#------------------------------------------------------------------------------ #$Date: 2019-11-11 20:41:26 +0200 (Mon, 11 Nov 2019) $ #$Revision: 227295 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/03/58/4035894.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4035894 loop_ _publ_author_name 'Ma, Yan-Na' 'Bian, Yajing' 'Liu, Xin' 'Zhang, Jie' 'Chen, Xuenian' _publ_section_title ; One-Pot Synthesis of Iodo-Dibenzothiazines from 2-Biaryl Sulfides. ; _journal_issue 1 _journal_name_full 'The Journal of organic chemistry' _journal_page_first 450 _journal_page_last 457 _journal_paper_doi 10.1021/acs.joc.8b02729 _journal_volume 84 _journal_year 2019 _chemical_formula_moiety 'C13 H10 I N O S' _chemical_formula_sum 'C13 H10 I N O S' _chemical_formula_weight 355.18 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2018-08-01 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.18 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 96.518(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 5.07560(10) _cell_length_b 16.2147(3) _cell_length_c 15.4288(2) _cell_measurement_reflns_used 4816 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 72.0740 _cell_measurement_theta_min 5.4410 _cell_volume 1261.57(4) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 8.0528 _diffrn_detector_type EosS2 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.985 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 17.00 105.00 1.00 1.00 -- 35.45 38.00 90.00 88 2 \w 23.00 89.00 1.00 1.00 -- 35.45-125.00 60.00 66 3 \w 23.00 89.00 1.00 1.00 -- 35.45-125.00 -60.00 66 4 \w 19.00 103.00 1.00 1.00 -- 35.45 57.00 -60.00 84 5 \w 23.00 89.00 1.00 1.00 -- 35.45-125.00 0.00 66 6 \w -32.00 52.00 1.00 1.00 -- 35.45 -57.00 -30.00 84 7 \w 19.00 103.00 1.00 1.00 -- 35.45 57.00 150.00 84 8 \w 39.00 109.00 1.00 1.90 -- 108.69 -95.00 150.00 70 9 \w 57.00 151.00 1.00 1.90 -- 108.69 178.00 60.00 94 10 \w 91.00 177.00 1.00 1.90 -- 108.69 45.00 150.00 86 11 \w 100.00 178.00 1.00 1.90 -- 108.69 111.00 0.00 78 12 \w 101.00 178.00 1.00 1.90 -- 108.69 104.00-137.00 77 13 \w 100.00 178.00 1.00 1.90 -- 108.69 111.00-120.00 78 14 \w 39.00 109.00 1.00 1.90 -- 108.69 -95.00 0.00 70 15 \w 37.00 147.00 1.00 1.90 -- 108.69 -15.00 150.00 110 16 \w 19.00 103.00 1.00 1.00 -- 35.45 57.00-120.00 84 17 \w 19.00 103.00 1.00 1.00 -- 35.45 57.00 0.00 84 18 \w -32.00 52.00 1.00 1.00 -- 35.45 -57.00 60.00 84 19 \w -34.00 54.00 1.00 1.00 -- 35.45 -38.00-150.00 88 20 \w 9.00 82.00 1.00 1.00 -- 35.45 77.00-180.00 73 21 \w -32.00 52.00 1.00 1.00 -- 35.45 -57.00 150.00 84 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, EosS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0892710000 _diffrn_orient_matrix_UB_12 -0.0905749000 _diffrn_orient_matrix_UB_13 -0.0102017000 _diffrn_orient_matrix_UB_21 -0.0491670000 _diffrn_orient_matrix_UB_22 0.0115547000 _diffrn_orient_matrix_UB_23 -0.0997296000 _diffrn_orient_matrix_UB_31 0.2878702000 _diffrn_orient_matrix_UB_32 -0.0261385000 _diffrn_orient_matrix_UB_33 -0.0080800000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0469 _diffrn_reflns_av_unetI/netI 0.0390 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.985 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -4 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 8562 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.985 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.274 _diffrn_reflns_theta_min 3.968 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 21.346 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.06229 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.870 _exptl_crystal_description block _exptl_crystal_F_000 688 _exptl_crystal_size_max 0.33 _exptl_crystal_size_mid 0.24 _exptl_crystal_size_min 0.14 _refine_diff_density_max 1.068 _refine_diff_density_min -0.753 _refine_diff_density_rms 0.126 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.077 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 155 _refine_ls_number_reflns 2453 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.077 _refine_ls_R_factor_all 0.0455 _refine_ls_R_factor_gt 0.0422 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0720P)^2^+0.7021P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1214 _refine_ls_wR_factor_ref 0.1252 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2236 _reflns_number_total 2453 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL myn-33-4_a.res in P2(1)/c myn-33-4.res created by SHELXL-2016/6 at 18:25:16 on 01-Aug-2018 REM Old TITL myn-33-4 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.128, Rweak 0.018, Alpha 0.036, Orientation as input REM Formula found by SHELXT: C13 O S I N CELL 1.54184 5.0756 16.2147 15.4288 90 96.518 90 ZERR 4 0.0001 0.0003 0.0002 0 0.002 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H I N O S UNIT 52 40 4 4 4 4 L.S. 10 PLAN 20 BOND $H LIST 6 fmap 2 acta REM REM REM WGHT 0.072000 0.702100 FVAR 0.34495 I1 3 0.141566 0.479572 0.327973 11.00000 0.06367 0.04350 = 0.05578 0.00133 0.00366 0.01556 S1 6 0.928013 0.140439 0.517200 11.00000 0.03352 0.03509 = 0.02711 0.00384 0.00710 0.00074 O1 5 0.755176 0.069310 0.511470 11.00000 0.03798 0.03703 = 0.05430 0.00361 0.01245 -0.00404 N1 4 0.829144 0.220577 0.555380 11.00000 0.05873 0.04108 = 0.02280 0.00066 0.01094 0.00520 C1 1 1.012691 0.162931 0.412953 11.00000 0.03367 0.03301 = 0.02564 -0.00335 0.00471 -0.00459 C2 1 1.196924 0.113129 0.376534 11.00000 0.04003 0.04092 = 0.03348 -0.00046 0.00777 0.00405 AFIX 43 H2 2 1.285494 0.071181 0.409027 11.00000 -1.20000 AFIX 0 C3 1 1.244589 0.127466 0.291521 11.00000 0.04414 0.04883 = 0.03142 -0.00952 0.01117 0.00459 AFIX 43 H3 2 1.369785 0.096299 0.266430 11.00000 -1.20000 AFIX 0 C4 1 1.102642 0.189312 0.243626 11.00000 0.05718 0.04698 = 0.02514 -0.00134 0.01189 0.00127 AFIX 43 H4 2 1.130414 0.197773 0.185740 11.00000 -1.20000 AFIX 0 C5 1 0.922570 0.238023 0.280163 11.00000 0.04888 0.03845 = 0.02581 0.00026 0.00844 -0.00025 AFIX 43 H5 2 0.831599 0.278803 0.246559 11.00000 -1.20000 AFIX 0 C6 1 0.873450 0.227297 0.367441 11.00000 0.03652 0.03314 = 0.02149 -0.00360 0.00581 -0.00772 C7 1 0.689667 0.280769 0.409226 11.00000 0.03503 0.03122 = 0.02654 -0.00180 0.00569 -0.00257 C8 1 0.531585 0.339101 0.361630 11.00000 0.04199 0.03681 = 0.03106 -0.00255 0.00408 0.00184 AFIX 43 H8 2 0.534531 0.342538 0.301580 11.00000 -1.20000 AFIX 0 C9 1 0.369931 0.392110 0.402427 11.00000 0.04979 0.03206 = 0.04040 -0.00381 0.00601 0.00421 C10 1 0.365709 0.388490 0.491985 11.00000 0.06583 0.04065 = 0.04710 -0.00846 0.02254 0.00652 AFIX 43 H10 2 0.259717 0.424627 0.519505 11.00000 -1.20000 AFIX 0 C11 1 0.519289 0.331113 0.539813 11.00000 0.06694 0.04379 = 0.03109 -0.00253 0.01595 0.00654 AFIX 43 H11 2 0.516727 0.328972 0.599946 11.00000 -1.20000 AFIX 0 C12 1 0.678492 0.276174 0.500146 11.00000 0.04318 0.03584 = 0.02553 -0.00232 0.01058 -0.00114 C13 1 1.216166 0.115689 0.586017 11.00000 0.04275 0.05921 = 0.03285 0.00648 0.00245 0.00505 AFIX 137 H13A 2 1.174562 0.111165 0.644994 11.00000 -1.50000 H13B 2 1.346116 0.158234 0.582604 11.00000 -1.50000 H13C 2 1.285574 0.064118 0.568128 11.00000 -1.50000 AFIX 0 HKLF 4 REM myn-33-4_a.res in P2(1)/c REM R1 = 0.0422 for 2236 Fo > 4sig(Fo) and 0.0455 for all 2453 data REM 155 parameters refined using 0 restraints END WGHT 0.0675 0.6665 REM Highest difference peak 1.068, deepest hole -0.753, 1-sigma level 0.126 Q1 1 0.3029 0.4801 0.3245 11.00000 0.05 1.07 Q2 1 0.1233 0.4693 0.3831 11.00000 0.05 0.73 Q3 1 0.1310 0.4088 0.3434 11.00000 0.05 0.63 Q4 1 0.1318 0.5506 0.3384 11.00000 0.05 0.60 Q5 1 0.0186 0.4768 0.3721 11.00000 0.05 0.59 Q6 1 -0.0385 0.4764 0.3439 11.00000 0.05 0.58 Q7 1 0.1414 0.4398 0.2659 11.00000 0.05 0.53 Q8 1 0.2771 0.3668 0.3538 