397.888 2 0 0 16-466.849 397.334 3 0 0 -16 62.0641 241.575 6 0 0 17-38.5313 382.819 2 0 0 -17 6.81735 291.664 6 0 0 18-441.803 422.151 2 0 0 -18-305.846 397.996 6 0 0 -19-609.803 445.645 6 0 0 19-505.790 587.556 2 0 0 20 5632.30 1147.71 2 0 0 -20 2499.42 690.689 6 0 0 21 235.974 481.454 2 0 -1 3 150145. 3317.34 2 0 -1 3 139602. 3336.16 3 0 -1 -3 132804. 3444.50 3 0 1 -3 150752. 3326.90 2 0 -1 3 154308. 3614.26 4 0 1 -3 157389. 3363.63 3 0 1 3 148993. 3527.68 3 0 1 3 150324. 3258.46 2 0 -1 -3 141126. 2924.70 1 0 1 3 164961. 2900.71 1 0 1 -4 1368.63 243.938 2 0 1 4 1322.80 129.751 1 0 -1 4 1038.72 280.916 4 0 1 4 1658.32 310.450 3 0 1 -4 1358.68 294.833 4 0 1 -4 1521.81 263.941 3 0 -1 -4 1126.04 141.611 1 0 -1 4 1490.33 252.372 2 0 -1 -4 798.042 239.606 3 0 -1 4 1395.78 267.383 3 0 1 4 1232.93 228.742 2 0 -1 -5 111940. 2949.78 2 0 -1 -5 105888. 2315.51 1 0 -1 5 113248. 3372.34 4 0 1 5 114505. 2254.32 1 0 1 5 110276. 3282.92 3 0 1 5 112372. 2954.09 2 0 1 -5 113822. 3090.12 3 0 -1 5 102234. 3101.18 3 0 -1 5 113449. 3016.02 2 0 1 -5 115167. 3017.76 2 0 -1 6 46560.2 2105.14 4 0 -1 -6 50427.8 1216.56 1 0 1 6 46027.6 1142.04 1 0 -1 6 47488.9 2005.73 3 0 1 6 49321.8 2126.38 3 0 1 6 50291.6 1843.09 2 0 -1 6 50608.3 1890.47 2 0 -1 -7 1420.28 249.127 6 0 -1 -7 1246.01 142.513 1 0 1 7 1615.92 354.253 2 0 -1 7 954.469 298.078 4 0 1 7 1452.00 376.226 3 0 -1 7 1021.65 324.525 3 0 1 7 1235.75 143.969 1 0 -1 7 1570.52 381.478 2 0 1 8 161696. 3265.80 1 0 1 8 154330. 4895.52 3 0 1 8 165595. 4468.17 2 0 -1 8 152143. 4753.06 3 0 -1 8 165625. 4536.86 2 0 -1 -8 172855. 3929.00 6 0 1 -9 77515.9 2604.58 6 0 1 9 82776.5 3383.00 3 0 -1 -9 88093.5 2496.99 6 0 1 9 75011.0 1767.58 1 0 1 9 83643.7 2973.15 2 0 -1 9 83476.9 3021.12 2 0 -1 9 78724.6 3222.06 3 0 1 10 311.058 282.492 2 0 1 -10 311.783 248.075 6 0 -1 -10 500.402 243.528 6 0 1 10 609.629 407.858 3 0 -1 10 149.124 219.285 2 0 -1 10 308.147 250.207 3 0 1 -11 8120.32 818.010 6 0 -1 -11 8522.58 754.534 6 0 -1 11 7689.02 1060.77 3 0 1 11 8353.14 969.998 2 0 -1 11 8053.43 957.975 2 0 1 11 7869.69 1085.50 3 0 1 12 2236.80 649.132 3 0 1 -12 2198.63 464.447 6 0 1 12 1211.73 437.708 2 0 -1 12 2069.49 560.485 2 0 -1 12 2219.38 573.212 3 0 -1 -12 2589.64 462.704 6 0 -1 13-63.0878 311.313 3 0 1 13 668.115 421.179 2 0 1 -13 624.496 320.906 6 0 -1 13 1087.62 472.286 2 0 1 13 746.462 498.459 3 0 -1 -13 1267.22 389.825 6 0 1 14 317.049 345.113 2 0 -1 14 590.291 395.880 2 0 -1 14-11.7773 453.683 3 0 -1 -14 231.525 222.483 6 0 1 14-76.9074 461.321 3 0 1 -14-249.330 286.594 6 0 -1 -15 34529.8 1883.42 6 0 1 15 33977.6 2331.31 2 0 1 15 32970.4 2619.56 3 0 1 -15 35247.0 2079.55 6 0 -1 15 33324.1 2569.52 3 0 -1 15 34535.7 2388.48 2 0 1 16 10517.2 1354.37 2 0 -1 16 8806.88 1256.56 2 0 1 16 12603.2 1702.43 3 0 1 -16 10662.3 1179.63 6 0 -1 -16 11681.7 1121.63 6 0 -1 17 6655.60 1142.37 2 0 -1 -17 4981.80 778.341 6 0 1 -17 5103.54 871.699 6 0 1 17 3751.88 886.744 2 0 -1 18 123.661 458.910 2 0 1 -18 205.603 317.226 6 0 1 18 619.453 513.711 2 0 -1 -18 180.733 302.938 6 0 -1 19 5620.24 1091.70 2 0 1 19 4839.66 1046.73 2 0 1 -19 5114.50 931.264 6 0 1 -20 5890.07 1062.82 6 0 1 20 5885.34 1173.67 2 0 1 -21 2500.70 787.002 6 0 1 21 4349.29 1077.14 2 0 1 22 129.842 584.146 2 0 2 -1 194184. 3915.74 5 0 -2 -2 9632.04 521.621 1 0 -2 2 8973.51 423.487 3 0 2 -2 9755.96 414.193 3 0 -2 -2 9044.30 568.646 3 0 -2 2 9829.06 487.459 1 0 2 2 10912.9 521.634 1 0 2 -2 9164.79 464.585 1 0 2 -2 9535.28 480.885 5 0 2 2 10205.4 584.050 3 0 2 3 28270.2 1201.20 3 0 -2 -3 25696.7 949.420 1 0 -2 3 26325.5 1004.38 3 0 -2 3 28990.2 879.857 1 0 2 -3 25194.7 852.925 1 0 2 3 29778.2 929.647 1 0 2 -3 29174.1 975.761 3 0 -2 -3 23507.4 1128.19 3 0 2 -4 1930.09 200.414 1 0 -2 -4 1975.72 338.146 3 0 -2 4 2104.97 329.603 3 0 2 -4 2052.87 290.442 3 0 2 4 2283.84 378.877 3 0 -2 -4 2038.54 243.823 1 0 2 -4 1957.30 305.602 2 0 -2 -4 2416.59 177.025 6 0 2 4 2234.31 226.360 1 0 -2 -5 103894. 2622.19 1 0 -2 -5 123731. 2494.92 6 0 -2 5 114346. 3497.59 4 0 2 -5 119831. 3093.01 3 0 2 5 110168. 3010.19 2 0 2 -5 113988. 2412.35 1 0 2 5 110527. 3380.17 3 0 2 5 119763. 2528.49 1 0 -2 5 108223. 3130.02 3 0 -2 -6 55781.8 1654.53 1 0 -2 -6 64394.1 1633.99 6 0 -2 6 56818.9 2227.33 3 0 -2 6 56889.6 2450.22 4 0 2 6 59760.4 2419.79 3 0 2 -6 65589.5 1431.88 1 0 2 6 61353.1 1553.13 1 0 2 6 59969.5 2101.46 2 0 -2 7 20988.9 1507.88 4 0 2 -7 22402.7 641.019 1 0 2 7 21663.5 1247.15 2 0 -2 -7 21947.6 867.272 1 0 2 7 20353.5 1435.51 3 0 -2 7 21008.7 1276.55 2 0 2 7 23822.1 819.498 1 0 -2 7 20947.4 1369.55 3 0 -2 -7 24800.0 951.033 6 0 -2 8 3608.98 568.111 2 0 -2 -8 3146.40 303.452 1 0 -2 8 3251.40 614.598 4 0 2 8 3266.89 284.984 1 0 -2 -8 3592.31 377.344 6 0 -2 8 4274.97 651.881 3 0 2 8 3741.53 676.602 3 0 2 8 4232.92 584.165 2 0 2 9 35603.8 1123.31 1 0 2 9 36955.4 2202.82 3 0 2 9 39765.7 1930.48 2 0 -2 9 37612.8 2273.11 4 0 2 -9 34860.4 1684.05 6 0 -2 9 38310.6 2119.91 3 0 -2 -9 38342.1 1426.73 6 0 -2 9 38500.7 1966.86 2 0 2 -10 15275.6 1111.04 6 0 2 10 15077.2 685.162 1 0 -2 10 14040.7 1445.52 4 0 -2 -10 17713.4 966.515 6 0 -2 10 16501.5 1324.19 2 0 -2 10 14461.2 1367.53 3 0 2 10 15823.1 1509.59 3 0 2 10 15811.2 1248.37 2 0 2 11 119754. 4617.08 3 0 -2 -11 124047. 3291.69 6 0 -2 11 119733. 4432.70 3 0 2 -11 110226. 3646.09 6 0 2 11 116394. 2716.60 1 0 -2 11 117347. 4121.61 2 0 2 11 113871. 3976.59 2 0 2 -12 9782.81 967.100 6 0 -2 -12 9467.00 784.253 6 0 -2 12 8964.15 1072.11 2 0 2 12 9123.34 1042.63 2 0 2 12 9533.98 1273.31 3 0 -2 12 7660.09 1080.88 3 0 2 12 8776.83 504.172 1 0 -2 -13 38532.3 1757.64 6 0 2 13 37747.8 2620.92 3 0 2 -13 36422.9 2011.58 6 0 -2 13 36307.4 2504.32 3 0 -2 13 36875.6 2310.28 2 0 2 13 39143.6 2317.09 2 0 2 14 1387.12 550.148 2 0 -2 14 905.899 511.384 2 0 2 14 2416.64 860.592 3 0 2 -14 707.281 384.035 6 0 -2 14 660.335 402.452 3 0 -2 -14 1543.16 413.906 6 0 2 -15 1778.91 498.809 6 0 2 15 1133.82 619.958 2 0 -2 -15 1489.66 353.053 6 0 -2 15 1583.70 616.629 3 0 -2 15 1781.30 557.735 2 0 2 15 1647.04 631.646 3 0 2 16 208.697 380.146 2 0 -2 -16-1.47343 213.324 6 0 2 -16-107.680 296.538 6 0 2 -17 236.581 337.943 6 0 -2 -17 283.010 241.414 6 0 2 17-194.101 428.794 2 0 2 18-516.669 504.271 2 0 2 -18 349.399 457.087 6 0 2 19-176.307 448.286 2 0 2 -19-446.841 483.635 6 0 2 -20 179.977 397.177 6 0 2 20 638.038 572.535 2 0 2 -21 3563.43 924.543 6 0 2 21 5525.19 1224.10 2 0 2 22 1384.77 517.569 2 0 2 -22 865.208 579.637 6 0 -3 0 168.114 127.305 1 0 3 0 14.8106 139.150 1 0 -3 -1 143.283 107.764 3 0 3 1 129.801 120.261 1 0 3 1 98.3849 98.2919 3 0 3 1 144.450 62.4600 6 0 -3 1 53.6416 98.0685 1 0 -3 -1 213.915 122.415 1 0 -3 1 112.177 95.3924 5 0 3 -1 16.3982 100.236 1 0 3 -2 333090. 