Crystallography Open Database

Information card for entry 4068961

Preview

Coordinates	4068961.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H56 Cl2 N2 O5 P2 Pd
Calculated formula	C40 H56 Cl2 N2 O5 P2 Pd
Title of publication	Diphosphination of Electron Poor Alkenes
Authors of publication	Hajdók, Imre; Lissner, Falk; Nieger, Martin; Strobel, Sabine; Gudat, Dietrich
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	6
Pages of publication	1644
a	11.1613 ± 0.0002 Å
b	14.9247 ± 0.0004 Å
c	24.853 ± 0.0006 Å
α	90°
β	92.592 ± 0.002°
γ	90°
Cell volume	4135.75 ± 0.17 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1268
Residual factor for significantly intense reflections	0.0685
Weighted residual factors for significantly intense reflections	0.1209
Weighted residual factors for all reflections included in the refinement	0.1373
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178579 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/89.	4068961.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4068961.cif
40063	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4068961 via cif-deposit CGI script.	4068961.cif