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Information card for entry 4112096
Preview
| Coordinates | 4112096.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | Dipp*Ge(CHSiMe3)(n2CHSiMe3)2GeDipp*.n-hexane |
|---|---|
| Formula | C78 H118 Ge2 N4 Si3 |
| Calculated formula | C78 H118 Ge2 N4 Si3 |
| Title of publication | Reactions of the Heavier Group 14 Element Alkyne Analogues Ar'EEAr' (Ar' = C6H3-2,6(C6H3-2,6-Pri2)2; E = Ge, Sn) with Unsaturated Molecules: Probing the Character of the EE Multiple Bonds |
| Authors of publication | Chunming Cui; Marilyn M. Olmstead; James C. Fettinger; Geoffrey H. Spikes; Philip P. Power |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2005 |
| Journal volume | 127 |
| Pages of publication | 17530 - 17541 |
| a | 12.8515 ± 0.0009 Å |
| b | 14.9117 ± 0.0011 Å |
| c | 20.4565 ± 0.0015 Å |
| α | 80.746 ± 0.003° |
| β | 80.117 ± 0.003° |
| γ | 83.322 ± 0.004° |
| Cell volume | 3795.9 ± 0.5 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0514 |
| Residual factor for significantly intense reflections | 0.0356 |
| Weighted residual factors for significantly intense reflections | 0.0853 |
| Weighted residual factors for all reflections included in the refinement | 0.0937 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178891 (current) | 2016-03-22 | cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/20. |
4112096.cif |
| 120077 | 2014-07-12 | Adding DOIs to range 4/11 structures. | 4112096.cif |
| 63716 | 2012-08-06 | cif/ Adding structures of 4112096 via cif-deposit CGI script. |
4112096.cif |
All data in the COD and the database itself are dedicated to the
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Users of the data should acknowledge the original authors of the
structural data.