6467.32 5 0 -3 2 325664. 6468.26 5 0 -3 -2 319474. 6586.15 1 0 3 2 337681. 6525.09 3 0 -3 2 326711. 6500.67 1 0 -3 -2 322762. 6553.35 3 0 3 -2 306296. 6401.39 1 0 3 2 322757. 6474.16 1 0 3 -3 12843.8 586.541 3 0 -3 -3 13169.3 832.016 3 0 3 -3 12223.1 658.367 1 0 -3 -3 14492.2 788.234 1 0 3 -3 14041.4 720.793 5 0 -3 3 13374.5 685.686 1 0 3 3 14033.6 833.782 3 0 -3 3 14433.1 643.863 3 0 3 3 15006.5 734.186 1 0 3 4 159160. 4116.19 3 0 3 -4 161248. 3666.99 5 0 -3 4 165215. 3546.77 1 0 -3 -4 161396. 3768.24 1 0 3 -4 154317. 3512.61 1 0 -3 -4 147604. 4068.20 3 0 3 -4 166266. 3621.58 3 0 -3 4 169141. 3764.30 3 0 3 4 165393. 3610.44 1 0 3 -5 52.7056 118.687 3 0 3 5 258.805 202.414 3 0 -3 5 218.657 173.841 3 0 -3 -5 87.3447 103.040 1 0 3 -5 111.183 98.4548 1 0 3 5 167.352 98.2539 1 0 -3 -5 77.8583 44.9175 6 0 3 6 147053. 4375.04 3 0 -3 -6 160500. 3133.79 6 0 -3 6 157555. 4141.79 3 0 3 6 155734. 3439.36 1 0 3 -6 154662. 3910.37 3 0 3 -6 154300. 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2176.81 826.215 6 -2 8 18 1330.09 708.528 2 2 8 -18 1275.81 831.767 6 2 -8 18 988.722 809.015 4 2 8 -17 49.1722 528.517 6 -2 8 17-197.011 471.873 2 2 -8 17 275.272 689.780 4 2 -8 16 7996.75 1491.53 4 2 8 -16 5778.10 1230.80 6 -2 8 16 7213.66 1321.77 2 2 -8 15-60.7850 320.042 3 2 8 -15 351.047 599.749 6 2 -8 15-311.275 644.794 4 -2 8 15 646.232 546.821 2 -2 8 14 2525.02 645.997 1 2 -8 14 4462.39 875.581 3 2 -8 14 2726.86 848.885 4 2 8 -14 4971.80 1081.40 6 -2 8 14 5193.76 1121.73 2 -2 8 13 1632.95 555.834 1 2 -8 13 1703.05 566.545 3 2 -8 13 799.107 524.717 4 2 8 -13 3000.63 897.873 6 -2 8 13 1960.16 750.480 2 2 -8 12 348.243 327.098 3 -2 8 12 809.148 442.831 1 2 8 -12 959.452 534.830 6 2 8 -12 486.569 319.948 1 2 -8 12 568.378 608.749 4 2 8 -11 1768.23 505.716 1 2 -8 11 1003.51 500.817 4 2 -8 11 1539.13 482.237 3 -2 8 11 1664.67 578.198 1 2 8 -11 1409.25 616.799 6 2 8 -10 2650.18 566.996 1 2 -8 10 2717.03 566.618 3 -2 8 10 3032.02 674.438 1 2 8 -10 2404.83 742.369 6 2 -8 9 1157.69 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261.135 3 2 8 1 165.519 330.410 1 -2 8 -1 12.5534 259.343 1 2 8 1 480.907 334.595 6 -2 8 -1 544.724 452.280 5 2 8 2 753.075 365.282 1 2 8 2 624.730 297.741 3 -2 8 -2 147.566 296.896 1 2 8 2 293.380 273.190 6 -2 8 -2 274.356 349.025 5 2 8 3 7118.17 778.818 3 -2 8 -3 6809.84 910.090 1 2 8 3 6866.92 835.565 6 2 8 3 6582.16 844.173 1 -2 8 -3 7913.71 1012.23 5 2 8 4 27019.8 1597.79 3 -2 8 -4 29175.3 1872.25 1 2 8 4 26645.0 1737.55 1 2 8 4 24996.4 1565.57 6 -2 8 -4 29997.1 1995.77 5 2 8 5 32030.7 1835.41 3 -2 8 -5 31833.0 1950.25 1 2 8 5 33672.5 1952.53 1 2 8 5 30446.1 1646.14 6 -2 8 -5 34626.4 2198.19 5 2 8 6 12030.5 1138.72 3 -2 8 -6 11763.3 1167.30 1 -2 8 -6 14350.7 1444.97 5 2 8 6 14229.5 1263.19 1 2 8 6 13455.9 1002.61 6 2 8 7 17771.1 1469.91 3 -2 8 -7 16509.0 1357.29 1 2 8 7 17117.9 1389.48 1 -2 8 -7 16597.1 1575.51 5 2 8 8 33463.1 2134.52 3 -2 8 -8 31715.7 1916.44 1 2 8 8 31954.4 1935.14 1 -2 8 -8 32124.5 2252.57 5 2 8 9 1595.91 604.907 3 -2 8 -9 1238.03 448.637 1 2 8 9 1512.22 480.861 1 -2 8 -9 2190.03 657.247 5 2 8 9 1700.74 465.330 2 -2 -8 10 1630.67 618.415 4 2 8 10 1238.22 522.984 3 -2 8 -10 2050.29 544.635 1 2 8 10 1509.78 455.237 1 -2 8 -10 1304.98 541.920 5 2 8 10 1791.39 460.864 2 -2 -8 11 976.931 496.297 4 2 8 11 203.807 301.984 1 -2 8 -11 689.370 355.313 1 2 8 11 1027.29 555.000 3 -2 8 -11 510.591 461.629 5 2 8 11 465.996 256.702 2 -2 -8 12 201.573 413.777 4 2 8 12-143.489 452.982 3 -2 8 -12 576.431 570.583 5 2 8 12 390.450 304.795 2 2 8 12 337.317 292.529 1 -2 -8 13 1115.62 472.863 4 2 8 13 547.715 457.416 3 2 8 13 1559.37 434.283 1 2 8 13 496.722 332.952 2 -2 8 -13 1699.55 699.837 5 2 8 14 2492.05 852.680 3 2 8 14 2907.30 656.154 2 -2 -8 14 3247.73 976.751 4 -2 8 -14 3526.49 906.813 5 -2 -8 15 89.7665 467.868 4 2 8 15 158.162 510.521 3 -2 8 -15-154.186 421.630 5 2 8 16 9192.62 1545.95 3 -2 8 -16 6700.58 1295.33 5 -2 -8 16 6873.26 1399.95 4 2 8 17 305.112 623.395 3 -2 8 -17-715.926 695.041 5 -2 -8 17 79.3510 475.290 4 2 8 18 534.058 645.115 3 -2 8 -18 862.700 677.587 6 2 8 19 349.206 647.932 3 -2 9 18-580.440 471.144 2 2 -9 18 80.6415 499.038 4 -2 9 17 105.825 556.699 2 2 -9 17 299.535 441.129 4 2 9 -17 568.619 617.801 6 2 -9 16 2286.42 897.594 4 2 9 -16 3828.18 1093.05 6 -2 9 16 2555.68 842.661 2 2 -9 15 806.510 642.370 4 2 9 -15 1761.56 753.628 6 -2 9 15 1005.74 484.533 2 -2 9 14 1840.71 612.791 1 2 9 -14 2118.02 847.141 6 2 -9 14 1852.91 803.164 4 -2 9 14 3275.08 982.025 2 2 -9 13 2427.73 796.311 4 -2 9 13 1906.93 644.137 1 -2 9 13 1122.96 565.144 2 2 9 -13 3644.19 957.642 6 2 -9 12 2615.40 879.797 4 -2 9 12 2932.14 782.726 1 2 9 -12 2357.87 559.523 1 2 9 -12 4023.93 988.421 6 2 -9 11 9291.38 1046.42 3 2 9 -11 10042.1 1115.66 1 -2 9 11 11227.1 1335.24 1 2 9 -11 8864.36 1354.55 6 2 -9 11 7408.36 1299.87 4 2 -9 10 4345.31 686.322 3 -2 9 10 2353.20 585.381 1 2 9 -10 3566.40 846.420 6 2 9 -10 5110.76 805.604 1 2 -9 9 9762.16 982.489 3 2 9 -9 10011.8 1109.86 1 -2 9 9 7436.76 1061.50 1 2 9 -9 8390.56 1259.65 6 2 9 -8 2285.92 568.151 1 2 -9 8 1919.38 428.963 3 -2 9 8 2278.63 609.615 1 2 9 -8 1801.34 631.082 6 2 9 -7 7516.05 944.171 1 2 -9 7 5060.34 682.948 3 2 9 -7 5458.24 979.008 6 -2 9 7 4914.17 859.309 1 2 -9 6 522.643 276.784 3 2 9 -6 602.317 357.982 1 -2 9 6 348.151 369.640 1 2 9 -6 1438.13 616.145 6 2 -9 5 2586.64 521.525 3 2 9 -5 3144.87 753.641 6 2 9 -5 3146.11 647.183 1 -2 9 5 3019.70 672.899 1 2 -9 4 13527.6 1158.69 3 -2 9 4 10176.1 1199.50 1 2 9 -4 14153.4 1312.93 1 2 9 -4 12845.7 1393.19 6 2 9 -3 