#------------------------------------------------------------------------------ #$Date: 2016-05-04 19:17:06 +0300 (Wed, 04 May 2016) $ #$Revision: 182519 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/08/64/4086452.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4086452 loop_ _publ_author_name 'Seow, Celestine' 'Xi, Hong-Wei' 'Li, Yongxin' 'So, Cheuk-Wai' _publ_section_title ; Synthesis of a Germylidenide Anion from the C--C Bond Activation of a Bis(germylene) ; _journal_issue 8 _journal_name_full Organometallics _journal_page_first 1060 _journal_paper_doi 10.1021/acs.organomet.5b01001 _journal_volume 35 _journal_year 2016 _chemical_absolute_configuration ad _chemical_formula_sum 'C32 H46 Ge2 N4' _chemical_formula_weight 631.91 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _atom_sites_solution_hydrogens geom _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.5992(6) _cell_length_b 18.2258(12) _cell_length_c 20.4920(14) _cell_measurement_reflns_used 920 _cell_measurement_temperature 103.(2) _cell_measurement_theta_max 33.2787 _cell_measurement_theta_min 0.3456 _cell_volume 3211.7(4) _computing_cell_refinement 'APEX3 v2015.9-0 (Bruker AXS)' _computing_data_collection 'APEX3 (Bruker AXS Inc., 2015)' _computing_data_reduction 'SAINT (Bruker AXS Inc., 2014)' _computing_molecular_graphics 'XP (Bruker AXS Inc., 2015)' _computing_publication_material 'APEX3 (Bruker AXS Inc., 2015)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT (Bruker AXS Inc., 2015)' _diffrn_ambient_temperature 103.(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0444 _diffrn_reflns_av_unetI/netI 0.0642 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 26890 _diffrn_reflns_theta_full 31.11 _diffrn_reflns_theta_max 31.11 _diffrn_reflns_theta_min 2.80 _diffrn_source 'fine-focus sealed tube' _diffrn_source_type 'Bruker KappaCCD' _exptl_absorpt_coefficient_mu 1.897 _exptl_absorpt_correction_T_max 0.70 _exptl_absorpt_correction_T_min 0.54 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 - Bruker AXS area detector scaling and absorption correction ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.307 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1320 _exptl_crystal_size_max 0.420 _exptl_crystal_size_mid 0.220 _exptl_crystal_size_min 0.200 _refine_diff_density_max 0.589 _refine_diff_density_min -0.339 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.129(9) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.991 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 356 _refine_ls_number_reflns 10261 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.991 _refine_ls_R_factor_all 0.0494 _refine_ls_R_factor_gt 0.0353 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0258P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0646 _refine_ls_wR_factor_ref 0.0684 _reflns_number_gt 8637 _reflns_number_total 10261 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file om5b01001_si_002.cif _cod_data_source_block scw985 _cod_depositor_comments ; The following automatic conversions were performed: '_exptl_absorpt_correction_type' value 'Multi-Scan' changed to 'multi-scan' according to /usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26. Automatic conversion script Id: cif_fix_values 4268 2015-11-12 08:31:59Z antanas Adding full bibliography for 4086452--4086454.cif. ; _cod_database_code 4086452 _shelx_res_file ; scw985.res created by SHELXL-2014/7 TITL scw985 in P2(1)2(1)2(1) CELL 0.71073 8.59920 18.22580 20.49200 90.0000 90.0000 90.0000 ZERR 4.00 0.00060 0.00120 0.00140 0.0000 0.0000 0.0000 LATT -1 SYMM 0.5-X, -Y, 0.5+Z SYMM -X, 0.5+Y, 0.5-Z SYMM 0.5+X, 0.5-Y, -Z SFAC C H N Ge UNIT 128 184 16 8 L.S. 4 ACTA BOND FMAP 2 twin PLAN 5 SIZE 0.20 0.22 0.42 TEMP -170 WGHT 0.025800 BASF 0.12924 FVAR 0.12080 MOLE 1 GE1 4 0.134886 0.762974 0.746951 11.00000 0.01282 0.01758 = 0.01336 0.00397 -0.00058 -0.00316 GE2 4 0.028059 0.869935 0.654381 11.00000 0.00913 0.01391 = 0.01220 0.00184 0.00118 -0.00169 C1 1 -0.001393 0.683689 0.781573 11.00000 0.01858 0.01445 = 0.01273 0.00056 0.00162 -0.00351 C2 1 0.024569 0.634345 0.833152 11.00000 0.02293 0.01637 = 0.01288 0.00188 0.00258 -0.00014 C3 1 0.164124 0.640933 0.874031 11.00000 0.02441 0.01953 = 0.01304 0.00554 0.00092 0.00258 AFIX 43 H3 2 0.200206 0.599513 0.897755 11.00000 -1.20000 AFIX 0 C4 1 0.380222 0.708485 0.917239 11.00000 0.01978 0.02133 = 0.01826 0.00260 -0.00269 -0.00177 C5 1 0.338311 0.757432 0.975190 11.00000 0.03095 0.03631 = 0.02011 -0.00491 0.00045 -0.00258 AFIX 137 H5A 2 0.261846 0.732330 1.002740 11.00000 -1.50000 H5B 2 0.294121 0.803626 0.959214 11.00000 -1.50000 H5C 2 0.432094 0.767725 1.000773 11.00000 -1.50000 AFIX 0 C6 1 0.450473 0.636801 0.941398 11.00000 0.02560 0.02993 = 0.02993 0.00552 -0.00738 -0.00095 AFIX 137 H6A 2 0.470036 0.604329 0.904175 11.00000 -1.50000 H6B 2 0.377986 0.612978 0.971611 11.00000 -1.50000 H6C 2 0.548627 0.646946 0.963962 11.00000 -1.50000 AFIX 0 C7 1 0.497647 0.748077 0.873348 11.00000 0.02395 0.03669 = 0.02410 0.00378 0.00280 -0.00617 AFIX 137 H7A 2 0.453906 0.795079 0.859115 11.00000 -1.50000 H7B 2 0.520261 0.717615 0.835099 11.00000 -1.50000 H7C 2 0.593852 0.756852 0.897768 11.00000 -1.50000 AFIX 0 C8 1 -0.084120 0.578521 0.844711 11.00000 0.02970 0.01509 = 0.01303 0.00251 0.00412 -0.00113 AFIX 43 H8 2 -0.064239 0.543016 0.877611 11.00000 -1.20000 AFIX 0 C9 1 -0.219269 0.574567 0.808948 11.00000 0.02688 0.01639 = 0.01868 -0.00086 0.00645 -0.00984 AFIX 43 H9 2 -0.294080 0.537855 0.818822 11.00000 -1.20000 AFIX 0 C10 1 -0.247500 0.624076 0.758219 11.00000 0.01967 0.01736 = 0.01538 -0.00212 0.00194 -0.00218 AFIX 43 H10 2 -0.340977 0.621650 0.733606 11.00000 -1.20000 AFIX 0 C11 1 -0.135485 0.676990 0.744620 11.00000 0.01740 0.01268 = 0.01157 -0.00021 0.00327 0.00093 C12 1 -0.153257 0.736856 0.693584 11.00000 0.01171 0.01380 = 0.01282 -0.00117 0.00126 -0.00335 AFIX 13 H12 2 -0.232737 0.723457 0.660013 11.00000 -1.20000 AFIX 0 C13 1 0.046795 0.710180 0.604913 11.00000 0.02003 0.01583 = 0.01198 -0.00106 0.00169 0.00266 C14 1 -0.053560 0.730976 0.546232 11.00000 0.03307 0.02377 = 0.01313 -0.00099 0.00048 0.00457 AFIX 137 H14A 2 -0.041680 0.783461 0.537113 11.00000 -1.50000 H14B 2 -0.162838 0.720238 0.555876 11.00000 -1.50000 H14C 2 -0.020532 0.702567 0.508067 11.00000 -1.50000 AFIX 0 C15 1 0.031323 0.627832 0.618818 11.00000 0.03621 0.01529 = 0.02098 -0.00226 0.00494 0.00361 AFIX 137 H15A 2 -0.077890 0.615932 0.627463 11.00000 -1.50000 H15B 2 0.094387 0.615030 0.656990 11.00000 -1.50000 H15C 2 0.067583 0.599906 0.580889 11.00000 -1.50000 AFIX 0 C16 1 0.216528 0.727202 0.589399 11.00000 0.02427 0.02903 = 0.02495 -0.00438 0.01047 0.00339 AFIX 137 H16A 2 0.281215 0.715507 0.627373 11.00000 -1.50000 H16B 2 0.227234 0.779398 0.578828 11.00000 -1.50000 H16C 2 0.250161 0.697636 0.552031 11.00000 -1.50000 AFIX 0 C17 1 -0.198955 0.808597 0.730659 11.00000 0.01225 0.01332 = 0.01372 -0.00119 0.00222 -0.00241 AFIX 13 H17 2 -0.261885 0.797617 0.770517 11.00000 -1.20000 AFIX 0 C18 1 -0.288579 0.855679 0.682960 11.00000 0.01163 0.01274 = 0.01680 -0.00377 0.00127 -0.00191 C19 1 -0.449372 0.862007 0.682013 11.00000 0.01116 0.01938 = 0.02298 -0.00201 0.00463 -0.00407 AFIX 43 H19 2 -0.510553 0.839536 0.715037 11.00000 -1.20000 AFIX 0 C20 1 -0.519923 0.901667 0.632107 11.00000 0.00832 0.02164 = 0.03358 -0.00460 0.00345 0.00187 AFIX 43 H20 2 -0.629752 0.907233 0.631357 11.00000 -1.20000 AFIX 0 C21 1 -0.429542 0.933093 0.583407 11.00000 0.01467 0.01527 = 0.02326 0.00019 -0.00260 0.00000 AFIX 43 H21 2 -0.478092 0.960469 0.549624 11.00000 -1.20000 AFIX 0 C22 1 -0.268573 0.924933 0.583532 11.00000 0.01153 0.01113 = 0.01795 -0.00255 0.00132 -0.00283 C23 1 -0.196121 0.886583 0.634253 11.00000 0.01195 0.01353 = 0.01456 -0.00220 0.00258 -0.00199 C24 1 -0.177240 0.956569 0.529252 11.00000 0.01228 0.01320 = 0.01542 -0.00103 -0.00371 0.00112 AFIX 43 H24 2 -0.226450 0.990264 0.500535 11.00000 -1.20000 AFIX 0 C25 1 0.052707 0.973290 0.465052 11.00000 0.01582 0.02411 = 0.01302 0.00344 0.00089 0.00088 C26 1 0.047067 0.919101 0.408646 11.00000 0.04085 0.04684 = 0.02566 -0.00970 0.01352 -0.01502 AFIX 137 H26A 2 -0.060959 0.912500 0.394586 11.00000 -1.50000 H26B 2 0.089631 0.871842 0.422833 11.00000 -1.50000 H26C 2 0.108894 0.938050 0.372178 11.00000 -1.50000 AFIX 0 C27 1 0.218848 0.980304 0.489592 11.00000 0.02028 0.05817 = 0.01950 0.00137 0.00319 -0.00961 AFIX 137 H27A 2 0.254190 0.932799 0.506382 11.00000 -1.50000 H27B 2 0.222973 1.016907 0.524581 11.00000 -1.50000 H27C 2 0.286500 0.995730 0.453635 11.00000 -1.50000 AFIX 0 C28 1 -0.007458 1.047818 0.442784 11.00000 0.03981 0.03916 = 0.04260 0.02558 0.01520 0.00536 AFIX 137 H28A 2 -0.019792 1.080033 0.480722 11.00000 -1.50000 H28B 2 -0.108162 1.041626 0.421083 11.00000 -1.50000 H28C 2 0.066878 1.069736 0.412222 11.00000 -1.50000 AFIX 0 C29 1 -0.047533 0.894867 0.804015 11.00000 0.02611 0.01874 = 0.01144 -0.00366 0.00109 -0.00549 C30 1 -0.078575 0.853383 0.867611 11.00000 0.03883 0.02845 = 0.01374 -0.00247 0.00185 -0.00992 AFIX 137 H30A 2 -0.000894 0.814499 0.872940 11.00000 -1.50000 H30B 2 -0.182711 0.831601 0.866137 11.00000 -1.50000 H30C 2 -0.072003 0.887480 0.904487 11.00000 -1.50000 AFIX 0 C31 1 -0.170202 0.954509 0.794592 11.00000 0.04779 0.01947 = 0.02833 -0.01113 -0.00345 0.00215 AFIX 137 H31A 2 -0.272867 0.931756 0.789955 11.00000 -1.50000 H31B 2 -0.146141 0.982839 0.755218 11.00000 -1.50000 H31C 2 -0.170326 0.987211 0.832554 11.00000 -1.50000 AFIX 0 C32 1 0.113262 0.929976 0.808614 11.00000 0.03449 0.02931 = 0.02161 -0.00751 0.00103 -0.01639 AFIX 137 H32A 2 0.137254 0.955076 0.767537 11.00000 -1.50000 H32B 2 0.191261 0.891861 0.816773 11.00000 -1.50000 H32C 2 0.114499 0.965531 0.844487 11.00000 -1.50000 AFIX 0 N1 3 -0.000782 0.754877 0.663089 11.00000 0.01166 0.01481 = 0.01067 0.00041 0.00378 -0.00085 N2 3 -0.046437 0.842306 0.747837 11.00000 0.01307 0.01470 = 0.01258 -0.00127 0.00240 -0.00518 N3 3 0.236900 0.701094 0.878047 11.00000 0.02012 0.02036 = 0.01564 0.00271 0.00001 -0.00223 N4 3 -0.036997 0.940545 0.519701 11.00000 0.01373 0.01966 = 0.01425 0.00225 0.00061 -0.00011 HKLF 4 REM scw985 in P2(1)2(1)2(1) REM R1 = 0.0353 for 8637 Fo > 4sig(Fo) and 0.0494 for all 10261 data REM 356 parameters refined using 0 restraints END WGHT 0.0258 0.0000 REM Highest difference peak 0.589, deepest hole -0.339, 1-sigma level 0.078 Q1 1 -0.0354 0.8686 0.6251 11.00000 0.05 0.51 Q2 1 0.0965 0.8733 0.6251 11.00000 0.05 0.48 Q3 1 0.0569 0.8986 0.6238 11.00000 0.05 0.46 Q4 1 0.2126 0.7632 0.7199 11.00000 0.05 0.46 Q5 1 0.2345 0.7576 0.7555 11.00000 0.05 0.45 ; _shelx_res_checksum 73289 _shelx_hkl_file ; 3 0 0 -0.09 0.08 4 0 0 201.43 8.14 5 0 0 -0.09 0.17 6 0 0 87.97 3.63 7 0 0 -0.60 0.22 9 0 0 -0.78 0.96 10 0 0 37.59 2.67 11 0 0 0.85 1.47 2 1 0 47.75 1.99 3 1 0 5.20 0.34 4 1 0 5.72 0.40 5 1 0 5.01 0.40 5 -1 0 4.67 0.27 6 1 0 1.77 0.32 7 1 0 0.39 0.31 8 1 0 41.87 2.36 9 1 0 27.80 2.01 10 -1 0 71.85 4.10 10 1 0 77.87 3.96 11 -1 0 9.00 1.89 11 1 0 10.59 1.70 12 -1 0 0.11 1.62 12 1 0 1.10 1.72 -1 2 0 180.22 6.92 1 -2 0 169.86 6.81 1 2 0 170.29 6.95 1 -2 0 170.94 6.93 -1 -2 0 178.41 6.95 -1 -2 0 178.07 6.81 1 2 0 143.75 6.80 2 2 0 0.82 0.22 2 2 0 1.85 0.25 2 -2 0 1.47 0.18 3 2 0 38.91 1.73 3 -2 0 39.66 1.64 3 2 0 40.45 1.76 4 2 0 62.10 2.69 4 -2 0 59.85 2.51 4 2 0 62.51 2.62 5 2 0 3.92 0.57 5 2 0 3.02 0.38 6 2 0 40.63 2.07 6 2 0 41.50 1.87 7 2 0 6.42 0.89 7 2 0 4.94 0.54 8 2 0 61.98 3.13 9 2 0 5.40 1.17 10 2 0 6.52 1.36 11 -2 0 1.03 1.69 11 2 0 3.38 1.42 12 2 0 5.16 1.91 12 -2 0 7.50 2.06 0 3 0 -0.13 0.13 0 -3 0 -0.22 0.17 0 -3 0 -0.18 0.15 0 -3 0 -0.31 0.13 -1 3 0 56.54 2.36 1 3 0 57.80 2.36 -1 -3 0 54.73 2.45 1 -3 0 59.00 2.43 -1 -3 0 58.77 2.36 1 3 0 58.46 2.42 1 3 0 58.86 2.46 1 -3 0 56.47 2.35 2 3 0 19.51 0.91 2 -3 0 21.31 0.93 2 3 0 19.71 0.97 -2 -3 0 19.42 0.97 3 -3 0 15.12 0.71 3 3 0 15.32 0.80 3 3 0 13.35 0.77 4 3 0 55.80 2.38 4 -3 0 52.20 2.25 4 3 0 54.04 2.37 5 3 0 17.31 1.05 5 3 0 15.90 0.94 5 -3 0 16.40 0.77 6 3 0 94.51 4.21 6 3 0 98.17 4.12 7 3 0 8.88 1.01 8 3 0 8.76 1.13 9 3 0 45.18 2.59 10 3 0 0.19 1.05 11 3 0 6.49 1.84 11 -3 0 6.09 1.78 12 -3 0 9.48 2.10 12 3 0 13.25 2.46 0 4 0 38.81 1.68 0 -4 0 38.84 1.77 1 -4 0 1.53 0.28 1 -4 0 2.84 0.25 1 4 0 2.20 0.26 -1 4 0 1.84 0.24 -1 -4 0 1.66 0.31 1 4 0 2.36 0.29 -2 -4 0 397.02 15.94 2 4 0 390.98 15.62 2 -4 0 389.08 15.89 3 -4 0 1.04 0.27 3 4 0 2.38 0.33 -3 -4 0 1.25 0.32 4 4 0 378.11 15.08 4 -4 0 359.54 14.96 4 4 0 371.86 14.82 5 4 0 9.92 0.76 5 -4 0 8.69 0.56 5 4 0 9.51 0.77 6 4 0 3.74 0.67 6 4 0 3.37 0.55 7 4 0 0.43 0.66 8 4 0 41.08 2.26 9 4 0 3.91 1.06 10 4 0 -0.80 0.98 11 4 0 -1.57 1.54 12 4 0 4.15 1.95 12 -4 0 0.89 1.81 0 -5 0 -0.28 0.25 0 5 0 -0.13 0.19 -1 5 0 0.66 0.22 -1 -5 0 -0.03 0.27 1 -5 0 -0.17 0.25 1 5 0 0.64 0.21 1 5 0 0.14 0.24 2 -5 0 24.57 1.23 -2 -5 0 24.38 1.26 2 5 0 25.84 1.14 2 5 0 24.68 1.28 3 -5 0 12.35 0.71 3 5 0 10.48 0.65 -3 -5 0 11.45 0.77 -4 -5 0 7.85 0.63 4 -5 0 6.37 0.54 4 5 0 7.68 0.61 5 -5 0 54.78 2.39 5 5 0 54.78 2.46 6 -5 0 176.52 7.14 6 5 0 170.13 7.19 7 5 0 7.76 0.88 8 5 0 33.23 1.94 9 5 0 1.24 0.89 10 5 0 -0.14 0.98 10 5 0 -0.49 1.39 11 5 0 7.69 1.98 12 5 0 41.50 3.64 0 6 0 486.58 19.02 0 -6 0 466.92 19.40 -1 6 0 62.89 2.69 -1 -6 0 62.75 2.85 1 -6 0 65.18 2.84 1 6 0 66.12 2.73 1 6 0 63.61 2.77 2 6 0 0.37 0.26 2 6 0 0.01 0.38 2 -6 0 -0.17 0.29 -2 -6 0 -0.11 0.34 -2 6 0 0.38 0.25 3 6 0 262.17 10.85 -3 -6 0 269.42 10.95 3 6 0 267.10 10.67 3 -6 0 263.83 10.89 -4 -6 0 68.57 3.03 4 6 0 69.40 2.91 4 -6 0 65.94 2.97 5 6 0 38.06 1.80 5 -6 0 38.13 1.78 6 6 0 6.29 0.74 6 -6 0 6.01 0.59 7 6 0 5.20 0.81 8 6 0 33.29 1.91 9 6 0 0.22 0.83 9 6 0 0.22 1.31 10 6 0 1.15 1.58 11 6 0 -0.48 1.70 12 6 0 -0.70 1.87 0 -7 0 -0.08 0.28 0 7 0 -0.07 0.28 1 7 0 10.43 0.66 1 -7 0 8.56 0.76 1 7 0 9.53 0.71 -1 7 0 10.32 0.64 -1 -7 0 9.69 0.73 2 7 0 124.95 5.32 -2 -7 0 126.59 5.41 2 7 0 125.80 5.19 2 -7 0 129.89 5.37 -2 7 0 124.96 5.20 -3 -7 0 51.83 2.37 3 -7 0 48.62 2.31 3 7 0 51.37 2.41 3 7 0 48.56 2.18 4 7 0 1.48 0.65 4 -7 0 0.89 0.41 -4 -7 0 2.32 0.52 4 7 0 1.28 0.38 5 7 0 100.52 4.59 5 7 0 98.44 4.24 5 -7 0 103.20 4.33 6 -7 0 12.28 0.93 6 7 0 11.98 0.95 6 7 0 13.23 1.43 7 7 0 17.62 1.78 7 7 0 16.52 1.23 8 7 0 33.03 1.90 8 7 0 32.41 2.57 9 7 0 2.24 1.48 9 7 0 4.03 0.95 10 7 0 32.27 2.90 11 7 0 9.10 2.07 12 7 0 -0.87 1.79 0 -8 0 455.02 18.69 0 8 0 458.27 18.28 -1 -8 0 8.75 0.85 1 8 0 8.91 0.77 -1 8 0 8.92 0.67 1 8 0 9.82 0.74 1 -8 0 10.22 0.85 2 -8 0 132.57 5.62 -2 -8 0 130.66 5.66 2 8 0 131.91 5.42 -2 8 0 133.79 5.43 2 8 0 127.59 5.54 3 8 0 37.68 2.01 -3 -8 0 41.48 2.05 3 -8 0 38.96 1.95 3 8 0 38.94 1.80 4 -8 0 2.97 0.57 -4 -8 0 3.23 0.66 4 8 0 4.29 0.81 4 8 0 4.35 0.53 5 -8 0 19.16 1.18 5 8 0 17.45 1.10 5 8 0 19.48 1.58 -5 -8 0 20.03 1.27 6 8 0 72.29 3.20 6 8 0 73.59 3.69 6 -8 0 72.92 3.28 7 8 0 40.58 2.08 7 8 0 42.62 2.70 8 8 0 18.09 1.35 8 8 0 18.09 2.04 9 8 0 6.81 1.70 10 8 0 12.73 2.13 11 8 0 -0.79 1.79 0 9 0 0.18 0.40 0 -9 0 0.23 0.49 1 9 0 49.21 2.32 1 -9 0 53.15 2.46 -1 9 0 51.83 2.25 1 9 0 48.81 2.28 -1 -9 0 46.87 2.45 2 9 0 132.04 5.82 -2 -9 0 140.94 5.99 -2 9 0 136.92 5.71 2 9 0 143.74 5.73 2 -9 0 135.82 5.92 3 9 0 34.62 1.87 3 9 0 34.26 1.64 3 -9 0 32.52 1.78 -3 -9 0 35.18 1.87 -4 -9 0 12.10 1.04 4 -9 0 10.58 0.96 4 9 0 9.96 1.11 4 9 0 11.38 0.82 5 9 0 -0.04 0.45 5 9 0 0.09 0.62 -5 -9 0 0.07 0.56 5 -9 0 0.17 0.51 6 9 0 7.76 1.13 6 9 0 7.97 0.81 6 -9 0 8.97 0.89 7 9 0 11.36 1.47 7 9 0 11.91 1.04 7 -9 0 12.90 1.06 8 9 0 49.15 3.13 8 9 0 45.12 2.35 9 9 0 39.80 3.14 10 9 0 77.36 4.66 11 9 0 1.43 1.47 0 10 0 282.57 11.55 0 -10 0 287.64 11.90 -1 -10 0 188.85 8.07 -1 10 0 190.00 7.74 1 -10 0 186.45 8.04 1 10 0 190.97 7.83 2 10 0 52.29 2.46 -2 10 0 48.35 2.29 2 10 0 50.87 2.32 -2 -10 0 49.27 2.54 2 -10 0 50.10 2.49 3 -10 0 0.22 0.52 3 10 0 -0.92 0.55 -3 -10 0 0.55 0.60 -3 10 0 -0.10 0.42 3 10 0 0.03 0.43 4 10 0 12.50 0.90 4 10 0 13.55 1.19 -4 -10 0 14.98 1.28 4 -10 0 11.85 1.12 5 -10 0 4.12 0.76 5 10 0 2.62 0.98 5 10 0 3.00 0.59 -5 -10 0 2.02 0.74 6 10 0 34.53 2.38 6 -10 0 38.41 2.03 6 10 0 35.05 1.83 7 10 0 27.75 2.05 7 -10 0 25.80 1.67 7 10 0 26.22 1.55 8 10 0 4.97 1.54 9 10 0 9.13 1.63 10 10 0 10.99 2.13 11 10 0 7.99 2.29 0 11 0 0.42 0.44 0 -11 0 -0.82 0.59 -1 -11 0 8.59 1.03 -1 11 0 9.09 0.80 1 -11 0 8.69 0.98 1 11 0 8.69 0.87 -2 11 0 14.51 1.02 2 -11 0 13.16 1.20 -2 -11 0 16.11 1.32 2 11 0 14.20 1.07 2 11 0 14.07 1.18 3 11 0 16.24 1.32 3 -11 0 15.13 1.25 -3 -11 0 16.57 1.34 -3 11 0 15.53 1.09 3 11 0 14.89 1.03 4 11 0 32.60 2.04 4 -11 0 33.78 1.98 -4 -11 0 34.15 2.07 4 11 0 33.70 1.69 5 -11 0 0.88 0.71 5 11 0 0.76 0.56 -5 -11 0 1.15 0.69 5 11 0 0.39 0.90 6 11 0 64.84 3.44 6 -11 0 62.45 3.11 6 11 0 62.20 2.86 7 11 0 0.47 1.22 7 -11 0 0.02 0.70 7 11 0 -0.35 0.63 8 11 0 13.31 2.05 9 11 0 49.80 3.53 10 11 0 2.13 1.81 11 11 0 3.32 2.04 0 12 0 39.41 1.99 0 -12 0 38.31 2.22 -1 -12 0 48.70 2.60 -1 12 0 49.45 2.27 1 -12 0 45.78 2.47 1 12 0 48.41 2.37 -2 12 0 41.42 2.04 -2 -12 0 42.79 2.36 2 12 0 40.86 2.19 2 -12 0 40.22 2.28 3 -12 0 3.37 0.81 3 12 0 3.01 0.65 -3 12 0 2.76 0.63 -3 -12 0 3.38 0.87 3 12 0 3.99 0.87 4 -12 0 107.53 4.91 4 12 0 103.21 4.90 -4 -12 0 103.49 4.95 4 12 0 113.53 4.62 5 12 0 15.24 1.08 5 -12 0 9.92 1.15 5 12 0 13.43 1.48 -5 -12 0 12.75 1.37 6 12 0 2.35 0.69 6 -12 0 3.04 0.86 6 12 0 2.52 1.15 7 -12 0 80.65 3.87 7 12 0 79.00 4.29 8 12 0 9.03 1.83 9 12 0 3.73 1.79 10 12 0 0.07 1.81 11 12 0 4.27 2.17 0 13 0 0.15 0.52 0 -13 0 -0.34 0.57 1 -13 0 53.51 2.86 -1 -13 0 53.13 2.89 -1 13 0 55.34 2.57 1 13 0 53.21 2.62 -2 -13 0 2.26 0.90 -2 13 0 3.18 0.68 2 -13 0 3.45 0.91 2 13 0 2.81 0.80 3 13 0 8.50 0.93 -3 13 0 8.99 0.91 -3 -13 0 8.45 1.19 3 13 0 9.42 1.13 3 -13 0 7.62 1.10 4 13 0 38.17 1.97 4 -13 0 38.17 2.25 4 13 0 38.50 2.34 -4 -13 0 38.41 2.35 5 -13 0 84.83 4.06 5 13 0 83.18 3.71 5 13 0 79.79 4.13 -5 -13 0 86.53 4.15 6 -13 0 85.80 4.11 6 13 0 87.08 3.77 6 13 0 79.45 4.31 7 13 0 5.86 1.53 7 -13 0 3.07 1.01 8 13 0 25.68 2.56 9 13 0 0.45 1.67 10 13 0 11.78 2.39 0 14 0 10.73 1.03 0 -14 0 8.50 1.24 -1 14 0 3.32 0.71 1 14 0 3.38 0.82 1 -14 0 1.70 0.90 -1 -14 0 0.46 0.90 2 -14 0 8.57 1.16 -2 -14 0 6.43 1.17 -2 14 0 8.57 0.95 2 14 0 8.18 1.05 3 -14 0 37.51 2.29 -3 14 0 37.36 1.96 3 14 0 36.68 2.22 -3 -14 0 34.74 2.33 4 -14 0 21.10 1.74 4 14 0 21.85 1.46 -4 -14 0 20.72 1.79 4 14 0 21.09 1.79 5 14 0 45.23 2.32 5 14 0 45.99 2.82 5 -14 0 49.01 2.76 -5 -14 0 45.06 2.70 6 14 0 29.67 1.78 6 -14 0 28.36 2.16 6 14 0 34.21 2.48 7 14 0 6.37 1.63 7 -14 0 5.71 1.23 8 14 0 14.09 2.11 9 14 0 1.79 1.81 10 14 0 0.36 1.81 0 15 0 0.51 0.70 0 -15 0 0.07 0.95 1 -15 0 44.62 2.68 1 15 0 42.65 2.41 -1 -15 0 43.52 2.71 -1 15 0 47.14 2.33 2 15 0 -0.32 0.77 2 -15 0 0.04 0.88 -2 15 0 0.13 0.65 -2 -15 0 -1.11 0.93 3 -15 0 7.24 1.24 -3 -15 0 6.39 1.28 3 15 0 11.60 1.30 -3 15 0 8.57 0.98 -4 -15 0 17.40 1.71 4 15 0 15.04 1.61 4 -15 0 15.49 1.59 5 15 0 48.22 2.89 5 -15 0 50.03 2.93 5 15 0 46.48 2.40 -5 -15 0 43.31 2.80 6 15 0 9.10 1.40 6 -15 0 7.34 1.36 7 -15 0 17.46 1.75 7 15 0 18.43 2.18 8 15 0 0.72 1.68 9 15 0 1.55 1.90 10 15 0 2.08 2.06 0 16 0 122.15 5.36 0 -16 0 123.08 5.81 -1 -16 0 2.83 1.15 1 16 0 1.65 0.81 1 -16 0 2.58 0.92 -1 16 0 1.67 0.80 2 -16 0 33.38 2.30 2 16 0 32.86 2.12 -2 -16 0 31.38 2.33 -2 16 0 27.89 1.84 3 -16 0 61.82 3.35 -3 -16 0 61.19 3.28 3 16 0 60.14 3.19 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0.77 1.51 5 20 0 0.84 1.38 6 20 0 2.18 1.67 6 -20 0 1.71 1.63 7 20 0 10.01 2.10 7 -20 0 8.45 2.01 8 20 0 1.32 1.97 0 21 0 0.57 0.97 0 -21 0 0.47 1.51 -1 -21 0 0.39 1.52 1 -21 0 2.66 1.57 1 21 0 1.60 1.10 -1 21 0 0.15 1.04 -2 -21 0 7.13 1.72 -2 21 0 6.19 1.22 2 21 0 8.41 1.53 2 -21 0 4.91 1.76 -3 -21 0 9.30 1.89 3 21 0 11.66 1.65 3 -21 0 9.34 1.92 4 -21 0 16.44 2.17 4 21 0 15.07 1.92 -4 -21 0 18.05 2.29 -5 -21 0 13.02 2.08 5 21 0 12.96 1.96 5 -21 0 15.34 2.16 6 -21 0 24.43 2.65 6 21 0 29.17 2.71 7 21 0 2.04 1.86 0 22 0 14.65 1.68 0 -22 0 13.35 1.99 1 22 0 -0.08 1.10 1 -22 0 -1.83 1.54 -1 22 0 0.23 1.09 -1 -22 0 1.16 1.63 -2 -22 0 7.31 1.91 2 22 0 5.99 1.43 2 -22 0 12.15 2.09 -3 -22 0 20.68 2.55 3 22 0 23.41 2.26 3 -22 0 24.31 2.63 4 -22 0 -2.16 1.49 -4 -22 0 -0.86 1.52 4 22 0 -0.93 1.45 5 22 0 8.07 1.82 5 -22 0 9.00 2.01 6 -22 0 6.88 1.99 6 22 0 9.61 2.02 0 23 0 -0.18 1.16 0 -23 0 -1.82 1.60 1 23 0 3.70 1.40 -1 -23 0 2.01 1.39 1 -23 0 4.58 1.88 -1 23 0 -0.27 1.19 -2 -23 0 1.53 1.70 2 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11.79 2 2 -1 145.88 5.91 2 2 -1 138.97 5.83 2 -2 1 142.29 5.85 2 2 1 148.28 5.91 2 -2 -1 145.83 5.87 2 2 1 145.70 5.79 -2 -2 1 139.21 5.90 3 2 -1 85.20 3.52 3 -2 1 87.67 3.42 3 2 -1 87.30 3.51 3 2 1 74.66 3.48 4 -2 1 29.47 1.27 4 2 -1 29.16 1.41 4 2 -1 30.09 1.52 4 2 1 33.66 1.40 5 2 -1 15.56 0.80 5 2 -1 14.90 0.98 5 2 1 10.57 0.73 6 2 -1 17.12 0.97 6 2 -1 14.98 1.23 6 2 1 17.38 0.94 7 2 -1 79.37 3.38 7 2 -1 78.43 3.62 7 2 1 75.72 3.56 7 2 1 77.72 3.35 8 2 -1 4.64 0.98 8 2 1 4.60 0.96 9 2 -1 25.51 2.04 9 2 1 24.34 1.88 10 2 -1 0.11 1.19 10 2 1 0.83 1.05 10 -2 -1 0.81 1.31 11 -2 1 28.03 2.60 11 2 -1 28.09 2.42 11 2 1 30.87 2.79 11 -2 -1 30.05 2.69 12 -2 1 19.86 2.50 12 -2 1 18.03 2.31 12 2 1 16.68 2.60 12 -2 -1 23.19 2.65 0 3 -1 152.04 5.97 0 -3 1 143.70 6.12 0 -3 1 148.55 5.97 0 3 1 148.84 6.00 0 -3 -1 148.21 6.12 0 3 -1 153.16 6.01 1 -3 1 404.00 17.16 -1 -3 -1 410.70 17.17 1 3 -1 431.65 17.20 -1 -3 -1 412.08 16.86 1 3 -1 