#------------------------------------------------------------------------------ #$Date: 2022-05-06 23:26:42 +0300 (Fri, 06 May 2022) $ #$Revision: 275143 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/03/59/4035900.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4035900 loop_ _publ_author_name 'Ando, Shin' 'Miyata, Ryota' 'Matsunaga, Hirofumi' 'Ishizuka, Tadao' _publ_section_title ; Influences of Phenyl Rings on NHC Ligands with Bicyclic Architectures. ; _journal_issue 1 _journal_name_full 'The Journal of organic chemistry' _journal_page_first 128 _journal_page_last 139 _journal_paper_doi 10.1021/acs.joc.8b02480 _journal_volume 84 _journal_year 2019 _chemical_formula_moiety 'C14 H16 Ag Cl N2' _chemical_formula_sum 'C14 H16 Ag Cl N2' _chemical_formula_weight 355.61 _chemical_name_systematic RM4010 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2018-11-19 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3510 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 14.0029(3) _cell_length_b 13.7401(3) _cell_length_c 14.1052(3) _cell_measurement_reflns_used 31037 _cell_measurement_temperature 98 _cell_measurement_theta_max 27.48 _cell_measurement_theta_min 2.05 _cell_volume 2713.86(10) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 98 _diffrn_detector_area_resol_mean 10.000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Rigaku R-AXIS RAPID' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71075 _diffrn_reflns_av_R_equivalents 0.0342 _diffrn_reflns_av_unetI/netI 0.0143 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 40692 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.479 _diffrn_reflns_theta_min 2.530 _diffrn_source 'sealed X-ray tube' _diffrn_source_target Mo _exptl_absorpt_coefficient_mu 1.665 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 1.000 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'ABSCOR (Rigaku, 1995)' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.741 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 1424 _exptl_crystal_recrystallization_method 'diffusion of n-hexane into a solution of CH2Cl2' _exptl_crystal_size_max 0.176 _exptl_crystal_size_mid 0.167 _exptl_crystal_size_min 0.021 _refine_diff_density_max 0.742 _refine_diff_density_min -0.796 _refine_diff_density_rms 0.102 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.276 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 165 _refine_ls_number_reflns 3113 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.276 _refine_ls_R_factor_all 0.0439 _refine_ls_R_factor_gt 0.0413 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0343P)^2^+14.6529P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1067 _refine_ls_wR_factor_ref 0.1078 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3004 _reflns_number_total 3113 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jo8b02480_si_003.cif _cod_data_source_block RM4010 _cod_database_code 4035900 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.966 _shelx_estimated_absorpt_t_min 0.758 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C3(H3), C2(H2), C8(H8), C6(H6) 2.b Secondary CH2 refined with riding coordinates: C7(H7A,H7B) 2.c Aromatic/amide H refined with riding coordinates: C13(H13), C10(H10), C12(H12), C11(H11) 2.d Idealised Me refined as rotating group: C4(H4A,H4B,H4C), C5(H5A,H5B,H5C) ; _shelx_res_file ; TITL shelx_b.res in Pbca shelx.res created by SHELXL-2018/3 at 10:18:21 on 19-Nov-2018 REM Old TITL shelx in Pcab #61 REM SHELXT solution in Pbca: R1 0.109, Rweak 0.005, Alpha 0.090 REM 3.299 for 371 systematic absences, Orientation a'=b, b'=a, c'=-c REM Formula found by SHELXT: C14 N2 Ag Cl CELL 0.71075 14.0029 13.7401 14.1052 90 90 90 ZERR 8 0.0003 0.0003 0.0003 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Ag Cl N UNIT 112 128 8 8 16 L.S. 20 PLAN 20 SIZE 0.176 0.167 0.021 TEMP -175.15 BOND LIST 6 fmap 2 acta REM REM REM WGHT 0.034300 14.652905 FVAR 0.20272 AG1 3 0.640886 0.610059 0.616158 11.00000 0.01565 0.01878 = 0.01677 -0.00082 0.00109 -0.00102 CL1 4 0.762404 0.639830 0.507248 11.00000 0.01435 0.03204 = 0.01847 -0.00035 0.00031 -0.00486 N1 5 0.441565 0.558648 0.688037 11.00000 0.01742 0.01596 = 0.01723 -0.00064 -0.00039 -0.00010 N2 5 0.543972 0.559134 0.803644 11.00000 0.01464 0.01784 = 0.01543 -0.00155 0.00133 0.00029 C1 1 0.532165 0.575237 0.711491 11.00000 0.01597 0.01295 = 0.02145 -0.00161 0.00209 -0.00005 C14 1 0.504588 0.357608 0.800264 11.00000 0.01540 0.01387 = 0.01930 0.00054 -0.00040 -0.00088 C9 1 0.438110 0.357842 0.726653 11.00000 0.01460 0.01250 = 0.02230 0.00187 -0.00105 -0.00435 C13 1 0.594686 0.317992 0.788038 11.00000 0.02251 0.01449 = 0.02709 0.00369 -0.00347 -0.00242 AFIX 43 H13 2 0.640159 0.318314 0.838019 11.00000 -1.20000 AFIX 0 C10 1 0.460006 0.318391 0.639075 11.00000 0.02767 0.01398 = 0.02056 0.00041 -0.00382 -0.00162 AFIX 43 H10 2 0.414848 0.318837 0.588814 11.00000 -1.20000 AFIX 0 C3 1 0.384361 0.523401 0.767708 11.00000 0.01411 0.01806 = 0.01802 0.00042 0.00184 0.00125 AFIX 13 H3 2 0.329392 0.567724 0.781277 11.00000 -1.20000 AFIX 0 C12 1 0.616335 0.277870 0.700520 11.00000 0.02090 0.01373 = 0.03132 0.00068 0.00153 0.00152 AFIX 43 H12 2 0.677495 0.249719 0.690636 11.00000 -1.20000 AFIX 0 C2 1 0.457823 0.523224 0.850300 11.00000 0.01590 0.01881 = 0.01866 -0.00075 0.00535 -0.00057 AFIX 13 H2 2 0.437425 0.566823 0.903333 11.00000 -1.20000 AFIX 0 C8 1 0.351750 0.414889 0.761555 11.00000 0.01310 0.01760 = 0.02915 0.00284 -0.00040 -0.00256 AFIX 13 H8 2 0.290308 0.402528 0.727486 11.00000 -1.20000 AFIX 0 C6 1 0.460366 0.414348 0.881408 11.00000 0.02136 0.01966 = 0.01752 0.00260 0.00064 -0.00147 AFIX 13 H6 2 0.487739 0.401331 0.945650 11.00000 -1.20000 AFIX 0 C11 1 0.550444 0.277986 0.626989 11.00000 0.02913 0.01548 = 0.02330 -0.00261 0.00471 -0.00328 AFIX 43 H11 2 0.567242 0.250143 0.567639 11.00000 -1.20000 AFIX 0 C7 1 0.352877 0.390132 0.869054 11.00000 0.02142 0.02599 = 0.02566 0.00248 0.00303 -0.00119 AFIX 23 H7A 2 0.310800 0.433099 0.906864 11.00000 -1.20000 H7B 2 0.338011 0.320972 0.882079 11.00000 -1.20000 AFIX 0 C4 1 0.631334 0.572565 0.856750 11.00000 0.01692 0.02897 = 0.02320 -0.00086 -0.00459 -0.00210 AFIX 137 H4A 2 0.681639 0.596130 0.814251 11.00000 -1.50000 H4B 2 0.650882 0.510379 0.884696 11.00000 -1.50000 H4C 2 0.620677 0.620289 0.907288 11.00000 -1.50000 AFIX 0 C5 1 0.399051 0.572542 0.595076 11.00000 0.01850 0.02735 = 0.01984 0.00214 -0.00481 0.00103 AFIX 137 H5A 2 0.355261 0.628143 0.597042 11.00000 -1.50000 H5B 2 0.363731 0.513827 0.577011 11.00000 -1.50000 H5C 2 0.449478 0.585031 0.548461 11.00000 -1.50000 AFIX 0 HKLF 4 REM shelx_b.res in Pbca REM wR2 = 0.1078, GooF = S = 1.276, Restrained GooF = 1.276 