23714.3 1266.26 3 -2 9 3 21085.4 1714.00 1 2 9 -3 19694.6 1556.29 1 2 9 -3 19889.6 1692.16 6 2 9 -2 7567.44 967.723 1 2 9 -2 7619.50 675.507 3 -2 9 2 6914.37 982.413 1 2 9 -2 6875.76 964.846 6 2 9 -1 9697.36 760.040 3 2 9 -1 8454.15 1009.68 1 -2 9 1 8900.31 1126.73 1 2 9 -1 6800.25 926.825 6 2 9 0 13708.0 931.363 3 -2 9 0 14078.1 1387.09 1 2 9 0 16026.9 1373.24 1 2 9 0 12988.8 1254.39 6 2 9 1 6216.73 648.973 3 2 9 1 6592.19 875.990 6 2 9 1 5831.15 856.051 1 -2 9 -1 7074.02 983.784 1 2 9 2 6989.08 730.381 3 2 9 2 7544.02 968.301 1 -2 9 -2 7141.95 988.080 1 2 9 2 6528.52 865.370 6 -2 9 -2 8821.37 1124.20 5 2 9 3 20118.3 1302.55 3 -2 9 -3 22737.6 1753.60 1 2 9 3 21451.2 1621.43 1 2 9 3 21318.7 1538.86 6 -2 9 -3 23994.1 1834.08 5 2 9 4 11385.1 1021.95 3 -2 9 -4 12651.9 1271.64 1 2 9 4 11529.4 1200.49 1 2 9 4 11067.7 1046.67 6 -2 9 -4 13062.8 1378.70 5 2 9 5 2002.64 433.908 6 2 9 5 3112.16 598.169 3 -2 9 -5 2732.09 629.289 1 -2 9 -5 3869.29 800.560 5 2 9 5 3062.93 633.729 1 -2 9 -6-14.1733 302.524 1 2 9 6 347.048 345.606 3 2 9 6 718.690 295.308 6 2 9 6 517.743 369.880 1 -2 9 -6 398.090 390.679 5 2 9 7 7061.55 963.062 3 2 9 7 7129.46 955.701 1 -2 9 -7 7078.39 950.384 1 -2 9 -7 7136.15 1112.36 5 2 9 8 2010.13 564.904 3 2 9 8 1986.73 509.734 1 -2 9 -8 1950.75 514.487 1 -2 9 -8 1476.85 588.849 5 2 9 9 8069.85 1117.67 3 2 9 9 8879.30 1040.67 1 -2 9 -9 8989.91 1056.68 1 -2 9 -9 10574.6 1369.69 5 -2 -9 10 3404.79 886.239 4 2 9 10 3553.20 713.184 1 2 9 10 4969.14 984.780 3 -2 9 -10 4409.59 765.232 1 -2 9 -10 4726.45 944.108 5 2 9 10 3351.41 648.544 2 -2 9 -11 11335.7 1198.14 1 2 9 11 10076.8 1361.64 3 2 9 11 10914.3 1162.79 1 -2 9 -11 11594.4 1518.96 5 2 9 11 10275.8 1108.93 2 -2 -9 11 9524.73 1430.79 4 -2 -9 12 1064.63 603.115 4 2 9 12 2449.46 792.114 3 2 9 12 1638.67 483.948 1 2 9 12 2678.86 614.262 2 -2 9 -12 1996.65 752.581 5 -2 -9 13 1296.18 667.091 4 2 9 13 1650.79 674.439 3 2 9 13 1587.89 503.138 1 2 9 13 1980.31 546.761 2 -2 9 -13 1510.51 696.937 5 -2 -9 14 1986.81 736.387 4 2 9 14 2092.30 866.409 3 -2 9 -14 3111.66 872.300 5 -2 -9 15 2509.98 892.011 4 2 9 15 1518.54 777.786 3 -2 9 -15 1805.25 707.833 5 -2 -9 16 3071.98 923.445 4 2 9 16 1363.75 721.265 3 -2 9 -16 3190.54 948.082 5 2 9 17-773.248 779.652 3 -2 9 -17 369.882 492.905 5 -2 -9 17 820.986 698.490 4 2 9 18 252.970 625.727 3 -2 -9 18-614.279 586.431 4 2 10 -17 3788.34 1092.56 6 -2 10 17 6063.17 1297.61 2 2 -10 17 4138.31 1115.29 4 2 -10 16-259.855 569.072 4 2 10 -16 1568.45 728.562 6 -2 10 16 1013.94 726.549 2 2 -10 15-224.956 627.778 4 2 10 -15 324.571 551.004 6 -2 10 15 487.771 561.548 2 2 -10 14 1261.67 719.581 4 -2 10 14 532.392 441.906 1 2 10 -14 716.781 538.668 6 -2 10 14 430.743 460.780 2 2 -10 13-1094.91 633.989 4 -2 10 13-135.162 368.043 1 2 -10 12-215.849 526.464 4 2 10 -12 348.152 277.820 1 -2 10 12-96.9600 344.174 1 2 10 -12 855.226 617.368 6 2 10 -11 1225.51 471.638 1 -2 10 11 140.343 384.541 1 2 10 -11 1390.86 734.842 6 -2 10 10 1176.03 552.738 1 2 10 -10 1903.21 552.412 1 2 10 -10 1795.88 707.821 6 2 10 -9 3693.27 726.805 1 2 10 -9 2707.02 800.015 6 -2 10 9 2437.98 715.396 1 2 10 -8 1794.23 713.484 6 -2 10 8 261.155 312.197 1 2 10 -8 1213.38 465.236 1 2 10 -7 3673.48 870.949 6 -2 10 7 3442.77 783.004 1 2 10 -7 3476.83 706.513 1 2 -10 6 1962.77 416.590 3 -2 10 6 3001.85 745.407 1 2 10 -6 2995.32 769.729 6 2 10 -6 2677.79 650.160 1 2 -10 5 14096.3 1103.72 3 -2 10 5 13809.4 1473.80 1 2 10 -5 15893.7 1463.82 1 2 10 -5 14636.7 1571.76 6 2 10 -4 5931.00 896.625 1 2 -10 4 5115.83 673.103 3 -2 10 4 4572.97 868.250 1 2 10 -4 6555.78 1014.98 6 2 -10 3 19554.0 1381.80 3 -2 10 3 19703.8 1738.99 1 2 10 -3 20873.5 1656.48 1 2 10 -3 17672.5 1642.01 6 2 10 -2 3710.34 782.216 1 2 10 -2 3253.02 732.065 6 -2 10 2 2990.87 711.429 1 2 10 -1 461.090 378.876 1 2 10 -1 566.119 179.823 3 2 10 -1 275.871 323.615 6 -2 10 1 580.195 358.936 1 2 10 0 2361.76 589.195 1 2 10 0 4186.63 464.730 3 2 10 0 3282.89 680.755 6 -2 10 0 3043.82 757.717 1 2 10 1 895.683 416.522 1 2 10 1 716.507 230.933 3 -2 10 -1 557.736 452.090 1 2 10 1 317.288 236.753 6 2 10 2 3587.74 746.145 1 2 10 2 3473.53 494.003 3 2 10 2 3399.54 686.307 6 -2 10 -2 3001.73 694.934 1 2 10 3 18684.6 1248.16 3 -2 10 -3 19170.5 1681.96 1 2 10 3 18571.0 1587.69 1 2 10 3 19752.1 1515.71 6 -2 10 -3 18464.1 1698.24 5 2 10 4 6079.38 753.166 3 -2 10 -4 4897.12 864.678 1 2 10 4 5091.45 855.370 1 2 10 4 5779.01 785.533 6 -2 10 -4 6862.95 1080.82 5 2 10 5 10397.9 1045.20 3 -2 10 -5 12042.5 1321.93 1 2 10 5 11367.3 1261.89 1 2 10 5 10514.4 967.182 6 -2 10 -5 13912.0 1499.35 5 2 10 6 3022.24 628.263 3 2 10 6 3238.61 641.636 1 -2 10 -6 3382.32 679.627 1 -2 10 -6 3564.46 830.968 5 2 10 7 6083.79 919.913 3 2 10 7 5852.56 909.025 1 -2 10 -7 6721.65 1085.21 5 -2 10 -7 5094.27 871.092 1 2 10 8 615.895 360.379 3 2 10 8 1066.44 463.902 1 -2 10 -8 1118.59 438.178 1 -2 10 -8 1617.07 686.948 5 2 10 9 2930.15 681.474 1 2 10 9 4281.19 832.905 3 -2 10 -9 2702.27 629.473 1 -2 10 -9 2875.42 812.901 5 2 10 10 1620.45 612.858 3 -2 10 -10 1485.82 484.933 1 -2 10 -10 943.074 601.970 5 2 10 10 1033.99 489.249 1 -2 -10 11 867.441 588.261 4 2 10 11 607.377 614.846 3 -2 10 -11 1233.66 561.368 1 2 10 11 748.616 419.507 1 -2 10 -11 601.233 579.903 5 2 10 11 453.264 316.910 2 -2 -10 12-363.525 408.057 4 2 10 12-76.4848 443.797 3 2 10 12-9.45970 325.184 1 -2 10 -12 717.963 596.759 5 2 10 12 61.3690 307.772 2 2 10 13 981.429 632.851 3 -2 -10 13-82.0432 412.419 4 2 10 13 418.582 342.029 1 -2 10 -13 559.396 664.016 5 2 10 14 1105.63 654.434 3 -2 -10 14 1163.19 606.452 4 -2 10 -14 821.347 545.128 5 -2 -10 15 298.661 447.045 4 2 10 15 1025.57 682.500 3 -2 10 -15 1098.86 736.295 5 -2 -10 16-80.4661 459.255 4 2 10 16 835.602 603.860 3 -2 10 -16 1043.78 660.903 5 -2 -10 17 3184.35 1037.66 4 2 10 17 3596.83 1129.82 3 -2 10 -17 2782.30 933.908 6 -2 10 -17 6200.71 1283.54 5 2 10 18-209.739 454.251 3 2 -11 17 1812.03 953.479 4 2 -11 16 1230.83 871.423 4 2 11 -16 1627.66 790.897 6 -2 11 16 1162.31 678.799 2 2 -11 15-113.634 623.012 4 2 11 -15 1073.69 681.740 6 -2 11 15-474.969 549.043 2 2 -11 14 1606.64 751.307 4 -2 11 14 1613.49 649.419 