11.00000 0.05 0.52 Q9 1 0.1479 0.5186 0.2637 11.00000 0.05 0.48 Q10 1 0.8202 0.2576 0.5156 11.00000 0.05 0.47 Q11 1 0.7166 0.4036 0.6515 11.00000 0.05 0.46 Q12 1 0.7639 0.1338 0.5227 11.00000 0.05 0.45 Q13 1 0.9084 0.0691 0.5040 11.00000 0.05 0.42 Q14 1 -0.1811 0.5367 0.3387 11.00000 0.05 0.42 Q15 1 0.9367 0.2119 0.5202 11.00000 0.05 0.42 Q16 1 0.9258 0.1997 0.5378 11.00000 0.05 0.41 Q17 1 0.0048 0.4781 0.2547 11.00000 0.05 0.39 Q18 1 1.0096 0.0914 0.1736 11.00000 0.05 0.38 Q19 1 0.2352 0.3769 0.4382 11.00000 0.05 0.37 Q20 1 1.0956 0.1389 0.5374 11.00000 0.05 0.37 REM The information below was added by Olex2. REM REM R1 = 0.0422 for 2236 Fo > 4sig(Fo) and 0.0455 for all 8822 data REM n/a parameters refined using n/a restraints REM Highest difference peak 1.07, deepest hole -0.75 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0455 REM R1_gt = 0.0422 REM wR_ref = 0.1252 REM GOOF = 1.077 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 8822 REM Reflections_gt = 2236 REM Parameters = n/a REM Hole = -0.75 REM Peak = 1.07 REM Flack = n/a ; _cod_data_source_file jo8b02729_si_001.cif _cod_data_source_block myn-33-4 _cod_database_code 4035894 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula 'C1 S1 O1 I1 H1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.87 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C4(H4), C5(H5), C8(H8), C10(H10), C11(H11) 2.b Idealised Me refined as rotating group: C13(H13A,H13B,H13C) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 8.279 _oxdiff_exptl_absorpt_empirical_full_min 0.487 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn I1 I 0.14157(8) 0.47957(2) 0.32797(2) 0.05456(18) Uani 1 1 d . S1 S 0.9280(2) 0.14044(7) 0.51720(6) 0.0316(2) Uani 1 1 d . O1 O 0.7552(6) 0.0693(2) 0.5115(2) 0.0426(8) Uani 1 1 d . N1 N 0.8291(8) 0.2206(3) 0.5554(2) 0.0404(9) Uani 1 1 d . C1 C 1.0127(8) 0.1629(3) 0.4130(3) 0.0307(9) Uani 1 1 d . C2 C 1.1969(9) 0.1131(3) 0.3765(3) 0.0379(10) Uani 1 1 d . H2 H 1.285494 0.071181 0.409027 0.045 Uiso 1 1 calc R C3 C 1.2446(10) 0.1275(3) 0.2915(3) 0.0409(11) Uani 1 1 d . H3 H 1.369785 0.096299 0.266430 0.049 Uiso 1 1 calc R C4 C 1.1026(10) 0.1893(3) 0.2436(3) 0.0425(11) Uani 1 1 d . H4 H 1.130414 0.197773 0.185740 0.051 Uiso 1 1 calc R C5 C 0.9226(10) 0.2380(3) 0.2802(3) 0.0374(10) Uani 1 1 d . H5 H 0.831599 0.278803 0.246559 0.045 Uiso 1 1 calc R C6 C 0.8734(8) 0.2273(3) 0.3674(2) 0.0302(9) Uani 1 1 d . C7 C 0.6897(8) 0.2808(3) 0.4092(3) 0.0308(9) Uani 1 1 d . C8 C 0.5316(9) 0.3391(3) 0.3616(3) 0.0366(10) Uani 1 1 d . H8 H 0.534531 0.342538 0.301580 0.044 Uiso 1 1 calc R C9 C 0.3699(10) 0.3921(3) 0.4024(3) 0.0407(10) Uani 1 1 d . C10 C 0.3657(11) 0.3885(3) 0.4920(3) 0.0500(13) Uani 1 1 d . H10 H 0.259717 0.424627 0.519505 0.060 Uiso 1 1 calc R C11 C 0.5193(11) 0.3311(3) 0.5398(3) 0.0465(12) Uani 1 1 d . H11 H 0.516727 0.328972 0.599946 0.056 Uiso 1 1 calc R C12 C 0.6785(9) 0.2762(3) 0.5001(3) 0.0343(9) Uani 1 1 d . C13 C 1.2162(10) 0.1157(4) 0.5860(3) 0.0451(12) Uani 1 1 d . H13A H 1.174562 0.111165 0.644994 0.068 Uiso 1 1 calc GR H13B H 1.346116 0.158234 0.582604 0.068 Uiso 1 1 calc GR H13C H 1.285574 0.064118 0.568128 0.068 Uiso 1 1 calc GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.0637(3) 0.0435(2) 0.0558(3) 0.00133(14) 0.00366(19) 0.01556(15) S1 0.0335(5) 0.0351(5) 0.0271(5) 0.0038(4) 0.0071(4) 0.0007(4) O1 0.0380(17) 0.0370(18) 0.054(2) 0.0036(15) 0.0125(15) -0.0040(14) N1 0.059(2) 0.041(2) 0.0228(16) 0.0007(15) 0.0109(16) 0.0052(19) C1 0.034(2) 0.033(2) 0.0256(19) -0.0033(16) 0.0047(16) -0.0046(18) C2 0.040(2) 0.041(2) 0.033(2) -0.0005(19) 0.0078(18) 0.004(2) C3 0.044(3) 0.049(3) 0.031(2) -0.010(2) 0.0112(19) 0.005(2) C4 0.057(3) 0.047(3) 0.025(2) -0.0013(19) 0.012(2) 0.001(2) C5 0.049(3) 0.038(2) 0.026(2) 0.0003(17) 0.0084(18) 0.000(2) C6 0.037(2) 0.033(2) 0.0215(17) -0.0036(16) 0.0058(16) -0.0077(18) C7 0.035(2) 0.031(2) 0.0265(19) -0.0018(16) 0.0057(16) -0.0026(18) C8 0.042(2) 0.037(2) 0.031(2) -0.0026(18) 0.0041(18) 0.002(2) C9 0.050(3) 0.032(2) 0.040(2) -0.0038(19) 0.006(2) 0.004(2) C10 0.066(3) 0.041(3) 0.047(3) -0.008(2) 0.023(2) 0.007(3) C11 0.067(3) 0.044(3) 0.031(2) -0.003(2) 0.016(2) 0.007(3) C12 0.043(2) 0.036(2) 0.0255(19) -0.0023(17) 0.0106(17) -0.001(2) C13 0.043(3) 0.059(3) 0.033(2) 0.006(2) 0.0025(19) 0.005(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.3257 6.8362 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O1 S1 N1 118.5(2) O1 S1 C1 108.7(2) O1 S1 C13 108.2(2) N1 S1 C1 107.6(2) N1 S1 C13 104.4(2) C1 S1 C13 109.2(2) C12 N1 S1 119.3(3) C2 C1 S1 119.6(3) C2 C1 C6 123.3(4) C6 C1 S1 116.9(3) C1 C2 H2 120.6 C3 C2 C1 118.8(4) C3 C2 H2 120.6 C2 C3 H3 120.4 C2 C3 C4 119.2(4) C4 C3 H3 120.4 C3 C4 H4 119.3 C5 C4 C3 121.5(4) C5 C4 H4 119.3 C4 C5 H5 119.4 C4 C5 C6 121.3(4) C6 C5 H5 119.4 C1 C6 C5 115.9(4) C1 C6 C7 121.8(4) C5 C6 C7 122.4(4) C8 C7 C6 121.6(4) C8 C7 C12 118.3(4) C12 C7 C6 120.1(4) C7 C8 H8 119.5 C9 C8 C7 121.1(4) C9 C8 H8 119.5 C8 C9 I1 119.4(3) C10 C9 I1 120.4(4) C10 C9 C8 120.2(5) C9 C10 H10 120.3 C11 C10 C9 119.5(4) C11 C10 H10 120.3 C10 C11 H11 119.3 C10 C11 C12 121.3(4) C12 C11 H11 119.3 N1 C12 C7 123.8(4) C11 C12 N1 116.6(4) C11 C12 C7 119.6(4) S1 C13 H13A 109.5 S1 C13 H13B 109.5 S1 C13 H13C 109.5 H13A C13 H13B 109.5 H13A C13 H13C 109.5 H13B C13 H13C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance I1 C9 2.091(5) S1 O1 1.446(3) S1 N1 1.534(4) S1 C1 1.750(4) S1 C13 1.754(5) N1 C12 1.406(6) C1 C2 1.401(6) C1 C6 1.403(6) C2 H2 0.9300 C2 C3 1.380(6) C3 H3 0.9300 C3 C4 1.396(7) C4 H4 0.9300 C4 C5 1.376(7) C5 H5 0.9300 C5 C6 1.408(5) C6 C7 1.474(6) C7 C8 1.394(6) C7 C12 1.412(5) C8 H8 0.9300 C8 C9 1.388(6) C9 C10 1.386(7) C10 H10 0.9300 C10 C11 1.374(8) C11 H11 0.9300 C11 C12 1.390(6) C13 H13A 0.9600 C13 H13B 0.9600 C13 H13C 0.9600 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 2 162.8 4.92 0 0 -2 151.07 4.3 0 0 -2 161.1 5.87 0 0 -3 -0.15 0.17 0 0 3 0.08 0.36 0 0 -3 0.05 0.47 0 0 -4 10.79 1.71 0 0 4 14.16 2.01 0 0 -4 13.41 1.12 0 0 -4 12.85 2.34 0 0 5 1.27 0.74 0 0 5 1.65 0.81 0 0 -5 0.86 0.63 0 0 -5 -0.38 0.52 0 0 -5 0.21 0.59 0 0 -5 1.6 0.35 0 0 6 2494.45 38.69 0 0 -6 2534.88 39.72 0 0 -6 2563.83 45.39 0 0 -7 0.93 1.05 0 0 7 -0.05 0.9 0 0 7 2.42 1.12 0 0 -7 1.8 1.15 0 0 -8 54.54 7.01 0 0 8 53.77 6.15 0 0 -8 69.55 8.38 0 0 -8 51.07 7.37 0 0 8 53.94 6.36 0 0 9 -0.7 0.96 0 0 -9 0.31 1.29 0 0 9 -1.31 1.47 0 0 9 -0.33 1.38 0 0 -9 0.11 0.56 0 0 10 47.03 6.85 0 0 -10 48.97 8.37 0 0 10 47.82 7.32 0 0 -11 1.79 1.29 0 0 11 0.36 0.62 0 0 12 662.86 24.2 0 0 13 0.55 1.49 0 0 14 80.82 8.96 0 0 15 0.97 1.15 0 0 -15 3.96 3.28 0 0 -16 1.38 2.14 0 0 -16 -1.06 1.34 0 0 -17 0 0.36 0 0 17 1.34 1.41 0 0 -17 0.45 0.55 0 0 18 13.06 2.79 0 0 -18 14.09 3.28 0 -1 -1 176.87 4.96 0 -1 1 170.54 4.04 0 1 1 177.61 3.7 0 -1 2 831.49 11.47 0 -1 2 827.87 13.19 0 1 -2 746.23 13.99 0 1 -2 886.48 13.76 0 -1 -2 842.79 13.44 0 1 -2 795 14.07 0 -1 -2 751.55 13.42 0 1 -3 5138.85 52.38 0 1 -3 5373.83 52.68 0 -1 3 4641.16 48.99 0 1 3 5236.95 51.21 0 -1 3 4944.27 46.52 0 1 -4 857.05 18.73 0 1 -4 847 18.33 0 1 4 839.53 17.41 0 -1 4 854.12 17.11 0 1 5 728.94 17.97 0 -1 -5 697.18 20.54 0 1 -5 787.7 20.07 0 -1 5 734.93 18.35 0 1 -5 674.39 19.88 0 -1 -5 719.35 15.69 0 1 -5 722.83 18.8 0 -1 -5 769.17 22.58 0 -1 5 724.69 17.44 0 1 5 756.68 18.13 0 -1 -6 525.87 20.44 0 -1 6 520.51 13.82 0 -1 6 500.7 16.68 0 1 -6 513.56 17.95 0 -1 -6 488.71 14.95 0 1 6 509.91 16.77 0 -1 -6 440.36 18.28 0 1 -6 498.92 17.45 0 1 6 509.91 16.3 0 1 -6 472.16 18.27 0 -1 6 482.26 15.55 0 -1 7 135.09 9.38 0 1 7 131.36 8.88 0 1 -7 136.1 10.12 0 -1 -7 133.78 8.93 0 1 -7 145.34 10.42 0 1 7 130.44 9.1 0 -1 -7 125.89 10.92 0 -1 7 126.43 8.62 0 -1 7 131.86 7.42 0 -1 -7 144.57 11.67 0 -1 8 285.71 15.19 0 -1 -8 