408.40 16.88 -1 3 1 398.31 16.88 1 -3 1 400.05 16.88 1 -3 -1 454.26 17.17 -1 3 -1 424.04 16.85 1 3 1 451.71 16.93 1 3 1 442.41 16.86 1 3 1 442.25 17.19 -1 -3 1 438.47 17.19 2 -3 1 24.87 1.11 2 3 -1 24.69 1.18 -2 -3 -1 24.44 1.14 2 3 -1 24.96 1.12 2 3 1 25.26 1.16 2 3 1 23.63 1.21 2 -3 -1 24.10 1.12 -2 -3 1 23.89 1.15 2 3 1 24.16 1.06 3 3 -1 0.79 0.27 3 -3 1 0.48 0.18 3 3 -1 0.49 0.27 3 3 1 0.86 0.25 -3 -3 1 0.50 0.23 3 3 1 0.49 0.23 3 -3 -1 0.87 0.21 4 -3 1 23.44 1.01 4 3 -1 23.29 1.21 4 3 -1 24.48 1.15 4 3 1 20.26 1.12 4 3 1 20.29 1.12 5 3 -1 41.79 2.13 5 3 -1 45.62 2.08 5 -3 1 44.17 1.91 5 3 1 49.32 2.08 5 3 1 47.86 2.13 6 3 -1 3.22 0.71 6 3 -1 4.04 0.52 6 3 1 1.77 0.44 6 3 1 3.12 0.66 7 3 -1 57.89 2.85 7 3 1 57.77 2.77 8 3 -1 21.45 1.58 8 3 1 21.36 1.56 9 3 -1 0.41 0.97 9 3 1 2.21 1.00 10 3 -1 20.76 1.87 10 3 1 20.68 1.80 10 3 1 17.25 2.14 11 3 -1 7.54 1.51 11 -3 -1 8.04 2.02 11 3 1 4.86 1.81 12 3 -1 0.08 1.74 12 -3 1 -0.49 1.66 12 -3 -1 -0.25 1.89 12 3 1 2.19 1.96 0 -4 1 14.53 0.66 0 -4 -1 13.39 0.75 0 4 -1 13.24 0.72 0 4 -1 13.97 0.66 0 4 1 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4 9.16 0.79 4 5 4 9.52 0.52 4 5 4 10.04 0.99 5 -5 4 4.53 0.54 5 5 -4 5.61 0.77 5 5 4 6.56 0.92 -5 -5 4 7.28 0.67 5 5 4 6.85 0.49 6 5 -4 11.63 1.08 6 -5 4 10.18 0.75 6 5 4 10.83 0.76 6 5 4 11.00 1.23 7 -5 4 4.43 0.50 7 5 -4 4.89 0.90 7 5 4 3.91 1.08 7 5 4 4.37 0.64 8 -5 4 53.11 2.32 8 5 -4 53.75 2.83 8 5 4 54.85 2.56 8 5 4 55.42 3.16 9 5 -4 42.36 2.57 9 5 4 38.03 2.80 10 -5 4 53.51 3.02 10 5 -4 51.94 3.03 10 5 4 54.20 3.50 11 5 -4 7.98 1.57 11 -5 4 6.23 1.49 11 -5 -4 2.86 2.13 11 5 4 5.43 1.77 12 -5 -4 1.45 2.09 12 5 4 -0.36 1.75 0 -6 4 2.48 0.49 0 6 -4 2.75 0.50 0 6 4 2.79 0.45 0 6 -4 2.51 0.29 -1 6 4 147.40 5.93 1 -6 4 146.74 6.07 1 6 -4 149.18 5.94 -1 -6 4 138.13 6.06 1 6 4 143.20 5.93 -1 6 -4 138.60 5.98 -1 6 -4 140.02 5.71 -2 6 4 20.87 1.19 -2 -6 -4 21.76 0.91 2 -6 4 21.90 1.23 2 6 -4 21.45 1.16 2 6 4 18.35 1.22 -2 -6 4 21.56 1.26 3 -6 4 0.48 0.42 3 -6 4 2.01 0.23 3 6 -4 0.94 0.45 3 6 4 1.48 0.56 -3 -6 4 1.61 0.48 4 -6 4 184.88 7.73 4 6 -4 184.67 7.67 4 6 4 185.84 7.40 -4 -6 4 186.20 7.80 4 6 4 187.33 7.81 5 6 -4 20.64 1.24 5 -6 4 20.60 1.12 5 6 4 16.73 1.42 5 6 4 17.71 0.88 -5 -6 4 16.68 1.16 6 6 -4 59.40 2.80 6 -6 4 58.46 2.57 -6 -6 4 55.60 2.59 6 6 4 55.38 2.43 6 6 4 53.34 2.94 7 -6 4 0.19 0.42 7 6 -4 1.47 0.75 7 6 4 0.79 0.77 7 6 4 0.20 0.46 8 -6 4 26.33 1.31 8 6 -4 24.14 1.90 8 6 4 25.81 2.07 9 6 -4 0.35 0.97 9 6 4 2.89 1.39 10 6 -4 30.05 2.17 10 6 4 25.63 2.54 11 6 4 12.17 2.23 11 -6 -4 11.15 2.33 12 6 4 8.65 2.16 12 -6 -4 9.76 2.47 0 7 4 97.50 4.25 0 7 -4 100.17 4.28 0 -7 4 100.91 4.40 0 7 -4 102.31 4.13 1 -7 4 44.71 2.14 -1 7 4 42.08 2.04 1 7 -4 40.21 2.04 1 7 4 42.36 2.07 -1 7 -4 45.39 1.82 -1 7 -4 43.89 2.13 -1 -7 4 45.81 2.17 -2 -7 -4 122.71 4.85 2 7 -4 121.19 5.05 2 -7 4 124.39 5.18 -2 7 4 122.31 5.09 -2 -7 4 115.68 5.20 2 7 4 113.58 5.09 3 -7 4 28.41 1.48 3 7 -4 25.08 1.40 3 -7 4 26.60 1.12 3 7 4 25.61 1.54 -3 -7 4 24.71 1.49 4 -7 4 43.53 2.19 4 7 -4 41.24 2.17 4 7 4 48.10 1.87 4 7 4 46.30 2.38 -4 -7 4 48.44 2.31 5 -7 4 12.60 0.96 5 7 -4 12.93 1.08 -5 -7 4 14.62 1.08 5 7 4 12.42 0.65 5 7 4 12.52 1.27 6 -7 4 62.09 2.84 6 7 -4 59.84 2.93 6 7 4 61.19 3.21 6 7 4 62.00 2.61 -6 -7 4 64.09 2.88 7 7 -4 17.69 1.47 7 -7 4 19.28 1.23 7 7 4 22.49 1.91 7 7 4 21.32 1.11 8 -7 4 1.40 0.51 8 7 -4 1.80 0.97 8 7 4 2.50 1.29 9 7 -4 43.15 2.62 9 7 4 45.06 2.84 10 7 -4 3.18 1.27 10 7 4 6.11 1.69 11 7 4 9.34 2.06 0 8 -4 23.99 1.44 0 -8 -4 24.34 1.49 0 8 -4 27.19 1.25 0 8 4 27.72 1.40 0 -8 4 24.71 1.50 1 -8 4 22.95 1.52 1 8 -4 23.66 1.45 1 8 -4 23.60 1.36 -1 8 4 25.81 1.46 1 8 4 29.98 1.53 1 -8 -4 31.13 1.54 -1 -8 4 30.09 1.62 -1 8 -4 30.98 1.61 -1 8 -4 31.04 1.24 2 8 -4 194.62 8.31 2 -8 4 195.15 8.50 -2 8 4 201.82 8.36 -2 -8 4 208.14 8.57 2 -8 -4 211.45 8.53 2 8 4 204.49 8.40 3 -8 4 25.16 1.54 3 -8 4 26.77 1.15 -3 -8 -4 26.24 1.16 -3 8 4 26.77 1.55 3 8 -4 27.97 1.47 3 8 4 28.38 1.64 -3 -8 4 29.29 1.62 4 8 -4 178.00 7.49 4 -8 4 187.04 7.63 -4 -8 4 179.42 7.70 4 8 4 177.82 7.67 5 -8 4 14.57 1.10 5 8 -4 16.26 1.14 5 8 4 13.91 1.38 -5 -8 4 14.82 1.19 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5 9 4 18.57 1.61 6 -9 4 63.21 2.86 6 9 -4 59.33 2.83 6 9 4 55.28 3.17 -6 -9 4 56.40 2.87 7 9 -4 22.44 1.63 7 -9 4 22.04 1.41 7 9 4 16.60 1.87 8 9 -4 14.79 1.42 8 -9 4 15.50 1.16 8 9 4 12.47 1.80 9 -9 4 3.24 0.69 9 9 -4 1.54 1.06 9 9 4 4.94 1.33 10 9 -4 -2.09 1.62 10 9 4 3.50 1.77 11 9 -4 -0.83 1.94 11 9 4 1.33 1.90 0 10 -4 57.39 2.47 0 -10 -4 56.71 2.79 0 10 4 55.33 2.61 0 -10 4 52.79 2.77 0 10 -4 55.64 2.70 -1 10 4 0.30 0.52 -1 -10 -4 -0.02 0.59 1 10 -4 0.40 0.56 1 -10 4 1.10 0.62 1 10 -4 0.30 0.42 1 10 4 0.62 0.57 1 -10 -4 -0.19 0.58 -1 -10 4 0.70 0.66 -1 10 -4 0.63 0.29 -2 10 4 82.12 3.57 2 10 -4 81.41 3.53 2 10 -4 76.85 3.50 2 -10 4 81.16 3.67 2 10 4 76.50 3.59 2 -10 -4 77.73 3.66 -2 10 -4 75.37 3.23 -2 -10 4 79.02 3.72 -3 10 4 106.97 4.64 3 10 -4 108.14 4.58 3 10 -4 101.50 4.62 3 -10 4 105.64 4.70 -3 -10 4 102.63 4.72 3 10 4 102.39 4.69 3 -10 -4 105.85 4.71 4 -10 4 53.21 2.75 4 10 -4 59.30 2.69 4 10 4 55.14 2.91 -4 -10 4 57.76 2.91 5 -10 4 25.46 1.62 5 10 -4 22.82 1.50 5 10 4 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30.71 1.99 5 -11 4 43.15 2.42 5 11 -4 41.62 2.30 5 11 -4 43.61 2.49 5 11 4 47.29 2.65 -5 -11 4 50.14 2.56 6 11 -4 9.49 1.48 6 -11 4 13.06 1.23 6 11 -4 10.99 1.18 6 11 4 9.83 1.35 -6 -11 4 10.34 1.22 7 11 -4 25.14 1.78 7 -11 4 25.39 1.75 7 11 -4 27.30 2.39 7 11 4 23.39 2.21 8 11 -4 7.70 1.18 8 11 -4 5.35 1.67 8 -11 4 6.30 1.02 8 11 4 9.07 1.70 9 11 -4 -1.13 1.57 9 -11 4 -1.02 0.72 9 11 4 -1.87 1.41 10 11 -4 7.35 2.01 10 11 4 6.82 2.06 11 11 -4 -0.55 2.02 11 11 4 -1.15 1.97 0 12 4 141.77 5.96 0 -12 4 139.32 6.22 0 -12 -4 133.45 6.18 0 12 -4 142.07 5.80 0 12 -4 136.52 6.04 1 12 -4 14.41 1.25 1 12 -4 14.71 1.02 -1 12 4 13.31 1.16 1 -12 4 11.94 1.26 -1 -12 -4 13.11 1.31 1 12 4 11.60 1.16 -1 -12 4 12.57 1.31 -1 12 -4 12.55 0.86 1 -12 -4 13.68 1.32 -2 12 4 24.63 1.62 -2 -12 -4 25.72 1.78 2 -12 4 25.63 1.74 2 12 -4 23.86 1.57 2 12 -4 25.78 1.53 2 -12 -4 25.28 1.74 -2 -12 4 26.35 1.81 2 12 4 22.75 1.65 -2 12 -4 25.91 1.25 3 -12 4 68.12 3.27 -3 12 4 62.16 3.11 3 12 -4 66.38 3.14 3 12 -4 61.28 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5 19.70 1.42 7 2 5 19.61 1.67 8 -2 5 1.56 0.34 8 2 -5 0.95 1.00 8 -2 5 -0.24 0.77 8 2 5 1.51 1.00 8 -2 -5 2.06 1.14 9 -2 5 3.09 1.18 9 2 -5 2.98 1.17 9 -2 -5 3.45 1.36 9 2 5 3.02 1.23 9 2 5 3.37 0.93 10 -2 5 -0.59 1.21 10 2 -5 2.05 1.31 10 -2 -5 1.65 1.57 10 2 5 -0.86 1.23 11 2 -5 22.60 2.38 11 -2 5 23.60 2.27 11 2 5 25.46 2.44 11 -2 -5 17.30 2.50 12 2 -5 6.24 1.74 12 -2 5 3.03 1.69 12 2 5 7.08 1.89 12 -2 -5 3.25 2.17 0 -3 -5 174.00 6.74 0 -3 5 162.47 6.93 0 3 5 160.48 6.78 0 3 -5 169.59 6.80 1 -3 5 214.62 8.42 -1 3 5 213.79 8.59 1 3 -5 216.03 8.58 1 -3 5 208.42 8.71 -1 -3 -5 210.62 8.44 1 3 5 209.83 8.56 -1 3 -5 214.21 8.42 -1 3 -5 204.49 8.58 -1 -3 5 211.09 8.75 2 -3 5 31.76 1.56 2 -3 5 31.67 1.37 2 3 -5 34.57 1.58 -2 -3 5 30.73 1.59 2 3 5 34.06 1.33 -2 3 -5 31.30 1.58 2 3 5 34.75 1.59 3 3 -5 111.61 4.64 3 -3 5 113.41 4.61 3 -3 5 112.49 4.47 3 3 5 103.41 4.62 -3 -3 5 105.96 4.66 3 3 5 108.54 4.38 4 -3 5 21.60 1.10 4 -3 5 21.72 1.09 4 3 -5 21.29 1.27 4 3 5 19.21 1.27 -4 -3 5 19.07 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2.72 -3 -5 5 67.24 3.03 3 5 5 69.01 3.04 4 -5 5 20.50 1.22 4 5 -5 22.52 1.34 4 5 5 21.59 1.34 -4 -5 5 22.64 1.32 4 5 5 23.37 0.92 5 -5 5 17.73 1.08 5 5 -5 19.14 1.28 5 5 5 18.04 1.42 -5 -5 5 18.77 1.14 5 5 5 18.80 0.88 6 5 -5 10.82 1.12 6 -5 5 10.33 0.83 6 5 5 12.90 0.77 -6 -5 5 12.80 0.95 6 5 5 11.49 1.27 7 -5 5 5.70 0.61 7 5 -5 4.87 0.97 7 5 5 5.23 1.14 7 5 5 6.00 0.64 8 -5 5 20.00 1.12 8 5 -5 23.00 1.76 8 5 5 24.61 2.04 9 -5 5 115.19 5.16 9 5 -5 112.65 5.27 9 5 5 107.95 5.44 10 -5 5 21.93 1.92 10 5 -5 22.34 2.10 10 5 5 24.03 2.37 10 -5 -5 22.76 2.52 11 5 -5 10.62 1.85 11 -5 -5 12.36 2.37 11 5 5 10.97 2.03 12 5 5 1.74 2.03 12 -5 -5 0.50 2.27 0 -6 5 633.09 26.21 0 6 5 650.98 25.74 0 6 -5 649.29 25.77 1 6 -5 42.41 2.04 -1 6 5 42.02 2.08 1 -6 5 41.29 2.13 1 6 5 47.09 2.10 -1 -6 5 44.99 2.18 -1 6 -5 46.68 1.81 -1 6 -5 45.12 2.14 2 -6 5 24.79 1.41 -2 6 5 24.85 1.43 2 6 -5 24.05 1.38 -2 -6 5 27.44 1.49 2 6 5 31.43 1.50 3 6 -5 11.56 0.89 3 -6 5 10.50 0.86 3 -6 5 10.40 0.49 3 -6 5 9.88 0.49 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1.69 -4 -7 5 33.09 1.79 4 7 5 27.89 1.83 5 -7 5 105.32 4.69 5 7 -5 103.16 4.70 -5 -7 5 116.08 4.80 5 7 5 109.19 4.86 6 7 -5 8.74 1.06 6 -7 5 11.24 0.93 6 7 5 10.05 0.57 6 7 5 12.19 1.37 -6 -7 5 11.38 0.96 7 -7 5 16.33 1.16 7 7 -5 18.46 1.51 7 7 5 11.92 1.57 8 7 -5 38.08 2.38 8 -7 5 38.00 1.91 8 7 5 43.13 2.76 9 7 -5 -0.15 0.97 9 -7 5 0.29 0.84 9 7 5 0.73 1.35 10 7 -5 46.93 2.96 10 7 5 49.05 3.44 11 7 5 5.07 1.91 11 -7 -5 4.96 2.13 0 8 -5 58.02 2.77 0 8 -5 60.44 2.59 0 8 5 60.98 2.77 0 -8 5 63.29 2.88 1 8 -5 78.41 3.58 -1 8 5 80.83 3.57 1 -8 5 83.32 3.70 -1 8 -5 81.69 3.63 -1 8 -5 84.68 3.31 -1 -8 5 76.36 3.67 1 8 5 80.33 3.56 2 -8 5 40.84 2.05 -2 8 5 41.82 2.03 2 8 -5 42.60 1.99 -2 -8 5 35.59 2.06 2 8 5 36.78 2.02 -3 8 5 174.49 7.20 3 8 -5 166.35 7.09 3 -8 5 171.89 7.24 3 8 5 167.26 7.20 -3 -8 5 172.31 7.31 4 -8 5 22.25 1.43 4 8 -5 22.94 1.47 4 8 5 24.05 1.62 -4 -8 5 24.27 1.57 5 -8 5 112.16 4.79 5 8 -5 110.06 4.76 -5 -8 5 105.16 4.85 5 8 5 108.29 4.97 6 -8 5 6.17 0.80 6 8 -5 6.80 1.01 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4.39 1.64 10 9 -5 0.65 1.17 10 9 5 1.29 1.68 11 9 -5 6.16 2.22 11 9 5 7.03 2.13 0 10 -5 52.72 2.62 0 -10 5 51.87 2.71 0 10 5 53.68 2.56 0 10 -5 54.03 2.36 -1 10 5 6.60 0.86 1 10 -5 7.27 0.72 1 10 -5 7.02 0.88 1 -10 5 6.21 0.89 -1 -10 5 6.42 0.95 1 10 5 10.88 1.00 -1 10 -5 8.57 0.56 -1 10 -5 9.29 0.95 2 10 -5 76.50 3.38 -2 10 5 73.12 3.44 2 10 -5 79.94 3.43 2 -10 5 70.50 3.51 2 10 5 74.71 3.43 -2 -10 5 73.02 3.54 3 10 -5 92.22 3.97 -3 10 5 85.45 4.03 3 -10 5 87.07 4.08 3 10 5 90.80 4.10 -3 -10 5 88.98 4.12 4 10 -5 200.62 8.32 4 -10 5 202.59 8.50 4 10 5 198.15 8.50 -4 -10 5 196.87 8.57 5 10 -5 21.11 1.45 5 -10 5 21.68 1.52 -5 -10 5 20.30 1.58 5 10 5 20.43 1.74 6 10 -5 6.55 1.05 6 -10 5 4.09 0.88 -6 -10 5 2.12 0.80 7 -10 5 5.89 0.94 7 10 -5 5.15 1.02 7 10 5 8.26 1.55 8 -10 5 19.55 1.45 8 10 -5 19.98 1.72 8 10 5 17.92 2.11 9 -10 5 1.65 0.74 9 10 -5 0.81 1.08 9 10 5 2.85 1.63 10 10 -5 -1.37 1.72 10 10 5 -1.15 1.65 11 10 -5 12.89 2.58 11 10 5 15.91 2.55 0 11 -5 -0.31 0.38 0 11 -5 -0.32 0.68 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6.54 2.15 -2 -24 6 8.23 2.21 2 24 6 7.21 1.85 -3 24 6 4.17 1.70 3 -24 6 1.93 1.96 3 24 6 7.55 1.95 -3 -24 6 0.03 1.83 4 24 -6 -1.14 1.45 4 -24 