1 2 11 -14 1700.31 782.264 6 -2 11 14 1068.81 640.376 2 2 -11 13-407.961 648.087 4 -2 11 13-243.503 373.319 1 2 -11 12 4549.62 1238.48 4 -2 11 12 1269.16 580.946 1 2 11 -12 4065.89 1058.06 6 2 11 -11 1672.53 571.513 1 -2 11 11 1330.35 574.399 1 2 11 -11 2128.55 839.226 6 2 11 -10 4481.74 824.311 1 -2 11 10 3713.46 895.196 1 2 11 -10 4460.96 1026.78 6 2 11 -9 1924.79 599.874 1 -2 11 9 1038.38 527.647 1 2 11 -9 2750.28 814.084 6 2 11 -8 6082.89 955.261 1 -2 11 8 5643.38 1012.34 1 2 11 -8 7458.53 1217.37 6 2 11 -7 3740.55 808.458 1 -2 11 7 3633.75 861.505 1 2 11 -7 3495.37 880.293 6 -2 11 6-221.375 411.971 1 2 11 -6-88.2693 329.439 1 2 11 -6 225.141 406.433 6 -2 11 5 9734.31 1314.55 1 2 11 -5 9511.78 1195.14 1 2 11 -5 10875.4 1406.93 6 2 11 -4 529.798 471.762 1 -2 11 4-30.4525 373.109 1 2 11 -4 536.576 489.834 6 2 11 -3 701.514 477.818 1 2 11 -3 217.922 336.157 6 -2 11 3 610.824 470.959 1 2 11 -2 15161.7 1497.43 1 2 11 -2 14499.1 1485.09 6 -2 11 2 11556.0 1431.44 1 2 11 -1 2662.39 660.132 6 -2 11 1 2408.89 692.777 1 2 11 -1 2079.16 595.680 1 2 11 0 6195.50 924.965 6 -2 11 0 8371.84 1186.50 1 2 11 0 9349.95 1200.28 1 2 11 1 2015.60 570.285 6 2 11 1 3013.37 720.849 1 -2 11 -1 1341.38 542.088 1 2 11 2 13690.4 1428.42 1 -2 11 -2 12460.6 1440.67 1 2 11 2 14231.9 1348.36 6 2 11 3 1233.70 341.489 3 -2 11 -3 879.864 483.804 1 2 11 3 1672.29 584.507 1 2 11 3 1023.06 379.202 6 2 11 4 172.106 206.195 3 2 11 4 325.223 410.704 1 -2 11 -4 917.428 516.470 1 2 11 4 617.992 298.060 6 2 11 5 12211.0 1166.09 3 -2 11 -5 14186.9 1509.84 1 2 11 5 10247.2 1241.16 1 -2 11 -5 12727.4 1525.20 5 2 11 6-298.350 247.901 3 2 11 6-576.671 483.097 1 -2 11 -6 36.6591 421.656 1 -2 11 -6 327.404 560.618 5 2 11 7 3207.59 723.659 1 2 11 7 2492.21 617.021 3 -2 11 -7 2896.75 710.906 1 -2 11 -7 4057.27 955.521 5 2 11 8 5349.97 897.742 1 2 11 8 4669.76 827.496 3 -2 11 -8 7798.94 1250.58 5 -2 11 -8 5316.01 952.504 1 2 11 9 909.275 456.300 3 -2 11 -9 1817.43 569.531 1 -2 11 -9 1880.53 708.164 5 2 11 9 1105.45 450.109 1 2 11 10 4991.25 976.143 3 -2 11 -10 5739.49 934.762 1 2 11 10 5063.80 886.359 1 -2 11 -10 6662.66 1235.25 5 2 11 11 666.686 466.022 3 -2 11 -11 1807.98 614.167 1 2 11 11 1397.87 519.884 1 -2 11 -11 2046.19 831.625 5 -2 -11 12 2483.68 837.282 4 2 11 12 2372.95 853.939 3 2 11 12 4594.14 832.625 1 -2 11 -12 4341.70 1035.86 5 -2 -11 13-372.240 439.638 4 2 11 13 728.079 601.138 3 2 11 13 344.308 374.129 1 -2 11 -13 75.2960 612.867 5 -2 -11 14 592.078 537.061 4 2 11 14 526.223 538.313 3 -2 11 -14 1830.07 791.734 5 -2 -11 15-249.205 574.934 4 2 11 15-518.423 604.434 3 -2 11 -15-85.4032 484.676 5 -2 -11 16 827.057 723.870 4 2 11 16 1895.37 822.528 3 -2 11 -16 626.301 675.695 6 -2 11 -16 836.060 687.676 5 2 11 17 2524.86 934.478 3 2 -12 15 748.720 731.693 4 -2 12 15 1080.90 710.752 2 2 -12 14 1023.56 744.346 4 -2 12 14 1218.80 689.775 1 2 12 -14 201.913 447.564 6 2 -12 13 2016.98 851.447 4 -2 12 13 1282.61 590.065 1 2 12 -13 2159.37 886.334 6 -2 12 12-689.960 639.149 1 2 12 -12 1756.80 830.975 6 -2 12 11 967.400 440.946 1 2 12 -11 1814.36 828.727 6 2 12 -11 1401.79 431.804 1 2 12 -10 1736.46 565.064 1 -2 12 10 546.028 495.459 1 2 12 -10 769.620 692.072 6 2 12 -9 1234.02 518.868 1 2 12 -9 855.001 669.321 6 -2 12 9 858.591 498.612 1 2 12 -8 3752.68 783.474 1 -2 12 8 3944.44 986.053 1 2 12 -8 4879.06 1047.92 6 2 12 -7 1884.33 588.691 1 2 12 -7 1397.51 650.836 6 -2 12 7 1027.39 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1 -4 3 -2 11963.1 1357.11 1 -4 -3 2 9548.83 692.063 2 4 3 2 8089.64 1183.09 6 4 -3 -2 9414.61 1208.77 6 -4 -3 2 8811.48 660.519 4 -4 -3 2 11224.9 1282.89 1 -4 3 -3 13316.7 1419.13 1 4 -3 -3 14038.8 1471.94 6 4 3 3 12607.1 1455.69 6 4 3 3 13521.1 1609.67 3 -4 -3 3 14186.1 918.177 2 -4 -3 3 14770.5 1460.29 1 -4 3 -4 19505.5 1741.07 1 4 3 4 22171.5 2064.75 3 4 -3 -4 19262.6 1754.87 6 4 3 4 18895.5 1794.84 6 -4 -3 4 20508.0 1221.09 2 -4 -3 4 23634.8 1872.79 1 -4 -3 5 290.472 280.672 1 4 3 5-281.031 462.369 3 -4 -3 5 200.554 211.176 2 -4 3 -5 270.996 410.577 1 4 -3 -5-222.496 347.484 6 -4 3 -6 33532.0 2291.48 1 4 3 6 33376.1 2570.48 3 4 -3 -6 31968.2 2282.23 6 -4 -3 6 31949.1 1763.12 2 -4 -3 6 32010.5 2219.86 1 -4 -3 7 1496.02 575.612 1 4 3 7 481.210 485.348 3 -4 -3 7 643.924 327.624 2 -4 3 -7 515.439 385.128 1 4 -3 -7 775.377 417.377 6 -4 -3 8 8877.26 1185.37 1 4 3 8 9037.75 1363.63 3 -4 -3 8 9227.01 1039.21 2 -4 3 -8 10738.3 1299.64 1 4 -3 -8 9642.56 1269.59 6 4 3 9 10959.8 1501.40 3 -4 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5588.30 1202.05 3 4 4 -15 5174.18 1220.76 6 -4 4 15 2709.86 859.951 2 4 -4 14 1458.39 734.537 3 4 4 -14 143.661 452.875 6 -4 4 14 1775.16 625.246 1 -4 4 14 889.968 598.029 2 4 -4 13 1142.74 596.433 3 -4 4 13 966.258 518.693 1 -4 4 13 1000.92 600.224 2 4 -4 12 10416.8 1519.87 3 4 4 -12 9476.06 1621.41 6 -4 4 12 8453.10 1324.50 1 -4 4 12 8704.40 1316.11 2 4 -4 11 1279.29 602.135 3 4 4 -11 2446.87 831.640 6 -4 4 11 1129.78 535.649 1 -4 4 11 2587.14 772.407 2 4 -4 10 6335.84 1184.32 3 4 4 -10 7626.47 1357.40 6 -4 4 10 7614.87 1231.84 1 -4 4 10 7780.20 1161.99 2 4 -4 9 10680.6 1538.75 3 4 4 -9 7572.37 1350.64 6 -4 4 9 8011.99 1226.56 1 -4 4 9 6752.81 1033.08 2 4 -4 9 7130.68 928.780 4 4 -4 8 906.724 550.232 3 4 4 -8 1687.90 609.832 6 -4 4 8 1970.38 635.016 1 -4 4 8 714.368 410.408 2 4 -4 8 1372.30 413.208 4 4 -4 7 3091.31 564.089 4 4 -4 7 4938.02 1124.98 3 4 4 -7 3382.40 898.026 6 -4 4 7 3659.08 829.618 1 4 -4 6 4230.07 618.942 4 4 -4 6 4394.96 964.585 3 4 4 -6 5909.92 1138.11 6 -4 4 6 3594.28 827.515 1 4 -4 5 8259.39 1292.75 3 4 4 -5 7393.51 1229.87 6 -4 4 5 8075.33 884.647 5 -4 4 5 7745.31 1145.16 1 4 -4 5 7256.24 743.648 4 4 4 -4 11371.6 1499.82 6 -4 4 4 10890.2 1030.81 5 -4 4 4 9550.87 1269.37 1 4 -4 4 8956.49 778.548 4 -4 4 3 20124.2 1848.31 1 4 4 -3 22167.4 1997.44 6 -4 4 3 24474.3 1596.24 5 4 4 -2 9082.58 1289.13 6 -4 4 2 7271.82 893.844 5 -4 4 2 8610.09 1206.60 1 4 4 -1 7246.66 1133.57 6 -4 4 1 8446.37 1171.21 1 4 4 0 12232.4 1443.27 6 -4 4 0 11065.2 1351.80 1 4 4 1 8847.08 1237.11 6 -4 4 -1 7064.34 1067.04 1 -4 -4 1 8940.79 687.713 4 4 4 2 5440.65 982.272 6 -4 4 -2 6563.28 1014.81 1 -4 -4 2 5663.49 615.516 4 -4 4 -3 24216.3 1933.32 1 4 4 3 21979.3 2039.52 3 4 4 3 23443.6 2008.23 6 4 -4 -3 22329.1 1856.29 6 -4 -4 3 22784.0 1317.49 4 -4 4 -4 11642.0 1349.41 1 4 4 4 10517.3 1414.33 3 4 -4 -4 11878.3 1346.90 6 4 4 4 10414.2 1331.22 6 -4 -4 4 9422.53 915.862 4 4 4 5 6078.28 1101.06 3 4 -4 -5 6240.48 992.081 6 -4 4 -5 5459.81 929.211 1 -4 -4 5 5834.73 757.508 4 4 4 6 3533.05 866.883 3 -4 -4 6 4506.88 654.478 2 4 -4 -6 4046.79 849.627 6 -4 4 -6 3549.99 812.685 1 -4 -4 6 4056.38 670.356 4 4 4 7 4846.33 1022.94 3 -4 -4 7 4494.32 692.868 2 4 -4 -7 5908.81 987.995 6 -4 4 -7 5419.09 929.617 1 -4 -4 7 5182.47 789.424 4 4 4 8 2534.27 801.110 3 -4 -4 8 1752.50 482.434 2 -4 4 -8 1209.45 502.510 1 4 -4 -8 1517.98 579.877 6 4 4 9 7452.90 1244.48 3 -4 -4 9 7444.63 981.064 2 -4 4 -9 6897.64 1088.41 1 4 -4 -9 7721.43 1141.39 6 4 4 10 8046.09 1312.70 3 -4 -4 10 9916.27 1170.80 2 -4 4 -10 8399.96 1186.11 1 4 -4 -10 9701.92 1322.18 6 4 4 11 1882.62 740.943 3 -4 -4 11 1957.81 579.517 2 -4 4 -11 2268.12 686.797 1 4 -4 -11 999.953 476.585 6 4 4 12 8300.10 1345.72 3 -4 -4 12 7464.95 1102.70 2 4 -4 -12 7207.33 1183.81 6 4 4 13 2523.31 894.347 3 -4 -4 13 981.336 568.217 2 4 -4 -13 908.582 510.446 6 4 4 14 3226.40 985.463 3 -4 -4 14 2570.23 782.643 2 4 -4 -14 1135.11 649.742 6 4 4 15 2911.38 891.103 3 -4 -4 15 5295.93 1103.27 2 4 4 16-229.883 553.366 3 4 4 17 871.093 629.791 3 4 -5 18 829.419 724.887 3 4 5 -18-603.411 923.065 6 4 -5 17 2483.77 946.493 3 4 5 -17-29.6663 841.635 6 -4 5 17 1736.90 820.916 2 4 -5 16-95.1744 535.369 3 -4 5 16 224.885 576.581 2 4 -5 15 7584.52 1365.57 3 4 5 -15 7415.48 1627.89 6 -4 5 15 7939.57 1371.43 2 4 -5 14 1907.60 728.735 3 4 5 -14 1435.30 826.684 6 -4 5 14 1202.32 533.165 1 -4 5 14 2473.36 841.138 2 4 -5 13-448.592 597.759 3 4 5 -13-144.405 523.076 6 -4 5 13 273.355 365.253 1 -4 5 13 11.0944 422.117 2 4 -5 12 5721.47 1169.50 3 4 5 -12 6432.52 1354.49 6 -4 5 12 5680.70 1137.08 1 -4 5 12 5129.41 1051.41 2 4 -5 11 222.789 422.441 3 4 5 -11-175.349 521.836 6 -4 5 11 525.543 516.476 1 -4 5 11 202.412 339.899 2 4 -5 11 189.940 310.029 4 4 -5 10 11786.8 1596.84 3 4 5 -10 11727.4 1725.55 6 -4 5 10 8500.34 1284.95 1 -4 5 10 9210.08 1300.42 2 4 -5 10 9192.05 1156.03 4 4 -5 9 7795.86 1033.98 4 4 -5 9 7608.98 1310.84 3 4 5 -9 10140.4 1563.57 6 -4 5 9 8071.44 1258.58 1 -4 5 9 9900.70 1296.30 2 4 -5 8 400.469 282.333 4 4 -5 8 1960.28 837.962 3 4 5 -8 1043.10 656.408 6 -4 5 8 1154.27 590.148 1 4 -5 7 9182.09 1403.10 3 4 5 -7 11789.1 1631.93 6 -4 5 7 9105.26 1295.45 1 4 -5 7 9966.39 1041.56 4 4 -5 6 3900.03 632.909 4 4 -5 6 5715.47 1126.75 3 4 5 -6 4795.47 1089.40 6 -4 5 6 3315.66 821.187 1 -4 5 5 21925.2 1971.51 1 4 -5 5 19251.9 2029.70 3 4 5 -5 21707.1 2129.92 6 -4 5 5 22948.2 1567.31 5 4 5 -4 2967.68 837.852 6 -4 5 4 1874.48 506.116 5 -4 5 4 580.244 416.384 1 4 5 -3 12302.4 1514.93 6 -4 5 3 11600.5 1155.83 5 -4 5 3 12131.1 1462.99 1 4 5 -2 7189.57 1168.74 6 -4 5 2 9427.45 1045.39 5 -4 5 2 8102.48 1167.64 1 4 5 -1 347.325 385.663 6 -4 5 1 860.708 339.208 5 -4 5 0 26322.5 2101.83 1 4 5 0 28655.0 2284.26 6 -4 5 0 25501.4 1858.50 5 4 5 1 1864.96 622.798 6 -4 5 -1 1298.09 564.494 1 4 5 2 9162.39 1333.95 3 4 5 2 6698.30 1111.83 6 -4 5 -2 7177.30 1098.29 1 -4 5 -3 11476.4 1360.27 1 4 5 3 13472.4 1578.34 3 4 5 3 13501.1 1572.96 6 -4 -5 3 10554.2 954.465 4 -4 -5 4 1391.45 393.362 4 4 5 4 1223.10 626.383 3 4 5 4 2315.77 724.417 6 -4 5 -4 1533.18 544.808 1 -4 5 -5 20345.9 1808.29 1 4 5 5 22031.0 2102.87 3 4 -5 -5 20534.7 1780.69 6 4 5 5 23054.1 1997.36 6 -4 -5 5 16678.3 1370.39 4 -4 -5 6 3455.09 672.924 4 4 5 6 4328.93 965.020 3 4 -5 -6 5277.36 937.322 6 -4 5 -6 3994.58 814.550 1 -4 -5 7 9018.88 1092.62 4 4 5 7 10012.1 1448.63 3 4 -5 -7 8641.09 1163.49 6 -4 5 -7 8129.77 1159.39 1 4 5 8 257.816 379.007 3 4 -5 -8 23.9059 340.673 6 -4 5 -8 496.255 439.780 1 -4 -5 8 513.427 370.428 4 4 5 9 10041.5 1423.93 3 4 -5 -9 10943.6 1340.21 6 -4 5 -9 8880.67 1214.28 1 -4 -5 9 9609.47 1238.14 4 -4 5 -10 12527.9 1447.48 1 4 5 10 10266.9 1482.39 3 4 -5 -10 12359.7 1438.10 6 4 5 11 21.1854 439.282 3 -4 5 -11-358.865 390.507 1 4 -5 -11 465.518 411.495 6 4 5 12 5098.55 1135.52 3 4 -5 -12 5292.25 1012.64 6 4 5 13 412.085 415.210 3 4 5 14 2340.98 857.895 3 4 5 15 6683.72 1408.74 3 4 5 16 637.817 632.771 3 4 5 17 1635.30 831.829 3 4 -6 18 644.761 536.548 3 4 -6 17 1115.96 679.767 3 4 6 -17 1711.86 843.870 6 -4 6 17 789.997 544.416 2 4 -6 16 1247.06 686.970 3 -4 6 16 1227.86 751.170 2 4 -6 15 929.009 642.128 3 4 6 -15 1079.76 766.228 6 -4 6 15 1521.78 734.638 2 4 -6 14 3772.74 1018.65 3 4 6 -14 1259.67 646.203 6 -4 6 14 3509.66 921.524 1 -4 6 14 3575.07 967.333 2 4 -6 13 2919.80 882.277 3 4 6 -13 2702.81 984.006 6 -4 6 13 3252.26 871.359 1 -4 6 13 3566.78 957.297 2 4 -6 12 3674.50 880.151 3 4 6 -12 7331.50 1596.92 6 -4 6 12 4607.97 1009.55 1 -4 6 12 5075.47 1087.55 2 4 -6 12 3854.21 845.623 4 4 -6 11 47.1638 446.210 3 4 6 -11 966.884 771.288 6 -4 6 11 1327.92 670.211 1 -4 6 11 497.591 476.321 2 4 -6 11 473.104 419.372 4 4 -6 10 5944.29 985.323 4 4 -6 10 7459.83 1278.21 3 4 6 -10 9591.67 1626.20 6 -4 6 10 7907.20 1284.04 1 -4 6 10 7574.37 1227.20 2 4 -6 9 4233.89 774.035 4 4 -6 9 4688.17 1064.07 3 4 6 -9 6162.11 1330.00 6 -4 6 9 5019.68 986.998 1 4 -6 8 2024.34 545.753 4 4 -6 8 1229.43 635.826 3 4 6 -8 2948.51 893.647 6 -4 6 8 2321.42 764.942 1 4 -6 7 1478.51 432.995 4 4 -6 7 1867.93 753.824 3 4 6 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10348.0 1327.07 1 -4 -6 6 7070.50 977.085 4 4 6 6 8696.45 1318.48 3 -4 6 -6 8531.77 1204.84 1 -4 -6 7 317.866 272.075 4 4 6 7 775.322 470.674 3 4 -6 -7 1604.93 518.485 6 -4 6 -7 614.057 417.002 1 -4 -6 8 1265.33 470.017 4 4 6 8 2492.78 799.494 3 4 -6 -8 2677.29 697.543 6 -4 6 -8 2051.62 659.419 1 -4 -6 9 6371.39 1041.96 4 4 6 9 7211.54 1230.83 3 4 -6 -9 6051.97 991.821 6 -4 6 -9 6003.32 1015.09 1 4 6 10 6383.13 1171.06 3 4 -6 -10 7387.27 1095.91 6 -4 6 -10 5524.50 973.091 1 -4 -6 10 5411.46 1038.36 4 4 6 11 1522.21 750.554 3 -4 6 -11 1609.95 596.803 1 4 -6 -11 1329.63 568.991 6 -4 -6 11 550.979 485.735 4 4 6 12 5068.40 1150.45 3 