Crystallography Open Database

Information card for entry 4075197

Preview

Coordinates	4075197.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	NOTE: This is compound 1
Formula	C30 H42 Ge2
Calculated formula	C30 H42 Ge2
SMILES	[Ge]([Ge](CCCC)(CCCC)CCCC)(c1ccccc1)(c1ccccc1)c1ccccc1
Title of publication	Preparation of Oligogermanes via the Hydrogermolysis Reaction
Authors of publication	Subashi, Esla; Rheingold, Arnold L.; Weinert, Charles S.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	13
Pages of publication	3211
a	10.051 ± 0.003 Å
b	15.141 ± 0.004 Å
c	20.97 ± 0.006 Å
α	109.043 ± 0.004°
β	100.239 ± 0.004°
γ	98.645 ± 0.004°
Cell volume	2893.2 ± 1.4 Å³
Cell temperature	215 ± 2 K
Ambient diffraction temperature	215 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0832
Residual factor for significantly intense reflections	0.0485
Weighted residual factors for significantly intense reflections	0.1199
Weighted residual factors for all reflections included in the refinement	0.14
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178640 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/51.	4075197.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075197.cif
49114	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4075197, 4075198 via cif-deposit CGI script.	4075197.cif