305.6 18.68 0 1 -8 322.7 17.86 0 1 8 287.23 15 0 1 -8 301.92 16.73 0 -1 -8 318.01 16.24 0 1 8 324.05 15.4 0 -1 8 297.47 14.68 0 -1 -8 300.56 18.87 0 -1 8 294.12 12.22 0 1 -9 1668.91 47.58 0 1 -9 1598.95 43.27 0 1 9 1442.17 37.03 0 -1 -9 1522.14 46.1 0 1 9 1544.16 39.64 0 -1 -9 1434.32 46.33 0 -1 9 1510.88 31.65 0 -1 9 1420.56 38.76 0 -1 9 1426.3 36.76 0 -1 -10 29.12 6.71 0 -1 10 22.89 5.1 0 1 -10 28.76 6.95 0 1 10 24.42 5.04 0 1 -10 27.38 5.9 0 1 10 22.09 5.17 0 -1 10 25.1 5.23 0 1 -11 301.22 21.42 0 1 11 272.94 19.48 0 -1 11 273.59 19.5 0 -1 -11 289.6 22.73 0 1 12 21.03 4.27 0 -1 12 18.42 3.97 0 1 13 0.77 1.34 0 -1 13 -0.38 1.45 0 -1 14 8.36 3.04 0 1 14 9.52 3.05 0 1 15 184.73 13.39 0 1 -15 259.04 21.16 0 -1 -15 169.56 11.91 0 -1 -15 256.29 20.27 0 -1 15 182.94 13.37 0 1 -16 1.43 1.59 0 -1 16 1.06 0.94 0 1 16 3.39 2.14 0 -1 -16 5.54 3.19 0 1 -16 5.09 2.85 0 -1 -17 119.39 10.93 0 1 -17 123.15 11.26 0 -1 17 110.73 9.43 0 1 -17 84.25 7.63 0 1 17 97.87 8.73 0 -1 -18 13.22 3.09 0 1 18 9.9 2.65 0 -1 18 14.56 3.16 0 1 -18 11.72 2.96 0 1 -18 9.47 2.07 0 2 0 423.8 11.61 0 -2 0 461.89 12.42 0 -2 1 102.35 4.48 0 2 1 102.57 3.88 0 -2 -1 93.55 3.81 0 -2 1 90.13 3.28 0 -2 -1 116.26 3.99 0 2 -1 100.97 4.68 0 -2 1 109.35 3.23 0 -2 -1 103.25 5.25 0 2 2 1321.62 16.79 0 -2 2 1343.87 21.06 0 -2 -2 1465.51 21.74 0 2 2 1358 20.84 0 -2 2 1292.81 14.71 0 -2 -2 1277.01 19.52 0 -2 -2 1345.14 14.17 0 2 -2 1412.5 18.86 0 -2 2 1330.03 18.33 0 2 -3 553.12 12.64 0 -2 3 534.42 11.1 0 -2 -3 547.13 13.4 0 -2 -3 493.76 13.5 0 2 3 559.31 13.34 0 -2 3 501.9 12.73 0 2 4 593.71 15.7 0 -2 4 645.22 13.34 0 2 -4 650.73 15.63 0 -2 4 611.3 15.27 0 2 -4 601.92 17.23 0 -2 -4 616.17 17.8 0 2 -5 27.04 3.44 0 -2 -5 24.05 2.51 0 -2 5 26.88 2.84 0 2 5 27.76 3.55 0 2 -5 24.94 3.71 0 -2 -5 21.9 4.15 0 -2 -5 23.82 3.91 0 -2 5 24.13 3.21 0 2 5 24.16 3.24 0 -2 5 28.31 3.68 0 -2 6 2782.74 43.6 0 -2 6 2910.93 39.15 0 2 -6 3056.67 50.78 0 2 6 2988.86 45.82 0 2 6 2938.37 45.42 0 -2 -6 2960.05 56.57 0 -2 6 2857.93 45.99 0 2 -6 3122.36 46.62 0 -2 -6 2861.98 39.57 0 -2 -6 2883.52 53.41 0 -2 -7 441.77 21.97 0 -2 7 448.66 14.31 0 -2 7 415.32 16.32 0 2 7 459.47 17.99 0 -2 -7 459.29 15.98 0 -2 -7 435.66 21.54 0 2 -7 440.74 17.55 0 2 7 437.06 17.17 0 2 -7 461.8 20.02 0 -2 7 439.07 17.78 0 2 -8 838.08 30.7 0 -2 8 815.89 26.74 0 2 8 817.09 25.76 0 -2 -8 866.69 33.77 0 -2 8 782.68 24.88 0 2 -8 845.22 27.17 0 -2 -8 874.36 34.29 0 -2 8 823.41 21.42 0 2 8 817.57 26.52 0 -2 9 21.09 4.22 0 -2 -9 20.1 5.43 0 -2 -9 19.64 5.55 0 -2 9 16.05 4.03 0 2 -9 16.58 4.13 0 2 -9 19.84 4.96 0 2 9 13.08 3.54 0 2 9 12.91 3.15 0 2 10 6.87 2.92 0 2 -10 8.05 3.78 0 2 -10 5.96 2.73 0 -2 10 6.96 2.91 0 -2 -10 6.07 3.29 0 -2 10 6.07 2.72 0 2 10 6.13 2.47 0 -2 -11 5.02 2.76 0 2 11 8.08 3.08 0 -2 11 4.86 2.72 0 2 12 444.6 19.88 0 -2 12 431.48 19.37 0 -2 13 224.05 14.49 0 2 13 225.85 14.72 0 2 14 247.18 15.72 0 -2 14 231.98 15.29 0 2 -15 72.92 10.85 0 2 15 59.03 7.54 0 -2 15 57.36 7.54 0 -2 -15 86.75 11.24 0 2 16 3.05 2.04 0 2 -16 1.91 1.66 0 -2 16 0.92 1 0 2 -16 1.39 1.59 0 -2 -16 1.42 1.17 0 -2 17 24.06 4.48 0 2 -17 19.78 3.89 0 2 -17 23.77 4.74 0 -2 -17 23.59 4.69 0 2 17 16.29 3.4 0 -2 18 37.14 4.92 0 2 -18 35.66 4.22 0 -2 -18 39.86 5.15 0 2 -18 36.78 4.9 0 -3 0 -0.07 0.64 0 3 0 2.5 1.28 0 3 1 1406.29 21.9 0 -3 -1 1491.33 27.43 0 -3 1 1385.93 24.31 0 3 -1 1453.89 28.05 0 -3 -1 1486.11 29.91 0 -3 1 1366 21.3 0 -3 1 1534.75 16.83 0 -3 -1 1485.39 20.78 0 -3 2 377.06 8.03 0 3 -2 362.35 9.38 0 -3 -2 362.64 10.32 0 -3 -2 396.15 12.73 0 3 2 334.17 11.25 0 -3 2 375.42 10.69 0 -3 -2 391.39 7.61 0 3 2 360.47 8.76 0 3 -2 366.39 11.14 0 -3 3 2657.45 38.41 0 -3 -3 2631.41 37.8 0 3 -3 2679.4 33.83 0 -3 3 2705.37 27.97 0 3 3 2652.41 37.91 0 -3 -3 2694.09 38.03 0 3 3 2751.64 31.29 0 -3 -4 480.55 14.95 0 3 4 491.81 14.87 0 -3 4 462.75 14.52 0 3 4 505.08 14.95 0 -3 4 469.67 12.45 0 -3 -4 488.37 16.61 0 3 -4 491.62 17.52 0 3 -4 513.07 13.78 0 -3 5 1004.5 20.25 0 -3 5 1036.03 24.94 0 -3 -5 1091.6 29.03 0 3 -5 1005.82 27.44 0 3 5 1023.38 23.76 0 3 5 1041.21 24.92 0 3 -5 1071.19 22.83 0 -3 5 991.54 23.13 0 -3 6 4.75 1.76 0 -3 6 2.6 1.13 0 -3 -6 2.37 1.51 0 3 -6 2.93 1.48 0 3 6 2.73 1.13 0 3 6 2.5 1.35 0 -3 -6 1.89 1.32 0 -3 -6 2.08 0.99 0 -3 6 2.94 0.96 0 3 -6 2.25 1.02 0 -3 -7 61.08 8.39 0 3 -7 61.76 7.81 0 3 -7 58.68 6.14 0 3 7 57.55 6.44 0 -3 7 54.6 5.05 0 -3 7 58.46 6.78 0 3 7 55.06 6.39 0 -3 7 55.81 6.08 0 -3 -7 69.75 9.42 0 -3 -8 52.6 8.55 0 -3 8 42.51 5.77 0 -3 -8 50.02 8.61 0 3 -8 56.92 8.19 0 -3 8 44.36 6.33 0 -3 8 47.16 5.13 0 3 -8 44.68 5.86 0 3 8 45.54 6.17 0 3 8 37.61 5.82 0 3 -9 705.22 25.98 0 -3 -9 682.47 34.37 0 -3 9 678.73 27.38 0 3 -9 703.59 32.64 0 3 9 675.59 26.09 0 -3 -9 758.96 36.98 0 -3 9 660.35 25.16 0 3 9 660.71 26.44 0 -3 10 229.74 15.85 0 -3 -10 235 21.48 0 -3 -10 274.89 23.86 0 3 10 230.22 16.11 0 3 -10 271.84 22.31 0 3 10 219.23 16.48 0 3 11 402.19 24.04 0 -3 -11 445.72 31.08 0 -3 12 1.58 1.42 0 3 12 1.2 0.73 0 3 13 3.16 1.39 0 -3 13 1.49 1.28 0 -3 -14 25.38 6.12 0 3 -14 23.82 6.47 0 -3 14 19.03 4.3 0 3 14 19.57 4.34 0 -3 15 106.14 10.37 0 3 15 98.64 9.69 0 3 -15 119.63 12.68 0 -3 -15 118.99 12.33 0 -3 16 91.72 9.32 0 -3 -16 102.16 10.47 0 3 16 90.49 8.86 0 3 -16 94.8 10.03 0 3 -16 96.3 10.15 0 3 -17 29.14 4.92 0 -3 17 34.63 5.43 0 3 -17 31.8 5.11 0 3 17 37.77 5.19 0 -3 -17 35.5 5.36 0 -3 -18 0.55 0.41 0 3 -18 0.97 0.79 0 -3 18 0.17 0.87 0 3 -18 1 0.74 0 4 0 412.23 14.31 0 -4 0 520.87 16.65 0 -4 -1 1148.04 19.34 0 4 1 1202.63 23.35 0 4 -1 1127.9 26.99 0 -4 1 1184.75 16.55 0 -4 1 1159.18 22.6 0 -4 -1 1132.5 27.38 0 -4 -2 2609.68 30.26 0 -4 -2 2404.53 40.6 0 4 -2 2552.24 38.95 0 -4 -2 2349.92 33.33 0 -4 2 2466.29 37.33 0 -4 2 2339.92 30.62 0 4 2 2355.59 31.65 0 -4 2 2420.8 26.73 0 4 3 54.65 4.99 0 4 3 50.49 5.06 0 4 -3 57.75 5.02 0 -4 -3 49.02 2.59 0 -4 3 53.2 3.23 0 -4 3 54.3 4.65 0 4 -3 57.51 4.27 0 -4 -3 52.93 5.23 0 4 3 55.28 3.76 0 -4 -3 51.1 4.79 0 -4 -4 518.98 18.04 0 4 -4 480.55 13.69 0 -4 -4 461.25 16.12 0 4 -4 464.09 14.53 0 -4 4 497.08 10.13 0 -4 4 462.13 14.08 0 4 4 477.72 16.16 0 4 4 490.9 16.65 0 -4 4 478.22 16.63 0 4 -4 470.68 19.07 0 -4 -5 151.69 9.53 0 4 5 142.74 9.13 0 -4 5 149.01 9.52 0 4 -5 146.79 8.08 0 4 -5 146.15 11.17 0 -4 5 148.33 5.39 0 -4 5 137.71 7.77 0 -4 -5 170.21 11.82 0 -4 6 836.65 20.91 0 -4 -6 983.69 32.61 0 4 -6 940.44 23.1 0 -4 6 839.35 24.24 0 4 6 882.69 24.83 0 -4 -6 774.66 17.52 0 4 6 896.09 26.34 0 4 -6 882.49 29.9 0 -4 -7 269.03 18.67 0 4 -7 230.94 16.22 0 4 7 224.97 13.2 0 -4 -7 240.16 19.21 0 4 7 251.12 14.58 0 -4 7 232.26 11.29 0 4 -7 247.32 12.57 0 -4 7 214.48 12.72 0 -4 8 830.53 27.69 0 4 -8 977 36.7 0 -4 8 893.9 24.41 0 -4 -8 950.76 41.25 0 4 8 931.15 29.8 0 4 8 922.76 30.3 0 4 -9 26.26 6.54 0 -4 9 13.76 3.7 0 -4 -9 29.88 7.37 0 -4 -9 17.68 6.17 0 4 9 17.73 4.39 0 4 9 21.33 4.73 0 -4 -10 209.06 21.75 0 4 -10 217.53 20.23 0 4 10 191.66 15.61 0 -4 10 194.53 15.17 0 4 10 193.56 15.34 0 -4 -11 75.75 13.66 0 4 -11 85.98 13.79 0 4 11 69.27 10.08 0 4 12 225.05 14.22 0 -4 12 210.86 13.64 0 -4 13 120.19 10.8 0 4 13 120.82 10.79 0 4 14 109.46 10.51 0 -4 14 116.06 10.89 0 4 -14 122.45 12.5 0 -4 -14 127.28 12.51 0 4 -15 19.56 4.72 0 4 15 16.59 3.9 0 -4 15 16.35 4.04 0 -4 -15 23.68 5.12 0 4 -16 10.5 3.38 0 -4 16 7.95 2.8 0 -4 -16 9.66 3.11 0 4 16 10.43 2.86 0 4 -16 5.73 2.36 0 4 -17 4.68 1.76 0 4 -17 5.75 2.28 0 -4 -17 7.62 2.38 0 -4 17 8.16 2.85 0 4 -18 81.91 6.44 0 -4 -18 77.66 6 0 -4 18 91.86 7.39 0 5 0 0.1 0.62 0 -5 0 0.71 0.69 0 5 0 1.77 1.45 0 -5 0 0.49 0.85 0 -5 -1 1074.95 29.93 0 -5 1 1253.12 33.84 0 -5 -1 1193.92 20.81 0 -5 1 1136.35 28.44 0 5 1 1128.17 25.4 0 5 -1 1094.17 28.05 0 -5 1 1286.18 25.89 0 5 -1 1145.12 28.54 0 -5 -2 721.22 16.56 0 -5 2 720.53 11.71 0 5 -2 670.68 23.13 0 -5 2 717.3 17.21 0 -5 2 712.15 21.25 0 -5 -2 