Crystallography Open Database

Information card for entry 4105666

Preview

Coordinates	4105666.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	(tpaMes)V(N2O)
Formula	C42 H45 N6 O V
Calculated formula	C42 H45 N6 O V
Title of publication	A Structurally Characterized Nitrous Oxide Complex of Vanadium
Authors of publication	Nicholas A. Piro; Michael F. Lichterman; W. Hill Harman; Christopher J. Chang
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	2108 - 2111
a	10.4388 ± 0.0007 Å
b	10.4441 ± 0.0007 Å
c	19.1656 ± 0.0014 Å
α	83.921 ± 0.004°
β	79.928 ± 0.004°
γ	62.462 ± 0.003°
Cell volume	1823.5 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0627
Residual factor for significantly intense reflections	0.0473
Weighted residual factors for significantly intense reflections	0.129
Weighted residual factors for all reflections included in the refinement	0.1378
Goodness-of-fit parameter for all reflections included in the refinement	1.085
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178802 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/56.	4105666.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4105666.cif
52427	2012-04-11	../uploads/cif-deposit/cod/cif Adding structures of 4105666 via cif-deposit CGI script.	4105666.cif