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Information card for entry 4038396
Preview
| Coordinates | 4038396.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C33 H32 N3 Ni O2 P |
|---|---|
| Calculated formula | C33 H32 N3 Ni O2 P |
| Title of publication | Nickel(II) - NɅNɅO Pincer Type Complexes Catalyzed N-alkylation of Amines with Alcohols via Hydrogen Auto Transfer Reaction. |
| Authors of publication | Balamurugan, Gunasekaran; Ramesh, Rengan; Malecki, Jan Grzegorz |
| Journal of publication | The Journal of organic chemistry |
| Year of publication | 2020 |
| a | 18.6292 ± 0.0011 Å |
| b | 12.8456 ± 0.0008 Å |
| c | 25.5273 ± 0.0014 Å |
| α | 90° |
| β | 106.687 ± 0.006° |
| γ | 90° |
| Cell volume | 5851.5 ± 0.6 Å3 |
| Cell temperature | 295 ± 2 K |
| Ambient diffraction temperature | 295 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | I 1 2/a 1 |
| Hall space group symbol | -I 2ya |
| Residual factor for all reflections | 0.0676 |
| Residual factor for significantly intense reflections | 0.0452 |
| Weighted residual factors for significantly intense reflections | 0.1164 |
| Weighted residual factors for all reflections included in the refinement | 0.1299 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 252185 (current) | 2020-05-20 | cif/ Adding structures of 4038396 via cif-deposit CGI script. |
4038396.cif |
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