for all data REM R1 = 0.0413 for 3004 Fo > 4sig(Fo) and 0.0439 for all 3113 data REM 165 parameters refined using 0 restraints END WGHT 0.0000 11.1585 REM Highest difference peak 0.742, deepest hole -0.796, 1-sigma level 0.102 Q1 1 0.4244 0.6580 0.6181 11.00000 0.05 0.74 Q2 1 0.6802 0.6361 0.6089 11.00000 0.05 0.62 Q3 1 0.5623 0.6482 0.7996 11.00000 0.05 0.56 Q4 1 0.3893 0.3759 0.7409 11.00000 0.05 0.53 Q5 1 0.5636 0.5938 0.6628 11.00000 0.05 0.48 Q6 1 0.3591 0.4215 0.8207 11.00000 0.05 0.47 Q7 1 0.5542 0.5952 0.6424 11.00000 0.05 0.47 Q8 1 0.5164 0.3219 0.6128 11.00000 0.05 0.46 Q9 1 0.4999 0.3820 0.8486 11.00000 0.05 0.43 Q10 1 0.6004 0.6652 0.6184 11.00000 0.05 0.43 Q11 1 0.6559 0.6524 0.8597 11.00000 0.05 0.43 Q12 1 0.5656 0.6255 0.7009 11.00000 0.05 0.42 Q13 1 0.7301 0.5954 0.5243 11.00000 0.05 0.42 Q14 1 0.5517 0.3520 0.7978 11.00000 0.05 0.42 Q15 1 0.7107 0.6008 0.8765 11.00000 0.05 0.42 Q16 1 0.7260 0.6194 0.5546 11.00000 0.05 0.40 Q17 1 0.4123 0.4007 0.8837 11.00000 0.05 0.40 Q18 1 0.5070 0.2952 0.6316 11.00000 0.05 0.39 Q19 1 0.3736 0.4649 0.7633 11.00000 0.05 0.39 Q20 1 0.6018 0.3221 0.6461 11.00000 0.05 0.39 ; _shelx_res_checksum 33124 _shelx_hkl_file ; 0 0 -2 1637.29 32.95 0 0 2 1670.16 31.99 0 0 2 1638.41 31.44 0 0 -2 1622.17 30.32 0 0 -3 -1.03 0.96 0 0 3 1.91 0.56 0 0 3 -0.32 0.80 0 0 -3 1.35 0.72 0 0 -4 3385.21 116.76 0 0 4 3341.36 113.41 0 0 4 3294.88 110.79 0 0 -4 3292.17 109.43 0 0 -5 -2.23 1.35 0 0 5 0.40 1.27 0 0 5 1.27 1.03 0 0 -5 1.51 0.96 0 0 -6 7.96 1.11 0 0 6 7.08 1.51 0 0 6 6.92 1.35 0 0 -7 1.51 1.83 0 0 7 1.99 1.67 0 0 7 2.23 1.43 0 0 -7 2.31 1.35 0 0 -8 3588.32 148.27 0 0 8 3529.74 147.88 0 0 8 3619.60 147.24 0 0 -8 3807.51 150.34 0 0 -9 2.55 2.47 0 0 9 3.02 2.15 0 0 9 -0.64 1.91 0 0 -9 0.00 1.75 0 0 -10 1609.36 45.37 0 0 10 1609.67 47.83 0 0 10 1552.21 45.68 0 0 -10 1609.36 44.57 0 0 -11 -2.31 3.10 0 0 11 0.72 2.87 0 0 11 3.10 2.47 0 0 -11 -1.99 2.23 0 0 -12 893.46 23.08 0 0 12 931.02 26.50 0 0 12 919.80 25.31 0 0 -12 863.53 23.00 0 0 -13 5.25 4.22 0 0 13 9.31 3.82 0 0 13 2.55 3.34 0 0 -13 5.97 2.94 0 0 -14 36.21 5.25 0 0 14 37.25 4.78 0 0 14 32.95 4.38 0 0 -14 32.71 3.74 0 0 -15 13.93 5.57 0 0 15 12.26 4.62 0 0 15 4.93 4.22 0 0 -15 3.66 3.66 0 0 -16 452.70 20.30 0 0 16 457.08 18.38 0 0 16 462.81 21.57 0 0 -16 473.39 15.52 0 0 -17 8.28 6.53 0 0 17 1.11 5.33 0 0 17 4.22 5.25 0 0 -17 0.64 4.30 0 0 -18 192.68 14.56 0 0 18 204.22 12.26 0 0 18 194.67 12.57 0 0 -18 203.83 10.35 -1 0 1 0.80 0.40 1 0 1 1.03 0.24 1 0 -1 0.56 0.48 1 0 -2 3069.32 91.61 -1 0 2 3051.50 88.34 -1 0 -2 3089.38 91.61 1 0 2 3064.31 89.78 1 0 2 3204.23 91.13 -1 0 -2 3221.74 90.33 -1 0 2 3063.99 91.77 1 0 -2 2854.59 84.60 1 0 -3 0.24 1.03 -1 0 3 1.59 0.88 1 0 3 1.59 0.56 1 0 3 -0.48 0.96 -1 0 -3 1.11 0.64 -1 0 3 -2.15 1.03 1 0 -3 1.35 0.80 1 0 -4 198.49 3.26 -1 0 4 187.19 2.31 1 0 4 188.31 2.87 1 0 4 183.21 2.47 -1 0 -4 196.11 2.39 -1 0 4 181.54 2.87 1 0 -4 188.15 2.71 1 0 -5 5.33 1.35 -1 0 -5 2.55 1.35 -1 0 5 0.64 0.80 1 0 5 4.38 1.27 1 0 5 3.58 0.96 -1 0 -5 -0.24 1.19 -1 0 5 2.15 1.19 1 0 -6 1416.91 33.35 -1 0 -6 1409.59 32.95 -1 0 6 1452.73 32.95 1 0 6 1367.33 31.68 1 0 6 1388.74 30.32 -1 0 6 1387.94 30.08 -1 0 -6 1407.44 30.08 1 0 -6 1415.08 31.12 1 0 -7 2.63 1.83 -1 0 -7 -1.19 1.83 -1 0 7 -0.64 1.11 1 0 7 -2.87 1.11 1 0 7 4.22 1.35 -1 0 7 -1.27 1.51 -1 0 -7 0.80 1.27 1 0 -7 -0.08 1.43 1 0 -8 115.24 3.98 -1 0 -8 122.01 3.74 -1 0 8 121.77 2.55 1 0 8 123.68 3.50 1 0 8 122.49 2.94 -1 0 8 123.84 3.42 -1 0 -8 119.46 2.79 1 0 -8 130.37 3.18 1 0 -9 4.14 2.55 -1 0 -9 2.55 2.55 -1 0 9 5.89 1.43 1 0 9 4.22 2.31 1 0 9 2.31 1.91 -1 0 9 8.68 2.07 -1 0 -9 3.18 1.67 1 0 -9 4.14 1.91 1 0 -10 1358.73 39.87 -1 0 -10 1327.06 39.08 -1 0 10 1370.83 38.04 1 0 10 1352.60 34.46 1 0 10 1345.44 35.74 -1 0 10 1301.43 36.53 -1 0 -10 1337.08 34.30 1 0 -10 1375.45 36.21 1 0 -11 -0.56 3.26 -1 0 -11 -0.40 3.18 -1 0 11 2.47 2.87 1 0 11 2.47 2.79 1 0 11 0.24 2.39 -1 0 11 0.72 2.63 -1 0 -11 3.74 2.87 1 0 -11 3.10 2.31 1 0 -12 322.81 8.12 -1 0 -12 323.21 10.90 -1 0 12 329.58 9.79 1 0 12 327.43 9.95 1 0 12 332.92 8.91 -1 0 12 330.77 9.55 -1 0 -12 315.81 8.12 1 0 -12 331.80 8.75 1 0 -13 20.37 4.38 -1 0 -13 2.55 2.71 -1 0 13 8.12 3.74 1 0 13 8.04 3.82 1 0 13 7.80 3.18 -1 0 13 8.75 3.50 -1 0 -13 10.74 3.66 1 0 -13 2.94 3.02 1 0 -14 123.92 7.56 -1 0 -14 117.79 7.88 -1 0 14 123.28 6.61 1 0 14 118.43 4.54 1 0 14 115.72 5.97 -1 0 14 120.42 6.29 -1 0 -14 121.45 5.25 1 0 -14 124.40 5.73 1 0 -15 0.96 5.25 -1 0 -15 8.36 5.01 -1 0 15 -3.26 4.54 1 0 15 -5.17 4.46 1 0 15 7.00 5.41 -1 0 15 1.35 5.49 -1 0 -15 7.72 3.50 1 0 -15 3.10 3.66 1 0 -16 143.82 9.39 -1 0 -16 126.39 9.47 -1 0 16 112.86 8.52 1 0 16 123.84 8.04 1 0 16 136.81 9.95 -1 0 16 116.68 7.96 -1 0 -16 117.39 6.61 1 0 -16 126.31 6.69 1 0 -17 1.67 6.29 -1 0 -17 1.83 6.13 -1 0 17 -1.75 5.57 1 0 17 0.88 5.33 1 0 17 2.79 6.69 -1 0 17 6.05 5.25 -1 0 -17 1.91 4.06 1 0 -17 0.56 4.38 1 0 -18 249.19 15.44 -1 0 -18 239.80 15.20 -1 0 18 222.93 13.69 1 0 18 245.93 13.21 1 0 18 227.78 17.03 -1 0 18 219.58 13.53 -1 0 -18 224.92 11.14 1 0 -18 233.91 11.70 2 0 0 1002.10 14.33 -2 0 0 1018.41 13.61 -2 0 0 1025.73 15.44 2 0 0 987.21 14.49 -2 0 -1 1.59 0.56 2 0 -1 0.40 0.72 -2 0 -1 1.11 0.40 2 0 -1 0.16 0.48 2 0 -2 3142.55 97.97 -2 0 2 3161.81 97.50 -2 0 -2 3166.82 97.26 2 0 2 3201.76 98.05 2 0 2 3358.23 100.28 -2 0 -2 3265.75 98.61 -2 0 2 3252.38 103.62 2 0 -2 3120.90 98.69 2 0 -3 -0.24 1.03 -2 0 3 3.10 0.88 -2 0 -3 1.51 0.96 2 0 3 2.47 0.56 2 0 3 0.56 0.96 -2 0 -3 3.10 0.80 -2 0 3 2.94 1.19 2 0 -3 3.82 1.03 2 0 -4 319.15 4.93 -2 0 4 317.64 4.62 -2 0 -4 319.79 4.78 2 0 4 321.46 4.54 2 0 4 313.10 3.98 -2 0 -4 309.44 3.66 -2 0 4 324.88 4.93 2 0 -4 322.73 3.90 2 0 -5 2.87 1.35 -2 0 5 2.71 0.88 -2 0 -5 5.09 1.35 2 0 5 3.18 1.27 2 0 5 3.34 1.27 -2 0 -5 1.91 0.88 -2 0 5 3.02 0.88 2 0 -5 1.75 1.27 2 0 -6 34.38 1.91 -2 0 -6 33.51 1.91 2 0 6 35.97 1.75 2 0 6 32.95 1.83 -2 0 -6 30.64 1.35 -2 0 6 30.88 1.83 2 0 -6 30.40 1.75 2 0 -7 -0.88 1.91 -2 0 -7 3.90 1.91 -2 0 7 2.94 1.75 2 0 7 7.16 1.75 2 0 7 5.49 1.35 -2 0 -7 5.49 1.27 -2 0 7 2.55 1.19 2 0 -7 7.64 1.59 2 0 -8 709.45 15.44 -2 0 -8 677.38 15.04 -2 0 8 669.34 14.25 2 0 8 694.65 14.49 2 0 8 670.85 12.81 -2 0 8 684.62 14.56 -2 0 -8 693.77 12.50 2 0 -8 697.67 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-4 -2 3 2798.56 96.06 4 -2 -3 2909.51 97.10 -4 -2 -4 89.86 2.39 4 2 -4 90.57 1.83 4 -2 4 96.78 1.75 4 -2 4 90.49 2.47 -4 -2 -4 92.64 1.27 4 2 -4 92.72 2.55 -4 2 4 97.73 2.55 -4 -2 4 89.06 2.47 4 -2 -4 95.59 1.91 -4 2 -4 91.92 1.75 -4 2 -4 89.46 1.67 -4 -2 4 92.64 1.99 4 -2 -4 89.30 2.39 4 2 -5 951.16 20.37 -4 2 5 929.99 17.67 4 -2 5 981.64 18.31 -4 -2 -5 935.96 20.06 4 -2 5 973.92 19.90 -4 -2 -5 955.46 14.49 4 2 -5 979.81 20.45 -4 2 5 923.70 19.58 -4 -2 5 981.01 20.14 -4 2 -5 972.49 18.23 4 2 5 950.68 19.58 4 2 5 987.37 14.72 -4 2 -5 981.09 19.50 -4 -2 5 970.82 21.17 4 -2 -5 942.25 19.26 4 2 -6 53.56 2.55 -4 2 6 45.84 1.91 4 -2 6 53.24 1.91 -4 -2 -6 51.65 2.55 4 -2 6 49.50 2.31 4 2 -6 49.42 2.63 -4 2 6 43.93 2.39 -4 -2 6 47.28 2.39 -4 2 -6 49.27 2.07 4 2 6 50.78 2.39 4 2 6 49.50 1.27 -4 2 -6 51.18 2.15 -4 -2 6 50.06 2.79 4 -2 -6 44.09 2.23 4 2 -7 1948.96 57.06 -4 2 7 1947.84 56.43 -4 -2 -7 2053.38 62.32 4 -2 7 2010.16 57.30 4 -2 7 1945.78 58.82 -4 -2 -7 1973.23 47.91 -4 2 7 1931.05 59.21 4 2 -7 1928.90 58.90 4 -2 -7 2076.22 60.73 -4 -2 7 1950.79 58.58 -4 2 -7 1960.50 57.62 4 2 7 1992.41 59.45 4 2 7 1966.07 48.39 -4 2 -7 1949.99 56.99 -4 -2 7 1960.18 62.08 4 -2 -7 1995.60 58.50 4 2 -8 325.12 6.37 -4 2 8 314.93 5.41 -4 -2 -8 319.47 6.21 4 -2 8 317.32 6.77 4 -2 8 324.48 7.24 -4 -2 -8 323.84 4.93 -4 2 8 330.45 7.56 4 2 -8 324.08 6.05 4 -2 -8 348.28 7.40 -4 -2 8 331.49 7.48 -4 2 -8 321.06 7.16 4 2 8 343.90 7.72 4 2 8 329.97 5.33 -4 2 -8 321.62 6.77 -4 -2 8 322.73 8.52 4 -2 -8 318.59 6.92 4 2 -9 32.39 3.34 -4 -2 -9 28.33 2.15 -4 2 9 28.33 2.71 4 -2 9 29.05 2.71 4 -2 9 34.14 2.79 -4 -2 -9 30.32 1.83 -4 2 9 29.29 2.94 4 2 -9 36.21 2.94 4 -2 -9 26.82 1.99 -4 2 -9 33.98 2.94 -4 -2 9 28.97 3.02 4 2 9 24.91 2.94 4 2 9 34.94 2.07 -4 2 -9 32.63 3.26 -4 -2 9 32.55 2.23 4 -2 -9 25.95 2.63 4 2 -10 -1.19 3.18 -4 -2 -10 -1.35 3.10 -4 2 10 4.06 2.55 4 -2 10 5.17 2.55 4 -2 10 1.51 3.34 -4 2 10 -0.48 2.79 -4 -2 -10 1.03 1.83 4 2 -10 8.68 2.87 4 -2 -10 5.49 2.87 -4 2 -10 3.18 2.79 -4 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8.20 -5 -4 1 495.28 9.39 -5 4 -1 506.82 9.39 -5 -4 1 479.28 8.04 5 4 1 494.64 7.24 -5 4 -1 528.94 10.19 -5 -4 -2 2843.53 98.61 5 4 -2 2829.37 100.84 5 -4 2 2775.01 75.13 -5 4 2 2871.55 78.08 5 -4 2 2842.66 100.84 -5 -4 -2 2903.78 85.24 5 4 -2 2832.87 94.39 -5 4 2 2748.82 97.34 5 4 2 2775.88 94.23 -5 -4 2 2686.58 94.87 -5 4 -2 2858.41 76.64 5 -4 -2 2854.52 78.31 -5 4 -2 2810.42 97.50 -5 -4 2 2825.62 95.74 5 4 2 2861.52 83.17 5 -4 -2 2789.97 96.62 -5 -4 -3 128.93 2.47 5 4 -3 113.89 3.50 5 -4 3 121.21 1.83 5 -4 3 123.68 3.58 -5 -4 -3 118.75 1.43 5 4 -3 118.27 3.10 -5 4 3 124.32 3.42 5 4 3 118.67 3.50 -5 -4 3 114.37 3.50 -5 4 -3 122.25 1.83 -5 4 -3 122.88 2.55 -5 -4 3 127.58 3.26 5 4 3 124.40 1.51 5 -4 -3 123.36 2.39 -5 -4 -4 40.83 2.39 5 4 -4 34.30 2.47 5 -4 4 36.77 1.51 -5 4 4 40.91 1.59 -5 -4 -4 35.97 2.55 5 -4 4 39.79 2.63 5 4 -4 42.58 2.31 -5 4 4 37.09 2.39 -5 -4 4 40.75 2.39 -5 4 -4 36.93 1.59 5 -4 -4 34.46 1.67 -5 4 -4 35.34 2.39 -5 -4 4 35.26 2.55 5 -4 -4 37.57 1.59 -5 -4 -5 8.83 1.99 5 4 -5 1.11 2.23 5 -4 5 1.83 1.19 -5 4 5 3.34 1.59 -5 -4 -5 5.97 2.23 5 -4 5 9.31 2.23 5 4 -5 1.99 1.35 -5 4 5 4.22 2.07 -5 -4 5 4.78 2.15 -5 4 -5 3.34 1.19 5 -4 -5 3.58 1.27 -5 4 -5 3.42 2.07 -5 -4 5 3.34 2.39 5 -4 -5 4.54 1.91 -5 -4 -6 1990.27 61.04 5 4 -6 2016.13 65.34 5 -4 6 1966.63 55.63 -5 4 6 2008.17 56.51 -5 -4 -6 1991.14 64.63 5 -4 6 1992.33 64.39 5 4 -6 1936.62 61.60 -5 4 6 2130.82 65.10 -5 -4 6 1965.83 62.08 -5 4 -6 2033.40 56.75 5 -4 -6 2067.70 58.74 -5 4 -6 1996.08 62.00 -5 -4 6 2003.72 65.50 5 -4 -6 2012.47 61.04 -5 -4 -7 14.17 2.55 5 4 -7 13.77 2.87 5 -4 7 10.98 1.83 -5 4 7 15.92 2.39 -5 -4 -7 14.56 2.79 5 -4 7 9.87 2.63 5 4 -7 11.06 2.71 -5 4 7 8.36 2.47 -5 -4 7 15.28 2.71 -5 4 -7 12.97 1.91 5 -4 -7 11.38 2.07 -5 4 -7 7.72 2.47 -5 -4 7 9.23 2.94 5 -4 -7 16.08 2.23 -5 -4 -8 250.15 6.69 5 4 -8 232.00 7.40 5 -4 8 238.69 5.49 -5 4 8 244.89 5.49 -5 -4 -8 245.13 7.48 5 -4 8 244.73 6.84 5 4 -8 249.99 7.32 -5 4 8 238.84 6.53 -5 -4 8 236.22 6.84 -5 4 -8 241.79 5.65 5 -4 -8 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32.55 -6 -4 -5 53.24 2.87 6 4 -5 52.93 3.18 -6 4 5 54.60 1.67 6 -4 5 53.56 1.67 -6 -4 -5 53.32 3.26 6 -4 5 53.32 3.26 -6 -4 -5 53.96 1.03 -6 -4 -5 55.79 0.96 6 4 -5 58.74 2.94 -6 4 5 58.26 3.02 -6 -4 5 46.80 3.02 6 -4 -5 50.70 2.23 -6 4 -5 54.28 2.15 -6 4 -5 48.79 2.07 -6 -4 5 51.89 3.18 6 -4 -5 53.48 2.87 -6 -4 -6 215.84 5.49 6 4 -6 219.98 6.29 -6 4 6 215.05 3.98 6 -4 6 210.91 3.90 -6 -4 -6 219.82 6.29 6 -4 6 221.97 6.05 6 4 -6 215.76 5.89 -6 4 6 214.41 5.89 -6 -4 6 211.63 5.73 6 -4 -6 218.39 5.09 -6 4 -6 219.58 4.14 -6 4 -6 209.24 4.22 -6 -4 6 218.39 6.53 6 -4 -6 209.56 5.57 -6 -4 -7 23.08 2.79 6 4 -7 17.75 3.26 -6 4 7 14.25 1.91 6 -4 7 24.43 1.91 -6 -4 -7 19.90 3.02 6 -4 7 21.09 3.02 6 4 -7 20.93 2.87 -6 4 7 21.01 2.94 -6 -4 7 16.55 2.87 6 -4 -7 21.57 2.23 -6 4 -7 16.63 2.07 -6 4 -7 17.91 2.79 -6 -4 7 25.47 3.34 6 -4 -7 15.12 2.63 -6 -4 -8 82.45 2.79 6 4 -8 83.09 4.46 -6 4 8 84.12 3.90 -6 -4 -8 74.34 4.54 6 -4 8 74.73 3.02 6 -4 8 83.49 4.30 6 4 -8 78.08 3.02 -6 4 8 82.77 4.30 6 -4 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774.31 21.97 -9 -6 -1 740.17 19.98 -9 6 1 768.82 20.61 -9 -6 -1 751.71 17.83 9 6 -1 771.37 17.35 -9 6 1 734.36 21.81 9 6 1 746.70 21.41 -9 -6 1 751.39 20.37 -9 6 -1 749.48 20.14 -9 -6 1 738.58 17.91 9 6 1 763.65 15.52 -9 6 -1 733.01 21.57 9 6 -2 444.18 13.21 -9 -6 -2 447.84 12.57 -9 6 2 492.33 10.11 -9 -6 -2 471.72 10.03 9 6 -2 443.63 10.43 -9 6 2 448.56 13.53 9 6 2 446.49 12.89 -9 -6 2 457.87 10.03 -9 6 -2 458.19 12.57 -9 -6 2 461.37 11.38 9 6 2 479.84 8.52 -9 6 -2 462.73 13.61 9 6 -3 94.23 5.09 -9 -6 -3 82.45 4.54 -9 6 3 84.92 4.62 -9 -6 -3 86.75 3.02 9 6 -3 91.05 3.98 -9 6 3 85.16 3.50 9 6 3 88.10 4.93 -9 -6 3 82.69 4.70 -9 6 -3 90.41 4.78 -9 -6 3 91.13 4.46 9 6 3 88.58 2.31 -9 6 -3 86.27 5.25 -9 -6 -4 14.56 3.42 9 6 -4 17.99 2.47 -9 6 4 15.68 1.19 -9 -6 -4 16.87 1.75 9 6 -4 17.75 3.10 -9 6 4 21.17 3.82 -9 6 -4 16.08 0.96 9 -6 -4 16.71 1.59 -9 6 -4 14.56 1.03 -9 -6 4 16.79 3.42 -9 6 -4 20.77 3.50 -9 -6 4 17.59 3.58 -9 6 -4 17.11 2.63 9 6 4 15.60 1.75 9 -6 -4 17.03 3.50 -9 -6 -5 223.40 7.88 9 6 -5 224.92 6.13 -9 6 5 227.15 4.22 -9 -6 -5 220.70 8.44 -9 -6 -5 222.77 3.82 -9 -6 -5 235.26 4.06 9 6 -5 235.42 7.40 -9 6 5 218.79 8.60 -9 6 -5 214.49 3.66 9 -6 -5 233.67 4.54 -9 -6 5 226.35 5.73 -9 6 -5 229.21 3.98 -9 6 -5 222.85 7.96 -9 -6 5 233.67 8.28 9 -6 -5 226.19 7.88 -9 6 -5 209.87 8.68 -9 -6 -6 342.47 10.66 9 6 -6 323.13 11.30 -9 -6 -6 337.22 11.62 9 -6 6 328.14 6.61 9 -6 6 352.26 11.54 9 6 -6 323.13 10.27 -9 6 6 349.95 11.46 9 -6 -6 345.57 7.64 -9 -6 6 329.34 10.66 -9 6 -6 337.69 6.77 -9 6 -6 321.22 10.74 -9 -6 6 341.43 11.46 9 -6 -6 336.50 10.74 -9 -6 -7 157.82 6.92 9 6 -7 141.35 7.48 -9 6 7 138.24 4.62 -9 -6 -7 139.36 7.08 9 -6 7 145.73 3.66 9 -6 7 156.71 7.32 9 6 -7 150.50 6.77 -9 6 7 150.74 7.08 9 -6 -7 155.28 5.33 -9 -6 7 153.05 6.61 -9 6 -7 148.99 3.82 -9 6 -7 138.01 6.77 -9 -6 7 147.32 7.48 9 -6 -7 138.32 4.62 -9 -6 -8 129.09 4.46 9 6 -8 112.06 7.24 -9 6 8 117.79 3.90 -9 -6 -8 126.47 7.00 9 -6 8 114.61 3.90 9 -6 8 116.44 