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Information card for entry 4086447
Preview
| Coordinates | 4086447.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | KM3-Pd |
|---|---|
| Formula | C33.33 H55.33 Cl5.98 P2 Pd |
| Calculated formula | C33.327 H55.327 Cl5.981 P2 Pd |
| Title of publication | Streamlined Preparation and Coordination Chemistry of Hybrid Phosphine‒Phosphaalkene Ligands |
| Authors of publication | Magnuson, Kevin W.; Oshiro, Shelly M.; Gurr, Joshua R.; Yoshida, Wesley Y.; Gembicky, Milan; Rheingold, Arnold L.; Hughes, Russell P.; Cain, Matthew F. |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 6 |
| Pages of publication | 855 - 859 |
| a | 14.5058 ± 0.0006 Å |
| b | 15.1344 ± 0.0007 Å |
| c | 19.3313 ± 0.0011 Å |
| α | 90° |
| β | 106.901 ± 0.003° |
| γ | 90° |
| Cell volume | 4060.6 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100.15 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1092 |
| Residual factor for significantly intense reflections | 0.0637 |
| Weighted residual factors for significantly intense reflections | 0.1498 |
| Weighted residual factors for all reflections included in the refinement | 0.1755 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.038 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181379 (current) | 2016-04-04 | cif/4/08/64/ Fixing incorrectly interpreted character in paper title of entries 408644[789] and 408645[01]. |
4086447.cif |
| 181374 | 2016-04-04 | cif/ Adding structures of 4086447 via cif-deposit CGI script. |
4086447.cif |
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Users of the data should acknowledge the original authors of the
structural data.