Crystallography Open Database

Information card for entry 4075166

Preview

Coordinates	4075166.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H30 N Ta
Calculated formula	C27 H30 N3 Ta3
Title of publication	Neutral and Cationic Alkyl Tantalum Imido Complexes: Synthesis and Migratory Insertion Reactions.
Authors of publication	Anderson, Laura L.; Schmidt, Joseph A. R.; Arnold, John; Bergman, Robert G.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	14
Pages of publication	3394 - 3406
a	11.1584 ± 0.0004 Å
b	11.1584 ± 0.0004 Å
c	10.1563 ± 0.0005 Å
α	90°
β	90°
γ	120°
Cell volume	1095.14 ± 0.08 Å³
Cell temperature	133.2 K
Ambient diffraction temperature	133.2 K
Number of distinct elements	4
Space group number	159
Hermann-Mauguin space group symbol	P 3 1 c
Hall space group symbol	P 3 -2c
Residual factor for all reflections	0.0258
Residual factor for significantly intense reflections	0.0239
Weighted residual factors for all reflections	0.0315
Weighted residual factors for significantly intense reflections	0.0307
Goodness-of-fit parameter for all reflections included in the refinement	1.253
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4075166.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075166.cif
49094	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4075166 via cif-deposit CGI script.	4075166.cif