7.00 9 6 -8 127.34 6.37 -9 6 8 118.75 6.84 9 -6 -8 113.81 4.46 -9 -6 8 118.67 4.46 -9 6 -8 116.68 5.01 -9 6 -8 125.75 6.37 -9 -6 8 125.43 7.08 9 -6 -8 119.70 6.29 -9 -6 -9 713.59 22.76 9 6 -9 676.26 19.66 -9 -6 -9 678.25 24.19 -9 6 9 690.67 19.82 9 -6 9 677.14 19.58 9 -6 9 709.45 24.91 -9 6 9 674.59 23.48 9 6 -9 705.07 22.76 9 -6 -9 694.81 21.81 -9 6 -9 713.67 17.91 -9 -6 9 668.30 22.36 -9 6 -9 697.67 22.92 -9 -6 9 702.37 25.79 9 -6 -9 717.57 22.52 -9 -6 -10 184.25 8.20 9 6 -10 151.77 6.61 -9 -6 -10 158.94 9.23 -9 6 10 175.17 7.40 9 -6 10 160.69 5.89 9 -6 10 156.23 8.60 -9 6 10 164.43 8.75 9 6 -10 156.95 8.60 9 -6 -10 162.68 8.20 -9 6 -10 163.39 7.72 -9 -6 10 145.33 8.04 -9 6 -10 160.05 7.80 -9 -6 10 145.89 9.87 9 -6 -10 156.23 7.80 -9 -6 -11 12.02 3.10 9 6 -11 8.36 5.57 -9 -6 -11 19.74 5.41 -9 6 11 9.31 3.50 9 -6 11 6.61 3.50 9 -6 11 15.84 5.01 -9 6 11 14.80 5.17 9 6 -11 -2.15 5.01 9 -6 -11 6.37 4.06 -9 6 -11 7.16 4.85 -9 -6 11 4.46 3.26 -9 6 -11 5.65 4.70 -9 -6 11 19.74 5.97 9 -6 -11 23.16 4.54 -9 -6 -12 46.96 6.45 9 6 -12 44.97 4.78 -9 -6 -12 46.48 7.00 -9 6 12 45.37 4.85 9 -6 12 42.50 6.21 9 -6 12 57.22 6.84 -9 6 12 51.81 6.69 9 6 -12 46.00 6.37 9 -6 -12 47.51 5.73 -9 6 -12 55.15 5.33 -9 -6 12 55.00 6.29 -9 6 -12 62.32 6.05 -9 -6 12 48.47 7.48 9 -6 -12 63.11 5.81 -9 -6 -13 258.26 13.37 9 6 -13 276.41 15.68 -9 -6 -13 272.03 15.04 -9 6 13 272.99 10.82 9 -6 13 262.96 11.30 9 -6 13 292.09 14.56 -9 6 13 273.23 13.93 9 6 -13 282.62 13.93 9 -6 -13 264.79 12.34 -9 6 -13 272.59 11.54 -9 -6 13 270.92 9.39 -9 6 -13 270.44 16.24 -9 -6 13 275.93 16.08 9 -6 -13 269.57 12.42 -9 -6 -14 123.28 8.60 9 6 -14 90.41 10.51 -9 -6 -14 104.34 9.87 -9 6 14 101.87 7.48 9 -6 14 103.46 7.56 9 -6 14 106.17 9.79 -9 6 14 97.02 9.55 9 6 -14 91.92 9.39 9 -6 -14 97.10 8.75 -9 6 -14 108.56 10.19 -9 -6 14 101.87 9.07 -9 -6 14 109.12 10.82 -9 6 -14 109.83 10.90 9 -6 -14 92.72 8.36 10 6 0 369.85 11.94 -10 -6 0 370.64 10.82 -10 6 0 385.76 11.54 -10 -6 0 380.67 10.66 10 6 0 375.34 9.95 -10 6 0 381.86 12.73 10 6 -1 130.76 5.89 -10 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71.07 5.41 -10 6 5 66.93 2.23 -10 -6 -5 64.39 5.41 -10 -6 -5 62.48 2.39 -10 -6 -5 65.90 2.47 10 6 -5 60.01 4.46 -10 6 -5 64.55 1.99 10 -6 -5 65.58 2.63 -10 -6 5 67.97 4.70 -10 6 -5 62.95 1.99 -10 6 -5 58.90 5.01 -10 -6 5 66.22 5.25 -10 6 -5 64.94 5.49 10 -6 -5 60.01 5.01 -10 -6 -6 66.38 4.85 10 6 -6 62.32 5.57 -10 6 6 60.89 2.79 -10 -6 -6 63.27 5.57 -10 -6 -6 59.45 1.75 10 6 -6 60.41 3.18 -10 6 6 57.78 5.73 10 -6 -6 59.53 3.26 -10 -6 6 68.29 3.34 -10 6 -6 62.40 2.79 -10 6 -6 63.19 5.09 -10 -6 6 68.92 5.33 10 -6 -6 65.10 3.34 -10 6 -6 56.27 5.65 -10 -6 -7 410.91 13.37 10 6 -7 382.50 14.72 -10 6 7 389.66 9.39 -10 -6 -7 395.71 10.74 10 6 -7 410.20 13.37 -10 6 7 402.48 14.72 -10 6 -7 406.70 8.99 10 -6 -7 406.54 10.90 -10 -6 7 398.18 13.29 -10 6 -7 429.94 9.63 -10 6 -7 411.15 13.77 -10 -6 7 404.23 15.12 10 -6 -7 398.50 10.51 -10 6 -7 381.55 14.41 -10 -6 -8 62.40 5.41 10 6 -8 65.26 6.21 -10 6 8 65.58 4.06 -10 -6 -8 66.46 6.13 10 -6 8 61.12 3.90 10 -6 8 69.08 5.97 -10 6 8 59.05 6.21 10 6 -8 59.53 5.49 10 -6 -8 61.44 3.66 -10 -6 8 61.84 5.49 -10 6 -8 57.78 3.26 -10 6 -8 71.55 5.49 -10 -6 8 67.65 4.30 10 -6 -8 64.55 5.65 -10 -6 -9 74.89 6.13 10 6 -9 78.16 6.84 -10 -6 -9 79.03 6.84 -10 6 9 74.57 3.90 10 -6 9 71.63 3.82 10 -6 9 72.98 6.45 -10 6 9 76.40 6.77 10 6 -9 77.12 6.37 10 -6 -9 78.00 5.81 -10 6 -9 66.77 5.09 -10 -6 9 77.60 4.14 -10 6 -9 72.98 5.97 -10 -6 9 86.11 7.24 10 -6 -9 82.77 5.89 -10 -6 -10 32.79 5.09 10 6 -10 17.43 6.13 -10 -6 -10 24.75 5.81 -10 6 10 23.16 3.50 10 -6 10 24.83 3.58 10 -6 10 23.56 5.49 -10 6 10 35.26 5.73 10 6 -10 30.64 5.33 10 -6 -10 30.32 4.38 -10 6 -10 25.55 3.82 -10 -6 10 27.30 5.09 -10 6 -10 29.85 5.09 -10 -6 10 33.35 6.45 10 -6 -10 24.12 4.93 -10 -6 -11 288.03 12.57 10 6 -11 251.82 14.41 -10 -6 -11 292.49 13.77 -10 6 11 287.39 11.46 10 -6 11 271.40 9.79 10 -6 11 294.80 13.13 -10 6 11 277.60 14.01 10 6 -11 274.42 12.97 10 -6 -11 283.97 11.06 -10 6 -11 285.48 12.65 -10 -6 11 265.27 12.42 -10 6 -11 297.42 12.26 -10 -6 11 267.66 10.43 10 -6 -11 288.35 12.10 -10 -6 -12 202.55 11.14 10 6 -12 209.48 12.81 -10 -6 -12 200.09 11.94 -10 6 12 216.56 8.60 10 -6 12 191.81 8.91 10 -6 12 205.58 11.94 -10 6 12 192.44 11.94 10 6 -12 202.15 11.38 10 -6 -12 210.19 12.97 -10 6 -12 209.24 9.47 -10 -6 12 209.00 11.30 -10 6 -12 213.38 10.66 -10 -6 12 205.42 13.13 10 -6 -12 200.01 10.51 -10 -6 -13 5.01 5.57 10 6 -13 12.50 6.69 -10 -6 -13 5.97 6.29 -10 6 13 2.87 4.38 10 -6 13 2.47 4.62 10 -6 13 -5.97 6.13 -10 6 13 2.31 6.37 10 6 -13 11.30 5.89 10 -6 -13 1.99 5.17 -10 6 -13 9.07 6.29 -10 -6 13 9.71 5.65 -10 6 -13 10.82 5.33 -10 -6 13 7.88 7.16 10 -6 -13 6.77 5.33 -10 -6 -14 67.81 8.99 10 -6 14 64.94 8.60 10 -6 -14 54.68 9.63 11 6 0 11.38 3.82 -11 -6 0 0.64 3.42 -11 6 0 0.72 3.58 -11 -6 0 -0.72 2.71 11 6 0 6.45 2.55 -11 6 0 -7.40 4.14 11 6 -1 140.47 6.69 -11 -6 -1 130.13 6.05 -11 6 1 116.76 6.21 -11 -6 -1 123.84 4.46 11 6 -1 119.94 4.78 -11 6 1 115.96 6.92 11 6 1 114.13 6.29 -11 -6 1 123.68 5.89 -11 6 -1 114.45 6.13 -11 -6 1 125.99 5.17 11 6 1 123.60 5.25 -11 6 -1 121.85 4.78 11 6 -2 47.28 4.78 -11 -6 -2 46.88 4.14 -11 6 2 39.56 4.78 -11 -6 -2 39.40 2.87 11 6 -2 44.57 3.66 -11 6 2 30.32 5.33 11 6 2 41.94 4.70 -11 -6 2 46.16 4.38 -11 6 -2 42.66 4.54 -11 -6 2 38.44 3.98 -11 6 -2 43.69 5.17 11 6 2 45.60 2.79 11 6 -3 5.41 3.90 -11 -6 -3 6.92 3.66 -11 6 3 3.90 3.74 -11 -6 -3 2.15 2.07 11 6 -3 -1.67 3.02 -11 6 3 1.51 2.79 11 6 3 1.91 3.82 -11 -6 3 5.25 3.58 -11 6 -3 9.31 3.74 -11 -6 3 0.64 3.42 -11 6 -3 -0.40 4.06 11 6 3 2.15 2.55 11 6 -4 13.13 4.22 -11 -6 -4 4.30 3.82 -11 -6 -4 4.54 4.14 -11 -6 -4 6.21 2.31 -11 -6 -4 8.75 2.55 11 6 -4 1.19 3.42 -11 6 4 4.78 4.54 11 -6 -4 5.65 0.72 -11 -6 4 9.47 3.74 -11 6 -4 3.58 2.63 -11 -6 4 8.99 3.82 -11 6 -4 15.28 2.87 -11 -6 -5 10.11 3.74 11 6 -5 7.48 4.22 -11 6 5 1.75 1.43 -11 -6 -5 8.91 4.22 -11 -6 -5 0.72 1.99 -11 -6 -5 2.63 2.15 11 6 -5 2.79 3.58 -11 6 5 -1.91 4.46 11 -6 -5 2.79 1.67 -11 -6 5 4.30 3.82 -11 6 -5 1.35 1.35 -11 6 -5 11.06 3.98 -11 -6 5 -0.72 3.90 -11 6 -5 3.90 4.38 11 -6 -5 10.90 3.98 -11 -6 -6 70.12 3.58 11 6 -6 66.85 6.13 -11 6 6 63.27 2.79 -11 -6 -6 73.46 5.89 -11 -6 -6 64.55 2.39 -11 -6 -6 64.86 2.47 -11 6 6 77.44 6.45 11 6 -6 64.63 5.17 -11 6 -6 62.32 2.71 11 -6 -6 64.23 3.66 -11 -6 6 77.04 5.57 -11 6 -6 63.83 2.79 -11 6 -6 72.50 5.57 -11 -6 6 69.24 6.05 -11 6 -6 74.34 6.13 11 -6 -6 62.95 3.82 -11 -6 -7 29.61 4.78 11 6 -7 35.26 3.66 -11 6 7 28.57 3.02 -11 -6 -7 37.25 5.25 -11 6 7 35.66 5.73 11 6 -7 27.86 4.62 -11 6 -7 30.40 2.79 11 -6 -7 30.56 3.66 -11 -6 7 28.97 4.70 -11 6 -7 32.55 2.94 -11 6 -7 37.57 4.78 -11 -6 7 33.27 5.65 11 -6 -7 23.08 3.18 -11 6 -7 29.37 3.50 -11 -6 -8 8.44 4.46 11 6 -8 10.90 5.09 -11 6 8 12.26 3.26 -11 -6 -8 0.24 5.09 -11 6 8 13.21 5.25 11 6 -8 9.63 4.46 -11 6 -8 11.30 2.31 11 -6 -8 8.99 3.02 -11 -6 8 14.49 4.46 -11 6 -8 9.87 3.34 -11 6 -8 12.26 4.46 -11 -6 8 14.25 5.41 11 -6 -8 13.29 4.78 -11 6 -8 11.78 4.85 -11 -6 -9 115.48 7.32 11 6 -9 113.57 8.36 -11 -6 -9 105.37 8.04 -11 6 9 117.55 4.78 -11 6 9 132.04 8.44 11 6 -9 107.60 5.17 -11 6 -9 108.40 4.38 11 -6 -9 120.97 5.81 -11 6 -9 115.96 6.21 -11 -6 9 108.08 4.85 -11 6 -9 117.47 7.32 -11 -6 9 108.16 8.75 11 -6 -9 107.84 7.32 -11 6 -9 114.29 8.12 -11 -6 -10 41.23 5.57 11 6 -10 25.07 6.45 -11 -6 -10 27.22 6.13 -11 6 10 30.72 4.06 -11 6 10 24.12 6.53 11 6 -10 28.17 5.81 -11 6 -10 28.41 4.54 11 -6 -10 24.19 6.05 -11 6 -10 20.69 4.93 -11 -6 10 28.02 5.33 -11 6 -10 30.56 5.49 -11 -6 10 24.99 6.77 11 -6 -10 36.13 5.65 -11 6 -10 23.88 6.05 -11 -6 -11 1.35 5.33 11 6 -11 0.32 6.29 -11 -6 -11 1.27 3.58 -11 6 11 0.40 4.70 -11 6 11 8.36 6.13 11 6 -11 4.78 5.09 11 -6 -11 5.81 4.30 -11 6 -11 3.34 5.09 -11 -6 11 -1.43 5.09 -11 6 -11 2.47 4.93 -11 -6 11 1.67 6.37 11 -6 -11 -1.03 5.09 -11 -6 -12 11.78 5.81 11 6 -12 7.64 6.53 -11 -6 -12 13.53 6.37 -11 6 12 10.27 4.38 11 -6 12 3.02 4.30 11 -6 12 14.01 6.37 -11 6 12 7.24 6.61 11 6 -12 7.72 5.89 11 -6 -12 9.07 5.17 -11 6 -12 3.98 4.54 -11 -6 12 11.62 5.73 -11 6 -12 12.57 5.41 -11 -6 12 10.43 7.00 11 -6 -12 5.41 5.57 -11 -6 -13 12.81 5.89 11 6 -13 4.30 7.00 -11 -6 -13 0.08 6.45 -11 6 13 3.34 4.54 11 -6 13 10.74 6.29 11 -6 13 6.53 6.29 -11 6 13 -3.90 6.69 11 6 -13 -8.91 6.21 11 -6 -13 -10.35 7.16 -11 6 -13 2.63 6.37 -11 -6 13 2.71 5.97 -11 6 -13 0.16 5.49 -11 -6 13 21.73 7.56 11 -6 -13 8.12 5.81 12 6 0 188.15 8.52 -12 -6 0 202.07 7.96 -12 6 0 189.98 8.36 -12 6 0 196.19 6.53 12 6 0 192.84 6.29 12 6 -1 21.41 4.70 -12 -6 -1 24.91 4.22 -12 6 1 21.65 2.87 -12 -6 -1 22.84 3.26 -12 6 1 24.19 5.09 12 6 -1 17.59 3.34 12 6 1 23.24 4.46 -12 -6 1 17.19 4.22 -12 6 -1 19.74 4.38 -12 -6 1 23.24 3.74 -12 6 -1 18.70 3.26 12 6 1 21.17 3.90 12 6 -2 7.88 4.22 -12 -6 -2 3.34 3.74 -12 6 2 1.83 4.06 -12 -6 -2 1.67 3.50 -12 6 2 -1.91 4.62 12 6 -2 4.93 3.18 12 6 2 8.44 4.14 -12 -6 2 3.50 3.82 -12 6 -2 4.78 3.90 -12 -6 2 3.34 3.50 -12 6 -2 -2.79 2.87 12 6 2 2.31 3.26 12 6 -3 81.10 6.29 -12 -6 -3 79.43 5.57 -12 6 3 74.65 3.98 -12 -6 -3 79.99 4.62 -12 6 3 79.35 4.62 12 6 -3 75.45 4.93 12 6 3 80.54 5.73 -12 -6 3 86.59 5.49 -12 6 -3 74.02 5.81 -12 -6 3 76.33 5.49 -12 6 -3 74.73 6.61 12 6 3 77.44 3.50 12 6 -4 25.07 4.93 -12 -6 -4 22.05 4.54 -12 -6 -4 25.55 4.78 -12 6 4 29.05 4.78 -12 -6 -4 21.33 3.10 -12 -6 -4 22.52 2.71 -12 6 4 23.16 5.49 12 6 -4 16.00 4.22 -12 -6 4 21.17 4.30 -12 6 -4 20.61 4.54 -12 -6 4 28.25 4.46 -12 6 -4 30.16 5.17 12 6 -5 28.25 5.17 -12 -6 -5 27.70 5.17 -12 -6 -5 23.00 2.87 -12 -6 -5 25.07 2.39 -12 6 5 24.91 5.81 12 6 -5 32.39 4.54 12 -6 -5 22.60 2.07 -12 -6 5 29.69 4.54 -12 6 -5 34.30 4.85 -12 -6 5 28.09 4.93 -12 6 -5 39.08 5.41 12 -6 -5 29.77 4.85 -12 -6 -6 7.24 2.79 12 6 -6 7.32 4.93 -12 6 6 6.13 2.15 -12 -6 -6 7.16 4.62 -12 -6 -6 11.94 2.39 -12 -6 -6 8.60 2.47 -12 6 6 13.13 5.17 12 6 -6 4.06 4.22 -12 6 -6 5.57 1.83 12 -6 -6 5.49 2.47 -12 -6 6 11.22 2.87 -12 6 -6 3.58 1.83 -12 6 -6 8.36 4.46 -12 -6 6 16.16 4.78 -12 6 -6 10.51 4.78 12 -6 -6 15.92 4.62 -12 -6 -7 82.93 6.21 12 6 -7 79.83 7.16 -12 6 7 78.79 4.14 -12 6 7 75.53 7.48 12 6 -7 77.28 4.30 -12 6 -7 72.50 3.74 12 -6 -7 81.42 5.25 -12 -6 7 74.97 6.29 -12 6 -7 76.72 3.74 -12 6 -7 78.87 6.21 -12 -6 7 93.44 7.32 -12 6 -7 89.14 7.08 12 -6 -7 85.00 6.77 -12 -6 -8 17.83 5.01 12 6 -8 16.40 6.05 -12 6 8 17.11 2.94 -12 -6 -8 21.57 5.57 -12 6 8 25.31 6.13 12 6 -8 19.26 5.17 -12 6 -8 16.87 3.50 12 -6 -8 20.53 4.38 -12 6 -8 12.42 3.58 -12 -6 8 24.67 4.93 -12 6 -8 26.66 5.17 -12 -6 8 35.18 6.13 -12 6 -8 22.05 5.57 12 -6 -8 25.79 5.17 -12 -6 -9 7.64 4.85 12 6 -9 1.75 5.73 -12 -6 -9 -5.81 5.49 -12 6 9 1.19 3.98 -12 6 9 9.63 5.73 12 6 -9 1.27 4.93 -12 6 -9 0.16 3.66 12 -6 -9 4.78 4.93 -12 6 -9 0.40 3.82 -12 -6 9 4.30 4.70 -12 6 -9 6.53 4.78 -12 -6 9 2.31 5.81 12 -6 -9 7.48 5.09 -12 6 -9 0.88 5.41 -12 -6 -10 101.63 8.04 12 6 -10 113.41 9.39 -12 -6 -10 97.10 9.07 -12 6 10 112.54 7.32 -12 6 10 115.01 9.79 12 6 -10 115.40 8.60 -12 6 -10 96.62 5.25 12 -6 -10 114.45 8.99 -12 6 -10 104.50 6.05 -12 -6 10 107.36 7.96 -12 6 -10 114.69 8.12 -12 -6 10 109.51 9.63 12 -6 -10 117.63 8.44 -12 6 -10 114.85 8.99 -12 -6 -11 53.32 6.84 12 6 -11 35.18 7.96 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8.44 -13 -6 6 184.57 8.68 -13 6 -6 170.08 8.99 -13 -6 6 171.67 9.71 -13 6 -6 165.23 9.95 13 -6 -6 177.80 9.55 -13 -6 -7 3.18 3.10 13 6 -7 15.52 5.81 -13 -6 -7 6.84 5.33 -13 6 7 0.56 5.89 13 6 -7 -4.78 4.70 -13 -6 7 10.51 4.70 -13 6 -7 1.91 4.85 -13 -6 7 4.70 5.57 -13 6 -7 -1.51 5.25 13 -6 -7 -2.63 5.17 -13 -6 -8 22.68 5.57 13 6 -8 31.44 6.92 -13 -6 -8 38.60 6.45 -13 6 8 27.38 7.00 13 6 -8 31.04 5.89 -13 -6 8 32.31 5.73 -13 6 -8 27.22 5.65 -13 -6 8 34.14 6.69 -13 6 -8 30.08 6.21 13 -6 -8 22.84 6.05 -13 -6 -9 192.84 10.59 13 6 -9 195.15 12.42 -13 -6 -9 166.74 11.38 -13 6 9 158.30 12.34 13 6 -9 191.81 11.06 -13 -6 9 178.12 10.03 -13 6 -9 186.00 10.11 -13 -6 9 198.10 12.50 -13 6 -9 181.46 11.30 13 -6 -9 197.46 10.82 -13 -6 -10 89.06 8.04 13 6 -10 93.44 9.63 -13 -6 -10 92.88 8.83 -13 6 10 94.55 10.11 13 6 -10 93.12 8.60 -13 -6 10 94.63 8.20 -13 6 -10 96.54 8.28 -13 -6 10 87.31 9.79 -13 6 -10 102.59 8.99 13 -6 -10 89.70 8.52 -13 -6 -11 22.21 6.69 13 6 -11 33.75 7.72 -13 -6 -11 26.18 7.32 -13 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6.61 6.37 11 8 -11 5.25 5.89 -11 8 -11 3.02 5.25 11 -8 -11 4.30 6.05 -11 8 -11 -2.71 5.73 -11 -8 11 -5.65 6.84 11 -8 -11 0.40 5.73 -11 -8 -12 45.60 7.56 11 8 -12 30.56 8.91 -11 -8 -12 46.80 8.52 -11 8 12 33.43 7.16 11 -8 12 33.51 8.12 -11 8 12 34.94 8.04 11 8 -12 33.67 7.40 11 -8 -12 23.16 7.80 -11 -8 12 44.89 7.48 -11 8 -12 40.75 7.24 -11 -8 12 41.15 8.75 11 -8 -12 43.53 7.08 12 8 0 11.62 5.01 -12 -8 0 10.19 4.38 -12 8 0 2.71 4.54 -12 -8 0 10.43 4.30 12 8 0 2.23 3.18 -12 8 0 8.68 5.25 12 8 -1 10.03 5.09 -12 -8 -1 11.30 4.38 -12 8 1 11.14 4.70 -12 -8 -1 5.41 3.10 12 8 -1 7.56 3.26 -12 8 1 8.44 3.42 12 8 1 7.08 4.85 -12 -8 1 4.46 4.38 -12 8 -1 4.06 4.54 -12 -8 1 3.50 3.66 12 8 1 9.07 3.66 -12 8 -1 2.31 3.50 12 8 -2 0.64 4.93 -12 -8 -2 -1.59 4.22 -12 8 2 0.80 4.62 -12 -8 -2 0.40 3.66 12 8 -2 1.59 3.42 -12 8 2 2.47 5.25 12 8 2 2.39 4.85 -12 -8 2 5.01 4.30 -12 8 -2 -2.71 4.54 -12 -8 2 7.88 4.78 12 8 2 4.93 2.63 -12 8 -2 4.06 5.33 12 8 -3 42.42 6.21 -12 -8 -3 37.25 3.50 -12 8 3 33.27 5.41 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2.79 3.82 10 -9 -9 0.16 4.54 -10 -9 9 7.32 5.41 -10 9 -9 7.00 5.49 -10 -9 9 8.20 3.90 -10 -9 -10 26.34 5.73 10 9 -10 21.97 6.84 -10 -9 -10 