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Information card for entry 4038399
Preview
| Coordinates | 4038399.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C44 H40 O5 P2 |
|---|---|
| Calculated formula | C44 H40 O5 P2 |
| Title of publication | Concise Synthesis of Phospholene and Its P-Stereogenic Derivatives. |
| Authors of publication | Hu, Wei; Li, Er-Qing; Duan, Zheng; Mathey, François |
| Journal of publication | The Journal of organic chemistry |
| Year of publication | 2020 |
| a | 20.6268 ± 0.0012 Å |
| b | 8.2898 ± 0.0009 Å |
| c | 11.4377 ± 0.0006 Å |
| α | 90° |
| β | 101.734 ± 0.005° |
| γ | 90° |
| Cell volume | 1914.9 ± 0.3 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.05 |
| Residual factor for significantly intense reflections | 0.0452 |
| Weighted residual factors for significantly intense reflections | 0.1218 |
| Weighted residual factors for all reflections included in the refinement | 0.1291 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.074 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 252219 (current) | 2020-05-21 | cif/ Adding structures of 4038399 via cif-deposit CGI script. |
4038399.cif |
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Users of the data should acknowledge the original authors of the
structural data.