691.45 22.99 0 -5 -2 722.51 17.21 0 5 -2 707.25 21.82 0 5 2 680.16 17.29 0 5 2 640.31 21.32 0 -5 3 1599.66 25.1 0 -5 3 1633.39 32.16 0 -5 -3 1646.45 22.1 0 -5 -3 1589.69 35.12 0 -5 -3 1672.75 31.08 0 5 -3 1713.41 39.27 0 5 3 1613.28 35.29 0 -5 3 1649.83 22.56 0 5 -3 1780.04 34.59 0 5 3 1537.51 25.29 0 -5 -4 532.23 19.28 0 5 -4 538.45 22.39 0 5 4 542.85 13.85 0 -5 4 516.04 17.12 0 5 4 573.82 19.27 0 5 -4 544.55 18.2 0 -5 4 549.76 13.71 0 5 4 536.44 19.69 0 -5 4 559.83 12.45 0 5 -5 907.33 30.8 0 -5 5 874.77 22.86 0 5 -5 864.13 23.18 0 5 5 873.36 25.2 0 5 -5 935.92 21.72 0 5 5 865.05 25.78 0 -5 -5 885.06 25.87 0 5 6 125.19 9.81 0 -5 6 131 10.29 0 -5 -6 163.01 13.25 0 5 6 143.43 11.12 0 5 -6 135.82 12.47 0 5 -6 156.52 9.25 0 -5 -6 152.75 10.94 0 -5 6 134.64 8.88 0 5 -6 131.6 9.06 0 -5 -7 180.09 17.99 0 5 7 161.13 12.44 0 5 7 159.23 11.69 0 5 -7 166.34 10.46 0 -5 -7 213.7 16.99 0 5 -7 169.83 14.7 0 -5 7 154.35 11.69 0 -5 7 166.94 10.39 0 5 -8 365.36 16.43 0 5 8 360.56 19.03 0 -5 -8 393.48 28.16 0 -5 8 359.36 16.2 0 5 -8 383.47 23.84 0 5 8 353.08 19.57 0 -5 8 346.09 18.59 0 5 -9 308.44 22.85 0 -5 -9 317.12 26.86 0 5 9 273.58 18 0 -5 9 286.6 18.12 0 5 9 280.79 18.22 0 -5 -10 65.96 12.26 0 5 10 60.81 9.1 0 5 -10 68.17 11.63 0 5 10 53.17 8.5 0 -5 10 50.06 7.99 0 -5 -10 59.27 12.5 0 -5 11 291.88 15.48 0 5 12 127.19 11 0 -5 12 123.82 10.71 0 -5 -13 9.2 3.32 0 5 -13 10.14 3.37 0 5 13 6.58 2.62 0 -5 13 10.9 3.38 0 5 14 128.7 11.2 0 5 -14 135.44 11.7 0 -5 -14 150.94 12.56 0 -5 14 118.86 11.06 0 5 15 78.18 8.42 0 5 -15 84.49 8.78 0 -5 15 83.46 9.07 0 -5 -15 84.92 8.84 0 -5 16 16.84 4.05 0 5 -16 14.88 3.94 0 5 -16 13.72 3.24 0 -5 -16 15.88 3.45 0 5 -17 31.14 4.15 0 5 -17 32.72 4.93 0 -5 17 29.95 4.9 0 -5 -17 32.26 4.22 0 5 -18 31.96 3.82 0 -5 18 33.52 4.22 0 6 0 1139.7 30.19 0 -6 0 1128.48 31.07 0 6 0 1105.58 28.68 0 -6 0 1137.28 33.91 0 -6 0 1115.63 19.94 0 -6 1 964.93 31.83 0 -6 1 1033.59 24.32 0 -6 -1 922.89 29.95 0 -6 -1 921.71 18.71 0 6 -1 949.76 27.54 0 -6 1 927.5 27.57 0 6 1 933.41 24.39 0 6 -1 868.59 25.67 0 6 1 862.54 26.51 0 6 2 481 20.28 0 6 -2 501.65 20.8 0 6 -2 545.16 20.85 0 -6 2 519.79 20.17 0 -6 -2 543.66 16.14 0 -6 -2 514.86 22.04 0 -6 -2 550.72 15.25 0 6 2 544.45 17.23 0 -6 2 572.21 16.81 0 -6 2 575.39 25.02 0 -6 3 16.31 2.58 0 -6 -3 16.25 3.72 0 6 -3 15.74 3.94 0 6 3 16.58 3.79 0 6 -3 14.11 3.44 0 6 3 15.14 2.46 0 -6 3 16.38 3.57 0 -6 -3 17.15 2.9 0 -6 4 168.9 10.97 0 6 4 171.11 12.36 0 6 -4 176.57 13.63 0 6 4 167.81 11.42 0 -6 -4 163.11 11.66 0 -6 -4 196.27 11.51 0 6 -4 177.72 11.63 0 -6 -5 615.02 23.39 0 6 -5 591.86 21.42 0 -6 5 563.7 20.39 0 6 5 605.58 22.83 0 6 -5 594.47 26.35 0 6 5 585.72 23.38 0 6 -6 720.8 24.32 0 -6 -6 762.74 27.07 0 -6 6 763 24.15 0 6 -6 776.47 31.8 0 6 6 755.99 26.55 0 -6 -7 528.96 33.41 0 6 7 516.5 22.69 0 6 -7 506.77 26.98 0 6 -7 498.75 20.38 0 6 7 508.93 23.92 0 -6 7 503.86 20.06 0 6 -8 324.12 22.67 0 6 8 305.29 18.41 0 -6 -8 358.14 28.59 0 6 8 302.26 19.28 0 6 -9 217.97 19.79 0 6 9 210.64 16.69 0 -6 -9 232.42 24.16 0 6 9 197.69 15.99 0 -6 -10 99.73 14.78 0 6 10 65.51 9.84 0 6 -10 74.58 12.17 0 -6 -10 67.56 13.78 0 6 11 186.61 12.57 0 -6 11 186.98 12.73 0 6 12 155.74 11.97 0 -6 12 149.41 11.91 0 -6 13 14.71 3.84 0 6 13 11.53 3.48 0 -6 -13 18.95 4.26 0 6 14 150.89 11.99 0 -6 14 145.39 12.24 0 -6 -14 160.65 11.94 0 6 -15 85.46 7.85 0 -6 -15 101.41 8.85 0 -6 -16 3.06 1.5 0 6 -16 3.05 1.83 0 -6 16 4.41 2.33 0 6 -17 43.68 5.3 0 -6 17 61.46 6.64 0 6 -18 0.02 0.34 0 -7 0 0.13 1.42 0 -7 0 -0.05 0.27 0 7 0 -0.15 0.43 0 7 -1 58.86 6.75 0 -7 1 59.22 7.17 0 -7 -1 59.72 4.49 0 -7 -1 53.9 7.57 0 7 1 56.25 7.03 0 -7 1 64.29 6.01 0 7 -1 66.24 7.5 0 7 1 67.73 6.71 0 -7 1 62.65 8.61 0 -7 2 619.11 24.05 0 7 2 574.3 23.95 0 -7 -2 667.79 17.1 0 -7 -2 591.83 25.86 0 -7 2 684.09 19.38 0 -7 2 643.66 28.36 0 7 -2 607.77 23.52 0 7 -2 582.16 23.32 0 -7 -2 629.11 19.25 0 7 2 643.34 20.45 0 -7 3 1411.51 44.07 0 7 3 1225.16 37.17 0 7 -3 1324.1 36.68 0 -7 -3 1286.48 38.57 0 -7 3 1317.17 36.04 0 7 -3 1345.46 38.57 0 7 -4 781.33 27.39 0 7 -4 759.1 30.05 0 -7 4 752.6 26.74 0 7 4 769.64 29.61 0 7 4 847.24 28.76 0 -7 -4 765.47 28.63 0 -7 -5 98.93 10.11 0 7 5 103 10.13 0 7 -5 105.38 10.02 0 7 -5 114.99 12.1 0 7 5 113.49 11.31 0 -7 5 98.46 9.38 0 -7 -6 12.19 3.53 0 7 6 7.99 2.99 0 7 -6 5.47 2.75 0 -7 6 7.87 2.56 0 -7 -6 11.82 3.66 0 7 6 8.85 2.88 0 7 -6 5.25 2.12 0 -7 7 33.76 5.63 0 7 7 24.6 5.31 0 7 -7 22.53 4.79 0 7 -7 25.5 6.29 0 -7 -7 30.43 6.27 0 -7 -7 26.1 7.77 0 7 7 25.32 5.85 0 -7 -8 347.64 29.45 0 7 8 309.23 19.71 0 7 8 322.72 21.23 0 7 -8 349.41 24.21 0 7 -9 585.88 33.09 0 7 9 563.52 28.44 0 7 9 562.08 29.09 0 -7 10 639.25 23.42 0 7 11 6.5 2.34 0 -7 11 3.99 1.87 0 7 12 25.97 4.81 0 -7 12 32.32 5.57 0 -7 13 3.05 1.75 0 7 13 3.98 2.02 0 -7 14 42.26 6.56 0 -7 15 15.48 3.96 0 7 -15 15.89 3.92 0 7 -16 21.96 4.1 0 -7 16 29.38 5.06 0 7 -17 56.01 5.36 0 -7 17 55.24 5.91 0 -8 0 1396.42 43.1 0 8 0 1393.79 37.4 0 -8 -1 1378.72 34.6 0 -8 1 1285.55 37.17 0 -8 1 1252.58 41.32 0 -8 -1 1288.26 41.17 0 8 -1 1281.2 36.3 0 8 1 1211.59 35.82 0 8 -1 1309.94 36.03 0 8 1 1289.53 32.11 0 -8 2 79.09 10.58 0 -8 -2 79.03 9.95 0 8 -2 76.42 8.53 0 8 -2 81.52 9.01 0 -8 2 71.3 8.56 0 8 2 82.13 9.48 0 8 -3 229.04 15.77 0 -8 3 215.55 15.15 0 -8 3 220.01 18.04 0 8 3 216.41 16.18 0 8 -3 236.63 15.57 0 -8 -3 220 16.71 0 -8 4 73.68 8.88 0 8 -4 69.73 8.69 0 8 -4 71.13 9.18 0 -8 4 71.6 10.6 0 8 4 76.45 9.27 0 8 4 66.17 9.24 0 -8 -4 65.98 9 0 8 5 1236.3 41.82 0 8 -5 1248.71 37.53 0 -8 5 1279.25 38.08 0 -8 -5 1181.11 39.24 0 8 5 1157.38 38.39 0 8 -5 1222.92 41.22 0 -8 5 1280 46.59 0 8 -6 444.97 25.39 0 -8 -6 430.96 23.74 0 -8 6 430.69 22.13 0 8 6 436.42 23.45 0 8 6 442.41 24.8 0 8 -6 457.06 22.81 0 8 7 738.42 32.05 0 -8 -7 801.3 33.62 0 -8 7 800.24 30.97 0 8 -7 843.26 31.53 0 8 -7 750.26 34.76 0 8 7 748.09 34.38 0 -8 -7 907.05 46.91 0 8 8 48.45 8.21 0 8 -8 44.97 8.82 0 8 8 43.44 8.53 0 -8 -8 63.94 12.9 0 8 9 23.34 5.86 0 8 9 25.41 6.56 0 -8 10 30.63 5.21 0 -8 11 18.26 4.16 0 -8 12 46.17 6.76 0 -8 13 120.66 11.04 0 -8 14 2.85 2.13 0 -8 15 8.99 2.78 0 8 -15 6.93 2.47 0 8 -16 3.61 1.66 0 -8 16 1.88 1.34 0 -8 17 8.47 2.15 0 8 -17 5.72 1.62 0 9 0 2.29 1.08 0 9 0 1.15 1.39 0 9 1 120.17 11.66 0 -9 1 121.7 13.3 0 -9 -1 124.73 13.27 0 9 -1 126.57 11.44 0 9 -1 131.07 11.89 0 -9 -2 1144.85 41.34 0 9 2 1129.79 37.95 0 9 -2 1156.03 36.13 0 -9 2 1142.85 42.3 0 9 -2 1209.5 38.95 0 -9 2 1111.63 36.54 0 -9 3 8.81 4.14 0 -9 -3 9.6 4.15 0 9 -3 12.61 3.72 0 -9 3 14.22 4.34 0 9 -3 9.84 3.34 0 9 3 8.51 3.44 0 9 4 1556.85 46.1 0 9 -4 1484.77 42.55 0 9 -4 1504.53 44.7 0 9 4 1505.31 48.05 0 -9 -4 1423.53 46.2 0 -9 4 1523.33 43.99 0 -9 4 1492.12 51.71 0 -9 5 133.21 15.67 0 -9 -5 134.34 14.13 0 9 5 129.85 14.33 0 9 -5 129.44 13.34 0 -9 5 138.75 12.97 0 9 -5 128.85 12.36 0 9 5 137.45 13.56 0 9 -6 25.41 5.52 0 -9 6 21.89 6.82 0 -9 -6 28.57 6.6 0 9 6 27.71 6.22 0 9 6 26.3 6.34 0 9 -6 22.48 5.77 0 -9 6 25.15 5.55 0 9 -7 40.81 7.28 0 -9 -7 58.7 11.95 0 9 -7 49.63 8.76 0 9 7 40.6 8.03 0 -9 -7 43.38 8.07 0 -9 7 49.35 10.48 0 9 -8 98.37 12.91 0 -9 8 106.4 15.51 0 -9 -8 128.04 18.37 0 9 8 95.53 13.24 0 9 8 92.2 12.19 0 -9 -9 11.69 3.52 0 -9 9 10.72 3.3 0 -9 10 485.3 20.46 0 -9 10 413.71 20.28 0 -9 11 377.09 19.47 0 -9 12 5.78 2.9 0 -9 13 32.84 5.6 0 -9 14 2.72 2.06 0 9 -14 3.19 1.91 0 -9 15 43.2 5.8 0 9 -15 41.78 5.12 0 9 15 42.76 5.58 0 -9 16 125.87 8.86 0 9 16 110.44 7.45 0 9 -16 110.89 7.35 0 -10 0 22.73 6.03 0 10 0 19.31 5.07 0 10 -1 1008.14 35.01 0 -10 -1 1007.91 40.35 0 10 1 932.29 35.25 0 -10 1 983.8 40.36 0 10 -1 1032.43 34.69 0 10 -2 164 14.42 0 10 2 149.07 14.24 0 -10 -2 143.26 15.08 0 -10 2 165.18 16.67 0 10 -2 138 12.98 0 -10 3 52.47 9.53 0 -10 -3 63.09 10.01 0 10 3 54.02 8.95 0 10 -3 58.45 9.16 0 -10 3 50.39 7.98 0 10 -3 45.68 7.36 0 