0.80 6.84 10 -9 10 5.09 4.46 10 -9 10 23.00 6.53 10 9 -10 13.69 5.73 -10 9 10 17.43 6.05 -10 9 -10 8.44 3.74 10 -9 -10 14.72 3.90 -10 -9 10 4.22 5.81 -10 9 -10 17.51 6.05 -10 -9 10 17.27 4.38 -10 -9 -11 122.73 9.07 10 9 -11 109.20 10.43 -10 -9 -11 122.25 10.66 10 -9 11 95.27 7.88 -10 9 11 108.08 8.28 10 -9 11 125.35 10.43 -10 9 11 99.01 9.79 10 9 -11 117.31 9.23 -10 9 -11 95.11 6.61 10 -9 -11 97.73 9.39 -10 -9 11 119.70 9.31 -10 9 -11 119.06 9.47 -10 -9 11 120.42 10.82 10 -9 -11 124.08 8.52 -10 -9 -12 7.56 6.21 10 9 -12 -2.63 7.00 -10 -9 -12 9.95 7.32 10 -9 12 3.10 4.38 -10 9 12 6.61 5.97 10 -9 12 10.19 7.24 -10 9 12 4.93 6.45 10 9 -12 12.18 6.21 -10 9 -12 5.25 6.05 10 -9 -12 -0.80 5.09 -10 -9 12 2.94 6.37 -10 9 -12 1.43 6.21 -10 -9 12 7.16 7.48 10 -9 -12 4.78 5.65 11 9 0 -5.89 4.93 -11 -9 0 0.24 4.38 -11 9 0 -3.34 4.22 -11 -9 0 0.72 3.98 11 9 0 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4.46 -7 12 -8 16.63 3.58 -7 -12 8 15.04 5.89 7 -12 -8 15.28 3.82 -7 -12 8 30.16 6.13 -7 12 -8 12.26 6.21 -7 -12 -9 14.56 5.73 7 12 -9 8.83 6.77 7 -12 9 7.72 3.82 -7 -12 -9 5.49 6.84 7 -12 9 17.27 7.08 -7 12 9 18.07 4.70 7 12 -9 15.68 5.73 -7 12 9 5.25 5.09 7 -12 -9 10.43 3.66 -7 12 -9 6.77 4.93 -7 -12 9 18.94 5.89 7 -12 -9 3.34 4.22 -7 -12 9 8.44 6.21 -7 12 -9 4.54 6.05 -7 -12 -10 28.25 5.81 7 12 -10 15.92 7.16 7 -12 10 6.61 5.65 -7 -12 -10 6.69 4.70 7 -12 10 17.27 7.24 -7 12 10 8.83 4.93 7 12 -10 11.14 6.05 -7 12 10 10.66 7.16 7 -12 -10 11.22 4.14 -7 12 -10 12.89 4.62 -7 -12 10 19.02 6.21 7 -12 -10 12.26 4.54 -7 -12 10 10.35 6.84 -7 12 -10 12.81 6.53 -7 -12 -11 26.50 6.61 7 12 -11 12.65 7.80 7 -12 11 15.20 6.61 -7 -12 -11 26.10 7.72 -7 12 11 18.78 5.17 7 -12 11 10.90 7.88 7 12 -11 25.71 6.84 -7 12 11 18.23 7.64 7 -12 -11 20.37 6.05 -7 12 -11 8.28 5.25 -7 -12 11 26.18 6.69 7 -12 -11 9.95 6.61 -7 -12 11 27.94 7.56 -7 12 -11 28.49 6.84 8 12 0 76.40 7.48 -8 -12 0 79.91 6.77 -8 12 0 84.84 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7.72 6.77 -5 13 9 4.30 4.14 5 13 -9 8.44 5.57 -5 13 9 3.18 4.70 5 -13 -9 1.75 5.17 -5 13 -9 6.05 4.30 -5 -13 9 4.14 5.57 5 -13 -9 6.45 4.62 -5 -13 9 12.18 6.13 -5 13 -9 1.27 5.97 -5 -13 -10 6.13 3.74 5 13 -10 15.76 6.69 5 -13 10 1.91 4.70 -5 -13 -10 13.21 6.92 5 -13 10 11.78 7.32 -5 13 10 4.54 5.65 5 13 -10 3.66 6.21 -5 13 10 2.47 4.85 5 -13 -10 9.23 5.73 -5 13 -10 4.46 4.70 -5 -13 10 10.82 5.97 5 -13 -10 9.07 4.85 -5 -13 10 -4.22 6.69 -5 13 -10 0.88 6.37 -5 -13 -11 14.41 5.97 5 13 -11 3.74 6.77 5 -13 11 7.48 5.09 -5 -13 -11 -1.19 7.16 5 -13 11 12.65 7.40 -5 13 11 4.62 5.89 5 13 -11 1.91 6.53 -5 13 11 2.07 6.45 5 -13 -11 3.50 4.62 -5 13 -11 -2.55 5.41 -5 -13 11 -4.78 6.21 5 -13 -11 3.18 7.08 -5 -13 11 1.35 6.92 -5 13 -11 10.98 6.53 6 13 0 35.10 5.73 -6 -13 0 26.82 4.85 6 -13 0 20.14 3.10 6 -13 0 25.15 2.94 -6 -13 0 30.16 3.82 -6 13 0 30.40 4.70 6 13 0 30.56 3.58 -6 13 0 27.86 5.49 6 13 -1 171.11 9.55 -6 -13 -1 178.04 8.44 6 -13 1 180.11 5.57 6 -13 1 154.64 5.25 -6 -13 -1 169.76 6.05 -6 13 1 171.43 7.80 6 13 -1 170.56 6.84 -6 13 1 160.93 9.15 6 13 1 167.69 9.55 -6 -13 1 176.61 8.44 6 -13 -1 169.84 5.25 6 -13 -1 155.67 5.33 -6 -13 1 165.07 7.16 -6 13 -1 161.48 8.28 6 13 1 179.63 7.32 -6 13 -1 196.82 9.47 6 13 -2 10.59 5.33 -6 -13 -2 7.48 4.46 6 -13 2 6.92 2.79 6 -13 2 6.21 5.01 -6 -13 -2 5.65 2.71 -6 13 2 17.19 4.06 6 13 -2 10.11 3.74 -6 13 2 12.73 4.70 -6 13 -2 7.00 2.39 6 13 2 11.78 5.01 -6 -13 2 3.82 4.62 6 -13 -2 8.04 2.79 6 -13 -2 9.07 2.71 -6 -13 2 9.47 3.98 -6 13 -2 7.64 4.46 6 13 2 10.66 3.34 6 13 -3 205.74 10.74 -6 -13 -3 202.07 9.55 6 -13 3 193.64 6.69 6 -13 3 191.73 10.51 -6 13 3 207.96 8.75 6 13 -3 207.17 8.20 -6 13 3 205.42 9.71 6 13 3 209.95 10.35 -6 13 -3 202.23 6.13 6 -13 -3 187.91 4.93 -6 -13 3 201.52 9.39 6 -13 -3 181.78 6.21 -6 -13 3 211.55 8.68 -6 13 -3 196.50 6.61 6 13 -4 69.16 6.84 -6 -13 -4 69.00 6.29 6 -13 4 57.46 4.46 -6 -13 -4 54.76 2.94 6 -13 4 60.96 7.32 -6 13 4 66.93 5.41 6 13 -4 76.80 5.49 -6 13 4 58.34 6.13 -6 13 -4 69.16 4.14 6 -13 -4 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10.35 7 13 -1 261.93 8.68 -7 13 1 268.45 12.10 7 13 1 245.13 12.42 -7 -13 1 244.57 11.38 7 -13 -1 271.71 5.81 -7 13 -1 258.03 10.98 -7 -13 1 247.04 9.23 7 13 1 266.62 9.47 -7 13 -1 271.63 12.89 7 13 -2 110.23 5.73 -7 -13 -2 102.59 7.24 7 -13 2 99.33 3.26 -7 -13 -2 105.93 5.41 -7 13 2 106.49 6.92 7 13 -2 106.41 5.89 -7 13 2 109.91 7.56 7 13 2 95.11 8.44 -7 -13 2 116.44 7.56 7 -13 -2 100.44 3.42 -7 13 -2 110.63 7.24 -7 -13 2 109.20 6.29 7 13 2 114.13 5.49 -7 13 -2 113.33 8.52 7 13 -3 218.87 11.46 -7 -13 -3 205.66 10.19 7 -13 3 200.16 5.49 7 -13 3 217.83 11.78 -7 -13 -3 192.68 6.77 -7 13 3 205.42 9.23 7 13 -3 218.23 8.60 -7 13 3 222.37 10.51 7 13 3 207.17 11.22 -7 -13 3 225.23 10.51 -7 -13 3 218.55 11.38 -7 13 -3 195.79 10.27 7 13 3 220.06 6.77 7 13 -4 2.47 5.57 -7 -13 -4 9.79 5.09 7 -13 4 3.58 2.63 7 -13 4 8.75 5.73 -7 13 4 10.11 4.22 7 13 -4 6.77 4.22 -7 13 4 2.55 5.09 -7 13 -4 3.02 2.31 7 -13 -4 5.01 2.71 -7 -13 4 14.64 5.09 7 -13 -4 2.31 2.79 -7 -13 4 7.16 4.46 -7 13 -4 13.85 5.17 7 13 -5 281.42 14.01 -7 -13 -5 288.91 12.81 7 -13 5 251.26 8.36 -7 -13 -5 278.24 10.11 7 -13 5 281.42 14.49 -7 13 5 275.77 11.06 7 13 -5 278.08 11.46 -7 13 5 298.22 12.42 -7 -13 5 278.08 12.34 7 -13 -5 256.04 7.40 -7 -13 5 262.96 15.36 -7 13 -5 261.13 13.13 7 13 -6 147.88 10.43 -7 -13 -6 131.88 6.21 -7 -13 -6 145.96 7.24 7 -13 6 140.08 10.82 -7 13 6 143.42 7.72 7 13 -6 143.18 8.36 -7 13 6 143.42 8.52 -7 -13 6 132.28 6.29 7 -13 -6 136.33 7.08 -7 -13 6 157.03 9.07 -7 13 -6 136.33 9.15 7 13 -7 27.22 6.92 -7 -13 -7 31.84 5.97 7 -13 7 18.15 4.46 -7 -13 -7 21.25 6.92 7 -13 7 31.36 7.32 -7 13 7 19.74 4.78 7 13 -7 28.49 5.57 -7 13 7 26.10 5.57 7 -13 -7 16.08 4.46 -7 -13 7 22.28 6.13 7 -13 -7 16.16 4.70 -7 -13 7 23.48 6.37 -7 13 -7 36.61 6.29 -7 -13 -8 -0.88 3.66 7 13 -8 3.10 6.53 7 -13 8 3.18 4.70 -7 -13 -8 3.66 6.69 7 -13 8 15.28 6.84 -7 13 8 0.96 4.46 7 13 -8 6.77 5.41 -7 13 8 2.94 5.25 7 -13 -8 4.30 4.46 -7 13 -8 5.01 4.78 -7 -13 8 -1.19 5.49 7 -13 -8 0.32 3.90 -7 -13 8 8.20 6.13 -7 13 -8 12.89 6.05 -7 -13 -9 278.56 14.33 7 13 -9 297.98 16.79 7 -13 9 235.42 13.21 -7 -13 -9 294.24 16.95 7 -13 9 256.75 12.10 -7 13 9 281.03 12.10 7 13 -9 276.25 14.41 -7 13 9 279.59 13.37 -7 -13 9 277.52 15.28 7 -13 -9 257.79 11.14 -7 -13 9 281.34 16.00 -7 13 -9 302.67 15.04 -7 -13 -10 18.46 4.22 7 13 -10 14.49 7.48 7 -13 10 10.66 4.78 -7 -13 -10 16.24 7.64 7 -13 10 15.76 5.09 -7 13 10 18.38 6.77 7 13 -10 15.28 6.61 -7 13 10 9.15 6.05 7 -13 -10 13.69 4.46 -7 13 -10 7.40 4.93 -7 -13 10 20.06 6.84 7 -13 -10 16.55 4.85 -7 -13 10 20.37 7.24 -7 13 -10 14.25 7.08 8 13 0 51.73 7.16 -8 -13 0 57.94 6.13 -8 13 0 50.94 3.98 -8 -13 0 47.36 5.89 8 13 0 44.73 4.38 -8 13 0 53.24 7.16 8 