Crystallography Open Database

Information card for entry 4064707

Preview

Coordinates	4064707.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H46 Ge N4 S4 Si2
Calculated formula	C30 H46 Ge N4 S4 Si2
SMILES	C(C)(C)(N1C(c2ccccc2)=[N](C(C)(C)C)[Si]1(=S)S[Ge]S[Si]1([N](C(C)(C)C)=C(c2ccccc2)N1C(C)(C)C)=S)C
Title of publication	Synthesis and Characterization of an Amidinate-Stabilized Siladithiocarboxylate and Its Germanium(II) Complex
Authors of publication	Zhang, Shu-Hua; Xi, Hong-Wei; Lim, Kok Hwa; So, Cheuk-Wai
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	13
Pages of publication	3686
a	24.1519 ± 0.0004 Å
b	8.7472 ± 0.0001 Å
c	17.9561 ± 0.0003 Å
α	90°
β	110.329 ± 0.001°
γ	90°
Cell volume	3557.15 ± 0.1 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0638
Residual factor for significantly intense reflections	0.0352
Weighted residual factors for significantly intense reflections	0.0852
Weighted residual factors for all reflections included in the refinement	0.1053
Goodness-of-fit parameter for all reflections included in the refinement	1.094
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178541 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/47.	4064707.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064707.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064707.cif
33011	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064706, 4064707 via cif-deposit CGI script.	4064707.cif