Crystallography Open Database

Information card for entry 4064712

Preview

Coordinates	4064712.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H38 O Os P2
Calculated formula	C24 H38 O Os P2
Title of publication	Direct Access to POP-Type Osmium(II) and Osmium(IV) Complexes: Osmium a Promising Alternative to Ruthenium for the Synthesis of Imines from Alcohols and Amines
Authors of publication	Esteruelas, Miguel A.; Honczek, Nicole; Oliván, Montserrat; Oñate, Enrique; Valencia, Marta
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	9
Pages of publication	2468
a	21.0249 ± 0.001 Å
b	9.6249 ± 0.0005 Å
c	11.681 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	2363.8 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0216
Residual factor for significantly intense reflections	0.0183
Weighted residual factors for significantly intense reflections	0.0417
Weighted residual factors for all reflections included in the refinement	0.0429
Goodness-of-fit parameter for all reflections included in the refinement	1.125
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178541 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/47.	4064712.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064712.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064712.cif
33014	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064710, 4064711, 4064712 via cif-deposit CGI script.	4064712.cif