10 4 144.78 14.26 0 10 4 132.81 14.7 0 10 -4 128.07 12.55 0 -10 -4 128.2 14.33 0 -10 4 137.51 16.14 0 10 -4 126.81 12.8 0 -10 4 119.71 12.65 0 10 -5 109.72 11.71 0 10 5 128.71 14.8 0 -10 -5 120.86 13.84 0 -10 5 119.4 15.63 0 10 5 104.92 12.67 0 10 -5 103.33 11.99 0 -10 5 112.26 12.36 0 10 6 7.66 3.4 0 10 -6 1.12 0.85 0 10 -6 4.28 2.44 0 -10 -6 3.8 2.18 0 -10 6 8.07 3.93 0 -10 6 2.4 2.45 0 10 6 2.47 1.97 0 10 7 634.43 33.18 0 -10 -7 768.25 43.47 0 -10 -8 39.74 6.44 0 -10 8 44.21 6.43 0 -10 -9 64.76 8.29 0 -10 9 65.6 8.09 0 -10 10 6.59 2.71 0 -10 10 5.88 2.4 0 -10 11 144.99 10.23 0 -10 11 142.19 11.93 0 -10 12 33.24 5.76 0 10 -13 432.12 17.66 0 -10 13 409.76 19.55 0 -10 14 27.21 4.8 0 10 -14 29.84 4.29 0 -10 15 11.35 2.74 0 10 15 12.55 2.82 0 10 -15 9.31 2.24 0 10 -16 4.78 1.19 0 -10 16 4.05 1.31 0 -11 0 0.53 0.94 0 11 0 3.84 2.45 0 11 1 198.52 16.89 0 11 -1 209.15 16.9 0 -11 1 200.5 18.88 0 -11 -1 206.85 19.05 0 -11 -2 800 37.63 0 -11 2 761.36 37.78 0 11 -2 777.39 32.75 0 11 2 818.59 35.58 0 11 3 6.17 2.79 0 11 -3 1.48 1.16 0 11 3 4.35 2.63 0 -11 -3 6.86 3.58 0 11 -3 5.75 3.02 0 -11 3 0.71 2.77 0 -11 -4 576.54 31.63 0 11 -4 588.48 27.84 0 -11 4 606.39 35.13 0 11 4 619.25 32.81 0 11 -4 588.18 31.39 0 11 4 611 30.7 0 11 5 117.22 14.66 0 -11 5 92.68 11.62 0 -11 5 100.21 14.57 0 -11 -5 107.56 13.74 0 11 -5 115.11 14.15 0 11 5 115.39 13.68 0 11 -5 103.07 11.64 0 -11 -6 53.43 7.32 0 -11 -6 63.38 11.93 0 -11 6 52.85 7.04 0 -11 7 14.5 3.74 0 -11 -7 11.29 3.81 0 -11 7 9.67 3.22 0 -11 -8 331.8 19.1 0 -11 8 359.06 18.75 0 -11 -9 2 1.39 0 -11 9 0.64 1.12 0 -11 9 1.03 1.51 0 -11 10 148.19 11.93 0 -11 10 157.84 10.9 0 -11 11 10.8 3.41 0 -11 11 11.54 2.92 0 -11 12 131.28 10.93 0 11 -12 146.65 9.48 0 -11 13 1.06 1.05 0 11 -13 1.42 0.8 0 11 -14 28.38 3.63 0 -11 14 35.08 4.96 0 11 -15 0.57 0.45 0 11 15 1.96 0.97 0 -11 15 1.22 0.76 0 12 0 14.84 4.93 0 -12 0 11.23 5.36 0 -12 -1 596.71 33.91 0 -12 1 634.71 35.46 0 12 -1 712.22 33.04 0 12 1 713.59 34.38 0 -12 -2 13.98 5.11 0 12 -2 13.58 4.62 0 12 2 7.01 2.64 0 -12 2 9.02 4.08 0 12 3 28.39 6.65 0 -12 -3 33.57 7.95 0 12 -3 23.68 5.77 0 -12 4 8.58 2.44 0 -12 4 6.41 2.49 0 -12 -4 9.47 3.15 0 -12 -5 608.84 25.09 0 -12 5 644.74 23.5 0 -12 5 647.7 24.38 0 -12 6 1.87 1.67 0 -12 -6 2.98 1.9 0 -12 6 1.18 0.95 0 -12 7 224.66 14.55 0 -12 7 233.2 13.77 0 -12 -7 218.24 15.31 0 -12 8 3 1.05 0 -12 8 6.71 2.61 0 -12 -8 4.52 2.53 0 -12 9 163.86 11.12 0 -12 9 144.5 11.65 0 -12 -9 131.62 11.95 0 -12 10 24.83 4.22 0 -12 10 20.8 4.39 0 -12 11 116.92 10.06 0 -12 11 116.75 8.51 0 -12 12 1.56 0.92 0 -12 12 2.52 1.15 0 -12 13 34.02 4.82 0 -12 14 2.52 1.11 0 12 15 22.76 2.87 0 -12 15 21.43 2.9 0 -13 0 0.17 1.11 0 -13 -1 52.06 6.99 0 -13 1 47.93 6.51 0 -13 -2 560.63 23.49 0 -13 2 595.32 22.93 0 -13 3 13.02 3.55 0 -13 -3 12.84 3.71 0 -13 4 324.58 16.9 0 -13 4 343.31 17.11 0 -13 -4 336.52 18.39 0 -13 -5 37.06 6.21 0 -13 5 40.83 6 0 -13 5 35.61 5.52 0 -13 -6 44.14 6.71 0 -13 6 40.45 5.77 0 -13 6 37.8 5.89 0 -13 7 1.71 1.74 0 -13 7 1.25 1.12 0 -13 -7 0.32 0.99 0 -13 7 1.28 1.94 0 -13 8 278.58 14.3 0 -13 8 262.15 15.38 0 -13 -9 0.97 1.36 0 -13 9 3.16 1.88 0 -13 9 0.99 0.54 0 -13 10 92.03 8.69 0 -13 10 94.89 7.79 0 -13 11 0.49 1.06 0 -13 11 1.23 1.45 0 -13 12 54.02 6.01 0 -13 12 47.61 4.54 0 -13 13 2.16 1.21 0 -13 14 59.52 4.92 0 13 14 65.57 5.2 0 -14 0 2.98 1.71 0 -14 1 456.37 17.42 0 -14 1 454.71 20.47 0 -14 -1 428.92 20.3 0 -14 2 147.08 11.31 0 -14 -2 143.27 11.68 0 -14 2 154.32 10.22 0 -14 -3 21.61 4.71 0 -14 3 23 4.07 0 -14 3 24.59 4.61 0 -14 -4 89.09 9.46 0 -14 4 75.32 8.01 0 -14 4 90.7 7.94 0 -14 5 253.77 14.91 0 -14 5 283.38 14.31 0 -14 -5 255.07 16 0 -14 5 270.09 14.84 0 -14 6 10.84 3.16 0 -14 6 11.76 2.93 0 -14 6 10.02 2.93 0 -14 -6 13.38 3.69 0 -14 -7 219.65 14.78 0 -14 7 233.64 13.08 0 -14 7 246.6 13.26 0 -14 7 237.31 14.1 0 -14 8 29.23 4.51 0 -14 8 27.12 4.66 0 -14 -8 24.74 4.96 0 -14 9 11.25 3.02 0 -14 -9 19.62 4.1 0 -14 9 17.63 3.44 0 -14 10 3.6 1.67 0 -14 10 5.29 1.78 0 -14 11 67.52 6.45 0 -14 11 60.51 5.29 0 -14 12 1.38 0.99 0 -14 12 1.29 0.8 0 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24.43 3.51 0 -16 9 6.32 1.74 0 -16 10 1.98 0.88 0 -16 11 1.6 0.69 0 16 11 1.66 0.89 0 -17 0 0.18 0.99 0 -17 -1 2.93 1.97 0 -17 1 2.75 2.21 0 -17 2 32.87 3.94 0 -17 -2 25.46 4.69 0 -17 2 28.07 4.4 0 -17 -3 194.25 12.1 0 -17 3 204.37 11.54 0 -17 3 195.42 9.87 0 -17 -4 155.86 10.69 0 -17 4 159.37 9.89 0 -17 4 161.08 8.98 0 -17 5 3.52 1.47 0 -17 -5 2.29 1.24 0 -17 5 2.6 1.11 0 -17 6 18.19 2.89 0 -17 -6 21.17 3.73 0 -17 6 21.36 3.22 0 -17 7 0.53 0.31 0 -17 -7 1.68 1.05 0 -17 8 27.88 3.33 0 -17 9 24.23 2.84 0 -18 0 23.08 3.8 0 -18 1 29.47 4.13 0 -18 -1 37.43 4.79 0 -18 2 36.71 4.56 0 -18 2 36.13 3.66 0 -18 -2 37.68 4.84 0 -18 -3 1.51 1.22 0 -18 3 0.67 0.63 0 -18 3 1.73 0.89 0 -18 -4 13.42 2.77 0 -18 4 12.93 2.26 0 -18 4 12.89 2.46 0 -18 5 45.48 4.33 0 -18 -5 47.15 5.05 0 -18 5 38.76 3.8 0 -18 6 94.12 5.82 0 -18 -6 89.52 6.71 0 -18 7 51.23 4.05 0 -18 8 11.65 1.78 0 -19 0 -0.1 0.44 0 -19 -1 1.01 0.86 0 -19 1 1.03 1.1 0 -19 -2 61.71 5.29 0 -19 2 70.34 5.35 0 -19 -3 70.81 5.6 0 -19 3 69.76 5.04 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4 -2 -15 0.53 0.6 4 -2 -14 59.39 5.48 4 2 -14 68.27 8.05 4 2 -14 80.77 9.37 4 -2 -14 82.09 9.15 4 -2 -13 8.46 2.25 4 2 -13 8.07 2.75 4 2 -13 13.25 4.54 4 -2 -13 13.27 4.33 4 2 -13 8.08 2.05 4 -2 -12 12.63 3.2 4 2 -12 19.36 5.92 4 2 -12 16.86 5.45 4 -2 -12 23.57 6.54 4 2 -12 15.89 3.43 4 -2 -11 6.36 2.55 4 -2 -11 5.33 2.05 4 2 -11 0.69 2.02 4 2 -11 2.65 2.79 4 -2 -11 9.66 5.07 4 2 -11 5.64 2.13 4 -2 -10 4.26 1.89 4 -2 -10 4.05 2.06 4 2 -10 1.88 3.25 4 2 -10 1 1.59 4 -2 -10 10.27 5.55 4 2 -10 4.04 2.37 4 -2 -9 71.24 8.12 4 -2 -9 63.25 8 4 2 -9 61.84 12.84 4 2 -9 61 8.28 4 2 -9 64.93 11.14 4 -2 -9 95.85 16.12 4 -2 -8 388.89 19.18 4 -2 -8 342.73 18.88 4 2 -8 321.65 27.92 4 2 -8 329.32 20.09 4 2 -8 322.03 23.76 4 -2 -8 421.18 32.66 4 -2 -7 1.99 1.88 4 -2 -7 1.81 0.99 4 2 -7 1.49 1.51 4 2 -7 1.75 0.99 4 -2 -7 0.79 0.77 4 -2 -7 2.26 1.29 4 2 -7 2.68 2.31 4 2 -6 210.38 12.7 4 -2 -6 196.38 12.98 4 -2 -6 193.2 14.19 4 2 -6 178.57 18 4 -2 -6 182.99 10.98 4 2 -6 176.02 14.41 4 2 -6 160.34 15.31 4 -2 -6 210.93 19.96 4 -2 -5 37.04 5.25 4 2 -5 27.46 4.44 4 -2 -5 29.86 4.92 4 -2 -5 29.4 5.65 4 2 -5 27.42 6.52 4 -2 -5 31.84 4.51 4 2 -5 30.17 6.46 4 -2 -5 34.08 7.69 4 2 -5 26.05 5.4 4 -2 -4 -0.39 1.47 4 2 -4 2.13 1.03 4 -2 -4 1.58 1.19 4 -2 -4 4.59 2.38 4 2 -4 4.27 2.7 4 2 -4 -0.64 1.46 4 -2 -4 2.09 1.88 4 -2 -4 -1.47 1.34 4 2 -4 -0.38 1.23 4 -2 -3 8.3 2.4 4 -2 -3 11.12 2.89 4 -2 -3 7.96 3 4 2 -3 9.96 3.54 4 2 -3 5.78 2.59 4 -2 -3 5.98 3.05 4 -2 -3 5.46 1.81 4 2 -3 9.73 2.76 4 -2 -3 8.84 3.18 4 -2 -2 235.63 13.21 4 -2 -2 234.01 15.57 4 2 -2 214.1 16.71 4 -2 -2 218.47 12.28 4 2 -2 212.81 14.09 4 -2 -2 219.74 15.98 4 2 -1 10.04 3.13 4 -2 -1 6.79 1.91 4 2 -1 10.49 3.74 4 -2 -1 8.59 2.34 4 2 -1 4.15 1.68 4 -2 -1 8.32 3 4 2 0 220.69 11.87 4 -2 0 199.63 12.2 4 -2 0 214.62 12.45 4 2 0 193.6 12.96 4 -2 0 231.63 15.77 4 2 0 210.85 15.16 4 2 1 177.33 10.42 4 -2 1 175.09 11.54 4 -2 1 187.58 11.83 4 2 1 183.05 12.65 4 -2 1 180.02 13.81 4 2 1 157.46 13.33 4 2 2 25.78 4.06 4 -2 2 22.74 4.27 4 -2 2 25.26 4.54 4 2 2 27.94 4.98 4 -2 2 21.05 4.45 4 2 2 22.81 4.99 4 2 3 45.25 5.14 4 -2 3 37.27 5.29 4 -2 3 39.72 5.85 4 2 3 44.43 6.53 4 -2 3 34.92 5.91 4 2 3 32.29 6.3 4 -2 4 231.77 13.28 4 -2 4 261.84 15.91 4 2 4 283.05 17.43 4 -2 4 215.66 15.01 4 2 4 196.2 15.61 4 -2 5 8.18 2.4 4 -2 5 12.79 4.22 4 2 5 4.85 2.35 4 -2 5 4.83 2.36 4 2 5 5.05 2.64 4 -2 6 197.31 17.39 4 2 6 186.81 17.08 4 -2 6 129.62 11.32 4 2 6 102.65 11.68 4 -2 7 72.75 8.34 4 2 7 74.5 10.02 4 -2 8 15.85 3.83 4 2 8 13.46 4.28 4 -2 9 2.77 1.72 4 2 9 2.23 1.99 4 -2 10 13.67 3.07 4 2 10 19.8 4.71 4 -2 11 0.16 0.49 4 2 