Crystallography Open Database

Information card for entry 4064699

Preview

Coordinates	4064699.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Pt-complex
Chemical name	Pt-complex
Formula	C19 H24 N2 O4 Pt S
Calculated formula	C19 H24 N2 O4 Pt S
Title of publication	Allylic C‒H Deprotonation of Olefins with PtII(OH) to Form η3-Allyl PtIIComplexes in Water and Aprotic Organic Solvents
Authors of publication	Khusnutdinova, Julia R.; Zavalij, Peter Y.; Vedernikov, Andrei N.
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	12
Pages of publication	3392
a	9.3702 ± 0.0009 Å
b	9.502 ± 0.0009 Å
c	11.3905 ± 0.0011 Å
α	72.504 ± 0.002°
β	88.877 ± 0.002°
γ	81.837 ± 0.002°
Cell volume	957.16 ± 0.16 Å³
Cell temperature	220 ± 2 K
Ambient diffraction temperature	220 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0334
Residual factor for significantly intense reflections	0.0295
Weighted residual factors for significantly intense reflections	0.075
Weighted residual factors for all reflections included in the refinement	0.0771
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178540 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/46.	4064699.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064699.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064699.cif
33008	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064699 via cif-deposit CGI script.	4064699.cif