Crystallography Open Database

Information card for entry 4086448

Preview

Coordinates	4086448.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H57 Cl2 N P2 Pt
Calculated formula	C34 H57 Cl2 N P2 Pt
Title of publication	Streamlined Preparation and Coordination Chemistry of Hybrid Phosphine‒Phosphaalkene Ligands
Authors of publication	Magnuson, Kevin W.; Oshiro, Shelly M.; Gurr, Joshua R.; Yoshida, Wesley Y.; Gembicky, Milan; Rheingold, Arnold L.; Hughes, Russell P.; Cain, Matthew F.
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	6
Pages of publication	855 - 859
a	17.151 ± 0.003 Å
b	15.554 ± 0.002 Å
c	28.094 ± 0.004 Å
α	90°
β	103.916 ± 0.003°
γ	90°
Cell volume	7274.6 ± 1.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	I 1 2/a 1
Hall space group symbol	-I 2ya
Residual factor for all reflections	0.0771
Residual factor for significantly intense reflections	0.0553
Weighted residual factors for significantly intense reflections	0.1285
Weighted residual factors for all reflections included in the refinement	0.1388
Goodness-of-fit parameter for all reflections included in the refinement	1.112
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
181379 (current)	2016-04-04	cif/4/08/64/ Fixing incorrectly interpreted character in paper title of entries 408644[789] and 408645[01].	4086448.cif
181375	2016-04-04	cif/ Adding structures of 4086448 via cif-deposit CGI script.	4086448.cif