11 3.3 1.88 4 2 12 68.47 6.74 4 3 -15 4.93 1.9 4 3 -15 3.83 1.46 4 -3 -15 6.54 1.9 4 3 -14 4.21 2.18 4 3 -14 3.93 1.69 4 -3 -14 4.52 1.99 4 3 -14 3 1.24 4 -3 -13 7.72 2.07 4 3 -13 12.87 4.61 4 3 -13 13.43 4.05 4 -3 -13 8.95 3.05 4 3 -13 5.5 1.91 4 -3 -12 6.33 2.02 4 3 -12 6.47 3.4 4 3 -12 4.84 2.89 4 -3 -12 9.62 3.9 4 3 -12 7.11 2.44 4 -3 -11 102.73 9.94 4 -3 -11 93.99 8.29 4 3 -11 76.45 9.09 4 3 -11 109.58 12.69 4 -3 -11 125.89 14.27 4 -3 -10 63.1 7.86 4 -3 -10 55.26 6.73 4 3 -10 57.15 8.66 4 3 -10 63.21 9.66 4 -3 -10 85.71 12.52 4 -3 -9 72.9 8.46 4 -3 -9 66.24 7.54 4 3 -9 59 9.19 4 3 -9 62.91 9.51 4 -3 -9 79.73 12.33 4 -3 -8 9.78 3.14 4 -3 -8 11.87 3.19 4 3 -8 5.85 3.79 4 3 -8 8.16 3.29 4 -3 -8 12.57 5.14 4 3 -8 12.99 4.33 4 -3 -7 33.87 5.47 4 -3 -7 30.69 5.28 4 3 -7 19.02 6.13 4 3 -7 29.74 6.19 4 -3 -7 35.02 7.65 4 3 -7 29.13 6.46 4 -3 -6 33.03 5.14 4 -3 -6 18.57 4.26 4 -3 -6 15.31 3.73 4 3 -6 12.54 4.65 4 3 -6 19.62 5.03 4 -3 -6 25.08 6.38 4 3 -6 18.31 4.83 4 -3 -5 537.12 20.93 4 -3 -5 476.46 20.68 4 -3 -5 474.47 21.21 4 3 -5 420.61 25.76 4 -3 -5 519.18 18.26 4 3 -5 471.75 25.42 4 3 -5 430.22 23.01 4 -3 -5 516.19 27.4 4 -3 -4 8.22 2.59 4 -3 -4 11.3 3.19 4 -3 -4 10.54 3.52 4 3 -4 9.34 3.16 4 3 -4 8.75 3.22 4 -3 -4 10.91 4.1 4 -3 -4 10.05 2.18 4 3 -4 11.41 3.81 4 -3 -3 129.46 10.1 4 -3 -3 115.77 9.64 4 -3 -3 124.99 11.05 4 3 -3 118.65 12.31 4 -3 -3 115.12 8.62 4 3 -3 124.21 11.73 4 -3 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3.02 4 4 -14 96.83 7.39 4 4 -14 98.51 7.81 4 -4 -14 106.61 8.07 4 4 -13 6.33 2.28 4 4 -13 4.74 1.87 4 -4 -13 4.76 2.06 4 4 -13 3.66 1.77 4 4 -12 2.93 2.43 4 4 -12 1.81 0.96 4 -4 -12 2.56 1.36 4 4 -12 4.08 2.21 4 -4 -11 32.03 5.56 4 -4 -11 28.74 4.32 4 4 -11 30.53 7.71 4 -4 -11 34.4 6.23 4 4 -11 28.83 5.63 4 4 -11 25.64 5.73 4 -4 -10 3.87 2.02 4 -4 -10 4.03 1.89 4 4 -10 0.61 1.12 4 4 -10 1.2 0.83 4 -4 -10 4.27 2.64 4 4 -10 2.25 0.69 4 -4 -9 -0.44 1.84 4 -4 -9 3.4 1.8 4 4 -9 4.73 4.68 4 4 -9 1.22 1.21 4 -4 -9 0.07 1.64 4 4 -9 1.92 1.73 4 -4 -8 220.44 15 4 -4 -8 207.44 13.05 4 4 -8 189.19 19.93 4 4 -8 170.29 18.07 4 4 -8 196.19 15 4 -4 -7 50.52 7.19 4 -4 -7 50.26 6.49 4 4 -7 43.73 8.95 4 4 -7 43.18 6.88 4 -4 -7 52.71 8.41 4 4 -7 42.5 8.78 4 -4 -6 15.28 4.06 4 -4 -6 17.09 3.78 4 4 -6 16.89 4.71 4 4 -6 17.18 4.41 4 -4 -6 19.58 5.17 4 4 -6 13.56 4.4 4 -4 -5 26.99 4.68 4 -4 -5 24.09 4.88 4 -4 -5 23.04 4.49 4 4 -5 17.11 4.89 4 4 -5 20.24 4.68 4 -4 -5 27.99 6.04 4 4 -5 21.44 5.62 4 -4 -4 39.93 5.74 4 -4 -4 34.32 5.75 4 -4 -4 36.98 5.94 4 4 -4 41.4 7.27 4 4 -4 43.35 6.83 4 -4 -4 42.53 7.17 4 4 -4 37.12 6.89 4 -4 -3 19.91 4.03 4 -4 -3 15.15 3.78 4 -4 -3 17.47 4.1 4 4 -3 24.62 5.37 4 -4 -3 28.12 4.1 4 4 -3 19.56 4.75 4 -4 -2 439.67 19.65 4 -4 -2 430.36 19.68 4 4 -2 512.88 24.5 4 -4 -2 484.76 17.91 4 4 -2 403.25 21.23 4 -4 -2 491.43 25.05 4 -4 -1 123.6 10.41 4 4 -1 159.14 13.32 4 -4 -1 136.73 9.52 4 4 -1 118.42 10.98 4 -4 -1 132.05 12.37 4 -4 0 319.75 17 4 -4 0 392.15 16.71 4 4 0 349.73 18.6 4 -4 0 359.34 20.2 4 -4 1 75.58 8.25 4 -4 1 82.48 7.86 4 4 1 64.82 7.78 4 -4 1 70.45 8.61 4 4 1 75.12 9.7 4 -4 2 0.8 1.3 4 -4 2 0.65 1.08 4 4 2 0.12 0.64 4 -4 2 0.18 1.11 4 4 2 -0.8 1.75 4 -4 3 5.2 2.16 4 -4 3 8.76 2.77 4 4 3 7.95 2.94 4 -4 3 7.27 2.46 4 4 3 6.64 2.64 4 -4 4 90.76 8.95 4 -4 4 109.09 11.05 4 4 4 126.92 11.33 4 -4 4 94.02 9.77 4 4 4 72.79 10.66 4 -4 5 151.27 11.23 4 -4 5 252.6 17.49 4 4 5 246.57 16.66 4 -4 5 165.99 12.81 4 4 5 110.32 13.63 4 -4 6 212.9 12.8 4 -4 6 218.54 14.49 4 -4 7 4.18 1.74 4 4 7 1.9 1.09 4 -4 8 8.05 2.69 4 4 8 8.46 3.51 4 -4 9 -0.02 0.63 4 4 9 -0.8 1.9 4 4 10 17.67 4.95 4 4 11 6.42 2.69 4 4 12 45.61 5.72 4 5 -15 7.89 2.03 4 5 -14 22.37 4.39 4 -5 -14 17.56 2.83 4 5 -14 14.18 2.47 4 5 -14 16.54 3.16 4 5 -13 4.66 1.58 4 -5 -13 6.74 1.98 4 5 -13 3.91 1.7 4 -5 -12 14.61 3.49 4 5 -12 15.95 4.79 4 5 -12 9.17 2.6 4 -5 -12 13.75 3.14 4 5 -12 11.74 3.59 4 -5 -11 65.33 7.73 4 5 -11 80.73 11.76 4 5 -11 48.22 8.61 4 5 -11 67.22 7.48 4 -5 -11 64.39 7.56 4 -5 -10 16.55 4.06 4 5 -10 25.67 6.82 4 5 -10 17.73 4.12 4 -5 -10 22.94 4.66 4 5 -10 10.48 4.17 4 -5 -9 63.72 8.2 4 5 -9 73.56 11.23 4 5 -9 59.84 7.61 4 -5 -9 68.86 8.35 4 -5 -8 4.52 2.03 4 -5 -8 4.83 1.92 4 5 -8 6.56 3.47 4 5 -8 6.97 2.54 4 -5 -8 4.82 2.24 4 5 -8 2.56 2.65 4 -5 -7 1.03 1.36 4 -5 -7 0.73 0.96 4 5 -7 0.89 1.55 4 5 -7 0.17 0.57 4 -5 -7 1.28 1.61 4 5 -7 0.16 2.23 4 -5 -6 3.93 2.25 4 -5 -6 0.69 0.56 4 5 -6 3.06 2.17 4 5 -6 0.65 1.62 4 -5 -6 2.28 1.61 4 5 -6 -1.68 2.53 4 -5 -5 231.12 14.34 4 -5 -5 198.99 14.69 4 -5 -5 223.67 13.94 4 5 -5 215.9 16 4 5 -5 164.91 15.9 4 5 -5 203.97 14.31 4 -5 -5 220.67 15.4 4 -5 -4 295.12 16.45 4 -5 -4 246.87 16.07 4 -5 -4 296.95 16.52 4 5 -4 275.4 17.47 4 5 -4 235.43 18.02 4 -5 -3 131.83 11.21 4 -5 -3 124.15 11.24 4 5 -3 113.75 11.79 4 -5 -2 21.8 4.68 4 -5 -2 19.07 4.28 4 -5 -2 22.59 3.65 4 5 -2 24.34 5 4 5 -2 26.96 5.46 4 -5 -1 39.15 6.18 4 -5 -1 41.56 6.41 4 -5 -1 44.78 5.41 4 5 -1 44.77 6.76 4 -5 -1 48.56 7.66 4 -5 0 3.11 1.84 4 -5 0 -1.16 1.54 4 5 0 0.54 1.22 4 -5 0 1.62 0.97 4 -5 1 67.06 8.27 4 -5 1 82.53 7.96 4 5 1 74.44 8.21 4 -5 1 74.8 9.1 4 -5 2 319.42 18.33 4 -5 2 421.18 19.02 4 5 2 432.58 19.95 4 -5 2 376.19 20.22 4 5 2 317.34 21.21 4 -5 3 139.99 11.9 4 -5 3 174.87 13.07 4 5 3 190.67 13.05 4 -5 3 165.69 13.17 4 5 3 126.39 13.95 4 -5 4 25.39 4.98 4 -5 4 30.32 5.45 4 5 4 13.97 4.9 4 -5 5 1.47 1.32 4 -5 5 1.89 1.72 4 5 5 0.5 2.1 4 -5 6 14.51 3.54 4 -5 6 15.89 3.89 4 5 6 5 3.12 4 -5 7 21.74 3.96 4 -5 7 24.06 4.63 4 5 7 12.3 5.09 4 -5 8 66.04 7.29 4 5 8 55.29 10.58 4 5 9 74.75 11.51 4 5 10 4.13 2.91 4 5 11 2.65 1.72 4 5 12 -0.77 0.8 4 6 -14 17.9 3.32 4 6 -14 10.36 2.37 4 6 -13 33.11 5.26 4 6 -13 27.92 4.79 4 -6 -12 56.25 6.7 4 6 -12 61.86 8.15 4 6 -12 48.83 7.36 4 -6 -12 56.5 5.67 4 -6 -11 5.29 2.29 4 6 -11 7.35 3.42 4 -6 -11 8.92 2.54 4 6 -11 8.18 3.97 4 -6 -10 46.91 6.91 4 6 -10 59.25 8.83 4 6 -10 48.78 6.03 4 -6 -10 51.47 6.21 4 6 -10 42.54 8.9 4 -6 -9 8.15 2.76 4 6 -9 10.56 3.84 4 6 -9 5.77 1.96 4 -6 -9 5.53 2.07 4 6 -9 4.1 3.45 4 -6 -8 45.14 7.26 4 6 -8 49.35 7.76 4 -6 -8 51.29 6.59 4 6 -8 34.26 8.3 4 -6 -7 191.39 14.88 4 6 -7 208.47 15.46 4 6 -7 173.04 17.47 4 -6 -7 206.91 13.7 4 -6 -6 130.71 12.38 4 6 -6 146.81 12.4 4 6 -6 134.91 14.5 4 -6 -6 148.68 11.75 4 -6 -5 22.85 4.53 4 -6 -5 26.65 5.66 4 6 -5 22.11 4.65 4 6 -5 29.44 6.18 4 -6 -4 54.65 7.21 4 -6 -4 48.47 7.51 4 6 -4 54.59 8.29 4 -6 -3 9.35 3.03 4 -6 -3 6.89 2.72 4 6 -3 6.12 2.55 4 -6 -2 64.8 8.18 4 -6 -2 70.66 8.94 4 6 -2 69.23 8.72 4 -6 -1 336.5 19.22 4 -6 -1 316.45 19.22 4 -6 0 50.93 7.65 4 -6 0 73.34 7.38 4 6 0 66.82 7.8 4 -6 1 24.66 5.33 4 -6 1 31.77 5.13 4 6 1 30.52 5.09 4 -6 1 27.12 5.46 4 -6 2 6.9 2.77 4 -6 2 12.52 4 4 6 2 8.85 2.68 4 -6 2 9.53 3.09 4 -6 3 9.44 3.23 4 -6 3 13.44 3.68 4 6 3 14.79 5.08 4 -6 4 34.34 6.31 4 -6 4 43.51 6.53 4 6 4 33.72 8.03 4 -6 5 109.88 10.6 4 -6 5 138.34 11.52 4 -6 6 70.68 8.01 4 -6 6 87.43 8.98 4 -6 7 19.93 3.86 4 -6 7 19.02 4.08 4 6 7 13.33 5.89 4 -6 8 3.87 1.38 4 6 8 2.76 3.73 4 6 9 15.47 5.2 4 6 10 36.16 6.82 4 6 11 65.53 7.7 4 6 12 13.19 2.75 4 7 -14 7.43 1.72 4 7 -14 6.07 1.78 -4 -7 13 35.92 4.21 4 7 -13 44.05 5.07 4 7 -13 35.92 4.99 4 -7 -12 16.57 3.39 4 7 -12 15.43 3.36 4 7 -12 19.39 4.37 4 -7 -11 1.4 1.37 4 7 -11 3.31 1.8 4 7 -11 4.89 2.85 4 -7 -10 75.87 8.69 4 7 -10 84.22 9.02 4 7 -10 73.11 10.36 4 -7 -9 82.41 9.36 4 7 -9 91.39 9.31 4 7 -9 83.65 11.4 4 -7 -8 25.46 5.86 4 7 -8 31.2 5.39 4 7 -8 25.11 6.44 4 -7 -7 148.9 13.71 4 7 -7 190.77 13.12 4 7 -7 168.61 15.52 4 -7 -6 59.27 8.87 4 7 -6 68.41 9.46 4 -7 -5 1.71 1.34 4 7 -5 6.62 2.94 4 -7 -4 179.18 13.42 4 -7 -4 151.15 14.09 4 7 -4 162.64 13.55 4 -7 -3 192 14.46 4 -7 -3 157.04 14.45 4 7 -3 199.79 14.39 4 -7 -2 28.23 5.69 4 -7 -2 25.65 5.85 4 7 -2 36.44 5.92 4 -7 -1 11.06 3.7 4 -7 -1 8.84 