4 6 12 4319.17 795.858 1 4 6 13 3418.08 960.488 3 4 6 14 1538.82 755.683 3 4 6 15 1823.18 846.994 3 4 6 16 1620.77 814.479 3 4 6 17 863.062 758.076 3 4 -7 18 1154.91 734.581 3 4 -7 17-50.7777 396.058 3 4 -7 16 1431.78 716.032 3 4 7 -16 1510.14 990.825 6 -4 7 16 490.039 530.040 2 4 -7 15 199.953 392.003 3 4 7 -15 1909.73 913.604 6 -4 7 15 1195.18 597.162 2 4 -7 14-344.131 507.154 3 4 7 -14-685.239 722.516 6 -4 7 14 206.241 530.536 1 -4 7 14-63.3678 492.617 2 4 -7 13 2537.60 810.152 3 4 7 -13 1687.82 982.335 6 -4 7 13 2840.99 910.308 2 -4 7 13 2791.09 830.683 1 4 -7 12 489.701 442.097 4 4 -7 12 610.277 468.841 3 4 7 -12 1503.52 842.311 6 -4 7 12 853.315 609.844 2 -4 7 12 525.336 385.900 1 4 -7 11 6843.80 1137.28 4 4 -7 11 7833.68 1265.74 3 4 7 -11 6564.68 1472.76 6 -4 7 11 8251.99 1324.24 2 -4 7 11 6930.08 1229.02 1 4 -7 10 608.250 461.375 4 4 -7 10 1176.15 582.318 3 4 7 -10 1323.59 742.745 6 -4 7 10 937.935 548.336 1 -4 7 9 525.822 524.262 1 4 -7 9 1293.18 506.854 4 4 -7 9 1169.23 577.592 3 4 7 -9 1137.13 836.790 6 -4 7 8 11421.4 1489.13 1 4 -7 8 12367.6 1609.81 3 4 7 -8 11068.6 1751.21 6 4 -7 8 10917.8 1298.51 4 -4 7 7 2701.31 806.008 1 4 -7 7 2081.51 708.607 3 4 7 -7 3127.64 949.106 6 -4 7 6 7129.39 1188.46 1 4 -7 6 8770.77 1357.53 3 4 7 -6 5744.65 1160.21 6 -4 7 5 4630.95 1008.51 1 4 -7 5 3896.22 951.215 3 4 7 -5 3516.52 944.134 6 -4 7 4 6053.13 1129.81 1 4 7 -4 6448.25 1217.25 6 -4 7 4 6603.70 968.092 5 -4 7 3 10239.6 1399.98 1 4 7 -3 12677.3 1664.38 6 -4 7 3 12734.7 1343.15 5 -4 7 2 5278.10 1035.78 1 4 7 -2 3305.84 864.772 6 -4 7 2 6599.19 983.602 5 -4 7 1 9900.94 1354.50 1 4 7 -1 10476.9 1466.25 6 -4 7 1 10591.2 1264.38 5 -4 7 0-60.7814 425.667 1 4 7 0-515.039 561.022 6 -4 7 0 246.209 381.050 5 -4 7 -1 9819.80 1359.23 1 4 7 1 10304.5 1416.76 3 4 7 1 6747.46 1147.26 6 -4 7 -1 8478.48 1242.00 5 -4 7 -2 5188.95 967.698 1 4 7 2 5088.60 1024.27 3 4 7 2 5916.42 1083.84 6 -4 7 -2 6896.13 1120.80 5 -4 7 -3 13288.1 1567.19 1 4 7 3 12789.6 1574.42 3 4 7 3 12617.6 1544.89 6 -4 7 -3 12809.8 1479.53 5 -4 7 -4 7789.55 1186.64 1 4 7 4 7488.71 1202.08 3 4 7 4 6068.47 1090.63 6 -4 7 -4 7728.46 1232.93 5 -4 7 -5 5426.89 1038.72 1 -4 -7 5 5620.87 838.262 4 4 7 5 7739.04 1256.21 3 4 7 5 6027.53 1058.95 6 -4 7 -6 8517.60 1236.48 1 -4 -7 6 6940.19 992.863 4 4 7 6 7115.24 1199.31 3 -4 -7 7 1311.14 498.464 4 4 7 7 1467.30 628.091 3 -4 7 -7 2570.71 704.091 1 -4 -7 8 8145.66 1139.11 4 4 7 8 8179.16 1292.97 3 -4 7 -8 10454.2 1337.63 1 -4 -7 9 1417.21 573.009 4 4 7 9 1940.49 693.050 3 -4 7 -9 1720.38 627.998 1 -4 -7 10 1444.15 621.317 4 4 7 10 958.263 506.175 3 -4 7 -10 1150.64 536.016 1 4 7 11 7499.60 1261.68 3 4 7 11 6985.04 1050.59 1 -4 7 -11 6660.32 1103.55 1 -4 -7 11 4715.55 1029.81 4 4 7 12 1309.89 714.195 3 4 7 12 561.660 391.115 1 -4 -7 12-475.166 509.540 4 4 7 13 2810.24 883.203 3 -4 -7 13 1358.63 668.217 4 4 7 14-691.872 685.594 3 4 7 15 730.387 598.599 3 4 7 16 1522.92 803.078 3 4 -8 15 103.450 412.579 3 4 8 -15-1031.95 987.991 6 -4 8 15-278.109 577.939 2 4 -8 14 2218.19 749.602 3 4 8 -14 1432.41 787.391 6 -4 8 14 3038.88 985.057 2 -4 8 14 1918.69 801.765 1 4 -8 13 2034.95 715.025 3 4 8 -13 1230.57 799.744 6 -4 8 13 3202.08 973.252 2 -4 8 13 3076.00 802.741 1 4 -8 12 358.725 414.416 4 4 -8 12 22.0534 421.158 3 4 8 -12 101.214 651.128 6 -4 8 12 808.257 630.730 2 -4 8 12 801.136 533.850 1 -4 8 11 7619.46 1320.96 1 4 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603.765 6 5 6 11-398.907 689.033 3 5 6 12 854.707 827.051 3 5 6 13 1371.65 730.227 3 5 6 14 1213.05 795.025 3 5 6 15 449.952 636.240 3 5 -7 16 638.766 663.133 3 5 -7 15 761.824 665.210 3 5 -7 14 511.620 542.293 3 -5 7 14 2135.77 835.697 1 -5 7 14 1055.89 706.684 2 5 -7 13-179.623 508.919 3 5 7 -13 610.855 588.576 6 -5 7 13 1525.78 785.601 1 -5 7 13 211.777 547.896 2 5 -7 12 3388.02 968.230 3 5 7 -12 1804.58 944.095 6 -5 7 12 4785.40 1204.18 1 -5 7 12 4220.17 1043.48 2 5 -7 11 1265.28 665.105 3 5 7 -11 373.392 773.472 6 -5 7 11 400.128 590.962 1 -5 7 11-651.932 632.697 2 5 -7 10 4060.98 1111.17 3 5 7 -10 2451.78 1023.22 6 -5 7 10 5127.22 1165.38 1 -5 7 10 4172.37 978.938 2 5 -7 9 1190.70 715.976 3 5 7 -9 891.950 840.924 6 -5 7 9-84.0865 440.826 1 5 -7 8 1482.93 708.207 3 5 7 -8 3365.61 1138.41 6 -5 7 8 3067.29 1014.03 1 5 -7 7 1750.62 772.173 3 5 7 -7 2549.65 1055.91 6 -5 7 7 1961.97 748.390 1 5 -7 6-69.8894 581.626 3 5 7 -6 1265.08 764.905 6 -5 7 6 249.532 451.829 1 5 -7 5 418.327 440.683 3 5 7 -5-375.750 619.776 6 -5 7 5 343.325 531.999 1 5 7 -4 2017.69 899.174 6 -5 7 4 2549.43 679.541 5 -5 7 4 2067.41 764.658 1 5 7 -3 1590.50 735.375 6 -5 7 3 1776.49 599.192 5 -5 7 3 924.073 595.722 1 5 7 -2 5301.35 1228.43 6 -5 7 2 5000.27 992.582 5 -5 7 2 4865.96 1149.73 1 5 7 -1 99.1584 415.437 6 -5 7 1 876.997 412.910 1 5 7 0 14164.0 1856.92 6 -5 7 0 13168.1 1555.54 5 -5 7 0 11488.6 1617.11 1 5 7 1 1472.34 768.801 3 5 7 1 472.462 586.519 6 -5 7 -1 1246.74 547.945 5 -5 7 -1 1091.33 571.000 1 5 7 2 5159.44 1173.84 3 5 7 2 6333.23 1256.19 6 -5 7 -2 4703.02 1001.33 5 -5 7 -2 5531.63 1146.75 1 5 7 3 2041.53 790.599 3 5 7 3 2278.10 772.633 6 -5 7 -3 2468.56 770.581 5 -5 7 -3 525.251 533.843 1 5 7 4 2914.69 988.774 3 5 7 4 1800.81 681.500 6 -5 7 -4 3336.22 937.266 5 -5 7 -4 2924.57 904.842 1 5 7 5 979.200 635.053 3 5 7 5 712.086 636.511 6 -5 7 -5-169.769 508.407 1 5 7 6-251.923 591.638 3 -5 7 -6 444.264 450.297 1 5 7 7 3409.66 1031.48 3 -5 7 -7 2615.74 754.142 1 5 7 8 3045.02 936.964 3 -5 7 -8 2590.45 795.362 1 5 7 9-468.815 580.597 3 -5 7 -9 77.6211 407.507 1 5 7 10 4834.78 1179.72 3 -5 7 -10 5091.25 1090.22 1 5 7 11-498.530 714.147 3 5 7 12 3422.78 1067.14 3 5 7 13 910.278 720.876 3 5 7 14 456.676 704.804 3 5 -8 14-486.830 531.899 3 -5 8 14 264.169 401.809 1 5 -8 13 340.040 442.849 3 -5 8 13 1379.05 769.704 1 -5 8 13 590.206 575.759 2 5 -8 12 114.143 509.725 3 5 8 -12 847.581 747.614 6 -5 8 12 445.063 594.978 1 -5 8 12-592.693 570.996 2 5 -8 11-1138.30 753.109 3 5 8 -11 140.727 633.107 6 -5 8 11 214.108 492.183 1 -5 8 11-510.044 683.323 2 5 -8 10 1454.58 784.536 3 5 8 -10 1359.27 856.077 6 -5 8 10 517.074 411.451 1 5 -8 9 2694.20 813.143 3 5 8 -9 2520.00 1006.35 6 -5 8 9 1914.28 661.736 1 5 -8 8-577.100 592.614 3 5 8 -8 314.179 522.913 6 -5 8 8-800.999 609.201 1 5 -8 7 4769.31 1128.27 3 5 8 -7 4398.40 1317.05 6 -5 8 7 4254.46 1089.38 1 5 -8 6 530.677 689.805 3 5 8 -6 1939.85 897.327 6 -5 8 6 2355.97 869.921 1 5 -8 5 8835.52 1549.95 3 5 8 -5 9628.35 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-7-991.388 865.599 6 -7 0 -8 1151.57 729.413 1 -7 0 8-378.971 531.872 1 7 0 -8 1291.07 895.711 6 -7 0 -9 4868.67 1221.49 1 -7 0 9 3837.90 1254.82 1 7 0 -9 3578.94 1320.26 6 -7 0 10 19.8609 635.714 1 -7 1 10 70.7179 471.443 1 -7 1 9-1350.92 920.992 1 -7 1 8 1608.66 918.999 1 7 1 -8 749.747 559.057 6 -7 -1 -7 2462.72 897.234 1 7 -1 7 2404.17 1127.10 3 -7 1 7 400.944 596.852 1 7 1 -7 1167.05 872.926 6 -7 -1 -6 5441.11 1305.08 1 7 -1 6 6213.77 1557.50 3 -7 1 6 4298.36 1240.80 1 7 1 -6 2835.62 1095.21 6 -7 -1 -5 2132.33 887.599 1 7 -1 5 166.832 774.818 3 -7 1 5 1311.84 666.416 1 7 1 -5 2957.04 1159.85 6 -7 -1 -4 5943.53 1384.82 1 7 -1 4 2827.25 1304.90 3 -7 1 4 2615.73 953.152 1 7 1 -4 1957.98 871.676 6 -7 -1 -3 893.519 805.401 1 -7 1 3 70.0317 568.626 1 7 1 -3 656.598 836.711 6 -7 -1 -2 576.822 669.315 1 -7 1 2-406.390 684.624 1 7 1 -2-158.931 624.752 6 -7 -1 -1 1879.21 867.831 1 -7 1 1 335.098 621.548 1 7 1 -1 2179.15 1069.49 6 -7 -1 0 2067.73 880.217 1 -7 1 0 788.741 507.184 1 -7 -1 1 90.7538 596.283 1 -7 1 -1 508.828 588.636 1 -7 -1 2 612.861 683.411 1 -7 1 -2 978.520 749.716 1 -7 -1 3 1987.12 954.469 1 -7 1 -3 1231.63 690.913 1 7 1 3-722.493 892.631 3 7 -1 -3 1121.95 748.355 6 -7 -1 4 1117.22 728.998 1 7 1 4 4087.91 1393.30 3 -7 1 -4 2596.61 1009.23 1 7 -1 -4 1372.35 727.466 6 -7 -1 5 2631.67 1002.71 1 7 1 5 1670.38 1225.16 3 -7 1 -5 2794.41 1121.29 1 7 -1 -5 1645.90 997.645 6 -7 -1 6 3287.88 1065.44 1 7 1 6 5605.76 1603.60 3 -7 1 -6 3672.82 1135.40 1 7 -1 -6 4690.96 1322.80 6 -7 -1 7 3035.27 1201.18 1 7 1 7 867.101 778.509 3 -7 1 -7 2561.43 978.721 1 7 -1 -7 1483.96 936.544 6 -7 -1 8 1279.42 632.077 1 -7 1 -8 2110.58 916.126 1 7 -1 -8-207.020 645.412 6 -7 1 -9 659.044 665.769 1 -7 -1 9 463.036 625.744 1 7 -1 -9 1771.79 1028.65 6 -7 -1 10 242.071 664.118 1 -7 2 9 25.4270 646.755 1 -7 2 8 1725.99 837.562 1 -7 2 7-1168.02 1000.31 1 7 2 -7 169.213 718.849 6 7 -2 6 733.550 837.962 3 -7 2 6-221.789 529.384 1 7 2 -6-809.056 754.751 6 7 -2 5 659.155 786.841 3 -7 2 5 1039.89 832.694 1 7 2 -5 1930.80 970.094 6 7 -2 4 1018.79 762.976 3 -7 2 4-312.354 710.957 1 7 2 -4 700.763 802.738 6 -7 -2 -3-21.3782 550.565 1 -7 2 3-563.520 698.832 1 -7 -2 -2 7792.45 1533.96 1 -7 2 2 5097.62 1345.97 1 7 2 -2 5892.20 1479.32 6 -7 -2 -1 2232.37 864.852 1 -7 2 1 23.4625 656.812 1 7 2 -1 1953.95 916.307 6 -7 -2 0 284.125 565.866 1 -7 2 0-78.4987 596.594 1 -7 -2 1 1170.23 709.220 1 -7 2 -1 296.174 477.282 1 -7 -2 2 6266.27 1419.73 1 -7 2 -2 6655.41 1473.50 1 -7 -2 3 814.035 548.052 1 7 2 3 792.109 856.844 3 -7 2 -3-500.061 667.364 1 -7 -2 4 1601.98 847.067 1 7 2 4 1668.03 1062.06 3 -7 2 -4-175.382 512.707 1 7 -2 -4-412.347 670.373 6 -7 -2 5 2241.80 854.051 1 7 2 5-316.158 915.110 3 -7 2 -5 1386.93 689.144 1 7 -2 -5 706.879 724.138 6 -7 -2 6 1493.76 960.173 1 7 2 6 701.498 834.619 3 -7 2 -6 737.260 823.681 1 7 -2 -6 1123.91 830.058 6 -7 -2 7-122.110 451.817 1 7 2 7 1773.93 932.162 3 -7 2 -7-402.951 672.050 1 7 -2 -7 594.545 630.782 6 -7 -2 8 43.4259 633.885 1 -7 2 -8 1180.72 823.881 1 7 -2 -8 1436.43 892.302 6 -7 -2 9 1282.61 906.901 1 -7 2 -9 547.054 644.736 1 7 -2 -9 862.438 698.360 6 7 -2 -10 1538.45 941.678 6 -7 3 8-401.705 562.720 1 7 -3 7 2028.77 1004.28 3 -7 3 7 3046.67 1080.23 1 7 3 -7 4645.12 1297.16 6 7 -3 6 226.742 939.402 3 -7 3 6-351.891 712.596 1 7 -3 5 4666.65 1518.42 3 -7 3 5 1873.37 949.447 1 7 3 -5 3734.58 1241.60 6 7 -3 4 1022.58 821.137 3 -7 3 4-690.054 568.237 1 -7 3 3 1490.86 738.228 1 7 3 -3 2287.20 1061.20 6 -7 3 2 32.4021 503.534 1 7 3 -2-1144.25 874.716 6 -7 3 1-95.1861 533.674 1 7 3 -1 212.005 880.202 6 -7 3 0 3936.72 1218.40 1 7 3 0 5908.98 1478.66 6 -7 3 -1-480.655 762.911 1 7 3 1 770.450 781.754 6 7 3 2-1750.10 1272.68 3 -7 3 -2 114.762 710.525 1 7 3 3 219.916 720.389 3 -7 3 -3 1087.76 561.253 1 7 3 4 237.616 763.686 3 -7 3 -4 514.894 600.649 1 7 3 5 7981.35 1868.62 3 -7 3 -5 6358.95 1435.26 1 7 3 6 111.192 834.497 3 -7 3 -6-125.043 594.312 1 7 -3 -6 1005.26 808.746 6 7 3 7 4613.92 1532.21 3 -7 3 -7 3396.48 1104.30 1 7 -3 -7 4119.68 1165.88 6 -7 3 -8-145.892 592.385 1 7 -3 -8 1316.63 894.985 6 -7 3 -9 819.305 673.831 1 7 -3 -9 486.241 579.381 6 7 -3 -10 1683.96 884.818 6 7 -4 7-1109.24 991.654 3 -7 4 7 919.521 659.377 1 7 -4 6 720.980 906.969 3 -7 4 6-676.671 743.398 1 7 4 -6-226.375 633.188 6 7 -4 5-1242.88 1209.52 3 -7 4 5-326.293 634.133 1 7 4 -5 1034.18 914.630 6 7 -4 4-62.2867 1144.00 3 -7 4 4 1060.33 631.215 1 7 4 -4 1716.10 835.723 6 -7 4 3 1755.14 878.447 1 7 4 -3 1659.07 920.586 6 -7 4 2 543.889 620.413 1 7 4 -2 798.928 648.477 6 -7 4 1 4710.74 1330.22 1 7 4 -1 3441.58 1166.11 6 -7 4 1 2287.39 746.453 5 -7 4 0 4579.53 1267.39 1 7 4 0 6064.14 1428.12 6 -7 4 0 4580.06 1028.88 5 -7 4 -1 3120.39 1072.76 1 7 4 1 2811.24 1072.89 6 7 4 2 1042.40 822.774 3 -7 4 -2-1051.83 767.391 1 7 4 3 2068.93 972.600 3 -7 4 -3 266.308 606.434 1 7 4 4 683.719 762.698 3 -7 4 -4 1489.66 886.551 1 7 4 5-64.2041 775.962 3 -7 4 -5-236.803 660.922 1 7 4 6 574.735 738.245 3 -7 4 -6-581.982 539.407 1 7 4 7 961.380 761.980 3 -7 4 -7 423.136 654.660 1 -7 4 -8 1761.92 853.618 1 7 -4 -8 2803.74 1162.93 6 -7 4 -9-160.800 634.031 1 7 -4 -9-162.886 666.690 6 7 -4 -10 1277.68 748.756 6 7 -5 6 1686.80 891.170 3 7 -5 5-1964.99 1181.40 3 -7 5 5-1148.81 848.714 1 7 5 -5 281.426 747.453 6 7 -5 4 1785.43 936.826 3 -7 5 4 1678.19 841.511 1 7 5 -4 4512.57 1380.07 6 -7 5 3 456.385 699.530 1 7 5 -3 197.943 629.043 6 -7 5 2 1484.06 924.722 1 7 5 -2 2090.69 1093.52 6 -7 5 1 87.9035 606.422 1 7 5 -1 59.1293 618.940 6 -7 5 1 1402.10 718.453 5 -7 5 0 3085.51 1087.20 1 7 5 0 1882.96 966.192 6 -7 5 0 1893.35 717.263 5 7 5 1-256.672 683.039 3 -7 5 -1 1386.58 782.905 1 7 5 1-4.06705 746.731 6 -7 5 -1 491.290 545.855 5 7 5 2 338.053 731.167 3 -7 5 -2 202.818 596.463 1 7 