6 -3.59 1.75 -4 -24 6 1.17 1.87 4 24 6 -0.21 1.66 0 25 6 -0.15 1.73 0 -25 6 -0.01 1.98 1 -25 6 6.24 2.24 -1 25 6 5.67 1.71 -1 -25 6 3.84 2.04 1 25 6 1.35 1.81 -2 25 6 9.16 1.91 2 -25 6 10.99 2.62 -2 -25 6 6.08 2.21 2 25 6 9.33 2.14 3 -25 6 5.25 2.22 -3 -25 6 3.93 2.00 3 25 6 1.84 1.75 0 0 -7 0.51 0.29 0 0 7 0.01 0.27 1 0 -7 2.59 0.43 1 0 7 2.47 0.35 -1 0 -7 2.28 0.35 2 0 7 1.62 0.35 -2 0 -7 1.46 0.31 2 0 -7 1.50 0.46 -3 0 7 260.15 10.84 3 0 7 261.30 10.62 3 0 -7 268.15 10.77 4 0 7 35.44 1.73 4 0 -7 36.80 1.94 -4 0 7 34.58 1.75 -5 0 7 35.55 1.73 5 0 7 32.61 1.81 5 0 -7 35.65 2.01 6 0 7 14.57 1.21 6 0 -7 12.51 1.25 7 0 -7 7.05 1.26 7 0 7 8.83 1.07 8 0 -7 17.00 1.81 8 0 7 19.12 1.61 9 0 7 0.26 1.09 9 0 -7 -1.25 1.21 10 0 7 6.21 1.52 10 0 -7 7.98 1.71 11 0 -7 30.09 2.74 11 0 7 23.94 2.33 12 0 -7 9.70 2.18 12 0 7 9.56 1.88 0 -1 7 6.85 0.55 0 -1 -7 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1.01 8 -2 -7 3.85 1.26 8 2 7 4.71 1.10 9 -2 7 29.12 2.14 9 2 -7 30.30 2.36 9 -2 -7 31.53 2.53 9 2 7 27.41 2.23 10 -2 7 1.90 1.27 10 2 -7 4.24 1.59 10 -2 -7 4.23 1.62 10 2 7 3.63 1.40 11 2 -7 33.18 2.84 11 -2 7 33.67 2.59 11 -2 -7 24.75 2.82 11 2 7 34.21 2.77 12 2 -7 1.25 1.72 12 2 7 1.53 1.67 12 -2 -7 1.30 1.97 0 3 -7 325.09 13.09 0 3 7 321.51 13.08 0 -3 -7 322.50 13.02 0 -3 7 329.67 13.35 1 -3 7 153.56 6.16 1 3 -7 149.64 6.31 -1 3 7 153.42 6.34 1 -3 7 152.51 6.44 -1 -3 -7 151.74 6.18 1 -3 -7 153.40 6.31 -1 3 -7 151.21 6.32 -1 -3 7 160.09 6.47 1 3 7 151.10 6.29 -2 -3 -7 34.42 1.56 -2 3 7 31.88 1.77 2 -3 7 31.39 1.76 2 -3 7 33.64 1.56 2 3 -7 33.12 1.78 2 3 7 42.87 1.80 -2 -3 7 38.29 1.86 2 3 7 41.68 1.57 2 -3 -7 43.26 1.87 -2 3 -7 40.07 1.82 3 3 -7 91.77 4.11 3 -3 7 93.27 3.88 -3 -3 7 97.04 4.15 3 3 7 96.23 3.82 3 3 7 92.93 4.07 4 3 -7 50.34 2.50 4 -3 7 52.47 2.27 -4 -3 7 52.55 2.45 4 3 7 50.38 2.46 5 3 -7 23.63 1.57 5 -3 7 25.15 1.29 5 3 7 21.45 1.48 -5 -3 7 23.28 1.33 6 -3 7 143.73 6.02 6 3 -7 147.04 6.25 6 -3 7 137.95 6.02 6 -3 -7 145.60 6.33 6 3 7 142.04 6.21 7 -3 7 11.48 0.90 7 -3 7 12.46 1.11 7 3 -7 11.61 1.36 7 3 7 12.56 1.36 7 -3 -7 12.05 1.55 8 -3 7 5.47 0.95 8 3 -7 7.99 1.31 8 -3 7 6.41 0.70 8 3 7 9.00 1.34 8 3 7 7.16 0.88 8 -3 -7 7.02 1.53 9 -3 7 55.78 3.04 9 3 -7 59.60 3.26 9 -3 -7 56.38 3.50 9 3 7 53.63 3.26 10 -3 7 1.37 1.14 10 3 -7 2.60 1.35 10 -3 -7 2.49 1.60 10 3 7 1.37 1.35 11 -3 7 5.69 1.40 11 3 -7 5.52 1.80 11 3 7 5.43 1.74 11 -3 -7 4.94 1.97 12 3 -7 7.85 1.94 12 3 7 11.77 2.22 12 -3 -7 7.85 2.30 0 4 7 4.69 0.59 0 4 -7 5.00 0.61 0 -4 -7 5.70 0.50 0 -4 7 5.70 0.66 1 -4 7 61.86 2.81 1 4 -7 62.40 2.74 -1 4 7 63.38 2.76 -1 -4 -7 61.50 2.56 -1 4 -7 62.53 2.53 1 4 7 59.91 2.71 -1 -4 7 60.42 2.82 -1 4 -7 56.91 2.74 -2 4 7 17.95 1.20 -2 -4 -7 18.34 0.86 2 -4 7 17.45 1.14 2 4 -7 19.67 1.18 2 -4 7 18.15 0.86 -2 -4 7 24.35 1.28 2 4 7 23.77 1.20 -2 4 -7 22.79 1.23 3 -4 7 12.87 0.91 3 -4 7 13.27 0.68 3 4 -7 14.25 1.03 3 4 7 13.39 1.00 -3 -4 7 13.92 1.00 4 4 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2 5 7 124.74 5.26 3 -5 7 108.15 4.33 3 -5 7 112.49 4.69 3 5 -7 106.22 4.65 3 5 7 110.63 4.68 -3 -5 7 101.57 4.72 4 -5 7 24.19 1.11 4 -5 7 21.97 1.35 4 5 -7 21.69 1.45 -4 -5 7 24.34 1.41 4 5 7 24.33 1.52 5 5 -7 11.86 1.16 5 -5 7 11.72 0.97 5 -5 7 11.33 0.82 5 5 7 15.53 1.28 -5 -5 7 15.53 1.09 6 -5 7 7.92 0.79 6 -5 7 7.58 0.80 6 5 -7 9.09 1.13 6 5 7 11.12 1.23 -6 -5 7 9.36 0.87 6 5 7 8.92 0.54 7 5 -7 6.18 1.12 7 -5 7 5.34 0.72 7 -5 7 5.13 0.80 7 5 7 5.90 1.16 8 5 -7 7.98 1.34 8 -5 7 10.60 1.13 8 -5 7 8.83 0.83 8 5 7 9.72 1.50 9 5 -7 56.89 3.42 9 -5 7 61.78 3.11 9 -5 -7 61.26 3.74 9 5 7 59.80 3.54 10 5 -7 15.37 1.94 10 -5 -7 14.71 2.29 10 5 7 10.81 1.87 11 5 -7 2.96 1.53 11 5 7 3.32 1.71 11 -5 -7 2.80 2.04 0 -6 7 81.82 3.59 0 6 -7 75.77 3.48 0 6 7 78.34 3.46 -1 6 7 40.23 2.14 1 6 -7 39.41 2.07 1 -6 7 44.16 2.21 -1 -6 -7 42.69 1.92 -1 6 -7 47.67 1.83 -1 6 -7 44.96 2.19 -1 -6 7 46.61 2.25 1 6 7 46.88 2.14 2 -6 7 16.07 1.09 -2 -6 -7 14.71 0.64 2 6 -7 15.03 0.97 -2 6 7 14.92 1.11 -2 -6 7 12.44 1.09 2 6 7 12.21 1.06 -2 6 -7 13.96 1.15 3 -6 7 146.91 6.27 3 6 -7 150.13 6.20 3 6 7 145.18 6.23 -3 -6 7 144.61 6.34 4 -6 7 0.53 0.52 4 6 -7 1.89 0.68 4 -6 7 0.93 0.24 -4 -6 7 1.01 0.54 4 6 7 1.29 0.69 5 -6 7 26.90 1.58 5 6 -7 26.77 1.71 5 -6 7 26.12 1.32 -5 -6 7 29.56 1.66 5 6 7 29.89 1.83 6 6 -7 16.85 1.44 6 -6 7 16.98 1.05 6 -6 7 17.54 1.21 6 6 7 13.50 1.39 -6 -6 7 15.08 1.17 7 -6 7 83.48 3.62 7 6 -7 79.04 3.90 7 -6 7 77.64 3.65 7 6 7 86.89 4.11 8 -6 7 2.27 0.64 8 -6 7 2.28 0.77 8 6 -7 3.17 1.13 8 6 7 3.03 1.26 9 6 -7 42.67 2.71 9 6 7 42.79 3.00 10 6 -7 8.03 1.60 10 -6 -7 9.65 2.26 10 6 7 12.98 1.98 11 6 -7 13.88 2.00 11 -6 -7 10.02 2.37 11 6 7 10.89 2.06 0 -7 7 3.58 0.73 0 7 -7 6.00 0.69 0 7 7 4.95 0.70 1 -7 7 46.09 2.30 -1 7 7 44.82 2.28 1 7 -7 44.41 2.26 -1 -7 7 47.33 2.33 -1 7 -7 45.65 2.27 1 7 7 48.04 2.27 -1 7 -7 47.67 1.92 -1 7 -7 47.32 1.92 -2 7 7 74.19 3.44 -2 -7 -7 76.71 3.06 2 7 -7 77.15 3.40 -2 -7 -7 76.15 3.06 2 -7 7 73.22 3.46 -2 7 -7 72.76 3.47 2 7 7 78.17 3.40 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5.74 1.65 6 19 -7 29.07 2.58 6 -19 7 24.30 2.58 6 19 -7 32.17 2.42 6 19 7 23.15 2.39 7 19 -7 1.45 1.66 7 -19 7 2.43 1.47 7 19 7 -0.72 1.70 8 19 -7 0.61 1.77 8 -19 7 1.49 1.64 8 19 7 1.02 1.85 0 -20 7 11.14 1.73 0 20 7 8.65 1.58 1 -20 7 3.04 1.60 1 20 -7 2.06 0.98 -1 20 7 0.23 1.26 1 20 7 4.14 1.38 -1 -20 7 0.41 1.44 2 20 -7 5.30 1.20 2 -20 7 2.57 1.61 -2 20 7 4.86 1.44 2 20 7 3.77 1.50 -2 -20 7 5.00 1.73 3 20 -7 1.39 1.21 3 -20 7 -0.09 1.39 -3 20 7 0.49 1.28 3 20 -7 -0.37 1.26 -3 -20 7 -0.29 1.46 3 20 7 2.19 1.37 4 -20 7 28.70 2.84 4 20 -7 34.32 2.64 4 20 -7 28.89 2.39 -4 20 7 26.84 2.58 -4 -20 7 27.02 2.70 4 20 7 29.08 2.59 5 20 -7 6.10 1.67 5 20 -7 5.88 1.57 5 -20 7 6.47 1.76 5 20 7 5.49 1.68 -5 -20 7 3.14 1.65 6 20 -7 5.14 1.59 6 20 -7 5.06 1.77 6 -20 7 5.51 1.89 6 20 7 4.93 1.85 7 20 -7 4.85 1.84 7 -20 7 6.68 1.84 7 20 7 5.87 1.98 0 21 7 10.76 1.75 0 -21 7 13.71 1.92 1 -21 7 3.92 1.77 -1 21 7 1.58 1.40 -1 -21 7 3.11 1.37 1 21 7 3.11 1.48 2 21 -7 26.08 2.02 -2 21 7 24.03 2.33 2 -21 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2.54 -5 1 8 45.41 2.24 5 1 8 47.35 2.33 5 -1 -8 48.69 2.57 -5 -1 8 48.92 2.29 6 1 -8 96.99 4.42 6 -1 8 94.19 4.15 6 -1 -8 93.72 4.44 6 1 8 91.37 4.21 7 -1 8 5.36 0.88 7 1 -8 5.32 1.17 7 -1 -8 6.62 1.31 7 1 8 4.86 1.03 8 1 -8 16.78 1.80 8 -1 8 17.89 1.60 8 1 8 17.65 1.68 8 -1 -8 16.98 1.87 9 -1 8 3.63 1.17 9 -1 8 3.80 0.68 9 1 -8 5.34 1.47 9 1 8 2.31 1.13 9 -1 -8 3.82 1.50 10 -1 8 11.06 1.66 10 1 -8 10.50 1.88 10 -1 -8 13.70 2.05 10 1 8 14.81 1.87 11 1 -8 0.51 1.61 11 -1 8 2.15 1.33 11 1 8 -0.42 1.50 11 -1 -8 0.97 1.75 12 1 -8 10.04 2.35 12 -1 -8 12.57 2.51 0 -2 -8 296.26 11.96 0 2 -8 300.67 12.02 0 2 8 294.65 12.00 -1 -2 -8 5.35 0.47 1 -2 8 5.22 0.46 1 2 -8 5.51 0.62 -1 2 8 5.39 0.63 -1 -2 8 5.18 0.64 1 2 8 5.03 0.55 1 -2 -8 6.34 0.61 -1 2 -8 5.89 0.60 2 -2 8 6.71 0.50 -2 -2 -8 7.65 0.54 2 2 -8 6.75 0.69 -2 -2 8 7.13 0.73 2 2 8 7.52 0.67 -2 2 -8 8.20 0.71 2 -2 -8 6.39 0.74 3 2 -8 1.57 0.48 3 -2 8 1.19 0.34 3 2 8 2.36 0.50 -3 -2 8 1.22 0.47 3 -2 -8 0.42 0.58 4 2 -8 96.94 4.34 4 -2 8 95.16 4.14 -4 2 8 94.71 4.27 4 -2 -8 101.43 4.45 4 2 8 101.01 4.30 -4 -2 8 103.99 4.34 5 2 -8 7.52 1.02 5 -2 8 5.95 0.67 -5 2 8 6.76 0.67 -5 -2 8 4.99 0.68 5 -2 -8 5.35 1.00 5 2 8 4.59 0.78 6 2 -8 60.74 3.15 6 -2 8 64.79 2.90 6 2 8 58.62 3.01 6 -2 -8 63.42 3.27 7 2 -8 6.86 1.23 7 -2 8 6.13 0.93 7 2 8 6.88 1.08 7 -2 -8 4.37 1.27 8 -2 8 72.42 3.54 8 -2 8 75.20 3.33 8 2 -8 74.09 3.84 8 -2 -8 72.28 3.95 8 2 8 75.05 3.80 9 2 -8 0.62 1.20 9 -2 8 -0.71 0.99 9 -2 8 0.81 0.56 9 -2 -8 0.09 1.42 9 2 8 1.46 1.25 10 -2 8 34.64 2.63 10 2 -8 40.54 2.89 10 2 8 40.99 2.82 10 -2 -8 44.30 3.15 11 -2 8 0.36 1.40 11 2 -8 2.91 1.65 11 2 8 1.17 1.48 11 -2 -8 3.77 1.83 0 -3 8 67.03 3.11 0 3 -8 68.83 3.00 0 -3 -8 69.96 2.94 0 3 8 67.85 3.01 1 -3 8 75.30 3.21 -1 3 8 80.76 3.42 1 -3 8 75.90 3.45 1 3 -8 73.52 3.37 -1 -3 -8 73.57 3.23 1 3 8 82.18 3.36 -1 -3 8 78.96 3.50 -1 3 -8 80.30 3.40 1 -3 -8 79.58 3.37 2 -3 8 328.21 13.20 2 3 -8 333.40 13.43 -2 -3 -8 339.79 13.23 -2 3 8 335.60 13.47 2 -3 -8 331.87 13.44 2 3 8 325.53 13.37 -2 -3 8 324.07 13.66 -2 3 -8 330.19 13.42 3 -3 8 10.71 0.60 3 3 -8 10.90 0.89 -3 -3 8 7.76 0.82 3 3 8 8.04 0.80 3 -3 -8 6.73 0.82 4 3 -8 45.62 2.34 4 -3 8 48.69 2.06 4 -3 -8 43.64 2.40 -4 -3 8 43.87 2.24 4 3 8 46.52 2.28 -5 3 8 14.60 0.97 5 3 -8 15.03 1.30 5 -3 8 14.18 0.95 5 -3 -8 13.03 1.37 -5 -3 8 13.73 1.07 5 3 8 14.45 1.23 6 -3 8 44.66 2.24 6 -3 8 47.03 2.25 6 3 -8 47.24 2.57 6 -3 -8 46.85 2.71 -6 -3 8 48.34 2.25 6 3 8 42.18 2.44 7 -3 8 0.67 0.69 7 3 -8 1.64 0.99 7 -3 8 0.61 0.56 7 3 8 2.16 0.95 7 -3 -8 2.62 1.19 8 -3 8 9.09 0.85 8 3 -8 8.84 1.40 8 -3 8 9.38 1.13 8 3 8 7.19 1.29 8 -3 -8 7.03 1.57 9 -3 8 6.96 1.21 9 3 -8 10.24 1.65 9 -3 8 7.70 0.78 9 3 8 7.17 1.43 9 -3 -8 5.81 1.69 10 3 -8 19.49 2.11 10 -3 8 17.18 1.77 10 -3 -8 17.96 2.33 10 3 8 21.43 2.15 11 3 -8 10.06 2.00 11 3 8 8.70 1.86 11 -3 -8 9.35 2.15 0 -4 -8 48.34 2.09 0 4 8 46.39 2.18 0 4 -8 45.13 2.19 0 -4 8 45.80 2.27 -1 4 8 55.45 2.53 -1 -4 -8 56.62 2.35 1 4 -8 54.22 2.53 1 -4 8 58.03 2.62 -1 -4 8 52.58 2.59 1 -4 -8 53.33 2.50 -1 4 -8 55.91 2.55 1 4 8 54.00 2.47 2 4 -8 71.26 3.24 -2 4 8 73.40 3.29 -2 -4 -8 72.45 2.98 2 -4 8 68.68 3.27 2 -4 8 69.25 2.96 -2 4 -8 76.87 3.28 2 -4 -8 76.41 3.28 2 4 8 72.69 3.22 -2 -4 8 74.22 3.35 3 4 -8 55.29 2.71 3 -4 8 57.49 2.40 3 -4 8 53.70 2.67 3 4 8 58.47 2.69 3 4 8 60.66 2.34 -3 -4 8 57.95 2.75 4 4 -8 48.33 2.53 4 -4 8 50.59 2.22 4 -4 8 49.02 2.42 -4 -4 8 57.07 2.56 4 4 8 52.60 2.08 4 4 8 49.17 2.45 5 4 -8 48.09 2.45 -5 4 8 44.96 2.17 5 -4 8 45.87 2.09 5 -4 8 46.04 2.24 -5 -4 8 45.41 2.28 5 4 8 43.84 2.38 6 4 -8 24.37 1.79 6 -4 8 27.34 1.51 6 -4 8 27.42 1.47 6 4 8 24.98 1.77 -6 -4 8 23.43 1.45 7 -4 8 56.33 2.67 7 4 -8 53.18 3.00 7 -4 8 56.99 2.72 7 4 8 57.93 2.54 7 4 8 55.79 3.03 7 -4 -8 57.36 3.25 8 -4 8 20.36 1.32 8 -4 8 19.03 1.51 8 4 -8 18.52 1.81 8 4 8 19.86 1.85 8 -4 -8 18.77 1.92 9 -4 8 33.18 1.75 9 4 -8 37.66 2.53 9 -4 8 34.04 2.23 9 -4 -8 30.25 2.75 9 4 8 34.72 2.61 10 4 -8 5.73 1.58 10 4 8 5.05 1.67 10 -4 -8 5.95 1.94 11 4 -8 15.12 2.17 11 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1.48 1.65 11 -7 -8 2.54 2.15 11 7 8 2.39 1.82 0 8 -8 92.42 4.16 0 8 8 94.51 4.10 0 -8 8 91.31 4.23 1 -8 8 16.51 1.14 -1 8 8 17.45 1.24 1 8 -8 15.86 1.09 1 8 8 15.13 1.19 -1 -8 8 12.96 1.23 -1 8 -8 14.80 1.28 -1 8 -8 13.50 0.68 -1 8 -8 13.91 0.68 2 8 -8 6.92 0.91 -2 -8 -8 5.86 0.43 2 -8 8 6.36 0.87 -2 8 8 6.96 0.96 -2 8 -8 7.20 1.01 -2 -8 8 6.65 0.84 2 8 8 7.32 0.92 3 8 -8 85.79 3.89 3 -8 8 84.05 3.95 -3 8 8 82.65 3.97 3 8 8 85.52 3.94 -3 -8 8 91.34 4.06 4 8 -8 34.40 1.97 4 -8 8 36.40 1.99 -4 -8 