3.86 4 7 -1 8.67 2.83 4 -7 0 6.09 2.81 4 -7 0 7.52 3.03 4 7 0 7.61 2.28 4 -7 1 48.87 7.97 4 -7 1 84.96 8.81 4 -7 2 60.65 9.13 4 -7 3 123.14 11.38 4 7 3 127.57 14.18 4 -7 4 85.11 10.32 4 -7 4 102.27 10.14 4 7 4 99.33 13.38 4 -7 5 2.66 2.35 4 -7 5 0.9 1.26 4 7 5 -1.8 2.35 4 -7 6 0.91 1.22 4 -7 6 0.47 0.7 4 7 6 2.06 2.81 4 -7 7 48.08 6.39 4 7 7 35.01 8.52 4 -7 8 110.95 8.72 4 7 8 104.3 13.49 4 7 9 11.72 4.2 4 7 10 24.93 5.23 4 7 11 10.12 2.73 -4 -8 13 22.26 3.02 4 8 -13 24.08 2.99 4 8 -13 24.01 3.61 -4 -8 12 41.36 4.65 4 -8 -12 44.31 5.15 4 8 -12 39.36 4.45 4 8 -12 45.49 5.9 -4 -8 11 9.1 2.21 4 -8 -11 11.12 2.95 4 8 -11 12.3 2.77 4 8 -11 13.87 3.51 -4 -8 10 41.92 5.06 4 -8 -10 34.95 5.51 4 8 -10 44.86 5.57 4 8 -10 45.38 7.09 -4 -8 9 31.57 4.86 4 -8 -9 30.39 5.6 4 8 -9 32.08 4.76 4 8 -9 34.73 6.5 4 -8 -8 8.49 3.71 4 8 -8 3.25 2.16 4 -8 -7 52.47 8.17 4 8 -7 66.94 8.78 4 -8 -6 92.13 11.08 4 8 -6 110.32 10.88 4 -8 -5 61.42 9.15 4 8 -5 74.56 8.7 4 -8 -4 60.05 7.68 4 -8 -4 42.98 7.79 4 8 -4 70.74 8.15 4 -8 -3 84.39 9.58 4 -8 -3 73.04 10.3 4 8 -3 88.6 8.93 4 -8 -2 6.27 3.4 4 -8 -2 7.42 3.47 4 8 -2 10.29 3 4 -8 -1 43.46 7.37 4 -8 -1 45.91 8.26 4 8 -1 68.77 7.24 4 -8 0 71.62 9.84 4 -8 0 66.71 10.1 4 -8 1 184.81 16.56 4 -8 2 18.11 5.29 4 -8 3 38.24 7.72 4 -8 4 45.12 8.16 4 8 4 72.66 10.75 4 -8 5 38.82 7.33 4 8 5 44.68 8.71 4 -8 6 34.31 6.19 4 8 6 32.73 7.48 4 -8 7 131.5 11.05 4 8 7 134.13 14.38 4 -8 8 0 0.56 4 8 8 0.93 1.51 4 8 9 0.64 0.9 4 8 9 3.9 2.12 4 8 10 15.7 3.45 4 8 11 11.21 2.45 4 9 -13 24.81 3.08 -4 -9 12 11.27 2.24 4 -9 -12 8.85 1.96 4 9 -12 12.5 2.67 -4 -9 11 28.5 3.87 4 -9 -11 36.31 4.77 4 9 -11 32.4 4.74 -4 -9 10 63.63 6.1 4 -9 -10 60.24 6.88 4 9 -10 60.12 6.96 -4 -9 9 0.8 0.71 4 -9 -9 2.22 1.14 4 9 -9 1.3 1.32 4 -9 -8 46.69 7.19 4 9 -8 53.52 6.9 4 -9 -7 5.6 3.09 4 9 -7 5.26 2.27 4 -9 -6 37.31 7.11 4 9 -6 50.6 6.62 4 -9 -5 56.12 8.83 4 9 -5 89.49 8.56 4 -9 -4 42.33 7.76 4 9 -4 58.1 6.76 4 -9 -3 14.15 3.75 4 -9 -3 12.65 4.36 4 9 -3 18.58 3.79 4 -9 -2 109.88 11.09 4 -9 -2 91.08 11.92 4 -9 -1 3.01 2.47 4 -9 -1 2.79 1.56 4 -9 0 56.25 8.66 4 -9 0 41.75 8.52 4 -9 1 21.05 5.31 4 -9 1 16.5 5.21 4 -9 2 18.1 5.71 4 -9 3 4.85 2.83 4 -9 4 147.09 15.24 4 -9 5 8.33 3.37 4 9 5 6.29 3.52 4 -9 6 29.43 5.84 4 9 6 37.41 6.65 4 9 7 8.37 2.45 4 -9 7 14.23 3.87 4 9 7 12.98 3.68 4 9 8 12.7 2.69 4 -9 8 21.04 3.79 4 9 8 21.93 4.42 4 9 9 17.17 3.03 4 9 9 21.88 4.06 4 9 10 79.49 6.52 4 10 -12 1.63 0.88 -4 -10 11 3.19 1.25 4 -10 -11 3.11 1.14 4 10 -11 3.03 1.34 -4 -10 10 1.44 1.27 4 -10 -10 -0.33 0.57 4 10 -10 1.87 1.29 -4 -10 9 49.58 5.31 4 -10 -9 45.07 5.96 4 10 -9 56.5 5.96 4 -10 -8 35.66 5.75 4 10 -8 46.56 5.62 4 -10 -7 90.74 9.91 4 10 -7 100.26 8.35 4 -10 -6 -0.28 1.21 4 10 -6 0.62 0.65 4 -10 -5 50.11 8.03 4 10 -5 61.74 6.38 4 -10 -4 -0.36 1.51 4 10 -4 2.27 1.2 4 -10 -3 69.96 7.88 4 -10 -3 45.92 8.05 4 -10 -2 54.85 7.42 4 -10 -2 32.38 7.06 4 -10 -1 118.41 11.38 4 -10 -1 63 10.19 4 -10 0 13.42 4.13 4 -10 0 5.46 2.61 4 -10 1 73.49 9.98 4 -10 1 16.51 5.44 4 -10 2 19.76 5.61 4 -10 3 2.54 2.3 4 -10 4 10.26 3.75 4 -10 5 63.54 9.11 4 10 5 43.35 5.71 4 10 6 1.89 1.07 4 -10 6 3.68 1.52 4 10 6 5.82 1.97 4 -10 7 118.05 10.01 4 10 7 91.48 7.63 4 10 7 122.81 9.57 4 -10 8 27.03 4 4 10 8 22.96 3.45 4 10 8 26.17 3.96 4 10 9 9.79 2.18 4 11 -11 26.12 2.9 -4 -11 10 85.74 5.8 4 -11 -10 89.66 6.69 4 11 -10 76.56 5.56 -4 -11 9 15.22 2.65 4 -11 -9 12.75 2.88 4 11 -9 12.07 2.39 4 -11 -8 4.41 1.85 4 11 -8 8.64 2.09 4 -11 -7 -1 1.07 4 11 -7 0.01 0.33 4 -11 -6 7.13 2.78 4 11 -6 4.5 1.59 4 -11 -5 12.09 3.63 4 -11 -4 175.24 14.37 4 -11 -3 8.16 2.24 4 -11 -3 6.08 2.97 4 -11 -2 78.11 7.98 4 -11 -2 67.14 9.49 4 -11 -1 4.45 1.94 4 -11 -1 2.65 1.81 4 -11 0 28.06 5.3 4 -11 0 16.5 5.32 4 -11 1 32.88 6.05 4 -11 1 27.13 6.51 4 -11 2 153.45 13.59 4 -11 2 173.53 15.65 4 -11 3 7.63 3.41 4 -11 4 11.8 4.11 4 11 5 16.23 3.37 4 -11 5 17.87 4.54 4 11 6 4.48 1.51 4 -11 6 9.21 2.95 4 11 7 7.7 1.92 4 -11 7 5.95 1.92 4 -11 8 43.57 4.3 -4 -12 9 12.67 2.11 4 -12 -9 12.31 2.43 4 12 -9 11.77 1.87 4 -12 -8 16.2 3.12 4 12 -8 16.13 2.35 4 -12 -7 130.04 9.67 4 -12 -6 18.16 3.84 4 -12 -5 5.64 2.26 4 -12 -4 10.43 3.11 4 -12 -3 3.7 2.12 4 -12 -2 18.73 3.41 4 -12 -2 15.55 4.27 4 -12 -1 179.97 11.37 4 -12 -1 146.83 13.17 4 -12 0 12.77 3.18 4 -12 0 13.87 4.31 4 -12 1 39.35 5.9 4 -12 1 54.58 8.1 4 -12 2 1.06 1.41 4 -12 2 3.6 2.87 4 -12 3 7.35 2.68 4 -12 4 13.68 3.56 4 -12 5 283.03 14.88 4 12 5 218.05 10.68 4 12 6 1.78 0.97 4 -12 6 0.42 0.71 4 -12 7 16.33 2.79 4 -13 -8 0.88 0.69 4 -13 -7 17.49 3.05 4 -13 -6 25.42 3.98 4 -13 -5 1.62 1.35 4 -13 -4 134.22 10.09 4 -13 -3 7.42 2.45 4 -13 -2 3.32 1.73 4 -13 -1 32.23 4.15 4 -13 -1 33.56 5.43 4 -13 0 1.73 1.15 4 -13 0 1.63 1.52 4 -13 1 0.48 0.95 4 -13 1 3.96 2.21 4 -13 2 215.88 11.71 4 -13 2 226.19 13.17 4 -13 3 35.23 4.68 4 13 4 14.3 2.47 4 -13 4 16.77 3.14 4 13 5 6.75 1.59 4 -13 5 9.56 2.21 4 -13 6 2.96 0.98 4 -14 -7 63.77 4.83 4 -14 -6 1.48 0.86 4 -14 -5 0.92 0.6 4 -14 -4 5.9 1.8 4 -14 -3 9.28 2.64 4 -14 -2 0.02 0.83 4 -14 -1 121.06 6.68 4 -14 -1 113.64 8.41 4 -14 0 12.16 2.2 4 -14 0 13.66 2.87 4 -14 1 3.55 1.23 4 -14 1 5.99 1.95 4 -14 2 17.95 2.76 4 -14 2 17.39 2.9 4 -14 3 7.87 1.79 4 -14 4 2.06 0.95 4 -15 -4 39.39 3.87 4 -15 -3 7.73 1.78 4 -15 -2 23.98 3.19 4 -15 -1 20.14 2.9 4 -15 0 43.85 4.14 5 0 -12 18.65 3.81 5 0 -11 0.92 0.99 5 0 -11 -3.15 3.68 5 0 -10 135.74 14.19 5 0 -10 95.59 6.73 5 0 -9 4.3 3.59 5 0 -9 0.73 2.28 5 0 -9 -0.15 0.73 5 0 -8 5.07 4.15 5 0 -8 1.94 1.12 5 0 -7 3.07 2.95 5 0 -7 0.84 0.89 5 0 -6 103.46 15.23 5 0 -6 68.21 7.4 5 0 -5 0.71 1.26 5 0 -5 0.77 0.53 5 0 -4 237.6 14.67 5 0 -3 -1.29 1.79 5 0 -2 88.82 9.03 5 0 -1 0.19 0.71 5 0 -1 -0.24 1.65 5 0 0 56.99 7.25 5 0 0 45.59 7.69 5 0 1 0.87 0.82 5 0 1 -0.7 0.89 5 0 2 72.42 8.58 5 0 2 63.19 8.9 5 0 3 0.26 1.17 5 0 3 1.8 1.19 5 0 4 58.3 8.74 5 0 4 39.59 7.09 5 0 5 -0.5 1.27 5 0 6 26.53 5.62 5 0 7 0.2 1.22 5 0 8 20.73 4.48 5 0 9 -1.97 1.22 5 1 -13 78.26 7.28 5 -1 -12 2.07 1.13 5 1 -12 5.96 2.32 5 -1 -11 1.96 1.24 5 1 -11 3.17 1.46 5 1 -11 -2.56 3.43 5 -1 -11 0.74 2.27 5 1 -11 1.86 0.7 5 -1 -10 5.67 2.61 5 1 -10 3.13 2.39 5 1 -10 0.17 2.03 5 -1 -10 -1.35 4.38 5 1 -10 4.12 1.39 5 -1 -9 10.08 3.68 5 1 -9 4.71 3.93 5 1 -9 8.03 2.27 5 -1 -8 1.53 2.68 5 1 -8 0.65 2.15 5 -1 -8 0.95 0.88 5 1 -8 -0.45 1.37 5 -1 -7 178.65 17.33 5 1 -7 171.26 22.42 5 -1 -7 130.42 9.1 5 1 -7 126.36 10.93 5 -1 -6 8.84 2.72 5 -1 -6 14.31 5.18 5 1 -6 13.9 5.75 5 -1 -6 9.6 2.47 5 1 -6 7.79 2.75 5 -1 -5 39.54 5.57 5 -1 -5 47.75 9.01 5 1 -5 49.01 11.18 5 -1 -5 34.43 4.94 5 1 -5 42.66 6.61 5 1 -4 3.73 4.3 5 -1 -4 -0.4 1.18 5 1 -4 0.02 1.47 5 -1 -3 27.37 4.6 5 1 -3 39.81 6.33 5 -1 -2 11.86 2.99 5 1 -2 11.24 3.36 5 -1 -1 113.06 9.66 5 -1 -1 107.41 9.45 5 1 -1 101.62 10.14 5 -1 -1 103.12 11.92 5 1 -1 107.95 12.63 5 -1 0 25.62 4.81 5 -1 0 17.03 3.82 5 1 0 14.48 3.99 5 -1 0 16.24 4.78 5 1 0 16.46 4.75 5 -1 1 176.41 11.78 5 -1 1 174.32 12.57 5 1 1 168.57 13.25 5 -1 1 156.52 13.89 5 1 1 146.7 14.05 5 -1 2 6.27 2.6 5 -1 2 0.43 0.77 5 1 2 -0.99 0.58 5 -1 2 3.88 3.51 5 1 2 1.41 1.54 5 -1 3 38.28 5.55 5 -1 3 35.23 6.21 5 1 3 31.69 5.89 5 -1 3 24.6 5.4 5 1 3 25.16 5.86 5 1 4 28.42 6.42 5 -1 4 18.75 4.63 5 1 4 17.87 5.02 5 -1 5 39.37 6.53 5 1 5 44.99 7.83 5 -1 6 22.94 4.8 5 1 6 24.47 5.67 5 -1 7 56.77 7.33 5 1 7 69.47 9.34 5 -1 8 8.26 2.57 5 1 8 10.41 3.43 5 -1 9 3.58 1.82 5 1 9 7.72 2.83 5 2 -13 6.8 2.16 5 -2 -12 6.2 1.87 5 2 -12 8.7 3.07 5 -2 -11 4.11 1.82 5 2 -11 3.6 2.14 5 2 -11 2.98 1.33 5 -2 -10 26.23 4.65 5 2 -10 26.41 8.43 5 2 -10 22.03 3.98 5 -2 -9 3.44 1.61 5 2 -9 4.61 4.85 5 2 -9 1.16 0.46 5 -2 -8 117.68 9.84 5 -2 -8 136.23 12.38 5 2 -8 118.03 19.5 5 2 -8 107.23 10.79 5 -2 -7 3.93 1.85 5 -2 -7 4.41 2.58 5 2 -7 1.88 3.77 5 -2 -7 2.68 1.1 5 2 -7 0.97 1.27 5 -2 -6 1.95 1.56 5 -2 -6 1.57 2.04 