5 2 1482.74 952.046 6 -7 5 -2 1090.64 647.966 5 7 5 3-1.58456 750.358 3 -7 5 -3-485.720 593.377 1 7 5 4 3819.14 1286.82 3 -7 5 -4 4200.83 1203.43 1 7 5 5-26.3270 603.108 3 -7 5 -5 504.858 437.492 1 7 5 6 2920.37 1143.71 3 -7 5 -6 2277.75 883.776 1 -7 5 -7-581.008 675.121 1 -7 5 -8 144.701 632.256 1 -7 5 -9 857.305 797.255 1 7 -6 5 464.692 909.733 3 7 -6 4 1.76398 1031.62 3 7 6 -3 640.311 867.885 6 -7 6 2 2023.92 913.221 1 7 6 -2 1842.50 964.830 6 -7 6 1 3309.83 1015.87 1 7 6 -1 2306.08 1030.53 6 -7 6 1 834.818 533.801 5 -7 6 0-36.7496 545.860 1 7 6 0-163.930 616.551 6 -7 6 0 806.469 524.316 5 7 6 1 387.683 975.014 3 -7 6 -1 3772.06 1184.43 1 7 6 1 1141.54 741.220 6 -7 6 -1 2223.63 878.388 5 7 6 2 1656.77 984.471 3 -7 6 -2 1626.92 849.597 1 7 6 2 2459.70 1142.02 6 -7 6 -2 2850.24 930.756 5 7 6 3 1110.78 876.297 3 -7 6 -3 299.988 575.569 1 -7 6 -3 83.7195 585.046 5 7 6 4 408.581 759.096 3 -7 6 -4-214.798 698.807 1 -7 6 -4 1644.49 847.550 5 7 6 5 1657.76 966.202 3 -7 6 -5 3385.67 1148.17 1 7 6 6 5506.66 1555.18 3 -7 6 -6 1442.54 884.353 1 -7 6 -7 189.466 543.514 1 -7 6 -8-23.5463 551.413 1 -7 6 -9 1254.42 781.019 1 7 -7 4 663.600 855.698 3 7 7 -2-845.832 828.269 6 7 7 -1 114.838 633.183 6 -7 7 1 777.626 664.896 5 7 7 0 674.261 622.881 3 7 7 0 2069.00 1193.90 6 -7 7 0 2616.96 946.498 5 7 7 1-594.137 611.548 6 -7 7 -1 404.622 507.900 5 7 7 2 222.571 848.177 6 -7 7 -2-420.559 561.101 5 7 7 3 1688.81 985.502 3 7 7 3 2041.91 1047.23 6 -7 7 -3-754.544 753.974 5 7 7 4 2215.16 1156.36 3 -7 7 -4 3948.62 1275.41 5 7 7 5 4154.92 1387.67 3 7 8 -1 402.338 952.861 3 -7 8 1-219.731 588.760 5 7 8 0 1110.50 976.888 3 -7 8 0 703.716 498.624 5 7 8 1-353.350 801.553 3 7 8 1 401.746 777.790 6 -7 8 -1-526.278 668.771 5 7 8 2-563.504 812.903 3 7 8 2 896.996 677.080 6 7 8 3 32.5139 783.567 3 7 8 3 748.108 798.382 6 7 8 4-141.288 498.727 3 7 8 5 465.635 627.523 3 -7 9 2 1024.33 727.778 5 -7 9 1 557.331 665.079 5 -7 9 0-717.252 628.907 5 0 0 0 0.00 0.00 0 TITL gon33 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 0.71073 5.787077 13.549260 16.835748 90.0000 90.0000 90.0000 ZERR 6.00 0.000199 0.000578 0.000553 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 66.00 60.00 6.00 6.00 TREF HKLF 4 END ; _shelx_hkl_checksum 61443 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag Br Br 1.15248(11) 0.84718(5) 0.20687(4) 0.0529(2) Uani 1 1 d O1 O 1.0169(7) 1.0833(3) -0.0352(3) 0.0410(10) Uani 1 1 d O2 O 0.6784(8) 1.2173(3) 0.0639(2) 0.0447(10) Uani 1 1 d O3 O 0.4657(8) 1.0836(3) 0.0888(2) 0.0388(10) Uani 1 1 d N N 0.6439(11) 1.1876(5) -0.0951(4) 0.0453(13) Uani 1 1 d F1 F 0.8933(8) 1.0576(3) -0.1872(2) 0.0610(12) Uani 1 1 d F2 F 0.6295(9) 0.9525(3) -0.1605(2) 0.0645(11) Uani 1 1 d F3 F 0.9862(9) 0.9180(3) -0.1381(2) 0.0713(15) Uani 1 1 d C1 C 0.8107(10) 1.0317(4) -0.0492(3) 0.0316(12) Uani 1 1 d C2 C 0.8290(13) 0.9897(4) -0.1339(4) 0.0455(15) Uani 1 1 d C3 C 0.6011(9) 1.1029(4) -0.0430(3) 0.0286(12) Uani 1 1 d C4 C 0.5889(8) 1.1423(4) 0.0417(3) 0.0300(11) Uani 1 1 d C5 C 0.4612(19) 1.1121(7) 0.1723(4) 0.057(2) Uani 1 1 d C6 C 0.7916(9) 0.9460(4) 0.0098(3) 0.0290(12) Uani 1 1 d C7 C 0.6096(11) 0.8797(4) 0.0056(4) 0.0367(13) Uani 1 1 d C8 C 0.5933(11) 0.8038(5) 0.0598(4) 0.0404(14) Uani 1 1 d C9 C 0.7531(12) 0.7931(5) 0.1192(4) 0.0414(14) Uani 1 1 d C10 C 0.9313(10) 0.8596(4) 0.1234(3) 0.0364(13) Uani 1 1 d C11 C 0.9562(10) 0.9359(4) 0.0691(3) 0.0331(12) Uani 1 1 d H7 H 0.497(12) 0.882(4) -0.034(3) 0.034(16) Uiso 1 1 d H5A H 0.366(16) 1.065(6) 0.197(5) 0.08(3) Uiso 1 1 d H8 H 0.465(12) 0.760(4) 0.057(3) 0.035(16) Uiso 1 1 d H3 H 0.463(11) 1.062(4) -0.055(3) 0.024(14) Uiso 1 1 d H11 H 1.066(10) 0.986(4) 0.072(3) 0.022(14) Uiso 1 1 d H1O H 0.997(14) 1.140(6) -0.057(4) 0.06(2) Uiso 1 1 d H10 H 0.743(9) 0.745(4) 0.157(3) 0.023(13) Uiso 1 1 d H1N H 0.607(16) 1.171(6) -0.138(5) 0.08(3) Uiso 1 1 d H5B H 0.613(19) 1.106(7) 0.193(5) 0.09(3) Uiso 1 1 d H5C H 0.386(19) 1.178(7) 0.178(5) 0.10(3) Uiso 1 1 d H2N H 0.559(16) 1.235(6) -0.086(4) 0.06(3) Uiso 1 1 d loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br 0.0427(3) 0.0749(5) 0.0413(3) 0.0123(3) -0.0019(3) 0.0073(4) O1 0.021(2) 0.035(2) 0.067(3) 0.018(2) 0.0021(19) 0.0038(18) O2 0.041(3) 0.038(2) 0.055(2) -0.0082(19) -0.001(2) -0.007(2) O3 0.044(2) 0.037(2) 0.036(2) -0.0026(17) 0.0024(18) -0.002(2) N 0.043(3) 0.045(3) 0.048(3) 0.010(2) 0.003(3) 0.019(3) F1 0.079(3) 0.057(2) 0.047(2) 0.0142(17) 0.027(2) 0.019(2) F2 0.087(3) 0.065(3) 0.041(2) -0.0088(18) -0.005(2) -0.009(3) F3 0.104(4) 0.056(3) 0.054(2) 0.0073(19) 0.029(2) 0.042(3) C1 0.024(3) 0.030(3) 0.041(3) 0.004(2) 0.003(2) 0.001(2) C2 0.056(4) 0.035(3) 0.045(3) 0.004(3) 0.012(3) 0.011(3) C3 0.020(3) 0.031(3) 0.035(3) 0.001(2) 0.000(2) 0.001(2) C4 0.019(2) 0.032(3) 0.039(3) 0.002(2) -0.003(2) -0.001(2) C5 0.079(6) 0.060(5) 0.033(3) 0.001(3) 0.000(4) 0.004(5) C6 0.027(3) 0.028(3) 0.032(3) 0.001(2) 0.003(2) 0.002(2) C7 0.035(3) 0.035(3) 0.039(3) -0.004(2) 0.001(3) -0.005(3) C8 0.040(4) 0.037(3) 0.045(3) 0.001(3) 0.002(3) -0.010(3) C9 0.048(4) 0.037(3) 0.039(3) 0.006(3) 0.013(3) -0.001(3) C10 0.032(3) 0.041(3) 0.036(3) 0.001(3) 0.006(2) 0.006(3) C11 0.028(3) 0.030(3) 0.041(3) -0.002(2) 0.006(2) 0.001(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C4 O3 C5 115.2(5) O1 C1 C6 109.2(4) O1 C1 C2 106.3(5) C6 C1 C2 109.0(4) O1 C1 C3 110.1(4) C6 C1 C3 111.8(4) C2 C1 C3 110.2(5) F3 C2 F1 106.0(5) F3 C2 F2 107.3(5) F1 C2 F2 106.0(5) F3 C2 C1 111.5(5) F1 C2 C1 112.8(5) F2 C2 C1 112.9(5) N C3 C4 107.0(5) N C3 C1 108.3(4) C4 C3 C1 108.4(4) O2 C4 O3 123.6(5) O2 C4 C3 124.6(5) O3 C4 C3 111.9(4) C11 C6 C7 119.7(5) C11 C6 C1 119.5(5) C7 C6 C1 120.8(5) C8 C7 C6 120.1(6) C9 C8 C7 121.1(6) C8 C9 C10 118.4(6) C9 C10 C11 122.3(6) C9 C10 Br 118.9(4) C11 C10 Br 118.8(5) C6 C11 C10 118.4(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Br C10 1.909(6) O1 C1 1.403(7) O2 C4 1.201(6) O3 C4 1.330(7) O3 C5 1.459(8) N C3 1.466(7) F1 C2 1.337(7) F2 C2 1.337(9) F3 C2 1.333(7) C1 C6 1.532(7) C1 C2 1.539(8) C1 C3 1.553(8) C3 C4 1.526(8) C6 C11 1.387(8) C6 C7 1.386(8) C7 C8 1.379(8) C8 C9 1.370(9) C9 C10 1.372(9) C10 C11 1.387(8)