8 32.50 1.98 4 8 8 31.49 2.04 5 8 -8 28.03 1.83 5 -8 8 27.17 1.20 5 -8 8 30.94 1.80 -5 -8 8 35.20 1.88 5 8 8 27.55 1.98 6 -8 8 5.84 0.92 6 8 -8 3.99 1.02 -6 -8 8 3.18 0.86 6 8 8 6.90 1.25 7 -8 8 56.41 2.87 7 8 -8 57.09 3.05 7 8 8 59.97 3.30 8 -8 8 30.35 1.84 8 8 -8 31.83 2.33 8 8 8 24.25 2.33 9 8 -8 17.65 1.89 9 -8 8 19.84 1.43 9 8 8 23.86 2.37 10 8 -8 2.09 1.51 10 -8 -8 1.04 2.01 10 8 8 4.02 1.75 11 8 -8 13.96 2.06 11 -8 -8 15.40 2.78 11 8 8 16.17 2.47 0 -9 8 18.11 1.47 0 9 -8 19.10 1.42 0 9 8 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22.38 1.72 6 5 9 19.47 1.64 -6 -5 9 18.99 1.37 7 5 -9 39.17 2.42 7 -5 9 37.55 2.05 7 -5 9 37.81 1.97 7 -5 -9 36.63 2.64 7 5 9 37.95 2.40 8 -5 9 3.39 0.78 8 -5 9 4.78 0.88 8 5 -9 2.44 1.25 8 5 9 3.08 1.23 8 -5 -9 5.80 1.34 9 5 -9 11.38 1.68 9 -5 9 8.51 0.93 9 5 9 6.81 1.54 9 -5 -9 7.02 1.58 10 5 -9 0.39 1.45 10 5 9 1.40 1.50 10 -5 -9 5.00 1.96 11 5 -9 8.06 2.05 11 5 9 9.88 1.99 11 -5 -9 13.55 2.45 0 6 9 1.20 0.60 0 -6 9 1.22 0.63 0 6 -9 2.47 0.68 0 -6 -9 2.26 0.46 1 6 -9 4.36 0.77 -1 6 9 5.04 0.81 -1 -6 -9 3.66 0.46 1 -6 9 3.53 0.62 -1 6 -9 5.96 0.82 1 -6 -9 6.16 0.69 -1 -6 9 5.73 0.85 1 6 9 8.27 0.75 2 -6 9 65.16 3.14 2 6 -9 67.62 3.10 -2 6 9 69.09 3.11 -2 -6 -9 65.60 2.73 -2 -6 9 65.62 3.15 2 6 9 67.46 3.07 -2 6 -9 62.85 3.12 3 6 -9 23.06 1.48 -3 6 9 20.42 1.41 3 -6 9 18.69 1.38 3 6 9 22.83 1.46 -3 -6 9 23.36 1.51 4 6 -9 60.62 2.92 4 -6 9 58.45 2.42 4 -6 9 59.28 2.89 4 6 9 60.92 2.93 -4 -6 9 57.38 2.92 5 -6 9 48.35 2.45 5 -6 9 48.77 2.12 5 6 -9 49.76 2.62 5 6 9 51.36 2.64 -5 -6 9 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26.89 2.04 7 -8 9 26.16 1.80 7 8 9 25.51 2.16 8 -8 9 29.01 1.92 8 8 -9 29.33 2.27 8 8 9 29.05 2.43 9 8 -9 5.18 1.43 9 -8 9 6.26 0.96 9 8 9 9.79 1.76 10 8 -9 5.85 1.61 10 -8 -9 4.88 2.14 10 8 9 2.44 1.70 11 8 -9 7.65 1.88 11 -8 -9 6.51 2.36 11 8 9 6.12 2.00 0 9 9 68.35 3.30 0 9 -9 69.38 3.29 0 -9 9 71.99 3.47 1 -9 9 40.12 2.33 -1 9 9 42.49 2.20 1 9 -9 38.29 2.25 1 9 9 44.90 2.27 -1 9 -9 42.97 1.77 -1 -9 9 41.38 2.37 -1 9 -9 41.40 2.32 -2 -9 -9 91.73 3.73 2 9 -9 89.89 4.13 -2 9 9 89.67 4.20 2 -9 9 95.18 4.27 -2 -9 9 92.94 4.30 2 9 9 85.09 4.07 -2 9 -9 89.62 4.19 3 9 -9 90.83 4.27 -3 9 9 93.63 4.41 3 -9 9 92.59 4.37 3 9 9 96.01 4.35 -3 -9 9 98.28 4.47 4 9 -9 20.13 1.68 4 -9 9 22.49 1.65 4 9 9 28.43 1.86 -4 -9 9 27.22 1.79 5 9 -9 46.87 2.70 5 -9 9 50.45 2.71 5 9 9 51.00 2.85 -5 -9 9 54.24 2.78 6 -9 9 4.42 0.99 6 9 -9 4.85 1.20 -6 -9 9 7.11 1.05 6 9 9 8.45 1.38 7 9 -9 4.46 1.18 7 -9 9 6.08 1.06 7 9 9 10.30 1.55 8 -9 9 6.40 1.07 8 9 -9 5.33 1.41 8 9 9 7.84 1.64 9 -9 9 37.05 2.20 9 9 -9 32.06 2.63 9 9 9 42.94 3.11 10 9 -9 14.94 2.00 10 9 9 15.00 2.23 10 -9 -9 7.01 2.26 11 9 -9 11.34 2.03 11 9 9 7.46 2.10 11 -9 -9 9.20 2.63 0 -10 9 131.32 5.88 0 10 -9 125.51 5.72 0 10 9 132.46 5.69 1 -10 9 83.84 4.00 -1 10 9 81.26 3.88 1 10 -9 79.74 3.87 -1 -10 9 82.53 3.96 -1 10 -9 79.20 3.93 -1 10 -9 86.88 3.39 1 10 9 81.74 3.84 2 10 -9 4.52 0.97 -2 10 9 4.03 1.00 2 -10 9 4.10 0.91 -2 -10 -9 4.65 0.45 -2 10 -9 0.72 0.96 2 10 9 3.78 0.92 -2 -10 9 3.14 0.95 3 10 -9 23.57 1.55 3 -10 9 21.88 1.69 -3 10 9 23.93 1.66 -3 -10 9 23.36 1.64 3 10 9 26.33 1.81 4 -10 9 36.43 2.33 4 10 -9 43.44 2.39 4 10 9 45.17 2.52 -4 -10 9 42.95 2.49 5 10 -9 45.68 2.55 5 -10 9 43.38 2.48 5 10 9 46.10 2.72 -5 -10 9 45.66 2.69 6 -10 9 16.86 1.52 6 10 -9 21.53 1.83 -6 -10 9 17.02 1.62 6 10 9 18.44 1.70 7 -10 9 29.33 1.97 7 10 -9 29.43 2.23 7 10 9 23.53 2.11 8 -10 9 23.48 1.82 8 10 -9 26.16 2.25 8 10 9 27.46 2.47 9 -10 9 18.65 1.60 9 10 -9 22.25 2.06 9 10 9 18.72 2.32 10 10 -9 2.89 1.58 10 10 9 3.82 1.83 0 -11 9 4.40 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6.84 0.49 1 12 9 6.44 1.13 -1 12 -9 6.07 1.23 2 12 -9 8.42 1.22 2 -12 9 6.10 1.14 -2 12 9 9.62 1.29 2 12 9 8.93 1.24 -2 -12 9 6.85 1.21 -3 12 9 24.83 1.96 3 -12 9 21.16 1.83 3 12 -9 23.62 1.83 -3 -12 9 23.41 1.94 3 12 9 28.27 1.93 4 -12 9 18.39 1.67 -4 12 9 23.88 2.00 4 12 -9 20.65 1.76 4 12 9 16.95 1.71 -4 -12 9 19.26 1.81 5 12 -9 36.70 2.40 5 -12 9 38.52 2.42 -5 -12 9 42.35 2.56 5 12 9 41.00 2.45 6 12 -9 13.05 1.53 6 -12 9 11.76 1.46 -6 -12 9 12.50 1.56 6 12 9 14.94 1.79 7 -12 9 2.48 1.09 7 12 -9 2.95 1.21 7 12 9 2.60 1.47 8 12 -9 21.77 2.04 8 -12 9 22.40 1.92 8 12 9 24.98 2.50 9 -12 9 5.61 1.25 9 12 -9 9.98 1.76 9 12 9 4.89 1.90 10 12 -9 22.26 2.46 10 12 9 21.76 2.77 0 13 9 17.33 1.56 0 13 -9 14.14 1.61 0 -13 9 13.72 1.60 0 13 -9 16.30 1.05 1 13 -9 16.23 1.16 1 -13 9 13.82 1.57 1 13 -9 14.77 1.55 -1 13 9 16.96 1.57 -1 13 -9 12.04 1.54 -1 13 -9 13.65 0.78 -1 -13 9 15.13 1.61 1 13 9 14.45 1.36 2 13 -9 18.51 1.32 -2 13 9 18.05 1.68 2 -13 9 21.18 1.78 2 13 -9 17.94 1.63 -2 -13 9 12.19 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1.28 0.66 -3 5 -10 0.91 0.69 3 -5 -10 0.23 0.70 3 5 10 0.86 0.64 4 5 -10 58.57 2.90 4 -5 10 58.94 2.86 4 -5 10 55.18 2.42 -4 -5 10 57.20 2.88 4 -5 -10 60.59 3.01 4 5 10 58.41 2.84 5 5 -10 50.01 2.56 5 -5 10 46.40 2.40 5 -5 10 42.58 2.03 5 -5 -10 45.48 2.67 -5 -5 10 44.40 2.44 5 5 10 49.40 2.50 6 -5 10 105.71 4.70 6 -5 10 107.81 4.42 6 5 -10 101.72 4.85 -6 -5 10 106.39 4.74 6 -5 -10 99.91 5.02 6 5 10 102.88 4.81 7 -5 10 23.03 1.60 7 -5 10 21.89 1.41 7 5 -10 24.92 2.07 7 -5 -10 23.34 2.19 7 5 10 22.41 1.91 8 -5 10 -0.69 0.73 8 5 -10 1.70 1.24 8 -5 10 0.33 0.73 8 5 10 -0.39 1.06 8 -5 -10 1.95 1.42 9 -5 10 1.27 0.76 9 5 -10 2.76 1.42 9 5 10 2.48 1.37 9 -5 -10 1.66 1.66 10 5 -10 0.35 1.49 10 5 10 -0.41 1.43 10 -5 -10 1.99 1.76 11 5 -10 -0.98 1.81 11 -5 -10 3.04 2.14 11 5 10 3.20 1.90 0 6 -10 0.92 0.66 0 6 10 1.49 0.66 0 -6 10 0.88 0.63 0 -6 -10 1.29 0.43 1 6 -10 53.13 2.56 -1 -6 -10 52.67 2.35 -1 6 10 55.04 2.65 1 -6 10 54.00 2.70 1 6 10 53.86 2.57 -1 -6 10 49.09 2.69 -1 6 -10 53.95 2.64 1 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2 14 43.30 2.15 1 -2 -14 41.20 2.15 -2 -2 -14 1.79 0.61 2 2 -14 2.79 0.86 2 -2 14 2.94 0.61 2 -2 -14 3.65 0.85 -2 -2 14 3.05 0.85 -2 2 -14 3.23 0.81 2 2 14 3.74 0.76 3 2 -14 7.29 1.11 -3 -2 -14 7.51 0.84 3 -2 14 6.89 0.75 -3 2 -14 5.40 0.92 3 2 14 7.43 0.89 3 -2 -14 10.32 1.20 -3 -2 14 8.33 1.10 4 2 -14 67.63 3.37 -4 2 14 65.42 3.23 4 -2 14 65.03 2.92 -4 2 -14 61.34 3.15 4 2 14 65.04 3.11 4 -2 -14 63.86 3.35 -4 -2 14 67.93 3.31 5 2 -14 16.34 1.71 -5 2 14 14.33 1.35 5 -2 14 14.67 1.13 5 2 14 17.16 1.36 -5 -2 14 17.91 1.55 5 -2 -14 18.16 1.73 6 2 -14 17.69 1.88 6 -2 14 17.85 1.35 6 -2 -14 20.19 1.84 6 2 14 21.71 1.66 -6 -2 14 19.88 1.63 7 2 -14 0.66 1.30 7 -2 14 2.02 0.82 7 2 14 1.24 1.03 7 -2 -14 3.09 1.43 8 -2 14 35.59 2.17 8 -2 14 37.39 2.39 8 2 -14 35.59 2.83 8 2 14 34.74 2.43 8 -2 -14 34.00 2.89 9 -2 14 6.56 1.25 9 2 -14 6.07 1.86 9 -2 -14 6.58 1.91 9 2 14 6.57 1.35 10 2 -14 32.79 3.08 10 2 14 32.23 2.62 10 -2 -14 34.55 3.21 0 3 14 38.83 2.06 0 -3 -14 35.35 1.90 0 -3 14 35.82 2.17 0 3 -14 35.38 1.95 -1 -3 -14 10.50 0.93 1 -3 14 9.66 1.15 -1 3 14 9.65 1.15 1 -3 14 9.53 0.88 1 3 -14 9.62 1.11 1 -3 -14 9.40 1.03 -1 3 -14 11.31 1.11 1 3 14 10.76 1.07 -1 -3 14 9.52 1.17 2 3 -14 106.63 4.63 2 -3 14 102.64 4.33 -2 -3 -14 103.95 4.38 -2 -3 14 104.20 4.76 2 3 14 95.36 4.47 2 -3 -14 98.25 4.56 -2 3 -14 101.58 4.60 -3 -3 -14 35.84 1.79 3 3 -14 35.93 2.17 3 -3 14 36.14 1.73 -3 -3 14 33.70 2.14 3 3 14 32.80 1.91 3 -3 -14 35.85 2.12 -3 3 -14 32.97 2.02 4 -3 14 16.06 1.03 4 3 -14 14.88 1.43 4 3 14 16.17 1.31 4 -3 -14 15.77 1.57 -4 -3 14 14.39 1.46 -5 3 14 53.61 2.76 5 -3 14 54.26 2.42 5 3 -14 51.73 2.97 -5 -3 14 47.17 2.75 5 3 14 49.40 2.64 5 -3 -14 50.79 2.99 6 3 -14 20.86 1.95 6 -3 14 16.58 1.26 6 -3 -14 17.31 1.93 -6 -3 14 19.89 1.65 6 3 14 15.82 1.48 7 -3 14 23.26 1.60 7 3 -14 24.22 2.28 7 -3 14 25.85 1.95 7 3 14 26.41 1.94 7 -3 -14 25.67 2.41 8 -3 14 10.80 1.41 8 3 -14 11.55 1.95 8 -3 -14 11.20 1.95 8 3 14 10.30 1.46 9 3 -14 5.16 1.83 9 -3 14 7.32 1.30 9 -3 -14 5.82 1.88 9 3 14 5.13 1.36 10 3 -14 18.07 2.52 10 -3 -14 21.12 2.76 10 3 14 23.65 2.25 0 -4 -14 142.90 6.23 0 -4 14 154.44 6.61 0 4 -14 145.96 6.37 0 4 14 149.17 6.38 1 4 -14 4.72 0.94 -1 4 14 3.32 0.76 -1 -4 -14 3.98 0.65 1 -4 14 3.92 0.94 1 4 14 3.83 0.84 1 -4 -14 3.09 0.79 -1 -4 14 3.22 0.92 -1 4 -14 3.34 0.88 2 4 -14 17.99 1.49 2 -4 14 19.24 1.10 -2 4 14 19.80 1.61 -2 -4 -14 17.22 1.11 2 -4 14 14.47 1.44 2 4 14 17.42 1.34 -2 4 -14 16.72 1.48 2 -4 -14 16.24 1.39 -2 -4 14 14.69 1.46 -3 -4 -14 2.10 0.55 3 -4 14 1.94 0.50 3 -4 14 2.98 0.90 3 4 -14 2.91 0.82 -3 -4 14 2.11 0.89 -3 4 -14 3.22 0.98 3 -4 -14 2.26 0.89 3 4 14 2.49 0.82 4 -4 14 29.16 1.45 4 4 -14 27.68 2.03 4 -4 14 29.30 1.93 -4 -4 14 28.81 1.92 4 -4 -14 23.20 1.79 4 4 14 28.04 1.86 5 -4 14 14.43 1.41 5 4 -14 14.18 1.63 -5 4 14 14.43 1.36 5 -4 14 14.87 1.02 5 4 14 14.25 1.41 -5 -4 14 16.00 1.54 5 -4 -14 10.51 1.56 6 -4 14 20.16 1.68 6 4 -14 19.35 1.90 6 -4 14 15.79 1.19 6 4 14 17.60 1.59 6 -4 -14 16.68 1.90 -6 -4 14 18.19 1.64 7 -4 14 25.90 1.93 7 4 -14 21.62 2.19 7 -4 -14 21.87 2.29 7 4 14 25.02 1.95 8 4 -14 19.45 2.20 8 -4 14 18.82 1.75 8 -4 -14 21.00 2.40 8 4 14 22.62 1.98 9 -4 14 4.66 1.19 9 4 -14 5.98 1.85 9 -4 -14 4.81 1.92 9 4 14 3.89 1.35 10 4 -14 4.95 1.89 10 4 14 6.17 1.73 10 -4 -14 3.52 2.15 0 -5 -14 21.09 1.42 0 5 14 21.96 1.62 0 5 -14 24.21 1.51 0 -5 14 21.00 1.56 1 -5 14 19.27 1.63 1 5 -14 21.44 1.44 -1 -5 -14 19.60 1.24 -1 5 14 22.56 1.67 1 5 14 18.83 1.35 -1 5 -14 20.36 1.62 -1 -5 14 18.67 1.56 1 -5 -14 19.56 1.38 -2 -5 -14 60.58 2.76 2 5 -14 63.66 3.06 2 -5 14 61.98 3.21 -2 5 14 62.07 3.19 2 -5 -14 62.74 3.06 2 5 14 61.86 3.03 -2 5 -14 59.80 3.09 -2 -5 14 62.45 3.24 3 -5 14 49.36 2.81 -3 -5 -14 50.60 2.33 3 5 -14 47.74 2.77 3 -5 14 51.83 2.30 3 -5 -14 55.83 2.81 3 5 14 54.77 2.67 -3 5 -14 51.97 2.80 -3 -5 14 53.04 2.86 4 -5 14 21.58 1.76 4 5 -14 20.68 1.84 4 -5 14 24.35 1.23 4 5 14 26.31 1.72 -4 -5 14 24.58 1.80 4 -5 -14 20.45 1.85 5 -5 14 8.16 1.17 5 -5 14 8.34 0.70 5 5 -14 8.34 1.40 5 5 14 4.88 1.08 -5 -5 14 6.99 1.10 5 -5 -14 6.78 1.39 6 5 -14 22.47 2.12 6 -5 14 22.54 1.86 6 -5 -14 21.97 2.17 -6 -5 14 27.09 2.00 6 5 14 27.61 2.01 7 5 -14 2.76 1.46 7 -5 14 1.60 1.05 7 5 14 2.67 1.15 7 -5 -14 1.68 1.54 8 -5 14 24.53 1.98 8 5 -14 24.44 2.39 8 -5 -14 29.45 2.76 8 5 14 24.77 2.16 9 5 -14 16.16 2.17 9 -5 14 12.94 1.52 9 5 14 12.36 1.79 9 -5 -14 14.28 2.39 10 5 -14 22.91 2.63 10 -5 -14 26.16 2.95 10 5 14 22.64 2.44 0 6 14 40.78 2.40 0 -6 -14 43.65 2.14 0 -6 14 44.63 2.54 0 6 -14 41.63 2.29 -1 6 14 72.21 3.54 1 -6 14 76.13 3.73 -1 -6 -14 73.73 3.28 1 6 -14 74.09 3.59 1 6 14 77.79 3.57 1 -6 -14 72.80 3.43 -1 6 -14 70.08 3.59 -1 -6 14 76.07 3.74 -2 6 14 12.30 1.42 2 6 -14 10.92 1.32 -2 -6 -14 13.39 0.94 2 -6 14 9.85 1.28 -2 6 -14 13.90 1.39 2 -6 -14 14.27 1.28 2 6 14 13.55 1.29 -2 -6 14 12.46 1.38 3 6 -14 5.20 1.15 3 -6 14 5.71 1.07 -3 -6 -14 5.49 