5 2 -6 1.6 2.06 5 -2 -6 2.47 1.43 5 2 -6 1.41 1.36 5 -2 -5 29.5 4.94 5 2 -5 28.79 8.25 5 -2 -5 25.98 4.01 5 2 -5 22.66 5.34 5 -2 -4 50.91 6.29 5 2 -4 59.91 11.43 5 -2 -4 48.6 5.79 5 2 -4 46.78 7.53 5 -2 -3 47.9 5.96 5 2 -3 50.26 7.84 5 -2 -2 159.42 11.66 5 -2 -2 149.58 10.62 5 2 -2 156.98 13.49 5 -2 -1 5.73 3.05 5 -2 -1 2.16 1.46 5 2 -1 0.72 1.17 5 -2 -1 3.82 2.08 5 -2 0 6.11 2.75 5 -2 0 3.69 1.68 5 2 0 3.57 2.15 5 -2 0 1.59 0.72 5 2 0 3.45 2.7 5 -2 1 9.11 3.01 5 -2 1 7.22 2.59 5 2 1 9.7 3.29 5 -2 1 5.96 2.46 5 2 1 5.66 3.61 5 -2 2 55.83 6.67 5 -2 2 59.5 7.43 5 2 2 65.01 8.46 5 -2 2 44.88 7.24 5 2 2 49.93 8.6 5 -2 3 80.68 7.75 5 -2 3 91.18 9.93 5 2 3 105.99 11.18 5 -2 3 74.24 9.09 5 2 3 60.21 9.52 5 -2 4 109.56 8.5 5 -2 4 163.67 14.07 5 2 4 157.27 14.52 5 -2 4 88.48 9.68 5 2 4 73.38 10.77 5 -2 5 8.91 2.65 5 2 5 2.03 2.91 5 -2 6 6.53 2.65 5 2 6 9.33 4.25 5 -2 7 25.35 4.61 5 2 7 25.48 6.21 5 -2 8 4.38 2 5 2 8 3.34 2.15 5 -2 9 16.63 3.26 5 2 9 17.79 4.28 5 3 -12 16.52 4.22 5 3 -12 10 2 5 3 -11 128.59 15.48 5 3 -11 72.87 6.97 5 -3 -10 11.84 2.85 5 3 -10 12.84 5.58 5 3 -10 11.69 3.18 5 -3 -9 18.54 3.82 5 3 -9 25.24 7.83 5 3 -9 13.07 3.91 5 -3 -8 15.67 3.72 5 -3 -8 12.94 3.54 5 3 -8 14.06 6.9 5 3 -8 12.16 4.19 5 -3 -7 8.87 2.88 5 3 -7 12.61 5.15 5 3 -7 4.82 2.8 5 -3 -6 51.47 6.72 5 3 -6 65.15 11.9 5 3 -6 51.62 8.7 5 -3 -5 157.44 11.75 5 -3 -5 174.05 9.94 5 3 -5 177.56 16.42 5 -3 -4 2.06 1.24 5 3 -4 8.76 4.26 5 -3 -4 4.77 1.74 5 3 -4 6.22 2.35 5 -3 -3 6.8 2.13 5 3 -3 4.02 2.27 5 -3 -2 14.45 4 5 -3 -2 9.27 2.41 5 3 -2 7.96 2.99 5 -3 -1 52.11 6.87 5 -3 -1 46.14 5.85 5 3 -1 50.09 7.7 5 -3 0 87.4 8.92 5 -3 0 91.3 8.56 5 3 0 80.08 9.39 5 -3 0 77.19 10.03 5 -3 1 66.61 7.71 5 -3 1 63.34 7.41 5 3 1 82.13 9.52 5 -3 1 62.93 8.76 5 3 1 66.24 9.87 5 -3 2 20.19 4.13 5 -3 2 26.48 4.97 5 3 2 23.3 4.91 5 -3 2 20.13 4.96 5 3 2 18.9 5.51 5 -3 3 3.41 1.7 5 3 3 4.01 1.57 5 -3 3 3.5 1.91 5 3 3 0.32 1.51 5 -3 4 10.82 2.74 5 3 4 17.38 4.81 5 -3 4 9.11 3.37 5 3 4 11.62 4.76 5 -3 5 6.77 2.31 5 -3 5 4.52 1.78 5 -3 6 24.12 4.59 5 3 6 14.24 5.06 5 -3 7 78.04 7.71 5 3 7 68.17 10.85 5 -3 8 0.9 0.7 5 3 8 -1.1 2.27 5 3 9 20.21 4.68 5 4 -12 9.7 3.23 5 4 -12 6.83 1.84 5 4 -11 4.47 2.45 5 4 -11 3.79 1.62 5 4 -10 38.18 8.23 5 4 -10 20.99 4.62 5 -4 -9 4.5 2.35 5 4 -9 0.93 1.1 5 4 -9 -0.8 1.89 5 -4 -8 63.04 7.54 5 4 -8 35 7.45 5 -4 -7 11.83 3.23 5 4 -7 15.52 5.12 5 4 -7 6.2 2.26 5 -4 -6 91.41 9.21 5 4 -6 91.57 12.85 5 -4 -5 0.6 0.44 5 4 -5 4.53 2.61 5 4 -5 4.77 1.13 5 -4 -4 7.12 2.68 5 -4 -4 8.2 2.08 5 4 -4 8.93 2.56 5 -4 -3 52.55 7.1 5 -4 -3 41.65 6.02 5 -4 -3 48.72 5.4 5 4 -3 40.73 7.35 5 -4 -2 119.36 10.88 5 -4 -2 129 9.31 5 4 -2 117.69 11.97 5 -4 -1 23.58 4.87 5 -4 -1 21.92 4.04 5 4 -1 23.5 5.13 5 -4 0 13.69 3.47 5 -4 0 17.81 3.63 5 4 0 20.14 4.69 5 -4 1 1.34 0.57 5 -4 1 3.08 2.18 5 4 1 3.2 1.96 5 -4 2 16.22 3.86 5 -4 2 31.96 6.04 5 4 2 25.33 4.92 5 -4 2 16.47 4.36 5 4 2 14.81 5.24 5 -4 3 -0.1 0.59 5 4 3 2.21 1.3 5 -4 3 2.93 2.57 5 4 3 -2.16 1.77 5 -4 4 135.81 10.19 5 -4 4 137.42 11.6 5 -4 5 25.15 4.02 5 -4 5 29.86 5.16 5 -4 6 17.4 3.01 5 -4 6 13.84 3.4 5 -4 7 3.53 1.57 5 4 7 4.28 3.64 5 4 8 16.78 4.86 5 4 9 7.38 2.63 5 5 -11 94.56 9.35 5 5 -11 57.6 6.82 5 5 -10 3.56 1.89 5 5 -10 -0.56 1.66 5 -5 -9 3.63 1.77 5 5 -9 6.48 2.73 5 5 -9 -0.72 2.16 5 -5 -8 12.57 3.23 5 5 -8 16.58 4.43 5 -5 -7 31.31 5.52 5 5 -7 38.55 6.89 5 -5 -6 21 4.54 5 5 -6 26.33 5.37 5 5 -6 14.46 4.8 5 -5 -5 92.44 9.62 5 5 -5 95.42 11.92 5 -5 -4 19.28 4.78 5 -5 -4 16.18 3.85 5 5 -4 10.3 3.84 5 -5 -3 10.32 3.46 5 -5 -3 8.46 2.67 5 5 -3 7.29 2.99 5 -5 -2 6.37 2.7 5 -5 -2 2.94 1.3 5 5 -2 3.87 1.66 5 -5 -1 14.56 4 5 -5 -1 12.51 2.99 5 5 -1 12.84 3.44 5 -5 0 3.79 2.38 5 -5 0 5.14 2.19 5 5 0 6.82 2.63 5 -5 1 113.12 9.93 5 5 1 131.96 10.95 5 -5 2 205.37 14.01 5 5 2 250.24 14.84 5 -5 3 0.96 1.2 5 5 3 0.74 1.43 5 5 3 4.95 2.82 5 -5 4 5.83 1.8 5 5 4 3.94 3.11 5 -5 5 34 4.86 5 5 5 28.4 7.49 5 -5 6 2.89 1.42 5 5 6 4.07 2.91 5 5 7 22.12 5.92 5 5 8 52.63 7.62 5 6 -11 7.85 2.09 5 6 -11 9.71 2.66 5 -6 -10 26.39 4.44 5 6 -10 30.95 4.76 5 6 -10 19.3 4.29 5 -6 -9 128.38 10.44 5 6 -9 130.3 13 5 -6 -8 12.3 3.24 5 6 -8 19.61 4.18 5 6 -8 11.28 3.34 5 -6 -7 22.83 4.69 5 6 -7 35.65 5.59 5 6 -7 20.1 5.24 5 -6 -6 11.62 3.39 5 6 -6 27.76 4.9 5 6 -6 20.26 5.1 5 -6 -5 1.92 1.92 5 6 -5 2.84 2.12 5 -6 -4 101.2 9.68 5 -6 -4 81.07 9.34 5 -6 -3 15.43 3.65 5 -6 -3 10.98 3.5 5 -6 -2 18.33 4.39 5 6 -2 25.27 4.71 5 -6 -1 26.61 5.56 5 -6 -1 43.08 5.6 5 6 -1 38.44 5.65 5 -6 0 7.65 3.05 5 6 0 8.2 2.41 5 -6 1 2.49 1.02 5 6 1 4.92 1.75 5 -6 2 37.33 6.73 5 6 2 74.31 7.18 5 -6 3 14.9 4 5 -6 4 42.04 6.24 5 6 4 58.06 9.08 5 -6 5 54.38 6.37 5 6 5 67.88 9.99 5 -6 6 1.88 0.87 5 6 6 3.26 2.14 5 6 7 7.08 2.84 5 7 -11 8.34 2 5 -7 -10 15.57 3.22 5 7 -10 21.64 3.98 5 -7 -9 1.26 1.09 5 7 -9 2.23 1.28 5 7 -9 2 1.54 5 -7 -8 -0.21 0.6 5 7 -8 0.48 0.81 5 7 -8 1.53 2.04 5 -7 -7 71.27 8.27 5 7 -7 104.28 10.19 5 -7 -6 21.3 4.75 5 7 -6 36.11 6 5 -7 -5 3.62 2.13 5 7 -5 2.13 1.21 5 -7 -4 58.51 7.04 5 7 -4 66.63 7.45 5 -7 -3 21.49 4.44 5 -7 -3 19.53 4.94 5 7 -3 29.15 4.72 5 -7 -2 2.93 1.8 5 -7 -2 3.02 1.65 5 7 -2 5.51 1.83 5 -7 -1 86.45 10.12 5 7 -1 159.83 10.48 5 -7 0 40.58 7.24 5 7 0 80.3 7.14 5 -7 1 8.92 3.08 5 7 1 22.64 3.5 5 -7 2 22.51 5.23 5 -7 3 10.28 3.33 5 -7 4 1.08 1.57 5 -7 5 28.02 4.75 5 7 5 37.47 5.99 5 -7 6 46.96 5.18 5 7 6 54.81 6.83 5 8 -10 59.22 5.33 5 -8 -9 22.18 3.73 5 8 -9 26.98 4.1 5 -8 -8 2.36 1.23 5 8 -8 0.28 0.9 5 -8 -7 12.19 3.08 5 8 -7 26.85 4.45 5 -8 -6 2.42 1.53 5 8 -6 8.15 2.53 5 -8 -5 2.63 1.35 5 8 -5 3.85 1.41 5 -8 -4 50.81 5.95 5 8 -4 57.88 6.05 5 -8 -3 71.57 7.64 5 8 -3 87.25 7.28 5 -8 -2 3.32 1.95 5 -8 -2 3 1.77 5 8 -2 6.18 1.91 5 -8 -1 23.76 4.94 5 8 -1 59.45 5.58 5 -8 0 0.3 1.7 5 -8 1 2.55 0.83 5 -8 2 12.51 3.84 5 -8 3 70.06 9.38 5 -8 4 2.41 1.89 5 -8 5 24.26 4.3 5 -8 6 2.66 1.31 5 -9 -9 4.42 1.44 5 9 -9 5.36 1.36 5 -9 -8 7.27 2.07 5 9 -8 9.13 2.04 5 -9 -7 14.67 3.18 5 9 -7 17.04 2.91 5 -9 -6 49.4 6.44 5 9 -6 77.26 6.19 5 -9 -5 3.54 1.31 5 9 -5 11.53 2.43 5 -9 -4 29.51 4.01 5 9 -4 32.57 3.93 5 -9 -3 13.21 2.86 5 -9 -3 5.69 2.56 5 9 -3 14.26 2.48 5 -9 -2 -0.11 0.81 5 -9 -2 2.13 1.58 5 -9 -1 12.89 3.37 5 -9 0 75.91 8.8 5 -9 1 4.66 1.83 5 -9 2 13.71 4.06 5 -9 3 0.85 0.55 5 -9 4 16.28 3.69 5 -9 5 28.72 4.27 5 -10 -8 15.87 2.6 5 -10 -7 16.25 2.99 5 -10 -6 33.46 4.61 5 10 -6 48.91 3.96 5 -10 -5 4.77 1.77 5 10 -5 8.73 1.63 5 -10 -4 -1.33 1.46 5 -10 -3 85.71 6.29 5 -10 -3 58.8 7.32 5 -10 -2 25.21 3.68 5 -10 -2 14.66 3.55 5 -10 -1 32.44 4.5 5 -10 0 27.06 4.45 5 -10 1 -0.51 1.45 5 -10 2 6.2 2.24 5 -10 3 80.85 7.9 5 -10 4 1.96 0.96 5 -11 -6 41.18 4.35 5 -11 -5 5.27 1.65 5 -11 -4 21.56 3.57 5 -11 -3 12.08 2.65 5 -11 -2 7.07 1.61 5 -11 -2 5.69 2.11 5 -11 -1 1.35 0.61 5 -11 0 26.32 3.54 5 -11 1 2.07 1.02 5 -11 2 65.93 5.86 5 -11 3 11.11 2.24 6 0 -6 2.03 0.84 6 0 -5 -1.7 1.57 6 0 -4 219.84 14.21 6 0 -3 -1.61 1.86 6 0 -2 4.35 2.57 6 0 -1 3.12 2.36 6 0 0 19.48 6.54 6 0 1 64.68 14.95 6 1 -6 2.25 0.62 6 -1 -5 3.99 1.28 6 1 -5 3.38 1.52 6 -1 -4 2.72 0.93 6 1 -4 1.71 0.78 6 -1 -3 -0.28 1.54 6 1 -3 1.91 1.23 6 -1 -2 6.19 2.26 6 1 -2 9.17 4.09 6 -1 -1 155.76 13.26 6 1 -1 181.14 18.12 6 -1 0 31.34 7.14 6 1 0 11.65 5.56 6 1 1 43.78 12.54 6 2 -6 11.02 3.43 6 2 -5 -0.3 0.89 6 -2 -4 26.09 3.75 6 2 -4 48.23 8.55 6 -2 -3 0.06 0.78 6 2 -3 -0.75 3.06 6 -2 -2 6.83 2.48 6 2 -2 3.37 1.8 6 -2 -1 13.24 4 6 2 -1 0.65 2.32 6 -2 0 70.92 9.55 6 2 0 15.45 5.88 6 2 1 24.31 9.56 6 3 -6 3.1 1.89 6 3 -5 43 8.17 6 3 -4 -1.61 3.03 6 -3 -3 71.77 6.24 6 3 -3 77.59 11.37 6 -3 -2 26.53 4.54 6 3 -2 3.79 1.35 6 3 -1 15.92 4.72 6 3 0 11.32 4.43 6 3 1 112.72 13.65 6 4 -6 77.58 9.99 6 4 -5 8.94 3.14 6 4 -4 1.39 0.97 6 4 -3 15.45 4.02 6 4 -2 61.82 8.33 6 4 -1 5.69 2.29 6 4 0 107.68 10.59 6 5 -4 -2.36 2.11 6 5 -3 28.12 4.6 6 5 -2 14.39 3.12