Crystallography Open Database

Information card for entry 4068986

Preview

Coordinates	4068986.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H68 N3 O2 Si4 Y
Calculated formula	C39 H68 N3 O2 Si4 Y
Title of publication	Bis- and Mono(amidate) Complexes of Yttrium: Synthesis, Characterization, and Use as Precatalysts for the Hydroamination of Aminoalkenes
Authors of publication	Stanlake, Louisa J. E.; Schafer, Laurel L.
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	14
Pages of publication	3990
a	11.6377 ± 0.0014 Å
b	19.076 ± 0.002 Å
c	20.423 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	4533.9 ± 0.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0877
Residual factor for significantly intense reflections	0.0466
Weighted residual factors for significantly intense reflections	0.0787
Weighted residual factors for all reflections included in the refinement	0.089
Goodness-of-fit parameter for all reflections included in the refinement	0.998
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178579 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/89.	4068986.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4068986.cif
40076	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4068986 via cif-deposit CGI script.	4068986.cif