0.56 -3 6 -14 4.45 1.10 -3 -6 14 5.35 1.08 3 6 14 5.19 1.00 3 -6 -14 6.43 1.10 4 -6 14 37.35 1.66 4 6 -14 37.67 2.38 4 -6 14 38.98 2.32 4 6 14 37.24 2.20 4 -6 -14 34.17 2.20 -4 -6 14 36.28 2.32 5 -6 14 24.49 1.92 5 6 -14 22.83 1.87 -5 -6 14 26.56 1.89 5 6 14 22.17 1.82 5 -6 -14 23.91 2.08 6 -6 14 66.83 3.47 6 6 -14 59.96 3.53 -6 -6 14 66.14 3.48 6 6 14 65.01 3.40 6 -6 -14 65.57 3.70 7 6 -14 12.76 1.81 7 -6 14 8.82 1.38 7 -6 -14 12.10 1.99 7 6 14 12.18 1.59 8 -6 14 40.67 2.70 8 6 -14 43.58 3.03 8 -6 -14 39.93 3.28 8 6 14 43.35 2.85 9 -6 14 0.72 1.14 9 6 -14 2.13 1.71 9 6 14 1.96 1.43 9 -6 -14 1.82 1.91 10 6 -14 21.50 2.57 10 -6 -14 23.66 2.95 10 6 14 18.57 2.25 0 7 14 2.24 0.78 0 -7 14 1.07 0.91 0 7 -14 1.63 0.95 0 -7 -14 2.03 0.67 -1 -7 -14 39.52 1.94 -1 7 14 38.94 2.37 1 7 -14 40.21 2.32 1 -7 14 42.57 2.46 -1 7 -14 35.74 2.18 -1 -7 14 34.89 2.25 1 7 14 37.10 2.26 1 -7 -14 41.23 2.12 2 -7 14 62.12 3.18 2 7 -14 64.24 3.11 -2 -7 -14 58.22 2.60 -2 7 14 57.33 3.03 2 7 14 60.81 3.00 -2 7 -14 53.94 3.06 -2 -7 14 58.89 3.19 2 -7 -14 53.09 2.91 3 7 -14 31.51 2.07 -3 7 14 26.93 2.19 -3 -7 -14 27.51 1.35 3 -7 14 28.73 2.04 -3 7 -14 29.12 2.16 3 -7 -14 26.57 1.96 3 7 14 30.03 1.93 -3 -7 14 30.04 2.09 4 7 -14 59.11 3.04 4 -7 14 60.98 3.16 4 -7 -14 52.85 3.14 -4 -7 14 57.86 3.18 4 7 14 58.33 3.04 5 -7 14 3.50 1.13 5 7 -14 -0.16 1.11 5 7 14 1.18 1.02 5 -7 -14 2.60 1.26 -5 -7 14 2.90 1.00 6 -7 14 28.73 2.13 6 7 -14 25.63 2.10 6 7 14 25.45 2.11 6 -7 -14 27.74 2.43 -6 -7 14 28.52 2.16 7 -7 14 13.96 1.58 7 7 -14 10.87 1.79 7 7 14 11.77 1.62 7 -7 -14 12.76 1.98 8 7 -14 3.32 1.60 8 -7 14 1.91 1.13 8 7 14 2.38 1.48 8 -7 -14 2.15 1.74 9 -7 14 19.15 1.81 9 7 -14 20.29 2.37 9 7 14 19.87 2.29 9 -7 -14 20.50 2.62 10 7 -14 7.25 2.12 10 -7 -14 4.01 2.27 10 7 14 3.73 1.71 0 8 -14 15.27 1.55 0 -8 -14 14.77 1.20 0 -8 14 14.70 1.55 0 8 14 14.18 1.47 -1 -8 -14 46.23 2.17 1 8 -14 46.88 2.49 -1 8 14 46.79 2.65 1 -8 14 52.45 2.77 -1 8 -14 42.36 2.60 1 8 14 43.98 2.53 1 -8 -14 41.08 2.31 -1 -8 14 41.62 2.67 2 8 -14 10.11 1.36 -2 -8 -14 11.07 0.81 2 -8 14 8.45 1.30 -2 8 14 8.91 1.37 -2 8 -14 9.62 1.40 2 8 14 10.37 1.27 -2 -8 14 10.43 1.26 2 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2 -9 14 25.97 2.03 -2 -9 -14 24.20 1.29 2 9 14 22.43 1.67 -2 -9 14 23.84 2.04 2 -9 -14 28.76 1.89 -2 9 -14 29.03 2.08 3 -9 14 6.25 1.20 3 9 -14 6.31 1.30 -3 9 14 5.80 1.35 3 -9 -14 8.42 1.23 -3 -9 14 8.00 1.18 -3 9 -14 5.08 1.38 3 9 14 8.32 1.28 4 9 -14 7.45 1.43 4 -9 14 9.99 1.37 -4 -9 14 7.00 1.32 4 9 14 8.41 1.34 4 -9 -14 8.48 1.41 5 9 -14 19.73 1.99 5 -9 14 20.27 1.85 5 9 14 23.79 1.96 -5 -9 14 25.07 2.04 5 -9 -14 20.82 2.09 6 9 -14 22.44 2.20 6 -9 14 25.61 2.13 6 -9 -14 24.83 2.38 -6 -9 14 29.39 2.26 6 9 14 25.75 2.19 7 9 -14 8.44 1.69 7 -9 14 7.99 1.43 7 9 14 7.00 1.57 7 -9 -14 5.03 1.78 8 9 -14 4.79 1.67 8 -9 14 4.89 1.34 8 -9 -14 3.55 1.87 8 9 14 3.05 1.51 9 -9 14 1.66 1.24 9 9 -14 2.79 1.74 9 9 14 2.47 1.62 9 -9 -14 -1.99 1.93 10 9 -14 1.90 1.86 10 -9 -14 0.52 2.19 10 9 14 2.91 1.83 0 -10 14 35.16 2.41 0 10 -14 34.03 2.35 0 10 14 33.15 2.29 0 -10 -14 34.73 1.92 1 10 -14 13.40 1.59 -1 10 14 10.27 1.47 -1 -10 -14 12.98 1.03 1 -10 14 10.62 1.45 1 10 14 13.14 1.46 1 -10 -14 10.71 1.22 -1 -10 14 10.97 1.36 -1 10 -14 13.50 1.61 2 -10 14 4.02 1.14 -2 10 14 0.63 1.15 -2 -10 -14 3.21 0.54 2 10 -14 2.07 1.16 -2 10 -14 3.33 1.27 2 -10 -14 4.15 1.08 2 10 14 4.23 1.12 -2 -10 14 2.51 1.13 3 10 -14 71.61 3.59 3 -10 14 64.51 3.58 -3 10 14 63.56 3.68 3 10 14 68.24 3.52 -3 -10 14 67.75 3.67 3 -10 -14 68.70 3.57 -3 10 -14 65.67 3.69 4 -10 14 44.16 2.66 4 10 -14 44.32 2.69 4 10 14 37.15 2.36 4 -10 -14 38.05 2.62 -4 -10 14 37.15 2.63 5 10 -14 25.30 2.22 5 -10 14 21.73 2.01 -5 -10 14 29.16 2.30 5 -10 -14 27.62 2.34 6 10 -14 21.00 2.11 6 -10 14 20.63 1.95 -6 -10 14 18.72 1.89 6 -10 -14 14.77 2.12 6 10 14 17.75 1.93 7 10 -14 12.19 1.87 7 -10 14 10.85 1.62 7 -10 -14 9.55 2.03 7 10 14 12.58 1.81 8 10 -14 29.88 2.68 8 -10 14 30.46 2.39 8 -10 -14 25.61 2.91 8 10 14 29.90 2.67 9 10 -14 8.84 1.95 9 -10 14 3.26 1.38 9 10 14 6.13 1.88 9 -10 -14 4.04 2.19 0 -11 -14 70.59 3.25 0 11 -14 65.97 3.62 0 -11 14 68.51 3.75 0 11 14 68.13 3.47 -1 -11 -14 12.36 1.01 1 -11 14 13.01 1.58 -1 11 14 10.97 1.54 1 11 -14 9.32 1.50 -1 -11 14 9.88 1.51 1 -11 -14 11.77 1.26 1 11 14 9.65 1.43 -1 11 -14 9.42 1.51 -2 -11 -14 54.54 2.40 2 11 -14 58.44 3.14 -2 11 14 55.14 3.19 2 -11 14 53.54 3.02 2 -11 -14 55.43 2.96 -2 -11 14 49.32 3.15 -2 11 -14 50.04 2.99 2 11 14 51.86 3.00 3 -11 14 15.64 1.74 3 11 -14 17.91 1.84 -3 11 14 17.40 1.93 -3 11 -14 14.88 1.90 3 11 14 15.87 1.72 3 -11 -14 15.03 1.65 -3 -11 14 18.28 1.88 4 11 -14 11.23 1.63 4 -11 14 10.39 1.52 4 11 14 13.05 1.61 4 -11 -14 10.12 1.61 -4 -11 14 13.15 1.69 5 -11 14 35.65 2.52 5 11 -14 37.98 2.61 -5 -11 14 33.38 2.52 5 11 14 37.13 2.58 5 -11 -14 31.21 2.68 6 11 -14 20.45 2.15 6 -11 14 22.65 2.11 6 -11 -14 19.44 2.33 6 11 14 23.85 2.19 -6 -11 14 20.61 2.03 7 -11 14 17.56 1.90 7 11 -14 20.46 2.25 7 -11 -14 15.35 2.30 7 11 14 15.71 2.07 8 -11 14 5.62 1.52 8 11 -14 6.53 1.94 8 11 14 4.93 1.72 8 -11 -14 2.57 1.99 9 11 -14 0.63 1.71 9 -11 14 0.31 1.32 9 11 14 1.84 1.72 9 -11 -14 1.87 2.09 0 12 14 34.19 2.40 0 -12 -14 32.61 1.92 0 -12 14 32.56 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9 15 4.02 1.37 3 9 -15 3.35 1.26 -3 -9 15 5.10 1.23 3 -9 -15 5.88 1.19 3 9 15 3.83 0.96 -3 9 -15 4.60 1.31 4 -9 15 4.42 1.22 4 9 -15 6.19 1.19 4 -9 -15 5.09 1.32 4 9 15 7.17 1.32 -4 -9 15 5.07 1.27 5 -9 15 108.32 5.05 5 9 -15 100.30 5.01 5 9 15 94.82 4.90 5 -9 -15 102.79 5.12 -5 -9 15 106.95 5.11 6 9 -15 25.91 2.29 6 -9 15 24.02 2.05 -6 -9 15 22.26 2.12 6 9 15 23.58 2.12 6 -9 -15 20.59 2.35 7 -9 15 25.50 2.22 7 9 -15 27.82 2.55 7 -9 -15 33.35 2.73 7 9 15 33.41 2.55 8 -9 15 3.40 1.41 8 9 -15 4.11 1.78 8 9 15 3.77 1.62 8 -9 -15 4.51 1.62 9 9 -15 1.36 1.73 9 -9 15 0.04 1.29 9 -9 -15 0.93 2.07 9 9 15 0.97 1.66 0 -10 15 2.89 1.20 0 10 -15 4.15 1.24 0 10 15 5.47 1.26 0 -10 -15 5.13 0.88 1 -10 15 0.61 1.06 -1 -10 -15 -0.05 0.58 1 10 -15 -0.02 1.12 -1 10 15 -0.87 1.05 1 10 15 1.50 1.07 -1 -10 15 -0.31 1.05 1 -10 -15 -0.55 0.79 -1 10 -15 1.48 1.14 2 10 -15 73.15 3.89 -2 -10 -15 76.33 3.28 -2 10 15 79.87 4.04 2 -10 15 78.90 4.03 2 -10 -15 76.53 3.71 2 10 15 75.67 3.84 -2 10 -15 70.04 3.95 -2 -10 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0 -22 30.15 2.23 -3 0 22 4.37 1.35 3 0 22 3.73 1.16 -3 0 -22 4.37 1.20 3 0 -22 6.97 1.55 4 0 22 3.99 1.13 -4 0 22 4.61 1.51 -4 0 -22 0.43 1.17 4 0 -22 3.12 1.52 5 0 22 6.66 1.32 5 0 -22 7.22 1.85 6 0 -22 16.95 2.33 7 0 -22 2.64 1.94 8 0 -22 17.80 2.68 0 1 -22 0.50 1.10 0 -1 -22 0.29 1.04 0 -1 22 1.20 0.98 -1 -1 -22 32.31 2.14 1 1 -22 31.08 2.39 -1 1 -22 32.64 2.23 1 -1 -22 27.01 2.26 -1 -1 22 29.27 2.51 1 1 22 28.48 2.20 2 1 -22 29.88 2.46 2 -1 22 33.89 2.23 -2 1 22 32.67 2.57 -2 -1 -22 30.66 2.24 2 1 22 33.58 2.32 -2 1 -22 30.45 2.26 -2 -1 22 32.38 2.62 2 -1 -22 33.26 2.46 3 -1 22 1.18 1.04 -3 -1 -22 -0.31 0.99 3 1 -22 -0.01 1.23 -3 1 22 0.35 1.18 -3 1 -22 0.59 1.13 -3 -1 22 1.49 1.24 3 -1 -22 1.07 1.34 3 1 22 0.92 1.11 -4 -1 -22 3.15 1.21 -4 1 22 5.13 1.40 4 -1 22 2.70 1.04 4 1 -22 2.69 1.23 -4 -1 22 1.58 1.26 4 -1 -22 5.82 1.64 4 1 22 2.56 1.15 -4 1 -22 2.54 1.30 5 1 -22 3.58 1.71 -5 1 22 1.09 1.19 5 -1 -22 5.10 1.72 5 1 22 1.75 1.14 -5 -1 22 3.68 1.34 6 1 -22 2.58 1.82 6 1 22 0.18 1.20 6 -1 -22 0.20 1.69 7 1 -22 5.88 2.06 7 -1 22 4.15 1.67 7 -1 -22 7.03 2.14 8 1 -22 11.96 2.51 8 -1 22 12.57 2.18 8 -1 -22 10.32 2.09 0 -2 22 19.09 2.11 0 2 22 24.34 2.06 0 2 -22 21.63 1.97 0 -2 -22 21.12 1.83 -1 -2 -22 28.76 1.99 1 2 -22 29.43 2.33 1 -2 22 27.03 2.45 1 -2 -22 27.29 2.17 -1 -2 22 29.23 2.47 1 2 22 29.45 2.17 -1 2 -22 23.68 2.14 -2 -2 -22 0.89 1.00 2 2 -22 2.01 1.32 2 -2 22 0.80 1.02 2 2 22 -0.53 1.03 -2 -2 22 1.50 0.99 2 -2 -22 0.42 1.20 -2 2 -22 -0.60 1.18 3 -2 22 17.90 1.54 -3 2 22 17.78 1.94 -3 -2 -22 18.81 1.69 3 2 -22 18.89 2.03 3 -2 22 13.73 1.97 -3 -2 22 16.72 1.97 3 2 22 16.25 1.75 3 -2 -22 14.44 1.88 -3 2 -22 13.54 1.70 4 2 -22 11.35 1.90 4 -2 22 18.01 2.17 -4 2 22 18.32 1.98 -4 -2 22 17.22 2.00 4 2 22 19.99 1.80 4 -2 -22 17.69 2.07 -4 2 -22 14.70 1.84 5 -2 22 12.79 1.97 5 2 -22 11.17 2.00 -5 2 22 8.94 1.60 -5 -2 22 10.11 1.83 5 2 22 11.85 1.50 5 -2 -22 12.17 1.99 6 -2 22 3.32 1.77 6 2 -22 4.15 1.80 6 2 22 2.48 1.34 6 -2 -22 4.03 1.86 7 -2 22 1.23 1.55 7 2 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1.78 0 -5 -22 8.48 1.27 -1 -5 -22 8.09 1.23 1 -5 22 5.47 1.58 -1 5 22 7.87 1.68 1 5 -22 8.00 1.59 1 5 22 7.65 1.47 -1 -5 22 7.55 1.62 -1 5 -22 6.67 1.51 1 -5 -22 6.64 1.32 2 5 -22 5.11 1.57 2 -5 22 3.15 1.53 -2 -5 -22 3.81 1.06 -2 -5 22 2.91 1.47 2 -5 -22 5.77 1.39 2 5 22 3.74 1.37 -2 5 -22 4.00 1.40 3 5 -22 10.33 1.83 3 -5 22 11.07 1.82 -3 -5 22 11.03 1.78 3 -5 -22 9.78 1.75 -3 5 -22 11.81 1.78 3 5 22 9.66 1.61 4 5 -22 12.50 1.99 4 -5 22 10.74 1.88 4 -5 -22 10.79 1.82 -4 5 -22 9.24 1.73 -4 -5 22 11.56 1.80 4 5 22 8.36 1.56 5 -5 22 22.96 2.44 5 5 -22 21.06 2.49 -5 -5 22 25.73 2.37 5 5 22 22.11 2.19 5 -5 -22 24.83 2.49 6 5 -22 29.09 2.94 6 -5 22 31.08 2.84 6 5 22 31.24 2.57 6 -5 -22 34.71 3.01 7 -5 22 1.70 1.61 7 5 -22 5.79 2.18 7 -5 -22 4.69 2.04 7 5 22 1.83 1.41 8 5 -22 1.13 2.11 8 -5 22 0.17 1.68 8 -5 -22 3.33 2.22 8 5 22 2.48 1.54 0 6 22 10.26 1.75 0 -6 22 9.73 1.78 0 6 -22 9.57 1.66 0 -6 -22 10.23 1.42 -1 6 22 7.29 1.72 -1 -6 -22 10.25 1.33 1 -6 22 10.41 1.85 1 6 -22 5.75 1.52 -1 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7 22 37.43 2.83 3 7 -22 7.36 1.79 3 -7 22 5.56 1.61 -3 -7 22 6.89 1.67 3 -7 -22 6.16 1.52 -3 7 -22 4.52 1.72 3 7 22 5.68 1.54 4 -7 22 9.46 1.87 4 7 -22 9.49 1.96 -4 7 -22 12.70 2.09 4 7 22 8.61 1.68 -4 -7 22 8.06 1.74 4 -7 -22 8.37 1.82 5 7 -22 23.33 2.57 5 -7 22 24.10 2.63 -5 -7 22 26.66 2.50 5 7 22 24.84 2.31 5 -7 -22 20.25 2.40 6 -7 22 1.36 1.56 6 7 -22 -0.57 1.76 6 -7 -22 2.71 1.80 6 7 22 -0.06 1.43 7 -7 22 19.69 2.49 7 7 -22 12.33 2.51 7 -7 -22 13.16 2.43 7 7 22 19.36 2.29 0 8 22 53.73 3.41 0 -8 22 52.95 3.52 0 8 -22 50.57 3.34 0 -8 -22 49.10 2.84 -1 8 22 0.10 1.53 1 8 -22 3.25 1.58 -1 -8 -22 0.58 0.93 1 -8 22 3.82 1.59 1 -8 -22 1.26 1.20 -1 8 -22 0.26 1.39 1 8 22 0.05 1.43 -1 -8 22 1.91 1.53 2 8 -22 14.28 1.81 2 -8 22 10.44 1.97 -2 8 22 14.82 2.21 -2 -8 22 16.83 1.93 2 8 22 14.64 1.92 -2 8 -22 14.58 2.09 2 -8 -22 12.26 1.67 3 -8 22 9.97 1.89 3 8 -22 8.59 1.92 -3 8 -22 9.28 1.86 3 8 22 10.06 1.74 -3 -8 22 9.70 1.82 3 -8 -22 9.89 1.78 4 8 -22 3.07 1.78 4 -8 22 0.19 1.55 -4 -8 22 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-26 0.96 1.83 2 10 26 2.33 1.93 2 -10 -26 -0.39 1.33 3 10 -26 35.25 3.30 3 -10 26 38.22 3.47 3 10 26 29.10 3.01 3 -10 -26 35.64 2.95 -3 10 -26 26.87 3.06 -3 -10 26 36.15 3.38 0 11 -26 3.53 2.03 0 11 26 1.37 2.00 0 -11 26 1.14 1.90 1 -11 26 1.86 1.97 -1 11 26 1.41 2.09 1 11 -26 2.73 2.05 -1 11 -26 0.70 1.80 -1 -11 26 0.85 1.82 1 11 26 0.50 1.92 2 11 -26 0.93 2.01 2 -11 26 0.62 1.88 2 -11 -26 4.03 1.61 2 11 26 2.84 2.00 -2 -11 26 3.03 1.95 -2 11 -26 4.61 2.12 3 -11 26 -0.38 1.92 3 11 -26 -0.35 1.97 -3 11 -26 -0.81 1.80 3 -11 -26 -0.48 1.71 -3 -11 26 1.70 1.93 3 11 26 0.73 1.88 0 12 -26 14.69 2.56 0 -12 26 15.05 2.59 0 12 26 18.45 2.78 1 12 -26 8.27 2.37 1 -12 26 4.09 2.11 -1 12 26 3.48 2.28 -1 -12 26 10.13 2.35 -1 12 -26 7.39 2.28 1 12 26 8.62 2.26 2 12 -26 14.31 2.49 2 -12 26 10.46 2.43 -2 -12 26 12.81 2.47 2 -12 -26 10.64 2.12 -2 12 -26 16.26 2.56 2 12 26 13.76 2.51 0 0 27 -0.09 1.66 0 0 -27 -0.27 1.52 1 0 27 3.42 1.84 -1 0 -27 3.68 1.61 1 0 -27 4.53 1.61 -1 0 27 4.27 1.82 -2 0 -27 -2.42 1.31 2 0 27 -0.78 1.77 2 0 -27 1.82 1.63 -2 0 27 -0.05 1.61 3 0 27 30.13 3.16 -3 0 27 29.66 2.89 3 0 -27 32.27 2.99 -4 0 27 3.03 1.72 4 0 27 7.55 2.23 4 0 -27 5.69 1.90 5 0 27 16.46 2.63 5 0 -27 13.91 2.34 0 -1 -27 1.66 1.38 0 1 27 -0.25 1.63 0 -1 27 -0.83 1.57 0 1 -27 0.15 1.41 -1 1 27 5.91 1.90 1 -1 27 5.05 1.95 -1 -1 -27 4.04 1.54 1 1 -27 5.91 1.70 -1 1 -27 4.12 1.66 1 1 27 5.19 1.61 -1 -1 27 5.99 1.58 1 -1 -27 2.97 1.56 2 -1 27 4.31 1.99 2 1 -27 4.38 1.73 -2 -1 -27 4.54 1.57 -2 1 27 5.69 1.87 -2 -1 27 1.47 1.71 2 -1 -27 3.82 1.79 -2 1 -27 4.57 1.62 -3 1 27 -0.07 1.57 3 1 -27 0.87 1.68 3 -1 27 2.74 1.95 3 -1 -27 3.72 1.77 -3 -1 27 -1.25 1.53 -3 1 -27 2.95 1.52 3 1 27 3.00 1.40 -4 1 27 10.44 2.05 4 1 -27 8.48 2.09 4 -1 27 8.24 2.26 4 -1 -27 11.32 2.16 -4 -1 27 13.33 2.17 5 -1 27 14.80 2.62 5 1 -27 15.51 2.47 5 -1 -27 17.06 2.50 0 -2 -27 1.84 1.51 0 -2 27 1.71 1.74 0 2 -27 4.57 1.78 -1 -2 -27 2.84 1.35 -1 2 27 4.88 1.81 1 -2 27 5.24 1.63 1 2 -27 5.09 1.83 1 -2 -27 3.65 1.51 -1 2 -27 7.16 1.71 -1 -2 27 6.23 1.92 -2 2 27 15.34 2.30 -2 -2 -27 15.12 1.95 2 -2 27 16.36 2.46 2 2 -27 15.66 2.20 -2 -2 27 16.85 2.36 -2 2 -27 15.27 2.12 2 -2 -27 16.29 2.15 2 2 27 15.65 2.01 3 -2 27 3.67 2.04 -3 2 27 1.32 1.66 3 2 -27 4.10 1.89 -3 -2 27 0.85 1.66 3 -2 -27 2.16 1.63 3 2 27 2.14 1.54 -3 2 -27 3.38 1.61 -4 2 27 10.38 2.04 4 -2 27 10.08 2.34 4 2 -27 7.89 2.19 4 -2 -27 9.82 2.17 -4 -2 27 7.60 2.11 5 2 -27 7.82 2.30 5 -2 27 13.76 2.74 5 -2 -27 8.68 2.16 0 3 -27 14.42 2.08 0 -3 -27 12.24 1.85 0 -3 27 13.80 2.31 -1 -3 -27 11.33 1.74 1 3 -27 7.59 1.91 1 -3 27 11.37 2.24 -1 3 -27 11.84 2.02 -1 -3 27 12.61 2.20 1 -3 -27 10.47 1.77 2 -3 27 1.20 1.80 2 3 -27 0.12 1.66 -2 3 27 0.27 1.57 -2 -3 27 0.27 1.57 -2 3 -27 -0.91 1.52 2 -3 -27 -1.34 1.57 2 3 27 -2.22 1.35 -3 3 27 16.26 2.35 3 -3 27 18.29 2.64 3 3 -27 18.52 2.44 -3 3 -27 14.83 2.22 3 -3 -27 17.55 2.29 3 3 27 21.27 2.29 -3 -3 27 16.56 2.42 4 3 -27 3.82 2.02 4 -3 27 6.68 2.19 -4 3 27 6.45 1.86 -4 3 -27 7.50 1.84 -4 -3 27 6.60 1.89 4 -3 -27 5.43 1.89 4 3 27 6.59 1.81 5 -3 27 3.66 2.13 5 3 -27 2.71 2.07 5 -3 -27 4.19 2.01 0 4 -27 2.92 1.81 0 -4 27 2.07 1.78 0 -4 -27 1.90 1.31 1 4 -27 28.64 2.77 -1 -4 -27 31.79 2.46 1 -4 27 32.24 3.08 1 4 27 34.01 2.87 1 -4 -27 28.12 2.59 -1 -4 27 27.66 2.90 -1 4 -27 27.96 2.68 2 -4 27 7.08 2.06 2 4 -27 8.76 2.01 2 -4 -27 8.17 1.77 -2 -4 27 10.34 2.15 -2 4 -27 9.20 1.95 2 4 27 12.43 2.10 3 -4 27 2.09 1.92 -3 4 27 -1.23 1.54 3 4 -27 -1.32 1.69 -3 4 -27 -1.41 1.58 3 -4 -27 0.40 1.57 -3 -4 27 -0.57 1.55 3 4 27 0.87 1.49 4 -4 27 3.93 2.10 -4 4 27 4.50 1.79 4 4 -27 0.96 1.89 -4 -4 27 2.20 1.72 -4 4 -27 2.58 1.80 4 4 27 2.16 1.71 4 -4 -27 2.93 1.94 0 -5 27 27.18 2.89 0 -5 -27 26.16 2.32 0 5 -27 26.65 2.74 1 5 -27 19.81 2.50 1 -5 27 17.64 2.58 1 5 27 21.19 2.51 1 -5 -27 19.83 2.10 -1 5 -27 14.42 2.21 -1 -5 27 18.18 2.50 2 5 -27 7.19 1.92 2 -5 27 9.75 2.20 2 -5 -27 5.70 1.80 -2 5 -27 7.39 1.83 2 5 27 6.40 1.83 -2 -5 27 6.38 1.96 3 5 -27 14.76 2.38 -3 5 27 12.07 2.14 3 -5 27 16.45 2.56 -3 -5 27 10.51 2.22 3 -5 -27 14.12 2.08 -3 5 -27 15.30 2.24 3 5 27 14.12 2.17 4 -5 27 0.00 2.00 4 5 -27 2.47 2.16 -4 5 -27 0.58 1.69 4 5 27 0.52 1.57 4 -5 -27 0.50 1.71 -4 -5 27 1.87 1.70 0 6 -27 24.72 2.72 0 -6 -27 19.05 2.09 0 -6 27 23.65 2.79 0 6 27 23.43 2.67 1 -6 27 2.90 1.83 1 6 -27 0.46 1.74 1 -6 -27 1.23 1.45 -1 -6 27 4.06 1.78 1 6 27 4.33 1.85 -1 6 -27 2.42 1.85 2 6 -27 9.48 2.17 2 -6 27 11.06 2.31 -2 -6 27 7.46 2.05 -2 6 -27 11.07 2.04 2 6 27 8.57 2.11 2 -6 -27 8.77 1.77 3 -6 27 3.69 2.00 3 6 -27 2.13 1.97 -3 6 -27 3.32 1.73 3 6 27 5.48 1.83 -3 -6 27 7.65 2.03 3 -6 -27 6.11 1.95 4 -6 27 -1.31 2.13 4 6 -27 0.23 1.98 -4 6 -27 0.90 1.66 4 -6 -27 1.01 1.69 4 6 27 0.06 1.57 -4 -6 27 -0.59 1.81 0 7 27 1.40 1.85 0 7 -27 1.62 1.80 0 -7 27 3.19 1.88 1 -7 27 10.85 2.33 1 7 -27 12.37 2.26 1 7 27 16.40 2.38 1 -7 -27 12.19 1.92 -1 -7 27 14.49 2.41 -1 7 -27 12.31 2.15 2 7 -27 -0.36 1.85 2 -7 27 -0.99 1.83 -2 7 -27 1.47 1.81 -2 -7 27 2.06 1.82 2 -7 -27 0.71 1.44 2 7 27 1.82 1.72 3 7 -27 5.47 2.16 3 -7 27 6.21 2.24 3 7 27 5.22 1.88 -3 -7 27 6.38 1.99 3 -7 -27 7.30 1.82 -3 7 -27 5.80 1.88 4 -7 27 6.13 2.23 4 7 -27 7.41 2.27 4 -7 -27 1.51 1.88 -4 -7 27 5.81 1.97 0 8 27 4.68 2.07 0 -8 27 4.04 2.07 0 8 -27 4.68 1.96 1 8 -27 12.17 2.29 1 -8 27 13.85 2.44 1 -8 -27 12.95 1.92 -1 8 -27 7.08 2.16 1 8 27 12.88 2.27 -1 -8 27 13.75 2.35 2 8 -27 1.99 2.01 2 -8 27 2.04 1.98 2 -8 -27 1.93 1.57 -2 -8 27 1.67 1.78 -2 8 -27 3.15 1.84 2 8 27 -2.57 1.67 3 -8 27 31.26 3.28 3 8 -27 34.45 3.24 -3 -8 27 33.03 3.20 3 -8 -27 26.33 2.65 3 8 27 29.59 2.92 -3 8 -27 28.12 3.06 0 9 27 18.11 2.61 0 9 -27 13.98 2.34 0 -9 27 13.01 2.44 1 -9 27 2.42 1.97 1 9 -27 -0.79 1.88 -1 -9 27 -0.10 1.87 -1 9 -27 0.66 1.82 1 -9 -27 -0.34 1.47 1 9 27 -0.34 1.86 2 -9 27 11.57 2.31 2 9 -27 9.68 2.30 -2 -9 27 8.69 2.24 -2 9 -27 7.66 2.15 2 9 27 5.43 2.03 2 -9 -27 9.60 1.93 3 -9 27 5.48 2.19 3 9 -27 7.93 2.30 3 -9 -27 6.44 1.81 -3 -9 27 6.62 2.06 -3 9 -27 3.26 2.13 0 -10 27 3.09 2.03 0 10 -27 2.62 2.05 0 10 27 2.08 2.10 1 -10 27 -1.32 1.82 1 10 -27 2.42 2.06 -1 10 27 0.42 2.06 -1 -10 27 -1.98 1.75 -1 10 -27 0.41 2.05 1 10 27 0.75 1.97 2 -10 27 15.98 2.67 2 10 -27 17.28 2.63 -2 -10 27 18.83 2.67 2 -10 -27 13.55 2.08 -2 10 -27 16.81 2.59 2 10 27 15.87 2.45 0 -11 27 11.79 2.38 0 11 -27 6.25 2.18 0 0 -28 3.93 1.59 0 0 28 3.15 1.89 1 0 -28 1.31 1.52 -1 0 -28 1.91 1.61 -1 0 28 2.04 1.84 1 0 28 1.50 1.90 -2 0 -28 2.71 1.59 -2 0 28 0.74 1.70 2 0 -28 4.84 1.76 2 0 28 2.75 2.04 3 0 -28 0.05 1.72 -3 0 28 -0.78 1.81 3 0 28 2.46 1.99 4 0 28 19.08 2.80 -4 0 28 21.28 2.58 4 0 -28 22.87 2.68 0 1 28 6.00 2.03 0 -1 28 4.77 1.98 0 -1 -28 7.00 1.83 0 1 -28 3.84 1.64 -1 1 28 1.48 1.83 1 -1 28 -1.52 1.77 -1 -1 -28 0.99 1.54 1 1 -28 0.57 1.54 -1 -1 28 0.31 1.32 1 -1 -28 1.82 1.67 -1 1 -28 -2.30 1.37 1 1 28 3.42 1.97 -2 1 28 19.31 2.67 -2 -1 -28 15.36 2.02 2 -1 28 16.01 2.61 2 1 -28 14.09 2.19 2 1 28 17.41 2.64 -2 1 -28 12.22 2.01 2 -1 -28 15.90 2.23 -2 -1 28 15.14 2.42 3 -1 28 16.90 2.69 -3 1 28 15.86 2.33 3 1 -28 13.30 2.27 -3 -1 28 12.99 2.30 3 -1 -28 17.44 2.35 -4 1 28 0.59 1.63 4 1 -28 2.04 1.98 4 -1 28 2.85 2.14 4 -1 -28 5.55 1.99 -4 -1 28 0.70 1.67 0 -2 28 4.20 1.97 0 2 -28 3.69 1.86 0 2 28 5.28 2.00 0 -2 -28 6.42 1.70 -1 2 28 5.34 1.97 1 -2 28 6.36 2.07 1 2 -28 9.54 1.91 -1 -2 -28 5.28 1.66 -1 2 -28 4.29 1.67 -1 -2 28 7.38 2.07 1 -2 -28 8.43 1.75 2 -2 28 1.35 1.94 2 2 -28 -0.91 1.62 -2 2 28 -0.77 1.57 -2 -2 28 -0.86 1.69 2 -2 -28 0.25 1.67 -2 2 -28 -0.59 1.55 -3 2 28 7.78 2.01 3 2 -28 6.47 1.99 3 -2 28 6.95 2.33 3 -2 -28 4.52 1.88 3 2 28 11.07 1.80 -3 2 -28 5.00 1.80 -3 -2 28 7.22 2.06 4 2 -28 10.36 2.26 4 -2 28 12.78 2.59 -4 2 28 13.73 2.24 4 -2 -28 9.52 2.11 -4 -2 28 10.88 2.21 0 -3 28 11.30 2.31 0 -3 -28 7.80 1.62 0 3 -28 4.69 1.83 -1 -3 -28 11.08 1.82 1 3 -28 12.10 2.08 -1 3 28 9.05 2.13 1 -3 28 10.23 2.32 -1 -3 28 6.17 2.07 1 -3 -28 9.27 1.92 -1 3 -28 12.03 2.13 -2 3 28 19.13 2.54 2 3 -28 18.59 2.44 2 -3 28 24.82 2.94 -2 3 -28 18.42 2.36 2 -3 -28 19.60 2.29 -2 -3 28 19.49 2.61 2 3 28 21.00 2.31 -3 3 28 2.72 1.76 3 3 -28 3.58 1.94 3 -3 28 5.00 2.10 3 -3 -28 3.92 1.76 3 3 28 5.57 1.67 -3 -3 28 2.99 1.88 -3 3 -28 2.77 1.71 4 -3 28 3.08 2.14 -4 -3 28 3.26 1.79 0 -4 -28 18.15 2.07 0 4 -28 14.16 2.33 0 -4 28 14.83 2.49 1 4 -28 4.31 1.85 1 -4 28 5.16 2.05 1 -4 -28 5.19 1.72 -1 4 -28 2.71 1.68 -1 -4 28 7.72 2.07 -2 4 28 2.79 1.97 2 -4 28 2.22 1.93 2 4 -28 2.93 1.88 2 -4 -28 5.52 1.73 -2 4 -28 5.91 1.87 -2 -4 28 1.64 1.77 2 4 28 4.70 1.89 3 -4 28 8.71 2.36 3 4 -28 11.72 2.26 -3 4 28 7.65 2.01 -3 -4 28 6.90 2.08 3 4 28 13.20 2.03 3 -4 -28 11.22 2.02 -3 4 -28 9.17 1.93 0 -5 -28 2.50 1.46 0 -5 28 2.38 1.97 0 5 -28 2.96 1.85 1 5 -28 23.90 2.79 1 -5 28 17.56 2.69 1 5 28 23.11 2.60 -1 -5 28 20.45 2.74 1 -5 -28 26.22 2.34 -1 5 -28 19.76 2.44 2 -5 28 20.41 2.81 2 5 -28 13.68 2.35 2 -5 -28 18.23 2.34 2 5 28 18.65 2.37 -2 5 -28 17.35 2.36 -2 -5 28 19.44 2.64 3 5 -28 2.68 2.08 3 -5 28 1.92 2.03 -3 5 28 5.38 2.02 3 5 28 4.33 1.95 -3 -5 28 3.18 1.84 3 -5 -28 -0.23 1.60 -3 5 -28 -0.03 1.59 0 6 -28 0.06 1.88 0 -6 28 2.57 1.88 1 6 -28 6.84 2.01 1 -6 28 4.96 2.11 -1 6 -28 5.17 2.00 -1 -6 28 6.07 2.12 1 -6 -28 3.33 1.50 1 6 28 9.76 2.10 2 6 -28 8.33 2.14 2 -6 28 8.82 2.30 -2 -6 28 12.22 2.30 2 6 28 11.16 2.24 2 -6 -28 6.24 1.85 -2 6 -28 7.78 1.98 3 6 -28 2.98 2.07 -3 6 28 5.38 1.91 3 -6 28 5.77 2.21 -3 -6 28 5.88 2.03 3 6 28 3.54 1.84 3 -6 -28 3.57 1.85 -3 6 -28 3.16 1.78 0 7 -28 5.05 2.00 0 7 28 3.53 2.00 0 -7 28 1.24 1.94 1 7 -28 5.85 2.08 1 -7 28 5.98 2.07 1 7 28 7.65 2.11 1 -7 -28 4.63 1.65 -1 -7 28 5.04 1.99 -1 7 -28 2.21 1.78 2 7 -28 17.65 2.56 2 -7 28 17.75 2.76 -2 -7 28 16.05 2.53 -2 7 -28 15.12 2.36 2 7 28 14.15 2.35 2 -7 -28 18.71 2.19 0 -8 28 -0.40 1.89 0 8 28 -0.98 1.87 0 8 -28 -1.53 1.71 1 -8 28 0.49 1.95 1 8 -28 0.74 2.08 -1 -8 28 -0.62 1.86 1 8 28 -0.38 1.83 1 -8 -28 1.06 1.55 -1 8 -28 2.58 1.85 2 -8 28 12.17 2.44 -2 -8 28 11.11 2.36 0 -9 28 1.86 2.00 0 0 29 0.65 1.83 0 0 -29 0.06 1.61 -1 0 -29 2.32 1.61 -1 0 29 2.86 1.90 1 0 29 1.60 1.99 1 0 -29 4.39 1.84 2 0 29 -2.74 1.91 -2 0 29 -0.90 1.71 -2 0 -29 -0.11 1.51 2 0 -29 1.55 1.68 0 1 -29 -0.64 1.68 0 1 29 -1.21 1.73 0 -1 29 -2.91 1.74 0 -1 -29 -0.93 1.43 1 1 -29 7.43 1.89 1 -1 29 7.87 2.28 -1 1 29 5.14 2.03 -1 -1 -29 7.84 1.72 1 1 29 9.11 2.33 -1 1 -29 5.30 1.73 1 -1 -29 5.47 1.79 -1 -1 29 4.24 1.96 2 1 -29 4.59 1.89 2 -1 29 5.16 2.22 -2 1 29 7.47 2.11 -2 -1 29 8.24 2.18 2 1 29 10.03 2.46 2 -1 -29 10.78 2.01 -2 1 -29 8.11 1.86 0 -2 -29 -1.87 1.35 0 2 -29 0.31 1.57 0 2 29 -0.08 1.81 0 -2 29 0.08 1.89 -1 -2 -29 9.05 1.70 1 2 -29 7.83 1.96 -1 2 29 4.25 2.01 1 -2 29 6.96 2.22 -1 -2 29 6.22 2.08 -1 2 -29 6.37 1.92 1 -2 -29 7.76 1.92 2 -2 29 2.80 2.10 -2 2 29 6.26 2.06 2 2 -29 2.77 1.84 -2 -2 29 4.43 2.00 2 -2 -29 2.48 1.85 -2 2 -29 3.30 1.73 0 -3 -29 21.50 2.28 0 3 -29 11.22 2.12 0 -3 29 17.26 2.61 1 3 -29 8.11 2.03 -1 3 29 10.18 2.24 1 -3 29 11.03 2.44 -1 3 -29 13.14 2.24 1 -3 -29 8.39 1.98 -1 -3 29 12.91 2.46 2 3 -29 9.34 2.13 2 -3 29 7.10 2.35 -2 3 29 7.19 2.11 -2 -3 29 5.98 2.09 -2 3 -29 6.22 1.89 2 -3 -29 6.83 1.86 0 -4 -29 1.62 1.56 0 4 -29 -1.18 1.63 0 -4 29 1.79 1.88 1 4 -29 6.15 2.01 1 -4 29 3.15 2.10 -1 -4 29 3.88 2.03 -1 4 -29 4.09 1.80 1 -4 -29 1.30 1.51 2 -4 29 15.24 2.65 -2 4 29 11.93 2.34 -2 -4 29 14.24 2.46 0 -5 29 16.26 2.69 0 5 -29 18.28 2.47 1 5 -29 8.91 2.11 1 -5 29 5.40 2.20 1 -5 -29 10.79 1.85 -1 -5 29 12.39 2.39 -1 5 -29 7.88 1.98 0 -6 29 0.32 1.96 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 64257 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_posn _atom_site_occupancy Ge Ge1 0.13489(4) 0.76297(2) 0.74695(2) 0.01458(7) Uani d . . 