13 -1 37.57 6.69 -8 -13 -1 28.49 5.89 -8 -13 -1 33.03 4.93 8 13 -1 35.10 5.41 -8 13 1 35.81 6.37 8 13 1 47.04 6.45 -8 -13 1 44.01 5.81 -8 13 -1 32.79 5.57 -8 -13 1 31.76 4.46 8 13 1 35.02 3.66 -8 13 -1 38.04 6.84 8 13 -2 13.53 5.97 -8 -13 -2 16.24 5.41 -8 -13 -2 19.90 3.10 -8 13 2 8.44 4.93 8 13 -2 23.48 4.14 -8 13 2 13.29 5.81 8 13 2 14.49 5.97 -8 -13 2 7.64 5.41 -8 13 -2 16.71 5.33 -8 -13 2 11.46 4.38 8 13 2 16.08 3.10 8 13 -3 97.65 8.60 -8 -13 -3 86.19 7.64 -8 13 3 91.61 6.84 8 13 -3 105.06 6.29 -8 13 3 94.63 7.96 8 13 3 76.96 8.44 -8 -13 3 91.21 7.72 -8 13 -3 97.34 7.72 -8 -13 3 87.55 6.77 -8 13 -3 97.73 8.83 8 13 -4 70.04 8.52 -8 -13 -4 99.49 7.72 -8 13 4 85.64 6.77 8 13 -4 85.64 6.45 -8 13 4 90.17 7.72 -8 -13 4 91.37 7.72 -8 13 -4 91.45 7.88 -8 -13 4 88.66 7.08 8 13 -5 21.49 6.69 -8 -13 -5 14.17 5.73 -8 -13 -5 4.85 6.84 8 -13 5 21.65 6.69 -8 13 5 19.66 5.01 8 13 -5 23.56 5.01 -8 13 5 24.59 5.89 -8 -13 5 17.75 3.82 -8 13 -5 31.36 6.05 -8 -13 5 14.49 5.57 8 13 -6 46.64 7.88 -8 -13 -6 50.70 6.61 -8 -13 -6 54.60 8.36 8 -13 6 51.81 8.04 -8 13 6 43.46 5.89 8 13 -6 52.69 6.21 -8 13 6 43.85 6.84 -8 -13 6 59.13 6.84 -8 -13 6 41.86 6.84 -8 13 -6 48.39 7.08 8 13 -7 168.41 8.28 -8 -13 -7 151.85 10.43 -8 -13 -7 134.90 11.94 8 -13 7 150.74 8.36 -8 13 7 160.93 8.83 8 13 -7 167.85 9.63 -8 13 7 152.57 10.11 -8 -13 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6.69 6.53 9 13 -3 11.46 6.53 -9 -13 -3 10.82 5.49 -9 13 3 11.46 5.01 9 13 -3 11.62 4.46 -9 13 3 9.15 6.05 9 13 3 7.24 6.29 -9 -13 3 11.38 5.65 -9 13 -3 7.00 5.57 -9 -13 3 9.71 6.37 -9 13 -3 4.46 4.30 9 13 -4 12.81 6.37 -9 -13 -4 5.33 5.57 -9 13 4 5.97 4.85 9 13 -4 6.05 4.62 -9 13 4 -1.51 5.97 -9 -13 4 -5.49 5.65 -9 13 -4 11.46 3.66 -9 -13 4 5.73 5.01 -9 13 -4 6.45 6.77 9 13 -5 25.47 6.77 -9 -13 -5 24.19 5.81 -9 -13 -5 1.59 7.16 -9 13 5 9.79 5.25 9 13 -5 14.88 5.09 -9 13 5 16.79 6.13 -9 -13 5 6.69 6.13 -9 13 -5 14.72 5.73 -9 -13 5 8.75 5.57 -9 13 -5 11.38 7.24 9 13 -6 12.26 6.84 -9 -13 -6 11.14 5.97 -9 -13 -6 16.55 7.48 9 -13 6 5.97 7.00 -9 13 6 4.70 5.25 9 13 -6 14.64 5.25 -9 13 6 7.32 6.13 -9 -13 6 11.14 6.21 -9 13 -6 9.39 6.21 -9 -13 6 11.94 5.89 9 13 -7 -5.01 7.24 -9 -13 -7 6.45 6.21 -9 -13 -7 8.52 7.16 9 -13 7 10.03 7.24 -9 13 7 8.83 5.25 9 13 -7 11.14 5.57 -9 13 7 12.10 6.29 -9 -13 7 8.28 6.21 -9 13 -7 8.52 6.53 -9 -13 7 7.24 6.05 9 13 -8 24.51 8.20 -9 -13 -8 31.52 7.16 -9 -13 -8 33.11 8.36 9 -13 8 19.82 8.36 -9 13 8 31.28 6.21 9 13 -8 27.62 6.61 -9 13 8 29.29 7.16 -9 -13 8 29.53 7.40 -9 -13 8 37.17 7.48 -9 13 -8 34.46 7.32 10 13 0 63.35 8.36 -10 -13 0 72.66 7.40 -10 13 0 68.29 7.24 -10 -13 0 62.72 5.57 10 13 0 67.57 5.41 -10 13 0 68.68 8.75 10 13 -1 0.80 6.45 -10 -13 -1 0.08 5.81 -10 13 1 16.08 5.57 -10 -13 -1 5.57 5.17 10 13 -1 6.53 4.22 -10 13 1 3.02 6.53 10 13 1 15.68 6.29 -10 -13 1 10.82 5.65 -10 13 -1 10.11 5.73 -10 -13 1 12.65 5.89 10 13 1 4.54 4.70 -10 13 -1 12.97 4.46 10 13 -2 27.54 7.00 -10 -13 -2 12.18 6.21 -10 13 2 26.42 5.97 10 13 -2 17.35 4.78 -10 13 2 23.80 4.62 10 13 2 14.88 6.92 -10 -13 2 25.63 6.37 -10 13 -2 16.08 6.13 -10 -13 2 15.44 5.17 -10 13 -2 26.03 7.32 10 13 -3 131.72 10.59 -10 -13 -3 122.09 9.07 -10 13 3 116.12 8.91 10 13 -3 117.55 9.39 -10 13 3 123.68 10.51 10 13 3 131.80 10.66 -10 -13 3 132.99 9.63 -10 13 -3 122.88 6.45 -10 -13 3 117.71 10.66 -10 13 -3 109.04 7.48 10 13 -4 12.18 6.69 -10 -13 -4 1.59 6.05 -10 13 4 9.47 5.41 10 13 -4 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52.13 7.88 1 17 -3 59.37 6.77 -1 17 3 53.24 6.69 -1 17 -3 52.61 6.37 1 -17 -3 48.71 5.81 -1 -17 3 65.42 6.69 1 -17 -3 61.60 6.77 -1 -17 3 56.43 7.72 -1 17 -3 54.12 7.16 1 17 3 54.04 5.65 1 17 3 56.43 7.80 1 17 -4 8.99 5.89 -1 -17 -4 4.93 5.25 1 -17 4 4.93 4.85 -1 -17 -4 19.98 6.45 1 -17 4 14.25 6.69 -1 17 4 7.32 4.54 1 17 -4 7.72 5.81 -1 17 4 6.37 5.01 -1 17 -4 4.46 5.17 1 -17 -4 3.58 4.78 -1 -17 4 7.16 5.41 1 -17 -4 13.21 5.57 -1 -17 4 3.90 6.45 -1 17 -4 6.29 5.97 1 17 4 19.10 5.65 1 17 4 12.18 4.70 1 17 -5 63.51 7.88 -1 -17 -5 48.47 6.69 1 -17 5 62.32 8.99 -1 -17 -5 55.79 10.51 1 -17 5 61.20 8.83 -1 17 5 60.49 5.89 1 17 -5 76.56 7.72 -1 17 5 57.06 6.37 -1 17 -5 72.35 9.31 1 -17 -5 54.68 6.37 -1 -17 5 62.48 7.00 1 -17 -5 55.31 7.48 -1 -17 5 60.25 10.90 -1 17 -5 64.78 7.56 2 17 0 133.71 9.71 -2 -17 0 150.74 9.07 2 -17 0 141.19 10.19 -2 -17 0 132.83 11.94 -2 17 0 164.03 9.07 2 17 0 145.01 8.52 2 17 -1 171.67 9.79 -2 -17 -1 159.57 9.15 2 -17 1 143.74 8.04 2 -17 1 151.06 10.43 -2 -17 -1 136.10 9.07 -2 17 1 146.68 11.38 2 17 -1 151.54 8.68 -2 17 1 159.02 13.29 2 17 1 156.47 9.95 -2 17 -1 152.73 8.60 2 -17 -1 140.63 8.28 -2 -17 1 146.76 9.23 2 -17 -1 156.15 9.47 -2 -17 1 154.16 9.71 -2 17 -1 164.83 11.86 2 17 1 160.85 10.66 2 17 -2 13.53 5.65 -2 -17 -2 16.71 5.41 2 -17 2 8.75 6.29 2 -17 2 12.89 6.45 -2 17 2 -0.48 5.01 2 17 -2 9.79 5.25 -2 17 2 18.31 5.73 -2 17 -2 16.95 6.61 2 -17 -2 14.33 4.70 -2 -17 2 7.80 6.92 2 -17 -2 17.27 5.49 -2 -17 2 10.19 6.05 -2 17 -2 15.20 5.65 2 17 2 20.30 6.05 2 17 -3 33.67 6.69 -2 -17 -3 33.67 6.05 2 -17 3 28.89 5.41 -2 -17 -3 43.46 7.24 2 -17 3 38.84 7.48 -2 17 3 40.11 5.57 2 17 -3 33.98 6.21 -2 17 3 39.95 8.20 -2 17 -3 39.24 5.73 2 -17 -3 33.03 5.25 -2 -17 3 37.33 6.21 2 -17 -3 29.29 5.97 -2 -17 3 32.07 8.83 -2 17 -3 32.87 6.69 2 17 3 32.23 6.29 2 17 3 29.13 5.25 2 17 -4 147.88 10.35 -2 -17 -4 127.66 9.39 2 -17 4 126.07 10.66 -2 -17 -4 147.08 10.98 2 -17 4 135.06 11.30 -2 17 4 142.30 8.20 2 17 -4 144.69 9.71 -2 17 4 143.50 11.62 -2 17 -4 129.25 8.99 2 -17 -4 122.33 7.96 -2 -17 4 149.23 9.39 2 -17 -4 129.33 9.07 -2 -17 4 138.56 10.51 -2 17 -4 146.20 9.79 2 17 -5 8.20 6.21 -2 -17 -5 5.17 5.25 2 -17 5 -3.26 6.84 -2 -17 -5 9.55 6.53 2 -17 5 4.85 6.92 -2 17 5 4.46 5.25 2 17 -5 18.23 6.05 -2 17 5 9.15 5.41 -2 17 -5 6.29 5.65 2 -17 -5 6.05 4.78 -2 -17 5 3.18 5.65 2 -17 -5 1.75 7.40 -2 -17 5 10.11 6.53 -2 17 -5 7.80 6.05 3 17 0 -4.70 5.57 -3 -17 0 -2.63 5.33 3 -17 0 4.30 5.49 3 -17 0 4.85 4.78 -3 -17 0 -1.99 5.09 -3 17 0 -1.11 6.45 3 17 0 -3.34 4.62 -3 17 0 6.53 5.97 3 17 -1 45.21 6.92 -3 -17 -1 52.13 6.45 3 -17 1 28.81 5.09 3 -17 1 35.50 7.32 -3 -17 -1 34.70 5.97 -3 17 1 49.50 6.21 3 17 -1 44.33 6.05 -3 17 1 39.16 7.24 -3 17 -1 40.11 5.49 3 17 1 37.96 6.92 -3 -17 1 43.22 6.61 3 -17 -1 34.38 6.61 3 -17 -1 38.20 5.81 -3 -17 1 39.71 6.53 -3 17 -1 48.47 6.45 3 17 1 43.46 5.65 3 17 -2 176.13 11.30 -3 -17 -2 171.19 10.35 3 -17 2 150.34 8.68 -3 -17 -2 161.33 9.15 3 -17 2 165.86 11.70 -3 17 2 183.29 11.86 3 17 -2 177.88 9.87 -3 17 2 161.56 10.82 3 17 2 156.47 10.98 -3 17 -2 167.22 9.07 3 -17 -2 164.35 8.60 -3 -17 2 164.59 10.27 3 -17 -2 159.50 11.54 -3 -17 2 172.39 10.35 -3 17 -2 173.58 10.27 3 17 2 166.34 10.98 3 17 -3 14.01 6.05 -3 -17 -3 5.25 5.65 3 -17 3 1.35 6.05 -3 -17 -3 8.60 