Crystallography Open Database

Information card for entry 4068976

Preview

Coordinates	4068976.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40.5 H57 N Ni P2 Si
Calculated formula	C40.5 H57 N Ni P2 Si
Title of publication	Mild Protocol for the Synthesis of Stable Nickel Complexes Having Primary and Secondary Silyl Ligands
Authors of publication	Adhikari, Debashis; Pink, Maren; Mindiola, Daniel J.
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	7
Pages of publication	2072
a	24.9191 ± 0.0013 Å
b	10.3235 ± 0.0005 Å
c	31.4006 ± 0.0016 Å
α	90°
β	110.577 ± 0.003°
γ	90°
Cell volume	7562.5 ± 0.7 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0486
Residual factor for significantly intense reflections	0.0351
Weighted residual factors for significantly intense reflections	0.0964
Weighted residual factors for all reflections included in the refinement	0.1021
Goodness-of-fit parameter for all reflections included in the refinement	0.86
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4068976.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4068976.cif
40072	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4068976 via cif-deposit CGI script.	4068976.cif