1 Ge Ge2 0.02806(4) 0.86993(2) 0.65438(2) 0.01175(7) Uani d . . 1 C C1 -0.0014(4) 0.68369(15) 0.78157(13) 0.0153(6) Uani d . . 1 C C2 0.0246(4) 0.63435(16) 0.83315(12) 0.0174(6) Uani d . . 1 C C3 0.1641(4) 0.64093(17) 0.87403(13) 0.0190(7) Uani d . . 1 H H3 0.2002 0.5995 0.8978 0.023 Uiso calc U R 1 C C4 0.3802(4) 0.70849(17) 0.91724(15) 0.0198(7) Uani d . . 1 C C5 0.3383(5) 0.7574(2) 0.97519(15) 0.0291(8) Uani d . . 1 H H5A 0.2618 0.7323 1.0027 0.044 Uiso calc U R 1 H H5B 0.2941 0.8036 0.9592 0.044 Uiso calc U R 1 H H5C 0.4321 0.7677 1.0008 0.044 Uiso calc U R 1 C C6 0.4505(4) 0.63680(19) 0.94140(17) 0.0285(8) Uani d . . 1 H H6A 0.47 0.6043 0.9042 0.043 Uiso calc U R 1 H H6B 0.378 0.613 0.9716 0.043 Uiso calc U R 1 H H6C 0.5486 0.6469 0.964 0.043 Uiso calc U R 1 C C7 0.4976(4) 0.74808(19) 0.87335(15) 0.0282(8) Uani d . . 1 H H7A 0.4539 0.7951 0.8591 0.042 Uiso calc U R 1 H H7B 0.5203 0.7176 0.8351 0.042 Uiso calc U R 1 H H7C 0.5939 0.7569 0.8978 0.042 Uiso calc U R 1 C C8 -0.0841(4) 0.57852(16) 0.84471(15) 0.0193(6) Uani d . . 1 H H8 -0.0642 0.543 0.8776 0.023 Uiso calc U R 1 C C9 -0.2193(4) 0.57457(17) 0.80895(15) 0.0207(7) Uani d . . 1 H H9 -0.2941 0.5379 0.8188 0.025 Uiso calc U R 1 C C10 -0.2475(4) 0.62408(16) 0.75822(14) 0.0175(6) Uani d . . 1 H H10 -0.341 0.6216 0.7336 0.021 Uiso calc U R 1 C C11 -0.1355(4) 0.67699(14) 0.74462(13) 0.0139(5) Uani d . . 1 C C12 -0.1533(3) 0.73686(16) 0.69358(13) 0.0128(5) Uani d . . 1 H H12 -0.2327 0.7235 0.66 0.015 Uiso calc U R 1 C C13 0.0468(4) 0.71018(16) 0.60491(14) 0.0159(6) Uani d . . 1 C C14 -0.0536(4) 0.73098(18) 0.54623(13) 0.0233(7) Uani d . . 1 H H14A -0.0417 0.7835 0.5371 0.035 Uiso calc U R 1 H H14B -0.1628 0.7202 0.5559 0.035 Uiso calc U R 1 H H14C -0.0205 0.7026 0.5081 0.035 Uiso calc U R 1 C C15 0.0313(4) 0.62783(16) 0.61882(14) 0.0242(7) Uani d . . 1 H H15A -0.0779 0.6159 0.6275 0.036 Uiso calc U R 1 H H15B 0.0944 0.615 0.657 0.036 Uiso calc U R 1 H H15C 0.0676 0.5999 0.5809 0.036 Uiso calc U R 1 C C16 0.2165(4) 0.7272(2) 0.58940(17) 0.0261(8) Uani d . . 1 H H16A 0.2812 0.7155 0.6274 0.039 Uiso calc U R 1 H H16B 0.2272 0.7794 0.5788 0.039 Uiso calc U R 1 H H16C 0.2502 0.6976 0.552 0.039 Uiso calc U R 1 C C17 -0.1990(4) 0.80860(15) 0.73066(14) 0.0131(6) Uani d . . 1 H H17 -0.2619 0.7976 0.7705 0.016 Uiso calc U R 1 C C18 -0.2886(4) 0.85568(15) 0.68296(14) 0.0137(6) Uani d . . 1 C C19 -0.4494(3) 0.86201(17) 0.68201(14) 0.0178(6) Uani d . . 1 H H19 -0.5106 0.8395 0.715 0.021 Uiso calc U R 1 C C20 -0.5199(4) 0.90167(17) 0.63211(15) 0.0212(7) Uani d . . 1 H H20 -0.6298 0.9072 0.6314 0.025 Uiso calc U R 1 C C21 -0.4295(4) 0.93309(16) 0.58341(15) 0.0177(7) Uani d . . 1 H H21 -0.4781 0.9605 0.5496 0.021 Uiso calc U R 1 C C22 -0.2686(4) 0.92493(16) 0.58353(14) 0.0135(6) Uani d . . 1 C C23 -0.1961(4) 0.88658(15) 0.63425(13) 0.0133(6) Uani d . . 1 C C24 -0.1772(4) 0.95657(16) 0.52925(14) 0.0136(6) Uani d . . 1 H H24 -0.2265 0.9903 0.5005 0.016 Uiso calc U R 1 C C25 0.0527(4) 0.97329(17) 0.46505(14) 0.0177(6) Uani d . . 1 C C26 0.0471(5) 0.9191(2) 0.40865(17) 0.0378(10) Uani d . . 1 H H26A -0.061 0.9125 0.3946 0.057 Uiso calc U R 1 H H26B 0.0896 0.8718 0.4228 0.057 Uiso calc U R 1 H H26C 0.1089 0.9381 0.3722 0.057 Uiso calc U R 1 C C27 0.2188(4) 0.9803(2) 0.48959(17) 0.0327(9) Uani d . . 1 H H27A 0.2542 0.9328 0.5064 0.049 Uiso calc U R 1 H H27B 0.223 1.0169 0.5246 0.049 Uiso calc U R 1 H H27C 0.2865 0.9957 0.4536 0.049 Uiso calc U R 1 C C28 -0.0075(5) 1.0478(2) 0.44278(19) 0.0405(10) Uani d . . 1 H H28A -0.0198 1.08 0.4807 0.061 Uiso calc U R 1 H H28B -0.1082 1.0416 0.4211 0.061 Uiso calc U R 1 H H28C 0.0669 1.0697 0.4122 0.061 Uiso calc U R 1 C C29 -0.0475(4) 0.89487(16) 0.80401(14) 0.0188(7) Uani d . . 1 C C30 -0.0786(5) 0.85338(19) 0.86761(14) 0.0270(8) Uani d . . 1 H H30A -0.0009 0.8145 0.8729 0.041 Uiso calc U R 1 H H30B -0.1827 0.8316 0.8661 0.041 Uiso calc U R 1 H H30C -0.072 0.8875 0.9045 0.041 Uiso calc U R 1 C C31 -0.1702(5) 0.95451(19) 0.79459(17) 0.0319(9) Uani d . . 1 H H31A -0.2729 0.9318 0.79 0.048 Uiso calc U R 1 H H31B -0.1461 0.9828 0.7552 0.048 Uiso calc U R 1 H H31C -0.1703 0.9872 0.8326 0.048 Uiso calc U R 1 C C32 0.1133(5) 0.92998(19) 0.80861(16) 0.0285(8) Uani d . . 1 H H32A 0.1373 0.9551 0.7675 0.043 Uiso calc U R 1 H H32B 0.1913 0.8919 0.8168 0.043 Uiso calc U R 1 H H32C 0.1145 0.9655 0.8445 0.043 Uiso calc U R 1 N N1 -0.0008(3) 0.75488(12) 0.66309(10) 0.0124(5) Uani d . . 1 N N2 -0.0464(3) 0.84231(12) 0.74784(12) 0.0134(5) Uani d . . 1 N N3 0.2369(3) 0.70109(14) 0.87805(12) 0.0187(6) Uani d . . 1 N N4 -0.0370(3) 0.94054(13) 0.51970(11) 0.0159(5) Uani d . . 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Ge1 0.01282(15) 0.01758(14) 0.01336(13) -0.00316(13) -0.00058(13) 0.00397(13) Ge2 0.00913(13) 0.01391(13) 0.01220(12) -0.00169(13) 0.00118(12) 0.00184(12) C1 0.0186(19) 0.0145(13) 0.0127(12) -0.0035(12) 0.0016(12) 0.0006(10) C2 0.0229(15) 0.0164(13) 0.0129(12) -0.0001(14) 0.0026(12) 0.0019(11) C3 0.0244(18) 0.0195(15) 0.0130(12) 0.0026(13) 0.0009(12) 0.0055(12) C4 0.0198(18) 0.0213(15) 0.0183(14) -0.0018(14) -0.0027(13) 0.0026(12) C5 0.031(2) 0.036(2) 0.0201(14) -0.0026(17) 0.0004(15) -0.0049(15) C6 0.026(2) 0.0299(17) 0.0299(16) -0.0010(17) -0.0074(15) 0.0055(15) C7 0.024(2) 0.0367(19) 0.0241(15) -0.0062(16) 0.0028(14) 0.0038(14) C8 0.0297(18) 0.0151(13) 0.0130(12) -0.0011(12) 0.0041(14) 0.0025(12) C9 0.027(2) 0.0164(15) 0.0187(15) -0.0098(14) 0.0064(14) -0.0009(12) C10 0.0197(15) 0.0174(14) 0.0154(13) -0.0022(12) 0.0019(12) -0.0021(12) C11 0.0174(14) 0.0127(12) 0.0116(12) 0.0009(11) 0.0033(13) -0.0002(11) C12 0.0117(15) 0.0138(12) 0.0128(11) -0.0033(12) 0.0013(11) -0.0012(11) C13 0.0200(18) 0.0158(13) 0.0120(12) 0.0027(13) 0.0017(12) -0.0011(10) C14 0.033(2) 0.0238(16) 0.0131(13) 0.0046(16) 0.0005(13) -0.0010(12) C15 0.0362(19) 0.0153(13) 0.0210(13) 0.0036(17) 0.0049(15) -0.0023(12) C16 0.0243(19) 0.0290(18) 0.0250(16) 0.0034(16) 0.0105(14) -0.0044(15) C17 0.0122(15) 0.0133(13) 0.0137(12) -0.0024(12) 0.0022(11) -0.0012(10) C18 0.0116(15) 0.0127(14) 0.0168(13) -0.0019(11) 0.0013(11) -0.0038(11) C19 0.0112(16) 0.0194(15) 0.0230(14) -0.0041(13) 0.0046(12) -0.0020(12) C20 0.0083(14) 0.0216(15) 0.0336(16) 0.0019(13) 0.0034(14) -0.0046(13) C21 0.0147(17) 0.0153(14) 0.0233(15) 0.0000(12) -0.0026(13) 0.0002(12) C22 0.0115(15) 0.0111(13) 0.0180(14) -0.0028(11) 0.0013(12) -0.0026(11) C23 0.0120(14) 0.0135(14) 0.0146(13) -0.0020(11) 0.0026(11) -0.0022(10) C24 0.0123(16) 0.0132(13) 0.0154(13) 0.0011(11) -0.0037(12) -0.0010(11) C25 0.0158(17) 0.0241(15) 0.0130(12) 0.0009(13) 0.0009(12) 0.0034(12) C26 0.041(3) 0.047(2) 0.0257(17) -0.015(2) 0.0135(18) -0.0097(16) C27 0.020(2) 0.058(3) 0.0195(16) -0.0096(18) 0.0032(14) 0.0014(17) C28 0.040(3) 0.039(2) 0.043(2) 0.0054(19) 0.015(2) 0.0256(18) C29 0.0261(19) 0.0187(14) 0.0114(12) -0.0055(14) 0.0011(13) -0.0037(11) C30 0.039(2) 0.0284(18) 0.0137(13) -0.0099(16) 0.0018(14) -0.0025(13) C31 0.048(3) 0.0195(17) 0.0283(18) 0.0021(17) -0.0034(18) -0.0111(14) C32 0.034(2) 0.0293(19) 0.0216(16) -0.0164(17) 0.0010(16) -0.0075(14) N1 0.0117(13) 0.0148(11) 0.0107(9) -0.0009(9) 0.0038(9) 0.0004(8) N2 0.0131(12) 0.0147(10) 0.0126(10) -0.0052(9) 0.0024(11) -0.0013(10) N3 0.0201(15) 0.0204(14) 0.0156(12) -0.0022(11) 0.0000(11) 0.0027(10) N4 0.0137(13) 0.0197(12) 0.0142(11) -0.0001(11) 0.0006(11) 0.0022(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C1 Ge1 N1 85.00(10) C1 Ge1 N2 93.37(11) N1 Ge1 N2 69.17(9) C1 Ge1 Ge2 122.68(9) N1 Ge1 Ge2 47.43(6) N2 Ge1 Ge2 46.32(6) C23 Ge2 N2 85.96(11) C23 Ge2 N1 93.14(10) N2 Ge2 N1 69.33(8) C23 Ge2 Ge1 123.31(8) N2 Ge2 Ge1 47.64(6) N1 Ge2 Ge1 46.36(6) C11 C1 C2 119.1(3) C11 C1 Ge1 111.0(2) C2 C1 Ge1 129.7(2) C8 C2 C1 119.0(3) C8 C2 C3 120.5(3) C1 C2 C3 120.4(3) N3 C3 C2 120.8(3) N3 C4 C6 115.4(3) N3 C4 C5 106.2(3) C6 C4 C5 110.0(3) N3 C4 C7 105.9(2) C6 C4 C7 109.5(3) C5 C4 C7 109.7(3) C9 C8 C2 120.7(3) C8 C9 C10 120.6(3) C11 C10 C9 118.4(3) C1 C11 C10 121.9(3) C1 C11 C12 113.4(2) C10 C11 C12 124.5(3) N1 C12 C11 111.0(2) N1 C12 C17 103.9(2) C11 C12 C17 107.0(2) N1 C13 C16 108.4(3) N1 C13 C14 109.7(2) C16 C13 C14 109.0(3) N1 C13 C15 111.1(2) C16 C13 C15 108.7(3) C14 C13 C15 109.9(3) N2 C17 C18 111.5(2) N2 C17 C12 103.8(2) C18 C17 C12 106.8(2) C19 C18 C23 121.6(3) C19 C18 C17 124.3(3) C23 C18 C17 113.7(3) C18 C19 C20 119.2(3) C21 C20 C19 119.9(3) C20 C21 C22 120.7(3) C21 C22 C23 119.8(3) C21 C22 C24 119.0(3) C23 C22 C24 121.1(3) C18 C23 C22 118.7(3) C18 C23 Ge2 110.0(2) C22 C23 Ge2 131.3(2) N4 C24 C22 122.4(3) N4 C25 C27 105.8(2) N4 C25 C26 107.2(3) C27 C25 C26 109.6(3) N4 C25 C28 114.1(3) C27 C25 C28 110.1(3) C26 C25 C28 109.9(3) N2 C29 C32 108.1(3) N2 C29 C31 111.3(3) C32 C29 C31 109.6(3) N2 C29 C30 109.9(2) C32 C29 C30 108.2(3) C31 C29 C30 109.8(3) C12 N1 C13 117.0(2) C12 N1 Ge1 99.36(15) C13 N1 Ge1 122.77(18) C12 N1 Ge2 110.89(17) C13 N1 Ge2 116.00(16) Ge1 N1 Ge2 86.20(8) C17 N2 C29 116.1(2) C17 N2 Ge2 98.82(17) C29 N2 Ge2 123.67(17) C17 N2 Ge1 111.28(16) C29 N2 Ge1 116.49(19) Ge2 N2 Ge1 86.04(9) C3 N3 C4 121.8(3) C24 N4 C25 121.5(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Ge1 C1 1.991(3) Ge1 N1 2.082(2) Ge1 N2 2.127(2) Ge1 Ge2 2.8710(4) Ge2 C23 1.995(3) Ge2 N2 2.081(2) Ge2 N1 2.119(2) C1 C11 1.385(4) C1 C2 1.406(4) C2 C8 1.402(4) C2 C3 1.468(4) C3 N3 1.265(4) C4 N3 1.477(4) C4 C6 1.522(5) C4 C5 1.528(4) C4 C7 1.533(4) C8 C9 1.376(5) C9 C10 1.398(4) C10 C11 1.391(4) C11 C12 1.519(4) C12 N1 1.489(4) C12 C17 1.562(4) C13 N1 1.501(3) C13 C16 1.526(5) C13 C14 1.528(4) C13 C15 1.533(4) C17 N2 1.490(4) C17 C18 1.512(4) C18 C19 1.388(4) C18 C23 1.395(4) C19 C20 1.392(4) C20 C21 1.389(4) C21 C22 1.392(4) C22 C23 1.399(4) C22 C24 1.479(4) C24 N4 1.256(4) C25 N4 1.485(4) C25 C27 1.520(5) C25 C26 1.521(4) C25 C28 1.523(5) C29 N2 1.498(4) C29 C32 1.527(5) C29 C31 1.527(5) C29 C30 1.530(4)