6.61 3 -17 3 4.93 6.77 -3 17 3 14.56 4.93 3 17 -3 13.69 5.73 -3 17 3 6.13 5.81 -3 17 -3 17.19 6.29 3 -17 -3 9.47 4.54 -3 -17 3 6.84 5.81 3 -17 -3 6.92 5.01 -3 -17 3 6.69 6.13 -3 17 -3 13.37 5.81 3 17 -4 8.60 6.13 -3 -17 -4 -0.88 5.73 3 -17 4 5.01 4.62 -3 -17 -4 -7.00 8.68 3 -17 4 7.72 6.84 -3 17 4 3.02 4.93 3 17 -4 7.40 5.65 -3 17 4 5.09 5.57 -3 17 -4 -0.32 4.78 3 -17 -4 0.88 5.81 -3 -17 4 2.87 5.65 3 -17 -4 2.79 5.01 -3 -17 4 10.03 6.21 -3 17 -4 7.96 5.73 4 17 0 66.22 8.12 -4 -17 0 60.33 9.39 4 -17 0 46.48 7.08 4 -17 0 64.78 7.88 -4 -17 0 70.44 6.92 -4 17 0 72.35 7.32 4 17 0 62.32 6.45 -4 17 0 81.82 8.60 4 17 -1 2.15 6.05 -4 -17 -1 4.62 5.57 4 -17 1 -0.24 5.25 4 -17 1 -2.23 5.81 -4 -17 -1 7.24 5.09 -4 17 1 6.05 5.17 4 17 -1 4.93 6.45 -4 17 1 5.49 6.21 4 17 1 8.99 6.13 -4 -17 1 10.59 5.41 4 -17 -1 2.63 3.98 4 -17 -1 -3.18 4.38 -4 -17 1 8.44 5.57 -4 17 -1 -9.15 5.57 4 17 1 3.34 4.62 -4 17 -1 -0.96 6.53 4 17 -2 1.59 7.88 -4 -17 -2 6.21 5.33 4 -17 2 2.47 5.25 4 -17 2 7.88 6.53 -4 -17 -2 -5.81 5.81 -4 17 2 -2.71 5.17 4 17 -2 -1.75 6.61 -4 17 2 -3.50 6.05 4 17 2 -1.35 5.97 -4 17 -2 -0.08 4.14 4 -17 -2 1.03 3.90 -4 -17 2 5.97 5.49 4 -17 -2 4.46 4.46 -4 -17 2 3.26 7.40 -4 17 -2 9.23 5.49 4 17 -3 19.82 6.77 -4 -17 -3 18.31 6.05 4 -17 3 8.44 4.62 -4 -17 -3 19.82 7.16 4 -17 3 16.32 7.08 -4 17 3 16.71 5.41 4 17 -3 12.02 5.81 -4 17 3 25.63 6.37 -4 17 -3 12.34 4.85 4 -17 -3 10.82 4.46 -4 -17 3 22.05 6.05 4 -17 -3 11.06 6.37 -4 -17 3 23.96 6.61 -4 17 -3 21.41 6.21 5 17 0 7.64 6.37 -5 -17 0 7.56 5.97 -5 -17 0 1.83 5.41 -5 17 0 1.75 5.57 5 17 0 3.10 6.61 -5 17 0 8.75 6.53 5 17 -1 11.06 6.37 -5 -17 -1 -1.99 5.73 -5 -17 -1 3.90 5.09 -5 17 1 9.87 5.65 5 17 -1 11.78 5.17 -5 17 1 2.31 6.53 5 17 1 0.40 6.13 -5 -17 1 -2.87 5.73 -5 -17 1 3.98 5.73 -5 17 -1 -0.32 5.89 5 17 1 6.37 6.21 -5 17 -1 14.64 6.84 5 17 -2 10.98 6.84 -5 -17 -2 11.78 5.97 -5 17 2 11.14 5.65 5 17 -2 2.07 7.08 -5 17 2 7.48 6.61 5 17 2 17.27 6.77 -5 -17 2 8.91 6.21 -5 -17 2 12.57 6.13 -5 17 -2 17.27 6.13 -5 17 -2 4.54 7.32 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 51520 _olex2_submission_original_sample_id RM4010 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn Ag1 Ag 0.64089(2) 0.61006(2) 0.61616(2) 0.01707(11) Uani 1 1 d . Cl1 Cl 0.76240(7) 0.63983(9) 0.50725(7) 0.0216(2) Uani 1 1 d . N1 N 0.4416(3) 0.5586(3) 0.6880(3) 0.0169(7) Uani 1 1 d . N2 N 0.5440(2) 0.5591(3) 0.8036(2) 0.0160(7) Uani 1 1 d . C1 C 0.5322(3) 0.5752(3) 0.7115(3) 0.0168(8) Uani 1 1 d . C14 C 0.5046(3) 0.3576(3) 0.8003(3) 0.0162(8) Uani 1 1 d . C9 C 0.4381(3) 0.3578(3) 0.7267(3) 0.0165(8) Uani 1 1 d . C13 C 0.5947(3) 0.3180(3) 0.7880(3) 0.0214(9) Uani 1 1 d . H13 H 0.640159 0.318314 0.838019 0.026 Uiso 1 1 calc R C10 C 0.4600(3) 0.3184(3) 0.6391(3) 0.0207(9) Uani 1 1 d . H10 H 0.414848 0.318837 0.588814 0.025 Uiso 1 1 calc R C3 C 0.3844(3) 0.5234(3) 0.7677(3) 0.0167(8) Uani 1 1 d . H3 H 0.329392 0.567724 0.781277 0.020 Uiso 1 1 calc R C12 C 0.6163(3) 0.2779(3) 0.7005(3) 0.0220(9) Uani 1 1 d . H12 H 0.677495 0.249719 0.690636 0.026 Uiso 1 1 calc R C2 C 0.4578(3) 0.5232(3) 0.8503(3) 0.0178(8) Uani 1 1 d . H2 H 0.437425 0.566823 0.903333 0.021 Uiso 1 1 calc R C8 C 0.3518(3) 0.4149(3) 0.7616(3) 0.0199(9) Uani 1 1 d . H8 H 0.290308 0.402528 0.727486 0.024 Uiso 1 1 calc R C6 C 0.4604(3) 0.4143(3) 0.8814(3) 0.0195(9) Uani 1 1 d . H6 H 0.487739 0.401331 0.945650 0.023 Uiso 1 1 calc R C11 C 0.5504(4) 0.2780(3) 0.6270(3) 0.0226(9) Uani 1 1 d . H11 H 0.567242 0.250143 0.567639 0.027 Uiso 1 1 calc R C7 C 0.3529(3) 0.3901(4) 0.8691(3) 0.0244(10) Uani 1 1 d . H7A H 0.310800 0.433099 0.906864 0.029 Uiso 1 1 calc R H7B H 0.338011 0.320972 0.882079 0.029 Uiso 1 1 calc R C4 C 0.6313(3) 0.5726(4) 0.8568(3) 0.0230(9) Uani 1 1 d . H4A H 0.681639 0.596130 0.814251 0.035 Uiso 1 1 calc GR H4B H 0.650882 0.510379 0.884696 0.035 Uiso 1 1 calc GR H4C H 0.620677 0.620289 0.907288 0.035 Uiso 1 1 calc GR C5 C 0.3991(3) 0.5725(4) 0.5951(3) 0.0219(9) Uani 1 1 d . H5A H 0.355261 0.628143 0.597042 0.033 Uiso 1 1 calc GR H5B H 0.363731 0.513827 0.577011 0.033 Uiso 1 1 calc GR H5C H 0.449478 0.585031 0.548461 0.033 Uiso 1 1 calc GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ag1 0.01565(17) 0.01878(18) 0.01677(17) -0.00082(12) 0.00109(11) -0.00102(12) Cl1 0.0144(5) 0.0320(6) 0.0185(5) -0.0004(4) 0.0003(4) -0.0049(4) N1 0.0174(17) 0.0160(17) 0.0172(17) -0.0006(14) -0.0004(14) -0.0001(14) N2 0.0146(16) 0.0178(17) 0.0154(17) -0.0016(13) 0.0013(14) 0.0003(14) C1 0.016(2) 0.0129(18) 0.021(2) -0.0016(16) 0.0021(16) -0.0001(16) C14 0.0154(19) 0.0139(18) 0.019(2) 0.0005(16) -0.0004(16) -0.0009(15) C9 0.0146(19) 0.0125(17) 0.022(2) 0.0019(15) -0.0010(16) -0.0043(15) C13 0.023(2) 0.0145(19) 0.027(2) 0.0037(17) -0.0035(18) -0.0024(17) C10 0.028(2) 0.0140(19) 0.021(2) 0.0004(16) -0.0038(18) -0.0016(18) C3 0.0141(19) 0.018(2) 0.018(2) 0.0004(16) 0.0018(16) 0.0013(16) C12 0.021(2) 0.014(2) 0.031(2) 0.0007(17) 0.0015(19) 0.0015(16) C2 0.0159(19) 0.019(2) 0.019(2) -0.0008(16) 0.0054(17) -0.0006(16) C8 0.013(2) 0.018(2) 0.029(2) 0.0028(18) -0.0004(17) -0.0026(16) C6 0.021(2) 0.020(2) 0.018(2) 0.0026(16) 0.0006(17) -0.0015(17) C11 0.029(2) 0.015(2) 0.023(2) -0.0026(17) 0.0047(19) -0.0033(18) C7 0.021(2) 0.026(2) 0.026(2) 0.0025(19) 0.0030(18) -0.0012(19) C4 0.017(2) 0.029(2) 0.023(2) -0.0009(19) -0.0046(17) -0.0021(18) C5 0.018(2) 0.027(2) 0.020(2) 0.0021(18) -0.0048(17) 0.0010(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C1 Ag1 Cl1 176.80(12) C1 N1 C3 112.8(4) C1 N1 C5 126.3(4) C5 N1 C3 120.8(4) C1 N2 C2 113.2(4) C1 N2 C4 126.2(4) C4 N2 C2 120.6(4) N1 C1 Ag1 125.1(3) N2 C1 Ag1 125.3(3) N2 C1 N1 109.5(4) C9 C14 C6 106.7(4) C13 C14 C9 121.1(4) C13 C14 C6 131.9(4) C14 C9 C8 106.9(4) C10 C9 C14 121.1(4) C10 C9 C8 131.8(4) C14 C13 C12 117.8(4) C9 C10 C11 117.8(4) N1 C3 C2 102.4(3) N1 C3 C8 115.7(4) C2 C3 C8 103.5(3) C13 C12 C11 121.3(4) N2 C2 C3 102.0(3) N2 C2 C6 115.6(4) C3 C2 C6 103.2(3) C9 C8 C3 106.1(3) C9 C8 C7 101.2(4) C7 C8 C3 98.7(4) C14 C6 C2 106.9(3) C14 C6 C7 101.6(4) C7 C6 C2 98.7(4) C12 C11 C10 120.9(4) C6 C7 C8 94.2(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Ag1 Cl1 2.3287(11) Ag1 C1 2.087(4) N1 C1 1.331(5) N1 C3 1.463(5) N1 C5 1.453(6) N2 C1 1.329(5) N2 C2 1.460(5) N2 C4 1.446(5) C14 C9 1.394(6) C14 C13 1.385(6) C14 C6 1.517(6) C9 C10 1.383(6) C9 C8 1.523(6) C13 C12 1.386(7) C10 C11 1.393(7) C3 C2 1.554(6) C3 C8 1.562(6) C12 C11 1.388(7) C2 C6 1.559(6) C8 C7 1.554(7) C6 C7 1.551(6) loop_ _cod_changelog_entry_id _cod_changelog_entry_author _cod_changelog_entry_date _cod_changelog_entry_text 1 'Vaitkus, Antanas' 2022-05-06T23:25:00+03:00 ; Replaced the "Â¥" sequence with backslash symbols ("\") in the '_diffrn_measurement_method' data item value. ;